#------------------------------------------------------------------------------ #$Date: 2016-04-02 19:27:36 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180784 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/15/2011594.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011594_Fobs loop_ _publ_author_name 'Crespo, Olga' 'Gimeno, M. Concepcion' 'Jones, Peter G.' 'Laguna, Antonio' _publ_section_title ; Solvent-free [\m-ferrocene-1,1'-diylbis(diphenylphosphine-P)]bis[chlorogold(I)] ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1433 _journal_page_last 1434 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.788 _cell_angle_gamma 90.000 _cell_length_a 9.0385 _cell_length_b 19.1300 _cell_length_c 9.9297 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bm1433Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\ESP\DUBIUS in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 429.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 168796.47 164106.20 473.28 o 4 0 0 69809.91 73289.01 473.28 o 6 0 0 12600.79 13429.83 306.32 o 8 0 0 5661.68 6092.97 293.47 o 10 0 0 105.62 -0.64 291.55 o 2 1 0 492.32 651.17 87.34 o 3 1 0 3476.10 3748.38 129.72 o 4 1 0 8534.53 9095.14 197.15 o 5 1 0 3113.35 3477.38 166.32 o 6 1 0 5929.39 5641.52 233.75 o 7 1 0 11642.80 11337.62 329.44 o 8 1 0 2290.27 2637.42 262.01 o 9 1 0 1963.61 1995.88 282.56 o 10 1 0 1276.40 1410.86 310.81 o 1 2 0 104785.49 105585.12 6635.93 o 2 2 0 93.27 178.52 91.83 o 3 2 0 111246.36 109376.73 506.68 o 4 2 0 5842.41 6140.49 181.09 o 5 2 0 25084.79 25258.72 339.07 o 6 2 0 293.35 181.74 177.24 o 7 2 0 4429.80 4711.00 256.87 o 8 2 0 407.89 577.32 237.61 o 9 2 0 624.45 974.82 269.71 o 10 2 0 155.00 -74.49 290.26 o 1 3 0 16869.17 18757.63 176.60 o 2 3 0 23041.99 23470.90 231.83 o 3 3 0 227.32 272.28 100.82 o 4 3 0 16973.79 17114.00 263.29 o 5 3 0 4877.61 5036.59 192.65 o 6 3 0 9203.59 9282.66 278.06 o 7 3 0 971.02 988.31 209.35 o 8 3 0 6720.87 6331.22 314.67 o 9 3 0 3911.86 3603.89 314.02 o 10 3 0 2815.92 2615.58 333.93 o 0 4 0 81984.67 80297.72 348.70 o 1 4 0 5317.93 5740.45 222.19 o 2 4 0 103274.52 99177.05 498.97 o 3 4 0 2102.97 2028.63 127.15 o 4 4 0 35245.49 33775.26 363.47 o 5 4 0 1162.44 1161.70 158.62 o 6 4 0 15984.59 15115.54 335.22 o 7 4 0 207.25 84.13 209.35 o 8 4 0 630.58 547.78 246.60 o 9 4 0 39.61 95.68 274.21 o 10 4 0 225.26 163.75 299.90 o 1 5 0 5145.95 5542.79 274.53 o 2 5 0 2223.63 2503.84 150.91 o 3 5 0 4413.60 4438.08 168.89 o 4 5 0 3095.30 