Crystallography Open Database

Information card for entry 2012593

2012592 << 2012593 >> 2012594

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Structure parameters

Chemical name	tri-μ-carbonyl-1:3κ^2^C;1:4κ^2^C;3:4κ^2^C-heptacarbonyl- 1κC,2κ^2^C,3κ^2^C,4κ^2^C-bis[1,2(η^5^)-tetramethylcyclopentadienyl]- tetrahedro-diiridiumdimolybdenum dichloromethane hemisolvate
Formula	C28.5 H27 Cl Ir2 Mo2 O10
Calculated formula	C28 H26 Cl Ir2 Mo2 O10
Title of publication	Decacarbonylbis(methylcyclopentadienyl)-<i>tetrahedro</i>-diiridiumdimolybdenum and decacarbonylbis(tetramethylcyclopentadienyl)-<i>tetrahedro</i>-diiridiumdimolybdenum dichloromethane hemisolvate
Authors of publication	Lucas, Nigel T.; Humphrey, Mark G.
Journal of publication	Acta Crystallographica Section C
Year of publication	2002
Journal volume	58
Journal issue	3
Pages of publication	m171 - m173
a	38.199 ± 0.004 Å
b	36.135 ± 0.005 Å
c	9.303 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	12841 ± 6 Å³
Cell temperature	296.2 K
Ambient diffraction temperature	296.2 K
Number of distinct elements	6
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.046
Residual factor for significantly intense reflections	0.023
Weighted residual factors for all reflections	0.026
Weighted residual factors for all reflections included in the refinement	0.023
Goodness-of-fit parameter for all reflections	0.79
Goodness-of-fit parameter for all reflections included in the refinement	0.82
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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