#------------------------------------------------------------------------------
#$Date: 2025-06-26 03:34:54 +0100 (Thu, 26 Jun 2025) $
#$Revision: 300218 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/35/2023531.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023531
loop_
_publ_author_name
'Repina, Olga V.'
'Nevskaya, Elena Yu.'
'Kritchenkov, Ilya S.'
'Khrustalev, Victor N.'
'Novikov, Alexander S.'
'Tskhovrebov, Alexander G.'
'Shikhaliyev, Namiq Q.'
'Niyazova, Aytan A.'
'Akkurt, Mehmet'
'Bhattarai, Ajaya'
_publ_section_title
;
Crystal structure and Hirshfeld surface analysis of
chlorido(2,6-dimethylphenyl
isocyanide)[N′-(2,6-dimethylphenyl)-N-(pyridin-2-yl)carbamimidoyl]platinum(II)
;
_journal_coeditor_code TX2098
_journal_issue 7
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989025005079
_journal_volume 81
_journal_year 2025
_chemical_formula_iupac '[Pt (C14 H14 N3) Cl (C9 H9 N1)]'
_chemical_formula_moiety 'C23 H23 Cl N4 Pt'
_chemical_formula_sum 'C23 H23 Cl N4 Pt'
_chemical_formula_weight 585.99
_chemical_name_systematic
'Chlorido(2,6-dimethylphenyl isocyanide)[N'-(2,6-dimethylphenyl)-N-(pyridin-2-yl)carbamimidoyl]platinum(II)'
_space_group_crystal_system triclinic
_space_group_IT_number 2
_space_group_name_Hall '-P 1'
_space_group_name_H-M_alt 'P -1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary difmap
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2019/3
_cell_angle_alpha 104.5350(10)
_cell_angle_beta 95.9220(10)
_cell_angle_gamma 90.2270(10)
_cell_formula_units_Z 2
_cell_length_a 7.7053(3)
_cell_length_b 9.7010(3)
_cell_length_c 15.0316(5)
_cell_measurement_reflns_used 9990
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 32.57
_cell_measurement_theta_min 2.66
_cell_volume 1081.31(6)
_computing_cell_refinement
;
SAINT (Bruker, 2013)
;
_computing_data_collection
;
APEX3 (Bruker, 2018)
;
_computing_data_reduction
;
SAINT (Bruker, 2013)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012)
;
_computing_publication_material
;
PLATON (Spek, 2020)
;
_computing_structure_refinement
;
SHELXL2016/6 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2016/6 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 100(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON-III CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0363
_diffrn_reflns_av_unetI/netI 0.0370
_diffrn_reflns_limit_h_max 11
_diffrn_reflns_limit_h_min -11
_diffrn_reflns_limit_k_max 14
_diffrn_reflns_limit_k_min -14
_diffrn_reflns_limit_l_max 22
_diffrn_reflns_limit_l_min -22
_diffrn_reflns_number 26083
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 32.599
_diffrn_reflns_theta_min 2.269
_exptl_absorpt_coefficient_mu 6.628
_exptl_absorpt_correction_T_max 0.495
_exptl_absorpt_correction_T_min 0.297
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015).
;
_exptl_crystal_colour red
_exptl_crystal_density_diffrn 1.800
_exptl_crystal_description prism
_exptl_crystal_F_000 568
_exptl_crystal_size_max 0.200
_exptl_crystal_size_mid 0.150
_exptl_crystal_size_min 0.100
_refine_diff_density_max 2.311
_refine_diff_density_min -1.840
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.093
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 268
_refine_ls_number_reflns 7860
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.093
_refine_ls_R_factor_all 0.0376
_refine_ls_R_factor_gt 0.0296
_refine_ls_shift/su_max 0.002
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0282P)^2^+2.7164P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0685
_refine_ls_wR_factor_ref 0.0712
_reflns_number_gt 6973
_reflns_number_total 7860
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file tx2098.cif
_cod_data_source_block I
_cod_database_code 2023531
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.351
_shelx_estimated_absorpt_t_max 0.557
_shelx_hkl_file
;
-1 0 0 3021.20 54.09
-1 0 0 3091.09 54.49
1 0 0 3583.74 55.09
1 0 0 3238.58 54.29
-2 0 0 3097.49 54.99
-2 0 0 3014.70 54.09
-2 0 0 3149.28 54.49
-2 0 0 3264.57 55.89
2 0 0 3104.79 54.29
-3 0 0 1306.17 27.70
-3 0 0 1355.16 27.10
-3 0 0 1347.57 28.80
3 0 0 1311.97 26.70
-4 0 0 1509.55 33.60
-4 0 0 1485.05 31.10
-4 0 0 1456.25 32.20
4 0 0 1476.85 31.10
-5 0 0 422.56 17.60
5 0 0 429.06 15.50
5 0 0 424.76 17.80
-6 0 0 190.88 15.70
6 0 0 169.58 15.30
6 0 0 212.78 14.30
6 0 0 220.58 16.00
-7 0 0 50.49 10.60
7 0 0 62.89 10.00
-8 0 0 81.09 12.80
-9 0 0 154.18 16.90
9 0 0 171.68 17.60
9 0 0 97.39 15.60
9 0 0 113.39 14.30
-10 0 0 142.19 18.50
10 0 0 102.69 15.50
10 0 0 97.29 18.00
10 0 0 132.09 17.40
-11 0 0 127.99 19.30
11 0 0 111.19 15.20
11 0 0 137.19 17.10
11 0 0 130.79 18.10
11 -1 0 43.00 14.00
11 -1 0 -2.60 12.60
11 -1 0 2.10 11.90
-11 1 0 -3.20 19.10
10 -1 0 25.00 12.60
10 -1 0 18.80 12.40
