#------------------------------------------------------------------------------ #$Date: 2025-05-21 03:05:01 +0100 (Wed, 21 May 2025) $ #$Revision: 299763 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/35/2023513.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023513 loop_ _publ_author_name 'Guseinov, Firudin I.' 'H\"okelek, Tuncer' 'Afanaseva, Ksenia A.' 'Shuvalova, Elena V.' 'Glukhov, Lev M.' 'Samigullina, Aida I.' 'Belay, Alebel N.' _publ_section_title ; Syntheses and structures of 1-[2,2-dichloro-1-hydroxy-3-(4-methylphenyl)-3-oxopropyl]urea and 1-[2,2-dichloro-3-(4-fluorophenyl)-1-hydroxy-3-oxopropyl]urea ; _journal_coeditor_code HB8127 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989025004359 _journal_volume 81 _journal_year 2025 _chemical_formula_iupac 'C11 H12 Cl2 N2 O3' _chemical_formula_moiety 'C11 H12 Cl2 N2 O3' _chemical_formula_sum 'C11 H12 Cl2 N2 O3' _chemical_formula_weight 291.13 _chemical_name_systematic ; 1-[2,2-Dichloro-3-(4-fluorophenyl)-1-hydroxy-3-oxopropyl]urea ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method ; Olex2 1.3 (compiled 2019.09.11 svn.r3662 for OlexSys, GUI svn.r5938) ; _cell_angle_alpha 90 _cell_angle_beta 94.8294(9) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.62183(13) _cell_length_b 8.77585(9) _cell_length_c 11.59930(11) _cell_measurement_reflns_used 11708 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 80.3330 _cell_measurement_theta_min 3.5200 _cell_volume 1280.26(2) _computing_cell_refinement ; CrysAlisPro 1.171.43.143a (Rigaku OD, 2024) ; _computing_data_collection 'CrysAlisPro system (CCD 43.143a 64-bit (release 25-10-2024))' _computing_data_reduction ; CrysAlisPro 1.171.43.143a (Rigaku OD, 2024) ; _computing_molecular_graphics ; Olex2 1.3 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 1.3 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0500 _diffrn_reflns_av_unetI/netI 0.0297 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 17344 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 80.733 _diffrn_reflns_theta_min 3.514 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 4.604 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.277 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2024) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.510 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 600 _exptl_crystal_size_max 0.45 _exptl_crystal_size_mid 0.35 _exptl_crystal_size_min 0.16 _refine_diff_density_max 0.509 _refine_diff_density_min -0.426 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 180 _refine_ls_number_reflns 2808 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.055 _refine_ls_R_factor_all 0.0374 _refine_ls_R_factor_gt 0.0368 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0655P)^2^+0.6302P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1031 _refine_ls_wR_factor_ref 0.1038 _reflns_number_gt 2738 _reflns_number_total 2808 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8127.cif _cod_data_source_block II _cod_database_code 2023513 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.231 _shelx_estimated_absorpt_t_max 0.526 _shelx_hkl_file ; 0 0 -1 2.51 0.47 0 0 2 1144.06 45.10 0 0 -2 1179.40 44.93 0 0 3 0.16 0.55 0 0 -3 0.41 0.47 0 0 4 4099.26 158.08 0 0 -4 4210.84 157.46 0 0 5 1.08 0.98 0 0 -5 1.08 0.97 0 0 -5 0.22 0.37 0 0 6 162.27 10.71 0 0 -6 150.55 13.14 0 0 -6 157.80 9.70 0 0 -6 148.17 11.65 0 0 -7 0.16 0.52 0 0 -7 -0.66 0.80 0 0 7 1.16 1.23 0 0 -7 1.09 1.14 0 0 8 105.38 9.54 0 0 -8 121.58 7.28 0 0 -8 109.02 12.12 0 0 -9 0.84 1.01 0 0 -9 0.41 0.85 0 0 -9 1.15 0.79 0 0 -9 1.13 1.20 0 0 -9 0.60 1.14 0 0 -10 573.07 27.14 0 0 -10 556.72 26.67 0 0 -10 583.89 25.26 0 0 -10 565.93 34.77 0 0 -11 1.24 0.90 0 0 -11 1.15 0.92 0 0 -11 0.32 1.17 0 0 -12 13.15 2.33 0 0 -12 13.23 2.07 0 0 -12 13.37 2.12 0 0 12 17.96 2.68 0 0 -13 0.14 0.58 0 0 -13 0.27 0.54 0 0 13 -0.15 0.82 0 0 -13 1.70 0.83 0 0 -14 215.64 9.68 0 0 -14 224.27 9.71 0 0 -14 233.20 9.66 0 0 14 197.02 8.97 0 -1 0 1.93 0.53 0 -1 1 1212.26 46.98 0 1 1 1242.29 47.64 0 1 -2 2832.42 112.20 0 1 2 3031.52 111.60 0 1 3 987.48 40.66 0 1 -3 1047.08 42.18 0 -1 -3 1005.28 38.57 0 1 4 1195.93 49.61 0 1 -4 1218.84 51.65 0 -1 -4 1208.22 47.18 0 1 -4 1341.36 51.82 0 1 5 595.86 27.31 0 1 -5 613.34 29.38 0 1 -5 672.31 28.98 0 -1 -5 578.83 24.52 0 1 6 1294.89 56.22 0 -1 6 1334.53 56.68 0 1 -6 1326.23 58.90 0 -1 -6 1325.35 59.57 0 1 -6 1433.72 57.37 0 1 -6 1420.44 62.22 0 1 7 160.32 11.59 0 -1 7 155.67 11.58 0 1 -7 169.98 15.05 0 -1 -7 146.59 13.07 0 1 -7 177.90 12.05 0 1 -7 143.04 12.85 0 1 -7 165.89 9.08 0 -1 -7 163.92 8.56 0 -1 8 46.14 6.09 0 1 8 48.81 6.15 0 1 -8 50.01 7.43 0 -1 -8 39.89 6.94 0 1 -8 53.15 8.52 0 -1 -8 48.64 4.08 0 1 -8 55.48 4.57 0 1 -9 1.25 1.00 0 -1 -9 1.85 1.00 0 -1 -9 0.81 1.20 0 -1 -9 3.04 2.06 0 1 -9 1.79 1.87 0 1 -9 1.03 0.94 0 1 -9 3.95 1.33 0 -1 -9 2.22 0.98 0 -1 -9 2.26 1.46 0 1 -9 1.95 1.30 0 -1 10 137.18 9.06 0 1 10 153.13 8.73 0 -1 -10 162.78 11.87 0 1 -10 148.98 9.71 0 1 -10 154.22 8.66 0 1 -10 144.98 8.42 0 1 -10 153.67 15.84 0 -1 -10 148.35 14.71 0 1 -10 152.44 9.18 0 -1 -10 155.18 8.82 0 1 -10 149.77 10.05 0 -1 -10 151.76 10.60 0 1 -11 7.40 1.47 0 1 -11 6.80 1.69 0 -1 -11 7.50 1.67 0 1 -11 7.16 1.45 0 -1 11 8.01 1.80 0 1 11 8.42 1.85 0 -1 -11 4.67 1.86 0 1 -11 5.03 1.58 0 1 -12 6.78 1.66 0 -1 -12 5.73 1.67 0 -1 -12 5.63 1.33 0 1 -12 5.27 1.38 0 -1 -12 5.82 1.38 0 1 -12 6.90 1.59 0 -1 -12 5.82 1.84 0 -1 12 4.59 1.36 0 1 12 4.01 1.38 0 -1 13 126.11 6.84 0 1 13 122.75 7.16 0 -1 -13 116.79 7.02 0 -1 -13 133.67 6.96 0 1 -13 129.38 7.00 0 1 -13 125.95 7.12 0 -1 -13 120.71 6.65 0 1 -13 121.55 7.19 0 1 -14 212.13 9.44 0 -1 -14 219.59 9.96 0 -1 14 218.95 9.24 0 1 14 232.07 9.51 0 -2 0 1719.58 66.97 0 -2 1 8.24 1.50 0 -2 -1 11.77 1.22 0 2 -1 8.64 1.00 0 -2 1 11.04 1.74 0 -2 2 2836.91 110.65 0 -2 -2 2968.00 111.67 0 2 -3 806.77 35.00 0 2 3 763.26 33.32 0 2 -4 6.85 2.06 0 2 -4 5.63 1.88 0 2 -4 4.93 1.96 0 -2 -4 4.82 1.64 0 2 4 5.38 1.67 0 2 -5 140.14 11.01 0 2 -5 152.56 11.87 0 2 -5 126.02 11.04 0 -2 -5 136.62 10.32 0 2 5 122.34 9.21 0 2 -6 249.32 16.77 0 2 -6 244.89 17.53 0 2 -6 270.92 17.07 0 -2 -6 218.58 15.10 0 2 6 214.35 14.07 0 2 -7 1138.99 55.69 0 -2 -7 1171.25 53.11 0 2 -7 1191.65 53.24 0 2 -7 1152.59 54.09 0 -2 7 1114.37 51.20 0 2 7 1109.55 50.65 0 2 -7 1186.23 46.54 0 -2 -7 1162.49 45.56 0 2 -8 255.17 20.33 0 -2 -8 266.67 18.89 0 2 -8 246.24 17.56 0 -2 8 277.66 17.43 0 2 8 231.85 16.31 0 -2 -8 262.06 12.43 0 2 -8 272.53 13.37 0 2 -8 268.81 19.71 0 -2 -9 7.28 2.25 0 -2 -9 9.71 3.57 0 2 -9 7.24 3.29 0 -2 -9 9.09 3.25 0 2 -9 14.14 4.15 0 -2 -9 7.03 1.98 0 -2 -9 13.11 3.12 0 2 -9 10.10 2.01 0 -2 -9 10.10 1.78 0 2 -9 10.74 2.01 0 2 -9 11.96 2.17 0 -2 9 8.69 1.81 0 2 -9 9.68 2.03 0 -2 -9 7.95 1.66 0 -2 -10 1.34 1.40 0 2 -10 0.82 1.40 0 -2 -10 0.44 1.18 0 -2 -10 1.14 1.20 0 2 -10 0.75 1.00 0 -2 -10 7.50 1.49 0 2 -10 1.92 1.00 0 2 -10 2.30 1.18 0 -2 -10 1.38 1.50 0 2 -10 6.58 3.40 0 -2 -10 1.45 1.52 0 2 -10 1.04 0.87 0 2 10 0.58 1.19 0 -2 10 0.43 0.68 0 2 11 98.47 6.55 0 -2 11 98.46 6.62 0 2 -11 96.81 6.74 0 -2 -11 94.11 6.14 0 -2 -11 104.03 8.96 0 2 -11 110.65 7.34 0 2 -11 98.56 6.45 0 -2 -11 101.20 6.40 0 2 -11 99.01 6.99 0 2 -11 98.77 6.41 0 -2 -11 91.06 7.73 0 -2 -12 281.16 15.17 0 2 12 301.06 13.75 0 -2 -12 261.98 14.49 0 2 -12 300.64 13.46 0 2 -12 278.55 14.13 0 -2 12 296.92 13.78 0 -2 -12 287.70 13.51 0 -2 -12 293.64 13.37 0 2 -12 293.60 14.24 0 2 -12 298.72 14.09 0 2 -12 303.65 13.44 0 -2 13 38.83 2.99 0 2 13 39.73 3.37 0 -2 13 41.19 2.87 0 -2 -13 37.90 2.81 0 2 -13 34.26 2.98 0 2 -13 35.97 3.10 0 -2 -13 39.60 2.97 0 2 -13 32.27 2.86 0 2 13 38.09 2.92 0 -2 -13 42.33 3.35 0 2 14 18.38 1.50 0 -3 0 0.59 0.71 0 -3 0 2.48 1.20 0 -3 1 906.57 38.80 0 -3 -1 955.60 39.39 0 -3 1 864.97 38.18 0 -3 -2 760.61 30.32 0 3 -2 677.65 29.80 0 -3 -2 961.67 35.10 0 -3 2 853.23 33.80 0 3 -3 661.50 29.01 0 -3 -3 669.64 28.94 0 -3 -3 730.26 31.72 0 -3 3 693.29 30.90 0 3 -4 29.63 3.86 0 -3 -4 20.48 3.11 0 -3 -4 28.75 4.21 0 3 -4 25.07 4.45 0 3 -5 119.88 12.27 0 3 -5 110.32 9.21 0 -3 -5 106.47 8.70 0 3 -5 118.72 10.91 0 3 -6 236.62 11.05 0 -3 -6 206.28 14.46 0 3 -6 220.34 15.81 0 3 -6 249.13 17.77 0 3 -7 402.96 17.50 0 -3 -7 400.82 16.84 0 -3 -7 387.63 23.39 0 3 -7 359.33 24.40 0 3 -7 340.02 23.11 0 3 -7 425.70 26.28 0 -3 -7 363.94 22.05 0 -3 -8 787.06 42.93 0 3 -8 971.96 47.55 0 3 -8 862.48 46.14 0 3 -8 1002.39 38.99 0 3 -8 967.61 38.72 0 -3 -8 883.49 36.72 0 3 -8 941.32 37.72 0 3 -8 981.60 48.25 0 -3 -8 842.45 44.44 0 -3 -9 3.22 1.83 0 3 -9 3.23 2.18 0 -3 -9 6.25 2.62 0 -3 9 4.73 1.29 0 3 -9 6.67 3.02 0 -3 -9 5.50 2.50 0 -3 -9 2.77 1.39 0 -3 -9 4.55 1.94 0 3 -9 6.12 1.64 0 3 -9 5.86 1.49 0 3 -9 4.85 1.56 0 -3 -9 3.31 1.02 0 3 -9 5.16 1.46 0 3 -9 4.81 1.50 0 3 -10 159.72 9.24 0 -3 -10 150.39 8.41 0 3 -10 169.43 9.49 0 -3 -10 176.10 12.21 0 -3 -10 135.09 9.69 0 3 -10 172.24 9.82 0 -3 -10 169.13 8.80 0 3 -10 161.76 9.47 0 3 -10 178.91 9.99 0 -3 10 158.21 8.90 0 3 10 150.67 9.06 0 -3 -10 156.07 10.71 0 -3 -11 59.57 4.24 0 3 -11 60.86 4.85 0 3 -11 58.29 4.71 0 3 -11 56.33 4.65 0 -3 -11 61.08 5.33 0 -3 -11 73.29 7.07 0 3 -11 65.67 5.08 0 -3 -11 61.81 4.47 0 -3 -11 57.91 5.75 0 3 11 67.89 5.10 0 -3 11 59.91 4.51 0 3 -11 66.42 5.15 0 -3 -12 64.09 4.16 0 -3 -12 60.22 4.00 0 3 -12 66.05 4.56 0 3 -12 61.00 4.39 0 -3 -12 62.16 5.99 0 3 -12 80.06 4.88 0 -3 12 62.45 4.36 0 -3 12 62.06 4.15 0 3 12 67.73 4.70 0 -3 -12 62.20 5.32 0 3 -12 61.24 4.46 0 -3 13 145.45 6.56 0 -3 -13 129.02 6.45 0 3 -13 129.97 6.40 0 -3 -13 145.54 7.65 0 3 13 149.08 6.99 0 -3 -13 135.28 6.99 0 3 14 0.74 0.29 0 -4 0 63.41 6.86 0 -4 0 62.73 6.62 0 -4 1 137.47 10.82 0 -4 1 140.66 10.63 0 -4 -1 161.66 11.34 0 -4 2 63.69 6.86 0 -4 -2 85.07 7.68 0 -4 -3 1.24 1.11 0 -4 3 1.67 1.34 0 4 -4 236.61 17.27 0 -4 -4 227.12 14.88 0 4 -4 196.18 11.36 0 -4 -5 116.06 10.31 0 4 -5 129.09 12.55 0 4 -5 103.55 8.14 0 4 -6 350.25 23.64 0 4 -6 277.55 17.63 0 4 -7 18.25 5.03 0 4 -7 21.02 5.54 0 4 -7 10.76 3.00 0 -4 -8 1062.56 49.77 0 4 -8 1149.50 47.60 0 4 -8 1468.42 63.50 0 4 -8 1349.69 50.04 0 4 -8 1262.32 48.58 0 -4 -8 1196.09 51.82 0 4 -8 1148.99 47.53 0 4 -8 1335.52 49.86 0 4 -8 1263.08 60.85 0 -4 -8 1187.51 57.01 0 -4 9 2.03 0.92 0 -4 -9 2.14 1.25 0 -4 -9 8.67 2.61 0 4 -9 4.31 2.55 0 4 -9 1.82 0.96 0 -4 -9 3.99 