#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2011483.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2011483
_journal_name_full  'Acta Crystallographica, Section C'
_journal_year  2000
_journal_volume  56
_journal_page_first  1312
_journal_page_last  1313
_publ_section_title
;
Bis(acridine-N)(nitrato-O,O')silver(I)
;
loop_
_publ_author_name
  'Sloufova, Ivana'
  'Slouf, Miroslav'
_chemical_name_common
;
Bis(acridine)(nitrato)silver
;
_chemical_formula_moiety  'C26 H18 Ag N3 O3'
_chemical_formula_sum  'C26 H18 Ag N3 O3'
_chemical_formula_iupac  '[Ag (N O3) (C13 H9 N)2]'
_chemical_formula_weight  528.30
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, -y, -z'
_cell_length_a  9.128(3)
_cell_length_b  10.096(2)
_cell_length_c  11.763(2)
_cell_angle_alpha  108.190(10)
_cell_angle_beta  91.93(2)
_cell_angle_gamma  94.23(2)
_cell_volume  1025.2(4)
_cell_formula_units_Z  2
_cell_measurement_temperature  293(2)
_exptl_crystal_density_diffrn  1.711
_diffrn_ambient_temperature  150.00(10)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  Ag  .102005(16)  -.059315(15)  .763808(14)  .02333(8) Uani d . 1 . . Ag
  N1D  .01666(18)  -.27270(18)  .88422(16)  .0226(4) Uani d . 1 . . N
  O2D  .0280(2)  -.31216(18)  .77284(15)  .0366(4) Uani d . 1 . . O
  O3D  .02457(19)  -.14307(16)  .93871(15)  .0325(4) Uani d . 1 . . O
  O4D  -.0019(2)  -.35780(18)  .93934(16)  .0376(4) Uani d . 1 . . O
  N1A  .34197(18)  -.02535(18)  .81562(15)  .0185(3) Uani d . 1 . . N
  C2A  .4336(2)  -.1265(2)  .76894(18)  .0192(4) Uani d . 1 . . C
  C3A  .3745(2)  -.2575(2)  .68879(19)  .0239(4) Uani d . 1 . . C
  H3A  .277(3)  -.2732(5)  .6707(6)  .027(6) Uiso calc R 1 . . H
  C4A  .4644(3)  -.3602(2)  .6388(2)  .0275(5) Uani d . 1 . . C
  H4A  .4218(13)  -.450(3)  .5833(17)  .039(7) Uiso calc R 1 . . H
  C5A  .6181(3)  -.3380(2)  .6662(2)  .0275(5) Uani d . 1 . . C
  H5A  .6794(18)  -.409(2)  .6294(11)  .033(7) Uiso calc R 1 . . H
  C6A  .6780(2)  -.2157(2)  .7449(2)  .0247(5) Uani d . 1 . . C
  H6A  .779(3)  -.2033(4)  .7639(6)  .031(7) Uiso calc R 1 . . H
  C7A  .5885(2)  -.1055(2)  .79918(18)  .0205(4) Uani d . 1 . . C
  C8A  .6455(2)  .0222(2)  .88053(19)  .0220(4) Uani d . 1 . . C
  H8A  .746(3)  .0371(5)  .9035(7)  .023(6) Uiso calc R 1 . . H
  C9A  .5535(2)  .1274(2)  .92762(18)  .0207(4) Uani d . 1 . . C
  C10A  .6057(2)  .2616(2) 1.0090(2)  .0255(5) Uani d . 1 . . C
  H10A  .707(3)  .2813(6) 1.0331(7)  .027(6) Uiso calc R 1 . . H
  C11A  .5116(3)  .3610(2) 1.0521(2)  .0270(5) Uani d . 1 . . C
  H11A  .5483(11)  .451(3) 1.1055(16)  .032(7) Uiso calc R 1 . . H
  C12A  .3594(3)  .3322(2) 1.01846(19)  .0258(5) Uani d . 1 . . C
  H12A  .294(2)  .403(2) 1.0496(10)  .037(7) Uiso calc R 1 . . H
