#------------------------------------------------------------------------------ #$Date: 2011-09-28 15:24:46 +0100 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/14/2011476.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011476_Fobs loop_ _publ_author_name 'Ooms, Fr\'ed\'eric' 'Norberg, Bernadette' 'Isin, Emre M.' 'Castagnoli, Neal' 'Van der Schyf, Cornelis J.' 'Wouters, Johan' _publ_section_title ; 7-Nitroindazole ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e474 _journal_page_last e475 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.232 _cell_angle_gamma 90.000 _cell_length_a 5.0200 _cell_length_b 9.6360 _cell_length_c 14.5060 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high .8112 _[local]_cod_data_source_file qd0040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jw7ni P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1005.22 940.84 4.67 o 4 0 0 3.14 2.87 .28 o 6 0 0 274.05 254.88 3.47 o 1 1 0 133.83 112.18 3.56 o 2 1 0 .11 1.34 .10 o 3 1 0 173.45 171.24 2.71 o 4 1 0 .02 .19 .40 o 5 1 0 15.17 14.57 .49 o 6 1 0 .10 .33 .15 o 0 2 0 771.71 769.44 2.07 o 1 2 0 5261.93 5258.17 58.15 o 2 2 0 975.22 934.73 5.11 o 3 2 0 85.38 72.50 1.85 o 4 2 0 23.78 25.46 .82 o 5 2 0 161.65 154.47 3.43 o 6 2 0 17.26 13.21 .42 o 1 3 0 251.27 278.10 12.50 o 2 3 0 .23 .29 .10 o 3 3 0 117.84 106.75 2.35 o 4 3 0 76.40 80.72 1.72 o 5 3 0 7.08 6.03 .34 o 0 4 0 .51 .77 .05 o 1 4 0 63.48 52.77 3.34 o 2 4 0 7.39 9.32 .29 o 3 4 0 54.09 56.04 1.30 o 4 4 0 4.68 4.70 .35 o 5 4 0 7.71 6.35 .34 o 1 5 0 460.88 472.62 2.98 o 2 5 0 2.95 2.11 .16 o 3 5 0 .11 .13 .45 o 4 5 0 .06 .19 .42 o 5 5 0 27.09 26.88 .87 o 0 6 0 298.00 304.07 2.59 o 1 6 0 .01 .20 .08 o 2 6 0 71.34 70.12 2.04 o 3 6 0 67.50 67.97 1.58 o 4 6 0 40.60 39.29 1.18 o 5 6 0 3.05 1.89 .20 o 1 7 0 46.33 50.65 2.01 o 2 7 0 6.70 8.11 .62 o 3 7 0 1.63 2.63 .26 o 4 7 0 8.91 9.38 .35 o 0 8 0 11.88 13.40 .62 o 1 8 0 25.99 25.87 .57 o 2 8 0 1.84 2.05 .24 o 3 8 0 10.65 10.74 .40 o 4 8 0 .77 1.10 .13 o 1 9 0 35.93 36.31 1.16 o 2 9 0 2.80 2.94 .21 o 3 9 0 6.08 6.22 .28 o 0 10 0 37.81 37.95 1.12 o 1 10 0 8.65 8.50 .33 o 2 10 0 6.29 5.99 .28 o 3 10 0 3.90 