3537.75 172.75 o 5 5 0 32349.15 32197.43 415.49 o 6 5 0 1741.81 1977.90 205.50 o 7 5 0 7008.85 6794.87 303.11 o 8 5 0 525.38 802.08 245.95 o 9 5 0 8387.01 8409.94 386.59 o 0 6 0 11632.14 11541.19 189.44 o 1 6 0 86770.83 85252.77 1889.60 o 2 6 0 21403.05 22393.97 317.88 o 3 6 0 35697.50 32761.90 384.02 o 4 6 0 697.38 518.88 150.91 o 5 6 0 22078.86 21113.47 364.76 o 6 6 0 1478.66 1419.21 207.42 o 7 6 0 6517.36 6676.71 303.11 o 8 6 0 220.03 276.14 244.67 o 9 6 0 183.70 180.45 263.93 o 1 7 0 2264.61 2588.82 253.98 o 2 7 0 8559.21 9477.88 250.45 o 3 7 0 1658.48 1816.07 177.24 o 4 7 0 11444.44 11204.69 290.26 o 5 7 0 84.24 43.67 172.75 o 6 7 0 12011.97 10856.63 333.93 o 7 7 0 304.61 211.92 223.48 o 8 7 0 8612.67 8038.12 366.04 o 9 7 0 9.89 34.04 276.78 o 0 8 0 53111.38 54197.11 425.12 o 1 8 0 23430.10 22627.90 216.73 o 2 8 0 26638.56 26650.31 393.01 o 3 8 0 15265.41 15445.62 330.72 o 4 8 0 29313.93 28130.53 432.83 o 5 8 0 4454.84 3839.57 244.03 o 6 8 0 469.38 486.77 211.28 o 7 8 0 519.35 823.27 242.74 o 8 8 0 1921.26 1658.74 279.35 o 9 8 0 37.61 28.90 279.99 o 1 9 0 8.98 95.19 95.62 o 2 9 0 2.52 52.66 174.03 o 3 9 0 10773.68 10927.27 314.67 o 4 9 0 618.95 644.10 195.22 o 5 9 0 7629.66 7498.05 286.41 o 6 9 0 52.10 117.52 216.41 o 7 9 0 11906.81 10203.54 389.16 o 8 9 0 550.73 592.73 270.36 o 9 9 0 3910.14 4150.38 367.97 o 0 10 0 40966.96 40618.29 426.40 o 1 10 0 39785.21 38127.37 302.16 o 2 10 0 12058.66 11469.91 314.02 o 3 10 0 16057.17 16019.73 387.23 o 4 10 0 17069.61 17024.73 410.99 o 5 10 0 7179.95 7142.28 323.66 o 6 10 0 964.87 912.53 245.95 o 7 10 0 3603.86 3954.52 305.03 o 8 10 0 930.51 1322.88 294.12 o 9 10 0 891.01 380.17 319.16 o 1 11 0 34.73 -20.71 112.64 o 2 11 0 2466.43 2611.53 142.06 o 3 11 0 3719.12 3883.88 277.42 o 4 11 0 8117.74 8301.41 339.71 o 5 11 0 14.75 96.97 237.61 o 6 11 0 8754.46 7639.97 373.10 o 7 11 0 1307.50 1155.28 286.41 o 8 11 0 4953.24 4858.71 361.55 o 0 12 0 11441.55 11169.37 290.91 o 1 12 0 31161.84 29652.04 308.25 o 2 12 0 18372.79 17323.34 258.84 o 3 12 0 17360.31 17155.10 434.75 o 4 12 0 5347.89 6112.88 317.88 o 5 12 0 5547.71 5848.94 344.85 o 6 12 0 6399.57 6468.00 362.19 o 7 12 0 602.16 840.61 288.34 o 8 12 0 374.01 773.18 291.55 o 1 13 0 3547.68 3551.01 166.85 o 2 13 0 118.13 63.94 144.33 o 3 13 0 1007.89 1224.63 269.71 o 4 13 0 311.71 251.73 260.08 o 5 13 0 6865.70 7644.47 384.02 o 6 13 0 986.95 734.01 302.46 o 7 13 0 952.09 1098.76 305.68 o 8 13 0 537.49 83.48 330.08 o 0 14 0 22194.39 21391.53 425.76 