10 -1 0 45.20 13.20
-10 1 0 26.70 14.00
9 -1 0 226.88 19.20
9 -1 0 218.58 20.60
9 -1 0 204.48 19.20
9 -1 0 186.68 18.60
-9 1 0 226.38 21.60
8 -1 0 468.95 22.60
8 -1 0 446.96 23.90
8 -1 0 477.15 21.20
8 -1 0 458.55 22.00
-8 1 0 495.45 23.80
7 -1 0 623.64 22.20
7 -1 0 572.64 23.10
-7 1 0 647.84 25.80
-7 1 0 615.24 23.60
6 -1 0 1150.98 30.90
-6 1 0 1127.29 31.10
-6 1 0 1164.88 29.50
5 -1 0 1432.96 33.00
-5 1 0 1377.76 32.40
-5 1 0 1372.86 34.40
-5 1 0 1396.96 30.80
4 -1 0 1336.37 29.70
-4 1 0 1336.37 28.00
-4 1 0 1310.47 31.00
-4 1 0 1308.47 29.30
3 -1 0 2626.14 48.80
-3 1 0 2538.75 45.70
-3 1 0 2582.94 47.00
-3 1 0 2633.54 49.70
-3 1 0 2631.94 48.20
2 -1 0 1437.46 28.70
2 -1 0 1441.46 28.30
2 -1 0 1439.46 26.50
-2 1 0 1424.66 26.20
-2 1 0 1458.55 26.60
1 -1 0 3210.28 56.09
1 -1 0 3252.27 55.29
1 -1 0 3359.16 55.09
1 -1 0 3162.28 54.69
1 -1 0 3453.55 56.59
-1 1 0 3239.98 55.29
-1 1 0 3141.89 55.99
-1 1 0 3155.88 54.69
-1 1 0 3356.16 55.09
-1 1 0 3430.56 56.49
-1 -1 0 1328.67 24.60
-1 -1 0 1382.96 24.00
-1 -1 0 1247.08 24.00
1 1 0 1411.76 24.30
1 1 0 1283.87 24.50
1 1 0 1163.68 23.70
-2 -1 0 104.39 7.70
-2 -1 0 92.29 4.50
-2 -1 0 101.09 7.80
2 1 0 104.39 7.40
2 1 0 99.09 5.00
2 1 0 93.09 7.10
-3 -1 0 223.68 10.10
3 1 0 217.48 7.90
3 1 0 222.78 9.60
3 1 0 221.68 10.20
-4 -1 0 5.40 5.50
4 1 0 1.00 5.20
4 1 0 6.30 4.40
4 1 0 11.20 5.80
-5 -1 0 140.39 12.50
5 1 0 132.89 11.40
5 1 0 139.39 9.90
-6 -1 0 443.26 19.90
6 1 0 431.36 19.00
6 1 0 395.36 19.90
6 1 0 432.46 16.60
-7 -1 0 125.39 13.80
7 1 0 133.49 13.60
7 1 0 166.48 14.40
7 1 0 185.78 17.10
8 1 0 592.04 22.00
8 1 0 636.84 26.10
8 1 0 609.74 28.00
8 1 0 647.94 23.30
-9 -1 0 422.16 24.80
9 1 0 456.75 26.00
9 1 0 435.46 22.00
9 1 0 427.66 20.00
9 1 0 446.06 26.30
-10 -1 0 277.27 24.90
10 1 0 275.97 22.40
10 1 0 272.37 24.20
10 1 0 250.37 18.20
-11 -1 0 275.17 25.90
11 1 0 174.98 18.00
11 1 0 279.97 26.40
11 -2 0 139.19 16.70
11 -2 0 116.79 17.90
10 -2 0 200.48 20.40
10 -2 0 217.48 21.00
-10 2 0 227.38 22.90
9 -2 0 505.35 23.40
9 -2 0 440.46 22.70
9 -2 0 408.16 26.20
9 -2 0 451.65 24.80
-9 2 0 474.25 26.00
8 -2 0 750.22 29.00
-8 2 0 737.63 30.40
-8 2 0 752.72 28.30
7 -2 0 998.40 30.80
-7 2 0 973.80 29.90
-7 2 0 930.91 31.70
-7 2 0 976.10 27.60
6 -2 0 958.50 28.60
-6 2 0 871.51 26.60
-6 2 0 914.51 24.90
-6 2 0 875.11 29.20
5 -2 0 657.73 23.20
-5 2 0 716.83 22.80
-5 2 0 695.33 19.30
-5 2 0 693.53 21.20
4 -2 0 1180.08 28.10
-4 2 0 1162.08 25.20
-4 2 0 1159.08 28.60
-4 2 0 1168.38 24.10
-4 2 0 1148.29 26.60
3 -2 0 27.80 6.00
-3 2 0 21.10 4.20
-3 2 0 35.80 6.40
-3 2 0 37.90 4.70
-3 2 0 30.20 5.30
2 -2 0 271.17 10.10
2 -2 0 256.07 10.40
-2 2 0 255.67 8.10
-2 2 0 269.37 10.30
-2 2 0 266.07 8.90
-2 2 0 256.87 8.50
1 -2 0 9.50 3.60
1 -2 0 9.10 3.20
1 -2 0 6.70 4.10
1 -2 0 5.60 2.90
-1 2 0 9.30 3.10
-1 2 0 6.40 2.80
-1 2 0 11.00 3.20
-1 2 0 8.10 3.60
0 -2 0 5.60 2.80
0 -2 0 3.50 3.00
0 -2 0 3.90 2.10
0 -2 0 7.20 2.80
0 2 0 0.60 2.40
0 2 0 7.50 2.90
0 2 0 3.80 2.50
0 2 0 -1.40 2.80
0 2 0 3.80 3.00
-1 -2 0 13.10 3.90
-1 -2 0 23.00 4.60
1 2 0 26.30 5.00
1 2 0 25.40 4.80
1 2 0 24.20 3.50
-2 -2 0 424.16 14.30
-2 -2 0 444.46 13.10
2 2 0 482.05 13.70
2 2 0 464.35 14.10
2 2 0 480.95 11.20
-3 -2 0 538.55 15.70
-3 -2 0 526.35 16.00
3 2 0 526.95 15.90
3 2 0 520.55 13.40
3 2 0 551.04 16.60
-4 -2 0 952.80 24.70
4 2 0 972.50 21.80
4 2 0 932.41 24.30
4 2 0 987.40 26.00
-5 -2 0 910.81 26.00
5 2 0 945.91 27.50
5 2 0 882.71 28.00
5 2 0 875.11 22.30
5 2 0 861.91 20.70
-6 -2 0 978.00 29.10
6 2 0 915.91 23.20
6 2 0 935.31 25.20
6 2 0 920.01 28.70
6 2 0 963.80 30.50
-7 -2 0 558.44 23.30
7 2 0 536.55 20.10
7 2 0 499.75 17.70
7 2 0 570.94 23.30
7 2 0 559.44 24.80
-8 -2 0 622.14 26.60
8 2 0 647.04 27.20
8 2 0 612.54 23.00
8 2 0 579.14 20.60
8 2 0 617.54 27.60
-9 -2 0 205.98 21.00
9 2 0 193.98 18.80
9 2 0 183.58 19.50
9 2 0 207.78 14.30
9 2 0 207.88 20.00
-10 -2 0 73.09 15.70
10 2 0 49.99 13.50
10 2 0 45.90 16.10
10 2 0 49.10 10.30
-11 -2 0 43.60 15.20
11 2 0 32.10 15.30
11 2 0 54.59 14.50
11 -3 0 196.78 21.90
11 -3 0 196.58 19.40
10 -3 0 290.67 24.60
10 -3 0 253.17 41.20
10 -3 0 334.77 22.70
10 -3 0 317.97 22.00
-10 3 0 332.67 24.80
9 -3 0 224.18 22.50
9 -3 0 254.47 20.20
9 -3 0 259.77 18.60
-9 3 0 262.87 24.30
-9 3 0 213.18 21.60
8 -3 0 283.07 21.60
-8 3 0 309.17 17.80
-8 3 0 280.07 21.70
-8 3 0 290.17 20.40
7 -3 0 266.27 19.30
-7 3 0 263.37 17.40
-7 3 0 259.77 18.70
-7 3 0 221.08 14.80
6 -3 0 156.98 16.30
-6 3 0 191.28 15.70
5 -3 0 12.20 8.10
-5 3 0 18.80 8.20
-5 3 0 10.60 5.80
-5 3 0 2.20 6.90
-5 3 0 2.80 6.10
4 -3 0 23.70 7.40
-4 3 0 17.90 7.10
-4 3 0 19.50 5.50
-4 3 0 14.70 6.10
-4 3 0 24.00 5.00
3 -3 0 139.69 10.50
-3 3 0 139.99 10.20
-3 3 0 134.99 8.70
-3 3 0 144.09 8.20
-3 3 0 141.59 7.30
2 -3 0 104.49 8.40
-2 3 0 104.09 8.40
-2 3 0 93.59 6.90