4.36 .21 o 1 11 0 4.15 3.94 .21 o 2 11 0 6.39 6.15 .25 o -5 0 1 82.64 88.30 2.58 o -3 0 1 71.97 70.12 1.72 o -1 0 1 5014.00 4630.52 23.32 o 1 0 1 2952.27 2935.68 18.29 o 3 0 1 88.52 84.23 1.90 o 5 0 1 106.08 112.36 2.88 o -6 1 1 1.41 .94 .18 o -5 1 1 9.85 11.23 .42 o -4 1 1 4.33 4.64 .31 o -3 1 1 20.69 22.56 .70 o -2 1 1 193.48 145.62 1.86 o -1 1 1 785.57 771.72 13.72 o 0 1 1 233.30 201.02 .96 o 1 1 1 3.18 2.43 1.11 o 2 1 1 149.72 156.65 1.98 o 3 1 1 50.04 54.43 1.57 o 4 1 1 81.45 84.21 2.41 o 5 1 1 59.28 59.83 1.49 o 6 1 1 2.64 1.97 .18 o -6 2 1 7.56 5.42 .30 o -5 2 1 147.19 140.12 3.27 o -4 2 1 282.17 298.22 4.50 o -3 2 1 1.25 1.24 .13 o -2 2 1 .66 4.21 .13 o -1 2 1 86.76 69.95 .93 o 0 2 1 2069.17 2137.52 4.80 o 1 2 1 12925.56 14256.74 108.96 o 2 2 1 887.26 896.31 5.08 o 3 2 1 82.57 83.57 1.99 o 4 2 1 16.10 18.63 .53 o 5 2 1 8.64 8.94 .39 o -5 3 1 31.75 25.50 .81 o -4 3 1 .80 1.52 .26 o -3 3 1 4.67 5.18 .26 o -2 3 1 135.46 150.25 2.22 o -1 3 1 64.70 69.76 1.77 o 0 3 1 2227.11 2211.28 5.87 o 1 3 1 218.32 208.19 1.53 o 2 3 1 11.81 13.54 .40 o 3 3 1 .05 .16 .32 o 4 3 1 1.08 1.35 .26 o 5 3 1 4.79 4.54 .30 o -5 4 1 .12 -.06 .17 o -4 4 1 302.36 319.59 4.87 o -3 4 1 21.41 22.37 .67 o -2 4 1 245.57 233.34 3.05 o -1 4 1 41.22 41.58 .78 o 0 4 1 .02 .34 .06 o 1 4 1 91.83 76.20 1.78 o 2 4 1 675.05 707.41 5.41 o 3 4 1 63.55 57.71 1.33 o 4 4 1 11.23 11.77 .45 o 5 4 1 27.62 27.62 .78 o -5 5 1 .19 .23 .17 o -4 5 1 18.30 18.42 .62 o -3 5 1 19.41 16.56 .54 o -2 5 1 79.47 76.77 1.95 o -1 5 1 45.76 47.39 .95 o 0 5 1 271.36 265.82 2.26 o 1 5 1 126.16 137.38 1.63 o 2 5 1 41.10 44.67 1.07 o 3 5 1 2.58 2.92 .29 o 4 5 1 7.29 8.71 .45 o 5 5 1 4.97 4.24 .23 o -5 6 1 .84 1.02 .13 o -4 6 1 .05 .06 .42 o -3 6 1 21.08 22.74 .66 o -2 6 1 .87 .44 .13 o -1 6 1 11.39 13.02 .30 o 0 6 1 31.17 32.95 .53 o 1 6 1 20.64 21.71 .47 o 2 6 1 .91 1.68 .16 o 3 6 1 .00 .00 .40 o 4 6 1 2.49 2.92 .26 o 5 6 1 .67 .46 .13 o -4 7 1 28.54 27.32 .93 o -3 7 1 24.99 28.06 .85 o -2 7 1 8.87 8.17 .34 o -1 7 1 103.16 101.94 3.86 o 0 7 1 320.77 329.15 2.46 o 1 7 1 81.17 77.98 3.08 o 2 7 1 29.85 28.87 .58 o 3 7 1 3.34 4.04 .28 o 4 7 1 5.80 6.07 .29 o -4 8 1 .13 .50 .13 o -3 8 1 23.21 23.41 .75 o -2 8 1 17.77 17.43 .55 o -1 8 1 .25 .48 .37 o 0 8 1 2.39 3.64 .26 o 1 8 1 136.53 148.54 2.27 o 2 8 1 38.77 37.63 1.17 o 3 8 1 .03 .13 .40 o 4 8 1 .31 .66 .13 o -4 9 1 32.54 36.71 1.02 o -3 9 1 .13 .49 .13 o -2 9 1 9.06 11.09 .39 o -1 9 1 8.69 9.76 .46 o 0 9 1 29.01 30.72 .67 o 1 9 1 .90 1.29 .21 o 2 9 1 81.18 75.98 2.21 o 3 9 1 .11 .10 .34 o -3 10 1 .71 .88 .15 o -2 10 1 .15 .67 .15 o -1 10 1 .06 -.21 .33 o 0 10 1 11.54 11.80 .37 o 1 10 1 16.74 16.13 .54 o 2 10 1 .35 .49 .12 o 3 10 1 7.57 8.17 .28 o -2 11 1 10.14 11.75 .33 o -1 11 1 2.75 2.32 .18 o 0 11 1 46.96 45.66 1.48 o 1 11 1 10.98 9.10 .30 o 2 11 1 2.80 1.71 .15 o -6 0 2 .14 -.14 .32 o -4 0 2 8.31 9.28 .37 o -2 0 2 90.25 83.65 1.44 o 0 0 2 3219.87 3134.53 16.46 o 2 0 2 37.70 34.21 .97 o 4 0 2 10.71 13.87 .47 o -6 1 2 9.39 7.84 .32 o -5 1 2 29.45 28.73 .87 o -4 1 2 27.28 27.87 .81 o -3 1 2 139.63 136.01 2.42 o -2 1 2 122.41 108.47 1.66 o -1 1 2 137.09 141.58 1.14 o 0 1 2 989.60 922.15 10.56 o 1 1 2 4076.35 4017.43 24.62 o 2 1 2 233.45 217.82 2.44 o 3 1 2 .96 2.49 .15 o 4 1 2 11.49 12.04 .44 o 5 1 2 1.27 1.52 .19 o -6 2 2 3.20 2.32 .22 o -5 2 2 108.87 105.18 2.85 o -4 2 2 36.70 41.59 1.23 o -3 2 2 16.86 17.34 .51 o -2 2 2 419.84 376.76 3.27 o -1 2 2 .28 1.98 .09 o 0 2 2 13.85 14.00 .84 o 1 2 2 6709.57 6818.06 90.90 o 2 2 2 204.55 209.58 2.53 o 3 2 2 1.07 .18 .13 o 4 2 2 .25 3.50 .29 o 5 2 2 .44 1.28 .20 o -5 3 2 67.22 72.37 1.63 o -4 3 2 31.57 33.63 .92 o -3 3 2 .95 .64 .13 o -2 3 2 381.15 376.26 3.53 o -1 3 2 223.88 199.20 1.50 o 0 3 2 .09 1.66 .50 o 1 3 2 1189.27 1202.38 6.67 o 2 3 2 91.54 97.86 1.87 o 3 3 2 6.10 5.25 .26 o 4 3 2 .32 .29 .48 o 5 3 2 7.76 7.37 .37 o -5 4 2 5.83 4.62 .31 o -4 4 2 330.20 336.38 4.99 o -3 4 2 446.77 444.34 5.12 o -2 4 2 50.94 52.59 1.45 o -1 4 2 576.62 533.64 4.22 o 0 4 2 97.96 79.77 .72 o 1 4 2 85.05 83.32 1.13 o 2 4 2 1898.16 1916.40 9.17 o 3 4 2 427.17 434.68 5.18 o 4 4 2 2.58 2.74 .26 o 5 4 2 2.70 3.65 .23 o -5 5 2 33.46 32.40 .97 o -4 5 2 .12 .16 .22 o -3 5 2 3.98 3.33 .29 o -2 5 2 80.94 73.21 1.89 o -1 5 2 201.00 201.65 4.72 o 0 5 2 418.15 421.89 2.34 o 1 5 2 1162.15 1174.93 4.86 