  C13A  .3045(2)  .2052(2)  .94223(18)  .0228(4) Uani d . 1 . . C
  H13A  .205(3)  .1880(5)  .9224(6)  .023(6) Uiso calc R 1 . . H
  C14A  .3998(2)  .0990(2)  .89289(17)  .0187(4) Uani d . 1 . . C
  N1B  -.07387(18)  -.03849(18)  .63764(15)  .0189(3) Uani d . 1 . . N
  C2B  -.1451(2)  .0799(2)  .66188(18)  .0191(4) Uani d . 1 . . C
  C3B  -.1034(2)  .1925(2)  .76843(19)  .0224(4) Uani d . 1 . . C
  H3B  -.028(2)  .1838(3)  .8206(15)  .023(6) Uiso calc R 1 . . H
  C4B  -.1717(2)  .3129(2)  .7951(2)  .0262(5) Uani d . 1 . . C
  H4B  -.1422(10)  .385(2)  .863(2)  .033(7) Uiso calc R 1 . . H
  C5B  -.2885(3)  .3271(2)  .7183(2)  .0294(5) Uani d . 1 . . C
  H5B  -.3372(15)  .412(3)  .7389(7)  .038(7) Uiso calc R 1 . . H
  C6B  -.3322(2)  .2221(2)  .6163(2)  .0271(5) Uani d . 1 . . C
  H6B  -.410(2)  .2331(4)  .5660(15)  .028(6) Uiso calc R 1 . . H
  C7B  -.2615(2)  .0946(2)  .58363(18)  .0215(4) Uani d . 1 . . C
  C8B  -.3010(2)  -.0157(2)  .47952(19)  .0236(4) Uani d . 1 . . C
  H8B  -.375(2)  -.0082(3)  .4285(15)  .023(6) Uiso calc R 1 . . H
  C9B  -.2288(2)  -.1376(2)  .45232(18)  .0211(4) Uani d . 1 . . C
  C10B  -.2632(2)  -.2535(2)  .3462(2)  .0271(5) Uani d . 1 . . C
  H10B  -.337(2)  -.2498(3)  .2926(17)  .034(7) Uiso calc R 1 . . H
  C11B  -.1881(3)  -.3694(2)  .3232(2)  .0299(5) Uani d . 1 . . C
  H11B  -.2107(7)  -.443(2)  .253(2)  .032(7) Uiso calc R 1 . . H
  C12B  -.0756(3)  -.3776(2)  .4058(2)  .0281(5) Uani d . 1 . . C
  H12B  -.0245(16)  -.459(3)  .3894(6)  .039(7) Uiso calc R 1 . . H
  C13B  -.0396(2)  -.2695(2)  .5089(2)  .0239(4) Uani d . 1 . . C
  H13B  .033(2)  -.2769(3)  .5616(16)  .025(6) Uiso calc R 1 . . H
  C14B  -.1142(2)  -.1452(2)  .53526(18)  .0192(4) Uani d . 1 . . C
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Ag  .01686(10)  .02092(11)  .02971(11)  .00245(6)  -.00459(6)  .00486(7)
  N1D  .0163(9)  .0223(9)  .0276(10)  .0022(7)  -.0009(7)  .0060(8)
  O2D  .0476(11)  .0311(9)  .0272(9)  .0082(8)  .0094(8)  .0019(7)
  O3D  .0415(10)  .0201(8)  .0308(9)  -.0011(7)  .0023(7)  .0016(7)
  O4D  .0452(10)  .0298(9)  .0415(10)  -.0025(8)  -.0031(8)  .0185(8)
  N1A  .0165(8)  .0222(9)  .0170(8)  .0031(7)  .0011(6)  .0062(7)
  C2A  .0178(10)  .0248(11)  .0175(9)  .0037(8)  .0025(8)  .0096(8)
  C3A  .0202(11)  .0279(11)  .0216(10)  .0043(9)  .0004(8)  .0048(9)
  C4A  .0330(12)  .0263(12)  .0212(10)  .0068(9)  .0043(9)  .0037(9)
  C5A  .0304(12)  .0311(12)  .0253(11)  .0140(10)  .0117(9)  .0113(9)
  C6A  .0181(11)  .0342(12)  .0288(11)  .0079(9)  .0073(9)  .0178(10)
  C7A  .0181(10)  .0267(11)  .0212(10)  .0043(8)  .0041(8)  .0131(9)
  C8A  .0149(10)  .0312(12)  .0244(11)  -.0008(8)  .0007(8)  .0159(9)
  C9A  .0203(10)  .0252(11)  .0195(10)  -.0012(8)  .0006(8)  .0118(8)
