#------------------------------------------------------------------------------ #$Date: 2026-09-04 22:11:24 +0100 (Fri, 04 Sep 2026) $ #$Revision: 306864 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/35/2023559.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023559 loop_ _publ_author_name 'Alam, Md. Rashed' 'Lane, Robert' 'Khajkini, Mojib Pourashouri' 'Baranets, Sviatoslav' _publ_section_title ; Eu5Ga2As6 and Ba5In2As6--x Sb x : new As-containing members of the Sr5Al2Sb6 structure type ; _journal_coeditor_code YP3254 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C Structural Chemistry' _journal_paper_doi 10.1107/S2053229626008302 _journal_volume 82 _journal_year 2026 _chemical_formula_moiety 'Ba5 In2 As5.51 Sb0.49' _chemical_formula_sum 'As5.51 Ba5 In2 Sb0.49' _chemical_formula_weight 1388.57 _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_Hall '-P 2ac 2n' _space_group_name_H-M_alt 'P n m a' _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2026.05.24 svn.rec792b02 for OlexSys, GUI svn.r7575) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.0735(3) _cell_length_b 10.3287(3) _cell_length_c 13.3046(3) _cell_measurement_reflns_used 9789 _cell_measurement_temperature 100.00 _cell_measurement_theta_max 23.625 _cell_measurement_theta_min 2.663 _cell_volume 1659.13(7) _computing_cell_refinement ; SAINT (Bruker, 2019) ; _computing_data_collection ; APEX5 (Bruker, 2019) ; _computing_data_reduction ; SAINT (Bruker, 2019) ; _computing_molecular_graphics ; DIAMOND (Putz & Brandenburg, 2006) ; _computing_publication_material ; publCIF (Westrip, 2010) and OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 VENTURE DUO with a PHOTON III C14 detector' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type AgK\a _diffrn_radiation_wavelength 0.56086 _diffrn_reflns_av_R_equivalents 0.0645 _diffrn_reflns_av_unetI/netI 0.0202 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 49442 _diffrn_reflns_theta_full 19.665 _diffrn_reflns_theta_max 23.636 _diffrn_reflns_theta_min 2.378 _diffrn_source_current 0.91 _diffrn_source_power 0.0455 _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 13.751 _exptl_absorpt_correction_T_max 0.2569 _exptl_absorpt_correction_T_min 0.1355 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour 'metallic dark black' _exptl_crystal_density_diffrn 5.559 _exptl_crystal_description plate _exptl_crystal_F_000 2339 _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.07 _exptl_crystal_size_min 0.07 _refine_diff_density_max 1.094 _refine_diff_density_min -0.953 _refine_ls_extinction_coef 0.00051(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2018 (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.271 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 72 _refine_ls_number_reflns 2666 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.271 _refine_ls_R_factor_all 0.0164 _refine_ls_R_factor_gt 0.0156 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0040P)^2^+4.0318P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0331 _refine_ls_wR_factor_ref 0.0333 _reflns_number_gt 2606 _reflns_number_total 2666 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yp3254sup1.cif _cod_data_source_block Ba5In2As5.5Sb0.5 _cod_original_formula_sum 'Ba5 In2 As5.51 Sb0.49' _cod_database_code 2023559 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.406 _shelx_estimated_absorpt_t_max 0.446 _shelx_hkl_file ; 0 2 0 97.39 5.00 0 2 0 78.09 9.90 0 -2 0 97.49 5.00 0 3 0 1.80 2.90 0 -3 0 0.50 0.60 0 3 0 0.90 0.70 0 3 0 0.20 0.40 0 -3 0 -0.70 2.20 0 4 0 9379.16 423.56 0 -4 0 9999.00 426.96 0 5 0 0.20 0.80 0 -5 0 -0.20 0.50 0 5 0 0.00 0.60 0 5 0 4.00 4.40 0 -5 0 -1.30 1.70 0 -6 0 1745.43 74.19 0 6 0 1731.73 73.79 0 6 0 1705.93 74.69 0 -7 0 0.90 3.60 0 7 0 0.70 0.40 0 7 0 -1.10 0.90 0 7 0 0.00 4.00 0 -7 0 0.10 0.80 0 8 0 2278.67 98.49 0 8 0 2012.50 130.39 0 -8 0 2365.06 97.89 0 8 0 2372.06 97.49 0 9 0 0.00 0.50 0 9 0 -0.50 1.00 0 -9 0 1.00 1.20 0 9 0 -5.10 6.30 0 9 0 -0.50 0.70 0 -9 0 -5.00 4.40 0 10 0 2828.62 116.09 0 10 0 2813.82 112.79 0 10 0 2728.73 117.19 0 10 0 2345.67 155.38 0 -11 0 2.10 6.40 0 -11 0 -0.30 1.00 0 11 0 1.10 1.40 0 11 0 -0.30 1.00 0 11 0 0.60 0.50 0 11 0 1.10 9.20 0 -12 0 475.35 49.70 0 12 0 503.25 26.90 0 12 0 523.25 25.90 0 12 0 514.55 22.80 0 -12 0 518.45 26.00 0 12 0 424.06 54.39 0 13 0 0.90 1.40 0 13 0 -0.20 0.60 0 -13 0 2.40 1.60 0 13 0 2.90 11.10 0 13 0 0.20 1.30 0 -13 0 5.30 8.90 0 14 0 1826.22 76.09 0 14 0 1543.25 124.69 0 -14 0 1653.43 114.49 0 -14 0 1894.81 79.99 0 14 0 1901.21 80.59 -1 -1 0 0.50 0.40 -1 1 0 0.20 0.20 -1 -1 0 0.90 0.20 1 -1 0 -0.20 0.30 1 -1 0 0.40 0.20 -1 -2 0 1.00 0.60 -1 -2 0 -1.30 1.10 -1 2 0 -0.60 1.80 -1 2 0 0.70 0.40 -1 2 0 0.40 0.30 1 2 0 1.50 1.70 1 -2 0 0.60 0.30 1 2 0 0.80 0.30 1 -2 0 4.30 2.60 1 -2 0 1.50 0.50 1 2 0 0.20 0.50 -1 -3 0 0.10 0.60 -1 3 0 1.40 2.20 -1 3 0 0.70 0.60 -1 3 0 0.00 0.30 -1 -3 0 1.10 1.90 1 3 0 -0.10 0.50 1 -3 0 0.60 0.50 1 3 0 1.20 1.90 1 -3 0 0.50 0.50 1 3 0 0.20 0.20 1 -3 0 -1.00 0.70 -1 -4 0 2.60 4.50 -1 4 0 0.30 0.50 -1 -4 0 0.30 0.70 -1 4 0 2.50 2.30 -1 4 0 1.50 0.80 1 -4 0 0.70 0.70 1 -4 0 4.80 3.10 1 4 0 -0.10 0.70 1 4 0 -0.10 3.00 1 4 0 1.70 0.50 -1 -5 0 9.10 6.20 -1 5 0 1.00 0.90 -1 5 0 5.90 1.60 -1 5 0 1.60 3.70 1 -5 0 3.00 1.10 1 5 0 0.50 1.10 1 5 0 3.10 3.40 1 -5 0 2.70 5.00 -1 6 0 1.40 1.00 -1 -6 0 1.10 1.00 -1 -6 0 3.40 4.80 -1 6 0 4.50 5.40 -1 6 0 -0.80 0.60 1 6 0 0.90 0.40 1 6 0 1.00 1.30 1 6 0 1.00 1.20 1 -6 0 0.30 0.60 1 -6 0 2.20 3.40 1 6 0 5.90 5.60 1 -6 0 0.80 0.80 -1 7 0 0.40 0.60 -1 -7 0 -0.80 0.80 -1 -7 0 0.90 4.20 -1 7 0 -4.60 4.20 1 7 0 0.50 0.60 1 -7 0 3.10 1.40 1 7 0 0.60 0.60 1 -7 0 0.60 2.30 1 7 0 0.20 0.40 1 -7 0 1.40 1.10 1 7 0 3.50 4.70 -1 8 0 1.80 0.60 -1 -8 0 1.70 3.70 -1 8 0 2.60 1.50 -1 -8 0 1.10 1.10 -1 8 0 -2.90 3.00 -1 8 0 3.50 1.40 1 8 0 0.00 0.70 1 8 0 0.00 4.50 1 -8 0 0.40 1.30 1 8 0 3.80 1.70 -1 9 0 -0.80 0.70 -1 9 0 0.20 0.50 -1 9 0 0.60 1.00 -1 9 0 -2.10 5.20 -1 -9 0 4.00 6.30 -1 -9 0 2.70 1.40 1 9 0 -0.20 0.40 1 9 0 3.70 1.80 1 -9 0 -0.10 0.80 1 -9 0 -3.80 3.50 1 9 0 0.40 1.00 -1 -10 0 -2.60 3.70 -1 10 0 2.50 0.80 -1 10 0 0.20 1.00 -1 10 0 -0.20 5.30 -1 10 0 0.70 1.40 1 10 0 0.20 1.20 1 -10 0 -0.30 4.20 1 -10 0 0.60 0.80 1 10 0 0.30 1.00 1 10 0 2.20 5.30 1 10 0 1.70 0.70 -1 11 0 1.40 8.60 -1 11 0 1.50 0.70 -1 11 0 0.70 1.20 -1 -11 0 -0.70 3.90 -1 11 0 0.50 1.00 -1 -11 0 1.20 1.30 1 11 0 3.40 1.60 1 11 0 0.90 0.50 1 -11 0 -1.50 4.90 1 11 0 0.10 1.10 1 11 0 1.20 9.10 1 -11 0 1.40 1.60 -1 12 0 6.30 14.00 -1 12 0 0.90 1.30 -1 12 0 1.90 1.50 -1 -12 0 1.40 7.10 -1 -12 0 1.10 1.70 1 12 0 