o 2 5 2 .53 -.40 .40 o 3 5 2 9.03 8.82 .42 o 4 5 2 .00 .00 .32 o 5 5 2 3.91 5.60 .27 o -5 6 2 3.12 3.06 .20 o -4 6 2 .04 .22 .16 o -3 6 2 126.04 123.40 2.95 o -2 6 2 83.80 78.88 2.16 o -1 6 2 23.67 18.75 .38 o 0 6 2 44.97 44.84 .52 o 1 6 2 .71 1.16 .23 o 2 6 2 109.69 107.24 2.56 o 3 6 2 13.73 14.81 .50 o 4 6 2 49.89 51.70 1.31 o 5 6 2 3.84 4.87 .23 o -5 7 2 .47 .96 .13 o -4 7 2 .06 .13 .29 o -3 7 2 30.50 34.37 .94 o -2 7 2 94.57 96.00 1.80 o -1 7 2 66.93 68.10 1.24 o 0 7 2 4.11 3.33 .14 o 1 7 2 25.09 24.84 .66 o 2 7 2 7.19 5.38 .26 o 3 7 2 4.32 3.34 .31 o 4 7 2 9.94 7.50 .32 o -4 8 2 1.25 .63 .16 o -3 8 2 23.01 23.46 .75 o -2 8 2 1.25 1.54 .24 o -1 8 2 9.61 10.24 .78 o 0 8 2 29.91 33.16 .61 o 1 8 2 15.51 14.62 .54 o 2 8 2 19.34 20.80 .62 o 3 8 2 8.94 8.18 .34 o 4 8 2 14.23 14.76 .47 o -4 9 2 8.00 5.74 .21 o -3 9 2 16.63 14.93 .46 o -2 9 2 .17 .80 .15 o -1 9 2 28.95 32.21 .88 o 0 9 2 .06 .06 .16 o 1 9 2 105.56 109.32 2.76 o 2 9 2 .56 .18 .28 o 3 9 2 8.32 7.09 .28 o -3 10 2 .06 -.12 .21 o -2 10 2 16.55 16.93 .49 o -1 10 2 26.88 25.81 .72 o 0 10 2 .46 .48 .13 o 1 10 2 57.22 55.31 1.31 o 2 10 2 14.67 16.78 .46 o 3 10 2 .00 .10 .18 o -2 11 2 1.85 2.08 .15 o -1 11 2 7.02 7.16 .27 o 0 11 2 .57 .31 .26 o 1 11 2 1.62 1.99 .15 o 2 11 2 .58 .51 .12 o -5 0 3 3.37 3.23 .27 o -3 0 3 12.99 15.91 .51 o -1 0 3 2171.29 2121.58 6.62 o 1 0 3 1461.57 1454.42 9.34 o 3 0 3 46.15 51.39 1.14 o 5 0 3 .12 -.13 .43 o -6 1 3 4.71 4.13 .24 o -5 1 3 1.44 1.19 .22 o -4 1 3 98.13 95.66 2.51 o -3 1 3 774.63 762.91 5.90 o -2 1 3 349.97 309.27 2.83 o -1 1 3 1443.82 1402.21 9.14 o 0 1 3 745.36 701.75 2.51 o 1 1 3 21.09 15.53 .30 o 2 1 3 .06 .36 .10 o 3 1 3 245.35 269.88 3.67 o 4 1 3 1.86 2.07 .26 o 5 1 3 .69 .59 .19 o -6 2 3 .80 .86 .15 o -5 2 3 .06 .00 .33 o -4 2 3 .24 .69 .23 o -3 2 3 3.05 4.65 .19 o -2 2 3 26.39 22.07 .56 o -1 2 3 641.20 641.75 8.21 o 0 2 3 1446.89 1366.34 8.46 o 1 2 3 1096.54 1092.46 4.49 o 2 2 3 .24 .15 .10 o 3 2 3 1.80 4.87 .24 o 4 2 3 8.48 9.35 .42 o 5 2 3 1.26 .89 .20 o -5 3 3 2.53 2.72 .24 o -4 3 3 230.55 238.51 4.16 o -3 3 3 19.42 20.13 .61 o -2 3 3 22.11 28.93 .72 o -1 3 3 1.11 .74 .40 o 0 3 3 94.65 88.30 .68 o 