o 1 14 0 5226.91 5116.07 196.77 o 2 14 0 31235.55 29632.60 360.11 o 3 14 0 7746.22 7956.56 392.37 o 4 14 0 7944.85 8034.27 400.72 o 5 14 0 3964.42 4583.85 349.34 o 6 14 0 3629.06 3641.78 344.21 o 7 14 0 1283.31 1403.15 342.28 o 8 14 0 39.92 -174.67 356.41 o 1 15 0 614.71 705.91 165.77 o 2 15 0 864.45 829.26 184.63 o 3 15 0 49.58 -14.77 287.05 o 4 15 0 1916.00 2333.03 332.65 o 5 15 0 3606.20 3719.48 363.47 o 6 15 0 2494.55 2397.24 382.09 o 7 15 0 170.85 245.31 323.01 o 0 16 0 6937.33 6940.00 321.09 o 1 16 0 18732.26 18033.98 644.10 o 2 16 0 861.90 709.33 196.18 o 3 16 0 9048.59 9870.25 426.40 o 4 16 0 3629.64 3590.41 374.39 o 5 16 0 3148.93 3463.90 363.47 o 6 16 0 388.32 393.01 342.92 o 7 16 0 538.60 516.95 369.25 o 1 17 0 28.87 -17.70 179.63 o 2 17 0 1394.79 1253.71 189.99 o 3 17 0 2110.65 2244.41 350.63 o 4 17 0 2230.91 2015.15 340.35 o 5 17 0 1316.21 1683.79 363.47 o 6 17 0 1964.57 2169.91 378.88 o 0 18 0 11668.24 11339.55 422.55 o 1 18 0 905.72 867.30 258.15 o 2 18 0 3557.91 3438.94 229.55 o 3 18 0 403.87 201.00 337.78 o 4 18 0 6399.91 6936.79 464.94 o 5 18 0 332.64 272.92 357.05 o 6 18 0 565.78 802.72 398.79 o 1 19 0 82.44 236.92 194.14 o 2 19 0 148.24 99.58 200.76 o 3 19 0 3884.14 4085.53 410.35 o 4 19 0 836.05 547.13 375.67 o 5 19 0 1335.43 1092.34 420.63 o 0 20 0 8.69 -12.20 296.69 o 1 20 0 6339.48 6483.23 286.34 o 2 20 0 727.25 1082.09 219.13 o 3 20 0 5087.01 5760.32 466.86 o 4 20 0 51.87 -168.25 385.31 o 1 21 0 771.60 646.78 235.94 o 2 21 0 152.58 362.82 233.89 o 3 21 0 2.91 260.08 372.46 o 0 22 0 3931.00 4231.94 394.30 o 1 22 0 299.29 576.09 231.56 o 2 22 0 4491.50 4555.45 304.25 o -9 0 1 2789.22 3156.94 287.05 o -7 0 1 28274.80 27803.02 445.03 o -5 0 1 57865.26 57892.83 473.93 o -3 0 1 101894.32 100449.20 457.87 o 1 0 1 79633.60 82258.66 210.91 o 3 0 1 23003.22 24027.02 261.37 o 5 0 1 11431.21 11737.05 256.23 o 7 0 1 26.77 148.98 200.36 o 9 0 1 246.35 -104.03 274.21 o -10 1 1 6095.90 6834.04 371.18 o -9 1 1 2867.38 3139.60 297.33 o -8 1 1 2560.72 2513.48 254.30 o -7 1 1 3690.93 3951.95 239.53 o -6 1 1 8032.81 7722.81 245.31 o -5 1 1 2669.77 2738.24 164.40 o -4 1 1 185.56 234.39 112.38 o -3 1 1 2180.31 2738.24 119.44 o -2 1 1 2580.28 2858.33 107.24 o 1 1 1 12562.45 13778.30 98.98 o 2 1 1 18783.77 21226.49 206.14 o 3 1 1 15005.27 16545.03 222.19 o 4 1 1 18324.84 19229.32 279.35 o 5 1 1 8145.35 8285.36 236.96 o 6 1 1 3346.26 3779.21 220.27 o 7 1 1 4993.38 5339.70 271.64 o 8 1 1 7788.80 7469.15 337.78 o 9 1 1 1862.41 