-2 3 0 107.29 6.70
-2 3 0 106.39 6.30
1 -3 0 1308.37 27.00
1 -3 0 1311.77 25.90
1 -3 0 1365.56 28.00
-1 3 0 1316.97 26.00
-1 3 0 1316.47 27.90
-1 3 0 1269.07 24.70
0 -3 0 2596.24 45.60
0 -3 0 2424.86 46.90
0 -3 0 2460.55 46.30
0 3 0 2420.56 43.70
0 3 0 2636.44 47.40
0 3 0 2475.85 45.90
-1 -3 0 2145.79 38.60
-1 -3 0 2058.39 41.60
1 3 0 1922.01 36.00
1 3 0 1920.31 38.90
1 3 0 2066.69 40.00
-2 -3 0 1873.81 41.00
2 3 0 2028.40 38.90
2 3 0 1810.22 39.00
2 3 0 1977.00 35.20
-3 -3 0 1118.79 26.40
-3 -3 0 1049.79 26.70
3 3 0 1147.09 23.30
3 3 0 1135.99 27.70
-4 -3 0 1397.86 35.10
-4 -3 0 1326.97 33.00
4 3 0 1387.46 32.90
4 3 0 1348.67 28.80
4 3 0 1447.76 34.50
-5 -3 0 959.80 27.40
5 3 0 935.71 27.60
5 3 0 955.90 23.80
5 3 0 963.40 29.00
-6 -3 0 631.44 23.90
6 3 0 591.94 20.30
6 3 0 582.64 23.60
6 3 0 605.44 24.70
-7 -3 0 266.87 18.20
7 3 0 236.28 18.30
7 3 0 240.78 19.30
7 3 0 230.98 15.80
-8 -3 0 133.79 15.70
8 3 0 164.98 18.00
8 3 0 158.08 17.10
8 3 0 184.78 16.60
-9 -3 0 51.19 13.40
9 3 0 31.30 14.30
9 3 0 35.00 11.80
-10 -3 0 8.10 12.60
10 3 0 21.40 12.90
10 3 0 16.30 14.10
-11 -3 0 62.99 16.20
11 3 0 47.30 17.20
11 3 0 35.50 13.90
11 -4 0 41.80 16.40
10 -4 0 36.80 16.60
10 -4 0 25.20 12.80
10 -4 0 19.60 12.00
-10 4 0 4.20 14.20
-10 4 0 37.70 14.60
9 -4 0 36.60 12.30
-9 4 0 36.10 14.00
-9 4 0 78.79 14.60
8 -4 0 90.49 15.00
-8 4 0 98.19 14.40
-8 4 0 112.29 11.90
-8 4 0 85.49 15.20
7 -4 0 187.78 18.50
-7 4 0 193.48 14.20
-7 4 0 181.98 16.90
6 -4 0 407.16 21.70
-6 4 0 448.46 17.00
-6 4 0 427.36 19.50
-6 4 0 432.06 27.20
5 -4 0 883.21 28.00
-5 4 0 881.41 22.20
-5 4 0 889.21 28.20
-5 4 0 894.21 22.90
4 -4 0 1334.47 33.70
-4 4 0 1343.57 33.80
-4 4 0 1339.77 28.30
-4 4 0 1334.97 28.80
-4 4 0 1342.77 30.40
3 -4 0 1964.20 42.40
-3 4 0 1981.60 38.60
-3 4 0 1960.20 37.80
-3 4 0 2016.00 42.90
-3 4 0 2024.40 39.40
2 -4 0 2880.41 54.79
-2 4 0 2810.52 51.99
-2 4 0 2850.41 52.09
-2 4 0 2786.72 50.79
1 -4 0 2901.41 56.39
1 -4 0 2963.60 55.09
1 -4 0 2956.80 54.09
-1 4 0 2875.81 52.29
-1 4 0 3111.19 56.99
-1 4 0 2955.20 54.19
0 -4 0 2880.41 53.39
0 -4 0 2868.11 52.39
0 -4 0 2955.10 55.39
0 4 0 2904.01 53.99
0 4 0 2816.12 51.09
0 4 0 2975.90 55.49
-1 -4 0 2581.64 49.50
-1 -4 0 2374.16 44.00
-1 -4 0 2642.64 47.50
1 4 0 2477.85 49.10
1 4 0 2362.86 47.90
1 4 0 2460.45 44.70
-2 -4 0 1404.76 32.70
-2 -4 0 1418.56 31.20
2 4 0 1466.25 32.40
2 4 0 1397.96 32.60
2 4 0 1459.85 28.20
-3 -4 0 422.66 15.70
-3 -4 0 459.35 16.90
3 4 0 472.85 13.70
3 4 0 433.96 16.80
3 4 0 459.25 17.30
-4 -4 0 380.06 16.30
-4 -4 0 332.47 15.60
4 4 0 351.76 17.00
4 4 0 352.76 13.70
4 4 0 357.16 17.10
-5 -4 0 73.79 10.90
5 4 0 74.39 11.30
5 4 0 50.99 11.10
5 4 0 74.09 9.20
-6 -4 0 20.20 9.10
6 4 0 9.30 8.00
6 4 0 11.40 9.80
6 4 0 18.10 8.80
-7 -4 0 24.10 17.10
7 4 0 2.80 10.90
7 4 0 5.30 8.80
-8 -4 0 150.68 16.60
8 4 0 190.08 16.90
8 4 0 160.38 18.20
8 4 0 148.19 17.10
-9 -4 0 48.60 13.80
9 4 0 87.19 13.50
9 4 0 101.79 17.40
-10 -4 0 232.98 24.60
10 4 0 180.78 21.10
10 4 0 197.78 20.40
-11 -4 0 159.68 20.10
11 4 0 163.08 20.40
11 4 0 158.38 17.90
10 -5 0 67.29 12.10
10 -5 0 25.80 16.20
-10 5 0 23.10 14.30
-10 5 0 24.00 16.70
9 -5 0 258.27 20.60
9 -5 0 262.97 25.20
-9 5 0 240.88 18.40
-9 5 0 253.57 37.20
-9 5 0 265.07 24.00
8 -5 0 391.16 25.70
-8 5 0 371.96 18.70
-8 5 0 393.76 25.60
-8 5 0 379.86 22.70
7 -5 0 631.14 30.70
-7 5 0 682.63 29.10
-7 5 0 654.13 25.30
-7 5 0 610.24 21.70
6 -5 0 787.12 29.10
-6 5 0 731.73 33.90
-6 5 0 788.82 21.60
-6 5 0 712.83 25.40
-6 5 0 775.82 25.20
5 -5 0 1205.98 35.00
-5 5 0 1213.08 28.40
-5 5 0 1233.38 29.20
-5 5 0 1262.37 31.50
-5 5 0 1241.98 35.40
4 -5 0 1655.63 40.40
-4 5 0 1622.74 34.80
-4 5 0 1683.63 40.20
-4 5 0 1644.94 34.40
-4 5 0 1635.04 36.10
3 -5 0 1530.45 36.50
-3 5 0 1505.15 32.30
-3 5 0 1570.04 33.10
-3 5 0 1508.25 31.60
-3 5 0 1544.95 37.00
2 -5 0 2092.09 44.40
-2 5 0 2170.88 42.30
-2 5 0 2157.58 40.80
-2 5 0 2126.19 45.80
1 -5 0 1007.00 24.20
1 -5 0 980.80 23.50
-1 5 0 991.20 21.80
-1 5 0 976.30 26.10
-1 5 0 1014.60 24.00
0 -5 0 610.84 17.60
0 -5 0 683.43 20.10
0 -5 0 654.23 17.10
0 5 0 643.84 18.90
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-4 4 -20 21.90 14.50
4 -4 20 2.60 16.30
6 3 -20 18.60 11.60
6 3 -20 20.30 15.10
-6 -3 20 46.90 15.00
5 3 -20 48.90 16.60
-5 -3 20 27.50 13.80
4 3 -20 20.20 15.50
-4 -3 20 -27.00 10.60
3 3 -20 3.80 7.80
3 3 -20 -19.20 11.90
-3 -3 20 -4.30 11.00
2 3 -20 22.50 9.90
2 3 -20 13.40 14.10
-2 -3 20 30.10 12.00
1 3 -20 58.99 16.60
1 3 -20 51.79 12.00
-1 -3 20 83.09 12.70
0 3 -20 86.09 14.20
0 -3 20 111.19 18.60
0 -3 20 84.29 12.20
-1 3 -20 68.49 14.20
1 -3 20 66.79 17.70
1 -3 20 49.99 10.20
-2 3 -20 134.99 17.50
2 -3 20 153.08 20.50
-3 3 -20 76.29 17.30
3 -3 20 69.79 17.90
-4 3 -20 68.29 16.90
4 -3 20 65.59 19.20
6 2 -20 18.20 15.00