1.74 0 -4 -9 3.62 2.14 0 4 -9 4.38 2.59 0 4 -9 1.56 0.71 0 4 -9 2.03 0.89 0 4 -10 462.81 21.19 0 4 -10 527.19 21.89 0 -4 -10 484.31 23.77 0 -4 10 515.14 21.63 0 4 10 522.09 22.25 0 -4 -10 473.09 22.98 0 -4 -10 524.25 25.52 0 -4 -11 18.10 2.71 0 -4 -11 24.57 3.78 0 4 -11 27.17 3.03 0 4 -11 24.08 2.49 0 -4 -11 26.69 3.49 0 4 -11 26.80 3.03 0 -4 11 22.73 2.41 0 4 11 21.79 2.84 0 -4 12 200.91 9.53 0 4 -12 234.01 10.56 0 4 12 202.71 10.15 0 -4 -12 204.86 11.02 0 4 -12 221.42 10.47 0 -4 -12 219.52 12.06 0 4 -13 60.95 3.39 0 4 -13 62.33 3.44 0 -4 -13 58.37 3.66 0 4 13 57.91 3.41 0 -5 0 -0.58 1.21 0 -5 0 -0.55 0.95 0 -5 1 544.93 29.87 0 -5 1 549.40 30.48 0 -5 -1 612.43 30.76 0 -5 -1 556.08 30.34 0 -5 -2 171.24 13.32 0 -5 2 173.75 13.93 0 -5 -2 181.23 13.91 0 -5 3 71.87 8.27 0 -5 -3 73.95 7.90 0 5 3 50.98 3.54 0 5 -3 65.27 9.59 0 -5 -4 274.46 17.46 0 5 -4 244.02 19.86 0 5 4 226.27 10.42 0 -5 -5 920.56 46.93 0 5 -5 1008.28 52.23 0 -5 -6 138.63 12.99 0 5 -6 147.31 15.77 0 -5 -6 154.58 10.17 0 -5 -7 109.15 8.58 0 5 -7 119.56 7.61 0 5 -7 124.43 7.64 0 5 -7 140.41 15.80 0 -5 7 111.47 6.55 0 5 -7 123.83 14.08 0 -5 -7 110.05 11.70 0 -5 -7 95.76 7.49 0 -5 -7 106.85 7.58 0 -5 -8 426.86 21.91 0 5 -8 454.65 20.06 0 5 -8 455.19 19.95 0 5 -8 483.53 31.95 0 -5 8 399.62 18.36 0 5 -8 433.77 29.52 0 -5 -8 372.01 20.13 0 5 -9 1089.39 40.13 0 5 -9 1083.32 40.25 0 -5 9 927.95 38.12 0 5 9 933.99 38.87 0 -5 -9 858.30 39.67 0 -5 -9 969.67 42.21 0 -5 -9 859.00 40.17 0 5 -10 11.34 2.08 0 -5 10 14.87 1.85 0 5 -10 14.03 2.32 0 -5 -10 14.30 2.59 0 -5 -10 12.14 2.28 0 -5 -10 13.64 2.86 0 -5 -11 4.90 1.57 0 -5 11 3.87 0.87 0 5 11 5.64 1.51 0 -5 -11 3.48 1.49 0 -5 -11 3.69 1.17 0 -5 -12 12.96 2.08 0 5 12 14.59 1.78 0 -5 -12 13.26 1.86 0 5 13 23.26 1.70 0 5 -13 25.89 1.74 0 5 -13 26.00 1.74 0 6 0 49.18 6.79 0 -6 0 74.74 9.39 0 -6 0 76.28 9.75 0 6 1 22.06 4.15 0 6 -1 21.09 4.77 0 -6 -1 41.29 6.79 0 -6 -1 37.45 6.59 0 -6 1 36.01 6.69 0 6 -2 62.97 8.95 0 -6 -2 59.96 8.28 0 -6 -2 79.77 9.25 0 -6 2 56.91 8.59 0 6 -3 56.08 8.86 0 -6 -3 43.16 7.12 0 -6 3 68.22 9.01 0 -6 -3 60.81 8.00 0 -6 -4 -0.70 0.85 0 -6 -4 -0.67 0.81 0 6 -4 2.07 2.17 0 6 -4 1.88 1.97 0 6 5 34.68 3.16 0 6 -5 32.69 3.08 0 6 -5 31.37 2.97 0 6 -5 27.53 6.87 0 -6 -5 28.66 5.66 0 -6 -5 23.45 5.51 0 -6 -5 33.24 3.61 0 -6 -5 29.78 3.38 0 -6 -5 32.27 3.51 0 -6 5 32.64 2.94 0 6 6 2.12 0.99 0 -6 -6 2.10 1.26 0 6 -6 2.40 1.02 0 6 -6 1.00 0.76 0 6 -6 -1.11 1.34 0 -6 6 2.31 0.82 0 -6 -6 3.67 2.17 0 6 -6 5.29 2.86 0 -6 -6 4.04 1.41 0 -6 -6 1.85 1.15 0 -6 -7 78.90 6.43 0 -6 -7 73.59 6.10 0 -6 -7 85.00 7.30 0 6 -7 87.20 5.94 0 6 -7 92.04 6.13 0 -6 7 88.22 5.44 0 6 7 84.44 5.74 0 -6 -8 82.17 6.34 0 -6 -8 82.32 7.06 0 6 -8 75.71 5.52 0 6 -8 75.81 5.53 0 6 8 66.69 5.14 0 -6 8 71.03 4.77 0 -6 -9 61.19 5.40 0 -6 -9 63.36 6.12 0 6 -9 61.57 4.79 0 6 -9 73.04 5.12 0 6 9 60.86 4.70 0 -6 9 65.10 4.23 0 6 10 120.89 6.90 0 -6 -10 115.74 7.54 0 -6 -10 127.72 8.57 0 -6 -10 109.97 7.11 0 6 -10 131.09 7.18 0 6 -10 133.93 7.31 0 -6 10 121.71 6.16 0 6 -11 29.94 2.58 0 6 11 26.56 2.49 0 -6 -11 25.48 2.66 0 6 -11 30.74 2.65 0 -6 -11 25.53 3.05 0 6 -12 27.01 1.99 0 6 -12 25.13 1.95 0 7 0 0.53 0.91 0 7 0 0.26 1.12 0 -7 0 0.15 0.67 0 -7 -1 395.81 25.63 0 -7 1 360.38 25.90 0 -7 -1 397.15 26.14 0 7 -1 327.97 14.86 0 -7 -1 362.07 15.68 0 -7 1 340.54 15.35 0 7 2 953.40 39.11 0 7 2 940.99 39.11 0 -7 2 970.10 38.49 0 -7 -2 1012.54 39.17 0 -7 -2 1069.08 50.62 0 -7 -2 1076.10 51.39 0 7 -2 963.52 38.01 0 7 3 48.60 4.41 0 7 3 49.66 4.43 0 7 -3 52.95 3.89 0 7 -3 35.13 7.40 0 -7 3 52.91 4.05 0 -7 -3 61.68 4.69 0 -7 -3 58.81 8.87 0 -7 -3 62.44 8.85 0 7 4 212.28 10.66 0 7 -4 196.87 9.77 0 -7 -4 201.49 17.61 0 7 -4 169.88 18.06 0 -7 4 205.62 10.20 0 -7 -4 213.37 11.20 0 -7 -4 205.67 17.45 0 7 -4 218.33 21.28 0 7 -5 171.59 18.92 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10.17 5 6 5 155.40 9.46 5 6 5 179.77 10.77 5 6 5 149.14 9.34 5 6 5 149.03 9.29 -5 6 -6 17.78 2.67 5 -6 6 28.48 2.89 5 -6 6 23.73 2.74 5 6 6 33.42 3.78 -5 6 -6 19.62 2.80 -5 -6 -6 27.98 3.61 5 6 6 24.32 2.53 5 6 7 8.62 1.55 -5 6 -7 10.18 1.93 5 -6 7 11.22 1.77 5 -6 7 10.39 1.70 -5 -6 -7 10.72 2.32 -5 -6 -7 8.68 2.07 -5 6 -7 6.51 1.66 5 6 7 11.08 2.14 5 6 8 20.94 2.10 -5 6 -8 20.25 2.52 5 -6 8 21.60 2.35 -5 -6 -8 23.25 3.10 -5 -6 -8 25.54 3.24 -5 6 -8 18.25 2.46 5 6 9 258.58 11.47 -5 -6 -9 293.27 13.66 -5 -6 -9 306.62 13.75 -5 6 -9 250.70 12.40 -5 6 -9 273.05 12.51 5 -6 9 276.17 12.17 5 -6 10 14.40 1.50 5 -6 10 15.25 1.55 -5 -6 -10 17.74 2.08 -5 6 -10 15.11 1.69 -5 -6 -10 21.07 2.19 -5 6 -10 14.82 1.71 -5 6 -11 0.73 0.34 -5 6 -11 1.04 0.37 -5 -6 -11 0.26 0.31 5 -6 11 0.13 0.31 5 -6 11 0.39 0.34 5 -6 11 0.29 0.23 5 7 -10 43.49 2.67 5 7 -10 46.54 2.79 5 7 -10 43.79 2.75 5 7 -10 42.01 2.70 5 7 -9 33.56 2.66 5 7 -9 34.57 2.71 5 7 -9 38.43 2.80 5 7 -8 77.01 4.68 5 7 -8 78.72 4.71 5 7 -8 68.03 4.62 5 -7 -8 67.00 5.63 5 7 -8 68.90 5.22 5 7 -7 14.64 1.91 5 7 -7 17.18 2.02 5 7 -7 18.94 2.25 5 -7 -7 17.12 2.89 5 7 -7 11.28 2.39 5 7 -6 279.46 12.47 5 7 -6 283.50 12.54 5 7 -6 276.32 13.08 5 7 -6 237.52 14.55 5 -7 -6 239.88 14.15 5 7 -5 88.46 5.17 5 7 -5 84.57 5.76 5 -7 -5 75.75 6.45 5 7 -5 83.39 5.09 5 -7 -5 75.14 5.24 5 -7 -5 78.28 5.67 5 -7 -4 20.24 2.57 5 -7 -4 21.22 2.71 -5 7 4 21.52 2.32 5 -7 -4 17.81 2.90 5 7 -4 21.54 2.64 5 -7 -4 17.15 2.27 5 -7 -4 17.14 2.44 5 7 -4 19.63 3.56 -5 7 3 -0.12 1.33 5 7 -3 0.19 0.73 5 7 -3 0.20 0.69 5 -7 -3 -0.71 0.77 5 7 -3 -0.62 1.41 5 -7 -3 -0.18 0.85 5 -7 -3 1.21 1.12 -5 7 2 57.23 4.22 5 7 -2 46.90 4.68 5 7 -2 52.36 4.57 5 7 -2 53.63 5.64 5 -7 -2 60.69 4.56 5 -7 -2 53.44 4.34 5 7 -2 66.68 6.06 5 7 -2 56.73 4.77 5 -7 -2 58.05 4.51 5 -7 -1 243.80 12.30 -5 7 1 241.29 11.83 5 7 -1 252.34 13.31 5 -7 -1 267.31 23.82 5 7 -1 231.79 14.64 5 -7 -1 259.96 12.36 5 -7 -1 251.45 12.33 5 7 -1 256.26 13.81 5 7 -1 261.75 12.94 5 7 -1 248.85 12.76 5 -7 0 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13.58 5 -8 -4 277.72 13.25 5 8 -4 307.06 13.94 -5 8 3 87.85 5.25 5 -8 -3 82.10 5.58 5 -8 -3 83.05 5.58 5 -8 -3 84.48 5.71 5 8 -3 87.93 5.96 5 8 -3 85.12 6.70 5 8 -3 84.78 5.82 -5 8 2 232.65 11.14 5 8 -2 246.72 12.23 5 -8 -2 231.96 11.62 5 -8 -2 236.15 11.61 5 -8 -2 237.10 11.76 5 8 -2 231.17 11.98 5 8 -2 253.36 13.10 -5 8 1 28.67 2.91 5 8 -1 23.72 3.03 5 8 -1 20.10 2.71 5 8 -1 28.69 3.92 5 -8 -1 20.50 2.58 5 -8 -1 24.43 2.74 5 -8 -1 27.01 2.85 5 8 -1 22.31 2.80 5 8 -1 23.34 3.04 5 8 0 50.89 4.29 5 8 0 51.37 4.45 5 8 0 59.46 5.82 5 -8 0 54.48 4.22 5 -8 0 60.02 4.36 5 8 0 48.00 4.37 5 8 0 54.15 4.52 -5 8 0 56.73 4.20 5 8 0 59.73 4.93 5 8 1 190.38 9.81 5 8 1 186.36 10.07 5 8 1 179.08 10.12 5 8 1 188.25 11.69 5 8 1 168.80 9.95 -5 -8 -1 190.32 9.97 5 -8 1 188.69 9.63 5 -8 1 183.66 9.56 5 8 1 200.74 10.61 5 -8 2 120.66 6.81 5 -8 2 120.41 6.81 5 -8 2 120.74 6.99 5 8 2 93.16 6.66 5 8 2 109.11 7.21 5 8 2 120.87 6.89 -5 8 -2 115.36 6.55 5 8 2 114.32 7.43 5 -8 2 109.11 6.75 5 8 2 104.60 7.07 -5 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1.17 9 5 7 8.89 1.63 9 5 8 30.98 2.36 -9 5 -8 22.02 2.31 -9 5 -8 18.14 2.20 9 5 8 31.01 2.20 9 -5 8 29.46 2.29 9 5 8 33.13 2.72 9 5 8 28.05 2.37 -9 5 -9 0.84 0.49 9 5 9 1.95 0.65 9 5 9 1.12 0.45 9 -5 9 1.14 0.46 -9 5 -9 0.58 0.50 9 6 -10 6.22 0.71 9 6 -10 6.88 0.73 9 -6 -10 4.58 0.62 9 -6 -9 2.09 0.76 9 6 -9 2.28 0.62 9 6 -9 2.24 0.66 9 -6 -8 15.35 1.60 9 6 -8 18.32 1.94 9 6 -8 18.79 1.97 9 6 -8 16.43 1.81 9 6 -8 20.86 2.07 9 6 -8 19.27 2.26 9 -6 -8 12.83 1.52 9 -6 -7 54.73 3.79 9 6 -7 57.33 3.97 9 -6 -7 54.22 4.91 9 6 -7 60.57 4.07 9 6 -7 54.69 3.91 9 6 -7 54.63 3.99 9 -6 -7 47.67 3.79 9 6 -7 51.69 4.58 9 6 -6 32.61 2.88 9 6 -6 27.69 2.68 9 6 -6 24.64 2.59 9 6 -6 26.02 2.72 9 -6 -6 23.06 2.75 9 -6 -6 26.92 3.62 9 6 -5 12.86 1.92 9 6 -5 14.58 2.06 9 6 -5 13.32 1.87 9 6 -5 16.09 2.03 9 -6 -5 13.77 2.71 9 6 -5 12.78 2.72 9 6 -5 13.24 2.51 9 6 -4 0.57 1.42 9 -6 -4 0.31 1.04 9 6 -4 0.16 0.59 9 6 -4 -0.17 0.65 9 6 -4 0.22 1.00 9 -6 -4 0.85 1.02 9 -6 -4 1.37 1.11 9 6 -4 0.30 1.21 9 6 -3 0.71 1.48 9 -6 -3 0.52 0.57 9 -6 -3 0.17 1.05 9 -6 -3 1.18 0.91 9 6 -3 0.70 1.09 9 -6 -3 0.59 0.87 9 6 -3 1.09 1.18 9 6 -3 1.69 0.84 9 6 -3 2.98 1.10 9 6 -2 97.69 6.29 9 6 -2 90.68 6.81 9 6 -2 97.62 6.25 9 -6 -2 93.21 6.11 9 -6 -2 91.24 6.04 9 6 -2 101.97 7.14 9 6 -1 561.00 23.10 9 -6 -1 465.14 21.18 9 6 -1 496.27 22.08 9 -6 -1 509.39 21.92 9 -6 -1 522.57 21.95 9 6 -1 516.26 22.26 9 6 -1 514.60 23.20 9 6 0 28.06 3.08 9 6 0 29.74 3.54 9 -6 0 33.92 2.91 9 6 0 24.57 2.89 9 6 0 31.25 3.11 9 -6 0 28.98 3.03 9 -6 0 33.57 3.18 9 6 1 57.35 4.65 9 -6 1 60.41 4.22 9 -6 1 61.44 4.54 9 -6 1 64.80 4.59 9 -6 1 60.51 4.39 9 6 1 66.30 4.76 9 6 1 57.62 4.66 9 6 2 1.05 0.79 9 6 2 1.76 0.82 9 6 2 0.99 0.82 9 -6 2 1.61 0.81 9 -6 2 0.90 0.83 9 -6 2 0.52 0.63 9 -6 2 0.15 0.87 9 6 2 -0.15 0.87 9 -6 3 411.73 17.45 9 -6 3 407.10 17.46 9 -6 3 424.35 17.56 9 6 3 379.36 17.71 9 6 3 364.70 17.63 9 6 3 395.89 17.26 9 -6 3 395.51 17.05 9 6 3 380.44 17.46 9 6 4 3.97 1.16 9 -6 4 4.56 1.22 9 -6 4 4.07 1.22 9 -6 4 5.32 1.18 9 -6 4 5.32 1.36 9 -6 5 38.96 2.98 9 -6 5 38.60 3.16 9 -6 5 43.02 3.25 9 -6 5 43.52 3.27 9 -6 6 8.51 1.33 9 -6 6 6.36 1.17 9 -6 6 6.95 1.11 9 -6 6 6.97 1.22 -9 6 -6 4.41 1.05 9 6 6 9.68 1.32 -9 6 -6 5.08 1.10 9 6 7 143.78 6.09 9 -6 7 132.21 5.46 9 6 7 121.18 5.18 -9 6 -8 8.57 1.02 9 -6 8 17.53 1.33 9 6 8 14.51 1.15 9 7 -8 57.39 3.56 9 7 -8 65.67 3.52 9 7 -8 65.39 3.53 9 7 -7 107.05 5.14 9 7 -7 96.38 5.60 9 7 -7 102.85 5.02 9 -7 -7 89.58 5.53 9 -7 -6 17.67 1.68 9 7 -6 17.35 1.89 9 7 -6 16.69 2.41 9 7 -6 17.49 1.90 9 -7 -6 15.65 2.26 9 -7 -6 14.23 1.70 9 7 -5 46.41 3.49 9 7 -5 47.02 3.45 9 7 -5 45.37 4.16 9 -7 -5 38.88 3.88 9 -7 -5 40.45 3.42 9 7 -4 226.23 10.57 9 7 -4 230.89 11.79 9 -7 -4 190.23 11.23 9 7 -4 209.94 11.77 9 7 -4 223.24 10.60 9 7 -3 22.49 2.78 9 7 -3 22.06 2.49 9 7 -3 23.36 2.53 9 -7 -3 22.89 2.55 9 -7 -3 22.31 2.53 9 7 -3 26.85 3.09 -9 7 3 21.77 2.09 9 7 -3 18.66 3.13 9 7 -2 133.25 7.71 9 7 -2 141.21 8.32 9 7 -2 141.28 7.81 9 -7 -2 138.23 7.66 9 -7 -2 135.47 7.59 9 7 -2 158.88 8.47 -9 7 2 148.99 7.14 9 7 -2 132.37 9.91 9 7 -1 49.86 4.12 9 -7 -1 56.01 4.17 9 -7 -1 60.42 4.26 9 7 -1 59.94 4.31 -9 7 1 58.03 4.03 9 7 -1 53.89 4.21 9 7 -1 64.98 4.93 9 7 -1 54.00 4.54 9 -7 0 33.46 3.04 9 -7 0 35.84 3.10 9 7 0 32.63 3.17 -9 7 0 35.98 3.11 9 7 0 33.01 3.47 9 7 0 32.04 3.12 9 -7 1 44.29 