0.50 0.60 1 12 0 1.20 1.20 1 -12 0 0.20 5.40 1 12 0 -0.30 1.40 1 -12 0 0.60 1.30 1 12 0 8.00 11.30 -1 -13 0 0.60 1.40 -1 13 0 1.70 1.40 -1 -13 0 9.00 11.40 -1 13 0 -2.00 10.60 -1 13 0 -1.30 0.90 -1 13 0 1.10 0.70 1 13 0 0.30 1.20 1 13 0 3.30 11.40 1 -13 0 1.40 1.60 1 -13 0 -0.70 6.50 1 13 0 0.70 1.50 1 13 0 1.40 0.80 -1 14 0 5.40 13.80 -1 14 0 -0.70 1.30 -1 14 0 0.70 0.70 -1 -14 0 7.90 11.80 -1 -14 0 -0.10 1.30 1 -14 0 0.60 8.00 1 14 0 -5.90 11.80 1 -14 0 0.10 1.30 1 14 0 1.50 1.70 1 14 0 0.90 0.80 1 14 0 2.50 2.00 -2 0 0 36.60 1.60 -2 0 0 35.20 1.70 -2 0 0 35.00 1.80 -2 0 0 34.30 3.60 2 0 0 34.60 1.60 -2 -1 0 122.09 5.40 -2 1 0 132.79 5.60 -2 1 0 121.79 5.60 2 1 0 128.19 5.40 2 1 0 133.69 9.30 2 -1 0 127.99 5.60 2 -1 0 122.39 5.70 2 -1 0 131.29 10.20 -2 2 0 167.18 7.70 -2 2 0 161.18 7.70 -2 -2 0 195.68 14.30 -2 2 0 182.98 14.50 -2 -2 0 171.68 7.40 2 -2 0 167.48 7.70 2 -2 0 165.38 13.80 2 2 0 199.18 14.40 2 -2 0 181.28 8.10 2 2 0 165.58 7.40 -2 3 0 488.95 31.80 -2 3 0 499.15 20.90 2 3 0 487.95 20.40 2 -3 0 487.95 20.90 2 -3 0 488.55 21.00 2 3 0 470.25 31.20 2 -3 0 451.25 30.40 -2 4 0 10.70 1.60 -2 4 0 12.00 1.60 -2 -4 0 17.60 6.90 -2 4 0 11.40 5.50 2 -4 0 13.20 1.80 2 -4 0 9.70 1.40 2 4 0 10.90 2.00 2 4 0 9.80 0.90 2 -4 0 11.50 5.30 2 4 0 15.00 6.40 -2 5 0 42.70 3.50 -2 5 0 57.69 14.90 -2 -5 0 42.80 11.60 -2 5 0 42.40 3.20 -2 -5 0 55.69 4.30 2 5 0 40.30 3.90 2 -5 0 47.70 3.40 2 -5 0 48.70 3.70 2 5 0 22.40 9.00 2 -5 0 36.60 11.00 2 5 0 45.10 2.60 -2 6 0 0.70 0.60 -2 -6 0 7.90 2.10 -2 6 0 1.20 0.60 -2 -6 0 -1.70 2.40 -2 6 0 8.60 5.60 2 -6 0 -1.10 2.40 2 -6 0 2.30 0.90 2 6 0 1.90 0.90 2 6 0 3.40 3.90 2 -6 0 1.70 1.00 2 6 0 2.30 0.70 -2 -7 0 1134.39 73.69 -2 7 0 957.20 73.19 -2 7 0 1129.29 46.30 -2 7 0 1075.89 48.70 2 -7 0 1041.30 47.00 2 7 0 1068.09 47.90 2 7 0 963.00 47.80 2 7 0 1065.79 44.70 2 -7 0 1108.99 46.60 -2 8 0 86.69 6.90 -2 8 0 50.59 21.30 -2 8 0 104.69 6.50 -2 -8 0 102.59 7.30 -2 -8 0 83.39 20.60 2 8 0 84.09 7.10 2 -8 0 53.59 15.60 2 -8 0 91.19 6.60 2 8 0 91.49 23.30 2 8 0 94.79 7.60 2 8 0 93.09 5.00 2 -8 0 78.89 6.60 -2 9 0 476.45 22.70 -2 9 0 380.86 47.30 -2 9 0 453.75 23.80 -2 -9 0 493.25 47.00 2 -9 0 446.16 23.30 2 9 0 507.35 24.30 2 -9 0 472.55 23.20 2 9 0 464.15 20.70 2 9 0 474.15 24.60 -2 10 0 9.40 2.20 -2 10 0 13.20 1.90 -2 -10 0 15.90 3.40 -2 10 0 10.20 3.00 -2 10 0 13.00 11.40 -2 -10 0 8.30 8.60 2 10 0 8.90 1.50 2 10 0 5.70 2.50 2 10 0 1.50 7.30 2 10 0 8.90 2.90 2 -10 0 0.20 6.70 -2 11 0 1086.99 93.59 -2 11 0 1143.39 53.89 -2 11 0 1264.57 52.89 -2 11 0 1212.98 49.99 -2 -11 0 1180.08 84.99 2 -11 0 1107.59 53.19 2 11 0 1165.48 49.99 2 11 0 1023.10 85.49 2 11 0 1240.68 53.89 2 11 0 1197.08 54.69 -2 -12 0 25.60 4.60 -2 12 0 12.60 3.60 -2 12 0 15.30 2.20 -2 -12 0 -2.90 8.50 -2 12 0 18.50 3.60 -2 12 0 13.60 15.90 2 12 0 12.60 12.20 2 12 0 15.60 2.10 2 -12 0 4.60 7.10 2 -12 0 10.30 3.10 2 12 0 18.10 4.00 2 12 0 14.80 3.90 -2 -13 0 300.07 39.40 -2 13 0 370.06 18.70 -2 13 0 336.57 15.70 -2 13 0 259.67 53.69 -2 13 0 317.77 19.20 2 13 0 301.97 19.30 2 -13 0 321.77 18.80 2 13 0 351.76 19.10 2 13 0 306.57 53.89 -2 14 0 14.00 17.00 -2 14 0 6.50 1.50 -2 -14 0 3.60 9.10 2 14 0 7.30 2.80 2 14 0 4.10 2.90 2 -14 0 -4.20 8.80 2 -14 0 8.00 2.60 2 14 0 5.90 1.60 2 14 0 6.60 9.00 -3 0 0 0.50 0.20 -3 0 0 0.70 1.20 -3 0 0 0.10 0.20 -3 0 0 0.40 0.20 3 0 0 1.00 0.20 3 0 0 1.70 1.30 3 0 0 0.40 0.30 3 0 0 0.40 0.20 -3 1 0 1.10 0.20 -3 -1 0 0.20 0.20 -3 1 0 0.00 0.20 -3 1 0 0.20 0.20 -3 -1 0 -0.30 0.60 3 -1 0 0.30 0.20 3 1 0 -0.10 0.70 3 -1 0 0.80 1.00 3 -1 0 0.70 0.30 3 1 0 0.40 0.20 3 1 0 0.20 0.20 -3 2 0 0.60 0.40 -3 -2 0 1.00 1.60 -3 2 0 1.30 1.80 -3 -2 0 1.10 0.30 3 -2 0 1.80 2.10 3 -2 0 0.70 0.30 3 2 0 0.90 0.30 3 -2 0 0.40 0.30 3 2 0 1.50 1.50 -3 3 0 -0.30 1.40 -3 -3 0 0.70 2.80 -3 3 0 0.40 0.40 -3 -3 0 0.60 0.20 -3 3 0 0.40 0.40 3 -3 0 0.00 1.20 3 3 0 0.70 0.20 3 -3 0 0.10 0.40 3 -3 0 0.20 0.30 3 3 0 -0.40 1.20 -3 -4 0 0.20 0.30 -3 -4 0 2.90 3.40 -3 4 0 2.10 2.80 -3 4 0 1.80 0.60 -3 4 0 0.20 0.40 3 -4 0 0.10 0.40 3 4 0 0.50 0.50 3 4 0 0.20 0.20 3 -4 0 0.20 2.00 3 4 0 0.30 2.40 3 -4 0 0.70 0.40 -3 -5 0 4.10 4.80 -3 5 0 1.30 2.80 -3 -5 0 0.60 0.40 -3 5 0 0.90 0.70 -3 5 0 1.40 0.70 3 5 0 1.90 1.10 3 -5 0 1.10 0.70 3 -5 0 2.20 3.80 3 5 0 3.70 4.60 3 5 0 1.10 0.40 3 -5 0 0.50 0.50 -3 6 0 -5.30 3.20 -3 6 0 -0.30 0.20 -3 6 0 1.60 0.90 -3 -6 0 2.40 4.60 3 -6 0 1.40 2.60 3 6 0 1.10 0.50 3 -6 0 0.50 0.70 3 6 0 4.00 1.50 3 -6 0 0.40 0.40 3 6 0 -1.20 2.30 -3 -7 0 5.10 6.20 -3 7 0 -1.30 2.40 -3 7 0 2.30 1.00 -3 7 0 1.40 0.80 3 7 0 5.90 6.80 3 -7 0 0.80 0.80 3 7 0 2.10 1.50 3 -7 0 0.50 0.80 -3 8 0 9.00 8.40 -3 8 0 0.60 0.90 -3 8 0 0.20 0.60 -3 -8 0 5.10 6.50 3 8 0 -5.10 3.60 3 8 0 1.10 1.00 3 8 0 0.40 0.40 3 -8 0 0.30 4.90 3 -8 0 0.10 0.70 3 8 0 0.20 0.90 3 -8 0 0.00 1.00 -3 -9 0 2.40 5.80 -3 9 0 -0.20 6.80 -3 9 0 2.50 1.10 -3 9 0 -0.20 0.70 3 9 0 1.50 0.70 3 -9 0 1.10 0.80 3 9 0 3.10 1.70 3 9 0 1.40 1.20 3 -9 0 2.50 4.50 3 -9 0 0.10 0.70 -3 10 0 0.10 0.60 -3 10 0 0.70 1.20 -3 -10 0 -0.30 6.10 -3 10 0 -1.80 5.60 3 10 0 1.00 1.30 3 10 0 1.70 5.60 3 10 0 2.60 1.80 3 -10 0 -0.20 0.70 3 -10 0 1.10 4.80 3 10 0 1.10 0.60 -3 11 0 2.90 11.60 -3 11 0 -0.60 0.80 -3 11 0 0.50 0.60 -3 11 0 -0.50 1.20 -3 -11 0 -2.70 6.60 3 -11 0 0.10 1.50 3 -11 0 -2.50 6.20 3 11 0 6.80 2.60 3 11 0 0.10 0.50 3 11 0 -0.60 5.40 3 11 0 1.10 1.40 -3 12 0 3.40 12.50 -3 12 0 0.20 1.00 -3 12 0 1.30 0.70 -3 -12 0 0.40 6.20 -3 12 0 0.60 1.00 3 12 0 3.20 1.70 3 12 0 1.20 1.10 3 -12 0 2.30 1.80 3 12 0 2.60 7.90 3 12 0 0.30 0.50 3 -12 0 -5.20 6.80 -3 13 0 1.20 1.10 -3 13 0 0.00 12.10 -3 13 0 1.20 0.80 -3 -13 0 3.00 9.30 -3 13 0 2.30 1.80 3 13 0 2.10 1.50 3 -13 0 -3.00 6.10 3 -13 0 -0.60 1.60 3 13 0 1.10 0.70 3 13 0 -0.20 9.20 3 13 0 0.30 1.30 -3 14 0 -1.50 1.60 -3 -14 0 -0.50 9.00 -3 14 0 -11.80 15.10 -3 14 0 0.40 0.70 -3 14 0 3.80 2.10 3 14 0 2.20 0.90 3 14 0 0.20 1.60 3 -14 0 -0.20 8.60 3 14 0 -0.50 1.40 3 14 0 8.10 11.90 3 -14 0 0.70 1.60 -4 0 0 1851.71 81.59 4 0 0 1791.42 81.39 -4 1 0 199.88 8.70 -4 -1 0 191.48 14.10 -4 1 0 192.68 8.40 -4 -1 0 202.38 8.50 -4 1 0 193.58 8.80 -4 1 0 203.38 13.80 4 -1 0 182.98 8.80 4 -1 0 200.48 8.50 4 -1 0 194.78 8.70 4 -1 0 198.38 13.80 4 1 0 213.48 14.70 4 1 0 200.18 8.70 4 1 0 202.68 8.50 -4 2 0 59.29 3.30 -4 -2 0 72.99 8.50 -4 -2 0 56.59 2.90 4 2 0 52.19 7.40 4 -2 0 64.09 11.20 4 -2 0 60.19 3.20 4 2 0 58.79 2.90 4 -2 0 54.49 6.70 -4 3 0 980.00 41.20 -4 3 0 903.91 41.20 -4 3 0 1089.29 56.29 -4 -3 0 1122.29 54.29 4 -3 0 962.80 54.59 4 3 0 968.40 52.79 4 -3 0 977.30 41.30 4 -3 0 944.51 41.30 -4 4 0 866.21 37.80 -4 -4 0 1031.00 54.39 -4 4 0 983.90 55.29 -4 4 0 891.61 37.90 4 