-6 -2 20 15.50 14.20
5 2 -20 63.69 17.00
-5 -2 20 40.00 14.80
4 2 -20 49.00 16.40
-4 -2 20 43.00 14.60
3 2 -20 55.79 11.60
3 2 -20 75.19 18.20
-3 -2 20 98.29 15.80
2 2 -20 77.49 18.10
2 2 -20 74.09 11.60
-2 -2 20 73.09 14.20
1 2 -20 227.68 19.00
1 2 -20 215.08 22.80
-1 -2 20 270.37 20.50
0 2 -20 178.48 17.30
0 -2 20 187.28 17.30
-1 2 -20 160.38 17.40
1 -2 20 146.59 20.20
1 -2 20 151.08 16.50
-2 2 -20 104.99 16.60
2 -2 20 58.19 11.50
2 -2 20 51.39 17.00
-3 2 -20 110.09 20.00
3 -2 20 100.69 18.20
-4 2 -20 48.30 15.70
4 -2 20 22.40 15.10
6 1 -20 147.19 22.40
-6 -1 20 105.49 17.60
5 1 -20 217.28 24.10
4 1 -20 157.98 21.10
-4 -1 20 112.69 17.80
3 1 -20 137.99 25.20
-3 -1 20 180.08 19.30
2 1 -20 205.78 15.80
2 1 -20 195.98 22.60
-2 -1 20 214.28 22.10
1 1 -20 135.79 19.30
1 1 -20 151.58 17.80
-1 -1 20 129.09 15.70
0 1 -20 108.29 14.60
0 1 -20 59.39 16.90
0 -1 20 108.99 14.80
-1 1 -20 53.59 14.00
1 -1 20 43.20 15.00
1 -1 20 36.80 12.00
-2 1 -20 12.70 12.80
2 -1 20 53.89 12.80
2 -1 20 55.69 16.20
-3 1 -20 24.40 15.00
3 -1 20 20.00 14.00
3 -1 20 -3.30 9.40
-4 1 -20 9.60 14.10
4 -1 20 -12.10 12.00
6 0 -20 175.48 22.80
5 0 -20 162.78 22.60
-5 0 20 136.39 20.80
4 0 -20 107.89 19.30
-4 0 20 102.79 18.80
3 0 -20 40.00 20.30
-3 0 20 89.19 16.80
2 0 -20 21.90 15.20
-2 0 20 18.00 13.00
1 0 -20 18.10 14.60
-1 0 20 12.20 12.10
0 0 -20 7.70 12.70
0 0 20 -19.40 10.20
1 0 20 28.30 12.10
1 0 20 41.20 14.70
2 0 20 18.20 13.80
2 0 20 42.90 12.20
3 0 20 56.99 15.20
5 -1 -20 -5.50 13.20
-5 1 20 -0.20 15.00
4 -1 -20 -4.70 12.60
-4 1 20 -6.80 14.10
3 -1 -20 -6.10 12.70
-3 1 20 1.70 13.50
2 -1 -20 40.20 15.80
-2 1 20 44.70 15.00
1 -1 -20 25.60 14.20
-1 1 20 49.20 15.00
0 -1 -20 43.40 14.80
0 1 20 31.50 12.40
0 1 20 51.09 14.50
1 1 20 50.29 13.50
1 1 20 38.20 13.70
2 1 20 93.89 16.70
2 1 20 71.49 15.30
2 1 20 75.59 14.60
3 1 20 136.79 16.90
3 1 20 143.99 19.70
4 -2 -20 112.99 19.40
-4 2 20 99.69 19.20
3 -2 -20 97.29 18.10
-3 2 20 78.19 17.60
2 -2 -20 86.79 18.60
-2 2 20 94.99 18.10
1 -2 -20 62.99 16.50
0 -2 -20 93.99 16.20
0 2 20 73.49 14.00
0 2 20 94.89 19.00
1 2 20 56.09 13.80
2 2 20 52.89 13.90
3 -3 -20 84.59 17.80
-3 3 20 82.09 18.20
2 -3 -20 91.49 17.60
-2 3 20 105.89 19.50
1 -3 -20 101.59 27.80
-1 3 20 80.99 16.90
0 -3 -20 1.40 11.40
0 3 20 -6.90 11.30
0 3 20 -22.00 11.90
3 8 -21 31.40 11.20
3 8 -21 38.20 13.00
-3 -8 21 58.89 18.20
-2 -8 21 28.60 17.20
1 8 -21 108.89 16.20
-1 -8 21 94.29 21.20
0 8 -21 132.39 18.00
0 -8 21 129.39 22.50
-1 8 -21 76.99 16.40
1 -8 21 63.59 20.00
4 7 -21 221.28 20.70
4 7 -21 212.78 17.20
3 7 -21 149.49 15.70
-3 -7 21 111.99 20.30
2 7 -21 71.59 12.90
-2 -7 21 74.59 19.20
1 7 -21 87.09 15.20
-1 -7 21 99.49 20.20
0 -7 21 56.59 18.70
-1 7 -21 120.29 17.90
1 -7 21 85.99 20.40
-2 7 -21 -10.00 11.90
2 -7 21 15.50 17.80
5 6 -21 267.07 22.60
4 6 -21 142.49 21.60
4 6 -21 186.28 16.60
-4 -6 21 191.08 19.30
3 6 -21 43.80 11.30
2 6 -21 25.80 11.00
-2 -6 21 48.30 17.40
1 6 -21 3.90 10.50
-1 -6 21 6.60 15.40
0 6 -21 9.00 12.00
0 -6 21 -5.30 14.70
-1 6 -21 19.40 15.00
1 -6 21 -2.50 15.90
-2 6 -21 38.60 14.80
2 -6 21 32.00 17.90
5 5 -21 -14.00 13.50
-5 -5 21 25.80 12.60
4 5 -21 -1.80 13.90
-4 -5 21 6.80 10.70
3 5 -21 3.00 14.20
3 5 -21 -10.30 8.60
-3 -5 21 -2.60 10.20
2 5 -21 21.70 10.80
1 5 -21 58.59 13.00
-1 -5 21 35.10 16.90
0 5 -21 72.99 14.00
0 -5 21 102.29 20.20
-1 5 -21 153.78 18.10
1 -5 21 177.18 23.60
-2 5 -21 110.09 16.70
2 -5 21 118.99 21.30
-3 5 -21 143.09 19.60
3 -5 21 138.19 23.20
5 4 -21 38.70 15.90
-5 -4 21 20.70 12.90
4 4 -21 59.49 17.10
-4 -4 21 62.59 12.80
3 4 -21 111.29 12.40
3 4 -21 112.29 19.90
-3 -4 21 88.59 13.60
2 4 -21 122.69 14.60
2 4 -21 140.19 21.20
-2 -4 21 139.49 14.60
1 4 -21 165.68 16.50
0 4 -21 256.37 21.00
0 -4 21 231.78 24.50
-1 4 -21 143.09 18.10
1 -4 21 111.19 20.60
-2 4 -21 30.90 14.20
2 -4 21 28.50 16.70
-3 4 -21 33.10 15.10
3 -4 21 29.10 16.30
5 3 -21 125.69 20.50
-5 -3 21 128.19 19.10
4 3 -21 188.78 23.30
-4 -3 21 177.68 18.30
3 3 -21 109.69 19.50
-3 -3 21 93.59 14.90
2 3 -21 112.29 19.40
2 3 -21 90.39 12.30
-2 -3 21 100.59 14.50
1 3 -21 66.79 13.10
-1 -3 21 36.50 11.90
0 3 -21 16.40 11.30
0 -3 21 11.70 16.30
0 -3 21 11.50 11.00
-1 3 -21 43.20 13.40
1 -3 21 14.40 16.00
2 -3 21 17.30 15.60
-3 3 -21 5.10 13.30
3 -3 21 8.20 14.80
5 2 -21 66.49 18.70
-5 -2 21 47.70 14.40
4 2 -21 30.90 15.80
-4 -2 21 23.10 13.60
3 2 -21 13.20 14.90
-3 -2 21 28.70 13.80
2 2 -21 -5.40 13.60
-2 -2 21 10.20 12.30
1 2 -21 15.50 18.40
1 2 -21 14.70 10.90
-1 -2 21 -13.00 10.50
0 2 -21 -1.60 10.80
0 -2 21 13.00 10.70
-1 2 -21 9.70 12.60
1 -2 21 2.40 9.70
2 -2 21 33.80 16.50
-3 2 -21 40.40 15.00
3 -2 21 52.09 16.90
5 1 -21 -11.20 14.10
-5 -1 21 18.20 14.20
4 1 -21 -18.90 12.70
3 1 -21 2.20 14.40
-3 -1 21 -5.10 12.90
2 1 -21 26.30 15.90
-2 -1 21 48.20 13.70