3.49 9 -7 1 49.54 3.64 9 7 1 38.92 3.51 9 7 1 43.94 3.91 9 7 1 36.81 3.43 9 -7 2 3.31 1.03 9 -7 2 4.93 1.26 9 -7 2 5.10 1.21 9 7 2 3.59 1.13 9 7 2 6.15 1.38 9 -7 2 6.96 1.20 9 7 2 4.46 1.35 9 -7 3 50.95 3.38 9 -7 3 49.19 3.53 9 -7 3 50.13 3.55 9 -7 3 47.54 3.46 9 7 3 42.77 3.81 9 -7 4 9.09 1.35 9 -7 4 8.89 1.37 9 -7 4 7.29 1.15 9 -7 4 5.74 1.19 9 -7 5 4.66 0.91 9 -7 5 5.22 1.04 9 -7 5 5.56 1.06 9 -7 6 1.44 0.53 9 -7 6 1.16 0.56 9 -7 6 1.97 0.62 9 7 6 0.97 0.61 9 7 7 7.83 0.85 9 -7 7 7.10 0.80 9 8 -7 100.45 4.56 9 8 -6 70.50 4.00 9 8 -5 1.94 0.63 9 8 -5 0.90 0.56 9 8 -5 2.44 0.80 9 -8 -5 1.54 0.47 9 8 -4 172.30 8.31 9 -8 -4 160.37 8.12 9 8 -4 179.02 8.36 9 8 -3 94.86 5.54 9 8 -3 107.08 5.92 9 8 -3 96.24 5.53 9 8 -3 95.88 6.20 9 8 -2 1.55 1.17 9 8 -2 1.12 0.69 9 8 -2 1.02 0.64 9 8 -2 2.16 0.91 -9 8 2 3.02 1.03 9 8 -2 3.40 0.92 9 8 -1 1.29 1.22 9 8 -1 1.30 0.75 9 8 -1 1.17 0.68 9 8 -1 1.86 0.78 -9 8 1 0.61 0.98 9 8 -1 1.10 0.53 9 8 0 35.87 2.98 9 8 0 38.50 3.20 -9 8 0 45.23 3.04 9 8 0 36.58 3.01 9 8 1 83.15 5.13 9 8 1 89.56 5.35 -9 8 -1 101.07 5.04 9 8 1 86.99 5.19 -9 8 -2 85.49 4.54 9 8 2 76.88 4.82 9 -8 3 18.46 1.75 9 -8 3 18.26 1.72 9 8 4 14.51 1.59 9 -8 4 11.34 1.27 9 -8 4 13.67 1.35 -9 8 -4 15.96 1.47 9 -8 5 0.27 0.35 9 -8 5 0.57 0.38 9 9 -3 26.35 1.74 9 9 -2 75.62 3.76 9 9 -2 77.06 3.78 9 9 -2 77.69 3.74 9 9 -1 10.00 1.21 9 9 -1 8.56 1.02 9 9 -1 8.44 1.01 9 9 -1 9.92 1.08 9 9 0 92.47 4.82 9 9 2 0.17 0.33 10 0 -12 17.37 1.46 10 0 -12 18.39 1.60 10 0 -11 0.55 0.50 10 0 -11 0.88 0.66 10 0 -11 0.56 0.53 10 0 -11 1.35 0.77 10 0 -10 9.37 1.84 10 0 -10 9.68 1.79 10 0 -10 9.83 1.92 10 0 -10 9.91 1.74 10 0 -10 8.89 1.61 10 0 -9 1.20 0.83 10 0 -9 0.26 0.70 10 0 -9 1.38 1.16 10 0 -9 -0.23 0.82 10 0 -9 0.86 0.82 10 0 -9 1.66 1.03 10 0 -9 0.73 1.06 10 0 -8 145.87 9.81 10 0 -8 134.24 9.34 10 0 -8 129.12 8.08 10 0 -8 129.84 8.78 10 0 -8 160.24 9.34 10 0 -8 130.58 8.02 10 0 -8 130.99 8.01 10 0 -7 0.21 0.83 10 0 -7 0.42 0.80 10 0 -7 3.17 1.38 10 0 -7 -0.30 0.72 10 0 -7 0.54 0.80 10 0 -7 1.06 1.02 10 0 -7 2.39 1.17 10 0 -6 3.73 1.59 10 0 -6 0.85 1.00 10 0 -6 1.08 1.01 10 0 -6 2.69 1.30 10 0 -6 2.32 1.07 10 0 -6 1.24 1.19 10 0 -6 1.11 0.95 10 0 -6 1.34 0.97 10 0 -6 1.29 1.08 10 0 -6 2.66 1.23 10 0 -5 0.25 0.60 10 0 -5 1.56 0.85 10 0 -5 0.58 0.70 10 0 -5 2.07 1.34 10 0 -5 3.90 2.63 10 0 -5 1.37 1.01 10 0 -5 -0.22 0.70 10 0 -5 2.17 1.08 10 0 -5 1.06 0.81 10 0 -5 -0.27 0.85 10 0 -4 23.48 3.20 10 0 -4 24.56 3.39 10 0 -4 28.65 6.69 10 0 -4 33.79 3.96 10 0 -4 25.43 2.98 10 0 -4 31.93 3.41 10 0 -4 29.21 3.61 10 0 -4 27.66 3.29 10 0 -4 21.10 2.93 10 0 -4 26.14 3.16 10 0 -4 25.08 3.11 10 0 -3 0.89 0.97 10 0 -3 0.74 0.79 10 0 -3 0.93 1.94 10 0 -3 -0.19 0.70 10 0 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1.33 10 0 7 1.52 1.17 -10 0 -8 701.39 31.31 10 0 8 772.25 31.53 10 0 9 0.13 0.72 10 0 9 0.11 0.53 10 0 9 -0.11 0.73 -10 0 -9 1.09 0.73 10 0 10 5.27 0.96 10 1 -12 60.60 3.39 10 -1 -12 61.08 3.48 10 -1 -12 69.40 3.40 10 1 -11 73.50 4.35 10 -1 -11 74.25 4.62 10 1 -11 76.14 4.92 10 1 -11 72.87 4.45 10 -1 -11 75.82 4.49 10 -1 -11 80.73 4.70 10 1 -10 142.06 7.78 10 -1 -10 133.53 8.09 10 -1 -10 116.82 8.16 10 1 -10 143.85 8.16 10 1 -10 129.04 7.75 10 -1 -10 129.65 7.71 10 -1 -10 124.45 7.63 10 1 -10 131.51 7.52 10 -1 -10 120.87 7.16 10 1 -10 135.72 7.42 10 1 -9 391.44 18.41 10 -1 -9 390.30 20.13 10 1 -9 415.36 19.23 10 -1 -9 396.80 19.95 10 -1 -9 410.66 18.53 10 -1 -9 382.65 19.03 10 -1 -9 449.70 18.73 10 1 -9 421.88 19.17 10 -1 -9 387.09 18.92 10 1 -9 394.04 18.63 10 1 -8 39.82 4.17 10 -1 -8 48.61 4.77 10 1 -8 41.89 4.36 10 -1 -8 45.34 4.43 10 1 -8 42.61 4.56 10 1 -8 45.49 4.15 10 -1 -8 45.86 4.02 10 1 -8 39.47 4.29 10 1 -8 49.02 4.81 10 -1 -8 45.85 5.25 10 -1 -8 39.59 5.03 10 -1 -8 42.26 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30.68 3.59 10 1 -5 34.06 3.66 10 1 -5 35.90 3.97 10 -1 -5 25.48 3.55 10 -1 -5 40.53 4.76 10 1 -5 31.17 3.77 10 1 -5 42.27 8.53 10 -1 -5 22.10 5.75 10 1 -5 31.91 3.87 10 -1 -5 31.65 4.24 10 -1 -5 33.10 3.50 10 1 -5 25.27 3.25 10 1 -5 29.07 3.37 10 1 -4 32.97 3.72 10 -1 -4 34.53 3.86 10 1 -4 45.57 4.03 10 1 -4 37.37 3.88 10 -1 -4 34.63 3.89 10 1 -4 42.12 4.21 10 -1 -4 44.10 4.85 10 1 -4 39.05 4.05 10 -1 -4 36.78 3.69 10 1 -4 36.03 3.87 10 -1 -4 38.55 3.65 10 -1 -4 35.56 3.43 10 -1 -4 37.48 3.76 10 1 -4 30.83 3.78 10 1 -4 34.42 7.57 10 -1 -4 34.70 6.92 10 1 -4 45.34 4.31 10 1 -4 29.39 3.75 10 -1 -4 47.49 5.13 10 1 -4 36.66 3.89 10 -1 -4 31.14 3.44 10 1 -4 42.39 3.96 10 1 -4 37.92 3.85 10 1 -3 90.91 6.39 10 -1 -3 92.00 6.42 10 1 -3 83.32 6.25 10 1 -3 101.99 6.67 10 -1 -3 93.61 5.95 10 -1 -3 101.41 7.24 10 1 -3 87.14 5.85 10 1 -3 81.15 6.32 10 1 -3 75.21 6.20 10 -1 -3 79.07 5.86 10 -1 -3 86.59 6.06 10 1 -3 95.33 6.68 10 -1 -3 87.33 6.17 10 1 -3 78.47 6.33 10 -1 -3 106.71 7.83 10 1 -3 81.28 6.33 10 1 -3 96.79 6.43 10 1 -3 93.55 12.52 10 -1 -3 95.16 11.69 10 1 -3 77.84 6.20 10 1 -3 84.57 6.21 10 -1 -3 95.60 6.28 10 -1 -3 96.67 6.24 10 1 -3 74.81 5.90 10 1 -2 743.32 32.20 10 1 -2 774.17 32.95 10 -1 -2 805.86 33.23 10 1 -2 837.98 32.97 10 -1 -2 842.72 33.61 10 -1 -2 843.42 32.54 10 1 -2 796.28 33.40 10 -1 -2 786.27 32.85 10 1 -2 740.76 33.26 10 -1 -2 751.22 32.60 10 1 -2 741.35 33.44 10 1 -2 798.92 33.45 10 -1 -2 814.08 32.90 10 1 -2 730.14 33.23 10 1 -2 818.47 45.71 10 -1 -2 797.61 43.13 10 1 -2 708.74 33.01 10 -1 -2 798.44 32.86 10 1 -2 802.99 33.01 10 1 -2 780.76 33.12 10 -1 -2 801.07 32.72 10 1 -1 159.05 9.13 10 1 -1 154.15 9.25 10 1 -1 171.92 9.86 10 -1 -1 171.89 9.03 10 1 -1 157.23 16.80 10 -1 -1 185.81 16.46 10 1 -1 162.09 9.53 10 -1 -1 175.28 9.43 10 1 -1 153.08 9.62 10 1 -1 150.29 9.68 10 -1 -1 160.00 9.24 10 -1 -1 166.98 9.43 10 1 -1 155.87 9.69 10 -1 -1 179.28 9.51 10 1 -1 155.41 9.16 10 1 -1 162.78 9.77 10 -1 -1 163.75 9.21 10 1 0 180.77 10.38 10 1 0 191.87 10.47 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10 -1 6 4.08 1.42 10 1 6 0.24 1.00 10 1 6 0.39 0.83 10 -1 6 1.90 0.98 10 1 6 0.24 1.35 10 -1 7 21.32 2.64 10 1 7 20.19 2.43 10 1 7 17.79 2.88 10 -1 7 23.45 2.91 10 1 7 26.05 3.16 10 -1 8 343.05 14.89 10 1 8 346.55 14.92 -10 1 -8 293.93 14.41 -10 -1 -8 299.07 14.18 10 1 8 331.24 15.13 10 -1 8 292.73 13.79 10 1 9 21.66 2.32 10 1 9 20.07 2.28 10 -1 9 20.03 2.16 10 1 9 22.47 2.25 -10 1 -9 18.56 2.08 -10 -1 -9 16.10 1.88 10 -1 10 0.15 0.46 10 1 10 0.50 0.51 10 1 10 0.48 0.50 10 1 10 0.99 0.46 10 -2 -12 15.24 1.08 10 -2 -11 203.82 9.12 10 2 -11 202.90 9.50 10 -2 -11 178.91 9.18 10 -2 -11 211.81 9.49 10 -2 -11 214.57 9.16 10 -2 -10 89.19 5.69 10 -2 -10 93.05 5.43 10 -2 -10 96.89 5.92 10 -2 -10 77.31 6.08 10 2 -10 94.81 5.64 10 2 -10 96.30 5.96 10 -2 -10 80.56 5.96 10 -2 -9 2.03 1.17 10 -2 -9 3.74 1.19 10 2 -9 3.77 1.19 10 -2 -9 4.76 1.66 10 2 -9 4.04 1.28 10 -2 -9 5.09 1.34 10 2 -9 6.50 1.63 10 2 -9 5.25 1.38 10 2 -8 133.58 7.74 10 -2 -8 145.90 7.82 10 2 -8 130.73 7.87 10 -2 -8 142.71 10.15 10 2 -8 148.56 8.71 10 -2 -8 116.96 9.42 10 2 -8 140.76 8.55 10 2 -8 114.93 8.00 10 2 -8 140.31 8.67 10 -2 -8 144.98 8.28 10 -2 -8 133.36 9.00 10 2 -8 119.26 8.07 10 -2 -7 19.56 3.14 10 2 -7 11.65 2.21 10 2 -7 11.95 2.23 10 2 -7 10.15 1.87 10 2 -7 8.88 2.04 10 2 -7 14.87 2.49 10 -2 -7 12.60 2.88 10 2 -7 11.49 2.13 10 2 -7 12.63 2.34 10 2 -7 10.50 1.85 10 2 -7 12.50 2.12 10 -2 -7 9.86 1.86 10 2 -7 11.08 2.14 10 -2 -7 14.33 2.02 10 -2 -7 14.21 2.36 10 2 -7 12.35 2.15 10 -2 -7 9.63 1.73 10 2 -7 9.40 1.97 10 2 -6 24.61 3.19 10 -2 -6 26.10 2.84 10 -2 -6 25.27 2.80 10 2 -6 24.54 3.17 10 2 -6 28.27 3.37 10 -2 -6 23.18 4.08 10 -2 -6 29.90 4.15 10 -2 -6 26.36 3.00 10 2 -6 29.48 3.41 10 2 -6 27.05 3.24 10 2 -6 29.48 3.58 10 2 -6 25.32 3.25 10 -2 -6 27.31 3.39 10 2 -6 24.81 3.19 10 2 -6 25.93 3.44 10 -2 -5 9.12 2.17 10 -2 -5 7.49 1.81 10 2 -5 6.01 1.54 10 -2 -5 6.41 1.38 10 2 -5 6.26 1.60 10 -2 -5 12.30 2.91 10 2 -5 4.33 1.38 10 -2 -5 7.14 2.11 10 2 -5 8.06 1.85 10 -2 -5 9.45 2.03 10 -2 -5 5.28 1.35 10 2 -5 6.34 1.60 10 2 -5 6.71 1.67 10 -2 -5 6.76 1.50 10 2 -5 8.44 1.93 10 -2 -5 5.76 1.49 10 -2 -4 310.47 14.51 10 -2 -4 280.90 16.50 10 2 -4 328.33 15.04 10 2 -4 287.02 14.12 10 2 -4 299.96 14.56 10 -2 -4 304.60 16.69 10 2 -4 300.18 14.31 10 2 -4 274.25 23.65 10 -2 -4 313.19 22.17 10 2 -4 284.63 15.02 10 2 -4 256.70 14.37 10 -2 -4 287.67 13.91 10 -2 -4 317.99 13.74 10 -2 -4 287.84 13.86 10 2 -4 261.62 14.53 10 -2 -4 292.89 14.07 10 2 -4 300.90 15.03 10 2 -4 261.30 14.32 10 2 -4 268.29 14.33 10 -2 -3 888.40 35.90 10 2 -3 913.74 35.44 10 2 -3 903.75 35.99 10 -2 -3 1009.75 38.46 10 2 -3 893.95 35.80 10 2 -3 841.32 48.49 10 -2 -3 927.04 45.67 10 2 -3 874.59 36.83 10 -2 -3 902.63 35.60 10 2 -3 776.69 36.14 10 -2 -3 881.37 35.32 10 2 -3 771.40 36.03 10 -2 -3 881.64 35.40 10 2 -3 796.79 36.06 10 2 -3 779.47 35.77 10 -2 -3 843.20 35.37 10 2 -3 914.62 36.54 10 2 -3 797.72 35.94 10 2 -2 289.52 14.99 10 -2 -2 347.07 15.77 10 2 -2 321.09 15.33 10 -2 -2 353.54 16.75 10 2 -2 309.35 16.25 10 2 -2 305.08 25.09 10 -2 -2 361.34 23.55 10 -2 -2 344.09 15.42 10 2 -2 290.79 15.83 10 2 -2 354.47 16.78 10 -2 -2 335.93 15.24 10 2 -2 303.68 16.00 10 -2 -2 339.37 15.37 10 2 -2 297.73 15.83 10 2 -2 340.24 16.02 10 2 -2 300.51 15.76 10 -2 -2 336.44 15.38 10 -2 -2 334.36 15.21 10 2 -2 306.48 15.96 10 2 -1 36.22 3.93 10 -2 -1 40.56 3.73 10 -2 -1 41.10 3.64 10 2 -1 39.37 3.89 10 2 -1 36.16 4.14 10 -2 -1 42.94 3.78 10 2 -1 39.27 4.18 10 2 -1 38.12 3.46 10 2 -1 41.11 4.35 10 -2 -1 42.17 7.19 10 2 -1 40.63 8.28 10 2 -1 28.10 3.64 10 -2 -1 43.54 3.79 10 2 -1 36.65 4.11 10 -2 -1 44.58 3.85 10 2 -1 37.58 3.81 10 2 0 152.76 9.08 10 2 0 137.77 8.37 10 2 0 144.11 9.16 10 -2 0 150.91 8.57 10 -2 0 163.28 8.53 10 2 0 156.63 9.48 10 -2 0 151.02 8.40 10 2 0 137.38 9.03 10 2 0 153.39 9.89 10 2 0 130.77 15.54 10 -2 0 165.86 14.88 10 2 0 131.48 9.03 10 -2 0 142.13 8.32 10 2 0 138.07 9.26 10 -2 0 148.97 8.51 10 2 0 134.08 8.72 10 2 1 201.66 19.90 10 -2 1 227.29 18.30 10 2 1 204.67 11.81 10 2 1 211.64 11.90 10 2 1 225.41 10.80 10 2 1 224.21 12.01 10 -2 1 235.63 11.30 10 2 1 193.25 11.78 10 2 1 203.42 12.48 10 -2 1 212.10 10.86 10 2 1 201.37 11.42 10 2 2 1.12 0.85 10 -2 2 0.99 0.69 10 2 2 -1.09 1.32 10 -2 2 0.80 1.37 10 2 2 0.62 0.91 10 2 2 1.30 1.33 10 -2 2 2.40 1.02 10 2 2 0.26 1.03 10 2 3 -0.46 0.84 10 2 3 0.77 1.03 10 -2 3 0.19 0.85 10 2 3 0.76 1.02 10 2 3 1.38 1.41 10 2 3 -1.08 1.84 10 -2 3 -0.84 