4 0 816.12 51.39 4 -4 0 866.31 52.99 4 -4 0 898.01 37.90 4 4 0 875.81 37.20 4 -4 0 872.11 38.00 -4 5 0 14.30 7.10 -4 -5 0 11.40 1.50 -4 -5 0 7.50 4.80 -4 5 0 12.90 1.80 -4 5 0 12.10 1.80 4 5 0 12.60 2.20 4 -5 0 12.70 1.90 4 -5 0 5.60 4.80 4 5 0 12.00 6.30 4 5 0 11.60 1.20 4 -5 0 17.40 2.40 -4 6 0 35.40 13.20 -4 6 0 29.90 2.80 -4 6 0 34.40 2.80 -4 -6 0 30.00 2.10 -4 -6 0 36.80 11.60 4 -6 0 32.80 3.10 4 6 0 31.70 10.50 4 6 0 38.80 3.70 4 -6 0 21.20 9.30 4 6 0 32.20 2.20 4 -6 0 25.60 2.60 -4 7 0 420.06 19.00 -4 -7 0 507.85 42.80 -4 7 0 422.76 19.50 4 7 0 397.06 17.90 4 -7 0 331.97 34.00 4 -7 0 422.36 19.20 4 7 0 397.36 20.60 4 -7 0 413.26 19.70 4 7 0 326.87 34.90 -4 8 0 117.79 7.80 -4 8 0 124.39 7.30 -4 -8 0 139.39 27.20 -4 8 0 170.98 33.50 4 -8 0 117.69 7.40 4 -8 0 115.59 7.90 4 8 0 124.69 8.90 4 -8 0 111.99 22.90 4 8 0 82.59 21.20 -4 -9 0 158.18 30.90 -4 9 0 168.88 9.20 -4 9 0 159.78 9.80 -4 9 0 170.48 35.20 4 -9 0 165.18 9.50 4 -9 0 104.19 23.80 4 -9 0 155.68 9.90 4 9 0 142.39 7.80 4 9 0 140.19 10.50 4 9 0 106.49 28.70 -4 10 0 168.68 36.90 -4 10 0 142.99 9.80 -4 10 0 162.78 9.30 -4 -10 0 160.88 33.30 4 10 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163.48 8.60 -10 4 0 138.99 6.70 -10 -4 0 135.49 17.70 -10 -4 0 135.19 6.70 -10 4 0 152.58 7.60 -10 4 0 132.19 7.50 10 4 0 137.29 7.40 10 -4 0 132.69 7.80 10 -4 0 124.69 23.30 10 -4 0 126.19 15.80 10 -4 0 139.59 7.60 10 4 0 151.28 19.20 10 4 0 143.09 7.30 10 4 0 145.89 6.90 -10 -5 0 96.09 19.10 -10 5 0 79.19 5.00 -10 5 0 73.69 4.10 -10 -5 0 74.89 4.20 -10 5 0 71.59 4.70 10 -5 0 102.69 22.30 10 5 0 61.29 14.90 10 -5 0 64.29 13.50 10 5 0 76.49 4.60 10 -5 0 72.29 5.10 10 -5 0 74.69 5.00 -10 -6 0 83.09 4.60 -10 6 0 81.49 4.60 -10 -6 0 100.59 20.10 -10 6 0 83.39 5.40 -10 6 0 84.39 5.20 10 6 0 88.69 18.90 10 -6 0 72.39 5.40 10 -6 0 62.29 17.50 10 6 0 82.49 5.10 10 -6 0 82.09 5.60 10 -6 0 77.99 15.60 10 6 0 81.99 4.60 -10 -7 0 803.32 56.39 -10 7 0 720.13 30.50 -10 7 0 695.33 31.50 -10 -7 0 708.83 30.30 -10 7 0 733.43 31.30 10 -7 0 692.93 47.30 10 7 0 694.33 30.40 10 -7 0 693.33 31.70 10 7 0 690.63 30.90 10 7 0 637.14 52.59 10 -7 0 672.63 56.59 -10 8 0 82.99 5.40 -10 -8 0 76.69 4.60 -10 -8 0 74.69 19.20 -10 8 0 84.19 5.60 10 8 0 69.79 6.20 10 -8 0 81.89 5.90 10 8 0 72.09 19.70 10 -8 0 72.79 5.80 10 -8 0 89.09 17.10 10 8 0 67.69 4.50 10 -8 0 53.19 17.90 -10 9 0 539.05 24.00 -10 9 0 513.15 23.80 -10 -9 0 507.85 23.20 10 9 0 520.75 22.70 10 9 0 395.46 44.00 10 -9 0 434.86 46.70 10 -9 0 510.15 24.70 10 9 0 511.55 25.60 10 -9 0 498.85 24.10 -10 10 0 62.99 23.40 -10 10 0 58.49 5.00 -10 -10 0 59.39 18.40 10 10 0 31.10 16.00 10 -10 0 57.19 5.10 10 -10 0 56.39 5.50 10 10 0 61.69 4.20 10 -10 0 65.79 21.20 10 10 0 55.29 5.90 -10 11 0 1030.10 44.40 -10 11 0 1113.49 89.39 -10 -11 0 1131.09 81.79 -10 11 0 1055.59 44.30 10 11 0 959.10 42.70 10 -11 0 1015.30 45.60 10 -11 0 776.22 72.19 10 11 0 890.01 46.10 10 -11 0 958.20 44.60 -10 -12 0 41.10 17.60 -10 12 0 38.00 4.10 -10 12 0 54.39 26.60 10 -12 0 31.60 5.30 10 -12 0 17.10 15.00 10 12 0 36.20 6.30 10 -12 0 37.10 5.00 10 12 0 17.90 12.90 -11 0 0 0.30 0.50 -11 0 0 2.20 2.50 -11 0 0 0.30 0.40 11 0 0 2.20 3.60 11 0 0 2.30 0.70 11 0 0 0.60 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4.70 1.10 -12 4 -3 4.10 0.70 -12 4 -3 5.80 1.40 12 4 -3 4.40 1.30 12 -4 3 5.70 1.60 12 4 -3 1.30 5.80 12 -4 3 -0.50 3.00 12 4 -3 4.10 1.00 12 4 -3 4.60 1.30 12 -4 3 2.30 1.00 12 -4 3 0.90 5.30 -12 -5 3 -4.70 3.60 -12 -5 3 1.30 0.70 -12 5 -3 1.10 0.70 -12 5 -3 1.00 0.70 -12 5 -3 2.00 0.60 12 -5 3 0.90 0.90 12 -5 3 2.70 4.50 12 5 -3 1.20 0.70 12 5 -3 0.60 0.80 12 -5 3 6.40 7.50 12 5 -3 0.70 0.50 12 5 -3 -1.30 4.60 12 -5 3 -0.20 0.60 -12 -6 3 31.80 12.50 -12 6 -3 33.20 3.00 -12 -6 3 33.20 2.60 -12 6 -3 36.70 2.20 -12 6 -3 29.90 2.90 12 -6 3 34.40 3.50 12 6 -3 33.70 2.70 12 6 -3 37.70 15.70 12 6 -3 31.90 2.90 12 -6 3 24.10 3.40 12 6 -3 28.10 2.80 12 -6 3 11.60 9.20 12 -6 3 31.90 10.70 -12 7 -3 1015.80 43.90 -12 7 -3 1049.09 43.90 -12 -7 3 1190.28 74.09 -12 7 -3 1068.29 42.50 -12 -7 3 985.50 43.10 12 -7 3 1000.40 44.40 12 7 -3 993.90 43.70 12 7 -3 1016.50 43.70 12 -7 3 955.90 62.19 12 7 -3 1011.00 43.10 12 7 -3 919.21 69.89 12 -7 3 1000.90 44.80 12 -7 3 865.01 72.19 -12 -8 3 10.90 8.30 -12 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12.00 -5 6 14 88.79 5.80 -5 6 14 97.79 7.60 -5 6 14 91.29 4.90 5 -6 -14 86.09 5.70 5 6 14 94.79 4.40 5 6 14 98.39 5.20 5 -6 -14 104.69 8.60 5 6 14 90.49 9.20 5 -6 -14 85.89 11.40 5 -6 -14 58.09 14.20 -5 5 14 9.50 1.90 -5 5 14 10.40 2.70 5 -5 -14 6.00 3.60 5 -5 -14 11.80 6.50 5 5 14 7.80 0.70 5 -5 -14 15.10 3.70 5 -5 -14 8.90 1.60 5 5 14 10.30 1.10 5 5 14 7.10 2.70 -5 4 14 239.78 12.60 -5 4 14 221.98 10.20 -5 4 14 192.28 12.80 5 -4 -14 208.18 18.10 5 4 14 241.28 15.40 5 -4 -14 231.88 10.70 5 4 14 237.58 10.60 5 -4 -14 176.88 19.30 5 -4 -14 229.68 13.80 -5 3 14 31.10 2.70 -5 3 14 27.40 3.10 5 -3 -14 23.20 7.50 5 3 14 31.50 5.40 5 -3 -14 31.90 2.30 5 -3 -14 34.10 5.00 5 -3 -14 27.20 7.10 5 3 14 32.90 2.30 -5 2 14 20.20 2.10 -5 2 14 17.70 2.60 5 2 14 17.50 4.10 5 -2 -14 15.30 5.80 5 -2 -14 23.40 7.20 5 -2 -14 20.60 3.60 5 -2 -14 20.30 1.60 5 2 14 23.80 1.70 -5 1 14 29.00 2.70 -5 1 14 24.60 2.30 5 -1 -14 41.60 9.70 5 1 14 27.20 1.80 5 -1 -14 22.00 7.30 5 -1 -14 28.80 1.90 5 -1 -14 24.10 3.90 -5 0 14 402.86 24.80 -5 0 14 419.46 18.50 -5 0 14 412.46 18.40 5 0 14 397.46 17.30 5 0 -14 408.06 17.50 5 0 -14 354.36 29.70 5 0 -14 393.46 20.00 5 0 -14 440.56 19.00 -5 -1 14 27.20 2.40 -5 -1 14 32.00 6.90 -5 -1 14 27.80 2.30 5 -1 14 25.80 1.70 5 1 -14 32.50 10.20 5 -1 14 30.20 2.50 5 1 -14 30.40 4.00 5 1 -14 28.00 2.90 5 -1 14 20.90 4.60 5 -1 14 27.40 3.40 5 1 -14 27.50 2.50 5 1 -14 29.80 1.90 -5 -2 14 25.00 2.20 -5 2 -14 23.00 1.30 -5 -2 14 23.20 6.70 5 -2 14 20.80 1.40 5 -2 14 16.50 4.00 5 2 -14 20.70 2.10 5 2 -14 19.50 1.60 5 -2 14 20.30 6.60 5 2 -14 24.10 3.30 5 -2 14 24.60 2.60 5 2 -14 12.30 7.90 5 2 -14 22.10 3.30 -5 -3 14 33.10 2.10 -5 3 -14 32.70 1.90 -5 -3 14 31.10 2.60 -5 -3 14 34.20 8.30 5 3 -14 39.00 3.80 5 3 -14 30.20 3.00 5 -3 14 31.40 4.10 5 3 -14 35.10 2.70 5 -3 14 42.20 7.10 5 3 -14 31.10 2.20 5 -3 14 32.00 1.80 5 -3 14 29.00 2.10 5 -3 14 13.60 7.00 -5 4 -14 238.08 10.50 -5 -4 14 251.97 22.10 -5 -4 14 242.58 11.20 5 -4 14 240.78 10.40 5 4 -14 248.08 10.80 5 4 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3.40 9.40 5 9 -14 3.60 2.40 5 -9 14 5.70 12.20 -6 8 14 0.50 0.80 -6 8 14 2.10 0.80 -6 8 14 2.20 1.50 6 8 14 3.80 9.80 6 -8 -14 9.40 8.10 6 8 14 4.30 0.80 6 8 14 3.10 1.20 6 -8 -14 -0.90 1.30 6 -8 -14 -0.20 4.00 6 -8 -14 1.70 1.50 6 8 14 1.20 1.60 -6 