#------------------------------------------------------------------------------ #$Date: 2011-09-16 16:46:08 +0100 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: svn://www.crystallography.net/cod/hkl/2/2011172.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011172_Fobs loop_ _publ_author_name 'Amspacher, David R.' 'Blanchard, Carol Z.' 'Saraiva, Marcelo C.' 'Waldrop, Grover L.' 'Strongin, Robert M.' 'Fronczek, Frank R.' _publ_section_title ; Benzyl 5-{2-[2-(diethoxyphosphinoyl)acetyl]-3-oxo-7-thia-2,4-diazabicyclo[3.3.0]oct-6-yl}pentanoate, a novel biotin derivative ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e305 _journal_page_last e306 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.077 _cell_angle_gamma 90.000 _cell_length_a 10.4550 _cell_length_b 12.4100 _cell_length_c 10.5920 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.7110 _[local]_cod_data_source_file qa0325Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Amspacher5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -13 0 5.07 -15.52 15.52 o 2 -13 0 256.06 240.72 20.37 o 0 -12 0 988.12 924.12 28.96 o 1 -12 0 63.35 76.21 10.11 o 2 -12 0 449.48 475.73 21.90 o 3 -12 0 276.58 308.89 19.46 o 4 -12 0 355.40 330.06 21.05 o 1 -11 0 459.08 448.06 20.71 o 2 -11 0 334.48 327.72 20.04 o 3 -11 0 350.57 348.56 19.71 o 4 -11 0 827.20 781.37 27.35 o 5 -11 0 122.97 127.50 11.06 o 0 -10 0 674.56 687.90 22.96 o 1 -10 0 101.22 113.38 12.07 o 2 -10 0 67.76 73.97 9.30 o 3 -10 0 219.53 250.40 16.30 o 4 -10 0 628.19 646.00 23.56 o 5 -10 0 2.80 16.13 8.07 o 6 -10 0 24.78 18.72 9.47 o 1 -9 0 174.78 190.52 14.57 o 2 -9 0 436.07 472.93 18.48 o 3 -9 0 191.49 181.38 15.25 o 4 -9 0 1071.21 1109.51 28.30 o 5 -9 0 413.10 397.26 20.01 o 6 -9 0 262.38 273.33 18.30 o 7 -9 0 316.63 280.60 19.41 o 0 -8 0 857.16 974.10 21.70 o 1 -8 0 1691.27 1792.26 29.44 o 2 -8 0 1076.60 1133.65 25.15 o 3 -8 0 123.13 133.09 10.69 o 4 -8 0 206.56 202.78 15.40 o 5 -8 0 445.22 428.66 19.73 o 6 -8 0 198.19 173.49 15.60 o 7 -8 0 137.81 123.18 12.00 o 8 -8 0 107.56 101.64 11.16 o 1 -7 0 870.56 920.21 20.31 o 2 -7 0 96.40 105.84 8.47 o 3 -7 0 1469.66 1580.85 27.65 o 4 -7 0 313.03 312.98 15.48 o 5 -7 0 725.61 726.92 22.21 o 6 -7 0 346.99 342.34 17.62 o 7 -7 0 10.58 7.38 7.84 o 8 -7 0 6.85 -2.88 6.22 o 0 -6 0 3045.47 3384.00 32.96 o 1 -6 0 531.90 