#------------------------------------------------------------------------------
#$Date: 2026-09-22 22:15:14 +0100 (Tue, 22 Sep 2026) $
#$Revision: 306895 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/35/2023570.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023570
loop_
_publ_author_name
'Thiam, Mariama'
'Diouf, Ngon\'e'
'Orton, James'
'Ndoye, Cheikh'
'Gueye, Amadou'
'Diouf, Ousmane'
'Thiam, Ibrahima Elhadji'
'Gaye, Mohamed'
'Coles, Simon'
_publ_section_title
;
Structures of bimetallic FeIII--FeIII and trimetallic FeIII--K--FeIII
complexes incorporating the deprotonated ligand
N,N′-bis(2-hydroxy-3-methoxybenzylidene)-1,2-phenylenediamine
;
_journal_issue 10
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989026009734
_journal_volume 82
_journal_year 2026
_chemical_formula_iupac '[Fe2 (C22 H18 N2 O4)2 O], 5H2 O'
_chemical_formula_moiety 'C44 H36 Fe2 N4 O9, 5(H2 O)'
_chemical_formula_sum 'C44 H46 Fe2 N4 O14'
_chemical_formula_weight 966.55
_chemical_name_systematic
'\m-Oxido-bis[(2-{[2-(3-methoxy-2-oxidobenzylideneamino)phenylimino]methyl}-6-methoxyphenolato)iron(III)] pentahydrate,'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary dual
_audit_creation_method
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_cell_angle_alpha 90
_cell_angle_beta 113.199(4)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 13.6001(4)
_cell_length_b 22.9342(5)
_cell_length_c 14.8502(5)
_cell_measurement_reflns_used 11083
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 37.8660
_cell_measurement_theta_min 1.7290
_cell_volume 4257.4(2)
_computing_cell_refinement
;
CrysAlisPro 1.171.43.121a (Rigaku OD, 2024)
;
_computing_data_collection
'CrysAlisPro system (CCD 43.124a 64-bit (release 23-05-2024))'
_computing_data_reduction
;
CrysAlisPro 1.171.43.121a (Rigaku OD, 2024)
;
_computing_molecular_graphics
;
Olex2 1.3 (Dolomanov et al., 2009)
;
_computing_publication_material
;
Olex2 1.3 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL2018/3 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2018/2 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 100(2)
_diffrn_detector_area_resol_mean 10
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'Rigaku FRE+ '
_diffrn_measurement_method 'profile data from \w-scans'
_diffrn_measurement_specimen_support 'MiTeGen MicroLoop'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71075
_diffrn_reflns_av_R_equivalents 0.0494
_diffrn_reflns_av_unetI/netI 0.0470
_diffrn_reflns_limit_h_max 22
_diffrn_reflns_limit_h_min -22
_diffrn_reflns_limit_k_max 38
_diffrn_reflns_limit_k_min -38
_diffrn_reflns_limit_l_max 24
_diffrn_reflns_limit_l_min -24
_diffrn_reflns_number 99080
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 36.319
_diffrn_reflns_theta_min 1.629
_exptl_absorpt_coefficient_mu 0.756
_exptl_absorpt_correction_T_max 0.985
_exptl_absorpt_correction_T_min 0.915
_exptl_absorpt_correction_type analytical
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2024)
;
_exptl_crystal_colour dark-red
_exptl_crystal_density_diffrn 1.508
_exptl_crystal_description '(cut) lath'
_exptl_crystal_F_000 2008
_exptl_crystal_size_max 0.14
_exptl_crystal_size_mid 0.13
_exptl_crystal_size_min 0.02
_refine_diff_density_max 0.701
_refine_diff_density_min -0.656
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.038
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 596
_refine_ls_number_reflns 20596
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.038
_refine_ls_R_factor_all 0.0678
_refine_ls_R_factor_gt 0.0444
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0651P)^2^+0.4018P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1101
_refine_ls_wR_factor_ref 0.1188
_reflns_number_gt 15233
_reflns_number_total 20596
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file hb8251.cif
_cod_data_source_block 2
_cod_database_code 2023570
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.902
_shelx_estimated_absorpt_t_max 0.985
_shelx_hkl_file
;
0 0 1 -0.18 0.16
0 0 2 152.76 6.24
0 0 2 151.35 6.23
0 0 3 0.11 0.34
0 0 -3 0.35 0.36
0 0 -3 0.09 0.38
0 0 -3 0.30 0.34
0 0 3 -0.03 0.47
0 0 -3 0.16 0.52
0 0 3 0.17 0.55
0 0 4 37.62 1.93
0 0 -4 37.34 1.79
0 0 4 38.43 1.88
0 0 -4 42.86 1.81
0 0 -4 40.28 1.84
0 0 4 39.56 1.89
0 0 -4 41.30 1.97
0 0 4 40.14 1.95
0 0 5 -0.21 0.61
0 0 -5 0.18 0.42
0 0 -5 0.35 1.53
0 0 5 -0.68 1.31
0 0 -5 0.47 0.45
0 0 -5 -0.04 0.49
0 0 -5 -0.33 0.67
0 0 5 0.09 0.67
0 0 5 -0.17 0.59
0 0 5 0.13 0.55
0 0 6 8.91 0.89
0 0 6 9.12 0.92
0 0 -6 10.49 0.95
0 0 -6 10.14 0.77
0 0 -6 10.43 0.83
0 0 6 10.43 0.91
0 0 -6 9.61 0.99
0 0 6 10.78 1.01
0 0 -7 0.08 0.49
0 0 -7 0.17 1.75
0 0 -7 0.15 0.57
0 0 7 -0.22 0.67
0 0 -7 -0.65 0.80
0 0 7 0.36 0.64
0 0 -8 634.18 26.11
0 0 -8 647.21 26.03
0 0 8 633.70 26.32
0 0 -8 663.97 26.41
0 0 8 634.36 26.19
0 0 -9 0.36 0.58
0 0 -9 0.06 0.66
0 0 9 -0.49 0.82
0 0 -9 0.22 0.91
0 0 9 -0.46 0.72
0 0 -10 1419.72 56.85
0 0 -10 1409.28 58.25
0 0 10 1384.63 57.22
0 0 -10 1444.40 57.36
0 0 10 1394.41 57.05
0 0 -11 0.44 0.72
0 0 -11 0.41 1.18
0 0 11 -0.46 0.81
0 0 11 0.12 1.05
0 0 -12 38.60 2.78
0 0 12 35.67 2.25
0 0 12 37.40 2.54
0 0 -13 1.54 1.43
0 0 13 -0.11 0.94
0 0 13 0.59 1.19
0 0 -14 11.11 1.83
0 0 14 8.53 1.32
0 0 14 9.04 1.65
0 0 -15 0.21 1.63
0 0 15 -0.86 1.11
0 0 15 1.23 1.42
0 0 16 15.68 2.00
0 0 -16 11.90 2.16
0 0 17 -2.23 1.80
0 0 -17 3.64 2.00
0 0 18 16.19 2.23
0 0 -18 18.25 2.71
0 0 -19 3.06 2.26
0 0 19 1.03 1.88
0 0 -20 7.67 2.51
0 0 20 4.89 2.09
0 0 -21 0.62 2.27
0 0 21 1.14 2.16
0 0 -22 7.10 2.71
0 0 22 1.48 2.13
0 -1 1 3032.71 120.54
0 1 1 2983.00 120.53
0 -1 1 3024.22 120.56
0 1 2 28.52 1.13
0 -1 2 30.08 1.19
0 1 -2 27.62 1.14
0 -1 2 26.31 1.17
0 1 2 27.98 1.12
0 1 2 28.12 1.17
0 -1 3 520.11 20.17
0 1 3 502.84 20.13
0 1 3 474.24 20.03
0 1 3 488.04 20.06
0 -1 -3 497.12 20.03
0 1 -3 492.68 20.12
0 1 3 501.80 20.02
0 -1 3 507.17 20.13
0 1 3 511.35 20.09
0 1 3 503.50 20.14
0 1 -3 499.99 20.15
0 -1 -4 64.87 2.84
0 1 4 65.85 2.86
0 -1 4 62.90 2.89
0 1 -4 61.48 2.76
0 1 4 61.35 2.70
0 1 4 61.77 2.76
0 -1 -4 63.36 2.71
0 1 -4 64.30 2.83
0 -1 4 62.07 2.82
0 1 -4 61.86 2.75
0 -1 -4 66.01 2.71
0 1 4 64.19 2.80
0 1 -4 63.86 2.90
0 1 4 62.62 2.86
0 -1 5 56.92 2.77
0 -1 -5 57.94 2.71
0 1 5 60.57 2.75
0 1 -5 56.80 2.63
0 1 5 58.04 2.64
0 1 -5 59.60 2.61
0 -1 -5 59.19 2.59
0 1 -5 56.24 2.68
0 -1 -5 58.96 2.57
0 1 5 61.44 2.69
0 1 -5 57.15 2.79
0 1 5 57.91 2.74
0 -1 6 4.11 0.75
0 -1 -6 4.29 0.71
0 1 6 2.48 0.71
0 1 -6 2.86 0.58
0 1 6 2.34 0.59
0 -1 6 3.25 0.74
0 -1 -6 3.06 0.51
0 1 -6 3.10 0.67
0 -1 -6 3.32 0.57
0 1 -6 2.98 0.58
0 1 6 2.83 0.64
0 -1 6 4.70 0.73
0 1 -6 3.60 0.83
0 1 6 3.44 0.80
0 1 7 35.91 2.12
0 -1 7 37.44 2.14
0 1 -7 38.85 1.92
0 1 7 37.79 2.00
0 -1 7 38.72 2.10
0 -1 -7 42.87 3.00
0 1 7 41.13 2.70
0 -1 -7 37.49 1.92
0 -1 -7 42.33 1.90
0 1 -7 37.42 2.02
0 1 -7 40.08 1.92
0 1 7 38.27 2.02
0 -1 -7 37.98 2.20
0 1 -7 43.17 2.25
0 1 -8 56.50 2.61
0 1 8 52.59 2.67
0 -1 8 53.64 2.80
0 1 -8 56.85 2.62
0 1 -8 56.38 2.74
0 -1 -8 58.53 2.58
0 -1 -8 55.26 2.62
0 -1 -8 59.71 3.78
0 1 -8 56.39 2.96
0 -1 -8 50.83 2.90
0 -1 8 54.14 2.88
0 1 8 53.98 2.84
0 1 -9 167.62 7.16
0 -1 -9 168.45 7.07
0 -1 -9 167.87 7.00
0 1 -9 170.08 8.41
0 1 -9 172.52 7.06
0 -1 -9 152.89 7.41
0 1 -9 163.59 7.45
0 -1 9 166.73 7.39
0 1 9 158.52 7.32
0 1 9 164.63 7.17
0 -1 9 162.94 7.26
0 1 -10 28.83 1.63
0 -1 -10 27.09 1.57
0 -1 -10 24.84 2.09
0 1 -10 31.28 2.15
0 1 10 27.42 1.92
0 -1 10 27.67 1.99
0 -1 10 26.08 1.83
0 1 10 26.38 1.71
0 1 -11 56.99 4.45
0 -1 -11 58.02 2.78
0 -1 11 55.16 3.22
0 1 11 57.87 3.24
0 -1 11 55.28 3.07
0 1 11 60.80 2.99
0 1 -11 55.63 3.35
0 -1 -11 56.79 3.42
0 1 12 106.98 5.27
0 -1 12 101.21 5.28
0 1 12 110.51 4.98
0 -1 12 110.60 5.11
0 -1 -12 99.28 5.41
0 1 -12 104.96 5.46
0 -1 13 25.11 2.13
0 1 13 24.08 2.06
0 -1 13 24.01 1.86
0 1 13 22.84 1.74
0 1 -13 19.77 2.20
0 -1 -13 23.26 2.26
0 1 14 50.92 3.34
0 -1 14 58.46 3.48
0 -1 14 57.02 3.16
0 1 14 55.89 3.02
0 1 -14 49.65 3.55
0 -1 -14 54.32 3.67
0 -1 15 35.33 2.81
0 1 15 35.51 2.73
0 -1 15 39.03 2.54
0 1 -15 39.26 3.10
0 -1 -15 33.36 2.99
0 -1 16 14.22 1.97
0 1 16 13.89 1.92
0 -1 16 15.93 1.73
0 -1 -16 12.59 2.33