1.01 10 2 3 1.61 1.23 10 -2 4 37.54 3.68 10 2 4 34.47 3.92 10 2 4 34.87 4.09 10 2 4 35.31 4.33 10 -2 5 7.54 1.39 10 -2 5 6.06 1.62 10 2 5 7.38 1.75 10 2 5 9.40 2.16 10 2 6 29.09 3.83 10 -2 6 28.56 3.08 10 2 6 25.35 3.10 10 2 6 27.84 3.27 10 -2 7 227.83 11.11 10 2 7 241.90 11.34 -10 2 -7 194.63 10.95 -10 -2 -7 214.96 10.74 10 2 7 226.71 12.24 10 2 7 218.86 11.09 10 -2 8 29.18 2.67 10 2 8 22.90 2.40 10 2 8 26.21 2.30 10 2 8 23.48 2.91 -10 2 -8 20.27 2.42 -10 -2 -8 22.62 2.31 10 2 9 -0.13 0.66 -10 2 -9 0.96 0.51 -10 -2 -9 0.43 0.39 10 -2 9 1.56 0.71 10 2 9 1.18 0.58 10 2 9 0.25 0.82 10 -2 10 11.79 1.10 10 2 10 11.83 1.26 10 2 10 13.00 1.30 10 -3 -11 -0.05 0.27 10 -3 -11 0.49 0.34 10 -3 -11 0.57 0.43 10 -3 -11 1.29 0.49 10 -3 -11 0.55 0.40 10 -3 -10 20.92 2.17 10 -3 -10 17.85 1.79 10 3 -10 17.60 2.02 10 -3 -10 14.80 2.13 10 -3 -10 14.07 2.05 10 -3 -10 16.39 1.87 10 -3 -9 162.33 7.89 10 3 -9 144.75 8.53 10 3 -9 164.45 8.55 10 -3 -9 126.10 8.97 10 -3 -9 147.10 9.47 10 -3 -9 161.78 8.02 10 -3 -9 171.27 8.77 10 3 -9 136.64 8.39 10 3 -8 21.71 2.66 10 -3 -8 22.34 2.53 10 -3 -8 26.08 3.24 10 3 -8 17.28 2.73 10 -3 -8 22.83 3.53 10 3 -8 23.52 2.80 10 -3 -8 12.01 2.78 10 -3 -8 22.22 2.87 10 3 -8 21.46 2.54 10 3 -8 16.97 2.68 10 3 -8 22.36 2.72 10 3 -7 425.93 19.97 10 3 -7 425.01 19.70 10 -3 -7 462.34 19.01 10 -3 -7 443.04 18.88 10 3 -7 416.20 19.63 10 3 -7 449.22 19.72 10 3 -7 446.03 19.96 10 -3 -7 460.13 21.40 10 -3 -7 467.84 19.90 10 3 -7 439.71 19.94 10 3 -7 461.26 20.27 10 3 -7 424.63 20.12 10 -3 -7 446.52 19.26 10 -3 -7 371.72 21.45 10 3 -6 240.24 12.86 10 3 -6 227.05 12.33 10 3 -6 231.12 12.43 10 -3 -6 256.92 11.81 10 -3 -6 251.55 11.73 10 3 -6 245.18 12.27 10 3 -6 247.83 12.23 10 3 -6 238.31 13.00 10 -3 -6 255.96 12.06 10 3 -6 256.84 12.39 10 3 -6 254.96 12.57 10 -3 -6 239.38 12.51 10 -3 -6 250.01 14.14 10 -3 -6 213.81 14.93 10 3 -6 248.04 12.56 10 3 -6 252.37 12.86 10 -3 -6 206.51 13.75 10 3 -5 12.62 2.16 10 3 -5 13.51 2.23 10 -3 -5 15.79 2.04 10 -3 -5 14.83 2.33 10 -3 -5 15.45 2.03 10 3 -5 13.40 2.60 10 3 -5 12.54 2.54 10 -3 -5 12.96 2.02 10 3 -5 15.54 2.23 10 3 -5 12.71 2.36 10 3 -5 13.81 2.16 10 -3 -5 12.04 3.05 10 3 -5 13.88 2.11 10 3 -5 14.30 2.13 10 3 -5 15.71 2.21 10 3 -5 13.30 2.59 10 -3 -5 14.14 2.76 10 -3 -5 12.44 2.10 10 -3 -4 34.42 3.13 10 -3 -4 32.61 3.05 10 3 -4 29.31 3.36 10 3 -4 29.61 3.39 10 3 -4 32.63 3.23 10 3 -4 29.01 7.10 10 -3 -4 33.13 6.07 10 3 -4 37.36 3.48 10 3 -4 32.84 3.51 10 3 -4 35.66 4.04 10 -3 -4 25.80 4.20 10 -3 -4 27.90 3.15 10 3 -4 32.02 3.91 10 3 -4 29.61 3.77 10 3 -4 32.86 3.36 10 -3 -4 25.99 2.92 10 3 -4 34.78 3.96 10 3 -4 32.47 3.52 10 -3 -3 26.28 2.98 10 -3 -3 29.79 4.05 10 3 -3 27.01 2.86 10 3 -3 27.90 3.13 10 3 -3 22.55 3.29 10 -3 -3 25.50 2.70 10 -3 -3 23.66 2.60 10 3 -3 25.85 3.13 10 3 -3 25.84 3.09 10 3 -3 23.64 3.62 10 -3 -3 23.19 2.68 10 3 -3 25.87 3.21 10 3 -3 21.04 2.69 10 -3 -3 26.19 2.81 10 3 -3 28.89 3.57 10 3 -3 22.01 3.03 10 3 -3 23.00 6.08 10 -3 -3 20.32 4.87 10 -3 -2 147.12 8.06 10 3 -2 141.14 8.70 10 -3 -2 147.11 8.03 10 3 -2 138.39 8.61 10 3 -2 133.42 8.36 10 3 -2 139.65 8.36 10 -3 -2 145.91 8.16 10 3 -2 158.51 9.34 10 3 -2 134.56 9.05 10 3 -2 151.19 10.00 10 -3 -2 159.93 8.35 10 3 -2 128.79 8.56 10 -3 -2 130.81 9.33 10 3 -2 153.49 8.11 10 3 -2 160.95 8.62 10 3 -2 149.08 9.65 10 3 -2 140.00 15.20 10 -3 -2 155.22 13.83 10 -3 -2 153.10 8.56 10 -3 -1 5.50 1.32 10 3 -1 5.12 1.60 10 3 -1 5.87 1.47 10 -3 -1 5.27 1.30 10 3 -1 3.06 1.33 10 3 -1 5.08 2.05 10 3 -1 4.42 1.31 10 -3 -1 4.16 1.16 10 3 -1 3.46 1.24 10 -3 -1 4.43 1.17 10 3 -1 6.62 1.91 10 3 -1 2.81 2.27 10 -3 -1 2.06 1.67 10 3 -1 4.11 1.41 10 3 0 0.93 1.58 10 -3 0 6.16 2.61 10 3 0 4.45 1.58 10 3 0 3.81 1.25 10 -3 0 2.60 0.92 10 3 0 1.90 1.11 10 -3 0 2.04 0.91 10 3 0 0.44 0.88 10 3 0 4.85 1.76 10 3 0 1.55 0.88 10 -3 0 1.67 0.95 10 3 0 6.25 1.57 10 -3 0 1.93 0.94 10 3 0 5.09 1.49 10 3 0 4.16 1.68 10 3 0 4.29 1.59 10 3 0 3.62 1.34 10 3 1 27.24 2.91 10 3 1 24.31 3.13 10 -3 1 23.16 2.69 10 -3 1 28.03 2.96 10 3 1 21.30 3.00 10 3 1 26.38 3.16 10 3 1 32.21 4.06 10 -3 1 31.09 3.01 10 3 1 23.18 3.05 10 3 1 24.48 3.49 10 3 1 23.43 3.21 10 3 1 29.24 3.72 10 3 1 30.84 6.55 10 -3 1 27.74 5.64 10 3 2 184.04 17.20 10 -3 2 179.84 15.69 10 3 2 183.37 11.31 10 -3 2 197.75 9.90 10 3 2 187.51 10.44 10 3 2 185.67 10.88 10 3 2 200.86 9.87 10 3 2 166.39 11.14 10 -3 3 54.45 4.21 10 3 3 51.40 4.43 10 3 3 47.80 4.74 10 3 3 44.95 5.10 10 3 3 55.08 4.11 10 3 4 137.52 9.27 10 3 4 138.92 7.50 10 3 4 119.20 9.14 10 -3 4 141.50 7.75 10 3 4 130.07 7.91 10 -3 5 98.97 5.98 10 -3 5 108.41 6.36 10 3 5 100.00 6.38 10 3 5 104.78 7.56 10 3 5 97.53 7.78 10 -3 6 777.52 31.92 10 3 6 806.09 34.47 10 -3 6 840.99 32.30 10 3 6 755.28 32.10 10 3 6 795.38 33.58 10 3 7 15.80 1.86 -10 3 -7 12.34 1.87 -10 -3 -7 13.47 1.72 10 -3 7 16.55 1.94 10 3 7 15.37 1.88 10 3 7 14.86 2.12 10 -3 8 2.33 0.73 10 3 8 2.58 1.32 -10 -3 -8 1.75 0.63 10 3 8 2.19 0.74 -10 3 -9 2.08 0.74 -10 3 -9 2.46 0.86 10 3 9 4.22 0.98 10 3 9 5.88 1.20 10 -3 9 4.30 0.70 10 3 10 57.41 2.45 10 3 10 57.61 2.50 10 -4 -11 53.31 2.73 10 -4 -10 7.88 1.04 10 -4 -10 12.62 1.41 10 -4 -10 10.72 1.50 10 -4 -10 12.40 1.61 10 -4 -10 11.03 1.07 10 -4 -9 5.76 1.43 10 -4 -9 7.86 1.16 10 -4 -9 9.85 1.86 10 -4 -9 8.99 1.45 10 -4 -8 275.84 12.92 10 4 -8 275.08 12.53 10 4 -8 251.82 12.39 10 4 -8 250.38 12.69 10 4 -8 269.52 13.40 10 4 -8 240.98 13.08 10 -4 -8 283.01 12.02 10 -4 -8 289.04 13.30 10 -4 -8 236.18 13.47 10 4 -7 29.74 2.98 10 -4 -7 27.11 4.06 10 4 -7 29.49 3.45 10 -4 -7 34.01 2.78 10 4 -7 30.32 3.54 10 4 -7 26.07 3.39 10 -4 -7 28.35 2.80 10 -4 -7 32.14 3.56 10 -4 -7 29.25 3.73 10 4 -6 21.50 2.51 10 4 -6 15.80 2.28 10 -4 -6 17.45 3.45 10 -4 -6 19.50 2.20 10 4 -6 19.08 2.91 10 4 -6 18.19 2.85 10 -4 -6 20.74 2.45 10 -4 -6 18.47 2.92 10 4 -6 18.92 2.61 10 -4 -5 6.42 1.48 10 4 -5 5.39 1.32 10 4 -5 3.58 1.33 10 -4 -5 1.59 1.37 10 -4 -5 4.30 1.10 10 4 -5 3.49 1.56 10 4 -5 5.53 1.70 10 4 -5 3.49 1.53 10 4 -5 3.63 1.44 10 4 -5 3.30 1.12 10 -4 -5 5.28 1.75 10 4 -4 392.76 17.29 10 -4 -4 395.56 17.08 10 4 -4 372.06 17.09 10 -4 -4 344.95 19.83 10 4 -4 356.38 18.02 10 -4 -4 401.66 16.76 10 4 -4 388.29 18.93 10 4 -4 323.36 16.74 10 -4 -4 410.21 17.69 10 4 -4 374.53 16.85 10 4 -4 353.61 16.66 10 4 -3 82.93 7.24 10 -4 -3 74.48 5.24 10 -4 -3 70.26 6.73 10 4 -3 65.53 5.85 10 4 -3 74.59 5.12 10 4 -3 75.06 5.15 10 -4 -3 83.99 5.17 10 4 -3 82.87 6.52 10 4 -3 73.60 5.62 10 4 -3 73.96 5.29 10 4 -3 81.50 5.60 10 -4 -3 63.75 5.14 10 -4 -3 73.10 5.38 10 4 -2 287.97 15.76 10 -4 -2 248.85 12.71 10 -4 -2 248.41 12.65 10 4 -2 242.79 13.12 10 4 -2 256.12 12.55 10 -4 -2 233.62 13.97 10 4 -2 247.68 14.02 10 4 -2 262.14 12.82 10 -4 -2 279.86 12.48 10 4 -2 275.16 14.18 10 4 -2 246.65 13.53 10 -4 -2 269.31 12.78 10 4 -2 295.06 13.29 10 4 -1 327.61 17.29 10 4 -1 402.62 19.78 10 4 -1 337.24 17.81 10 4 -1 372.42 17.48 10 -4 -1 391.75 16.11 10 -4 -1 337.66 16.14 10 -4 -1 339.13 16.11 10 4 -1 348.82 16.30 10 4 -1 349.91 16.33 10 -4 0 456.79 20.04 10 4 0 488.44 20.69 10 4 0 447.63 22.38 10 -4 0 442.17 20.25 10 -4 0 448.49 20.25 10 -4 1 7.41 1.54 10 4 1 7.96 2.03 10 -4 1 8.71 1.64 10 4 1 5.47 1.48 10 4 1 4.82 1.24 10 -4 1 4.96 1.24 10 4 1 8.06 1.92 10 4 1 4.64 1.26 10 4 1 4.25 1.65 10 4 2 277.83 12.46 10 4 2 221.02 11.85 10 4 2 223.13 11.82 10 4 2 255.75 12.14 10 4 2 239.46 14.19 10 4 2 289.47 14.01 10 -4 2 270.87 12.24 10 -4 2 258.38 12.03 10 4 2 239.10 13.85 10 -4 2 271.32 12.36 10 -4 2 267.02 12.33 10 4 3 52.08 4.90 10 -4 3 57.45 4.11 10 4 3 46.61 5.24 10 -4 3 52.10 4.03 10 -4 3 50.05 3.99 10 4 3 58.78 4.20 10 4 3 54.57 4.03 10 4 3 54.04 5.37 10 4 4 120.90 6.48 10 4 4 112.43 7.99 10 -4 4 111.84 6.39 10 4 4 106.85 8.03 10 -4 4 103.51 6.20 10 -4 4 97.02 6.14 10 4 5 124.26 6.92 10 4 5 135.44 8.84 10 4 5 126.43 8.40 10 4 5 145.38 9.06 10 4 6 32.93 2.76 10 4 6 30.25 3.45 10 4 6 34.77 3.79 10 4 6 36.54 3.66 10 4 7 45.72 3.72 10 4 7 53.92 4.31 10 4 8 34.26 2.50 10 4 8 40.08 3.11 -10 4 -9 11.32 1.41 -10 4 -9 11.68 1.37 10 -5 -10 0.72 0.36 10 -5 -9 71.39 4.60 10 -5 -9 72.82 3.90 10 -5 -8 1.10 0.46 10 5 -8 1.96 0.72 10 5 -8 0.89 0.88 10 -5 -8 0.89 0.65 10 -5 -8 1.56 0.74 10 -5 -7 1.50 0.75 10 5 -7 0.20 1.00 10 5 -7 -0.17 0.86 10 -5 -7 0.26 0.77 10 5 -7 0.17 0.76 10 5 -7 0.13 0.51 10 -5 -7 0.46 0.50 10 -5 -7 0.68 0.80 10 5 -6 43.24 3.67 10 -5 -6 38.04 4.70 10 -5 -6 49.08 3.53 10 -5 -6 52.50 4.49 10 5 -6 49.02 4.12 10 5 -6 50.55 4.17 10 5 -5 32.30 3.10 10 5 -5 36.09 3.30 10 5 -5 26.42 3.58 10 -5 -5 25.55 3.86 10 5 -5 31.82 3.95 10 -5 -5 33.24 3.67 10 -5 -5 30.06 2.85 10 5 -5 27.35 2.92 10 5 -4 8.53 2.48 10 -5 -4 8.40 1.55 10 5 -4 7.31 2.16 10 5 -4 9.10 1.65 10 5 -4 6.40 1.40 10 5 -4 6.69 1.59 10 -5 -4 6.27 2.16 10 5 -3 18.83 2.42 10 -5 -3 18.44 2.20 10 -5 -3 17.32 3.05 10 5 -3 18.42 2.63 10 -5 -3 17.68 2.39 10 -5 -3 22.64 2.65 10 5 -3 19.85 3.15 10 5 -3 17.45 2.44 10 5 -2 94.87 6.26 10 -5 -2 101.72 6.05 10 5 -2 84.01 8.00 10 5 -2 101.67 6.98 10 -5 -2 92.71 6.18 10 -5 -2 96.12 6.22 10 5 -2 107.15 7.47 10 5 -2 105.06 6.50 10 5 -1 504.63 21.69 10 5 -1 449.94 22.79 10 -5 -1 551.23 21.48 10 5 -1 512.23 25.54 10 5 -1 481.32 22.50 10 5 -1 485.63 21.59 10 -5 -1 483.26 21.39 10 -5 -1 497.79 21.46 10 5 -1 556.65 22.86 10 5 -1 438.89 21.92 10 -5 0 8.28 1.66 10 -5 0 8.00 1.67 10 5 0 5.85 1.69 10 5 0 5.91 1.68 10 5 0 6.66 1.49 10 5 0 4.82 1.34 10 5 1 0.17 0.65 10 5 1 0.34 0.62 10 5 1 0.23 0.74 10 -5 1 1.90 0.79 10 -5 1 0.61 0.79 10 -5 1 0.76 0.93 10 5 1 -0.46 0.83 10 5 1 0.78 0.91 10 5 2 3.35 1.24 10 -5 2 2.04 0.87 10 -5 2 3.84 1.20 10 -5 2 2.18 1.01 10 5 2 1.79 1.05 10 5 2 2.04 1.06 10 5 3 236.25 12.94 10 -5 3 255.94 11.94 10 -5 3 262.31 12.09 10 -5 3 254.25 12.02 10 5 3 254.84 13.19 10 5 3 263.01 12.01 10 5 4 0.57 0.86 10 -5 4 1.27 0.74 10 -5 4 2.04 0.97 10 -5 4 2.01 0.87 10 5 4 0.86 0.83 10 5 5 158.09 8.76 10 5 5 159.99 7.98 10 -5 5 164.64 8.14 10 5 5 169.08 8.99 10 -5 6 111.37 5.94 10 5 6 124.61 6.70 10 5 6 106.13 6.32 10 5 6 108.24 5.82 10 5 6 127.27 7.12 -10 5 -7 0.94 0.71 10 5 7 2.92 0.84 -10 5 -7 1.83 0.81 10 5 8 24.12 1.71 10 5 8 25.25 1.51 -10 5 -8 13.84 1.55 10 -6 -9 154.83 6.94 10 6 -8 18.88 1.93 10 -6 -8 15.74 1.90 10 6 -8 19.24 1.67 10 -6 -8 13.17 1.32 10 6 -8 18.25 1.68 10 -6 -7 128.80 6.91 10 6 -7 122.39 7.49 10 -6 -7 125.97 7.73 10 6 -7 142.32 6.95 10 -6 -7 142.12 6.87 10 6 -7 154.77 7.13 