1 3 3 6.65 5.56 .61 o 2 3 3 2422.43 2533.21 10.06 o 3 3 3 1.86 3.01 .22 o 4 3 3 9.88 10.44 .42 o 5 3 3 4.33 3.97 .27 o -5 4 3 19.25 16.11 .48 o -4 4 3 174.70 176.83 3.63 o -3 4 3 158.28 156.83 3.06 o -2 4 3 55.87 54.19 1.51 o -1 4 3 33.48 37.72 .77 o 0 4 3 47.47 43.46 .56 o 1 4 3 312.08 339.80 2.37 o 2 4 3 1374.45 1396.45 8.05 o 3 4 3 14.92 15.75 .47 o 4 4 3 10.29 10.98 .45 o 5 4 3 6.03 6.08 .30 o -5 5 3 5.43 7.41 .30 o -4 5 3 4.12 5.86 .35 o -3 5 3 1.97 2.79 .29 o -2 5 3 256.80 273.77 3.71 o -1 5 3 3.40 3.60 1.10 o 0 5 3 123.24 114.85 1.04 o 1 5 3 21.96 16.37 .52 o 2 5 3 1.78 2.44 .19 o 3 5 3 1.37 2.33 .26 o 4 5 3 11.84 10.29 .42 o 5 5 3 .37 .36 .10 o -5 6 3 5.01 5.30 .23 o -4 6 3 .80 .51 .19 o -3 6 3 584.74 597.68 6.49 o -2 6 3 167.06 162.98 3.13 o -1 6 3 6.98 7.69 .21 o 0 6 3 38.87 31.80 .44 o 1 6 3 68.17 65.09 1.33 o 2 6 3 37.70 48.16 1.25 o 3 6 3 582.72 589.24 6.48 o 4 6 3 32.57 32.69 1.02 o 5 6 3 7.92 7.65 .27 o -4 7 3 65.51 67.02 1.99 o -3 7 3 61.00 56.94 1.44 o -2 7 3 .78 .90 .15 o -1 7 3 1.57 1.89 .38 o 0 7 3 171.08 181.53 2.67 o 1 7 3 7.92 11.22 1.83 o 2 7 3 181.84 168.80 4.06 o 3 7 3 33.78 29.74 1.07 o 4 7 3 .30 .22 .16 o -4 8 3 21.96 21.76 .71 o -3 8 3 3.82 3.56 .24 o -2 8 3 78.82 81.03 2.38 o -1 8 3 24.09 26.86 .58 o 0 8 3 39.58 39.15 .59 o 1 8 3 .09 -.12 .36 o 2 8 3 113.46 109.45 2.78 o 3 8 3 1.64 3.11 .21 o 4 8 3 17.54 16.14 .44 o -4 9 3 .83 .55 .10 o -3 9 3 16.12 16.68 .55 o -2 9 3 8.63 7.64 .34 o -1 9 3 43.10 44.79 1.28 o 0 9 3 4.87 4.91 .23 o 1 9 3 6.28 4.96 .31 o 2 9 3 .46 .37 .13 o 3 9 3 .15 .13 .21 o -3 10 3 12.51 13.50 .43 o -2 10 3 .13 .10 .12 o -1 10 3 .19 .06 .15 o 0 10 3 21.27 20.61 .44 o 1 10 3 6.49 5.51 .28 o 2 10 3 8.28 6.19 .28 o -2 11 3 .27 .27 .09 o -1 11 3 3.67 3.10 .18 o 0 11 3 .01 .08 .11 o 1 11 3 .18 .27 .12 o -6 0 4 2.36 2.03 .18 o -4 0 4 .03 .85 .20 o -2 0 4 .18 .64 .06 o 0 0 4 935.15 973.80 1.90 o 2 0 4 75.37 88.20 1.71 o 4 0 4 .32 1.16 .22 o -6 1 4 .01 .07 .24 o -5 1 4 30.12 28.71 .87 o -4 1 4 107.57 123.46 2.93 o -3 1 4 14.96 16.29 .52 o -2 1 4 875.34 920.46 5.09 o -1 1 4 3.60 3.04 .19 o 0 1 4 930.32 875.59 3.88 o 1 1 4 201.41 183.03 1.39 o 2 1 4 645.69 664.29 4.73 