2099.27 300.54 o -10 2 1 2597.56 3031.71 331.36 o -9 2 1 310.75 185.59 255.59 o -8 2 1 12291.33 12336.85 381.45 o -7 2 1 1060.24 1231.05 215.13 o -6 2 1 33800.22 32607.14 428.97 o -5 2 1 11.13 84.13 135.50 o -4 2 1 54402.12 53371.27 410.35 o -3 2 1 6600.17 6419.84 155.41 o -2 2 1 84230.98 78291.55 378.24 o -1 2 1 209.13 212.48 51.29 o 0 2 1 35050.34 37287.87 1650.39 o 1 2 1 7865.33 8630.94 225.08 o 2 2 1 18772.53 18869.06 203.57 o 3 2 1 23.00 41.74 97.61 o 4 2 1 3308.58 3327.76 157.33 o 5 2 1 3349.19 3659.76 192.65 o 6 2 1 1239.73 1211.14 192.01 o 7 2 1 243.73 61.01 204.21 o 8 2 1 15.36 -10.92 230.54 o 9 2 1 52.37 -30.82 253.66 o -10 3 1 746.30 976.11 304.39 o -9 3 1 5159.01 5573.45 322.37 o -8 3 1 3325.07 3549.31 265.86 o -7 3 1 6206.89 6052.51 272.92 o -6 3 1 326.85 488.05 177.24 o -5 3 1 2207.80 2480.08 170.18 o -4 3 1 1919.38 2144.87 146.42 o -3 3 1 1161.86 1261.23 116.88 o -2 3 1 8983.96 9406.60 180.45 o -1 3 1 11105.48 12458.43 627.09 o 0 3 1 206.68 281.82 54.15 o 1 3 1 911.24 859.21 86.05 o 2 3 1 3059.94 3084.37 118.16 o 3 3 1 18618.87 19707.75 252.38 o 4 3 1 954.92 963.26 132.93 o 5 3 1 13767.25 13872.93 287.05 o 6 3 1 6751.60 6754.41 258.15 o 7 3 1 4851.23 5089.89 265.22 o 8 3 1 947.02 1342.15 248.52 o 9 3 1 1830.42 2378.62 287.05 o -10 4 1 232.71 629.97 293.47 o -9 4 1 9184.62 9386.05 396.86 o -8 4 1 1331.66 1446.82 247.88 o -7 4 1 14794.60 14694.28 372.46 o -6 4 1 3512.10 3836.36 216.41 o -5 4 1 62293.74 58881.78 522.73 o -4 4 1 11235.92 10936.90 230.54 o -3 4 1 65341.76 63145.19 446.31 o -2 4 1 23502.43 24892.68 285.77 o -1 4 1 184678.88 184787.23 8515.25 o 0 4 1 7972.73 8275.72 191.69 o 1 4 1 39341.42 41765.98 749.10 o 2 4 1 3179.38 3094.65 130.36 o 3 4 1 22263.50 21810.23 280.63 o 4 4 1 291.57 194.58 129.08 o 5 4 1 490.33 468.15 158.62 o 6 4 1 16.04 -101.46 183.02 o 7 4 1 956.00 1091.06 220.91 o 8 4 1 14.56 166.97 240.82 o 9 4 1 566.07 580.53 276.78 o -10 5 1 3369.93 3518.48 349.99 o -9 5 1 890.79 911.25 280.63 o -8 5 1 9950.41 9509.99 362.19 o -7 5 1 1314.44 1186.74 224.76 o -6 5 1 2364.45 2192.39 209.99 o -5 5 1 2.53 -28.90 153.48 o -4 5 1 3705.78 3761.23 183.02 o -3 5 1 536.80 678.78 133.57 o -2 5 1 413.62 371.82 129.08 o -1 5 1 350.86 325.97 104.03 o 0 5 1 787.33 809.97 75.98 o 1 5 1 2549.77 2664.39 163.43 o 2 5 1 15508.19 14879.87 240.82 o 3 5 1 2801.76 2408.16 148.98 o 4 5 1 2482.82 2315.05 159.90 o 5 5 1 1144.96 1158.49 166.32 o 6 5 1 9871.78 9639.71 303.75 o 7 5 1 1410.74 1162.98 234.39 o 8 5 1 2686.18 2722.19 