10 -6 -6 13.02 1.82 10 -6 -6 8.92 1.84 10 6 -6 7.75 1.86 10 6 -6 9.99 1.50 10 6 -6 10.36 1.55 10 -6 -5 105.57 6.45 10 6 -5 92.31 6.61 10 -6 -5 88.55 6.70 10 6 -5 91.90 6.79 10 6 -5 97.88 5.75 10 6 -5 102.38 5.90 10 -6 -4 18.54 1.94 10 6 -4 18.96 3.08 10 -6 -4 16.99 2.65 10 6 -4 20.22 2.34 10 6 -4 23.02 2.45 10 6 -4 23.75 3.13 10 6 -3 3.17 1.88 10 -6 -3 2.44 1.08 10 -6 -3 2.41 1.13 10 -6 -3 2.63 0.90 10 6 -3 2.22 1.29 10 6 -3 3.91 1.14 10 6 -3 3.69 1.18 10 6 -2 44.38 3.74 10 6 -2 42.59 3.68 -10 6 2 46.28 3.35 10 -6 -2 45.40 3.77 10 -6 -2 44.92 3.73 10 6 -2 50.76 4.41 10 -6 -2 43.37 3.19 10 6 -1 555.01 24.73 10 6 -1 506.99 28.12 10 -6 -1 572.55 24.68 10 -6 -1 574.06 24.67 10 6 -1 680.21 25.54 10 -6 -1 588.61 24.04 10 6 -1 561.42 24.81 10 6 -1 728.99 26.71 10 6 0 15.09 2.10 10 -6 0 13.52 1.71 10 6 0 19.53 2.64 10 6 0 14.96 2.09 10 -6 0 12.48 1.92 10 -6 0 13.42 1.97 10 6 1 270.92 13.32 10 -6 1 292.20 13.25 10 -6 1 297.75 13.24 10 6 1 265.79 13.28 10 6 1 315.23 14.45 10 -6 1 291.27 12.76 10 -6 2 1.92 0.83 10 -6 2 1.69 0.96 10 -6 2 1.41 0.86 10 6 2 1.90 1.00 10 -6 3 59.12 3.92 10 -6 3 55.90 3.88 10 -6 3 56.19 3.91 10 6 3 55.17 4.52 10 6 3 56.96 3.91 10 6 4 0.41 0.69 10 6 4 1.72 1.00 10 -6 4 0.62 0.67 10 -6 4 0.94 0.72 10 -6 4 0.72 0.82 10 -6 5 1.44 0.66 -10 6 -5 0.77 0.54 10 6 5 2.53 1.06 -10 6 -5 0.35 0.50 10 6 5 1.15 0.65 -10 6 -6 52.58 3.43 -10 6 -6 56.85 3.47 -10 6 -7 8.29 0.87 -10 6 -7 7.58 0.83 10 7 -7 36.01 2.23 10 7 -7 34.78 2.22 10 -7 -7 28.43 2.27 10 7 -6 35.58 2.50 10 -7 -6 35.65 2.46 10 -7 -6 27.83 2.04 10 7 -6 35.65 2.50 10 7 -6 34.64 2.90 10 7 -5 2.20 0.97 10 -7 -5 1.33 0.66 10 7 -5 0.78 0.62 10 7 -5 1.48 0.73 10 7 -4 20.59 2.11 10 7 -4 24.88 2.62 10 7 -4 18.19 2.51 10 -7 -4 22.06 2.38 10 7 -4 23.39 2.22 10 7 -3 2.54 1.40 10 7 -3 0.29 0.82 10 7 -3 1.65 0.80 10 7 -3 2.35 0.84 10 7 -2 3.94 1.01 10 7 -2 3.60 0.96 10 7 -2 5.58 1.24 10 7 -2 5.42 2.10 -10 7 2 3.84 1.14 10 -7 -2 4.73 1.17 10 -7 -2 4.55 1.18 10 7 -1 68.68 4.73 10 7 -1 75.18 4.88 10 7 -1 85.84 4.68 -10 7 1 82.15 4.55 10 -7 -1 78.37 4.85 10 -7 -1 78.94 4.83 10 7 0 1.41 1.32 10 7 0 1.90 0.76 10 7 0 1.01 0.67 -10 7 0 1.80 1.33 10 -7 0 1.16 0.86 10 -7 0 1.61 0.93 -10 7 -1 130.30 6.56 10 -7 1 124.41 6.55 10 -7 1 120.42 6.47 10 7 1 127.47 8.58 10 -7 2 70.38 4.23 10 -7 2 63.28 4.09 10 7 2 71.97 5.12 10 7 2 81.87 5.83 10 -7 3 161.03 7.92 10 -7 3 164.41 7.93 10 7 3 188.23 9.19 10 7 3 191.02 9.38 10 7 4 38.94 2.84 10 7 4 41.61 3.14 10 -7 4 32.52 2.37 10 -7 4 32.07 2.37 -10 7 -5 124.91 5.68 10 7 6 162.41 6.93 10 8 -5 10.82 1.03 10 8 -5 9.39 0.99 10 8 -4 136.56 6.34 10 -8 -4 122.76 6.18 10 8 -4 137.40 6.34 10 8 -3 129.09 6.35 10 8 -3 150.35 6.24 10 8 -3 133.47 6.82 10 -8 -3 134.18 6.52 10 8 -3 139.84 6.72 10 8 -3 128.05 6.33 10 8 -2 102.83 5.71 10 8 -2 90.67 4.21 10 8 -2 86.19 4.75 10 8 -2 97.15 5.12 10 8 -2 91.35 4.83 -10 8 1 10.70 1.19 10 -8 -1 9.38 1.26 10 -8 -1 9.65 1.28 10 8 -1 8.41 1.28 -10 8 0 9.26 1.25 10 -8 0 7.97 1.15 10 -8 0 10.84 1.28 10 8 0 8.15 1.29 10 8 0 8.89 1.63 -10 8 -1 4.50 1.04 10 -8 1 3.21 0.79 10 -8 1 3.44 0.81 10 8 1 2.60 0.77 10 8 1 3.45 1.05 -10 8 -2 149.03 6.35 10 -8 2 130.65 6.31 10 -8 2 133.97 6.32 10 8 3 0.37 0.45 -10 8 -3 0.75 0.67 10 -8 3 0.39 0.39 10 -8 3 0.33 0.41 -10 8 -4 0.55 0.40 11 0 -11 0.22 0.36 11 0 -11 0.21 0.36 11 0 -10 207.93 9.58 11 0 -10 192.83 9.62 11 0 -10 193.70 9.84 11 0 -10 197.25 9.91 11 0 -10 185.62 10.01 11 0 -9 1.96 1.02 11 0 -9 1.50 0.92 11 0 -9 0.55 0.74 11 0 -9 0.86 0.87 11 0 -8 42.41 4.37 11 0 -8 40.27 4.42 11 0 -8 35.96 4.09 11 0 -8 38.51 3.96 11 0 -8 38.21 3.50 11 0 -8 38.03 3.49 11 0 -8 36.74 3.51 11 0 -7 1.16 0.93 11 0 -7 0.98 1.07 11 0 -7 0.58 0.80 11 0 -7 1.82 1.04 11 0 -7 -0.20 0.77 11 0 -7 0.25 0.78 11 0 -6 176.41 10.45 11 0 -6 173.30 10.91 11 0 -6 174.28 9.73 11 0 -6 182.84 9.51 11 0 -6 161.34 9.54 11 0 -6 168.70 10.34 11 0 -6 180.75 11.10 11 0 -6 144.61 10.01 11 0 -6 165.11 9.74 11 0 -5 -1.33 0.71 11 0 -5 -0.19 0.77 11 0 -5 0.28 0.76 11 0 -5 0.23 0.54 11 0 -5 0.29 0.71 11 0 -5 0.87 0.87 11 0 -5 0.43 0.73 11 0 -5 1.09 1.14 11 0 -4 17.78 2.74 11 0 -4 19.60 2.76 11 0 -4 17.20 2.41 11 0 -4 20.90 2.99 11 0 -4 17.06 2.72 11 0 -4 18.06 2.93 11 0 -4 15.67 2.48 11 0 -4 14.79 2.82 11 0 -4 13.61 2.33 11 0 -4 18.98 2.54 11 0 -3 0.23 1.02 11 0 -3 0.82 0.86 11 0 -3 0.45 0.85 11 0 -3 0.20 0.76 11 0 -3 0.91 0.83 11 0 -3 0.24 0.96 11 0 -3 0.25 0.67 11 0 -3 5.01 2.97 11 0 -3 1.54 0.99 11 0 -3 1.13 0.98 11 0 -3 1.09 1.19 11 0 -2 1029.04 44.04 11 0 -2 1094.47 43.86 11 0 -2 1056.42 44.16 11 0 -2 1036.03 43.64 11 0 -2 1180.98 44.00 11 0 -2 1006.86 44.06 11 0 -2 1084.25 56.68 11 0 -2 1166.53 44.35 11 0 -2 1066.89 44.21 11 0 -2 1027.36 43.99 11 0 -1 3.03 1.43 11 0 -1 1.18 1.21 11 0 -1 0.82 1.02 11 0 -1 1.07 0.96 11 0 -1 1.82 1.17 11 0 -1 1.14 0.99 11 0 -1 1.65 1.17 11 0 -1 -1.01 1.22 11 0 0 318.59 15.01 11 0 0 323.54 15.21 11 0 0 289.47 15.23 11 0 0 293.32 15.17 11 0 0 292.22 15.45 11 0 0 313.89 15.72 11 0 0 304.36 24.59 11 0 1 0.96 0.96 11 0 1 1.04 1.26 11 0 1 1.01 1.01 11 0 1 2.43 1.21 11 0 1 0.21 0.78 11 0 2 271.60 13.25 11 0 2 248.84 13.34 11 0 2 251.89 22.30 11 0 2 254.13 13.08 11 0 2 222.17 12.52 11 0 3 0.66 1.00 11 0 3 1.86 1.12 11 0 3 0.66 1.22 11 0 3 -0.49 1.23 11 0 4 78.96 6.25 11 0 4 74.53 5.95 11 0 4 80.23 6.13 11 0 4 82.94 5.85 11 0 5 0.21 1.28 11 0 5 0.83 1.00 11 0 5 0.47 1.12 11 0 6 224.80 11.77 11 0 6 234.15 12.24 11 0 6 234.18 11.87 11 0 7 0.16 1.01 11 0 7 -0.36 1.10 11 0 7 0.75 0.87 11 0 8 23.89 2.28 -11 0 -8 24.46 2.46 -11 0 -9 -0.08 0.35 11 0 9 -0.26 0.58 11 -1 -11 28.13 2.08 11 -1 -11 28.80 2.29 11 -1 -11 30.03 2.17 11 -1 -10 22.91 2.36 11 -1 -10 21.66 2.37 11 -1 -10 16.26 2.24 11 1 -10 20.70 2.27 11 -1 -10 21.63 2.45 11 -1 -9 12.64 2.30 11 1 -9 15.50 2.24 11 -1 -9 12.20 2.21 11 1 -9 10.95 2.09 11 -1 -9 11.90 2.02 11 1 -9 8.82 1.80 11 -1 -9 11.11 2.04 11 -1 -9 13.75 2.00 11 1 -9 11.80 1.84 11 -1 -8 0.91 0.86 11 -1 -8 1.62 1.13 11 1 -8 1.32 0.96 11 1 -8 0.71 0.80 11 -1 -8 0.64 0.75 11 1 -8 1.15 0.84 11 1 -8 1.39 0.88 11 -1 -8 2.05 1.23 11 1 -8 -0.21 0.80 11 1 -8 1.60 1.00 11 -1 -8 0.45 0.79 11 -1 -8 0.15 0.72 11 1 -8 0.71 0.86 11 1 -8 0.90 0.81 11 -1 -8 1.59 1.13 11 -1 -7 10.05 2.29 11 1 -7 12.37 2.19 11 1 -7 11.41 2.10 11 -1 -7 12.17 2.09 11 -1 -7 13.10 2.02 11 -1 -7 13.49 2.06 11 1 -7 12.51 2.14 11 -1 -7 11.07 2.17 11 1 -7 14.01 2.41 11 1 -7 15.94 2.37 11 -1 -7 12.52 2.54 11 1 -7 11.43 2.26 11 1 -7 15.50 2.37 11 -1 -7 15.54 2.63 11 1 -6 13.72 2.22 11 -1 -6 12.78 2.42 11 1 -6 12.24 2.16 11 1 -6 9.44 1.98 11 -1 -6 9.45 1.97 11 1 -6 13.60 2.21 11 1 -6 11.74 2.29 11 1 -6 20.43 2.73 11 -1 -6 13.69 2.77 11 1 -6 8.74 2.02 11 -1 -6 10.60 2.49 11 1 -6 9.88 2.04 11 -1 -6 11.94 2.00 11 1 -6 11.77 2.17 11 -1 -6 10.87 1.95 11 1 -6 12.86 2.38 11 1 -5 48.76 4.38 11 -1 -5 47.30 4.50 11 1 -5 51.66 4.83 11 -1 -5 51.45 4.80 11 -1 -5 53.46 5.52 11 1 -5 51.49 4.49 11 1 -5 43.65 4.47 11 -1 -5 49.18 4.44 11 1 -5 53.25 5.05 11 -1 -5 55.26 5.63 11 1 -5 43.22 4.44 11 -1 -5 47.14 4.20 11 1 -5 47.99 4.44 11 -1 -5 50.96 4.37 11 1 -5 48.89 4.62 11 -1 -5 52.65 4.17 11 -1 -4 25.36 3.29 11 -1 -4 24.21 3.07 11 1 -4 19.34 3.06 11 1 -4 24.08 3.15 11 1 -4 24.38 2.88 11 -1 -4 25.23 3.55 11 1 -4 22.71 3.08 11 1 -4 19.16 2.92 11 -1 -4 25.46 3.06 11 1 -4 21.81 3.00 11 1 -4 26.89 3.16 11 1 -4 21.19 3.10 11 -1 -4 23.59 3.38 11 -1 -4 36.64 4.43 11 -1 -4 25.40 3.01 11 -1 -4 22.49 2.81 11 1 -4 21.36 3.06 11 1 -4 23.50 3.13 11 -1 -4 24.06 2.74 11 1 -3 145.17 9.24 11 -1 -3 155.82 9.49 11 -1 -3 166.09 8.91 11 1 -3 179.57 9.68 11 -1 -3 180.84 10.31 11 1 -3 168.96 9.70 11 -1 -3 165.95 9.50 11 1 -3 153.60 9.78 11 1 -3 150.15 9.59 11 -1 -3 161.04 9.34 11 1 -3 144.47 9.19 11 -1 -3 166.19 9.20 11 1 -3 151.09 9.33 11 1 -3 151.06 9.64 11 1 -3 177.04 9.55 11 -1 -3 188.29 11.12 11 1 -3 141.71 16.57 11 -1 -3 152.12 15.63 11 -1 -3 173.15 9.43 11 1 -3 151.16 9.69 11 -1 -3 159.32 9.24 11 1 -3 143.63 9.48 11 1 -2 16.12 2.59 11 -1 -2 16.72 2.69 11 1 -2 16.64 2.36 11 -1 -2 19.40 2.69 11 -1 -2 23.25 2.69 11 1 -2 20.43 2.91 11 -1 -2 18.49 2.69 11 1 -2 20.39 2.78 11 1 -2 16.31 2.80 11 -1 -2 24.11 2.96 11 -1 -2 20.26 2.63 11 1 -2 15.17 2.69 11 1 -2 18.73 5.84 11 -1 -2 17.97 5.25 11 1 -2 17.74 2.76 11 -1 -2 21.00 3.13 11 1 -2 17.11 2.78 11 -1 -2 19.14 2.67 11 1 -2 18.09 2.88 11 -1 -2 19.67 2.74 11 1 -1 4.90 1.37 11 1 -1 2.63 1.23 11 -1 -1 4.57 1.46 11 1 -1 5.53 3.54 11 -1 -1 4.49 2.66 11 1 -1 4.93 1.54 11 -1 -1 5.44 1.53 11 1 -1 4.16 1.57 11 -1 -1 4.76 1.49 11 -1 -1 4.41 1.49 11 1 -1 6.97 1.95 11 -1 -1 4.61 1.47 11 1 -1 4.75 1.64 11 -1 -1 6.30 1.62 11 1 -1 4.65 1.66 11 -1 -1 6.31 1.43 11 1 -1 4.77 1.61 11 -1 0 5.64 1.35 11 1 0 4.67 1.60 11 1 0 4.80 1.58 11 1 0 3.60 1.40 11 -1 0 3.55 1.29 11 -1 0 4.76 1.57 11 1 0 1.80 1.12 11 -1 0 4.51 1.41 11 1 0 3.51 1.52 11 -1 0 4.65 1.47 11 -1 0 4.02 1.40 11 1 0 1.30 1.10 11 1 0 4.22 1.33 11 1 0 6.71 3.58 11 -1 0 2.72 2.20 11 1 1 374.48 18.44 11 1 1 406.23 18.58 11 1 1 410.86 30.33 11 -1 1 440.91 28.91 11 -1 1 407.31 18.18 11 -1 1 413.57 18.47 11 1 1 389.65 19.08 11 1 1 361.30 19.35 11 -1 1 370.45 18.56 11 1 1 326.12 19.43 11 -1 1 363.89 18.71 11 -1 1 407.94 17.86 11 1 1 422.25 19.44 11 -1 2 227.15 11.62 11 1 2 185.69 19.82 11 -1 2 240.65 20.33 11 -1 2 218.52 11.19 11 1 2 220.64 12.53 11 -1 2 222.97 11.84 11 1 2 204.34 12.20 11 1 3 9.52 2.03 11 -1 3 11.66 2.02 11 -1 3 9.85 2.14 11 1 3 12.15 2.42 11 -1 3 11.28 1.93 11 1 3 12.03 2.41 11 -1 4 888.96 35.55 11 1 4 776.18 35.63 11 -1 4 822.61 34.35 11 1 4 893.83 36.54 11 1 4 852.00 35.37 11 1 4 824.03 35.73 11 -1 5 127.87 7.85 11 1 5 118.81 8.06 11 1 5 123.01 8.11 11 -1 5 110.97 7.21 11 1 5 123.76 7.66 11 1 5 134.73 8.59 11 1 6 7.43 1.86 11 1 6 6.43 1.48 11 1 6 5.87 1.70 11 -1 6 6.64 1.61 11 1 6 6.45 1.68 11 1 7 2.42 1.12 11 -1 7 1.62 0.92 11 1 7 2.36 1.15 11 1 7 1.60 1.20 -11 1 -7 0.95 0.74 -11 -1 -7 1.28 0.75 -11 1 -8 284.51 14.48 -11 -1 -8 307.54 14.43 11 1 8 356.47 15.09 11 -1 8 389.02 15.17 11 1 8 379.31 15.07 11 1 8 336.24 14.97 11 1 9 2.34 0.64 11 -1 9 4.13 0.87 11 1 9 4.38 0.87 11 -2 -11 1.86 0.43 11 2 -11 1.34 0.47 11 -2 -11 1.61 0.47 11 -2 -11 1.15 0.40 11 -2 -11 1.49 0.43 11 -2 -10 424.59 17.30 11 -2 -10 439.01 16.99 11 -2 -10 368.86 17.38 11 -2 -10 380.17 17.51 11 -2 -9 219.99 10.08 11 2 -9 218.77 10.61 11 -2 -9 205.60 10.68 11 2 -9 213.43 10.56 11 2 -9 215.46 10.59 11 -2 -9 181.45 10.95 11 -2 -9 183.56 