o 3 1 4 150.06 148.91 2.87 o 4 1 4 42.34 47.30 1.32 o 5 1 4 5.75 5.14 .33 o -6 2 4 9.78 9.12 .34 o -5 2 4 .41 .48 .17 o -4 2 4 3.52 3.67 .30 o -3 2 4 .08 .76 .13 o -2 2 4 4.99 6.38 .18 o -1 2 4 336.26 323.28 4.69 o 0 2 4 190.36 177.79 2.88 o 1 2 4 1.14 1.60 .87 o 2 2 4 .20 .86 .13 o 3 2 4 .70 .81 .16 o 4 2 4 54.81 56.05 1.46 o 5 2 4 5.18 5.13 .30 o -5 3 4 17.28 17.95 .52 o -4 3 4 7.40 8.38 .39 o -3 3 4 6.35 7.38 .29 o -2 3 4 211.55 238.78 2.94 o -1 3 4 116.34 112.58 1.23 o 0 3 4 3.09 3.72 .06 o 1 3 4 461.66 455.69 7.42 o 2 3 4 13.34 12.17 .34 o 3 3 4 50.62 49.28 1.29 o 4 3 4 19.50 21.39 .61 o 5 3 4 4.82 4.71 .27 o -5 4 4 1.40 1.36 .20 o -4 4 4 8.12 8.04 .43 o -3 4 4 5.76 7.35 .29 o -2 4 4 138.13 128.56 2.38 o -1 4 4 176.90 167.59 6.39 o 0 4 4 175.28 155.26 1.94 o 1 4 4 38.43 28.97 .53 o 2 4 4 203.56 201.96 3.17 o 3 4 4 61.76 66.06 1.48 o 4 4 4 29.72 26.21 .83 o 5 4 4 5.06 4.27 .27 o -5 5 4 23.90 23.72 .70 o -4 5 4 40.92 47.01 1.32 o -3 5 4 311.12 330.51 4.65 o -2 5 4 141.99 143.45 2.74 o -1 5 4 210.34 221.85 2.18 o 0 5 4 34.31 36.22 .44 o 1 5 4 79.26 78.93 2.58 o 2 5 4 277.62 283.60 4.03 o 3 5 4 437.92 440.90 5.54 o 4 5 4 8.81 8.73 .38 o 5 5 4 .07 .06 .23 o -5 6 4 .00 .19 .10 o -4 6 4 9.72 8.30 .35 o -3 6 4 82.85 78.76 1.66 o -2 6 4 381.49 394.30 4.93 o -1 6 4 1.66 2.14 .14 o 0 6 4 53.95 58.40 .82 o 1 6 4 35.26 38.22 2.86 o 2 6 4 7.08 5.33 .34 o 3 6 4 37.70 42.39 1.29 o 4 6 4 58.79 53.63 1.28 o -4 7 4 .35 .66 .16 o -3 7 4 71.15 82.34 2.40 o -2 7 4 21.07 23.41 .53 o -1 7 4 2.15 2.10 .26 o 0 7 4 19.37 21.54 .65 o 1 7 4 1.66 2.80 .17 o 2 7 4 .03 .29 .14 o 3 7 4 14.48 11.39 .44 o 4 7 4 .47 .76 .13 o -4 8 4 1.46 1.15 .16 o -3 8 4 3.69 4.45 .28 o -2 8 4 120.23 114.45 2.84 o -1 8 4 206.96 224.08 2.85 o 0 8 4 18.68 20.53 .30 o 1 8 4 3.62 2.29 .18 o 2 8 4 23.78 20.78 .62 o 3 8 4 1.15 1.68 .19 o 4 8 4 32.08 27.75 .66 o -3 9 4 8.78 9.37 .31 o -2 9 4 .16 .21 .18 o -1 9 4 4.77 5.24 .31 o 0 9 4 1.65 1.43 .80 o 1 9 4 3.95 4.65 .31 o 2 9 4 .03 .15 .24 o 3 9 4 9.70 9.20 .31 o -3 10 4 5.65 4.80 .21 o -2 10 4 51.58 58.26 1.18 o -1 10 4 68.80 71.27 1.45 o 0 10 4 .82 .59 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