1 1 -21 97.49 13.60
1 1 -21 108.19 21.80
-1 -1 21 99.39 14.90
0 1 -21 168.08 17.10
0 -1 21 144.19 16.40
-1 1 -21 124.39 16.60
1 -1 21 132.29 15.50
1 -1 21 166.88 30.40
2 -1 21 115.39 14.40
4 0 -21 63.59 17.80
-4 0 21 93.99 18.60
3 0 -21 104.59 20.70
2 0 -21 79.79 18.00
-2 0 21 102.39 17.30
1 0 -21 177.78 21.30
-1 0 21 170.98 16.60
-1 0 21 143.49 18.10
0 0 21 123.29 16.60
1 0 21 56.59 14.00
2 0 21 23.20 12.00
3 -1 -21 114.49 19.70
-3 1 21 108.49 18.70
2 -1 -21 106.29 19.40
-2 1 21 70.59 16.00
1 -1 -21 -1.70 13.20
0 -1 -21 -9.20 13.00
0 1 21 15.60 13.00
0 1 21 1.40 11.00
1 1 21 15.10 14.80
1 1 21 0.00 11.20
2 -2 -21 31.50 15.60
1 -2 -21 -9.80 12.10
-1 2 21 -1.60 12.30
2 7 -22 33.70 13.00
1 7 -22 51.39 13.20
-1 -7 22 49.20 19.20
3 6 -22 116.29 13.80
2 6 -22 133.99 15.60
-2 -6 22 85.99 19.40
1 6 -22 160.38 17.30
-1 -6 22 169.98 23.90
0 6 -22 135.89 16.40
0 -6 22 153.28 22.40
-1 6 -22 80.29 15.60
1 -6 22 50.39 19.60
3 5 -22 184.68 17.20
2 5 -22 105.29 13.80
-2 -5 22 96.69 20.90
1 5 -22 44.30 12.40
-1 -5 22 46.80 17.50
0 5 -22 80.09 15.00
0 -5 22 46.80 17.90
-1 5 -22 -4.10 11.00
1 -5 22 34.90 18.10
4 4 -22 65.89 18.60
-4 -4 22 30.10 12.80
3 4 -22 39.30 16.40
-3 -4 22 -13.10 10.30
2 4 -22 -8.90 9.30
1 4 -22 20.50 10.90
-1 -4 22 -7.50 13.50
0 4 -22 43.00 13.30
0 -4 22 31.00 17.30
-1 4 -22 66.49 15.70
1 -4 22 30.50 17.50
4 3 -22 -15.50 13.60
-4 -3 22 4.50 11.60
3 3 -22 40.00 17.00
-3 -3 22 20.50 12.00
2 3 -22 26.40 10.90
2 3 -22 33.40 15.60
-2 -3 22 27.60 12.20
1 3 -22 96.09 13.90
-1 -3 22 65.09 13.60
0 3 -22 64.39 14.30
0 -3 22 60.09 17.60
1 -3 22 125.29 20.80
3 2 -22 104.29 20.10
-3 -2 22 138.89 17.70
2 2 -22 104.89 19.70
-2 -2 22 122.69 15.80
1 2 -22 75.79 12.90
-1 -2 22 39.40 12.70
0 2 -22 130.59 15.90
0 -2 22 81.39 18.20
0 -2 22 131.89 15.40
-1 2 -22 97.29 16.90
1 -2 22 82.69 18.40
3 1 -22 83.89 19.60
-3 -1 22 62.19 20.90
2 1 -22 73.79 18.10
-2 -1 22 75.79 15.50
1 1 -22 40.40 16.20
-1 -1 22 33.90 12.60
0 1 -22 13.80 12.20
0 -1 22 4.30 11.40
1 0 -22 -4.20 13.00
0 0 0 0.00 0.00
;
_shelx_hkl_checksum 37671
_shelx_res_file
;
TITL AT-178 in P-1
shelx.res
created by SHELXL-2019/3 at 17:18:22 on 10-Apr-2025
CELL 0.71073 7.7053 9.7010 15.0316 104.535 95.922 90.227
ZERR 2.00 0.0003 0.0003 0.0005 0.001 0.001 0.001
LATT 1
SFAC C H N CL PT
UNIT 46 46 8 2 2
MERG 2
OMIT -7 3 0
OMIT -8 4 0
OMIT -7 4 0
OMIT 7 -6 1
OMIT -9 2 1
OMIT 5 -7 2
OMIT 4 -9 3
OMIT 5 -9 3
OMIT -10 0 2
OMIT -11 -2 3
OMIT 6 -9 1
OMIT -9 0 2
EQIV $1 -x+1, -y+1, -z+1
HTAB N2 N3_$1
FMAP 2
PLAN 15
SIZE 0.100 0.150 0.200
ACTA
BOND $H
CONF
L.S. 13
TEMP -173.00
WGHT 0.028200 2.716400
FVAR 0.38192
PT1 5 0.534406 0.134013 0.288124 11.00000 0.01269 0.01191 =
0.02260 0.00688 0.00389 -0.00027
CL1 4 0.516849 -0.090970 0.179190 11.00000 0.03353 0.01389 =
0.04123 0.00193 0.01970 -0.00046
N1 3 0.388116 0.069860 0.377566 11.00000 0.01234 0.01437 =
0.02631 0.00970 0.00358 0.00015
N2 3 0.438047 0.301519 0.455974 11.00000 0.02708 0.01768 =
0.01740 0.00461 0.00163 -0.00969
N3 3 0.610469 0.439474 0.398332 11.00000 0.02848 0.01709 =
0.01789 0.00766 0.00338 -0.00741
N4 3 0.759838 0.211725 0.150762 11.00000 0.01746 0.01547 =
0.02465 0.00296 0.00428 -0.00168
C1 1 0.538290 0.314658 0.385473 11.00000 0.01812 0.01574 =
0.01758 0.00822 -0.00172 -0.00410
C2 1 0.366663 0.173103 0.453331 11.00000 0.01581 0.01860 =
0.01780 0.00851 -0.00103 -0.00608
C3 1 0.279398 0.145860 0.525016 11.00000 0.02036 0.02494 =
0.01773 0.01011 -0.00109 -0.00781
AFIX 43
H3 2 0.265681 0.219578 0.578710 11.00000 -1.20000
AFIX 0
C4 1 0.214165 0.010033 0.515805 11.00000 0.01987 0.02333 =
0.02639 0.01590 0.00162 -0.00277
AFIX 43
H4 2 0.156299 -0.011383 0.563766 11.00000 -1.20000
AFIX 0
C5 1 0.233578 -0.096402 0.435337 11.00000 0.01989 0.01525 =
0.04106 0.01262 0.00939 -0.00013
AFIX 43
H5 2 0.187654 -0.190204 0.427571 11.00000 -1.20000
AFIX 0
C6 1 0.319949 -0.062683 0.368133 11.00000 0.02137 0.01359 =
0.03477 0.00682 0.00999 -0.00032
AFIX 43
H6 2 0.332495 -0.134323 0.313232 11.00000 -1.20000
AFIX 0
C7 1 0.733408 0.470666 0.342051 11.00000 0.02572 0.01460 =
0.01274 0.00409 0.00132 -0.00687
C8 1 0.682663 0.552016 0.278774 11.00000 0.02368 0.01383 =
0.01497 0.00368 0.00237 -0.00287
C9 1 0.811965 0.601991 0.234864 11.00000 0.02798 0.01805 =
0.01540 0.00543 0.00545 -0.00439
AFIX 43
H9 2 0.780448 0.658775 0.192975 11.00000 -1.20000
AFIX 0
C10 1 0.985924 0.569739 0.251657 11.00000 0.02479 0.02606 =
0.02111 0.00760 0.00328 -0.00984
AFIX 43
H10 2 1.072772 0.606706 0.222696 11.00000 -1.20000
AFIX 0
C11 1 1.032898 0.483484 0.310762 11.00000 0.02097 0.02717 =
0.03002 0.01248 -0.00324 -0.00827
AFIX 43
H11 2 1.151099 0.457850 0.319630 11.00000 -1.20000
AFIX 0
C12 1 0.907645 0.434103 0.357293 11.00000 0.02375 0.02453 =
0.02172 0.01072 -0.00550 -0.01022