595.32 15.09 o 2 -6 0 9.01 17.84 5.98 o 3 -6 0 921.20 1039.45 20.76 o 4 -6 0 377.34 382.53 15.10 o 5 -6 0 396.70 389.60 16.78 o 6 -6 0 253.89 239.12 15.14 o 7 -6 0 685.03 618.80 23.06 o 8 -6 0 310.85 330.52 19.20 o 9 -6 0 47.49 52.55 9.90 o 1 -5 0 962.41 1085.63 17.82 o 2 -5 0 950.84 1062.00 18.47 o 3 -5 0 227.48 221.15 11.11 o 4 -5 0 426.40 394.69 14.32 o 5 -5 0 20.70 28.70 6.90 o 6 -5 0 1020.83 947.76 23.79 o 7 -5 0 160.17 155.02 14.75 o 8 -5 0 33.88 23.69 8.77 o 9 -5 0 42.35 38.51 9.91 o 0 -4 0 3439.21 3640.35 27.97 o 1 -4 0 836.93 853.51 15.05 o 2 -4 0 615.60 665.12 14.61 o 3 -4 0 607.78 611.14 14.64 o 4 -4 0 338.24 355.80 13.59 o 5 -4 0 359.49 376.49 14.99 o 6 -4 0 1553.92 1517.01 28.08 o 7 -4 0 79.30 51.43 9.23 o 8 -4 0 65.31 72.65 9.00 o 9 -4 0 488.16 508.29 23.23 o 1 -3 0 1021.69 1107.79 14.57 o 2 -3 0 983.80 1016.34 15.60 o 3 -3 0 576.29 603.53 13.93 o 4 -3 0 1863.85 1933.39 24.92 o 5 -3 0 190.55 188.74 11.67 o 6 -3 0 384.88 354.84 16.01 o 7 -3 0 105.64 106.90 10.91 o 8 -3 0 251.47 250.81 17.54 o 9 -3 0 27.03 25.22 9.32 o 0 -2 0 6282.55 6646.91 25.20 o 1 -2 0 838.00 891.54 11.54 o 2 -2 0 3065.43 3031.20 22.68 o 3 -2 0 1089.57 1056.13 16.74 o 4 -2 0 677.30 709.68 15.78 o 5 -2 0 1930.21 1895.09 26.91 o 6 -2 0 1548.02 1498.01 26.91 o 7 -2 0 28.30 12.63 8.24 o 8 -2 0 138.89 161.82 15.07 o 9 -2 0 266.05 286.24 19.16 o 10 -2 0 24.63 16.35 9.37 o 1 -1 0 487.26 483.06 7.36 o 2 -1 0 7506.36 6867.05 29.87 o 3 -1 0 2174.43 1967.50 20.56 o 4 -1 0 4686.04 4444.90 34.33 o 5 -1 0 694.25 626.51 16.76 o 6 -1 0 339.31 340.91 14.74 o 7 -1 0 107.23 93.00 9.93 o 8 -1 0 616.90 594.06 21.97 o 9 -1 0 34.41 32.68 8.99 o 10 -1 0 125.04 135.48 11.09 o 2 0 0 4271.02 3886.77 19.26 o 3 0 0 4494.42 4108.17 23.11 o 4 0 0 479.74 517.04 11.12 o 5 0 0 549.51 588.44 12.50 o 6 0 0 48.27 56.35 7.34 o 7 0 0 794.66 779.94 17.99 o 8 0 0 241.55 250.81 13.86 o 9 0 0 2.91 -2.19 4.66 o 10 0 0 101.57 103.20 11.77 o 11 0 0 19.81 4.34 6.93 o 12 0 0 45.22 52.55 12.50 o 13 0 0 8.06 6.70 9.13 o 1 1 0 501.67 471.25 6.15 o 2 1 0 7439.29 6550.69 25.02 o 3 1 0 2192.61 1926.61 16.96 o 4 1 0 4712.05 4481.03 29.31 o 5 1 0 688.89 633.62 13.61 o 6 1 0 345.08 338.53 12.32 o 7 1 0 107.16 132.49 10.38 o 8 1 0 615.23 630.39 18.75 o 9 1 0 34.72 27.06 9.25 o 10 1 0 124.36 117.54 12.28 o 11 1 0 136.08 163.79 15.15 o 12 1 0 37.88 63.73 