Crystallography Open Database

Information card for entry 2013048

2013047 << 2013048 >> 2013049

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Coordinates	2013048.cif
Structure factors	2013048.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	(R)-di-μ-acetato-κ^2^O:O'-bis{[2-(1-aminoethyl)phenyl- κ^2^C^1^,N]palladium(II)}
Formula	C20 H26 N2 O4 Pd2
Calculated formula	C20 H26 N2 O4 Pd2
SMILES	[Pd]13(OC(C)=[O][Pd]4(OC(=[O]1)C)c1ccccc1[C@@H](C)[NH2]4)c1ccccc1[C@@H](C)[NH2]3
Title of publication	(<i>R</i>)-Di-μ-acetato-κ^2^<i>O</i>:<i>O</i>'-bis{[2-(1-aminoethyl)phenyl-κ^2^<i>C</i>^1^,<i>N</i>]palladium(II)}, (<i>R</i>)-di-μ-chloro-bis{[2-(1-aminoethyl)phenyl-κ^2^<i>C</i>^1^,<i>N</i>]palladium(II)} and [<i>SP</i>-4-4]-(<i>R</i>)-[2-(1-aminoethyl)phenyl-κ^2^<i>C</i>^1^,<i>N</i>]chloro(pyridine-κ<i>N</i>)palladium(II)
Authors of publication	Calmuschi, Beatrice; Englert, Ulli
Journal of publication	Acta Crystallographica Section C
Year of publication	2002
Journal volume	58
Journal issue	11
Pages of publication	m545 - m548
a	10.423 ± 0.004 Å
b	13.398 ± 0.005 Å
c	15.861 ± 0.005 Å
α	90°
β	93.429 ± 0.009°
γ	90°
Cell volume	2211 ± 1.4 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.105
Residual factor for significantly intense reflections	0.065
Weighted residual factors for significantly intense reflections	0.155
Weighted residual factors for all reflections included in the refinement	0.177
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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