10.79 11 -2 -9 202.17 10.00 11 -2 -8 16.83 2.50 11 -2 -8 15.29 2.02 11 2 -8 18.26 2.46 11 -2 -8 16.87 2.25 11 -2 -8 13.18 2.50 11 2 -8 17.06 2.43 11 2 -8 15.70 2.31 11 -2 -7 95.04 7.14 11 2 -7 107.46 6.76 11 2 -7 95.96 6.56 11 -2 -7 113.49 6.59 11 2 -7 101.76 6.88 11 2 -7 113.73 7.19 11 -2 -7 104.77 6.92 11 -2 -7 104.27 7.75 11 2 -7 112.06 7.31 11 2 -7 115.07 7.11 11 -2 -7 98.84 8.31 11 2 -7 105.40 6.87 11 2 -7 96.69 6.67 11 -2 -7 111.69 6.32 11 -2 -7 103.44 6.18 11 -2 -6 12.95 2.46 11 2 -6 11.13 1.96 11 2 -6 14.40 2.26 11 -2 -6 11.54 1.96 11 2 -6 7.97 1.95 11 2 -6 10.04 1.95 11 -2 -6 9.03 2.26 11 2 -6 11.00 2.05 11 -2 -6 9.04 2.42 11 2 -6 10.98 2.06 11 -2 -6 10.35 1.73 11 -2 -6 12.31 1.87 11 2 -6 9.78 2.00 11 -2 -6 13.69 2.31 11 -2 -5 15.93 2.62 11 -2 -5 20.75 2.78 11 -2 -5 18.03 2.51 11 2 -5 21.14 2.89 11 2 -5 23.57 3.12 11 -2 -5 21.90 3.60 11 2 -5 22.96 2.83 11 2 -5 22.61 2.86 11 -2 -5 18.43 2.85 11 2 -5 24.66 2.85 11 2 -5 20.81 2.83 11 -2 -5 20.72 3.57 11 -2 -5 20.26 2.48 11 2 -5 25.91 3.22 11 -2 -5 22.74 2.63 11 2 -5 20.98 2.94 11 -2 -4 39.58 4.06 11 2 -4 42.88 3.87 11 -2 -4 47.78 4.67 11 2 -4 45.14 4.17 11 -2 -4 47.62 5.33 11 -2 -4 48.48 4.12 11 2 -4 49.94 4.68 11 2 -4 42.40 4.25 11 2 -4 37.72 4.03 11 2 -4 46.55 4.00 11 2 -4 53.25 4.54 11 2 -4 43.46 4.43 11 -2 -4 51.56 5.33 11 2 -4 38.74 4.20 11 -2 -4 48.77 4.02 11 2 -4 37.83 4.19 11 -2 -4 56.12 4.27 11 -2 -4 48.17 3.72 11 -2 -3 287.35 14.40 11 2 -3 281.80 14.99 11 -2 -3 307.22 14.25 11 2 -3 274.95 14.97 11 -2 -3 295.59 15.48 11 2 -3 286.28 13.64 11 2 -3 304.13 14.35 11 2 -3 299.15 15.28 11 2 -3 249.38 14.26 11 -2 -3 288.83 14.08 11 2 -3 281.17 14.70 11 2 -3 305.88 14.95 11 -2 -3 306.76 16.59 11 2 -3 293.99 14.24 11 -2 -3 296.43 14.05 11 2 -3 267.80 14.66 11 -2 -3 302.50 14.05 11 2 -3 272.11 14.78 11 2 -2 309.16 15.39 11 2 -2 340.77 16.86 11 -2 -2 359.43 15.94 11 2 -2 296.72 16.39 11 2 -2 343.19 15.56 11 -2 -2 338.76 16.37 11 2 -2 322.01 16.78 11 -2 -2 341.30 15.81 11 2 -2 325.03 16.53 11 2 -2 283.49 15.97 11 2 -2 347.04 16.40 11 -2 -2 364.26 15.71 11 2 -2 269.45 24.76 11 -2 -2 364.10 24.31 11 2 -2 297.79 16.29 11 -2 -2 341.65 15.59 11 2 -2 303.82 16.46 11 -2 -2 350.67 15.72 11 2 -1 28.50 3.28 11 2 -1 27.04 7.02 11 -2 -1 27.41 6.02 11 2 -1 32.42 3.79 11 -2 -1 33.48 3.35 11 2 -1 30.02 3.79 11 2 -1 30.20 3.53 11 2 -1 25.96 3.44 11 -2 -1 29.44 3.24 11 -2 -1 27.26 3.02 11 2 -1 28.91 3.69 11 2 -1 23.83 3.35 11 -2 -1 27.54 3.04 11 2 -1 28.93 3.68 11 -2 -1 34.28 3.39 11 2 -1 30.66 3.91 11 2 0 1.14 1.04 11 2 0 -0.26 0.84 11 2 0 1.28 1.07 11 -2 0 1.65 0.91 11 -2 0 0.76 0.76 11 2 0 1.67 1.15 11 -2 0 2.24 1.00 11 2 0 2.20 1.09 11 2 0 0.73 0.93 11 -2 0 2.09 1.13 11 -2 0 0.56 0.82 11 2 0 1.32 1.15 11 2 0 0.68 0.83 11 2 0 1.12 1.36 11 -2 0 -0.81 0.98 11 2 1 134.38 8.68 11 2 1 118.98 8.70 11 -2 1 149.85 8.49 11 2 1 125.68 8.88 11 -2 1 142.46 8.26 11 2 1 120.85 8.62 11 -2 1 135.41 7.77 11 2 1 131.24 8.44 11 -2 1 151.38 8.28 11 2 1 120.64 8.55 11 2 1 131.50 8.80 11 2 1 132.30 9.36 11 2 2 15.00 2.89 11 2 2 17.58 2.30 11 2 2 15.18 2.68 11 -2 2 21.18 2.44 11 2 2 19.48 2.66 11 2 2 14.19 2.72 11 -2 2 19.33 2.57 11 2 3 6.62 1.56 11 2 3 5.26 1.99 11 2 3 8.09 2.31 11 -2 3 5.67 1.52 11 2 3 8.08 2.02 11 2 3 8.16 2.04 11 2 4 14.84 2.84 11 2 4 12.77 2.34 11 2 4 8.83 2.39 11 -2 4 11.23 1.99 11 2 4 13.93 2.39 11 2 5 45.64 4.28 11 2 5 42.54 4.71 11 -2 5 40.72 3.71 11 2 5 40.07 3.91 11 2 6 49.42 4.74 11 -2 6 45.87 3.79 11 2 6 44.51 3.87 11 2 6 40.69 4.35 11 2 6 45.25 3.99 -11 2 -7 4.62 1.16 -11 -2 -7 2.86 0.87 11 -2 7 3.12 1.07 11 2 7 4.64 1.15 11 2 7 5.28 1.62 11 2 7 4.16 1.04 11 2 7 3.02 1.24 -11 2 -8 24.25 2.44 -11 -2 -8 31.56 2.46 11 2 8 38.78 2.51 11 2 8 45.87 3.35 11 2 8 38.23 3.15 11 -2 8 34.47 2.67 11 2 8 37.82 2.71 -11 2 -9 1.25 0.58 11 2 9 4.23 0.79 11 -2 9 4.26 0.71 -11 2 -9 1.77 0.60 11 2 9 3.85 0.84 11 -3 -10 17.85 1.52 11 -3 -10 16.27 1.66 11 -3 -10 17.23 1.62 11 -3 -10 18.49 1.92 11 -3 -9 2.59 0.95 11 -3 -9 2.78 0.84 11 -3 -9 2.19 0.92 11 -3 -9 2.73 0.84 11 -3 -9 2.41 1.03 11 -3 -8 230.33 11.82 11 3 -8 223.11 11.32 11 3 -8 239.21 11.58 11 -3 -8 249.54 11.27 11 -3 -8 248.05 12.34 11 -3 -7 28.84 2.46 11 -3 -7 30.04 2.51 11 3 -7 22.19 2.56 11 3 -7 23.46 2.60 11 3 -7 22.14 2.85 11 -3 -7 26.53 2.55 11 3 -7 20.93 2.55 11 3 -7 21.90 2.69 11 -3 -7 24.11 3.69 11 3 -7 20.83 2.48 11 -3 -7 24.58 2.69 11 -3 -7 23.06 3.17 11 3 -6 8.84 1.85 11 -3 -6 8.15 2.32 11 3 -6 7.79 1.57 11 -3 -6 9.54 1.62 11 3 -6 7.78 1.65 11 -3 -6 4.88 1.15 11 3 -6 4.96 1.37 11 -3 -6 5.62 1.21 11 -3 -6 7.43 1.67 11 3 -5 1.65 1.07 11 3 -5 4.04 1.32 11 -3 -5 2.79 1.58 11 3 -5 3.79 1.21 11 -3 -5 3.85 1.06 11 -3 -5 4.93 1.19 11 3 -5 2.37 1.10 11 -3 -5 7.42 1.72 11 3 -5 3.79 1.17 11 -3 -5 3.96 1.17 11 3 -5 4.50 1.52 11 -3 -4 506.34 21.71 11 3 -4 483.46 21.37 11 3 -4 506.39 21.88 11 3 -4 474.28 22.74 11 -3 -4 472.99 23.72 11 3 -4 446.50 21.71 11 -3 -4 509.46 21.06 11 3 -4 482.68 22.00 11 -3 -4 507.92 21.08 11 3 -4 474.19 22.86 11 3 -4 468.82 21.49 11 -3 -4 540.15 21.54 11 3 -4 496.80 22.80 11 3 -4 433.14 21.68 11 -3 -4 495.44 23.88 11 -3 -4 542.79 22.52 11 3 -3 21.59 3.32 11 -3 -3 14.95 2.76 11 3 -3 19.38 3.00 11 3 -3 17.19 2.43 11 -3 -3 21.15 2.52 11 3 -3 18.63 2.90 11 3 -3 21.15 2.98 11 3 -3 19.09 2.67 11 -3 -3 17.34 2.18 11 3 -3 20.16 2.75 11 -3 -3 16.81 2.20 11 -3 -3 15.59 2.43 11 -3 -2 347.34 15.57 11 3 -2 331.77 17.18 11 -3 -2 343.55 15.14 11 3 -2 302.64 15.72 11 -3 -2 336.49 14.92 11 -3 -2 321.55 14.89 11 3 -2 299.53 15.64 11 3 -2 302.71 15.57 11 3 -2 307.46 15.23 11 -3 -2 348.54 15.23 11 3 -2 329.90 16.15 11 3 -2 299.51 16.17 11 3 -2 333.83 16.97 11 3 -2 304.85 15.30 11 -3 -1 40.93 3.50 11 3 -1 31.74 3.62 11 -3 -1 37.60 3.44 11 3 -1 34.14 3.80 11 3 -1 40.22 4.06 11 3 -1 51.73 5.18 11 -3 -1 36.99 3.44 11 3 -1 42.24 3.94 11 -3 -1 37.57 3.49 11 3 -1 47.16 4.30 11 3 -1 35.79 4.29 11 3 -1 40.48 4.07 11 3 -1 50.88 4.59 11 -3 0 23.67 2.58 11 3 0 13.70 2.75 11 3 0 13.25 2.24 11 -3 0 19.34 2.42 11 3 0 16.49 2.37 11 3 0 12.46 2.23 11 3 0 17.68 2.59 11 -3 0 19.18 2.31 11 3 0 14.95 2.45 11 -3 0 17.15 2.24 11 3 0 17.07 2.68 11 3 0 15.33 2.62 11 3 1 12.27 2.47 11 3 1 18.63 2.94 11 3 1 13.12 2.31 11 -3 1 14.61 2.09 11 3 1 11.85 2.18 11 -3 1 15.29 2.17 11 -3 1 17.71 2.27 11 3 1 20.47 3.07 11 3 1 15.29 2.29 11 -3 1 14.36 2.14 11 3 1 14.82 2.37 11 3 1 18.26 2.70 11 3 1 15.26 2.15 11 3 2 87.98 7.28 11 3 2 114.24 7.87 11 3 2 88.22 6.48 11 -3 2 104.61 6.43 11 -3 2 103.60 6.42 11 3 2 88.43 6.54 11 3 2 104.38 7.24 11 -3 2 110.70 6.43 11 3 2 100.45 6.70 11 3 2 113.27 6.41 11 3 2 94.10 6.45 11 -3 2 107.17 6.62 11 3 2 91.87 6.86 11 -3 3 10.45 1.73 11 3 3 11.14 1.93 11 3 3 9.30 2.45 11 3 3 10.74 1.93 11 -3 3 8.98 1.71 11 3 3 9.07 1.79 11 -3 3 10.38 1.75 11 3 3 12.46 1.86 11 3 3 8.96 2.30 11 3 4 4.36 1.15 11 -3 4 2.08 0.97 11 3 4 3.33 1.11 11 3 4 4.23 1.57 11 3 4 1.18 1.19 11 3 4 1.66 1.46 11 -3 5 15.86 1.97 11 3 5 15.78 2.04 11 3 5 14.28 2.71 11 3 5 13.86 2.39 11 3 5 13.58 1.81 11 3 5 15.28 2.76 11 3 6 347.08 15.67 11 -3 6 325.13 13.65 11 3 6 309.29 14.54 11 3 6 307.76 13.32 -11 -3 -6 274.22 13.24 11 3 6 306.65 15.10 11 3 7 140.12 7.50 11 3 7 136.04 6.71 11 3 7 119.57 6.02 11 -3 7 128.09 6.18 11 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11 4 -2 49.39 4.72 11 4 -2 49.61 4.67 11 -4 -2 49.84 4.10 11 4 -2 47.13 4.83 11 -4 -1 83.87 5.59 11 4 -1 88.39 7.43 11 4 -1 69.32 5.89 11 -4 -1 86.56 5.26 11 4 -1 78.71 5.88 11 4 -1 63.89 5.98 11 4 -1 78.01 6.54 11 4 -1 95.17 6.68 11 4 0 103.03 8.03 11 4 0 93.14 7.18 11 -4 0 91.62 5.72 11 4 0 89.57 7.31 11 4 0 108.24 7.25 11 4 1 120.25 8.50 11 4 1 100.06 7.78 11 -4 1 111.15 6.33 11 4 1 111.19 7.51 11 4 1 95.63 7.75 11 4 2 69.29 5.65 11 4 2 69.97 6.25 11 4 2 76.00 6.31 11 4 2 68.09 5.77 11 -4 2 71.52 4.75 11 4 2 69.55 6.20 11 4 2 85.83 5.20 11 4 3 68.16 5.90 11 -4 3 74.71 4.84 11 4 3 83.47 6.47 11 4 3 82.46 5.05 11 4 4 101.86 7.21 11 4 4 100.15 6.97 11 -4 4 90.69 5.40 11 4 4 104.22 7.12 11 4 4 97.89 5.58 11 4 5 139.14 8.50 11 4 5 159.68 8.77 11 -4 5 138.50 7.01 11 4 5 152.63 8.61 11 4 5 139.19 7.15 11 4 6 241.55 10.65 11 -4 6 223.92 10.32 11 4 6 269.71 12.08 11 4 6 266.23 11.92 11 4 7 10.58 1.23 11 4 7 12.45 1.49 11 4 7 12.57 1.69 -11 4 -8 3.22 0.76 -11 4 -8 2.63 0.76 11 -5 -9 151.53 6.50 11 -5 -8 28.63 1.85 11 -5 -8 37.53 3.05 11 5 -8 35.27 2.75 11 -5 -8 37.14 2.59 11 5 -7 237.32 12.56 11 -5 -7 243.31 12.96 11 -5 -7 268.36 11.25 11 -5 -7 287.83 12.66 11 -5 -7 280.32 11.49 11 -5 -7 291.55 12.40 11 -5 -6 25.01 2.19 11 -5 -6 28.99 3.00 11 -5 -6 23.93 3.06 11 5 -6 22.66 3.00 11 -5 -5 105.53 5.80 11 -5 -5 98.00 6.74 11 -5 -5 93.15 7.01 11 5 -5 105.92 7.19 11 5 -4 29.05 3.57 11 5 -4 26.42 2.90 11 -5 -4 31.05 2.86 11 -5 -4 33.62 3.66 11 -5 -3 96.73 6.09 11 -5 -3 104.64 5.93 11 5 -3 105.06 7.27 11 5 -3 104.06 6.70 11 5 -2 19.07 2.61 11 5 -2 18.51 3.35 11 -5 -2 19.87 2.23 11 5 -2 21.83 2.85 11 5 -1 145.01 8.02 11 -5 -1 136.40 7.31 11 5 -1 116.14 7.90 11 5 -1 150.76 8.67 11 5 -1 117.95 9.45 11 5 0 63.57 5.79 11 5 0 67.29 5.41 11 5 0 65.88 5.39 11 5 0 81.90 7.18 11 5 0 83.78 5.97 11 -5 0 74.10 4.84 11 5 1 61.98 4.98 11 5 1 52.12 5.27 11 5 1 58.80 4.88 11 5 1 60.14 5.95 11 5 2 31.17 2.82 11 5 2 30.50 3.30 11 5 2 30.68 3.96 11 5 2 34.40 3.54 11 5 2 36.37 4.21 11 5 3 19.39 2.96 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318.47 11.92 11 -6 5 241.60 10.39 -11 6 -6 23.88 1.69 11 6 6 30.84 1.96 11 7 -6 0.45 0.41 11 -7 -5 21.88 1.73 11 -7 -5 25.93 2.05 11 7 -4 103.17 5.33 11 7 -4 99.45 5.15 11 7 -3 41.88 2.84 11 -7 -3 40.50 3.12 11 7 -3 38.71 3.05 11 7 -3 36.25 3.46 11 7 -2 3.44 0.96 11 7 -2 3.12 0.71 -11 7 1 139.68 6.19 11 7 -1 140.17 8.28 11 7 -1 127.32 7.05 -11 7 0 67.38 3.62 11 7 0 64.59 4.22 11 -7 0 56.14 3.26 -11 7 -1 6.23 1.27 11 7 1 5.95 1.13 11 7 1 5.53 1.49 -11 7 -2 75.21 4.06 11 7 2 77.05 4.75 -11 7 -3 3.38 0.92 11 7 3 1.89 0.65 11 7 3 1.87 0.69 11 7 4 -0.06 0.35 11 8 -3 69.92 3.45 11 -8 -2 22.02 1.64 11 -8 -1 0.49 0.32 11 8 0 89.67 4.51 11 8 1 19.54 1.46 12 0 -10 10.42 1.21 12 0 -10 9.31 1.25 12 0 -10 9.36 1.29 12 0 -9 1.23 0.81 12 0 -9 0.62 0.63 12 0 -9 0.30 0.54 12 0 -9 0.32 0.55 12 0 -8 25.73 2.81 12 0 -8 20.58 2.75 12 0 -8 23.50 2.65 12 0 -8 21.55 2.72 12 0 -8 23.64 2.49 12 0 -7 0.17 0.72 12 0 -7 0.59 0.67 12 0 -7 0.33 0.71 12 0 -7 0.33 0.77 12 0 -7 -0.64 0.99 12 0 -7 0.74 0.94 12 0 -7 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3.77 