7 14 17.10 1.80 -6 7 14 15.70 3.50 -6 7 14 20.30 3.00 6 -7 -14 21.80 7.70 6 7 14 15.20 4.30 6 -7 -14 15.90 8.00 6 -7 -14 18.50 5.70 6 7 14 17.30 1.40 6 -7 -14 21.30 3.00 -6 6 14 -0.10 0.90 -6 6 14 0.60 0.60 -6 6 14 0.10 0.40 6 -6 -14 1.40 1.50 6 -6 -14 2.60 1.10 6 -6 -14 3.30 4.20 6 6 14 1.10 0.90 6 6 14 1.30 1.50 6 -6 -14 0.10 3.40 6 6 14 1.20 0.50 -6 5 14 6.60 1.10 -6 5 14 10.60 2.50 -6 5 14 9.40 1.70 6 5 14 6.60 3.80 6 5 14 4.50 2.50 6 5 14 7.90 0.80 6 -5 -14 9.10 1.70 6 -5 -14 15.90 7.10 6 -5 -14 4.50 4.00 6 -5 -14 5.70 2.30 6 5 14 6.70 1.30 6 5 14 2.40 2.40 -6 4 14 87.49 6.40 -6 4 14 91.29 5.60 6 4 14 88.79 4.90 6 -4 -14 69.99 14.70 6 4 14 88.49 8.60 6 4 14 89.69 4.10 6 -4 -14 76.49 6.90 6 -4 -14 98.99 12.50 6 4 14 97.29 4.90 6 -4 -14 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7.90 6 2 -14 151.68 8.60 6 -2 14 107.09 15.30 6 2 -14 135.79 6.60 -6 -3 14 3.50 4.00 -6 -3 14 4.70 1.10 -6 -3 14 7.80 1.30 -6 3 -14 8.60 0.90 6 3 -14 7.80 2.00 6 -3 14 10.60 1.40 6 -3 14 5.40 1.70 6 -3 14 4.80 6.30 6 3 -14 5.50 1.40 6 -3 14 5.50 3.20 6 3 -14 9.30 8.00 6 3 -14 9.10 1.70 6 3 -14 7.40 1.10 -6 4 -14 93.19 4.70 -6 -4 14 90.29 5.40 -6 -4 14 111.09 14.40 6 4 -14 92.89 5.50 6 -4 14 90.09 6.90 6 4 -14 83.39 8.20 6 4 -14 62.39 19.20 6 -4 14 67.19 18.10 6 4 -14 87.19 5.40 6 -4 14 107.59 11.50 6 4 -14 95.89 5.00 6 -4 14 95.89 4.80 -6 -5 14 5.00 1.40 -6 5 -14 7.60 1.20 -6 -5 14 13.00 6.00 6 5 -14 5.70 8.90 6 5 -14 3.40 1.90 6 5 -14 7.20 1.30 6 -5 14 11.30 5.00 6 5 -14 7.50 1.40 6 -5 14 8.20 1.10 6 5 -14 10.50 2.00 6 -5 14 9.60 2.70 6 -5 14 14.80 10.70 -6 -6 14 -1.30 5.30 -6 6 -14 0.60 0.60 -6 -6 14 0.50 0.60 -6 6 -14 0.70 4.80 6 6 -14 3.70 7.00 6 6 -14 -2.20 1.00 6 -6 14 2.20 1.60 6 6 -14 2.90 0.90 6 -6 14 4.30 8.60 6 6 -14 0.30 0.60 -6 -7 14 17.80 2.00 -6 7 -14 14.30 2.00 -6 -7 14 14.10 6.90 -6 7 -14 16.60 1.30 -6 7 -14 17.60 10.00 6 7 -14 1.40 10.20 6 -7 14 13.60 3.40 6 7 -14 17.50 1.90 6 7 -14 12.20 1.80 6 -7 14 15.20 9.60 -6 8 -14 2.30 0.60 -6 8 -14 3.40 8.00 -6 -8 14 1.00 0.70 -6 -8 14 1.40 7.20 -6 8 -14 1.40 0.80 6 8 -14 2.20 1.60 6 -8 14 19.00 12.40 6 -8 14 0.70 1.20 6 8 -14 2.60 10.80 6 8 -14 2.70 0.90 -7 7 14 88.99 5.90 -7 7 14 84.49 4.90 -7 7 14 92.29 7.40 7 7 14 76.79 4.30 7 7 14 78.29 8.60 7 7 14 87.89 5.90 7 -7 -14 75.39 13.80 7 -7 -14 92.99 6.00 7 -7 -14 82.49 7.70 7 7 14 71.39 18.20 7 -7 -14 57.49 16.20 7 7 14 80.69 4.80 -7 6 14 95.29 6.60 -7 6 14 119.79 8.30 -7 6 14 110.39 6.00 7 6 14 110.59 6.00 7 -6 -14 105.49 14.10 7 6 14 123.49 7.00 7 -6 -14 118.19 6.90 7 -6 -14 94.49 19.30 7 6 14 114.69 5.40 7 6 14 120.19 10.60 7 -6 -14 108.79 8.80 -7 5 14 31.50 3.00 -7 5 14 38.10 5.10 -7 5 14 31.90 2.40 7 -5 -14 22.40 3.90 7 5 14 32.10 2.00 7 -5 -14 26.30 8.40 7 -5 -14 47.90 13.40 7 5 14 35.10 3.10 -7 4 14 70.69 5.40 -7 4 14 71.89 4.70 -7 4 14 67.29 3.90 7 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2.10 7 -1 14 5.20 5.90 -7 -2 14 49.80 4.20 -7 2 -14 44.40 2.40 -7 -2 14 44.30 3.00 -7 -2 14 41.10 9.40 7 2 -14 36.50 3.20 7 -2 14 47.50 3.90 7 -2 14 34.50 11.20 7 2 -14 43.30 4.10 7 2 -14 21.10 10.40 7 -2 14 45.40 7.80 7 -2 14 44.50 3.00 7 2 -14 43.90 2.90 7 2 -14 40.30 3.70 -7 -3 14 28.20 8.90 -7 3 -14 31.50 2.00 -7 -3 14 29.20 2.90 7 3 -14 29.20 2.70 7 3 -14 32.10 2.90 7 -3 14 30.80 3.40 7 3 -14 30.90 2.40 7 -3 14 33.10 2.40 7 -3 14 49.99 8.50 7 3 -14 13.50 9.80 7 -3 14 14.70 9.00 -7 -4 14 76.29 4.60 -7 4 -14 69.69 3.80 -7 -4 14 64.89 13.00 7 4 -14 67.69 4.60 7 -4 14 69.89 4.10 7 4 -14 69.59 6.10 7 -4 14 70.09 5.80 7 4 -14 69.39 19.90 7 4 -14 70.29 4.60 7 -4 14 45.70 15.80 7 -4 14 70.59 9.80 7 4 -14 83.69 5.80 -7 -5 14 35.80 10.60 -7 -5 14 31.50 2.70 -7 5 -14 29.30 2.30 7 -5 14 31.30 2.30 7 5 -14 30.20 2.40 7 -5 14 7.20 10.40 7 -5 14 29.20 4.50 7 5 -14 37.30 2.80 7 5 -14 14.20 9.50 7 5 -14 34.00 2.90 -7 6 -14 117.99 6.20 -7 -6 14 109.19 19.50 -7 -6 14 127.69 6.70 7 6 -14 77.89 21.80 7 -6 14 103.09 24.20 7 -6 14 132.09 15.10 7 6 -14 125.89 6.30 7 -6 14 106.09 8.50 7 6 -14 122.39 6.40 7 -6 14 109.49 5.80 7 6 -14 112.09 6.60 -7 -7 14 102.79 20.70 -7 -7 14 80.89 5.10 -7 7 -14 85.09 5.00 7 7 -14 87.39 5.30 7 7 -14 84.39 5.10 7 7 -14 64.99 7.10 7 -7 14 79.99 21.70 7 -7 14 96.69 7.90 -7 -8 14 18.50 11.10 -8 7 14 22.20 2.20 -8 7 14 22.10 4.00 -8 7 14 19.80 2.70 8 7 14 23.70 1.90 8 7 14 21.70 4.80 8 -7 -14 29.80 12.10 8 -7 -14 29.20 5.60 8 7 14 23.30 3.40 8 -7 -14 20.00 9.10 8 7 14 24.60 2.20 8 7 14 22.10 11.30 -8 6 14 0.90 0.70 -8 6 14 1.40 0.90 -8 6 14 1.70 1.20 8 6 14 -2.00 5.70 8 -6 -14 0.80 1.70 8 6 14 0.80 0.60 8 6 14 2.50 1.20 8 -6 -14 -3.20 5.60 8 6 14 0.50 0.40 8 -6 -14 -0.20 3.90 8 -6 -14 4.40 1.30 -8 5 14 0.70 0.60 -8 5 14 0.60 1.00 -8 5 14 1.40 1.00 8 -5 -14 3.70 4.60 8 5 14 0.30 0.40 8 -5 -14 0.80 0.80 8 5 14 1.50 1.00 8 5 14 1.00 0.60 8 -5 -14 -0.50 6.10 8 5 14 -0.40 4.40 8 -5 -14 1.10 1.20 -8 4 14 183.08 9.50 -8 4 14 184.18 8.80 8 4 14 179.58 8.40 8 -4 -14 213.98 23.20 8 4 14 195.08 16.60 8 4 14 146.09 15.70 8 -4 -14 179.38 11.30 8 4 14 175.88 8.20 8 -4 -14 172.78 9.10 8 -4 -14 180.88 19.50 8 4 14 175.68 9.90 -8 3 14 4.60 1.40 -8 3 14 4.50 1.40 8 3 14 0.50 4.00 8 -3 -14 -2.60 3.70 8 3 14 4.70 0.80 8 -3 -14 4.20 1.60 8 -3 -14 3.60 4.70 8 3 14 6.20 1.00 8 -3 -14 3.60 0.90 8 3 14 2.80 3.70 8 3 14 4.20 0.80 -8 2 14 96.49 5.70 -8 2 14 91.99 6.10 8 -2 -14 85.49 15.80 8 -2 -14 92.09 18.60 8 2 14 85.19 11.30 8 2 14 92.29 4.40 8 -2 -14 98.79 5.20 8 2 14 91.99 4.30 8 2 14 92.79 10.70 8 -2 -14 88.09 6.70 8 2 14 91.49 4.80 -8 1 14 5.50 1.30 -8 1 14 4.60 1.30 8 -1 -14 2.50 1.30 8 -1 -14 3.90 0.90 8 1 14 5.40 1.10 8 1 14 9.40 5.80 8 1 14 5.10 3.80 8 -1 -14 3.40 5.10 -8 0 14 450.95 20.00 -8 0 14 439.66 19.90 -8 0 14 488.95 31.00 8 0 -14 439.96 19.20 8 0 14 437.56 19.60 8 0 14 451.45 26.30 8 0 14 356.26 30.30 8 0 -14 435.26 21.00 8 0 -14 399.26 34.00 -8 -1 14 4.30 1.10 -8 -1 14 4.80 1.10 -8 -1 14 1.20 3.60 8 -1 14 3.80 1.70 8 -1 14 7.20 3.60 8 1 -14 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414.06 19.10 3 4 -17 397.76 18.40 -3 -5 17 54.39 11.80 -3 -5 17 46.40 3.50 -3 5 -17 47.80 2.70 -3 5 -17 65.99 13.10 3 5 -17 49.60 2.90 3 -5 17 46.80 2.90 3 5 -17 30.60 12.80 3 5 -17 47.60 4.00 3 5 -17 47.00 3.50 3 -5 17 42.70 10.80 -3 6 -17 59.09 4.30 -3 6 -17 64.59 3.70 -3 6 -17 85.19 16.30 -3 -6 17 63.49 4.10 3 6 -17 61.29 4.00 3 -6 17 62.79 3.60 3 6 -17 29.20 13.60 3 6 -17 65.59 5.30 3 -6 17 76.49 18.50 3 6 -17 63.59 4.20 -4 5 17 8.60 2.30 -4 5 17 9.70 1.80 4 5 17 7.60 2.70 4 -5 -17 11.90 3.80 4 5 17 9.60 1.80 4 -5 -17 7.50 2.80 -4 4 17 30.50 4.10 -4 4 17 32.20 2.90 4 4 17 37.20 5.90 4 4 17 30.50 2.50 -4 3 17 8.40 2.10 -4 3 17 11.70 2.00 4 3 17 8.00 1.30 4 3 