0 1 -16 12.78 2.20
0 -1 -17 34.51 3.32
0 1 -17 34.22 3.23
0 -1 17 38.79 3.08
0 1 17 39.71 2.99
0 1 17 34.41 3.02
0 1 -18 0.26 2.06
0 -1 -18 0.52 2.03
0 1 18 -1.90 1.80
0 -1 18 0.44 1.62
0 -1 18 0.97 1.82
0 1 18 0.96 1.80
0 -1 -19 0.56 2.28
0 1 -19 -0.56 2.18
0 -1 19 0.51 2.07
0 1 19 0.77 1.97
0 1 -20 18.55 2.97
0 -1 -20 14.15 2.79
0 -1 20 13.10 2.58
0 1 20 11.07 2.44
0 1 -21 1.55 2.27
0 -1 -21 4.95 2.60
0 1 21 4.82 2.34
0 1 -22 -1.29 2.57
0 1 22 1.18 2.37
0 2 0 549.57 22.07
0 -2 1 268.20 11.12
0 2 1 272.06 11.03
0 2 1 278.56 11.04
0 2 2 1.22 0.32
0 -2 2 0.37 0.45
0 2 2 0.99 0.33
0 2 -2 1.33 0.37
0 -2 2 1.27 0.44
0 -2 2 1.35 0.52
0 2 2 1.81 0.33
0 2 -2 1.23 0.36
0 2 2 1.15 0.42
0 -2 3 970.28 39.01
0 2 -3 970.10 39.00
0 2 3 961.78 38.95
0 2 3 967.24 38.86
0 2 3 974.82 38.86
0 -2 3 945.27 39.01
0 2 3 968.27 38.91
0 2 3 984.75 38.98
0 2 -3 968.79 38.99
0 2 4 1.91 0.51
0 2 -4 1.38 0.58
0 -2 4 2.05 0.64
0 2 -4 2.37 0.54
0 2 4 1.46 0.39
0 -2 4 1.77 0.60
0 -2 -4 2.28 0.32
0 2 -4 1.44 0.62
0 2 4 2.18 0.34
0 2 4 1.59 0.51
0 2 -4 1.48 0.63
0 2 4 1.53 0.61
0 2 -5 65.05 2.99
0 2 5 63.38 2.92
0 2 -5 63.68 2.70
0 2 5 59.77 2.71
0 2 -5 59.33 2.83
0 2 5 65.06 2.77
0 2 -5 64.56 2.82
0 -2 -5 63.74 2.71
0 -2 -5 62.06 2.72
0 2 -5 61.93 2.92
0 2 5 65.32 2.70
0 -2 5 64.29 2.99
0 2 5 62.89 2.91
0 2 5 61.93 2.84
0 2 -6 0.48 0.71
0 -2 6 0.74 0.71
0 2 6 1.22 0.65
0 2 -6 1.08 0.56
0 2 6 0.75 0.42
0 2 -6 1.29 0.37
0 2 6 0.91 0.47
0 -2 6 0.27 0.69
0 -2 -6 0.98 0.43
0 -2 -6 1.06 0.45
0 2 -6 0.62 0.63
0 2 -6 0.17 0.52
0 2 6 1.22 0.58
0 2 7 157.89 6.66
0 -2 7 152.45 6.72
0 2 7 154.07 6.28
0 2 -7 149.64 6.50
0 2 7 149.09 6.47
0 -2 7 149.27 6.69
0 2 -7 157.30 6.49
0 -2 -7 152.25 6.41
0 2 -7 150.02 6.59
0 -2 -7 156.60 6.40
0 2 7 152.37 6.53
0 2 -7 152.75 6.74
0 2 8 83.61 3.53
0 2 -8 85.83 3.80
0 -2 8 86.95 4.03
0 2 8 82.32 3.79
0 -2 -8 82.13 3.72
0 -2 -8 84.89 3.70
0 2 -8 86.44 3.92
0 2 -8 85.35 5.03
0 2 -8 86.68 3.79
0 2 -8 81.54 4.09
0 2 8 85.18 4.00
0 -2 8 86.65 4.08
0 -2 -9 57.78 2.69
0 2 -9 55.91 2.73
0 2 -9 57.41 2.74
0 2 -9 59.23 4.18
0 2 -9 56.54 3.11
0 -2 9 53.72 2.97
0 2 9 55.08 2.76
0 2 9 60.04 3.02
0 -2 9 59.21 3.08
0 2 -10 50.75 3.03
0 -2 10 47.36 2.80
0 2 10 53.00 2.61
0 2 10 49.37 2.86
0 -2 10 55.13 2.95
0 2 -11 162.81 7.53
0 -2 11 166.85 7.32
0 2 11 157.85 7.04
0 2 11 165.23 7.36
0 -2 11 156.61 7.40
0 2 -12 1.69 1.32
0 -2 12 0.42 1.15
0 2 12 0.65 1.20
0 -2 12 1.30 1.03
0 2 12 1.26 0.86
0 2 -13 23.41 3.66
0 2 13 19.73 1.85
0 -2 13 15.86 1.81
0 2 13 18.77 1.48
0 -2 13 17.21 1.67
0 2 -13 19.45 2.15
0 2 14 -0.62 1.37
0 -2 14 0.50 1.30
0 -2 14 0.93 1.10
0 2 -14 -0.19 1.52
0 -2 15 1.45 1.39
0 2 15 0.17 1.34
0 -2 15 0.84 1.12
0 2 -15 1.65 1.58
0 2 16 0.73 1.40
0 -2 16 1.37 1.52
0 -2 16 -0.15 1.25
0 2 -16 1.34 1.81
0 -2 17 6.62 1.45
0 2 -17 5.81 2.05
0 2 17 4.67 1.60
0 -2 17 4.41 1.74
0 2 17 5.57 1.88
0 2 -18 0.52 1.95
0 2 18 0.21 1.68
0 -2 18 -1.34 1.72
0 2 18 0.96 1.85
0 2 -19 2.22 2.13
0 2 19 -0.25 1.83
0 2 -20 -0.59 2.43
0 2 20 -0.27 2.01
0 2 -21 -0.62 2.31
0 2 21 -2.82 2.33
0 2 -22 14.80 3.10
0 2 22 13.18 2.75
0 3 0 0.18 0.35
0 3 0 -0.10 0.48
0 3 1 15.13 0.44
0 3 1 15.75 0.46
0 3 -1 15.14 0.42
0 -3 1 14.50 0.73
0 3 2 3.03 0.38
0 -3 -2 3.60 0.35
0 3 -2 3.63 0.47
0 3 2 3.34 0.46
0 -3 2 2.09 0.63
0 3 2 3.10 0.43
0 -3 -2 3.18 0.44
0 3 2 3.37 0.36
0 3 -2 3.21 0.48
0 -3 -3 266.56 10.83
0 3 3 266.13 10.83
0 -3 3 269.21 10.99
0 3 3 266.36 10.84
0 -3 3 269.12 11.01
0 3 3 264.72 10.86
0 3 -3 278.89 10.95
0 3 3 267.11 10.86
0 3 3 261.90 10.90
0 3 -3 264.09 10.92
0 3 4 3.71 0.67
0 3 -4 3.30 0.67
0 3 -4 4.19 0.67
0 3 4 4.01 0.55
0 -3 4 2.78 0.68
0 -3 4 4.36 0.73
0 3 -4 4.08 0.73
0 3 4 3.46 0.40
0 3 4 3.87 0.55
0 3 4 3.43 0.52
0 -3 5 19.68 1.33
0 3 5 21.83 1.24
0 3 -5 21.39 1.30
0 3 -5 19.29 1.22
0 3 5 20.96 1.05
0 3 -5 20.71 1.34
0 -3 5 20.48 1.34
0 -3 -5 21.22 0.99
0 3 5 20.03 1.01
0 3 5 21.06 1.18
0 3 5 19.55 1.27
0 -3 5 19.36 1.27
0 3 -5 20.81 1.35
0 -3 6 25.83 1.54
0 3 -6 25.54 1.60
0 3 -6 24.25 1.31
0 3 -6 24.96 1.46
0 3 6 25.41 1.28
0 3 6 26.27 1.30
0 -3 6 27.13 1.59
0 3 -6 26.90 1.43
0 3 6 26.51 1.24
0 -3 -6 25.59 1.24
0 3 -6 24.22 1.54
0 3 6 27.13 1.43
0 -3 6 28.22 1.66
0 3 6 22.86 1.48
0 3 -7 358.02 14.22
0 3 -7 339.67 13.78
0 3 7 329.94 13.85
0 3 -7 336.61 13.99
0 3 7 341.75 13.88
0 3 -7 344.51 13.97
0 3 -7 328.76 14.09
0 -3 -7 334.43 13.82
0 3 7 348.22 13.98
0 -3 7 336.35 14.20
0 3 7 353.00 14.11
0 3 8 6.13 0.56
0 3 -8 7.01 0.78
0 3 -8 5.94 0.47
0 3 8 5.63 0.68
0 -3 8 6.03 1.00
0 3 -8 5.65 0.78
0 -3 -8 6.59 0.64
0 3 -8 5.89 0.87
0 3 -8 5.36 1.02
0 -3 8 6.99 1.00
0 3 8 5.40 0.93
0 3 9 188.71 7.61
0 -3 -9 178.60 7.74
0 3 -9 197.45 9.44
0 3 9 184.24 7.84
0 3 -9 185.84 8.26
0 -3 9 184.72 8.21
0 3 9 187.90 8.12
0 3 -10 57.10 4.59
0 -3 10 61.90 3.39
0 3 10 66.80 3.06
0 3 10 63.79 3.36
0 -3 10 65.95 3.46
0 3 -10 60.80 3.47
0 -3 11 391.30 16.67
0 3 11 416.84 16.31
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10 3 -11 178.17 7.54
10 3 -11 157.74 8.34
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-10 3 11 148.85 7.42
-10 3 10 49.13 2.44
-10 3 10 42.27 2.96
-10 -3 10 43.87 2.69
10 3 -10 51.55 2.95
-10 3 10 43.07 3.16
-10 -3 10 45.24 3.16
10 -3 -10 44.52 3.20
10 3 -10 46.95 3.62
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10 3 -10 53.27 3.83
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-10 3 9 1.01 1.24
-10 -3 9 2.54 1.03
10 3 -9 3.80 1.18
-10 3 9 3.48 1.40
-10 -3 9 2.85 1.42
10 3 -9 3.72 1.87
10 3 -9 3.58 1.82
-10 -3 8 2.01 0.99
-10 3 8 0.60 1.27
-10 3 8 1.42 0.42
10 3 -8 2.75 1.13
10 3 -8 0.20 1.76
-10 -3 7 27.93 1.92
-10 3 7 22.26 2.20
10 3 -7 27.66 2.03
-10 -3 6 1.98 1.27
-10 3 6 2.58 0.88
-10 3 6 4.29 1.40
-10 -3 6 2.00 0.95
10 3 -6 0.78 1.66
-10 -3 5 91.40 5.07
-10 3 5 102.03 4.72
10 -3 -5 105.73 5.04
-10 3 5 109.24 5.34
-10 -3 5 94.75 4.75
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-10 3 4 -0.19 0.83
-10 -3 4 -0.14 1.13
10 -3 -4 -0.13 1.12
10 3 -4 0.38 1.61
10 -3 -3 17.78 1.07
10 3 -3 19.17 1.41
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-10 3 3 18.61 1.53
-10 -3 3 17.36 1.66
-10 -3 3 22.30 1.91
10 -3 -3 16.16 1.66
10 3 -3 14.79 2.05
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10 -3 -2 1.41 1.07
10 -3 -2 0.89 0.58
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-10 -3 1 -0.37 1.04
10 -3 -1 0.46 1.04
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-10 -3 0 0.26 1.05
10 -3 0 -0.34 1.10
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-10 -3 0 0.79 0.73
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-10 -3 -1 2.07 1.11
-10 -3 -1 0.55 0.96
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-10 -3 -2 9.48 1.26
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-10 -3 -4 0.80 0.86
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10 -3 5 0.44 1.18
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-10 -3 -5 0.89 0.82
10 -3 5 1.08 1.05
-10 3 -5 1.78 1.44
10 -3 6 10.25 1.67
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-10 -3 -6 9.64 1.07
10 -3 6 9.74 1.38
-10 -3 -6 11.49 1.83
-10 3 -6 12.72 1.97
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10 -3 7 10.67 2.02
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-10 3 -7 6.48 1.87
-10 -3 -7 7.62 0.94
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-10 -3 -7 8.25 1.79
-10 3 -7 7.27 1.98
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10 -3 8 5.47 1.64
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-10 -3 -8 8.72 1.99
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-10 -3 -9 16.49 2.33
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10 3 9 13.62 2.21
-10 -3 -10 2.03 1.93
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10 3 10 4.16 1.94
-10 3 -11 22.69 2.83
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10 -3 11 21.89 2.60
10 3 11 24.03 2.67
-10 3 -12 21.96 3.14
10 3 12 18.11 2.67
10 -3 12 22.07 2.78
-10 3 -13 25.03 3.15
10 3 13 19.06 2.99
10 -3 13 14.97 2.60
-10 3 -14 -1.44 2.43
10 3 14 2.39 2.09
10 -3 14 -1.25 2.12
-10 3 -15 -2.70 2.62
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10 -3 15 -1.04 2.17
-10 3 -16 1.25 2.65
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-10 -4 24 8.23 2.76