14 0 2 56.79 4.37 14 0 2 55.50 4.30 14 0 2 57.33 4.39 14 0 3 -0.15 0.73 14 0 3 0.33 0.59 14 0 3 -0.28 0.66 14 0 3 1.45 0.88 14 0 3 -0.18 0.49 14 0 4 48.36 2.98 14 0 4 38.52 2.56 14 0 4 44.97 3.38 14 0 4 45.26 3.43 14 0 4 53.09 3.64 14 0 5 -0.09 0.56 14 0 5 0.09 0.57 14 0 5 0.55 0.54 14 0 6 3.26 0.63 14 0 6 2.77 0.54 14 0 6 2.41 0.52 14 -1 -8 50.95 2.79 14 -1 -7 71.66 4.17 14 -1 -7 69.27 4.07 14 -1 -6 148.94 7.23 14 1 -6 150.66 7.56 14 -1 -6 161.02 7.31 14 1 -6 144.13 7.46 14 1 -6 141.44 7.33 14 -1 -6 152.51 7.38 14 -1 -6 151.45 7.73 14 1 -5 23.39 2.42 14 -1 -5 26.24 2.35 14 1 -5 30.29 2.55 14 1 -5 22.92 2.41 14 -1 -5 25.39 2.35 14 -1 -5 23.79 2.58 14 1 -5 21.81 2.35 14 -1 -5 24.91 2.40 14 1 -4 2.57 0.90 14 1 -4 3.13 1.04 14 -1 -4 2.96 1.01 14 1 -4 2.92 1.02 14 -1 -4 1.77 0.77 14 1 -4 1.22 0.85 14 -1 -4 2.50 0.90 14 -1 -4 3.51 1.13 14 -1 -3 38.78 3.69 14 1 -3 36.56 3.43 14 -1 -3 43.06 3.52 14 1 -3 43.33 3.71 14 -1 -3 43.78 3.45 14 1 -3 40.33 3.62 14 -1 -3 47.54 3.60 14 -1 -3 44.19 2.97 14 1 -3 43.96 3.58 14 -1 -2 254.56 12.52 14 -1 -2 263.78 11.54 14 1 -2 251.35 12.72 14 -1 -2 274.50 12.43 14 1 -2 256.73 12.83 14 -1 -2 283.06 12.56 14 1 -2 277.70 12.73 14 -1 -2 240.84 12.71 14 1 -2 251.95 12.66 14 -1 -2 272.26 12.58 14 1 -1 0.36 0.90 14 -1 -1 1.50 0.83 14 1 -1 0.70 0.87 14 -1 -1 2.19 1.00 14 -1 -1 1.73 1.07 14 -1 -1 1.88 0.99 14 1 -1 1.51 1.02 14 -1 -1 2.20 0.69 14 1 -1 0.65 0.76 14 -1 -1 0.79 0.87 14 1 -1 1.18 1.00 14 1 -1 0.84 0.86 14 -1 -1 2.60 1.11 14 -1 0 79.79 5.30 14 1 0 72.14 5.27 14 -1 0 95.50 5.66 14 1 0 88.38 5.67 14 1 0 68.94 5.29 14 -1 0 80.10 5.21 14 1 0 74.44 5.49 14 -1 0 85.19 5.38 14 1 0 86.74 5.55 14 -1 0 68.12 5.21 14 -1 0 85.61 5.45 14 1 0 82.65 5.73 14 1 1 89.89 5.92 14 -1 1 98.00 5.78 14 1 1 83.89 5.85 14 -1 1 99.20 5.85 14 1 1 93.48 5.82 14 1 1 85.64 5.75 14 -1 1 91.40 5.75 14 -1 1 97.09 5.39 14 1 1 92.29 5.92 14 -1 1 88.83 5.64 14 -1 1 91.61 5.76 14 1 1 86.79 5.94 14 1 2 54.34 4.30 14 -1 2 61.18 4.25 14 1 2 51.81 4.26 14 -1 2 54.68 4.10 14 1 2 56.17 4.18 14 1 2 54.87 4.21 14 -1 2 62.22 4.41 14 -1 2 67.63 3.92 14 1 2 59.92 4.38 14 -1 2 61.44 4.21 14 -1 2 62.92 4.35 14 1 2 58.99 4.48 14 1 3 45.07 3.59 14 -1 3 46.06 3.48 14 1 3 41.84 3.52 14 -1 3 46.05 3.52 14 1 3 47.97 3.52 14 1 3 44.07 3.50 14 -1 3 44.26 3.50 14 -1 3 47.72 2.98 14 1 3 49.94 3.65 14 -1 3 55.92 3.61 14 -1 3 49.44 3.58 14 1 3 47.00 3.70 14 1 4 18.23 1.89 14 -1 4 18.42 1.97 14 1 4 17.59 1.85 14 1 4 16.59 1.75 14 1 4 15.93 1.85 14 -1 4 15.45 1.78 14 1 4 16.82 1.92 14 -1 4 19.60 1.97 14 -1 4 17.49 1.89 14 1 4 15.35 1.88 14 -1 5 4.63 0.91 14 1 5 5.63 0.99 14 1 5 5.01 0.80 14 1 5 5.29 0.86 14 -1 5 6.29 1.00 14 1 5 5.25 0.91 14 -1 5 3.71 0.79 14 1 5 5.15 0.90 14 -1 5 3.50 0.78 14 1 5 4.85 0.75 14 -1 6 8.30 0.85 14 -1 6 6.96 0.78 14 1 6 8.50 0.85 14 1 6 7.28 0.75 14 -1 6 7.19 0.77 14 1 6 6.49 0.74 14 -1 6 7.48 0.78 14 -2 -7 19.37 1.67 14 -2 -7 16.87 1.69 14 -2 -6 15.37 1.74 14 -2 -6 15.06 1.55 14 -2 -5 2.37 0.79 14 -2 -5 1.28 0.59 14 2 -5 1.54 0.72 14 -2 -5 1.02 0.56 14 2 -5 1.41 0.74 14 2 -5 2.33 0.84 14 -2 -4 71.00 4.27 14 2 -4 58.87 4.27 14 -2 -4 70.98 4.08 14 2 -4 64.35 4.50 14 2 -4 57.26 4.23 14 -2 -4 64.47 3.95 14 -2 -3 4.47 1.08 14 2 -3 2.40 0.95 14 -2 -3 3.51 0.92 14 2 -3 2.37 0.95 14 -2 -3 4.11 0.97 14 -2 -3 3.19 1.16 14 2 -3 3.22 1.11 14 -2 -2 12.36 1.60 14 -2 -2 9.43 1.42 14 2 -2 9.10 1.65 14 2 -2 10.51 1.72 14 -2 -2 11.23 1.89 14 2 -2 10.01 1.79 14 -2 -2 13.27 1.87 14 -2 -2 10.19 1.56 14 2 -1 5.53 1.33 14 -2 -1 5.39 1.13 14 2 -1 6.96 1.42 14 -2 -1 6.56 1.24 14 -2 -1 6.77 1.50 14 -2 -1 7.42 1.36 14 2 -1 4.70 1.32 14 -2 -1 6.28 1.43 14 2 -1 5.91 1.50 14 2 -1 7.47 1.60 14 -2 -1 6.51 1.27 14 2 0 55.48 4.34 14 -2 0 64.65 4.24 14 2 0 60.01 4.48 14 -2 0 67.16 4.30 14 2 0 67.32 4.97 14 -2 0 71.71 4.49 14 -2 0 70.90 4.66 14 -2 0 69.38 4.41 14 2 0 56.69 4.50 14 2 1 52.87 4.03 14 -2 1 59.14 3.92 14 2 1 53.05 4.08 14 -2 1 62.53 4.03 14 2 1 58.43 4.58 14 -2 1 66.47 4.22 14 2 1 67.06 4.79 14 -2 1 59.87 4.22 14 -2 1 59.39 4.00 14 2 1 57.55 4.28 14 2 2 30.49 2.77 14 -2 2 35.46 2.75 14 2 2 30.51 2.77 14 -2 2 34.58 2.76 14 2 2 34.18 3.24 14 -2 2 34.58 2.83 14 2 2 36.74 3.33 14 -2 2 34.13 2.96 14 -2 2 37.25 2.88 14 2 2 34.26 2.97 14 2 3 45.16 3.24 14 -2 3 48.62 3.22 14 2 3 43.55 3.24 14 -2 3 45.23 3.19 14 2 3 47.25 3.74 14 -2 3 52.74 3.43 14 2 3 52.49 3.90 14 -2 3 55.80 3.64 14 -2 3 52.82 3.37 14 2 3 51.13 3.49 14 -2 4 26.04 2.02 14 -2 4 23.57 1.97 14 2 4 24.79 2.32 14 -2 4 28.90 2.20 14 2 4 30.31 2.51 14 -2 4 27.13 2.23 14 -2 4 28.50 2.12 14 -2 5 121.10 5.75 14 -2 5 115.22 5.73 14 -2 5 146.97 6.09 14 2 5 143.16 6.25 14 2 5 139.05 6.17 14 -2 5 152.72 6.22 14 -2 5 132.71 5.84 14 -3 -7 118.37 5.20 14 -3 -7 123.80 5.18 14 -3 -7 107.29 5.33 14 -3 -6 24.22 1.92 14 -3 -5 77.34 4.08 14 -3 -5 80.69 4.55 14 -3 -4 78.34 4.06 14 -3 -4 77.66 4.04 14 -3 -4 86.64 4.47 14 -3 -4 84.57 4.94 14 -3 -3 191.90 8.57 14 -3 -3 192.32 8.60 14 -3 -3 201.95 8.96 14 -3 -3 201.59 9.63 14 -3 -2 1.50 0.57 14 -3 -2 1.33 0.54 14 -3 -2 0.86 0.60 14 -3 -2 1.15 0.82 14 3 -1 110.56 7.07 14 -3 -1 123.86 5.96 14 -3 -1 122.63 5.99 14 -3 -1 128.41 6.29 14 3 -1 113.67 6.91 14 -3 -1 123.60 6.58 14 3 0 52.49 4.32 14 -3 0 57.63 3.89 14 -3 0 52.42 3.26 14 -3 0 51.86 3.28 14 -3 0 63.00 3.66 14 3 0 56.58 4.32 14 -3 1 101.45 5.10 14 -3 1 100.70 5.00 14 -3 1 99.02 5.02 14 3 1 94.96 6.22 14 -3 1 102.86 5.26 14 3 1 92.08 6.06 14 -3 2 26.05 1.91 14 -3 2 21.32 1.74 14 -3 2 23.51 1.81 14 3 2 24.03 2.61 14 -3 2 26.20 2.06 14 -3 3 19.57 1.46 14 -3 3 23.56 1.71 14 -3 3 18.03 1.39 14 -3 3 15.94 1.36 14 3 3 21.32 2.17 14 -3 4 8.47 0.89 14 3 4 9.52 1.27 14 3 5 91.61 4.04 14 3 5 79.56 3.93 14 -4 -6 0.63 0.30 14 -4 -6 0.67 0.31 14 -4 -5 3.77 0.65 14 -4 -5 3.63 0.73 14 4 -4 37.56 2.78 14 -4 -4 35.25 2.00 14 -4 -3 116.42 5.62 14 4 -3 106.98 5.74 14 -4 -3 99.74 4.74 14 -4 -2 120.84 5.99 14 -4 -2 108.70 5.08 14 4 -2 108.51 6.12 14 -4 -1 58.54 3.71 14 -4 -1 52.28 2.91 14 -4 -1 54.21 3.39 14 4 -1 54.65 3.86 14 -4 0 198.13 8.58 14 4 0 169.23 8.67 14 -4 0 163.21 7.42 14 -4 0 189.98 8.20 14 4 1 63.17 3.80 14 -4 1 66.55 3.56 14 4 2 101.21 5.27 14 -4 2 99.05 4.96 14 4 3 44.37 2.76 14 -4 3 45.64 2.63 14 4 4 2.91 0.48 14 -4 4 2.82 0.47 14 -5 -4 4.16 0.62 14 -5 -3 6.97 0.77 14 -5 -2 38.22 2.32 14 -5 -1 5.59 0.82 14 -5 0 0.06 0.37 14 -5 1 17.23 1.23 14 -5 1 20.75 1.53 14 -5 2 21.37 1.44 15 0 -5 -0.08 0.42 15 0 -5 0.47 0.43 15 0 -5 0.08 0.42 15 0 -4 2.63 0.88 15 0 -4 2.66 0.74 15 0 -4 2.55 0.77 15 0 -3 -0.11 0.65 15 0 -3 0.43 0.58 15 0 -3 -0.11 0.51 15 0 -2 824.41 33.21 15 0 -2 832.24 33.21 15 0 -2 850.70 33.29 15 0 -2 837.82 32.43 15 0 -1 0.37 0.47 15 0 -1 0.71 0.71 15 0 -1 0.36 0.71 15 0 -1 0.59 0.68 15 0 0 326.14 14.08 15 0 0 321.98 14.07 15 0 0 310.21 13.10 15 0 0 333.46 14.22 15 0 0 313.83 13.99 15 0 1 -0.47 0.66 15 0 1 -0.17 0.32 15 0 1 -0.11 0.52 15 0 1 -0.33 0.59 15 0 1 0.11 0.57 15 0 2 214.91 10.16 15 0 2 216.04 10.18 15 0 2 230.85 10.22 15 0 2 247.75 10.47 15 0 3 0.32 0.43 15 0 3 0.73 0.48 15 0 3 -0.08 0.54 15 0 3 0.38 0.51 15 0 4 27.74 1.81 15 0 4 24.42 1.75 15 0 4 29.64 1.90 15 0 4 27.30 1.78 15 -1 -6 0.73 0.38 15 -1 -5 0.29 0.44 15 -1 -5 -0.19 0.41 15 1 -5 0.70 0.45 15 -1 -5 0.25 0.36 15 1 -5 0.77 0.50 15 -1 -5 0.50 0.49 15 -1 -4 29.96 2.35 15 -1 -4 31.94 2.28 15 1 -4 28.98 2.37 15 1 -4 27.05 2.31 15 -1 -4 32.44 2.30 15 -1 -4 29.96 2.46 15 -1 -3 23.31 2.07 15 1 -3 19.00 1.97 15 1 -3 21.13 2.10 15 -1 -3 21.76 1.96 15 1 -3 16.40 1.88 15 -1 -3 21.08 1.91 15 1 -3 19.81 1.89 15 1 -2 12.64 1.68 15 -1 -2 17.78 1.90 15 1 -2 17.90 1.94 15 -1 -2 17.41 1.79 15 1 -2 15.54 1.86 15 -1 -2 18.42 1.83 15 1 -2 18.35 1.84 15 1 -1 9.20 1.42 15 -1 -1 11.81 1.53 15 1 -1 9.53 1.48 15 -1 -1 11.25 1.45 15 1 -1 9.35 1.44 15 -1 -1 10.65 1.44 15 1 -1 8.12 1.28 15 1 0 1.25 0.62 15 1 0 0.82 0.62 15 -1 0 0.60 0.57 15 1 0 1.03 0.62 15 -1 0 0.78 0.58 15 1 0 0.53 0.66 15 -1 0 1.15 0.73 15 -1 1 7.83 1.21 15 1 1 11.70 1.35 15 -1 1 9.91 1.34 15 1 1 7.55 1.28 15 1 1 7.92 1.27 15 -1 1 12.03 1.47 15 1 1 10.36 1.52 15 1 1 9.07 1.29 15 -1 1 9.69 1.36 15 1 1 8.57 1.35 15 1 2 31.58 2.50 15 -1 2 36.23 2.52 15 1 2 33.23 2.57 15 -1 2 31.95 2.44 15 1 2 28.46 2.24 15 1 2 35.51 2.50 15 -1 2 36.89 2.61 15 1 2 37.00 2.59 15 -1 2 37.50 2.61 15 1 2 34.30 2.64 15 1 3 3.43 0.71 15 -1 3 3.87 0.74 15 1 3 4.40 0.78 15 -1 3 3.90 0.74 15 -1 3 3.43 0.77 15 1 3 4.66 0.88 15 -1 3 4.45 0.79 15 1 4 88.09 3.85 15 1 4 73.89 3.66 15 -1 4 84.20 3.74 15 1 4 73.91 3.67 15 -1 4 77.75 3.70 15 -1 4 95.27 3.93 15 -2 -5 45.45 2.55 15 -2 -4 0.69 0.36 15 -2 -4 0.84 0.38 15 -2 -4 1.07 0.61 15 -2 -4 0.20 0.39 15 -2 -3 70.48 3.78 15 -2 -3 65.59 3.48 15 2 -3 62.96 3.92 15 -2 -3 60.62 3.42 15 -2 -3 63.07 3.97 15 -2 -2 126.97 5.80 15 -2 -2 105.17 5.41 15 -2 -2 106.04 5.39 15 2 -2 118.22 6.07 15 -2 -2 115.81 6.05 15 -2 -1 10.73 1.23 15 -2 -1 10.74 1.24 15 2 -1 10.53 1.49 15 -2 -1 12.41 1.40 15 -2 -1 10.45 1.42 15 -2 -1 11.73 1.56 15 -2 0 4.64 0.84 15 -2 0 5.48 0.88 15 -2 0 5.05 0.93 15 -2 0 5.70 1.05 15 2 0 6.38 1.17 15 -2 1 99.02 4.87 15 -2 1 93.94 4.84 15 -2 1 108.51 5.15 15 2 1 103.45 5.55 15 -2 1 106.49 5.27 15 2 1 98.51 5.43 15 -2 2 15.65 1.34 15 -2 2 13.89 1.28 15 -2 2 19.49 1.62 15 2 2 14.59 1.54 15 -2 2 20.92 1.58 15 2 2 16.52 1.70 15 2 3 0.53 0.32 15 2 3 0.77 0.37 15 -2 3 0.54 0.34 15 -3 -4 170.06 7.47 15 3 -3 3.15 0.73 15 -3 -3 3.63 0.59 15 3 -2 43.14 2.94 15 -3 -2 41.09 2.39 15 3 -1 112.73 5.91 15 -3 -1 120.11 5.75 15 -3 -1 109.66 5.11 15 3 0 30.87 2.39 15 -3 0 30.90 2.25 15 -3 0 25.65 1.76 15 3 1 26.26 2.09 15 -3 1 26.26 1.93 15 -3 1 24.00 1.53 15 3 2 61.54 3.30 15 4 -2 10.54 0.96 15 -4 -2 12.36 1.04 15 4 -1 4.46 0.63 15 -4 -1 4.84 0.66 15 4 0 55.74 2.82 16 0 -3 0.09 0.21 16 0 -3 0.26 0.26 16 0 -2 5.26 0.75 16 0 -2 6.92 0.82 16 0 -2 6.09 0.77 16 0 -1 0.43 0.31 16 0 -1 0.64 0.34 16 0 -1 0.26 0.34 16 0 0 44.23 2.53 16 0 0 46.45 2.53 16 0 0 45.59 2.50 16 -1 -2 131.74 5.67 16 1 -2 130.44 5.77 16 -1 -2 137.37 5.69 16 1 -2 124.52 5.73 16 -1 -2 149.15 5.90 16 -1 -1 0.97 0.33 16 1 -1 0.62 0.29 16 -1 -1 1.28 0.35 16 1 -1 0.66 0.32 16 -1 -1 0.74 0.35 16 -1 0 46.53 2.46 0 0 0 0.00 0.00 TITL G-62_g in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 12.621835 8.775848 11.599297 90.0000 94.8294 90.0000 ZERR 4.00 0.000128 0.000094 0.000115 0.0000 0.0009 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Cl UNIT 44.00 48.00 8.00 12.00 8.