17 10.50 3.20 -4 2 17 3.50 1.40 -4 2 17 1.50 0.80 4 2 17 2.40 1.70 4 2 17 1.00 0.50 -4 1 17 9.10 1.60 -4 1 17 10.70 2.00 4 1 17 8.30 2.50 4 -1 -17 8.70 3.60 4 1 17 11.80 1.20 4 -1 -17 9.80 3.30 -4 0 17 95.09 5.80 -4 0 17 95.49 5.70 4 0 17 92.59 4.80 4 0 17 104.29 7.50 -4 -1 17 13.10 1.80 -4 -1 17 16.70 2.80 4 1 -17 11.50 6.00 4 -1 17 10.70 1.10 4 1 -17 11.70 1.30 4 -1 17 11.90 2.60 4 1 -17 12.40 0.90 -4 -2 17 1.10 0.90 -4 -2 17 1.00 2.90 -4 -2 17 1.40 0.50 4 2 -17 4.30 5.70 4 2 -17 1.40 0.50 4 2 -17 2.90 1.10 -4 -3 17 11.20 4.80 -4 -3 17 8.00 1.50 4 -3 17 10.20 1.00 4 3 -17 1.00 5.70 4 -3 17 9.30 2.30 4 3 -17 10.20 2.10 4 -3 17 10.60 1.50 4 -3 17 8.70 1.10 4 -3 17 8.80 2.50 4 3 -17 9.10 1.60 -4 -4 17 46.80 9.60 -4 4 -17 34.80 1.80 -4 -4 17 35.60 2.90 4 -4 17 28.30 7.20 4 4 -17 32.20 2.90 4 -4 17 36.10 2.30 4 4 -17 38.20 2.40 4 4 -17 20.20 11.70 4 4 -17 34.30 3.40 -4 5 -17 7.90 1.00 -4 -5 17 8.90 1.60 -4 -5 17 14.00 7.00 4 5 -17 -2.30 8.40 4 5 -17 9.10 1.90 4 -5 17 7.30 5.70 4 5 -17 8.20 1.20 4 5 -17 8.70 2.20 4 -5 17 8.50 1.10 -5 5 17 6.20 2.10 -5 5 17 7.80 1.80 5 5 17 11.20 3.30 5 5 17 7.30 1.40 5 -5 -17 2.00 5.00 5 -5 -17 4.80 4.60 -5 4 17 15.20 3.50 -5 4 17 13.60 2.30 5 -4 -17 11.70 5.60 5 -4 -17 9.20 4.40 5 4 17 11.90 3.90 5 4 17 10.80 1.60 -5 3 17 65.99 5.00 -5 3 17 54.69 4.10 5 3 17 60.09 3.50 5 -3 -17 51.59 9.10 5 3 17 66.39 7.00 5 -3 -17 52.19 9.70 -5 2 17 4.60 1.20 -5 2 17 6.00 1.60 5 2 17 8.10 1.20 5 -2 -17 5.50 7.00 5 2 17 3.60 2.00 5 -2 -17 6.00 4.60 -5 1 17 20.50 2.70 -5 1 17 16.00 2.40 5 -1 -17 18.00 1.30 5 -1 -17 12.30 6.10 5 -1 -17 14.30 1.50 5 1 17 28.10 5.30 5 1 17 16.30 1.40 -5 0 17 41.10 3.20 -5 0 17 38.10 3.10 5 0 17 39.50 2.40 5 0 -17 28.40 9.60 5 0 -17 42.40 2.30 5 0 17 52.99 6.70 -5 -1 17 20.50 2.00 -5 -1 17 19.00 2.10 5 1 -17 18.40 2.60 5 -1 17 16.90 3.50 5 1 -17 8.10 7.60 5 1 -17 17.90 1.40 -5 -2 17 5.70 1.40 -5 -2 17 7.10 1.20 -5 -2 17 4.50 3.40 5 -2 17 6.90 0.90 5 2 -17 3.60 1.50 5 2 -17 7.70 1.60 5 -2 17 6.70 1.90 5 -2 17 5.50 1.10 5 2 -17 -4.10 5.70 -5 -3 17 74.49 11.80 -5 -3 17 63.79 4.20 5 3 -17 63.49 3.50 5 -3 17 62.89 4.30 5 -3 17 62.89 3.50 5 -3 17 64.99 5.90 5 3 -17 59.69 5.00 5 -3 17 59.19 7.10 5 -3 17 64.39 3.30 -5 -4 17 10.00 1.80 -5 -4 17 9.30 5.60 -5 4 -17 10.90 0.90 5 -4 17 13.20 2.20 5 -4 17 17.90 7.10 5 4 -17 10.80 1.90 5 -4 17 10.50 1.00 5 4 -17 10.20 2.50 5 4 -17 1.70 5.70 5 -4 17 17.10 7.10 5 4 -17 10.10 1.30 5 -5 17 -1.00 5.80 5 -5 17 12.40 2.50 5 5 -17 3.60 12.10 5 -5 17 8.70 4.30 5 5 -17 6.20 2.50 5 5 -17 4.30 1.20 -6 4 17 74.59 5.90 -6 4 17 71.99 4.80 6 -4 -17 62.39 4.80 6 4 17 68.29 9.30 6 -4 -17 59.69 6.60 6 -4 -17 56.49 11.30 6 4 17 69.49 4.00 -6 3 17 10.30 1.90 -6 3 17 11.80 2.50 6 -3 -17 8.50 1.40 6 -3 -17 9.40 3.10 6 -3 -17 8.10 5.30 6 3 17 10.80 1.40 6 3 17 15.80 4.30 -6 2 17 109.29 6.90 -6 2 17 109.59 6.40 6 2 17 107.39 5.30 6 2 17 114.09 9.60 6 -2 -17 111.99 5.40 6 -2 -17 79.89 14.60 6 -2 -17 102.09 8.40 -6 1 17 2.30 1.00 -6 1 17 2.00 1.10 6 1 17 4.70 0.80 6 -1 -17 -0.30 1.30 6 -1 -17 2.60 0.70 6 -1 -17 3.50 1.30 6 -1 -17 4.80 4.90 6 -1 -17 -0.30 5.20 6 1 17 4.20 2.30 -6 0 17 68.89 4.40 -6 0 17 63.89 4.30 6 0 -17 67.79 4.60 6 0 -17 55.39 5.70 6 0 17 62.69 3.20 6 0 17 64.09 6.30 6 0 -17 75.19 13.70 6 0 -17 42.30 11.30 6 0 -17 63.09 4.60 -6 -1 17 2.30 0.90 -6 -1 17 4.20 3.90 -6 -1 17 3.30 0.90 6 1 -17 3.60 0.80 6 -1 17 2.90 0.50 6 1 -17 1.80 1.50 6 1 -17 4.70 1.70 6 1 -17 -0.80 6.20 6 -1 17 4.80 1.90 -6 -2 17 112.39 6.40 -6 -2 17 111.29 5.80 -6 -2 17 114.69 12.50 6 -2 17 115.59 5.80 6 -2 17 112.39 8.00 6 2 -17 90.69 18.90 6 2 -17 116.59 5.60 6 2 -17 104.09 7.30 -6 -3 17 9.30 1.70 -6 -3 17 8.20 4.50 6 3 -17 13.80 3.00 6 3 -17 10.90 1.90 6 -3 17 10.30 1.90 6 -3 17 14.50 2.80 6 -3 17 10.70 5.00 6 3 -17 14.10 1.40 6 3 -17 18.10 8.90 6 -3 17 11.70 1.30 6 -3 17 14.90 3.90 -6 -4 17 71.79 4.70 -6 4 -17 71.39 3.40 6 -4 17 78.59 13.30 6 4 -17 65.89 6.10 6 -4 17 69.99 5.20 6 -4 17 72.49 3.80 6 4 -17 69.59 4.10 6 -4 17 65.89 13.40 6 4 -17 74.89 4.90 -7 2 17 134.39 7.80 -7 2 17 124.39 7.20 7 -2 -17 110.89 9.10 7 -2 -17 96.19 16.50 7 2 17 129.99 6.00 7 2 17 121.19 10.40 7 -2 -17 116.89 16.30 7 -2 -17 133.69 6.50 -7 1 17 7.50 1.70 -7 1 17 11.50 2.00 7 1 17 9.90 0.90 7 -1 -17 11.30 1.40 7 -1 -17 15.50 2.40 7 1 17 14.50 3.90 7 -1 -17 8.10 2.70 7 -1 -17 1.30 6.10 7 -1 -17 1.90 5.90 -7 0 17 2.50 0.90 -7 0 17 1.00 0.80 7 0 -17 0.70 1.00 7 0 -17 1.00 0.60 7 0 -17 1.10 5.40 7 0 -17 -3.10 5.60 7 0 -17 0.20 1.30 7 0 17 1.00 1.80 -7 -1 17 8.70 1.50 -7 -1 17 9.80 1.70 -7 -1 17 11.40 5.10 7 1 -17 9.90 9.10 7 1 -17 9.00 2.60 7 -1 17 8.30 2.70 7 1 -17 9.30 2.20 7 1 -17 8.00 1.20 -7 -2 17 128.09 7.20 -7 -2 17 117.29 15.80 -7 -2 17 122.09 6.50 7 2 -17 122.79 6.30 7 -2 17 141.39 6.80 7 2 -17 91.99 19.80 7 2 -17 131.69 7.50 7 2 -17 130.79 8.40 7 2 -17 127.59 8.40 7 -2 17 140.49 7.10 7 -2 17 114.49 9.70 7 -2 17 126.69 9.30 7 -2 17 130.09 8.70 0 4 18 12.80 2.90 0 3 18 0.50 0.70 0 3 18 0.70 1.20 0 2 18 81.29 6.00 0 2 18 69.39 4.40 0 1 18 0.10 0.80 0 1 18 1.20 0.60 0 0 18 3.90 1.30 0 0 18 2.90 0.90 0 -1 18 0.70 0.60 0 -1 18 0.00 0.40 0 -2 18 70.79 4.20 0 -2 18 70.49 3.80 0 -3 18 1.10 0.70 0 -4 18 16.80 4.60 0 -4 18 18.30 1.80 0 4 -18 17.30 1.00 -1 4 18 9.40 2.50 1 4 18 8.90 2.60 1 4 18 10.60 2.70 -1 3 18 38.50 4.30 1 3 18 44.80 5.00 1 3 18 40.10 3.00 -1 2 18 2.30 1.30 1 2 18 0.00 1.10 1 2 18 1.00 0.60 -1 1 18 0.50 0.60 -1 1 18 0.40 0.80 1 1 18 0.40 0.60 1 1 18 0.00 0.80 -1 0 18 28.60 2.40 -1 0 18 28.00 2.70 1 0 18 28.10 2.30 1 0 18 30.10 2.90 -1 -1 18 0.20 0.60 -1 -1 18 1.20 0.60 1 -1 18 0.60 0.60 1 -1 18 1.90 0.80 -1 -2 18 2.10 0.80 -1 -2 18 1.30 0.50 1 -2 18 1.00 0.60 1 -2 18 1.10 0.60 -1 -3 18 38.20 4.60 -1 -3 18 38.90 2.80 1 -3 18 36.40 2.60 1 3 -18 36.10 6.40 -1 -4 18 11.70 4.30 -1 -4 18 7.80 1.40 -1 4 -18 9.00 4.30 1 4 -18 6.20 5.70 1 -4 18 6.60 1.20 1 4 -18 7.80 0.70 1 4 -18 8.10 0.90 1 -4 18 4.30 2.90 -2 4 18 65.29 4.50 -2 4 18 80.09 7.20 2 4 18 64.39 9.30 2 4 18 67.29 4.30 -2 3 18 72.09 4.70 -2 3 18 76.09 6.00 2 3 18 72.49 4.50 2 3 18 77.49 7.00 -2 2 18 1.30 0.70 -2 2 18 0.90 0.90 2 2 18 -0.40 1.00 2 2 18 0.20 0.50 -2 1 18 4.20 1.40 -2 1 18 3.60 1.20 2 1 18 4.60 1.10 2 1 18 4.90 1.70 -2 0 18 54.39 3.90 2 0 18 54.59 4.40 2 0 18 57.99 3.50 -2 -1 18 4.10 1.10 -2 -1 18 4.50 1.70 2 -1 18 4.90 1.00 2 -1 18 4.40 1.20 -2 -2 18 0.40 0.50 -2 -2 18 1.00 1.00 2 -2 18 1.40 0.60 2 -2 18 0.60 0.50 -2 -3 18 74.99 7.40 2 -3 18 65.99 3.90 2 3 -18 68.99 11.40 -2 -4 18 77.99 9.30 -2 -4 18 63.99 4.60 2 4 -18 53.29 12.60 2 4 -18 69.69 3.50 2 -4 18 64.69 3.90 2 4 -18 72.09 3.80 2 -4 18 66.59 7.40 2 4 -18 69.99 4.50 3 4 18 115.49 10.80 -3 3 18 