11.72 o 13 1 0 85.27 121.19 15.02 o 0 2 0 6276.15 6426.23 20.64 o 1 2 0 859.89 767.04 9.27 o 2 2 0 3054.37 2743.46 17.54 o 3 2 0 1082.97 1010.61 13.10 o 4 2 0 689.77 731.80 13.23 o 5 2 0 1933.61 1900.69 22.45 o 6 2 0 1517.48 1420.31 22.31 o 7 2 0 30.62 36.77 8.75 o 8 2 0 139.10 151.19 12.67 o 9 2 0 269.80 265.72 15.95 o 10 2 0 23.01 21.00 10.03 o 11 2 0 46.13 42.11 11.87 o 12 2 0 34.78 49.78 11.99 o 13 2 0 40.13 27.74 13.01 o 1 3 0 1025.84 1090.71 11.90 o 2 3 0 943.54 846.00 12.73 o 3 3 0 567.03 543.72 11.41 o 4 3 0 1864.99 1835.03 19.86 o 5 3 0 188.93 178.61 9.98 o 6 3 0 385.97 407.08 14.03 o 7 3 0 105.95 117.54 9.76 o 8 3 0 260.80 255.74 14.41 o 9 3 0 25.05 41.11 8.92 o 10 3 0 1.73 -11.64 11.64 o 11 3 0 7.78 -7.24 9.50 o 12 3 0 60.49 84.04 13.46 o 13 3 0 24.00 2.30 6.61 o 0 4 0 3410.16 3471.45 21.24 o 1 4 0 839.24 844.49 12.72 o 2 4 0 617.70 568.62 11.67 o 3 4 0 609.75 535.34 11.92 o 4 4 0 349.06 363.13 11.29 o 5 4 0 355.16 339.49 12.33 o 6 4 0 1528.18 1485.08 23.82 o 7 4 0 78.13 73.76 9.28 o 8 4 0 66.96 60.28 9.40 o 9 4 0 475.25 464.57 18.87 o 10 4 0 68.12 79.39 11.47 o 11 4 0 61.27 72.00 12.23 o 12 4 0 3.01 -4.14 8.27 o 1 5 0 932.84 994.30 14.62 o 2 5 0 950.18 1016.34 15.60 o 3 5 0 219.42 170.46 9.75 o 4 5 0 426.01 339.95 12.35 o 5 5 0 21.96 14.22 7.78 o 6 5 0 1026.83 945.37 20.59 o 7 5 0 160.26 150.25 12.63 o 8 5 0 31.97 16.56 9.63 o 9 5 0 42.92 49.42 10.15 o 10 5 0 91.40 100.60 11.89 o 11 5 0 129.75 116.98 14.49 o 12 5 0 2.34 6.96 9.10 o 0 6 0 2984.18 3197.89 26.21 o 1 6 0 533.75 571.07 12.30 o 2 6 0 9.84 -0.48 1.82 o 3 6 0 914.90 889.24 16.89 o 4 6 0 387.24 348.08 13.44 o 5 6 0 400.32 364.11 14.74 o 6 6 0 248.26 239.12 13.94 o 7 6 0 694.84 630.39 20.04 o 8 6 0 313.62 318.93 17.01 o 9 6 0 47.57 32.53 10.58 o 10 6 0 216.36 211.31 16.84 o 11 6 0 14.37 1.97 5.79 o 12 6 0 6.00 -2.19 6.45 o 1 7 0 879.13 893.07 16.93 o 2 7 0 105.11 111.74 10.34 o 3 7 0 1479.39 1590.08 23.62 o 4 7 0 310.10 244.73 13.69 o 5 7 0 738.39 696.02 19.02 o 6 7 0 349.40 327.25 15.83 o 7 7 0 10.10 8.69 9.12 o 8 7 0 5.99 13.46 9.83 o 9 7 0 23.93 29.38 11.02 o 10 7 0 103.33 92.26 13.86 o 11 7 0 153.69 170.46 18.83 o 12 7 0 234.70 258.62 21.95 o 0 8 0 854.90 897.69 17.74 o 1 8 0 1701.21 1696.55 23.34 o 2 8 0 1096.77 1171.25 21.15 o 3 8 0 118.32 135.48 11.09 o 4 8 0 199.98 211.31 14.22 o 5 8 0 443.40 415.43 17.84 o 