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 SIZE 0.16 0.35 0.45 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 54128 _shelx_res_file ; TITL g-62_g_a.res in P2(1)/c g-62_g.res created by SHELXL-2018/3 at 16:07:34 on 23-Dec-2024 REM Old TITL G-62_g in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.085, Rweak 0.025, Alpha 0.019, Orientation as input REM Formula found by SHELXT: C11 N2 O3 Cl2 CELL 1.54184 12.62183 8.77585 11.5993 90 94.8294 90 ZERR 4 0.00013 0.00009 0.00011 0 0.0009 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl N O UNIT 44 48 8 8 12 EQIV $1 +X,1.5-Y,-0.5+Z EQIV $2 -X,-0.5+Y,0.5-Z EQIV $3 -X,0.5+Y,0.5-Z EQIV $4 -X,1-Y,1-Z L.S. 11 PLAN 5 SIZE 0.16 0.35 0.45 TEMP -173 CONF HTAB N1 O4_$1 HTAB N1 O4_$2 HTAB N3 O2_$3 HTAB O4 O2_$4 BOND $H list 4 MORE -1 fmap 2 53 acta REM REM REM WGHT 0.065500 0.630200 FVAR 0.61138 CL1 3 0.226292 0.882414 0.406871 11.00000 0.02394 0.01729 = 0.02111 0.00018 0.00407 -0.00221 CL2 3 0.248189 0.702795 0.619151 11.00000 0.02628 0.02911 = 0.01385 -0.00215 0.00155 0.00153 O2 5 0.023921 0.375164 0.314047 11.00000 0.03126 0.01943 = 0.01643 -0.00014 0.00646 -0.00603 O4 5 0.032861 0.723842 0.489259 11.00000 0.02290 0.02065 = 0.01504 0.00206 0.00733 0.00161 O6 5 0.275914 0.458818 0.394183 11.00000 0.02701 0.02220 = 0.02902 -0.00488 0.00570 0.00147 N1 4 0.038257 0.499745 0.145617 11.00000 0.03045 0.01890 = 0.01443 -0.00086 0.00372 -0.00606 N3 4 0.083273 0.622870 0.316165 11.00000 0.02533 0.01516 = 0.01392 0.00159 0.00317 -0.00104 C2 1 0.046828 0.493436 0.261849 11.00000 0.01994 0.01785 = 0.01685 0.00011 0.00427 0.00029 C4 1 0.106816 0.630309 0.438991 11.00000 0.02175 0.01756 = 0.01394 0.00084 0.00416 -0.00119 AFIX 13 H4A 2 0.103457 0.525355 0.472057 11.00000 -1.20000 AFIX 0 C5 1 0.220708 0.694739 0.465688 11.00000 0.02255 0.01823 = 0.01499 -0.00048 0.00348 -0.00067 C6 1 0.304850 0.586898 0.417466 11.00000 0.02346 0.02257 = 0.01561 -0.00060 0.00395 0.00267 C7 1 0.414414 0.640443 0.401654 11.00000 0.02148 0.02579 = 0.02030 0.00212 0.00296 0.00263 C8 1 0.468191 0.563447 0.318773 11.00000 0.02769 0.03073 = 0.02580 -0.00057 0.00612 0.00437 AFIX 43 H8 2 0.433483 0.484415 0.274165 11.00000 -1.20000 AFIX 0 C9 1 0.572454 0.602356 0.301497 11.00000 0.02787 0.03904 = 0.03077 0.00651 0.01054 0.00808 AFIX 43 H9 2 0.607516 0.551826 0.243057 11.00000 -1.20000 AFIX 0 C10 1 0.626169 0.713783 0.368202 11.00000 0.02311 0.03773 = 0.03717 0.01617 0.00632 0.00182 C11 1 0.572426 0.790012 0.451412 11.00000 0.02685 0.03460 = 0.03579 0.00401 -0.00001 -0.00413 AFIX 43 H11 2 0.608274 0.866470 0.497716 11.00000 -1.20000 AFIX 0 C12 1 0.467170 0.755541 0.467420 11.00000 0.02626 0.03050 = 0.02597 -0.00100 0.00388 -0.00102 AFIX 43 H12 2 0.431028 0.810101 0.523000 11.00000 -1.20000 AFIX 0 C13 1 0.741301 0.751374 0.353511 11.00000 0.02582 0.05290 = 0.05457 0.02098 0.01038 -0.00183 AFIX 137 H13A 2 0.762750 0.702446 0.283178 11.00000 -1.50000 H13B 2 0.786149 0.713990 0.420656 11.00000 -1.50000 H13C 2 0.749543 0.862022 0.347188 11.00000 -1.50000 AFIX 0 H1A 2 0.058987 0.573870 0.110391 11.00000 0.02991 H1B 2 0.018302 0.419608 0.109894 11.00000 0.02814 H3 2 0.072534 0.700962 0.280464 11.00000 0.02295 H4 2 0.013524 0.682858 0.543189 11.00000 0.03363 HKLF 4 REM g-62_g_a.res in P2(1)/c REM wR2 = 0.1038, GooF = S = 1.055, Restrained GooF = 1.055 for all data REM R1 = 0.0368 for 2738 Fo > 4sig(Fo) and 0.0374 for all 2808 data REM 180 parameters refined using 0 restraints END WGHT 0.0655 0.6302 REM Highest difference peak 0.509, deepest hole -0.426, 1-sigma level 0.072 Q1 1 0.2660 0.6405 0.4458 11.00000 0.05 0.51 Q2 1 0.1658 0.6625 0.4484 11.00000 0.05 0.46 Q3 1 0.3631 0.6184 0.4152 11.00000 0.05 0.43 Q4 1 0.6775 0.7257 0.3637 11.00000 0.05 0.37 Q5 1 0.7579 0.8028 0.2975 11.00000 0.05 0.31 ; _shelx_res_checksum 28237 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl1 0.22629(3) 0.88241(4) 0.40687(3) 0.02066(13) Uani d 1 . . Cl Cl2 0.24819(3) 0.70279(5) 0.61915(3) 0.02309(13) Uani d 1 . . O O2 0.02392(10) 0.37516(13) 0.31405(10) 0.0221(3) Uani d 1 . . O O4 0.03286(9) 0.72384(13) 0.48926(10) 0.0192(2) Uani d 1 . . O O6 0.27591(10) 0.45882(14) 0.39418(11) 0.0259(3) Uani d 1 . . N N1 0.03826(12) 0.49974(17) 0.14562(12) 0.0212(3) Uani d 1 . . N N3 0.08327(11) 0.62287(15) 0.31617(12) 0.0180(3) Uani d 1 . . C C2 0.04683(12) 0.49344(18) 0.26185(13) 0.0181(3) Uani d 1 . . C C4 0.10682(12) 0.63031(17) 0.43899(13) 0.0176(3) Uani d 1 . . H H4A 0.103457 0.525355 0.472057 0.021 Uiso calc 1 . . C C5 0.22071(13) 0.69474(17) 0.46569(13) 0.0185(3) Uani d 1 . . C C6 0.30485(13) 0.58690(19) 0.41747(13) 0.0204(3) Uani d 1 . . C C7 0.41441(13) 0.6404(2) 0.40165(14) 0.0225(3) Uani d 1 . . C C8 0.46819(15) 0.5634(2) 0.31877(16) 0.0279(4) Uani d 1 . . H H8 0.433483 0.484415 0.274165 0.033 Uiso calc 1 . . C C9 0.57245(15) 0.6024(2) 0.30150(17) 0.0321(4) Uani d 1 . . H H9 0.607516 0.551826 0.243057 0.039 Uiso calc 1 . . C C10 0.62617(15) 0.7138(2) 0.36820(18) 0.0325(4) Uani d 1 . . C C11 0.57243(15) 0.7900(2) 0.45141(18) 0.0326(4) Uani d 1 . . H H11 0.608274 0.866470 0.497716 0.039 Uiso calc 1 . . C C12 0.46717(15) 0.7555(2) 0.46742(16) 0.0275(4) Uani d 1 . . H H12 0.431028 0.810101 0.523000 0.033 Uiso calc 1 . . C C13 0.74130(16) 0.7514(3) 0.3535(2) 0.0440(5) Uani d 1 . . H H13A 0.762750 0.702446 0.283178 0.066 Uiso calc 1 . . H H13B 0.786149 0.713990 0.420656 0.066 Uiso calc 1 . . H H13C 0.749543 0.862022 0.347188 0.066 Uiso calc 1 . . H H1A 0.059(2) 0.574(3) 0.110(2) 0.030(6) Uiso d 1 . . H H1B 0.0183(19) 0.420(3) 0.110(2) 0.028(6) Uiso d 1 . . H H3 0.0725(18) 0.701(3) 0.280(2) 0.023(5) Uiso d 1 . . H H4 0.014(2) 0.683(3) 0.543(3) 0.034(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.0239(2) 0.0173(2) 0.0211(2) -0.00221(12) 0.00407(14) 0.00018(12) Cl2 0.0263(2) 0.0291(2) 0.01385(19) 0.00153(14) 0.00155(14) -0.00215(13) O2 0.0313(6) 0.0194(6) 0.0164(5) -0.0060(4) 0.0065(4) -0.0001(4) O4 0.0229(5) 0.0207(5) 0.0150(5) 0.0016(4) 0.0073(4) 0.0021(4) O6 0.0270(6) 0.0222(6) 0.0290(6) 0.0015(5) 0.0057(5) -0.0049(5) N1 0.0304(7) 0.0189(6) 0.0144(6) -0.0061(5) 0.0037(5) -0.0009(5) N3 0.0253(6) 0.0152(6) 0.0139(6) -0.0010(5) 0.0032(5) 0.0016(5) C2 0.0199(7) 0.0179(7) 0.0168(7) 0.0003(5) 0.0043(5) 0.0001(5) C4 0.0217(7) 0.0176(7) 0.0139(7) -0.0012(5) 0.0042(5) 0.0008(5) C5 0.0225(7) 0.0182(7) 0.0150(7) -0.0007(6) 0.0035(5) -0.0005(5) C6 0.0235(7) 0.0226(7) 0.0156(7) 0.0027(6) 0.0039(5) -0.0006(6) C7 0.0215(7) 0.0258(8) 0.0203(7) 0.0026(6) 0.0030(6) 0.0021(6) C8 0.0277(8) 0.0307(9) 0.0258(8) 0.0044(7) 0.0061(6) -0.0006(7) C9 0.0279(9) 0.0390(10) 0.0308(9) 0.0081(8) 0.0105(7) 0.0065(7) C10 0.0231(8) 0.0377(10) 0.0372(10) 0.0018(7) 0.0063(7) 0.0162(8) C11 0.0269(9) 0.0346(10) 0.0358(10) -0.0041(7) 0.0000(7) 0.0040(8) C12 0.0263(8) 0.0305(9) 0.0260(8) -0.0010(7) 0.0039(6) -0.0010(7) C13 0.0258(10) 0.0529(14) 0.0546(13) -0.0018(9) 0.0104(9) 0.0210(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 0 -1 0.1564 0 0 1 0.1462 1 0 0 0.2293 -1 0 0 0.1924 0 1 0 0.0987 0 -1 0 0.1323 0 -1 -1 0.0914 1 0 1 0.1507 0 1 -1 0.1334 1 -1 0 0.1161 0 1 1 0.0705 1 -4 -6 0.1010 -4 -4 -4 0.1359 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C4 O4 H4 . . 109(2) ? C2 N1 H1A . . 121.9(18) ? C2 N1 H1B . . 117.0(16) ? H1A N1 H1B . . 121(2) ? C2 N3 C4 . . 122.18(13) ? C2 N3 H3 . . 115.9(17) ? C4 N3 H3 . . 118.9(17) ? O2 C2 N1 . . 121.23(15) n O2 C2 N3 . . 123.58(14) n N1 C2 N3 . . 115.19(14) ? O4 C4 N3 . . 110.47(13) n O4 C4 H4A . . 109.1 ? O4 C4 C5 . . 109.93(12) ? N3 C4 H4A . . 109.1 ? N3 C4 C5 . . 109.05(12) n C5 C4 H4A . . 109.1 ? Cl2 C5 Cl1 . . 109.48(8) n C4 C5 Cl1 . . 108.99(11) ? C4 C5 Cl2 . . 108.20(10) ? C4 C5 C6 . . 110.76(13) n C6 C5 Cl1 . . 111.85(11) ? C6 C5 Cl2 . . 107.47(11) ? O6 C6 C5 . . 116.31(14) ? O6 C6 C7 . . 122.32(15) ? C7 C6 C5 . . 121.38(14) ? C8 C7 C6 . . 116.30(16) ? C8 C7 C12 . . 119.18(16) ? C12 C7 C6 . . 124.44(15) ? C7 C8 H8 . . 120.0 ? C9 C8 C7 . . 120.07(18) ? C9 C8 H8 . . 120.0 ? C8 C9 H9 . . 119.4 ? C10 C9 C8 . . 121.10(18) ? C10 C9 H9 . . 119.4 ? C9 C10 C11 . . 118.69(17) ? C9 C10 C13 . . 121.3(2) ? C11 C10 C13 . . 120.0(2) ? C10 C11 H11 . . 119.6 ? C12 C11 C10 . . 120.89(19) ? C12 C11 H11 . . 119.6 ? C7 C12 H12 . . 120.0 ? C11 C12 C7 . . 120.02(17) ? C11 C12 H12 . . 120.0 ? C10 C13 H13A . . 109.5 ? C10 C13 H13B . . 109.5 ? C10 C13 H13C . . 109.5 ? H13A C13 H13B . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cl1 C5 . 1.7864(16) ? Cl2 C5 . 1.7861(16) ? O2 C2 . 1.248(2) ? O4 C4 . 1.4060(18) ? O4 H4 . 0.78(3) ? O6 C6 . 1.205(2) ? N1 C2 . 1.345(2) ? N1 H1A . 0.82(3) ? N1 H1B . 0.84(3) ? N3 C2 . 1.360(2) ? N3 C4 . 1.432(2) ? N3 H3 . 0.81(3) ? C4 H4A . 1.0000 ? C4 C5 . 1.551(2) ? C5 C6 . 1.561(2) ? C6 C7 . 1.486(2) ? C7 C8 . 1.397(2) ? C7 C12 . 1.400(3) ? C8 H8 . 0.9500 ? C8 C9 . 1.390(3) ? C9 H9 . 0.9500 ? C9 C10 . 1.388(3) ? C10 C11 . 1.396(3) ? C10 C13 . 1.514(2) ? C11 H11 . 0.9500 ? C11 C12 . 1.390(3) ? C12 H12 . 0.9500 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1A O4 4_575 0.82(3) 2.27(3) 3.0261(19) 153(2) yes N1 H1B O4 2_545 0.84(3) 2.14(3) 2.9798(18) 177(2) yes N3 H3 O2 2 0.81(3) 2.19(3) 2.9445(18) 156(2) yes O4 H4 O2 3_566 0.78(3) 1.83(3) 2.5979(16) 168(3) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cl1 C5 C6 O6 . . . . -139.23(13) ? Cl1 C5 C6 C7 . . . . 40.85(18) ? Cl2 C5 C6 O6 . . . . 100.57(15) ? Cl2 C5 C6 C7 . . . . -79.35(16) ? O4 C4 C5 Cl1 . . . . -60.19(14) ? O4 C4 C5 Cl2 . . . . 58.79(14) ? O4 C4 C5 C6 . . . . 176.34(12) ? O6 C6 C7 C8 . . . . 25.0(2) ? O6 C6 C7 C12 . . . . -151.71(18) ? N3 C4 C5 Cl1 . . . . 61.06(14) ? N3 C4 C5 Cl2 . . . . -179.97(10) ? N3 C4 C5 C6 . . . . -62.41(16) ? C2 N3 C4 O4 . . . . -110.90(16) ? C2 N3 C4 C5 . . . . 128.18(15) ? C4 N3 C2 O2 . . . . 5.2(2) ? C4 N3 C2 N1 . . . . -173.78(14) ? C4 C5 C6 O6 . . . . -17.42(19) ? C4 C5 C6 C7 . . . . 162.65(14) ? C5 C6 C7 C8 . . . . -155.04(15) ? C5 C6 C7 C12 . . . . 28.2(2) ? C6 C7 C8 C9 . . . . -177.58(17) ? C6 C7 C12 C11 . . . . 175.43(17) ? C7 C8 C9 C10 . . . . 2.2(3) ? C8 C7 C12 C11 . . . . -1.2(3) ? C8 C9 C10 C11 . . . . -1.9(3) ? C8 C9 C10 C13 . . . . 177.11(18) ? C9 C10 C11 C12 . . . . -0.1(3) ? C10 C11 C12 C7 . . . . 1.6(3) ? C12 C7 C8 C9 . . . . -0.6(3) ? C13 C10 C11 C12 . . . . -179.03(19) ?