3.00 1.40 -3 3 18 2.60 1.10 3 3 18 0.70 1.70 3 3 18 1.80 0.70 -3 2 18 88.09 5.90 -3 2 18 83.09 5.20 3 2 18 84.49 4.70 3 2 18 80.19 6.90 -3 1 18 3.60 1.20 -3 1 18 1.90 0.80 3 1 18 4.40 1.80 3 1 18 3.10 0.80 -3 0 18 195.58 10.20 -3 0 18 203.38 10.30 3 0 18 207.68 9.60 3 0 18 223.88 11.70 -3 -1 18 1.90 0.70 -3 -1 18 1.90 0.80 3 -1 18 2.80 0.80 3 -1 18 3.20 1.30 -3 -2 18 87.79 4.50 -3 -2 18 88.99 5.20 3 2 -18 79.59 10.20 3 -2 18 87.89 5.00 3 -2 18 85.29 4.60 -3 -3 18 3.90 3.00 -3 -3 18 1.90 0.80 3 3 -18 3.10 5.50 3 3 -18 3.00 0.70 3 3 -18 1.70 0.50 3 -3 18 1.90 0.70 -3 -4 18 126.49 12.80 3 -4 18 123.29 9.00 3 -4 18 111.59 9.70 3 4 -18 85.69 18.00 -4 3 18 536.65 24.10 -4 3 18 489.65 22.60 4 3 18 510.25 26.50 4 3 18 477.65 21.80 -4 2 18 51.59 3.80 -4 2 18 45.10 4.00 4 2 18 49.00 3.10 4 2 18 54.29 5.70 -4 1 18 111.19 6.50 -4 1 18 105.09 6.10 4 1 18 93.39 7.70 4 1 18 104.79 5.40 -4 0 18 5.00 1.30 -4 0 18 6.40 1.40 4 0 18 7.60 1.10 4 0 -18 4.80 2.30 4 0 -18 6.90 2.40 4 0 18 7.50 2.30 -4 -1 18 112.59 6.00 -4 -1 18 110.49 6.30 4 -1 18 114.69 7.20 4 -1 18 109.29 5.50 4 1 -18 116.29 11.10 -4 -2 18 50.19 3.50 -4 -2 18 50.69 3.60 -4 -2 18 54.59 6.80 4 -2 18 52.79 3.00 4 2 -18 51.59 2.60 4 2 -18 47.80 2.90 -4 -3 18 478.55 29.00 -4 -3 18 512.85 22.50 4 -3 18 514.25 21.50 4 3 -18 498.35 21.30 -5 2 18 146.19 8.20 5 2 18 147.69 10.50 5 -2 -18 111.29 10.10 -5 1 18 4.00 1.30 -5 1 18 3.10 1.20 5 1 18 1.90 1.40 5 1 18 2.40 0.70 5 -1 -18 2.80 3.70 5 -1 -18 1.70 3.80 -5 0 18 202.18 10.30 -5 0 18 201.78 10.30 5 0 -18 212.28 17.10 5 0 18 211.18 12.50 5 0 18 202.18 9.20 -5 -1 18 3.20 1.10 -5 -1 18 4.90 1.10 5 -1 18 2.90 1.60 5 -1 18 4.20 0.80 5 1 -18 4.30 0.80 5 1 -18 0.20 5.30 5 1 -18 2.60 0.90 -5 -2 18 132.99 12.50 5 -2 18 144.39 8.20 0 0 19 0.60 0.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 64539 _shelx_res_file ; TITL ag_sbar0354_a.res in Pnma ag_sbar0354.res created by SHELXL-2019/3 at 12:08:01 on 05-Aug-2026 REM Old TITL ag_sbar0354 in Pnma REM SHELXT solution in Pnma: R1 0.143, Rweak 0.002, Alpha 0.006 REM 2.462 for 167 systematic absences, Orientation as input REM Formula found by SHELXT: As5 In3 Ba5 CELL 0.56086 12.0735 10.3287 13.3046 90 90 90 ZERR 4 0.0003 0.0003 0.0003 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,-Z SYMM 0.5+X,0.5-Y,0.5-Z SFAC As Ba In Sb DISP As 0.2758 1.3314 4329.4752 DISP Ba -0.694 1.5004 5108.0197 DISP In -1.2843 0.8542 2974.2942 DISP Sb -1.0547 1.0104 3442.1 UNIT 22.06 20 8 1.94 EADP As5 Sb5 EXYZ As5 Sb5 L.S. 4 0 0 PLAN 7 SIZE 0.07 0.07 0.08 TEMP -173.15 CONF list 4 MORE -1 fmap 2 53 acta REM REM REM WGHT 0.004000 4.031800 EXTI 0.000510 FVAR 0.07736 0.51458 BA1 2 0.171075 0.526088 0.468094 11.00000 0.00515 0.00663 = 0.00522 -0.00055 0.00034 -0.00038 BA2 2 0.422396 0.025807 0.264438 11.00000 0.00414 0.00767 = 0.00703 0.00014 -0.00022 -0.00002 BA3 2 0.339371 0.250000 0.677159 10.50000 0.00961 0.00384 = 0.00607 0.00000 -0.00050 0.00000 IN1 3 0.080827 0.250000 0.059685 10.50000 0.00447 0.00589 = 0.00468 0.00000 0.00046 0.00000 IN2 3 0.185368 0.250000 0.299894 10.50000 0.00443 0.00450 = 0.00440 0.00000 -0.00012 0.00000 AS1 1 0.175060 0.057070 0.171780 11.00000 0.00436 0.00429 = 0.00623 -0.00060 -0.00019 0.00021 AS2 1 0.499698 0.250000 0.083888 10.50000 0.00469 0.00545 = 0.00610 0.00000 -0.00116 0.00000 AS3 1 0.146302 0.250000 0.872454 10.50000 0.00624 0.00569 = 0.00464 0.00000 0.00076 0.00000 AS4 1 0.351946 0.250000 0.432920 10.50000 0.00374 0.00853 = 0.00464 0.00000 -0.00044 0.00000 AS5 1 0.046525 0.250000 0.606747 20.50000 0.00507 0.00530 = 0.00604 0.00000 0.00035 0.00000 SB5 4 0.046525 0.250000 0.606747 -20.50000 0.00507 0.00530 = 0.00604 0.00000 0.00035 0.00000 HKLF 4 REM ag_sbar0354_a.res in Pnma REM wR2 = 0.0333, GooF = S = 1.271, Restrained GooF = 1.271 for all data REM R1 = 0.0156 for 2606 Fo > 4sig(Fo) and 0.0164 for all 2666 data REM 72 parameters refined using 0 restraints END WGHT 0.0040 4.0318 REM Highest difference peak 1.094, deepest hole -0.953, 1-sigma level 0.267 Q1 1 0.1756 0.5595 0.4185 11.00000 0.05 1.09 Q2 1 0.1857 0.4642 0.4601 11.00000 0.05 1.05 Q3 1 0.1741 0.4878 0.4061 11.00000 0.05 1.02 Q4 1 0.0262 0.4250 0.0086 11.00000 0.05 0.99 Q5 1 0.1909 0.5776 0.4395 11.00000 0.05 0.94 Q6 1 0.2381 0.2500 0.2284 10.50000 0.05 0.94 Q7 1 0.3445 0.2500 0.4798 10.50000 0.05 0.89 ; _shelx_res_checksum 90810 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ba Ba1 0.17108(2) 0.52609(2) 0.46809(2) 0.00567(4) Uani d 1 . . Ba Ba2 0.42240(2) 0.02581(2) 0.26444(2) 0.00628(4) Uani d 1 . . Ba Ba3 0.33937(2) 0.250000 0.67716(2) 0.00651(5) Uani d 1 . . In In1 0.08083(2) 0.250000 0.05968(2) 0.00501(6) Uani d 1 . . In In2 0.18537(2) 0.250000 0.29989(2) 0.00444(6) Uani d 1 . . As As1 0.17506(2) 0.05707(3) 0.17178(2) 0.00496(6) Uani d 1 . . As As2 0.49970(3) 0.250000 0.08389(3) 0.00541(8) Uani d 1 . . As As3 0.14630(3) 0.250000 0.87245(3) 0.00552(8) Uani d 1 . . As As4 0.35195(3) 0.250000 0.43292(3) 0.00564(8) Uani d 1 . . As As5 0.04652(2) 0.250000 0.60675(2) 0.00547(11) Uani d 0.515(5) . . Sb Sb5 0.04652(2) 0.250000 0.60675(2) 0.00547(11) Uani d 0.485(5) . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ba1 0.00515(7) 0.00663(9) 0.00522(7) -0.00038(5) 0.00034(5) -0.00055(6) Ba2 0.00414(7) 0.00767(9) 0.00703(8) -0.00002(5) -0.00022(5) 0.00014(6) Ba3 0.00961(10) 0.00384(11) 0.00607(10) 0.000 -0.00050(7) 0.000 In1 0.00447(11) 0.00589(14) 0.00468(11) 0.000 0.00046(8) 0.000 In2 0.00443(11) 0.00450(14) 0.00440(11) 0.000 -0.00012(8) 0.000 As1 0.00436(11) 0.00429(14) 0.00623(12) 0.00021(9) -0.00019(8) -0.00060(10) As2 0.00469(15) 0.00545(19) 0.00610(16) 0.000 -0.00116(12) 0.000 As3 0.00624(15) 0.00569(19) 0.00464(16) 0.000 0.00076(12) 0.000 As4 0.00374(15) 0.0085(2) 0.00464(16) 0.000 -0.00044(12) 0.000 As5 0.00507(15) 0.00530(18) 0.00604(15) 0.000 0.00035(10) 0.000 Sb5 0.00507(15) 0.00530(18) 0.00604(15) 0.000 0.00035(10) 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source As As 0.2758 1.3314 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ba Ba -0.6940 1.5004 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' In In -1.2843 0.8542 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -1.0547 1.0104 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Ba2 Ba1 Ba2 8_666 7_565 146.958(5) ? In1 Ba1 Ba2 2_565 8_666 85.012(6) ? In1 Ba1 Ba2 2_565 7_565 73.814(5) ? In2 Ba1 Ba2 . 7_565 56.973(5) ? In2 Ba1 Ba2 . 8_666 127.257(6) ? In2 Ba1 In1 . 2_565 127.610(7) ? In2 Ba1 As5 . 5_566 111.407(7) ? In2 Ba1 As5 . . 73.873(7) ? As1 Ba1 Ba2 8_666 7_565 97.968(6) ? As1 Ba1 Ba2 8_666 8_666 50.631(6) ? As1 Ba1 In1 8_666 2_565 42.946(7) ? As1 Ba1 In2 8_666 . 