  C10A  .0227(11)  .0290(12)  .0262(11)  -.0055(9)  -.0028(9)  .0127(9)
  C11A  .0349(13)  .0216(11)  .0231(11)  -.0034(9)  -.0027(9)  .0069(9)
  C12A  .0311(12)  .0238(11)  .0228(11)  .0052(9)  .0022(9)  .0072(9)
  C13A  .0202(11)  .0262(11)  .0212(10)  .0035(8)  -.0006(8)  .0064(9)
  C14A  .0185(10)  .0229(10)  .0167(9)  .0012(8)  .0010(8)  .0092(8)
  N1B  .0154(8)  .0189(8)  .0224(9)  .0005(6)  .0019(7)  .0067(7)
  C2B  .0160(9)  .0206(10)  .0230(10)  .0011(8)  .0057(8)  .0098(8)
  C3B  .0182(10)  .0224(11)  .0256(11)  .0005(8)  .0012(9)  .0065(9)
  C4B  .0284(12)  .0216(11)  .0279(11)  .0025(9)  .0058(9)  .0065(9)
  C5B  .0322(12)  .0250(12)  .0356(13)  .0120(10)  .0096(10)  .0132(10)
  C6B  .0229(11)  .0336(13)  .0308(12)  .0098(9)  .0047(9)  .0169(10)
  C7B  .0179(10)  .0267(11)  .0237(10)  .0038(8)  .0060(8)  .0127(9)
  C8B  .0170(10)  .0342(12)  .0226(10)  .0022(9)  .0004(8)  .0131(9)
  C9B  .0173(10)  .0271(11)  .0199(10)  -.0014(8)  .0034(8)  .0092(9)
  C10B  .0224(11)  .0370(13)  .0200(10)  -.0007(9)  -.0006(9)  .0073(9)
  C11B  .0313(12)  .0285(12)  .0233(11)  -.0026(9)  .0031(9)  -.0004(10)
  C12B  .0293(12)  .0231(11)  .0295(12)  .0039(9)  .0071(9)  .0040(9)
  C13B  .0219(11)  .0238(11)  .0254(11)  .0029(8)  .0009(9)  .0069(9)
  C14B  .0164(9)  .0216(10)  .0201(10)  -.0007(8)  .0045(8)  .0075(8)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Ag N1B . 2.216(2) y
  Ag N1A . 2.226(2) y
  Ag O2D . 2.627(2) y
  Ag O3D . 2.558(2) y
  N1D O4D . 1.233(2) ?
  N1D O2D . 1.255(2) ?
  N1D O3D . 1.260(2) ?
  N1A C14A . 1.356(3) ?
  N1A C2A . 1.360(3) ?
  C2A C3A . 1.418(3) ?
  C2A C7A . 1.430(3) ?
  C3A C4A . 1.368(3) ?
  C3A H3A .  .8977 ?
  C4A C5A . 1.415(3) ?
  C4A H4A .  .9810 ?
  C5A C6A . 1.354(3) ?
  C5A H5A .  .9475 ?
  C6A C7A . 1.428(3) ?
  C6A H6A .  .9300 ?
  C7A C8A . 1.395(3) ?
  C8A C9A . 1.392(3) ?
  C8A H8A .  .9344 ?
  C9A C10A . 1.429(3) ?
  C9A C14A . 1.430(3) ?
  C10A C11A . 1.356(3) ?
  C10A H10A .  .9462 ?
  C11A C12A . 1.416(3) ?
  C11A H11A .  .9567 ?
  C12A C13A . 1.362(3) ?
  C12A H12A .  .9533 ?
  C13A C14A . 1.424(3) ?
  C13A H13A .  .9204 ?
  N1B C2B . 1.359(3) ?
  N1B C14B . 1.359(3) ?
  C2B C3B . 1.422(3) ?
  C2B C7B . 1.429(3) ?
  C3B C4B . 1.360(3) ?
  C3B H3B .  .9320 ?
  C4B C5B . 1.418(3) ?
  C4B H4B .  .9087 ?
  C5B C6B . 1.355(3) ?
  C5B H5B .  .9637 ?
  C6B C7B . 1.432(3) ?
  C6B H6B .  .9456 ?
  C7B C8B . 1.389(3) ?
  C8B C9B . 1.392(3) ?
  C8B H8B .  .9112 ?
  C9B C10B . 1.427(3) ?
  C9B C14B . 1.429(3) ?
  C10B C11B . 1.358(3) ?
  C10B H10B .  .9188 ?
  C11B C12B . 1.415(3) ?
  C11B H11B .  .9252 ?
  C12B C13B . 1.365(3) ?
  C12B H12B .  .9467 ?
  C13B C14B . 1.425(3) ?
  C13B H13B .  .9141 ?