#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2011386.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2011386
_journal_name_full  'Acta Crystallographica, Section C'
_journal_year  2000
_journal_volume  56
_journal_page_first  1075
_journal_page_last  1076
_publ_section_title
;
catena-poly[[Silver(I)-\m-[(E)-1,2-bis(2-pyridyl)ethylene-N:N']]nitrate]
;
loop_
_publ_author_name
  'Tong, Ming-Liang'
  'Chen, Xiao-Ming'
_chemical_formula_moiety  'Ag, C12H10N2, NO3'
_chemical_formula_sum  'C12 H10 Ag N3 O3'
_chemical_formula_iupac  '[Ag C12 H10 N2] + , N O3 -'
_chemical_formula_weight  352.10
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/n'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x+1/2, y+1/2, -z+1/2'
  '-x, -y, -z'
  'x-1/2, -y-1/2, z-1/2'
_cell_length_a  8.516(3)
_cell_length_b  10.915(4)
_cell_length_c  13.054(6)
_cell_angle_alpha  90.00
_cell_angle_beta  95.310(10)
_cell_angle_gamma  90.00
_cell_volume  1208.2(8)
_cell_formula_units_Z  4
_cell_measurement_temperature  293(2)
_exptl_crystal_density_diffrn  1.936
_diffrn_ambient_temperature  293(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  Ag1  .05989(3)  .34643(3)  .199478(19)  .05313(14) Uani d . 1 . . Ag
  N1  -.0113(3)  .3417(3)  .3553(2)  .0378(6) Uani d . 1 . . N
  N2  .6033(3)  .1320(2)  .5391(2)  .0381(6) Uani d . 1 . . N
  C1  -.1542(4)  .3853(3)  .3727(3)  .0454(8) Uani d . 1 . . C
  H1A  -.2240  .4112  .3148  .080 Uiso d R 1 . . H
  C2  -.2040(4)  .3957(3)  .4693(3)  .0485(9) Uani d . 1 . . C
  H2A  -.3069  .4277  .4781  .080 Uiso d R 1 . . H
  C3  -.1058(5)  .3587(3)  .5523(3)  .0516(9) Uani d . 1 . . C
  H3A  -.1384  .3647  .6206  .080 Uiso d R 1 . . H
  C4  .0409(4)  .3127(3)  .5360(3)  .0483(9) Uani d . 1 . . C
  H4A  .1115  .2851  .5929  .080 Uiso d R 1 . . H
  C5  .0873(4)  .3063(3)  .4369(2)  .0370(7) Uani d . 1 . . C
  C6  .2407(4)  .2576(3)  .4143(2)  .0414(8) Uani d . 1 . . C
  H6A  .2569  .2447  .3433  .080 Uiso d R 1 . . H
  C7  .3591(4)  .2300(3)  .4825(2)  .0406(8) Uani d . 1 . . C
  H7A  .3467  .2482  .5533  .080 Uiso d R 1 . . H
  C8  .5073(4)  .1737(3)  .4583(2)  .0359(7) Uani d . 1 . . C
  C9  .5484(4)  .1607(3)  .3581(2)  .0445(8) Uani d . 1 . . C
  H9A  .4803  .1921  .3015  .080 Uiso d R 1 . . H
  C10  .6881(4)  .1038(3)  .3409(3)  .0480(9) Uani d . 1 . . C
  H10A  .7175  .0942  .2721  .080 Uiso d R 1 . . H
  C11  .7833(4)  .0592(4)  .4230(3)  .0505(9) Uani d . 1 . . C
  H11A  .8800  .0181  .4122  .080 Uiso d R 1 . . H
  C12  .7379(4)  .0757(3)  .5207(3)  .0480(9) Uani d . 1 . . C
  H12A  .8048  .0448  .5782  .080 Uiso d R 1 . . H
  N3  .4266(4)  .5123(3)  .2767(2)  .0496(8) Uani d . 1 . . N
  O1  .2829(3)  .5328(3)  .2610(2)  .0789(9) Uani d . 1 . . O
  O2  .4815(4)  .4198(3)  .2396(2)  .0743(9) Uani d . 1 . . O
  O3  .5142(4)  .5839(3)  .3266(3)  .0945(11) Uani d . 1 . . O
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Ag1  .05061(18)  .0805(2)  .02771(15)  .00475(16)  .00050(10)  .00141(14)
  N1  .0360(13)  .0443(15)  .0329(13)  -.0055(12)  .0029(10)  .0005(12)
  N2  .0389(14)  .0428(16)  .0323(13)  -.0032(12)  .0012(11)  .0023(11)
  C1  .0379(18)  .047(2)  .051(2)  -.0006(15)  .0036(15)  .0020(16)
  C2  .045(2)  .045(2)  .058(2)  -.0016(16)  .0154(17)  -.0029(17)
  C3  .058(2)  .057(2)  .0431(19)  -.0047(19)  .0195(17)  -.0081(17)
  C4  .049(2)  .062(2)  .0347(17)  -.0005(17)  .0077(15)  -.0007(16)
  C5  .0376(16)  .0420(18)  .0313(16)  -.0052(14)  .0020(13)  -.0022(13)
  C6  .0437(18)  .051(2)  .0299(16)  .0021(16)  .0035(13)  -.0004(14)
  C7  .0405(17)  .052(2)  .0292(15)  -.0015(15)  .0033(13)  -.0038(14)
  C8  .0380(16)  .0382(18)  .0309(15)  -.0084(14)  .0003(12)  .0004(13)
  C9  .0508(19)  .051(2)  .0312(16)  -.0049(17)  .0031(14)  -.0011(16)
  C10  .053(2)  .051(2)  .0418(19)  -.0018(17)  .0154(16)  -.0067(16)
  C11  .045(2)  .055(2)  .053(2)  .0060(17)  .0122(16)  -.0013(18)
  C12  .045(2)  .050(2)  .047(2)  .0039(16)  -.0011(16)  .0071(17)
  N3  .0516(19)  .059(2)  .0380(16)  .0036(16)  .0039(14)  .0072(14)
  O1  .0528(18)  .116(3)  .0683(19)  .0192(18)  .0084(15)  -.0126(19)
  O2  .082(2)  .065(2)  .074(2)  .0249(17)  -.0008(17)  -.0039(16)
  O3  .092(3)  .083(2)  .102(3)  -.012(2)  -.021(2)  -.020(2)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Ag1 N2 4_565 2.173(3) yes
  Ag1 N1 . 2.176(3) yes
  N1 C1 . 1.345(4) ?
  N1 C5 . 1.351(4) ?
  N2 C12 . 1.341(4) ?
  N2 C8 . 1.352(4) ?
  N2 Ag1 4_666 2.173(3) ?
  C1 C2 . 1.372(5) ?
  C2 C3 . 1.367(5) ?
  C3 C4 . 1.381(5) ?
  C4 C5 . 1.389(5) ?
  C5 C6 . 1.465(4) ?
  C6 C7 . 1.317(4) ?
  C7 C8 . 1.464(4) ?
  C8 C9 . 1.392(4) ?
  C9 C10 . 1.378(5) ?
  C10 C11 . 1.371(5) ?
  C11 C12 . 1.379(5) ?
  N3 O3 . 1.226(4) ?
  N3 O2 . 1.230(4) ?
  N3 O1 . 1.243(4) ?