-10 4 23 25.01 3.04
-10 -4 23 20.55 3.08
-10 -4 22 -1.82 2.46
-10 4 22 -1.13 2.25
-10 4 21 52.22 4.09
-10 -4 21 45.04 4.02
10 4 -20 51.57 3.22
-10 4 20 50.64 4.03
-10 -4 20 49.09 4.17
-10 -4 19 0.87 1.43
10 4 -19 1.12 1.28
-10 4 19 0.58 1.76
-10 -4 19 0.27 2.05
-10 4 19 -1.02 2.05
-10 4 18 57.06 3.79
-10 -4 18 58.94 3.66
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-10 4 18 57.72 4.09
-10 -4 18 56.13 4.16
-10 -4 17 2.48 1.82
-10 -4 17 2.31 1.77
-10 4 17 4.61 1.68
-10 -4 17 3.77 1.64
10 4 -17 4.18 1.39
10 4 -16 40.17 2.73
-10 4 16 34.48 2.97
-10 -4 16 39.76 3.19
-10 4 15 87.64 5.20
-10 -4 15 100.25 5.38
10 -4 -15 95.98 6.19
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-10 4 14 3.38 1.59
-10 -4 14 2.72 1.70
10 -4 -14 -0.59 2.72
10 4 -14 -0.14 1.23
10 -4 -14 0.18 0.50
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-10 -4 13 171.71 8.91
-10 4 13 188.98 8.96
10 4 -13 204.34 8.73
-10 4 13 192.99 8.08
10 -4 -13 188.31 7.95
-10 -4 12 17.74 2.15
-10 4 12 19.84 2.13
10 4 -12 21.37 1.90
-10 4 12 20.96 1.36
10 -4 -12 17.81 1.28
-10 4 12 20.42 1.96
-10 4 11 34.84 2.86
-10 -4 11 37.52 2.83
10 4 -11 35.90 2.56
10 4 -11 33.40 3.35
10 -4 -11 39.51 3.53
-10 4 11 39.03 2.00
-10 4 11 35.37 2.61
-10 4 10 258.71 11.75
-10 4 10 274.92 11.11
10 4 -10 271.84 11.71
-10 -4 10 263.50 11.94
-10 4 10 262.06 12.01
-10 4 10 260.73 10.95
10 4 -10 276.34 12.51
10 -4 -10 278.64 12.54
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-10 -4 9 18.90 1.66
10 4 -9 18.95 1.80
-10 4 9 16.50 1.96
-10 -4 9 16.53 1.97
10 4 -9 19.61 2.60
-10 4 9 17.79 0.98
10 4 -9 15.43 2.52
10 -4 -9 21.29 2.63
-10 4 8 45.20 3.09
-10 -4 8 47.68 2.70
10 4 -8 51.90 3.70
10 4 -8 45.24 3.49
10 -4 -8 42.21 3.44
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-10 4 7 0.16 0.81
-10 -4 7 0.53 0.90
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-10 -4 6 40.20 2.71
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-10 -4 5 8.22 1.50
10 -4 -5 9.81 1.48
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10 -4 -4 147.79 7.13
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10 -4 -4 155.91 7.62
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10 -4 -2 3.09 1.16
10 -4 -2 5.07 0.66
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10 -4 -1 3.66 1.15
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-10 4 -1 8.43 1.42
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-10 -4 -2 39.34 2.55
-10 -4 -2 32.47 2.14
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-10 -4 -3 73.30 3.70
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10 -4 3 82.89 4.51
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-10 -4 -5 13.57 1.28
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-10 4 -5 16.87 2.03
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-10 -4 -6 25.79 2.39
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-10 -4 -7 0.80 0.65
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10 -4 8 18.96 1.87
-10 -4 -8 19.34 2.37
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-10 -4 -9 19.28 2.82
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-10 -4 -9 23.76 2.77
-10 -4 -10 8.74 2.23
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-10 -4 -11 -0.75 2.30
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-10 -4 -14 -2.65 2.62
-10 4 -14 -0.29 2.37
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-10 -5 23 -0.94 2.22
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-10 -5 22 81.41 5.43
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-10 5 19 4.39 1.71
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10 -5 -16 7.08 2.65
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10 -5 -15 8.92 2.79
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10 5 -14 164.12 8.45
10 -5 -14 162.26 8.43
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-10 -5 13 24.19 2.44
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10 -5 -13 22.49 1.31
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10 -5 -12 107.31 4.65
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-10 -5 11 21.39 2.20
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10 5 -11 17.29 1.71
10 -5 -11 16.80 1.26
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10 5 -10 5.58 1.41
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10 -5 -9 5.70 0.98
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10 -5 -9 7.84 2.12
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10 -5 -8 15.02 1.36
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10 -5 -8 11.93 2.29
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10 -5 -7 8.07 1.50
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10 -5 -5 0.57 1.67
10 5 -5 -1.34 1.73
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-10 -5 4 105.68 5.39
10 -5 -4 107.68 5.42
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10 -5 -4 104.44 5.81
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10 -5 -3 6.95 0.55
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10 -5 -3 11.00 1.98
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-10 -5 2 50.97 3.07
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10 -5 -2 52.17 2.38
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10 -5 -1 1.21 1.28
-10 -5 1 1.08 1.14
-10 -5 1 0.23 1.01
-10 -5 1 0.98 0.74
10 5 -1 0.10 0.93
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-10 -5 0 28.17 2.24
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-10 -5 -1 9.12 1.48
-10 -5 -1 10.53 1.26
10 -5 1 9.47 1.50
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-10 -5 -2 43.30 2.80
-10 -5 -2 40.29 2.40
10 -5 2 40.57 2.65
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-10 -5 -3 4.61 0.98
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10 -5 3 3.75 1.23
-10 5 -3 4.13 1.44
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10 -5 4 43.23 3.27
-10 5 -4 47.98 3.36
-10 -5 -4 50.26 2.49
10 -5 4 45.35 2.85
-10 -5 -4 42.21 3.06
-10 5 -4 44.44 3.12
10 -5 5 2.81 1.19
10 -5 5 1.68 1.60
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-10 5 -5 1.66 1.52
-10 -5 -5 2.26 0.81
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10 -5 6 7.85 1.85
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-10 -5 -6 10.61 0.95
10 -5 6 13.10 1.57
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10 -5 7 1.69 1.27
-10 5 -7 4.31 1.79
-10 -5 -7 2.66 1.66
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10 5 8 10.42 1.92
10 -5 8 14.90 1.95
-10 -5 -8 10.83 2.09
-10 5 -8 11.35 2.11
10 -5 8 14.32 1.72
-10 -5 -8 11.40 2.00
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10 -5 9 26.66 2.54
-10 -5 -9 29.59 2.93
-10 5 -9 26.81 2.85
10 -5 9 29.21 2.24
-10 -5 -9 25.51 2.67
-10 -5 -10 4.74 2.11
-10 5 -10 10.36 2.21
10 -5 10 6.43 1.80
10 5 10 9.00 2.03
-10 -5 -11 3.54 2.18
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10 5 11 1.98 1.81
-10 -5 -12 42.75 3.87
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10 -5 12 48.47 3.56
10 5 12 46.35 3.64
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10 -5 13 -3.70 2.28
-10 5 -14 53.17 4.33
-10 -5 -14 50.15 4.36
10 -5 14 46.18 3.79
-10 -5 -15 7.35 3.07
-10 5 -15 11.30 2.84
10 -5 15 15.19 2.62
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-10 -6 24 1.28 2.50
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-10 -6 23 38.83 3.92
-10 -6 22 5.85 2.56
-10 6 22 3.56 2.25
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-10 6 21 56.04 4.37
-10 -6 21 59.72 4.54
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-10 -6 20 22.15 2.93
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10 6 -20 20.90 2.09
-10 -6 19 6.16 1.84
-10 6 19 8.53 1.95
-10 6 19 8.74 2.08
-10 -6 19 4.41 2.11
10 6 -19 8.95 1.65
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-10 -6 18 47.57 3.86
10 6 -18 44.17 3.08
-10 -6 18 46.67 3.49
-10 6 18 51.13 3.48
10 6 -17 28.04 2.39
-10 6 17 30.10 2.65
-10 -6 17 24.02 2.63
10 6 -16 6.41 2.79
10 -6 -16 10.24 2.98
10 6 -16 6.57 1.55
-10 6 16 8.06 1.89
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10 6 -15 0.93 1.26
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10 6 -14 6.30 1.48