6 8 0 210.11 175.88 14.69 o 7 8 0 136.67 99.83 12.09 o 8 8 0 108.47 87.62 12.05 o 9 8 0 194.09 218.10 17.49 o 10 8 0 72.66 66.21 13.63 o 11 8 0 46.30 30.37 13.76 o 1 9 0 171.93 176.56 11.97 o 2 9 0 446.14 459.58 16.01 o 3 9 0 185.87 183.82 13.96 o 4 9 0 1080.96 1144.96 24.40 o 5 9 0 421.63 359.70 17.09 o 6 9 0 263.90 237.53 16.28 o 7 9 0 313.39 252.85 17.61 o 8 9 0 47.58 51.99 11.70 o 9 9 0 62.57 73.09 12.55 o 10 9 0 4.84 2.01 6.05 o 11 9 0 7.41 20.08 12.47 o 0 10 0 673.53 700.78 18.40 o 1 10 0 101.73 104.00 10.76 o 2 10 0 69.99 75.98 10.99 o 3 10 0 208.68 241.11 14.79 o 4 10 0 625.06 621.37 20.54 o 5 10 0 3.25 -14.42 14.42 o 6 10 0 26.49 21.72 11.77 o 7 10 0 15.28 8.47 9.75 o 8 10 0 198.00 190.87 15.30 o 9 10 0 10.01 0.96 3.45 o 10 10 0 22.96 9.63 13.99 o 1 11 0 461.73 458.49 17.64 o 2 11 0 335.96 350.00 16.38 o 3 11 0 341.20 367.56 17.27 o 4 11 0 823.61 783.54 23.79 o 5 11 0 125.07 118.09 13.99 o 6 11 0 235.31 198.77 18.15 o 7 11 0 66.88 56.73 13.20 o 8 11 0 220.10 217.34 16.33 o 9 11 0 22.00 13.94 13.94 o 10 11 0 28.24 16.88 14.17 o 0 12 0 987.02 916.31 23.39 o 1 12 0 62.28 72.21 10.94 o 2 12 0 442.78 455.17 18.68 o 3 12 0 278.24 291.49 17.59 o 4 12 0 360.54 416.48 19.98 o 5 12 0 58.55 70.26 13.38 o 6 12 0 35.94 3.93 7.41 o 7 12 0 288.64 257.38 20.66 o 8 12 0 125.65 113.66 16.20 o 9 12 0 12.03 0.00 1.66 o 1 13 0 4.32 -11.82 11.82 o 2 13 0 250.28 274.17 17.49 o 3 13 0 259.82 304.82 18.43 o 4 13 0 94.64 73.09 14.09 o 5 13 0 345.00 383.52 21.68 o 6 13 0 33.86 24.57 14.94 o 7 13 0 43.85 6.56 10.03 o 8 13 0 111.53 102.16 17.18 o 0 14 0 66.65 46.04 12.23 o 1 14 0 75.65 79.39 12.38 o 2 14 0 6.39 1.72 4.77 o 3 14 0 8.86 -14.32 14.32 o 4 14 0 9.57 -11.04 13.51 o 5 14 0 11.27 1.94 6.08 o 6 14 0 29.66 48.16 15.55 o 7 14 0 2.41 -23.61 23.61 o 1 15 0 53.40 71.12 12.60 o 2 15 0 212.77 255.74 18.53 o 3 15 0 20.50 -3.88 7.31 o 4 15 0 31.64 45.87 13.96 o 5 15 0 26.56 18.93 15.58 o 6 15 0 65.54 91.51 16.99 o 0 16 0 126.06 113.93 15.38 o 1 16 0 13.61 8.17 12.43 o 2 16 0 17.23 1.56 4.66 o 3 16 0 147.39 152.78 16.23 o 4 16 0 18.62 -5.49 10.86 o 5 16 0 49.43 60.08 16.76 o 1 17 0 62.61 87.38 14.69 o 2 17 0 25.22 39.64 14.59 o -2 -13 1 17.33 2.30 5.67 o -1 -13 1 172.76 182.08 17.37 o 0 -13 1 38.70 40.68 7.41 o 1 -13 1 14.04 -20.76 20.76 o -4 -12 1 21.39 9.71 10.03 o -3 -12 1 289.68 306.18 19.83 o -2 -12 