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Information card for entry 2012330
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| Coordinates | 2012330.cif |
|---|---|
| Structure factors | 2012330.hkl |
| Original IUCr paper | HTML |
| Chemical name | [6-carbonyl-6,6-bis(triphenylphosphine)-nido-6-osmadecaborane(13)] |
|---|---|
| Formula | C37 H43 B9 O Os P2 |
| Calculated formula | C37 H41 B9 O Os P2 |
| Title of publication | The <i>nido</i>‒osmaboranes [2,2,2-(CO)(PPh~3~)~2~-<i>nido</i>-2-OsB~5~H~9~] and [6,6,6-(CO)(PPh~3~)~2~-<i>nido</i>-6-OsB~9~H~13~] |
| Authors of publication | Bould, Jonathan; Kennedy, John D.; Thomas, Rhodri Ll.; Rath, Nigam P.; Barton, Lawrence |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2001 |
| Journal volume | 57 |
| Journal issue | 11 |
| Pages of publication | 1245 - 1247 |
| a | 10.4617 ± 0.0001 Å |
| b | 15.6821 ± 0.0001 Å |
| c | 22.6315 ± 0.0003 Å |
| α | 90° |
| β | 91.08 ± 0.01° |
| γ | 90° |
| Cell volume | 3712.3 ± 0.07 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.084 |
| Residual factor for significantly intense reflections | 0.057 |
| Weighted residual factors for all reflections included in the refinement | 0.116 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.179 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
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