10 6 -14 1.45 2.42
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-10 6 13 128.69 6.38
-10 -6 13 128.68 6.36
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-10 6 13 117.54 5.18
-10 6 13 115.62 5.90
-10 -6 12 51.38 3.40
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10 -6 -12 50.08 2.38
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10 -6 -11 52.51 4.15
10 -6 -11 55.32 2.72
-10 6 11 51.81 3.40
10 -6 -10 124.65 5.54
-10 6 10 115.70 6.15
10 6 -10 131.62 6.10
-10 -6 10 123.16 6.25
10 -6 -10 123.49 6.02
10 6 -10 128.84 6.82
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10 -6 -9 33.97 3.32
10 6 -9 36.60 3.23
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-10 -6 9 39.14 2.49
10 -6 -9 37.50 2.17
10 6 -8 34.20 2.33
-10 6 8 28.73 1.76
-10 -6 8 29.08 2.16
10 -6 -8 31.26 1.95
10 6 -8 32.39 2.97
-10 -6 7 17.84 2.01
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10 -6 -7 23.47 2.10
-10 -6 7 22.37 1.81
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-10 -12 -4 3.91 1.56
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-10 -12 -5 91.63 5.24
-10 12 -5 98.48 5.20
-10 -12 -5 101.24 5.33
10 -12 5 100.76 5.50
10 12 5 95.67 5.42
10 -12 5 92.94 4.83
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10 -12 6 10.37 1.52
-10 -12 -6 11.72 1.98
-10 12 -6 9.40 1.87
10 -12 6 9.63 2.05
10 12 6 9.29 2.07
-10 -12 -6 11.54 1.86
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-10 -12 -7 48.39 3.47
-10 12 -7 51.66 3.51
10 12 7 46.02 3.60
10 -12 7 48.82 3.55
-10 -12 -7 42.21 3.27
-10 12 -8 19.81 2.79
10 -12 8 28.51 2.38
-10 -12 -8 28.45 2.83
10 -12 8 33.21 3.06
-10 -12 -8 21.05 2.43
-10 12 -9 -0.64 2.03
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-10 -12 -9 0.68 1.94
10 -12 9 4.85 2.08
-10 -12 -9 0.20 1.56
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-10 -12 -10 0.83 1.75
-10 -12 -11 6.38 2.30
-10 12 -11 -0.71 2.22
10 12 11 4.25 2.12
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10 -12 11 3.87 2.15
10 12 11 2.90 1.77
10 12 12 4.69 2.12
10 -12 12 8.62 1.94
-10 -12 -12 6.46 2.50
-10 12 -12 7.74 2.39
10 12 12 12.07 2.25
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10 -12 13 52.93 3.90
-10 -12 -13 63.44 4.59
-10 12 -13 61.11 4.49
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-10 -12 -14 -0.29 2.48
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-10 -13 22 21.24 3.18
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-10 -13 21 5.79 2.39
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10 13 -21 3.43 1.84
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-10 -13 20 10.60 2.59
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10 13 -20 5.91 1.88
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-10 -13 19 73.45 5.26
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-10 -13 19 84.04 5.42
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-10 -13 18 -0.57 2.04
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-10 -13 17 20.66 2.92
-10 -13 16 11.18 2.14
-10 -13 16 10.11 2.38
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-10 -13 15 25.43 2.77
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-10 -13 14 34.17 2.82
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10 -13 -11 0.42 1.73
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-10 13 9 206.58 10.12
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-10 -13 8 0.64 1.39
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10 -13 -7 11.28 2.14
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10 -13 -6 3.47 1.55
10 -13 -6 3.06 1.84
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-10 -13 5 4.74 1.53
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10 -13 -5 7.30 1.72
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10 -13 -4 0.19 1.52
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10 -13 -4 2.80 1.75
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10 -13 -3 3.20 1.60
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10 -13 -2 0.57 1.46
10 -13 -2 -0.58 1.90
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10 13 -1 1.29 1.29
-10 -13 1 0.72 0.70
10 -13 -1 1.14 1.45
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10 -13 0 4.22 1.58
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-10 -13 -1 0.17 1.39
-10 13 -1 -1.30 1.95
10 -13 1 -0.39 1.54
10 13 1 0.17 1.47
-10 -13 -2 131.25 6.61
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10 -13 2 121.64 6.65
-10 13 -2 139.56 7.35
-10 -13 -3 26.79 2.39
-10 13 -3 24.40 2.18
-10 -13 -3 23.38 2.26
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-10 -13 -4 0.49 1.43
-10 13 -4 -0.76 1.47
-10 -13 -4 0.18 1.40
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10 -13 5 -0.21 1.81
-10 -13 -5 -0.70 1.66
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-10 -13 -6 44.08 3.16
-10 13 -6 37.24 2.96
10 -13 6 36.33 3.18
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-10 -13 -6 37.85 3.00
-10 13 -7 79.02 4.80
10 -13 7 65.38 3.89
-10 -13 -7 70.66 4.44
-10 13 -7 68.03 4.32
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10 13 7 77.22 4.65
-10 -13 -7 65.48 4.21
-10 13 -8 5.30 2.37
10 -13 8 4.88 1.63
-10 -13 -8 7.65 2.09
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-10 -13 -8 4.04 1.81
-10 13 -9 15.44 2.37
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-10 -13 -9 16.56 2.55
-10 13 -9 12.82 2.20
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-10 -13 -9 8.33 2.03
-10 13 -10 8.95 2.46
10 -13 10 4.61 1.90
-10 13 -10 9.60 2.44
-10 -13 -10 6.27 2.25
10 -13 10 7.17 2.38
-10 -13 -10 2.46 1.91
-10 13 -11 44.24 3.59
10 -13 11 41.05 3.11
10 -13 11 36.79 3.46
10 13 11 39.10 3.26
10 13 12 18.05 2.74
10 -13 12 18.27 2.49
-10 -13 -12 18.25 2.92
-10 13 -12 18.31 2.75
10 13 13 10.30 2.51
10 -13 13 14.16 2.26
-10 -13 -13 17.40 2.94
-10 13 -13 13.98 2.85
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10 13 14 -0.56 2.12
-10 -13 -14 3.22 2.45
-10 13 -14 2.70 2.30
-10 -14 22 17.11 2.90
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-10 -14 21 0.27 2.12
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10 14 -21 -0.63 1.75
-10 -14 20 1.97 2.15
-10 -14 20 0.59 2.12
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10 14 -20 1.06 1.75
-10 -14 19 4.89 2.15
-10 -14 19 5.08 2.35
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-10 -14 18 83.67 5.56
-10 14 18 88.46 4.97
-10 14 18 85.08 5.08
-10 -14 18 89.84 5.53
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-10 -14 17 -0.60 2.26
-10 -14 17 1.54 1.80
-10 -14 16 6.29 2.47
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-10 -14 16 4.13 1.85
10 14 -16 0.30 2.58
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-10 -14 15 13.62 2.56
-10 14 15 9.53 2.06
-10 -14 15 12.61 2.26
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10 -14 -14 0.27 2.18
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10 -14 -13 -0.25 2.27
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-10 -14 13 -0.61 1.53
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10 -14 -12 15.81 2.66
-10 -14 12 15.31 2.04
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-10 14 12 14.53 1.57
-10 14 12 14.62 2.42
10 -14 -11 4.76 1.75
-10 14 11 5.13 2.07
10 -14 -10 1.91 1.66
-10 14 10 0.12 1.27
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-10 14 10 1.08 0.51
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-10 14 9 8.62 1.61
10 -14 -9 6.12 2.16
-10 14 9 5.74 0.74
10 14 -9 3.64 1.96
10 14 -9 7.54 2.95
-10 14 8 38.86 3.24
10 14 -8 32.27 3.66
-10 -14 8 31.74 2.52
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10 -14 -8 28.52 2.87
10 14 -8 28.15 2.51
-10 -14 7 3.65 1.48
10 -14 -7 7.64 1.91
10 14 -7 2.00 1.88
10 -14 -7 6.47 1.86
-10 14 7 6.62 0.88
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-10 -14 6 3.77 1.49
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10 -14 -6 1.80 1.63
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10 -14 -5 56.12 3.63
-10 14 5 51.56 2.65
10 -14 -5 46.82 2.36
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10 -14 -4 1.66 1.68
-10 -14 4 -0.99 1.46
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10 -14 -4 1.77 1.51