278.70 o 9 5 1 658.55 843.18 276.14 o -10 6 1 3849.82 4445.14 378.24 o -9 6 1 1769.69 1916.25 311.46 o -8 6 1 9196.42 9244.13 366.68 o -7 6 1 2203.63 2431.28 249.16 o -6 6 1 28933.91 27212.22 449.52 o -5 6 1 21811.65 21058.88 360.90 o -4 6 1 64546.34 61201.96 537.50 o -3 6 1 6084.80 6191.22 216.41 o -2 6 1 79586.45 83165.03 570.89 o -1 6 1 21630.74 22662.37 660.48 o 0 6 1 50628.26 50368.04 488.70 o 1 6 1 3793.49 3804.11 107.08 o 2 6 1 36335.62 37277.04 401.36 o 3 6 1 8571.53 8361.13 221.55 o 4 6 1 7811.19 7545.57 233.11 o 5 6 1 345.84 407.78 164.40 o 6 6 1 1752.46 1787.18 213.84 o 7 6 1 71.73 -74.49 214.49 o 8 6 1 127.67 312.10 250.45 o 9 6 1 601.87 733.37 282.56 o -9 7 1 4839.19 5295.39 353.84 o -8 7 1 251.42 306.32 256.87 o -7 7 1 6324.50 6319.01 309.53 o -6 7 1 2.32 141.92 206.78 o -5 7 1 2208.76 2259.18 206.78 o -4 7 1 3016.48 3368.86 197.79 o -3 7 1 304.57 403.93 164.40 o -2 7 1 231.98 245.31 156.05 o -1 7 1 3759.34 3829.33 107.69 o 0 7 1 3402.15 3467.94 102.65 o 1 7 1 10088.43 10277.47 150.41 o 2 7 1 952.52 1190.59 166.32 o 3 7 1 12858.10 12347.76 277.42 o 4 7 1 2927.94 3080.52 192.01 o 5 7 1 8291.12 7708.04 276.14 o 6 7 1 18.81 -19.91 206.78 o 7 7 1 7354.75 6877.71 328.79 o 8 7 1 976.11 976.11 271.00 o 9 7 1 2405.14 2363.21 330.08 o -9 8 1 3197.75 3754.16 347.42 o -8 8 1 2385.12 2516.05 293.47 o -7 8 1 19670.06 18812.55 458.51 o -6 8 1 7231.20 7085.13 315.95 o -5 8 1 21595.24 20752.57 407.14 o -4 8 1 12249.51 11923.93 315.95 o -3 8 1 53741.34 56313.71 570.25 o -2 8 1 26191.68 27567.34 396.22 o -1 8 1 30413.37 30779.81 1276.33 o 0 8 1 20320.45 21408.45 202.22 o 1 8 1 30490.87 29614.06 245.58 o 2 8 1 4522.03 4714.22 227.97 o 3 8 1 2931.92 2794.75 206.14 o 4 8 1 403.75 385.31 177.24 o 5 8 1 3173.02 3190.97 231.18 o 6 8 1 18.56 177.24 212.56 o 7 8 1 23.68 222.84 223.48 o 8 8 1 134.52 88.62 267.15 o 9 8 1 143.39 -58.44 285.77 o -9 9 1 628.58 526.58 314.67 o -8 9 1 1691.86 1654.25 285.77 o -7 9 1 147.24 76.42 240.17 o -6 9 1 9776.15 9244.77 344.85 o -5 9 1 108.73 529.80 208.07 o -4 9 1 43.55 -165.68 184.30 o -3 9 1 240.63 359.62 188.80 o -2 9 1 203.57 280.63 173.39 o -1 9 1 13.43 146.83 96.86 o 0 9 1 11477.11 11921.02 172.86 o 1 9 1 119.50 153.50 96.86 o 2 9 1 1965.40 2021.57 206.14 o 3 9 1 239.63 69.36 193.94 o 4 9 1 19159.00 17750.39 383.38 o 5 9 1 7.24 44.31 197.79 o 6 9 1 3131.29 2683.65 251.09 o 7 9 1 15.62 -33.39 233.75 o 8 9 1 4760.17 4000.12 346.13 o 9 9 1 54.49 192.65 293.47 o -9 10 1 535.07 902.26 319.80 o -8 10 1 7118.26 