1 154.29 155.34 13.79 o -1 -12 1 33.46 34.17 9.48 o 0 -12 1 112.61 127.06 8.70 o 1 -12 1 233.59 260.28 17.87 o 2 -12 1 109.94 113.66 12.63 o 3 -12 1 208.67 194.08 17.94 o -6 -11 1 127.32 131.02 12.09 o -5 -11 1 57.23 54.05 10.41 o -4 -11 1 203.64 191.23 16.74 o -3 -11 1 28.69 24.19 8.49 o -2 -11 1 1178.73 1194.28 30.26 o -1 -11 1 171.63 171.80 15.87 o 0 -11 1 98.71 106.27 7.31 o 1 -11 1 526.52 487.60 22.18 o 2 -11 1 267.87 275.02 17.94 o 3 -11 1 1.50 -6.70 9.07 o 4 -11 1 11.12 3.93 5.92 o 5 -11 1 141.11 126.06 13.30 o -7 -10 1 107.13 101.13 11.14 o -6 -10 1 1223.53 1226.52 33.37 o -5 -10 1 134.98 125.76 12.42 o -4 -10 1 407.88 420.69 20.61 o -3 -10 1 170.09 156.63 12.57 o -2 -10 1 130.39 113.38 12.07 o -1 -10 1 138.75 143.39 11.72 o 0 -10 1 72.96 59.02 6.75 o 1 -10 1 955.45 917.87 25.75 o 2 -10 1 413.41 459.03 19.86 o 3 -10 1 201.59 214.32 16.21 o 4 -10 1 89.11 94.99 10.05 o 5 -10 1 24.86 -0.70 3.17 o 6 -10 1 134.74 177.25 15.43 o -7 -9 1 3.82 -12.17 12.77 o -6 -9 1 95.05 82.16 9.80 o -5 -9 1 86.10 87.38 10.59 o -4 -9 1 285.42 299.45 16.50 o -3 -9 1 171.30 171.14 14.49 o -2 -9 1 778.46 783.54 22.35 o -1 -9 1 310.88 311.60 16.36 o 0 -9 1 179.87 190.45 10.43 o 1 -9 1 1790.91 1889.49 32.46 o 2 -9 1 23.33 12.72 8.54 o 3 -9 1 710.62 702.15 22.51 o 4 -9 1 594.23 549.73 21.73 o 5 -9 1 196.88 197.70 15.57 o 6 -9 1 291.89 287.12 19.20 o 7 -9 1 95.81 91.28 11.80 o -8 -8 1 2.89 -3.35 5.50 o -7 -8 1 665.95 639.47 24.75 o -6 -8 1 103.43 96.25 9.60 o -5 -8 1 295.93 281.90 16.86 o -4 -8 1 712.59 678.46 20.79 o -3 -8 1 204.40 225.00 15.07 o -2 -8 1 338.63 358.72 16.10 o -1 -8 1 70.18 65.17 7.91 o 0 -8 1 941.37 990.23 16.05 o 1 -8 1 923.70 984.58 22.63 o 2 -8 1 284.26 278.02 14.61 o 3 -8 1 342.28 335.23 16.50 o 4 -8 1 110.69 115.58 11.36 o 5 -8 1 206.39 237.93 15.88 o 6 -8 1 6.54 -3.25 6.32 o 7 -8 1 146.09 142.46 12.91 o -9 -7 1 163.25 184.52 11.89 o -8 -7 1 284.77 288.43 17.94 o -7 -7 1 24.44 19.73 8.36 o -6 -7 1 688.68 670.44 22.66 o -5 -7 1 752.33 713.79 22.71 o -4 -7 1 9.98 21.12 6.52 o -3 -7 1 83.81 106.37 10.36 o -2 -7 1 999.49 1013.87 21.32 o -1 -7 1 2586.91 2762.38 32.48 o 0 -7 1 664.69 721.68 12.96 o 1 -7 1 395.56 393.17 14.80 o 2 -7 1 452.32 445.34 15.77 o 3 -7 1 93.22 109.85 9.45 o 4 -7 1 172.46 188.74 14.16 o 5 -7 1 94.26 105.57 8.74 o 6 -7 1 92.76 87.86 10.86 o 7 -7 1 309.30 267.80 