10 14 -4 0.65 1.41
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-10 -14 3 11.72 1.69
10 14 -3 9.22 1.55
-10 14 3 8.15 2.28
10 -14 -3 11.00 1.92
10 14 -3 10.68 1.74
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10 14 -2 11.62 1.77
10 -14 -2 8.28 1.79
10 -14 -2 7.67 0.61
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10 -14 -2 9.51 2.03
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10 14 -1 5.27 1.49
10 14 -1 2.32 1.39
10 -14 -1 4.08 0.69
10 -14 -1 4.39 1.69
-10 -14 1 4.74 0.84
-10 -14 0 5.37 1.53
10 14 0 6.39 1.49
10 -14 0 7.86 1.86
-10 -14 0 4.83 0.67
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-10 -14 -1 1.06 1.47
-10 14 -1 1.09 2.12
10 -14 1 2.24 1.71
10 14 1 0.70 1.47
-10 -14 -2 105.02 5.51
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-10 14 -2 105.77 6.24
-10 14 -3 2.93 2.17
-10 -14 -3 2.12 1.42
-10 14 -3 0.14 1.33
-10 -14 -3 2.69 1.48
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-10 -14 -4 6.81 1.77
-10 14 -4 9.52 1.62
-10 -14 -4 10.10 1.85
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-10 -14 -5 9.89 1.81
-10 14 -5 6.61 1.67
-10 -14 -5 7.10 1.67
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-10 -14 -6 1.44 1.57
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-10 -14 -6 5.20 1.81
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10 14 6 1.79 1.81
-10 14 -7 20.03 2.85
10 -14 7 24.24 2.04
-10 -14 -7 25.40 2.61
-10 14 -7 22.97 2.52
10 14 7 16.92 2.62
10 -14 7 25.50 2.76
-10 -14 -7 20.06 2.35
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-10 -14 -8 1.70 1.83
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-10 -14 -8 0.96 1.70
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10 14 9 -0.52 2.03
10 -14 9 1.16 2.01
-10 -14 -9 1.58 1.63
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10 14 10 70.78 4.33
10 -14 10 71.71 4.13
-10 -14 -10 67.13 4.67
-10 14 -10 65.97 4.41
10 14 10 79.02 5.05
10 -14 10 74.18 4.69
-10 -14 -10 62.52 4.29
-10 -14 -11 2.79 2.36
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-10 -14 -12 93.00 5.74
-10 14 -12 86.53 5.53
10 -14 13 4.15 1.96
-10 -14 -13 6.96 2.70
-10 14 -13 4.61 2.46
10 -14 14 2.27 1.78
-10 -14 -14 -0.58 2.53
-10 14 -14 1.87 2.26
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10 15 -21 1.08 1.82
-10 -15 21 0.84 2.12
-10 -15 21 -1.51 2.43
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-10 -15 20 84.60 5.47
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-10 -15 18 0.81 2.02
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-10 -15 17 1.03 1.91
-10 -15 16 49.63 4.07
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-10 -15 16 50.73 3.85
-10 -15 15 -0.92 1.94
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10 -15 -15 0.27 2.45
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-10 -15 14 56.25 3.80
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10 15 -12 2.21 2.08
-10 -15 12 -0.57 1.55
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10 -15 -11 9.77 2.01
-10 -15 11 6.25 1.68
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10 15 -9 47.81 3.56
10 -15 -9 41.00 3.52
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-10 15 9 45.05 3.71
-10 15 8 78.53 4.18
-10 15 8 67.90 4.75
10 15 -8 78.06 4.64
10 15 -8 71.13 4.31
-10 15 8 71.72 3.31
-10 -15 8 78.16 4.33
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10 15 -7 7.07 1.61
10 15 -7 4.35 1.99
10 -15 -7 5.03 1.88
-10 -15 7 6.73 1.71
-10 -15 6 73.35 4.12
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10 15 -6 68.76 4.02
10 -15 -6 73.57 4.43
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10 -15 -5 11.44 0.92
-10 -15 5 14.16 1.85
10 -15 -5 11.95 2.00
10 15 -5 9.94 1.74
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10 -15 -4 2.45 1.60
10 15 -4 2.24 1.83
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10 -15 -3 13.31 2.00
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10 -15 -2 2.27 1.55
10 -15 -2 2.18 0.48
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10 15 -2 2.47 1.81
10 -15 -2 3.83 1.77
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10 -15 -1 6.27 1.84
10 15 -1 4.04 1.89
10 -15 -1 4.17 1.81
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-10 -15 -2 3.25 1.49
-10 -15 -2 5.46 1.61
10 -15 2 3.48 1.83
10 15 2 2.10 1.62
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-10 -15 -3 9.82 1.75
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-10 -15 -4 5.65 1.59
-10 -15 -4 4.66 1.59
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-10 -15 -6 133.67 6.72
-10 15 -6 132.10 6.63
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10 -15 6 125.69 7.01
-10 -15 -6 133.82 6.72
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10 -15 7 20.31 1.92
-10 -15 -7 16.57 2.36
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-10 -15 -8 1.90 1.84
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-10 -15 -8 0.19 1.68
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10 15 12 26.10 3.35
10 -15 12 20.70 2.91
10 -15 12 16.36 2.28
-10 -15 -12 25.09 3.17
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10 15 13 -0.62 2.57
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-10 15 -13 1.27 2.24
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-10 -15 -14 35.32 3.62
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-10 -16 22 6.78 2.64
10 16 -22 6.37 2.04
-10 -16 21 17.88 2.84
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-10 -16 18 50.75 4.14
-10 -16 18 49.24 4.44
-10 16 18 59.96 3.74
-10 -16 17 22.75 2.79
-10 16 17 25.18 2.61
-10 -16 17 31.29 3.43
-10 16 16 16.40 2.28
-10 -16 16 21.80 2.65
-10 -16 16 23.06 3.14
-10 16 16 16.06 2.26
-10 16 15 13.12 2.31
-10 -16 15 14.18 2.32
-10 -16 15 17.26 2.88
-10 16 15 18.36 2.26
-10 -16 14 7.53 1.85
-10 16 14 6.32 2.07
-10 -16 13 16.95 2.15
10 16 -13 16.50 1.73
-10 16 13 14.91 2.39
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-10 -16 11 2.83 1.48
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-10 -16 10 2.32 1.33
-10 16 10 0.50 1.97
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10 -16 -9 3.09 1.85
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10 -16 -6 7.61 1.91
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10 -16 -2 12.12 2.18
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10 -18 -12 8.19 2.13
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10 -18 -10 8.20 2.17
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-10 20 9 4.11 2.41
-10 20 9 3.06 1.84
10 -20 -9 1.24 1.83
-10 -20 9 2.33 1.35
10 20 -8 3.35 1.66
-10 20 8 1.79 2.27
10 -20 -8 2.95 1.80
-10 -20 8 1.99 1.24
-10 -20 8 3.16 1.81
-10 20 7 24.26 3.14
-10 20 7 22.84 2.68
10 20 -7 25.53 2.51
10 20 -7 23.03 2.41
10 20 -7 26.69 3.76
-10 -20 7 20.80 2.49
10 20 -6 18.66 2.25
10 20 -6 20.76 2.41
-10 -20 6 25.49 1.87
-10 20 6 21.58 3.16
-10 20 6 21.32 2.72
10 20 -5 10.33 1.88
-10 -20 5 12.48 1.34
-10 20 5 12.22 2.61
-10 20 5 10.76 2.32
10 20 -4 10.55 1.89
-10 20 4 9.86 2.75
10 -20 -4 17.60 2.45
10 20 -4 13.72 3.23
-10 -20 4 12.51 1.30
10 20 -3 27.16 2.60
-10 -20 3 31.22 2.77
-10 20 3 24.86 3.41
10 20 -3 28.12 2.50
10 -20 -3 26.31 2.93
-10 -20 3 27.44 1.73
10 20 -2 12.08 3.05
10 20 -2 8.21 2.11
-10 -20 2 6.90 1.96
10 -20 -2 11.68 2.26
10 20 -2 8.50 1.95
10 20 -2 5.89 1.71
10 20 -1 1.31 1.50
10 -20 -1 4.88 2.20
-10 -20 1 -0.20 1.58
10 20 0 4.35 1.89
10 -20 0 6.00 1.97
-10 -20 0 4.41 1.32
-10 20 0 3.33 2.43
-10 -20 0 5.83 1.82
10 20 0 3.52 1.60
10 -20 0 9.38 2.35
10 20 0 4.98 1.91
10 20 1 5.45 2.01
10 -20 1 2.36 1.95
-10 20 -1 0.67 2.58
-10 -20 -1 -1.01 1.60
10 20 1 3.09 1.53
-10 -20 -1 1.85 1.31
-10 20 -1 0.93 1.17
10 -20 1 0.26 1.90
10 20 1 0.91 1.96
-10 20 -2 1.33 2.57
-10 -20 -2 0.20 1.57
-10 -20 -2 1.97 1.39
-10 20 -2 0.12 1.26
10 -20 2 1.34 2.01
10 20 2 -0.47 1.90
-10 -20 -3 -1.79 1.61
-10 -20 -3 -1.68 1.46
-10 20 -3 -1.97 1.45
10 -20 3 0.82 2.03
-10 20 -3 -0.66 2.64
-10 20 -4 27.45 3.46
10 20 4 30.19 3.09
-10 -20 -4 28.11 2.63
10 -20 4 17.76 2.85
-10 -20 -4 19.48 2.26
-10 20 -4 20.50 2.08
-10 -20 -5 4.80 1.84
10 -20 5 7.33 2.34
-10 20 -5 5.14 2.57
-10 -20 -5 1.77 1.76
-10 20 -5 5.25 1.62
-10 20 -6 1.88 2.49
10 -20 6 0.57 2.19