6936.79 396.22 o -7 10 1 6366.48 6826.98 355.77 o -6 10 1 21570.07 21489.14 496.40 o -5 10 1 8256.74 7794.09 326.23 o -4 10 1 20901.51 20725.60 442.46 o -3 10 1 28466.32 28074.66 479.06 o -2 10 1 23894.45 24534.34 418.06 o -1 10 1 8838.80 8216.67 372.14 o 0 10 1 19687.40 19918.77 224.18 o 1 10 1 15995.09 14971.70 214.13 o 2 10 1 12977.63 12577.02 335.86 o 3 10 1 1148.51 1346.00 224.76 o 4 10 1 5480.90 5068.05 288.34 o 5 10 1 851.49 877.21 226.05 o 6 10 1 2331.61 1844.33 258.15 o 7 10 1 556.05 427.05 268.43 o 8 10 1 23.28 211.92 275.49 o -9 11 1 4913.18 4934.48 396.86 o -8 11 1 198.27 -28.90 290.91 o -7 11 1 4519.93 4747.61 339.71 o -6 11 1 2818.00 2954.01 308.24 o -5 11 1 753.81 661.44 252.38 o -4 11 1 34.07 39.17 231.18 o -3 11 1 515.37 612.64 215.77 o -2 11 1 1640.96 1570.69 179.17 o -1 11 1 2025.60 2260.67 127.18 o 0 11 1 1461.13 1494.75 122.13 o 1 11 1 12417.32 12367.87 206.07 o 2 11 1 117.75 161.79 116.18 o 3 11 1 10212.81 10861.77 366.04 o 4 11 1 1636.72 1923.32 251.09 o 5 11 1 4189.56 4170.93 303.75 o 6 11 1 64.44 174.03 242.74 o 7 11 1 5564.13 5382.08 346.13 o 8 11 1 52.96 298.61 290.26 o -8 12 1 1341.82 1712.68 325.58 o -7 12 1 571.02 816.85 290.26 o -6 12 1 7313.79 7451.17 375.03 o -5 12 1 11957.76 11864.21 409.71 o -4 12 1 12570.27 12125.57 411.63 o -3 12 1 8606.24 8954.51 350.63 o -2 12 1 15869.25 15484.46 422.55 o -1 12 1 15757.71 14965.40 232.48 o 0 12 1 9644.02 8863.73 194.51 o 1 12 1 2972.34 3031.47 183.02 o 2 12 1 3940.29 3972.13 219.95 o 3 12 1 8385.86 8576.26 357.05 o 4 12 1 544.12 676.85 265.86 o 5 12 1 56.89 47.52 242.10 o 6 12 1 119.99 146.42 258.15 o 7 12 1 825.99 727.59 292.19 o 8 12 1 184.37 -156.05 296.69 o -8 13 1 4644.69 4746.97 395.58 o -7 13 1 1150.56 1143.07 313.38 o -6 13 1 668.99 852.81 297.97 o -5 13 1 1353.81 1703.69 301.82 o -4 13 1 220.27 129.72 250.45 o -3 13 1 158.68 84.77 249.16 o -2 13 1 4778.61 4798.43 181.45 o -1 13 1 1.63 -42.34 130.62 o 0 13 1 1866.31 2017.24 219.30 o 1 13 1 430.21 415.78 134.68 o 2 13 1 11196.68 10536.49 253.02 o 3 13 1 1509.99 1276.00 274.21 o 4 13 1 6947.87 6799.36 370.54 o 5 13 1 492.83 663.37 274.21 o 6 13 1 8826.13 8469.02 416.13 o 7 13 1 91.98 19.27 291.55 o 8 13 1 1665.04 1987.54 357.05 o -8 14 1 2522.63 2548.16 382.09 o -7 14 1 2792.39 3386.20 369.89 o -6 14 1 3073.89 3401.61 349.34 o -5 14 1 12663.67 11831.46 466.22 o -4 14 1 2534.17 3508.85 326.23 o -3 14 1 8158.77 8526.82 394.94 o -2 14 1 6066.30 6192.98 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