123.755(8) ? As1 Ba1 As2 8_666 2_565 84.551(9) ? As1 Ba1 As2 8_666 6_556 124.015(10) ? As1 Ba1 As3 8_666 2_564 82.980(9) ? As1 Ba1 As4 8_666 . 80.973(9) ? As1 Ba1 As5 8_666 . 83.946(8) ? As1 Ba1 As5 8_666 5_566 124.702(9) ? As2 Ba1 Ba2 2_565 7_565 145.282(7) ? As2 Ba1 Ba2 6_556 7_565 101.257(8) ? As2 Ba1 Ba2 6_556 8_666 91.492(8) ? As2 Ba1 Ba2 2_565 8_666 53.734(7) ? As2 Ba1 In1 2_565 2_565 85.622(8) ? As2 Ba1 In1 6_556 2_565 162.793(7) ? As2 Ba1 In2 2_565 . 145.903(9) ? As2 Ba1 In2 6_556 . 44.319(7) ? As2 Ba1 As2 2_565 6_556 105.855(5) ? As2 Ba1 As4 2_565 . 160.556(10) ? As2 Ba1 As4 6_556 . 72.379(8) ? As2 Ba1 As5 6_556 . 41.633(8) ? As2 Ba1 As5 2_565 5_566 42.851(8) ? As2 Ba1 As5 6_556 5_566 92.063(7) ? As2 Ba1 As5 2_565 . 92.911(7) ? As3 Ba1 Ba2 2_564 8_666 122.179(8) ? As3 Ba1 Ba2 2_564 7_565 50.910(6) ? As3 Ba1 In1 2_564 2_565 40.469(8) ? As3 Ba1 In2 2_564 . 105.650(8) ? As3 Ba1 As2 2_564 6_556 146.329(10) ? As3 Ba1 As2 2_564 2_565 95.582(8) ? As3 Ba1 As4 2_564 . 95.456(8) ? As3 Ba1 As5 2_564 5_566 86.229(8) ? As3 Ba1 As5 2_564 . 163.645(9) ? As4 Ba1 Ba2 . 8_666 106.832(8) ? As4 Ba1 Ba2 . 7_565 50.653(6) ? As4 Ba1 In1 . 2_565 92.484(7) ? As4 Ba1 In2 . . 43.365(7) ? As4 Ba1 As5 . . 72.772(7) ? As4 Ba1 As5 . 5_566 154.192(9) ? As5 Ba1 Ba2 . 7_565 121.807(7) ? As5 Ba1 Ba2 5_566 7_565 115.862(7) ? As5 Ba1 Ba2 . 8_666 53.884(5) ? As5 Ba1 Ba2 5_566 8_666 93.719(7) ? As5 Ba1 In1 . 2_565 126.828(7) ? As5 Ba1 In1 5_566 2_565 104.958(6) ? As5 Ba1 As5 5_566 . 109.363(5) ? Ba1 Ba2 Ba1 8_655 7_565 115.560(4) ? Ba1 Ba2 Ba3 8_655 5_656 111.944(6) ? Ba1 Ba2 Ba3 7_565 5_656 107.533(6) ? In1 Ba2 Ba1 6_656 7_565 92.586(6) ? In1 Ba2 Ba1 6_656 8_655 136.776(6) ? In1 Ba2 Ba3 6_656 5_656 87.358(5) ? In1 Ba2 In2 6_656 6_656 51.977(6) ? In2 Ba2 Ba1 6_656 7_565 143.086(6) ? In2 Ba2 Ba1 . 7_565 55.065(5) ? In2 Ba2 Ba1 . 8_655 84.812(6) ? In2 Ba2 Ba1 6_656 8_655 90.701(6) ? In2 Ba2 Ba3 6_656 5_656 83.521(5) ? In2 Ba2 Ba3 . 5_656 160.954(7) ? In2 Ba2 In1 . 6_656 85.974(6) ? In2 Ba2 In2 . 6_656 106.054(5) ? As1 Ba2 Ba1 6_656 8_655 121.332(7) ? As1 Ba2 Ba1 . 7_565 65.390(6) ? As1 Ba2 Ba1 . 8_655 51.815(6) ? As1 Ba2 Ba1 6_656 7_565 123.091(7) ? As1 Ba2 Ba3 6_656 5_656 49.540(7) ? As1 Ba2 Ba3 . 5_656 141.451(8) ? As1 Ba2 In1 . 6_656 129.416(8) ? As1 Ba2 In1 6_656 6_656 45.003(7) ? As1 Ba2 In2 6_656 . 129.930(9) ? As1 Ba2 In2 6_656 6_656 40.685(7) ? As1 Ba2 In2 . . 43.698(7) ? As1 Ba2 In2 . 6_656 126.017(8) ? As1 Ba2 As1 6_656 . 166.576(12) ? As1 Ba2 As2 . . 85.299(9) ? As1 Ba2 As2 6_656 . 81.886(9) ? As1 Ba2 As3 6_656 2_554 102.273(10) ? As1 Ba2 As3 . 2_554 91.149(10) ? As1 Ba2 As4 . . 87.223(9) ? As1 Ba2 As4 6_656 . 89.702(9) ? As1 Ba2 As5 . 2_554 87.291(8) ? As1 Ba2 As5 6_656 2_554 97.895(8) ? As2 Ba2 Ba1 . 8_655 53.636(7) ? As2 Ba2 Ba1 . 7_565 138.105(8) ? As2 Ba2 Ba3 . 5_656 113.867(8) ? As2 Ba2 In1 . 6_656 83.355(8) ? As2 Ba2 In2 . . 83.040(7) ? As2 Ba2 In2 . 6_656 41.838(7) ? As2 Ba2 As5 . 2_554 95.619(7) ? As3 Ba2 Ba1 2_554 7_565 54.071(7) ? As3 Ba2 Ba1 2_554 8_655 110.515(8) ? As3 Ba2 Ba3 2_554 5_656 59.749(8) ? As3 Ba2 In1 2_554 6_656 112.583(9) ? As3 Ba2 In2 2_554 6_656 142.083(9) ? As3 Ba2 In2 2_554 . 106.842(8) ? As3 Ba2 As2 2_554 . 161.361(10) ? As3 Ba2 As4 2_554 . 104.061(9) ? As3 Ba2 As5 2_554 2_554 65.901(8) ? As4 Ba2 Ba1 . 7_565 57.177(6) ? As4 Ba2 Ba1 . 8_655 125.158(8) ? As4 Ba2 Ba3 . 5_656 122.100(8) ? As4 Ba2 In1 . 6_656 44.958(8) ? As4 Ba2 In2 . . 44.300(8) ? As4 Ba2 In2 . 6_656 86.823(7) ? As4 Ba2 As2 . . 94.054(8) ? As4 Ba2 As5 . 2_554 168.449(9) ? As5 Ba2 Ba1 2_554 8_655 57.497(6) ? As5 Ba2 Ba1 2_554 7_565 111.273(7) ? As5 Ba2 Ba3 2_554 5_656 58.949(6) ? As5 Ba2 In1 2_554 6_656 142.789(8) ? As5 Ba2 In2 2_554 6_656 104.611(7) ? As5 Ba2 In2 2_554 . 130.985(8) ? Ba2 Ba3 Ba2 3_656 8_666 90.229(4) ? Ba2 Ba3 Ba2 5_656 8_666 153.734(6) ? Ba2 Ba3 Ba2 5_656 2 90.229(4) ? Ba2 Ba3 Ba2 3_656 5_656 87.431(7) ? Ba2 Ba3 Ba2 3_656 2 153.734(6) ? Ba2 Ba3 Ba2 2 8_666 80.468(6) ? As1 Ba3 Ba2 8_666 2 127.692(8) ? As1 Ba3 Ba2 8_666 8_666 47.302(6) ? As1 Ba3 Ba2 2 2 47.302(6) ? As1 Ba3 Ba2 2 5_656 49.657(6) ? As1 Ba3 Ba2 2 3_656 137.085(8) ? As1 Ba3 Ba2 8_666 5_656 137.085(8) ? As1 Ba3 Ba2 2 8_666 127.692(8) ? As1 Ba3 Ba2 8_666 3_656 49.657(6) ? As1 Ba3 As1 2 8_666 173.204(13) ? As1 Ba3 As3 2 . 88.862(7) ? As1 Ba3 As3 2 6_657 92.868(6) ? As1 Ba3 As3 8_666 6_657 92.868(6) ? As1 Ba3 As3 8_666 . 88.862(7) ? As1 Ba3 As4 8_666 . 88.858(7) ? As1 Ba3 As4 2 . 88.858(7) ? As1 Ba3 As5 8_666 . 86.631(6) ? As1 Ba3 As5 2 . 86.631(6) ? As1 Ba3 As5 8_666 6_657 93.036(7) ? As1 Ba3 As5 2 6_657 93.036(6) ? As3 Ba3 Ba2 . 3_656 109.004(7) ? As3 Ba3 Ba2 6_657 2 138.733(4) ? As3 Ba3 Ba2 . 8_666 47.586(5) ? As3 Ba3 Ba2 . 2 47.586(5) ? As3 Ba3 Ba2 6_657 3_656 49.164(4) ? As3 Ba3 Ba2 6_657 8_666 138.733(4) ? As3 Ba3 Ba2 . 5_656 109.004(7) ? As3 Ba3 Ba2 6_657 5_656 49.164(4) ? As3 Ba3 As3 . 6_657 141.995(9) ? As3 Ba3 As5 . 6_657 82.917(9) ? As3 Ba3 As5 . . 62.944(9) ? As3 Ba3 As5 6_657 6_657 59.078(8) ? As4 Ba3 Ba2 . 3_656 98.960(7) ? As4 Ba3 Ba2 . 2 107.243(7) ? As4 Ba3 Ba2 . 5_656 98.960(7) ? As4 Ba3 Ba2 . 8_666 107.243(7) ? As4 Ba3 As3 . 6_657 77.226(10) ? As4 Ba3 As3 . . 140.779(12) ? As4 Ba3 As5 . 6_657 136.304(11) ? As4 Ba3 As5 . . 77.835(10) ? As5 Ba3 Ba2 6_657 8_666 105.764(6) ? As5 Ba3 Ba2 6_657 5_656 53.116(4) ? As5 Ba3 Ba2 . 2 51.300(5) ? As5 Ba3 Ba2 . 3_656 136.284(3) ? As5 Ba3 Ba2 . 5_656 136.284(3) ? As5 Ba3 Ba2 . 8_666 51.300(5) ? As5 Ba3 Ba2 6_657 2 105.764(6) ? As5 Ba3 Ba2 6_657 3_656 53.116(4) ? As5 Ba3 As3 . 6_657 155.061(11) ? As5 Ba3 As5 . 6_657 145.861(8) ? Ba1 In1 Ba1 2_564 8_655 71.143(7) ? Ba2 In1 Ba1 6_556 2_564 157.026(8) ? Ba2 In1 Ba1 4_455 8_655 157.026(8) ? Ba2 In1 Ba1 6_556 8_655 102.305(5) ? Ba2 In1 Ba1 4_455 2_564 102.305(4) ? Ba2 In1 Ba2 4_455 6_556 74.915(8) ? As1 In1 Ba1 . 2_564 106.104(10) ? As1 In1 Ba1 . 8_655 55.266(7) ? As1 In1 Ba1 7_565 8_655 106.105(10) ? As1 In1 Ba1 7_565 2_564 55.267(7) ? As1 In1 Ba2 . 6_556 55.326(7) ? As1 In1 Ba2 . 4_455 108.468(10) ? As1 In1 Ba2 7_565 6_556 108.467(10) ? As1 In1 Ba2 7_565 4_455 55.325(7) ? As1 In1 As1 . 7_565 93.462(15) ? As1 In1 As4 . 6_556 113.333(10) ? As1 In1 As4 7_565 6_556 113.332(10) ? As3 In1 Ba1 1_554 2_564 58.665(8) ? As3 In1 Ba1 1_554 8_655 58.665(8) ? As3 In1 Ba2 1_554 6_556 137.541(7) ? As3 In1 Ba2 1_554 4_455 137.541(7) ? As3 In1 As1 1_554 7_565 113.185(10) ? As3 In1 As1 1_554 . 113.184(10) ? As3 In1 As4 1_554 6_556 109.645(15) ? As4 In1 Ba1 6_556 2_564 139.805(6) ? As4 In1 Ba1 6_556 8_655 139.805(6) ? As4 In1 Ba2 6_556 4_455 58.403(7) ? As4 In1 Ba2 6_556 6_556 58.403(7) ? Ba1 In2 Ba1 7_565 . 