-10 -20 -6 -0.54 1.71
-10 -20 -6 1.03 1.63
-10 20 -6 1.45 1.51
-10 20 -7 1.82 2.51
10 -20 7 6.67 2.64
-10 -20 -7 5.41 1.74
-10 20 -7 9.26 1.97
-10 -20 -7 3.68 1.74
-10 20 -8 18.16 2.95
10 -20 8 13.47 2.67
-10 -20 -8 18.37 2.28
-10 -20 -8 17.00 2.33
-10 20 -8 11.11 2.08
10 -20 9 0.29 2.38
-10 -20 -9 -1.65 1.65
-10 -20 -9 -1.66 1.87
-10 20 -9 -0.96 1.87
-10 20 -10 38.12 3.55
-10 -20 -10 26.24 2.84
10 -20 10 27.54 3.46
-10 -20 -10 43.51 3.38
-10 20 -10 39.80 3.17
10 -20 11 -4.43 2.57
-10 -20 -11 -0.69 2.08
10 -20 12 27.27 3.42
-10 -20 -12 33.23 3.34
-10 -21 20 0.68 2.66
-10 -21 20 -1.39 2.12
-10 -21 19 6.34 2.64
-10 -21 19 5.64 2.43
-10 -21 18 3.96 2.49
-10 -21 18 -0.26 2.04
-10 -21 17 21.26 3.37
-10 -21 17 28.53 3.00
-10 -21 16 11.42 2.90
-10 21 16 6.30 1.91
-10 -21 16 12.89 2.26
-10 -21 15 6.67 2.55
-10 21 15 6.28 2.12
-10 -21 15 5.98 1.94
-10 -21 14 32.26 3.74
-10 21 14 34.87 3.55
-10 -21 14 39.70 3.17
-10 -21 13 14.29 3.19
10 21 -13 19.97 2.26
-10 21 13 13.46 2.86
-10 -21 13 22.70 2.41
10 -21 -12 22.81 2.62
-10 -21 12 15.78 3.10
-10 21 12 16.99 2.32
-10 21 12 14.08 2.90
10 -21 -12 16.52 2.71
-10 -21 12 16.23 2.09
-10 -21 11 13.66 2.87
10 -21 -11 18.01 2.64
-10 -21 11 17.25 2.03
-10 21 11 12.60 2.77
10 21 -10 9.21 2.21
10 -21 -10 7.92 2.19
-10 -21 10 11.06 1.75
-10 21 10 11.06 2.78
-10 21 10 11.08 2.26
10 21 -9 22.49 2.51
-10 21 9 22.79 3.23
-10 21 9 23.06 2.64
10 -21 -9 17.85 2.79
-10 -21 9 21.25 2.00
-10 21 8 7.42 2.58
10 -21 -8 10.96 2.29
-10 -21 8 8.42 1.44
-10 -21 8 9.39 2.07
10 21 -7 7.94 1.98
10 21 -7 8.91 1.93
10 -21 -7 5.40 2.07
-10 -21 7 10.70 1.43
-10 21 7 7.86 2.49
-10 21 7 4.49 2.02
-10 21 6 6.07 2.55
-10 21 6 8.48 2.29
-10 -21 6 3.30 1.08
10 -21 -6 4.00 1.80
10 21 -6 6.67 1.73
-10 21 5 20.71 3.14
-10 -21 5 18.92 1.51
10 -21 -5 13.40 2.09
10 21 -5 14.96 2.13
10 21 -4 -0.20 1.49
-10 21 4 -0.66 2.25
10 -21 -4 1.03 2.02
-10 -21 4 0.30 0.81
10 21 -4 -0.46 1.90
-10 -21 4 -0.63 1.75
10 21 -3 10.48 1.94
-10 -21 3 8.42 1.84
-10 21 3 7.33 2.67
10 -21 -3 7.28 2.06
-10 -21 3 8.42 0.97
-10 -21 2 2.09 1.64
10 21 -2 3.31 1.64
10 -21 -2 3.69 2.03
10 21 -2 2.58 1.80
10 21 -1 1.65 1.86
-10 -21 1 2.73 1.71
10 21 -1 0.77 1.56
10 21 -1 -0.35 1.92
10 -21 -1 -0.17 1.72
10 -21 -1 -2.40 2.03
-10 -21 1 -0.32 1.10
-10 -21 0 4.14 1.27
-10 21 0 6.29 1.32
-10 21 0 3.08 2.67
-10 -21 0 7.60 1.86
10 21 0 3.03 1.64
10 -21 0 9.47 2.22
10 21 0 7.94 2.02
10 21 1 1.53 1.86
10 -21 1 1.53 1.96
-10 21 -1 1.13 1.21
-10 -21 -1 2.97 1.37
-10 21 -1 2.06 2.49
10 21 1 3.90 1.62
-10 -21 -1 2.47 1.73
10 -21 1 2.20 1.99
10 21 1 0.72 1.98
10 -21 2 11.10 2.23
-10 21 -2 14.78 3.09
-10 -21 -2 12.70 2.14
-10 -21 -2 10.92 1.62
-10 21 -2 10.93 1.55
10 -21 2 10.60 2.45
10 21 2 12.87 2.49
-10 21 -3 30.38 3.83
10 -21 3 37.13 3.59
-10 -21 -3 35.06 2.51
-10 21 -3 30.28 2.39
-10 -21 -3 34.36 2.98
-10 21 -4 38.41 3.97
-10 -21 -4 33.68 3.00
10 -21 4 33.41 3.55
-10 -21 -4 33.15 2.62
-10 21 -4 31.13 2.50
-10 -21 -5 10.29 2.08
10 -21 5 10.52 2.65
-10 21 -5 7.97 2.98
-10 -21 -5 9.37 1.90
-10 21 -5 6.02 1.67
-10 21 -6 7.10 2.66
10 -21 6 6.83 2.59
-10 -21 -6 4.62 1.83
-10 21 -6 7.71 1.72
-10 -21 -6 9.71 1.94
-10 21 -7 13.16 2.87
10 -21 7 11.10 2.92
-10 -21 -7 16.07 2.07
-10 -21 -7 7.49 1.94
-10 21 -7 13.57 2.09
-10 21 -8 7.55 2.86
10 -21 8 9.40 2.67
-10 -21 -8 7.35 1.91
-10 -21 -8 6.84 1.95
-10 21 -8 5.70 1.90
-10 21 -9 6.07 2.70
10 -21 9 9.15 2.72
-10 -21 -9 2.88 1.74
-10 -21 -9 11.66 2.10
-10 -21 -10 12.32 2.29
-10 21 -10 9.54 2.72
10 -21 10 12.52 2.77
10 -21 11 47.50 4.28
-10 -21 -11 43.36 3.64
-10 -22 19 3.95 2.70
-10 -22 19 1.59 2.20
-10 -22 18 2.21 2.55
-10 -22 18 2.54 2.07
-10 -22 17 4.49 2.61
-10 -22 17 2.43 1.90
-10 22 16 1.95 1.75
-10 -22 16 4.52 2.64
-10 -22 16 -0.92 1.95
-10 -22 15 21.27 3.34
-10 22 15 16.41 2.66
-10 -22 15 16.83 2.39
-10 -22 14 -0.38 2.57
-10 22 14 -3.08 2.30
-10 -22 14 1.65 1.71
-10 -22 13 74.20 5.29
10 22 -13 55.42 3.77
-10 22 13 48.47 4.48
-10 -22 13 64.52 3.95
-10 -22 12 17.77 3.12
10 -22 -12 21.66 2.92
-10 -22 12 23.38 2.33
-10 22 12 19.84 3.28
-10 22 12 28.39 2.67
10 -22 -11 7.11 2.28
-10 -22 11 7.31 1.66
-10 22 11 7.26 2.58
10 -22 -10 1.22 1.87
10 -22 -10 3.95 2.25
-10 -22 10 3.82 1.47
10 22 -10 2.83 3.30
-10 22 10 0.93 2.41
-10 22 10 1.52 1.90
10 22 -9 2.70 1.85
10 -22 -9 5.86 1.89
10 -22 -9 5.24 2.27
-10 -22 9 3.62 1.36
-10 22 9 5.02 2.55
-10 22 9 2.38 1.93
10 -22 -8 20.10 2.35
10 -22 -8 17.58 2.67
-10 -22 8 16.81 1.73
10 22 -7 2.84 1.75
10 -22 -7 6.10 2.09
-10 -22 7 7.80 1.27
-10 22 7 3.20 2.11
-10 22 7 1.63 2.45
-10 22 6 13.04 2.45
-10 22 6 10.23 2.68
10 22 -6 9.69 1.94
10 22 -6 12.25 2.11
10 22 -6 9.89 3.17
-10 -22 6 13.10 1.39
-10 22 5 0.67 2.55
10 22 -5 1.27 1.55
10 22 -5 -1.12 1.68
10 -22 -5 0.74 1.58
-10 -22 5 0.58 0.90
-10 -22 5 0.87 1.82
-10 22 4 5.09 2.62
-10 22 4 8.31 2.21
-10 -22 4 8.15 0.97
10 22 -4 5.38 1.80
-10 -22 4 11.06 2.18
10 22 -3 9.14 1.84
-10 -22 3 9.76 2.06
-10 22 3 7.54 2.65
10 -22 -3 9.69 2.26
10 22 -3 12.85 3.07
10 22 -3 5.51 2.14
10 22 -2 0.97 1.90
-10 -22 2 6.46 1.87
10 22 -2 3.79 1.60
10 -22 -2 3.27 2.18
10 22 -2 2.32 1.70
10 22 -1 -1.97 2.00
-10 -22 1 1.29 1.71
10 22 -1 1.38 1.58
10 -22 -1 0.64 1.72
10 22 -1 -0.17 1.73
10 -22 -1 3.87 2.14
-10 -22 1 0.81 1.07
-10 -22 0 0.84 1.72
10 22 0 2.51 1.69
-10 22 0 3.88 2.49
10 -22 0 1.40 2.22
-10 -22 0 1.18 1.21
-10 22 0 2.06 1.14
-10 -22 -1 0.11 1.28
-10 22 -1 -1.20 1.18
10 22 1 1.89 1.56
-10 -22 -1 -1.47 1.72
-10 22 -1 0.35 2.63
10 -22 1 -0.85 2.13
10 22 1 -1.12 1.94
10 -22 1 -1.09 1.91
-10 22 -2 2.79 1.28
-10 -22 -2 9.87 1.57
-10 -22 -2 13.12 2.28
-10 22 -2 2.47 2.64
10 -22 2 2.89 2.26
10 -22 2 1.34 2.04
10 22 2 9.70 2.24
-10 22 -3 31.22 3.83
10 -22 3 36.09 3.56
-10 22 -3 31.00 2.35
-10 -22 -3 30.67 2.38
-10 -22 -3 31.14 2.90
-10 22 -4 3.13 2.89
-10 -22 -4 -1.43 1.75
10 -22 4 0.30 2.30
-10 -22 -4 2.25 1.50
-10 22 -4 1.60 1.41
-10 -22 -5 46.13 3.46
10 -22 5 46.02 4.01
-10 22 -5 44.40 4.33
-10 -22 -5 43.92 3.05
-10 22 -6 -0.33 2.48
10 -22 6 -2.45 2.49
-10 -22 -6 1.06 1.55
-10 -22 -6 -1.13 1.51
-10 22 -7 0.97 2.59
10 -22 7 4.66 2.55
-10 -22 -7 3.53 1.72
-10 -22 -7 7.24 1.82
-10 22 -8 -0.93 2.39
10 -22 8 0.94 2.39
-10 -22 -8 0.88 1.58
-10 -22 -8 1.83 1.68
-10 22 -9 0.59 2.34
10 -22 9 3.46 2.64
-10 -22 -9 0.88 1.62
-10 -22 -9 -1.36 1.93
10 -22 10 2.20 2.38
-10 22 -10 3.64 2.50
10 -22 11 1.88 2.60
-10 -23 19 25.93 3.60
-10 -23 19 29.92 3.26
-10 -23 18 1.50 2.51
-10 -23 18 -0.75 2.13
-10 -23 17 13.74 3.14
-10 -23 17 16.75 2.45
-10 -23 16 6.15 2.67
-10 -23 16 2.05 1.88
-10 -23 15 10.09 2.93
-10 23 15 9.35 2.44
-10 -23 15 9.25 2.03
-10 -23 14 15.47 3.10
-10 23 14 17.77 3.04
-10 -23 14 17.99 2.37
-10 -23 13 1.16 2.50
-10 23 13 2.07 2.32
10 23 -13 1.60 1.81
10 -23 -13 -0.27 2.12
-10 -23 13 1.52 1.58
-10 -23 12 17.16 3.37
-10 23 12 20.08 3.29
-10 23 12 27.99 2.68
10 -23 -12 17.52 2.81
-10 -23 12 22.93 2.36
-10 -23 11 4.85 2.65
-10 23 11 2.18 2.55
10 -23 -11 7.54 2.40
-10 -23 11 8.46 1.71
-10 -23 10 19.31 3.19
10 -23 -10 25.08 3.05
-10 -23 10 21.00 2.10
-10 23 10 24.81 3.48
-10 23 10 24.37 2.83
10 -23 -9 4.57 2.12
-10 -23 9 5.39 1.37
-10 23 9 6.63 2.20
-10 23 9 1.95 2.67
10 -23 -8 4.05 2.16
-10 -23 8 1.32 1.13
-10 23 8 2.79 2.09
-10 23 8 1.65 2.51
10 -23 -7 40.97 3.00
10 23 -7 40.04 3.32
10 -23 -7 45.64 3.80
-10 -23 7 43.63 2.56
-10 23 7 34.20 3.36
-10 23 7 46.07 4.25
10 23 -6 0.66 1.66
-10 23 6 -1.15 2.15
-10 23 6 0.68 2.50
10 -23 -6 0.55 2.07
-10 -23 6 1.52 1.02
-10 23 5 5.87 2.64
10 -23 -5 6.94 1.71
10 23 -5 4.78 1.73
10 23 -5 5.52 3.17
-10 -23 5 6.27 1.97
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10 23 -4 -2.53 2.99
10 -23 -4 1.11 1.53
10 23 -4 -0.85 1.67
-10 -23 4 1.56 1.83
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10 -23 -3 -0.28 2.19
10 23 -3 2.08 1.62
10 -23 -3 -0.14 1.56
-10 -23 2 2.21 1.88
-10 -23 2 0.63 1.02
10 23 -2 -1.02 1.71
10 -23 -2 1.98 2.13
10 23 -2 5.63 2.83
-10 -23 1 3.11 2.02
10 23 -1 -1.21 1.72
10 -23 -1 1.21 1.64
10 -23 -1 4.86 2.34
-10 -23 1 -0.86 1.15
-10 -23 0 2.53 1.19
-10 -23 0 2.35 1.79
10 23 0 1.58 1.66
-10 23 0 2.53 2.55
10 -23 0 -0.29 2.33
10 -23 0 -0.16 1.87
10 23 1 56.74 3.59
-10 -23 -1 49.78 3.64
-10 23 -1 43.17 4.47