C13 1 0.492077 0.578884 0.258587 11.00000 0.02335 0.02264 =
0.02809 0.00996 0.00697 0.00179
AFIX 123
H13A 2 0.423489 0.535280 0.296317 10.50000 -1.50000
H13B 2 0.474198 0.681757 0.273333 10.50000 -1.50000
H13C 2 0.454504 0.537103 0.192970 10.50000 -1.50000
H13D 2 0.477972 0.634147 0.212097 10.50000 -1.50000
H13E 2 0.427263 0.487670 0.235081 10.50000 -1.50000
H13F 2 0.446956 0.632323 0.315444 10.50000 -1.50000
AFIX 0
C14 1 0.959417 0.341579 0.421710 11.00000 0.02616 0.03935 =
0.03993 0.02524 -0.01161 -0.01438
AFIX 137
H14A 2 1.086152 0.349498 0.438079 11.00000 -1.50000
H14B 2 0.925098 0.242238 0.391146 11.00000 -1.50000
H14C 2 0.900736 0.372707 0.477880 11.00000 -1.50000
AFIX 0
C15 1 0.675011 0.193822 0.206335 11.00000 0.01541 0.01403 =
0.02482 0.00357 0.00432 0.00004
C16 1 0.893163 0.218361 0.095796 11.00000 0.02015 0.02137 =
0.02161 -0.00402 0.00917 -0.00601
C17 1 0.868456 0.296795 0.029430 11.00000 0.02551 0.04038 =
0.01273 0.00280 0.00405 -0.00542
C18 1 1.008066 0.303772 -0.021499 11.00000 0.03350 0.09340 =
0.01608 0.01573 0.00974 -0.00217
AFIX 43
H18 2 0.998231 0.356724 -0.066964 11.00000 -1.20000
AFIX 0
C19 1 1.161197 0.234291 -0.006565 11.00000 0.02902 0.09603 =
0.02423 0.00624 0.01534 -0.00346
AFIX 43
H19 2 1.255256 0.241513 -0.041498 11.00000 -1.20000
AFIX 0
C20 1 1.179606 0.154755 0.058151 11.00000 0.01870 0.05087 =
0.03132 -0.00726 0.00747 0.00067
AFIX 43
H20 2 1.284531 0.106110 0.066206 11.00000 -1.20000
AFIX 0
C21 1 1.044617 0.145762 0.111601 11.00000 0.02048 0.02242 =
0.03177 -0.00457 0.00605 -0.00279
C22 1 0.699014 0.367717 0.012928 11.00000 0.02849 0.04838 =
0.01915 0.01243 0.00102 -0.00269
AFIX 137
H22A 2 0.661132 0.418583 0.072357 11.00000 -1.50000
H22B 2 0.609921 0.295356 -0.019962 11.00000 -1.50000
H22C 2 0.715665 0.435391 -0.024357 11.00000 -1.50000
AFIX 0
C23 1 1.059066 0.062652 0.183315 11.00000 0.02539 0.02845 =
0.06465 0.01564 0.00748 0.00543
AFIX 137
H23A 2 1.162807 0.004344 0.176843 11.00000 -1.50000
H23B 2 0.954809 0.000691 0.175119 11.00000 -1.50000
H23C 2 1.069049 0.128459 0.244974 11.00000 -1.50000
AFIX 0
H2 2 0.433926 0.371950 0.496969 11.00000 -1.20000
HKLF 4
REM AT-178 in P-1
REM wR2 = 0.0712, GooF = S = 1.093, Restrained GooF = 1.093 for all data
REM R1 = 0.0296 for 6973 Fo > 4sig(Fo) and 0.0376 for all 7860 data
REM 268 parameters refined using 0 restraints
END
WGHT 0.0282 2.7164
REM Highest difference peak 2.311, deepest hole -1.840, 1-sigma level 0.174
Q1 1 0.5469 0.1579 0.3605 11.00000 0.05 2.31
Q2 1 0.4270 0.1857 0.2810 11.00000 0.05 2.20
Q3 1 0.5319 0.1063 0.2214 11.00000 0.05 2.16
Q4 1 0.6408 0.0787 0.2833 11.00000 0.05 2.00
Q5 1 0.6491 0.0996 0.3284 11.00000 0.05 1.99
Q6 1 0.4306 0.1674 0.2392 11.00000 0.05 1.86
Q7 1 0.4560 0.5576 0.0920 11.00000 0.05 1.33
Q8 1 0.6604 0.3976 -0.0807 11.00000 0.05 1.32
Q9 1 0.3515 0.6441 0.1866 11.00000 0.05 1.28
Q10 1 0.6587 0.1159 0.3824 11.00000 0.05 1.14
Q11 1 0.4670 0.5949 0.1949 11.00000 0.05 1.13
Q12 1 0.4398 0.2231 0.3808 11.00000 0.05 1.06
Q13 1 0.5520 0.1796 0.4180 11.00000 0.05 0.94
Q14 1 0.3548 0.6588 0.2428 11.00000 0.05 0.83
Q15 1 0.5746 0.5246 0.1479 11.00000 0.05 0.78
;
_shelx_res_checksum 18437
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt Pt1 0.53441(2) 0.13401(2) 0.28812(2) 0.01514(4) Uani d 1 . .
Cl Cl1 0.51685(14) -0.09097(9) 0.17919(8) 0.0293(2) Uani d 1 . .
N N1 0.3881(4) 0.0699(3) 0.3776(2) 0.0167(5) Uani d 1 . .
N N2 0.4380(4) 0.3015(3) 0.4560(2) 0.0208(6) Uani d 1 . .
N N3 0.6105(4) 0.4395(3) 0.3983(2) 0.0205(6) Uani d 1 . .
N N4 0.7598(4) 0.2117(3) 0.1508(2) 0.0194(6) Uani d 1 . .
C C1 0.5383(4) 0.3147(4) 0.3855(2) 0.0167(6) Uani d 1 . .
C C2 0.3667(4) 0.1731(4) 0.4533(2) 0.0169(6) Uani d 1 . .
C C3 0.2794(5) 0.1459(4) 0.5250(3) 0.0204(7) Uani d 1 . .
H H3 0.265681 0.219578 0.578710 0.024 Uiso calc 1 . .
C C4 0.2142(5) 0.0100(4) 0.5158(3) 0.0215(7) Uani d 1 . .
H H4 0.156299 -0.011383 0.563766 0.026 Uiso calc 1 . .
C C5 0.2336(5) -0.0964(4) 0.4353(3) 0.0240(8) Uani d 1 . .
H H5 0.187654 -0.190204 0.427571 0.029 Uiso calc 1 . .
C C6 0.3199(5) -0.0627(4) 0.3681(3) 0.0226(7) Uani d 1 . .
H H6 0.332495 -0.134323 0.313232 0.027 Uiso calc 1 . .
C C7 0.7334(5) 0.4707(3) 0.3421(2) 0.0176(6) Uani d 1 . .
C C8 0.6827(5) 0.5520(3) 0.2788(2) 0.0175(6) Uani d 1 . .
C C9 0.8120(5) 0.6020(4) 0.2349(2) 0.0200(7) Uani d 1 . .
H H9 0.780448 0.658775 0.192975 0.024 Uiso calc 1 . .
C C10 0.9859(5) 0.5697(4) 0.2517(3) 0.0237(7) Uani d 1 . .
H H10 1.072772 0.606706 0.222696 0.028 Uiso calc 1 . .
C C11 1.0329(5) 0.4835(4) 0.3108(3) 0.0256(8) Uani d 1 . .
H H11 1.151099 0.457850 0.319630 0.031 Uiso calc 1 . .
C C12 0.9076(5) 0.4341(4) 0.3573(3) 0.0231(7) Uani d 1 . .
C C13 0.4921(5) 0.5789(4) 0.2586(3) 0.0238(7) Uani d 1 . .
H H13A 0.423489 0.535280 0.296317 0.036 Uiso calc 0.5 . .