18.53 o 8 -7 1 95.65 93.25 10.94 o -9 -6 1 49.09 60.88 9.65 o -8 -6 1 19.05 4.58 7.54 o -7 -6 1 99.42 94.99 9.78 o -6 -6 1 361.06 342.34 16.68 o -5 -6 1 333.18 322.61 15.73 o -4 -6 1 317.62 324.47 14.37 o -3 -6 1 722.43 729.01 18.07 o -2 -6 1 46.49 37.88 5.87 o -1 -6 1 315.29 350.48 13.01 o 0 -6 1 2327.16 2555.93 20.26 o 1 -6 1 931.07 935.11 18.90 o 2 -6 1 700.41 767.04 17.84 o 3 -6 1 249.20 233.59 13.38 o 4 -6 1 682.78 632.33 19.43 o 5 -6 1 89.57 83.11 8.69 o 6 -6 1 93.87 98.54 10.74 o 7 -6 1 498.63 433.47 21.45 o 8 -6 1 0.58 10.53 8.69 o -9 -5 1 223.57 212.81 17.66 o -8 -5 1 437.30 434.55 20.39 o -7 -5 1 699.96 671.10 22.68 o -6 -5 1 426.71 452.98 18.09 o -5 -5 1 767.04 764.19 19.93 o -4 -5 1 253.05 284.50 12.60 o -3 -5 1 776.30 842.26 17.94 o -2 -5 1 1387.50 1404.82 21.24 o -1 -5 1 223.04 247.15 10.53 o 0 -5 1 761.23 861.42 11.75 o 1 -5 1 1482.45 1524.04 21.10 o 2 -5 1 157.74 150.56 10.11 o 3 -5 1 292.71 320.77 12.91 o 4 -5 1 285.06 295.03 13.71 o 5 -5 1 733.32 685.87 20.23 o 6 -5 1 307.06 330.52 16.38 o 7 -5 1 37.67 33.57 8.36 o 8 -5 1 690.19 613.05 25.50 o -10 -4 1 7.67 4.24 6.15 o -9 -4 1 251.11 252.45 18.00 o -8 -4 1 445.39 418.58 20.03 o -7 -4 1 655.52 618.17 21.12 o -6 -4 1 393.15 392.14 15.82 o -5 -4 1 2396.58 2373.79 30.11 o -4 -4 1 1508.69 1516.01 23.06 o -3 -4 1 86.73 71.55 5.89 o -2 -4 1 1373.99 1464.32 19.71 o -1 -4 1 2432.84 2648.54 23.86 o 0 -4 1 3093.65 3272.58 18.75 o 1 -4 1 1956.40 2052.95 22.17 o 2 -4 1 787.98 843.00 15.70 o 3 -4 1 388.44 364.11 13.26 o 4 -4 1 472.63 423.34 14.31 o 5 -4 1 67.75 72.21 7.66 o 6 -4 1 240.84 232.41 15.32 o 7 -4 1 174.68 210.56 14.57 o 8 -4 1 24.82 7.31 8.01 o 9 -4 1 63.97 55.19 10.91 o -10 -3 1 184.62 191.23 18.52 o -9 -3 1 81.10 67.27 9.93 o -8 -3 1 268.93 241.11 16.40 o -7 -3 1 289.76 237.53 15.48 o -6 -3 1 178.39 199.14 12.72 o -5 -3 1 219.35 211.31 11.60 o -4 -3 1 2338.53 2251.19 25.66 o -3 -3 1 1355.63 1309.03 18.63 o -2 -3 1 3417.51 3645.01 26.43 o -1 -3 1 2661.57 2896.61 22.18 o 0 -3 1 2759.23 2942.54 15.80 o 1 -3 1 459.52 465.68 11.11 o 2 -3 1 72.69 68.53 6.18 o 3 -3 1 2850.83 2886.92 29.06 o 4 -3 1 1122.36 1091.58 20.42 o 5 -3 1 62.73 61.69 7.48 o 6 -3 1 675.36 645.34 20.94 o 7 -3 1 121.25 120.34 11.31 o 8 -3 1 271.19 264.46 18.42 o 9 -3 1 51.70 60.28 9.60 o -10 -2 1 59.23 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