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-10 -23 -2 1.62 1.23
-10 -23 -2 -0.63 1.89
-10 23 -2 1.09 2.63
10 -23 2 0.60 2.21
10 -23 2 -0.55 1.91
-10 -23 -3 11.98 1.66
-10 -23 -3 14.30 2.19
-10 23 -3 15.51 3.17
10 -23 3 11.83 2.67
10 -23 3 10.57 2.29
-10 23 -4 8.92 2.98
10 -23 4 7.09 2.60
-10 -23 -4 7.95 1.66
-10 -23 -4 11.09 2.12
-10 23 -5 1.41 2.55
-10 -23 -5 -1.02 1.81
10 -23 5 0.63 2.26
-10 -23 -5 3.18 1.51
-10 23 -6 19.93 3.38
10 -23 6 25.02 3.29
-10 -23 -6 19.70 2.34
-10 -23 -6 21.08 2.19
-10 23 -7 12.95 3.09
10 -23 7 12.50 2.93
-10 -23 -7 12.85 1.96
-10 -23 -7 6.63 1.76
-10 -23 -8 0.52 1.60
10 -23 8 -1.94 2.71
-10 23 -8 -0.64 2.51
10 -23 9 6.80 2.80
-10 23 -9 9.17 2.83
10 -23 10 7.44 2.87
-10 23 -10 10.05 2.81
-10 -24 18 35.40 3.97
-10 -24 18 30.75 3.16
-10 -24 17 6.22 2.75
-10 -24 17 0.94 1.80
-10 -24 16 19.98 3.61
-10 -24 16 26.86 2.73
-10 -24 15 0.40 2.44
-10 24 15 0.84 2.24
-10 -24 15 2.33 1.78
-10 -24 14 1.98 2.76
-10 24 14 1.17 2.35
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-10 -24 13 -2.36 2.92
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10 24 -13 -0.75 1.92
10 -24 -13 -0.55 2.17
-10 -24 13 -0.74 1.68
-10 -24 12 31.11 3.89
-10 24 12 23.73 3.57
-10 24 12 31.14 2.96
10 -24 -12 26.69 3.21
-10 -24 12 25.06 2.40
-10 -24 11 2.69 2.42
-10 24 11 4.16 2.57
10 -24 -11 2.76 2.12
-10 -24 11 2.21 1.50
-10 -24 10 24.41 3.55
10 -24 -10 21.55 3.00
-10 -24 10 18.97 2.01
-10 24 10 24.09 2.93
-10 24 10 18.37 3.36
10 -24 -9 60.25 4.48
-10 -24 9 49.85 3.11
-10 24 9 52.18 4.01
-10 24 9 47.50 4.72
10 -24 -8 22.22 2.88
-10 -24 8 18.26 1.73
-10 24 8 16.11 2.61
10 24 -7 7.87 2.08
-10 24 7 8.33 2.41
-10 24 7 8.32 2.97
10 -24 -7 7.60 2.41
-10 -24 7 9.26 1.29
-10 -24 6 27.34 2.86
-10 24 6 21.02 2.91
-10 24 6 26.37 3.53
10 -24 -6 21.69 2.93
10 24 -6 22.29 2.63
10 24 -5 32.56 2.94
-10 -24 5 33.62 3.10
10 24 -5 30.82 4.13
-10 24 5 24.93 3.64
-10 24 4 -1.02 2.22
-10 24 4 -1.44 2.69
10 24 -4 -2.18 1.72
-10 -24 4 0.23 1.86
-10 24 3 -1.45 2.90
10 24 -3 1.92 1.58
-10 -24 3 0.69 1.75
10 24 -2 5.86 1.80
-10 -24 2 3.87 1.90
10 -24 -2 4.38 2.29
10 24 -1 -0.62 1.68
10 -24 -1 0.30 2.28
-10 -24 1 1.37 1.86
-10 -24 0 8.71 2.09
10 24 0 4.23 1.86
-10 24 0 2.22 2.90
10 -24 0 2.99 2.49
-10 -24 -1 2.60 1.88
10 24 1 0.20 1.65
-10 24 -1 1.12 2.68
10 -24 1 0.91 2.16
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-10 -24 -2 13.68 2.28
-10 24 -2 11.90 3.14
10 -24 2 10.17 2.69
-10 -24 -3 4.18 1.82
-10 24 -3 2.59 2.76
10 -24 3 9.08 2.38
-10 -24 -4 15.71 2.26
-10 24 -4 9.16 3.30
10 -24 4 7.95 2.74
-10 -24 -5 -1.02 1.76
10 -24 5 -0.97 2.54
-10 24 -5 0.36 2.83
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-10 -24 -6 3.78 1.71
10 -24 7 1.65 2.49
-10 24 -7 2.39 2.49
-10 -24 -7 1.02 1.62
-10 24 -8 -0.66 2.70
10 -24 8 0.33 2.54
-10 24 -9 2.50 2.55
10 -24 9 0.33 2.47
10 -24 10 10.64 3.02
10 24 10 15.46 3.18
-10 -25 18 -1.93 2.14
-10 -25 18 1.54 2.80
-10 -25 17 -2.30 1.80
-10 -25 17 -1.19 2.79
-10 -25 16 7.46 2.11
-10 -25 16 11.55 2.94
-10 25 15 5.42 2.50
-10 -25 15 10.36 2.05
-10 -25 15 7.66 2.94
-10 25 14 26.86 3.73
-10 -25 14 33.01 2.78
-10 -25 14 26.22 3.75
-10 25 13 -0.62 2.58
10 25 -13 1.97 1.96
10 -25 -13 1.11 2.12
-10 -25 13 -0.54 1.67
-10 -25 13 2.81 2.70
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10 -25 -12 -1.68 2.17
-10 -25 12 0.67 1.45
-10 -25 12 -1.19 2.66
-10 25 11 34.48 4.35
10 -25 -11 39.25 3.81
-10 -25 11 39.13 2.82
-10 -25 11 31.47 4.02
-10 25 10 61.50 4.25
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22 -6 -8 6.43 2.51
-22 6 8 2.90 2.24
-22 -6 7 2.83 2.12
-22 6 7 -0.32 2.43
-22 -6 7 4.31 2.23
22 -6 -7 0.95 2.43
-22 6 7 3.23 2.12
22 -6 -7 0.48 3.70
-22 -6 6 -0.25 2.10
-22 6 6 -0.31 2.51
-22 -6 6 2.45 2.22
22 6 -6 -0.65 2.54
22 -6 -6 1.97 2.57
-22 6 6 7.38 2.42
22 6 -6 6.14 3.90
22 -6 -6 4.29 3.86
-22 7 13 -1.40 2.67
-22 -7 13 0.62 2.41
-22 -7 13 -1.28 2.16
-22 7 12 0.35 2.45
-22 -7 12 0.30 2.26
-22 -7 12 -0.52 2.12
22 -7 -12 0.97 2.04
22 7 -12 3.34 3.58
22 -7 -12 0.98 4.01
-22 7 11 29.38 3.89
-22 -7 11 36.60 3.60
-22 -7 11 29.31 3.37
22 -7 -11 39.24 3.40
22 7 -11 36.49 5.20
22 -7 -11 35.22 5.30
-22 7 10 1.01 2.44
-22 -7 10 1.99 2.38
-22 -7 10 -3.17 2.35
22 -7 -10 5.52 2.31
22 7 -10 2.36 3.69
-22 -7 9 6.04 2.46
-22 7 9 3.32 2.60
-22 -7 9 3.21 2.10
22 -7 -9 -0.87 2.37
-22 7 9 1.60 2.12
-22 -7 8 1.06 1.91
-22 7 8 -0.65 2.44
-22 -7 8 -0.54 2.22
22 -7 -8 0.91 2.20
-22 7 8 -1.66 2.12
-22 -7 7 4.80 2.17
-22 7 7 -0.96 2.30
-22 -7 7 -0.27 2.20
22 -7 -7 6.02 2.54
-22 7 7 2.92 2.02
22 7 -7 2.34 3.92
22 -7 -7 5.25 3.96
-22 -7 6 0.72 2.01
-22 7 6 1.89 2.43
-22 -7 6 0.83 2.24
22 -7 -6 -3.60 2.62
-22 7 6 2.00 2.12
22 7 -6 -3.76 4.01
-22 -8 12 10.56 2.56
-22 -8 12 10.47 2.78
22 8 -12 12.77 3.94
22 -8 -12 15.21 4.31
-22 8 12 12.27 2.97
-22 -8 11 -0.53 2.10
-22 -8 11 3.20 2.59
22 8 -11 3.29 3.66
-22 8 11 -0.35 2.59
-22 -8 10 5.34 2.46
-22 8 10 1.37 2.74
-22 -8 10 1.07 2.11
-22 -8 9 0.81 2.12
-22 8 9 0.34 2.67
-22 -8 9 1.08 2.12
-22 -8 8 9.36 2.41
-22 8 8 13.23 3.00
-22 8 8 9.92 2.25
-22 -8 8 11.53 2.59
-22 -8 7 10.68 2.45
-22 8 7 9.76 2.78
-22 -8 7 12.20 2.67
-22 8 7 8.80 2.39
22 8 -7 6.06 4.08
22 -8 -7 11.91 4.10
22 -9 -10 2.97 2.17
-22 -9 10 3.54 2.27
-22 9 10 1.73 2.53
-22 -9 10 2.22 2.32
22 -9 -10 2.43 3.93
22 -9 -9 -1.43 2.26
-22 -9 9 -1.10 2.29
-22 9 9 2.05 2.41
-22 -9 9 2.41 2.10
22 9 -9 2.47 3.99
0 0 0 0.00 0.00
TITL 2024ncs0418_1b in P2(1)/c
REM P2(1)/c (#14 in standard setting (mkl: cell=1,tostdtrans=1,'abc'))
CELL 0.71075 13.600131 22.934207 14.850191 90.0000 113.1986 90.0000
ZERR 4.00 0.000442 0.000507 0.000469 0.0000 0.0037 0.0000
LATT 1
SYMM -x, y+1/2,-z+1/2
SFAC C H N O Fe
UNIT 176.00 184.00 16.00 56.00 8.00
REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0
TEMP -173
SIZE 0.02 0.13 0.14
TREF
HKLF 4
END
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 2938
_shelx_res_file
;
TITL 2024ncs0418_1b_a.res in P2(1)/c
a6y(oac)3.res
created by SHELXL-2018/3 at 08:44:29 on 17-Aug-2026
REM Old TITL 2024ncs0418_1b in P2(1)/c
REM SHELXT solution in P2(1)/c: R1 0.080, Rweak 0.004, Alpha 0.034
REM 0.466 for 235 systematic absences, Orientation as input
REM Formula found by SHELXT: C44 N9 O9 Fe2
CELL 0.71075 13.6001 22.9342 14.8502 90 113.199 90
ZERR 4 0.0004 0.0005 0.0005 0 0.004 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H Fe N O
UNIT 176 184 8 16 56
EQIV $1 -1+X,+Y,-1+Z
EQIV $2 +X,0.5-Y,-0.5+Z
EQIV $3 1-X,1-Y,1-Z
EQIV $4 2-X,1-Y,1-Z
L.S. 4 0 0
PLAN 5
SIZE 0.02 0.13 0.14
TEMP -173(2)
CONF
HTAB O12 O10
HTAB O13 O5
HTAB O13 O8
HTAB O14 O12_$1
HTAB O14 O13
HTAB O10 O1
HTAB O10 O2
HTAB O10 O3
HTAB O10 O4
HTAB O11 O2
HTAB O11 O3
HTAB O12 O11
HTAB O13 O6
HTAB O13 O7
HTAB O11 O1
HTAB C7 O10_$2
HTAB C36 O14_$3
HTAB C44 O11_$4
HTAB
BOND
MORE -1
BOND $H
fmap 2 53
acta
OMIT -9 4 4
OMIT -3 10 3
OMIT -2 5 6
OMIT -1 2 2
OMIT 0 0 6
OMIT 0 1 6
OMIT 0 2 2
OMIT 2 0 0
REM
REM
REM
WGHT 0.065100 0.401800
FVAR 0.17876
C1 1 1.088760 0.267168 0.677404 11.00000 0.01268 0.01337 =
0.01278 0.00022 0.00547 0.00200
C2 1 1.162485 0.248549 0.771159 11.00000 0.01400 0.01710 =
0.01216 0.00044 0.00543 0.00185
C3 1 1.216558 0.196267 0.783130 11.00000 0.01696 0.01824 =
0.01629 0.00424 0.00758 0.00336
AFIX 43
H3 2 1.265479 0.184681 0.846347 11.00000 -1.20000
AFIX 0
C4 1 1.199212 0.160255 0.701865 11.00000 0.02180 0.01487 =
0.02031 0.00337 0.01120 0.00388
AFIX 43
H4 2 1.236234 0.124227 0.710186 11.00000 -1.20000
AFIX 0
C5 1 1.128707 0.177027 0.610190 11.00000 0.02267 0.01349 =
0.01803 0.00076 0.01082 0.00345
AFIX 43
H5 2 1.116761 0.152104 0.555782 11.00000 -1.20000
AFIX 0
C6 1 1.073720 0.230829 0.595709 11.00000 0.01455 0.01422 =
0.01294 0.00022 0.00691 0.00090
C7 1 1.010931 0.248284 0.496483 11.00000 0.01704 0.01371 =
0.01365 -0.00118 0.00760 -0.00014
AFIX 43
H7 2 1.006415 0.221706 0.445933 11.00000 -1.20000
AFIX 0
C8 1 0.906905 0.312843 0.370058 11.00000 0.01335 0.01448 =
0.00987 -0.00124 0.00551 -0.00124
C9 1 0.898055 0.277443 0.290477 11.00000 0.01797 0.01651 =
0.01337 -0.00295 0.00672 -0.00007
AFIX 43
H9 2 0.929948 0.239845 0.301535 11.00000 -1.20000
AFIX 0
C10 1 0.842880 0.297121 0.195612 11.00000 0.02040 0.02140 =
0.01100 -0.00365 0.00595 -0.00310
AFIX 43