H H13B 0.474198 0.681757 0.273333 0.036 Uiso calc 0.5 . .
H H13C 0.454504 0.537103 0.192970 0.036 Uiso calc 0.5 . .
H H13D 0.477972 0.634147 0.212097 0.036 Uiso calc 0.5 . .
H H13E 0.427263 0.487670 0.235081 0.036 Uiso calc 0.5 . .
H H13F 0.446956 0.632323 0.315444 0.036 Uiso calc 0.5 . .
C C14 0.9594(6) 0.3416(5) 0.4217(3) 0.0335(10) Uani d 1 . .
H H14A 1.086152 0.349498 0.438079 0.050 Uiso calc 1 . .
H H14B 0.925098 0.242238 0.391146 0.050 Uiso calc 1 . .
H H14C 0.900736 0.372707 0.477880 0.050 Uiso calc 1 . .
C C15 0.6750(4) 0.1938(3) 0.2063(3) 0.0182(6) Uani d 1 . .
C C16 0.8932(5) 0.2184(4) 0.0958(3) 0.0223(7) Uani d 1 . .
C C17 0.8685(5) 0.2968(5) 0.0294(3) 0.0268(8) Uani d 1 . .
C C18 1.0081(7) 0.3038(7) -0.0215(3) 0.0468(14) Uani d 1 . .
H H18 0.998231 0.356724 -0.066964 0.056 Uiso calc 1 . .
C C19 1.1612(7) 0.2343(8) -0.0066(3) 0.0505(15) Uani d 1 . .
H H19 1.255256 0.241513 -0.041498 0.061 Uiso calc 1 . .
C C20 1.1796(6) 0.1548(6) 0.0582(3) 0.0365(11) Uani d 1 . .
H H20 1.284531 0.106110 0.066206 0.044 Uiso calc 1 . .
C C21 1.0446(5) 0.1458(4) 0.1116(3) 0.0267(8) Uani d 1 . .
C C22 0.6990(6) 0.3677(5) 0.0129(3) 0.0314(9) Uani d 1 . .
H H22A 0.661132 0.418583 0.072357 0.047 Uiso calc 1 . .
H H22B 0.609921 0.295356 -0.019962 0.047 Uiso calc 1 . .
H H22C 0.715665 0.435391 -0.024357 0.047 Uiso calc 1 . .
C C23 1.0591(6) 0.0627(5) 0.1833(4) 0.0386(11) Uani d 1 . .
H H23A 1.162807 0.004344 0.176843 0.058 Uiso calc 1 . .
H H23B 0.954809 0.000691 0.175119 0.058 Uiso calc 1 . .
H H23C 1.069049 0.128459 0.244974 0.058 Uiso calc 1 . .
H H2 0.434(8) 0.372(6) 0.497(4) 0.046 Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Pt1 0.01269(5) 0.01191(5) 0.02260(7) -0.00027(4) 0.00389(4) 0.00688(4)
Cl1 0.0335(5) 0.0139(3) 0.0412(6) -0.0005(3) 0.0197(4) 0.0019(3)
N1 0.0123(12) 0.0144(12) 0.0263(15) 0.0002(10) 0.0036(11) 0.0097(11)
N2 0.0271(15) 0.0177(13) 0.0174(14) -0.0097(12) 0.0016(12) 0.0046(11)
N3 0.0285(15) 0.0171(13) 0.0179(14) -0.0074(11) 0.0034(12) 0.0077(11)
N4 0.0175(13) 0.0155(12) 0.0247(15) -0.0017(10) 0.0043(11) 0.0030(11)
C1 0.0181(15) 0.0157(14) 0.0176(15) -0.0041(11) -0.0017(12) 0.0082(12)
C2 0.0158(14) 0.0186(14) 0.0178(15) -0.0061(11) -0.0010(12) 0.0085(12)
C3 0.0204(16) 0.0249(16) 0.0177(16) -0.0078(13) -0.0011(12) 0.0101(13)
C4 0.0199(16) 0.0233(16) 0.0264(18) -0.0028(13) 0.0016(13) 0.0159(14)
C5 0.0199(16) 0.0153(14) 0.041(2) -0.0001(12) 0.0094(15) 0.0126(15)
C6 0.0214(16) 0.0136(14) 0.035(2) -0.0003(12) 0.0100(15) 0.0068(14)
C7 0.0257(16) 0.0146(13) 0.0127(14) -0.0069(12) 0.0013(12) 0.0041(11)
C8 0.0237(16) 0.0138(13) 0.0150(15) -0.0029(12) 0.0024(12) 0.0037(11)
C9 0.0280(17) 0.0181(14) 0.0154(15) -0.0044(13) 0.0055(13) 0.0054(12)
C10 0.0248(17) 0.0261(17) 0.0211(17) -0.0098(14) 0.0033(14) 0.0076(14)
C11 0.0210(17) 0.0272(18) 0.030(2) -0.0083(14) -0.0032(14) 0.0125(16)
C12 0.0238(17) 0.0245(16) 0.0217(17) -0.0102(14) -0.0055(14) 0.0107(14)
C13 0.0234(17) 0.0226(16) 0.0281(19) 0.0018(14) 0.0070(15) 0.0100(15)
C14 0.0262(19) 0.039(2) 0.040(2) -0.0144(17) -0.0116(17) 0.025(2)
C15 0.0154(14) 0.0140(13) 0.0248(17) 0.0000(11) 0.0043(13) 0.0036(12)
C16 0.0201(16) 0.0214(15) 0.0216(17) -0.0060(13) 0.0092(13) -0.0040(13)
C17 0.0255(18) 0.040(2) 0.0127(16) -0.0054(16) 0.0041(13) 0.0028(15)
C18 0.033(2) 0.093(4) 0.0161(19) -0.002(3) 0.0097(17) 0.016(2)
C19 0.029(2) 0.096(5) 0.024(2) -0.003(3) 0.0153(18) 0.006(3)
C20 0.0187(18) 0.051(3) 0.031(2) 0.0007(18) 0.0075(16) -0.007(2)
C21 0.0205(17) 0.0224(16) 0.032(2) -0.0028(13) 0.0060(15) -0.0046(15)
C22 0.028(2) 0.048(3) 0.0192(18) -0.0027(18) 0.0010(15) 0.0124(18)
C23 0.025(2) 0.028(2) 0.065(3) 0.0054(16) 0.007(2) 0.016(2)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C15 Pt1 C1 . . 98.97(14) ?
C15 Pt1 N1 . . 178.85(14) ?
C1 Pt1 N1 . . 80.71(12) ?
C15 Pt1 Cl1 . . 85.69(10) ?
C1 Pt1 Cl1 . . 175.33(10) ?
N1 Pt1 Cl1 . . 94.63(9) ?
C2 N1 C6 . . 119.7(3) ?
C2 N1 Pt1 . . 113.5(2) ?
C6 N1 Pt1 . . 126.8(3) ?
C2 N2 C1 . . 119.2(3) ?
C2 N2 H2 . . 125(4) ?
C1 N2 H2 . . 115(4) ?
C1 N3 C7 . . 123.1(3) ?
C15 N4 C16 . . 166.0(4) ?
N3 C1 N2 . . 114.0(3) ?
N3 C1 Pt1 . . 134.9(3) ?
N2 C1 Pt1 . . 111.2(2) ?
N1 C2 N2 . . 115.2(3) ?
N1 C2 C3 . . 121.3(3) ?
N2 C2 C3 . . 123.4(3) ?
C4 C3 C2 . . 118.6(3) ?
C4 C3 H3 . . 120.7 ?
C2 C3 H3 . . 120.7 ?
C3 C4 C5 . . 119.7(3) ?
C3 C4 H4 . . 120.2 ?
C5 C4 H4 . . 120.2 ?
C6 C5 C4 . . 118.7(3) ?
C6 C5 H5 . . 120.6 ?
C4 C5 H5 . . 120.6 ?
N1 C6 C5 . . 122.0(4) ?
N1 C6 H6 . . 119.0 ?
C5 C6 H6 . . 119.0 ?
C12 C7 C8 . . 121.0(3) ?