103.588(9) ? Ba1 In2 Ba2 . 7_565 67.962(4) ? Ba1 In2 Ba2 7_565 7_565 127.253(8) ? Ba1 In2 Ba2 . 4_455 68.977(5) ? Ba1 In2 Ba2 7_565 . 67.962(4) ? Ba1 In2 Ba2 7_565 4_455 123.100(8) ? Ba1 In2 Ba2 . . 127.252(8) ? Ba1 In2 Ba2 7_565 6_556 68.977(5) ? Ba1 In2 Ba2 . 6_556 123.101(8) ? Ba2 In2 Ba2 7_565 . 77.207(8) ? Ba2 In2 Ba2 . 4_455 160.204(8) ? Ba2 In2 Ba2 6_556 4_455 70.305(7) ? Ba2 In2 Ba2 7_565 4_455 102.853(5) ? Ba2 In2 Ba2 7_565 6_556 160.203(8) ? Ba2 In2 Ba2 . 6_556 102.853(5) ? As1 In2 Ba1 7_565 7_565 174.044(11) ? As1 In2 Ba1 . . 174.044(11) ? As1 In2 Ba1 7_565 . 78.559(7) ? As1 In2 Ba1 . 7_565 78.560(7) ? As1 In2 Ba2 7_565 . 115.318(10) ? As1 In2 Ba2 . 7_565 115.317(11) ? As1 In2 Ba2 7_565 7_565 58.696(7) ? As1 In2 Ba2 . . 58.696(7) ? As1 In2 Ba2 . 4_455 105.156(10) ? As1 In2 Ba2 7_565 6_556 105.155(10) ? As1 In2 Ba2 . 6_556 52.220(7) ? As1 In2 Ba2 7_565 4_455 52.219(7) ? As1 In2 As1 7_565 . 98.765(16) ? As1 In2 As2 7_565 6_556 109.245(10) ? As1 In2 As2 . 6_556 109.247(10) ? As1 In2 As4 . . 117.679(10) ? As1 In2 As4 7_565 . 117.680(10) ? As2 In2 Ba1 6_556 . 67.090(7) ? As2 In2 Ba1 6_556 7_565 67.090(7) ? As2 In2 Ba2 6_556 6_556 58.061(8) ? As2 In2 Ba2 6_556 . 134.983(7) ? As2 In2 Ba2 6_556 4_455 58.061(8) ? As2 In2 Ba2 6_556 7_565 134.984(7) ? As4 In2 Ba1 . 7_565 68.181(7) ? As4 In2 Ba1 . . 68.181(7) ? As4 In2 Ba2 . 4_455 137.158(7) ? As4 In2 Ba2 . 7_565 60.338(8) ? As4 In2 Ba2 . 6_556 137.158(7) ? As4 In2 Ba2 . . 60.338(8) ? As4 In2 As2 . 6_556 104.056(15) ? Ba2 As1 Ba1 . 8_655 77.553(7) ? Ba2 As1 Ba1 6_556 8_655 138.453(10) ? Ba2 As1 Ba2 6_556 . 140.372(10) ? Ba3 As1 Ba1 2_554 8_655 87.282(9) ? Ba3 As1 Ba2 2_554 . 86.710(9) ? Ba3 As1 Ba2 2_554 6_556 80.803(9) ? In1 As1 Ba1 . 8_655 81.789(9) ? In1 As1 Ba2 . 6_556 79.672(9) ? In1 As1 Ba2 . . 131.430(12) ? In1 As1 Ba3 . 2_554 135.754(12) ? In2 As1 Ba1 . 8_655 125.445(12) ? In2 As1 Ba2 . 6_556 87.095(10) ? In2 As1 Ba2 . . 77.606(9) ? In2 As1 Ba3 . 2_554 138.219(12) ? In2 As1 In1 . . 79.678(11) ? Ba1 As2 Ba1 8_655 2_564 83.884(10) ? Ba1 As2 Ba1 8_655 6_656 142.042(12) ? Ba1 As2 Ba1 2_564 6_656 74.144(6) ? Ba1 As2 Ba1 8_655 4 74.144(6) ? Ba1 As2 Ba1 6_656 4 105.164(11) ? Ba1 As2 Ba1 2_564 4 142.042(12) ? Ba1 As2 Ba2 2_564 7_565 72.630(6) ? Ba1 As2 Ba2 2_564 . 126.505(12) ? Ba1 As2 Ba2 8_655 7_565 126.505(12) ? Ba1 As2 Ba2 8_655 . 72.630(6) ? Ba2 As2 Ba1 . 6_656 145.048(12) ? Ba2 As2 Ba1 . 4 75.993(5) ? Ba2 As2 Ba1 7_565 4 145.048(12) ? Ba2 As2 Ba1 7_565 6_656 75.994(5) ? Ba2 As2 Ba2 7_565 . 83.882(11) ? In2 As2 Ba1 6_656 4 68.591(8) ? In2 As2 Ba1 6_656 6_656 68.591(7) ? In2 As2 Ba1 6_656 2_564 138.012(5) ? In2 As2 Ba1 6_656 8_655 138.012(5) ? In2 As2 Ba2 6_656 7_565 80.102(10) ? In2 As2 Ba2 6_656 . 80.101(10) ? As5 As2 Ba1 6_656 2_564 72.246(9) ? As5 As2 Ba1 6_656 4 71.737(8) ? As5 As2 Ba1 6_656 8_655 72.246(9) ? As5 As2 Ba1 6_656 6_656 71.737(8) ? As5 As2 Ba2 6_656 7_565 137.336(6) ? As5 As2 Ba2 6_656 . 137.336(6) ? As5 As2 In2 6_656 6_656 112.030(16) ? Ba1 As3 Ba1 2_565 8_656 84.509(11) ? Ba1 As3 Ba3 2_565 . 81.216(9) ? Ba1 As3 Ba3 8_656 6_557 134.108(7) ? Ba1 As3 Ba3 2_565 6_557 134.108(7) ? Ba1 As3 Ba3 8_656 . 81.216(9) ? Ba2 As3 Ba1 8_666 2_565 75.019(5) ? Ba2 As3 Ba1 8_666 8_656 154.636(12) ? Ba2 As3 Ba1 2 2_565 154.636(12) ? Ba2 As3 Ba1 2 8_656 75.020(5) ? Ba2 As3 Ba2 2 8_666 119.561(13) ? Ba2 As3 Ba3 2 . 80.997(8) ? Ba2 As3 Ba3 2 6_557 71.087(7) ? Ba2 As3 Ba3 8_666 6_557 71.087(7) ? Ba2 As3 Ba3 8_666 . 80.997(8) ? Ba3 As3 Ba3 . 6_557 121.796(11) ? In1 As3 Ba1 1_556 2_565 80.868(10) ? In1 As3 Ba1 1_556 8_656 80.868(10) ? In1 As3 Ba2 1_556 8_666 109.841(8) ? In1 As3 Ba2 1_556 2 109.841(8) ? In1 As3 Ba3 1_556 6_557 82.493(12) ? In1 As3 Ba3 1_556 . 155.711(16) ? Ba1 As4 Ba1 7_565 . 103.865(11) ? Ba2 As4 Ba1 . . 141.969(12) ? Ba2 As4 Ba1 7_565 . 72.170(5) ? Ba2 As4 Ba1 . 7_565 72.170(5) ? Ba2 As4 Ba1 7_565 7_565 141.968(12) ? Ba2 As4 Ba2 7_565 . 88.008(11) ? Ba3 As4 Ba1 . 7_565 80.956(8) ? Ba3 As4 Ba1 . . 80.956(8) ? Ba3 As4 Ba2 . . 133.132(7) ? Ba3 As4 Ba2 . 7_565 133.133(7) ? In1 As4 Ba1 6_656 7_565 126.721(6) ? In1 As4 Ba1 6_656 . 126.721(6) ? In1 As4 Ba2 6_656 7_565 76.639(9) ? In1 As4 Ba2 6_656 . 76.639(9) ? In1 As4 Ba3 6_656 . 90.636(13) ? In2 As4 Ba1 . . 68.454(7) ? In2 As4 Ba1 . 7_565 68.454(7) ? In2 As4 Ba2 . . 75.362(9) ? In2 As4 Ba2 . 7_565 75.361(9) ? In2 As4 Ba3 . . 128.673(15) ? In2 As4 In1 . 6_656 140.691(17) ? Ba1 As5 Ba1 7_565 . 100.303(9) ? Ba1 As5 Ba1 3_546 . 130.115(9) ? Ba1 As5 Ba1 5_566 . 70.637(5) ? Ba1 As5 Ba1 3_546 7_565 70.637(5) ? Ba1 As5 Ba1 5_566 7_565 130.115(9) ? Ba1 As5 Ba1 3_546 5_566 78.921(8) ? Ba1 As5 Ba3 7_565 6_557 129.824(5) ? Ba1 As5 Ba3 5_566 . 140.170(4) ? Ba1 As5 Ba3 5_566 6_557 74.490(6) ? Ba1 As5 Ba3 . 6_557 129.824(5) ? Ba1 As5 Ba3 3_546 6_557 74.490(6) ? Ba1 As5 Ba3 3_546 . 140.170(4) ? Ba2 As5 Ba1 8_666 7_565 149.872(10) ? Ba2 As5 Ba1 2 3_546 74.253(5) ? Ba2 As5 Ba1 2 5_566 138.279(9) ? Ba2 As5 Ba1 2 7_565 68.619(5) ? Ba2 As5 Ba1 8_666 5_566 74.253(5) ? Ba2 As5 Ba1 8_666 3_546 138.279(9) ? Ba2 As5 Ba1 8_666 . 68.619(5) ? Ba2 As5 Ba1 2 . 149.872(10) ? Ba2 As5 Ba2 8_666 2 106.397(10) ? Ba2 As5 Ba3 8_666 . 75.346(6) ? Ba2 As5 Ba3 8_666 6_557 67.934(6) ? Ba2 As5 Ba3 2 6_557 67.934(6) ? Ba2 As5 Ba3 2 . 75.346(6) ? Ba3 As5 Ba1 . 7_565 74.684(6) ? Ba3 As5 Ba1 . . 74.684(6) ? Ba3 As5 Ba3 . 6_557 116.181(9) ? As2 As5 Ba1 6_556 . 66.630(7) ? As2 As5 Ba1 6_556 3_546 64.903(8) ? As2 As5 Ba1 6_556 7_565 66.630(7) ? As2 As5 Ba1 6_556 5_566 64.903(8) ? As2 As5 Ba2 6_556 8_666 126.763(5) ? As2 As5 Ba2 6_556 2 126.763(5) ? As2 As5 Ba3 6_556 . 117.407(13) ? As2 As5 Ba3 6_556 6_557 126.411(13) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Ba1 Ba2 7_565 4.1032(2) ? Ba1 Ba2 8_666 4.1010(2) ? Ba1 In1 2_565 3.9757(3) ? Ba1 In2 . 3.6290(3) ? Ba1 As1 8_666 3.3012(3) ? Ba1 As2 2_565 3.4602(3) ? Ba1 As2 6_556 3.5905(3) ? Ba1 As3 2_564 3.4394(3) ? Ba1 As4 . 3.6221(3) ? Ba1 As5 5_566 3.6390(3) ? Ba1 As5 . 3.7143(3) ? Ba2 Ba3 5_656 4.1222(3) ? Ba2 In1 6_656 3.8074(3) ? Ba2 In2 . 3.7114(3) ? Ba2 In2 6_656 4.0219(3) ? Ba2 As1 . 3.2468(3) ? Ba2 As1 6_656 3.1827(3) ? Ba2 As2 . 3.4646(3) ? Ba2 As3 2_554 3.2967(3) ? Ba2 As4 . 3.3332(3) ? Ba2 As5 2_554 3.5577(3) ? Ba3 As1 8_666 3.1772(3) ? Ba3 As1 2 3.1772(3) ? Ba3 As3 6_657 3.7640(5) ? Ba3 As3 . 3.4907(5) ? Ba3 As4 . 3.2531(5) ? Ba3 As5 . 3.6577(4) ? Ba3 As5 6_657 3.8106(4) ? In1 As1 . 2.7367(4) ? In1 As1 7_565 2.7367(4) ? In1 As3 1_554 2.6135(5) ? In1 As4 6_556 2.7652(5) ? In2 As1 7_565 2.6252(4) ? In2 As1 . 2.6252(4) ? In2 As2 6_556 2.7233(5) ? In2 As4 . 2.6790(5) ? As2 As5 6_656 2.5986(5) ? _cod_database_fobs_code 2023559