C12 C7 N3 . . 119.4(3) ?
C8 C7 N3 . . 119.2(3) ?
C9 C8 C7 . . 118.4(3) ?
C9 C8 C13 . . 122.2(3) ?
C7 C8 C13 . . 119.4(3) ?
C10 C9 C8 . . 120.9(3) ?
C10 C9 H9 . . 119.5 ?
C8 C9 H9 . . 119.5 ?
C11 C10 C9 . . 120.0(3) ?
C11 C10 H10 . . 120.0 ?
C9 C10 H10 . . 120.0 ?
C10 C11 C12 . . 120.5(4) ?
C10 C11 H11 . . 119.7 ?
C12 C11 H11 . . 119.7 ?
C11 C12 C7 . . 119.0(3) ?
C11 C12 C14 . . 120.3(4) ?
C7 C12 C14 . . 120.7(3) ?
C8 C13 H13A . . 109.5 ?
C8 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C8 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
H13D C13 H13E . . 109.5 ?
H13D C13 H13F . . 109.5 ?
H13E C13 H13F . . 109.5 ?
C12 C14 H14A . . 109.5 ?
C12 C14 H14B . . 109.5 ?
H14A C14 H14B . . 109.5 ?
C12 C14 H14C . . 109.5 ?
H14A C14 H14C . . 109.5 ?
H14B C14 H14C . . 109.5 ?
N4 C15 Pt1 . . 171.2(3) ?
N4 C16 C21 . . 117.0(4) ?
N4 C16 C17 . . 118.8(4) ?
C21 C16 C17 . . 124.2(4) ?
C18 C17 C16 . . 116.4(4) ?
C18 C17 C22 . . 121.9(4) ?
C16 C17 C22 . . 121.7(3) ?
C19 C18 C17 . . 120.8(5) ?
C19 C18 H18 . . 119.6 ?
C17 C18 H18 . . 119.6 ?
C20 C19 C18 . . 121.3(4) ?
C20 C19 H19 . . 119.4 ?
C18 C19 H19 . . 119.4 ?
C19 C20 C21 . . 120.2(4) ?
C19 C20 H20 . . 119.9 ?
C21 C20 H20 . . 119.9 ?
C20 C21 C16 . . 117.2(4) ?
C20 C21 C23 . . 122.2(4) ?
C16 C21 C23 . . 120.6(4) ?
C17 C22 H22A . . 109.5 ?
C17 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C17 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C21 C23 H23A . . 109.5 ?
C21 C23 H23B . . 109.5 ?
H23A C23 H23B . . 109.5 ?
C21 C23 H23C . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Pt1 C15 . 1.910(3) ?
Pt1 C1 . 1.979(3) ?
Pt1 N1 . 2.048(3) ?
Pt1 Cl1 . 2.3709(9) ?
N1 C2 . 1.340(5) ?
N1 C6 . 1.355(4) ?
N2 C2 . 1.350(4) ?
N2 C1 . 1.404(4) ?
N2 H2 . 0.80(6) ?
N3 C1 . 1.291(4) ?
N3 C7 . 1.413(4) ?
N4 C15 . 1.157(5) ?
N4 C16 . 1.394(4) ?
C2 C3 . 1.405(5) ?
C3 C4 . 1.377(5) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.401(6) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.369(5) ?
C5 H5 . 0.9500 ?
C6 H6 . 0.9500 ?
C7 C12 . 1.401(5) ?
C7 C8 . 1.408(5) ?
C8 C9 . 1.399(5) ?
C8 C13 . 1.506(5) ?
C9 C10 . 1.390(6) ?
C9 H9 . 0.9500 ?
C10 C11 . 1.389(5) ?
C10 H10 . 0.9500 ?
C11 C12 . 1.398(5) ?
C11 H11 . 0.9500 ?
C12 C14 . 1.504(5) ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C13 H13D . 0.9800 ?
C13 H13E . 0.9800 ?
C13 H13F . 0.9800 ?
C14 H14A . 0.9800 ?
C14 H14B . 0.9800 ?
C14 H14C . 0.9800 ?
C16 C21 . 1.396(6) ?
C16 C17 . 1.398(6) ?
C17 C18 . 1.394(6) ?
C17 C22 . 1.505(6) ?
C18 C19 . 1.387(8) ?
C18 H18 . 0.9500 ?
C19 C20 . 1.382(8) ?
C19 H19 . 0.9500 ?
C20 C21 . 1.394(6) ?
C20 H20 . 0.9500 ?
C21 C23 . 1.496(7) ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N2 H2 N3 2_666 0.80(6) 2.15(6) 2.943(4) 173(6) yes
C6 H6 Cl1 . 0.95 2.70 3.308(4) 123 yes
C13 H13A N3 . 0.98 2.36 2.848(5) 110 yes
C22 H22B Cl1 2_655 0.98 2.78 3.660(5) 150 yes
C3 H3 Cg3 2_666 0.95 2.99 3.898(4) 162 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C7 N3 C1 N2 . . . . 172.0(3) ?
C7 N3 C1 Pt1 . . . . -8.2(6) ?
C2 N2 C1 N3 . . . . -175.3(3) ?
C2 N2 C1 Pt1 . . . . 4.9(4) ?
C6 N1 C2 N2 . . . . -179.5(3) ?
Pt1 N1 C2 N2 . . . . 2.6(4) ?
C6 N1 C2 C3 . . . . 2.1(5) ?
Pt1 N1 C2 C3 . . . . -175.9(3) ?
C1 N2 C2 N1 . . . . -5.0(5) ?
C1 N2 C2 C3 . . . . 173.4(3) ?
N1 C2 C3 C4 . . . . -0.5(5) ?
N2 C2 C3 C4 . . . . -178.8(4) ?
C2 C3 C4 C5 . . . . -1.0(6) ?
C3 C4 C5 C6 . . . . 1.0(6) ?
C2 N1 C6 C5 . . . . -2.1(6) ?
Pt1 N1 C6 C5 . . . . 175.6(3) ?
C4 C5 C6 N1 . . . . 0.6(6) ?
C1 N3 C7 C12 . . . . -80.3(5) ?
C1 N3 C7 C8 . . . . 106.8(4) ?
C12 C7 C8 C9 . . . . -3.3(5) ?
N3 C7 C8 C9 . . . . 169.5(3) ?
C12 C7 C8 C13 . . . . 175.0(3) ?
N3 C7 C8 C13 . . . . -12.2(5) ?
C7 C8 C9 C10 . . . . 1.4(5) ?
C13 C8 C9 C10 . . . . -176.9(3) ?
C8 C9 C10 C11 . . . . 1.8(6) ?
C9 C10 C11 C12 . . . . -3.1(6) ?
C10 C11 C12 C7 . . . . 1.2(6) ?
C10 C11 C12 C14 . . . . -179.6(4) ?
C8 C7 C12 C11 . . . . 2.0(6) ?
N3 C7 C12 C11 . . . . -170.8(3) ?
C8 C7 C12 C14 . . . . -177.2(4) ?
N3 C7 C12 C14 . . . . 10.0(5) ?
C15 N4 C16 C21 . . . . 9.9(16) ?
C15 N4 C16 C17 . . . . -169.7(13) ?
N4 C16 C17 C18 . . . . 177.9(4) ?
C21 C16 C17 C18 . . . . -1.6(6) ?
N4 C16 C17 C22 . . . . -3.0(6) ?
C21 C16 C17 C22 . . . . 177.4(4) ?
C16 C17 C18 C19 . . . . 0.7(8) ?
C22 C17 C18 C19 . . . . -178.3(5) ?
C17 C18 C19 C20 . . . . 0.8(9) ?
C18 C19 C20 C21 . . . . -1.5(8) ?
C19 C20 C21 C16 . . . . 0.7(7) ?
C19 C20 C21 C23 . . . . -179.2(5) ?
N4 C16 C21 C20 . . . . -178.6(3) ?
C17 C16 C21 C20 . . . . 1.0(6) ?
N4 C16 C21 C23 . . . . 1.2(6) ?
C17 C16 C21 C23 . . . . -179.2(4) ?