H10 2 0.838676 0.273414 0.141756 11.00000 -1.20000
AFIX 0
C11 1 0.793425 0.351699 0.178918 11.00000 0.01942 0.02239 =
0.01050 -0.00007 0.00415 -0.00176
AFIX 43
H11 2 0.753453 0.364358 0.113722 11.00000 -1.20000
AFIX 0
C12 1 0.802324 0.387534 0.256970 11.00000 0.01883 0.01749 =
0.01173 0.00041 0.00446 -0.00027
AFIX 43
H12 2 0.768362 0.424589 0.245216 11.00000 -1.20000
AFIX 0
C13 1 0.861296 0.369080 0.352920 11.00000 0.01318 0.01463 =
0.01060 -0.00163 0.00533 -0.00161
C14 1 0.865850 0.459078 0.431425 11.00000 0.01236 0.01464 =
0.01246 0.00064 0.00542 0.00000
AFIX 43
H14 2 0.842477 0.476080 0.368075 11.00000 -1.20000
AFIX 0
C15 1 0.883396 0.497578 0.512626 11.00000 0.01112 0.01246 =
0.01417 -0.00127 0.00600 -0.00077
C16 1 0.856874 0.557183 0.490789 11.00000 0.01384 0.01366 =
0.01821 0.00072 0.00755 0.00007
AFIX 43
H16 2 0.828358 0.569966 0.424586 11.00000 -1.20000
AFIX 0
C17 1 0.872204 0.596510 0.564852 11.00000 0.01708 0.01331 =
0.02247 -0.00100 0.00953 0.00029
AFIX 43
H17 2 0.853918 0.636313 0.549479 11.00000 -1.20000
AFIX 0
C18 1 0.914544 0.578440 0.662790 11.00000 0.01878 0.01565 =
0.02031 -0.00407 0.00893 -0.00001
AFIX 43
H18 2 0.924599 0.605938 0.713507 11.00000 -1.20000
AFIX 0
C19 1 0.941745 0.520678 0.685853 11.00000 0.01655 0.01534 =
0.01479 -0.00375 0.00508 -0.00001
C20 1 0.927757 0.478861 0.611057 11.00000 0.01228 0.01222 =
0.01486 -0.00190 0.00548 -0.00039
C21 1 1.243687 0.272015 0.941207 11.00000 0.01779 0.02510 =
0.01142 0.00256 0.00405 0.00299
AFIX 137
H21A 2 1.315565 0.264844 0.943232 11.00000 -1.50000
H21B 2 1.217041 0.236589 0.960896 11.00000 -1.50000
H21C 2 1.246519 0.303823 0.986232 11.00000 -1.50000
AFIX 0
C22 1 0.992729 0.536258 0.856968 11.00000 0.05430 0.02465 =
0.01572 -0.00602 0.00852 0.00618
AFIX 137
H22A 2 1.024290 0.515325 0.919384 11.00000 -1.50000
H22B 2 0.921502 0.550476 0.847949 11.00000 -1.50000
H22C 2 1.038435 0.569379 0.857384 11.00000 -1.50000
AFIX 0
C23 1 0.528399 0.251715 0.445779 11.00000 0.01251 0.01158 =
0.01185 -0.00011 0.00551 -0.00005
C24 1 0.467782 0.222901 0.356091 11.00000 0.01529 0.01241 =
0.01139 -0.00089 0.00637 -0.00036
C25 1 0.430125 0.166877 0.354615 11.00000 0.02262 0.01378 =
0.01572 -0.00257 0.00823 -0.00378
AFIX 43
H25 2 0.390311 0.148472 0.293762 11.00000 -1.20000
AFIX 0
C26 1 0.450412 0.136906 0.442774 11.00000 0.02800 0.01320 =
0.01793 -0.00109 0.01000 -0.00430
AFIX 43
H26 2 0.425375 0.098106 0.441344 11.00000 -1.20000
AFIX 0
C27 1 0.506333 0.163674 0.530811 11.00000 0.02341 0.01365 =
0.01472 0.00175 0.00876 -0.00174
AFIX 43
H27 2 0.518748 0.143494 0.590172 11.00000 -1.20000
AFIX 0
C28 1 0.545889 0.221361 0.534019 11.00000 0.01448 0.01321 =
0.01156 0.00025 0.00583 -0.00018
C29 1 0.596476 0.247605 0.628811 11.00000 0.01412 0.01431 =
0.01115 0.00259 0.00554 0.00131
AFIX 43
H29 2 0.599779 0.225325 0.683861 11.00000 -1.20000
AFIX 0
C30 1 0.683722 0.322889 0.741438 11.00000 0.01240 0.01774 =
0.00945 0.00022 0.00485 0.00078
C31 1 0.705752 0.291333 0.827994 11.00000 0.01770 0.02288 =
0.01134 0.00237 0.00670 0.00046
AFIX 43
H31 2 0.688947 0.250992 0.825223 11.00000 -1.20000
AFIX 0
C32 1 0.752103 0.319214 0.917524 11.00000 0.02374 0.03074 =
0.00923 0.00171 0.00619 -0.00104
AFIX 43
H32 2 0.766979 0.297903 0.976298 11.00000 -1.20000
AFIX 0
C33 1 0.777170 0.378472 0.922077 11.00000 0.02735 0.03116 =
0.01058 -0.00306 0.00549 -0.00458
AFIX 43
H33 2 0.809004 0.397159 0.983975 11.00000 -1.20000
AFIX 0
C34 1 0.756002 0.410321 0.837000 11.00000 0.02320 0.02224 =
0.01227 -0.00325 0.00540 -0.00445
AFIX 43
H34 2 0.773706 0.450562 0.840548 11.00000 -1.20000
AFIX 0
C35 1 0.708398 0.382730 0.745965 11.00000 0.01403 0.01851 =
0.01053 -0.00030 0.00534 0.00021
C36 1 0.665106 0.466480 0.646415 11.00000 0.01313 0.01526 =
0.01348 -0.00257 0.00609 -0.00139
AFIX 43
H36 2 0.669278 0.486802 0.703553 11.00000 -1.20000
AFIX 0
C37 1 0.638237 0.499640 0.558050 11.00000 0.01150 0.01253 =
0.01536 -0.00166 0.00574 -0.00085
C38 1 0.615994 0.559985 0.561639 11.00000 0.01459 0.01337 =
0.02120 -0.00363 0.00811 -0.00116
AFIX 43
H38 2 0.620872 0.576832 0.621696 11.00000 -1.20000
AFIX 0
C39 1 0.587633 0.594111 0.479605 11.00000 0.01510 0.01229 =
0.02498 -0.00107 0.00853 -0.00060
AFIX 43
H39 2 0.572358 0.634290 0.482858 11.00000 -1.20000
AFIX 0
C40 1 0.581093 0.569665 0.390372 11.00000 0.01515 0.01314 =
0.02158 0.00393 0.00754 0.00055
AFIX 43
H40 2 0.561737 0.593468 0.333634 11.00000 -1.20000
AFIX 0
C41 1 0.602703 0.511276 0.385108 11.00000 0.01346 0.01271 =
0.01572 0.00097 0.00620 -0.00096
C42 1 0.629635 0.474074 0.468570 11.00000 0.01123 0.01108 =
0.01503 0.00051 0.00568 -0.00059
C43 1 0.383093 0.233119 0.182104 11.00000 0.01786 0.02140 =
0.01063 -0.00304 0.00420 -0.00211
AFIX 137
H43A 2 0.372500 0.262585 0.131329 11.00000 -1.50000
H43B 2 0.313892 0.222924 0.183858 11.00000 -1.50000
H43C 2 0.415559 0.198218 0.167304 11.00000 -1.50000
AFIX 0
C44 1 0.570677 0.515861 0.214742 11.00000 0.02738 0.02015 =
0.01772 0.00650 0.00949 -0.00069
AFIX 137
H44A 2 0.567734 0.489983 0.161224 11.00000 -1.50000
H44B 2 0.623386 0.546720 0.223027 11.00000 -1.50000
H44C 2 0.500134 0.533374 0.199164 11.00000 -1.50000
AFIX 0
FE1 3 0.923441 0.353103 0.565286 11.00000 0.01062 0.01160 =
0.00918 -0.00053 0.00416 0.00124
FE2 3 0.669025 0.351622 0.541082 11.00000 0.01054 0.01061 =
0.00868 0.00020 0.00452 -0.00008
N1 4 0.959920 0.297334 0.470262 11.00000 0.01277 0.01417 =
0.01090 -0.00076 0.00562 0.00031
N2 4 0.879338 0.402878 0.437539 11.00000 0.01190 0.01372 =
0.00992 -0.00154 0.00465 -0.00037
N3 4 0.638248 0.299586 0.645357 11.00000 0.01167 0.01474 =
0.00906 -0.00012 0.00453 -0.00029
N4 4 0.684288 0.410501 0.654442 11.00000 0.01299 0.01419 =
0.01077 -0.00067 0.00499 -0.00045
O1 5 1.173805 0.287702 0.844175 11.00000 0.01989 0.02201 =
0.01199 -0.00103 0.00233 0.00657
O2 5 1.041588 0.317518 0.672000 11.00000 0.01668 0.01853 =
0.01239 -0.00194 0.00206 0.00710
O3 5 0.959488 0.424898 0.638371 11.00000 0.02119 0.01331 =
0.01250 -0.00113 0.00394 0.00160
O4 5 0.983944 0.497856 0.778705 11.00000 0.03479 0.01933 =
0.01197 -0.00357 0.00423 0.00601
O5 5 0.451841 0.255823 0.274810 11.00000 0.01950 0.01574 =
0.00922 -0.00027 0.00366 -0.00337
O6 5 0.561153 0.305207 0.441852 11.00000 0.01654 0.01208 =
0.01083 0.00080 0.00434 -0.00287
O7 5 0.644617 0.418710 0.457176 11.00000 0.01827 0.01106 =
0.01298 0.00086 0.00773 0.00191
O8 5 0.600966 0.483067 0.303398 11.00000 0.02671 0.01357 =
0.01380 0.00336 0.00892 0.00065
O9 5 0.799370 0.324773 0.560549 11.00000 0.01253 0.01411 =
0.01409 0.00272 0.00670 0.00196
AFIX 6
O10 5 1.010723 0.370773 0.846466 11.00000 0.03328 0.02499 =
0.02532 0.00523 0.01744 0.00705
H10A 2 1.033811 0.344794 0.816773 11.00000 -1.50000
H10B 2 0.989409 0.399583 0.805018 11.00000 -1.50000
AFIX 6
O11 5 1.190783 0.420115 0.764962 11.00000 0.02254 0.04166 =
0.02970 0.00429 0.00776 -0.00742
H11A 2 1.124104 0.426667 0.727741 11.00000 -1.50000
H11B 2 1.194509 0.382485 0.773752 11.00000 -1.50000
AFIX 6
O12 5 1.197896 0.433862 0.964656 11.00000 0.04281 0.05701 =
0.02464 0.00039 0.00575 -0.00051
H12A 2 1.135376 0.418501 0.932145 11.00000 -1.50000
H12B 2 1.221847 0.442892 0.920136 11.00000 -1.50000
AFIX 6
O13 5 0.510352 0.371502 0.252801 11.00000 0.05145 0.01861 =
0.01577 -0.00117 0.01031 -0.01067
H13A 2 0.502313 0.343602 0.288940 11.00000 -1.50000
H13B 2 0.552296 0.396394 0.294381 11.00000 -1.50000
AFIX 6
O14 5 0.336959 0.451637 0.164041 11.00000 0.03584 0.02694 =
0.02670 -0.00486 0.01158 -0.00381
H14A 2 0.303822 0.446857 0.101121 11.00000 -1.50000
H14B 2 0.385680 0.424467 0.182002 11.00000 -1.50000
AFIX 0
HKLF 4
REM 2024ncs0418_1b_a.res in P2(1)/c
REM wR2 = 0.1188, GooF = S = 1.038, Restrained GooF = 1.038 for all data
REM R1 = 0.0444 for 15233 Fo > 4sig(Fo) and 0.0678 for all 20596 data
REM 596 parameters refined using 0 restraints
END
WGHT 0.0651 0.4017
REM Instructions for potential hydrogen bonds
HTAB C7 O10_$2
HTAB C36 O14_$3
HTAB C44 O11_$4
REM Highest difference peak 0.701, deepest hole -0.656, 1-sigma level 0.093
Q1 1 1.1302 0.2598 0.7256 11.00000 0.05 0.70
Q2 1 0.7374 0.3013 0.8758 11.00000 0.05 0.63
Q3 1 1.3603 0.5197 0.9835 11.00000 0.05 0.62
Q4 1 0.8987 0.4858 0.5594 11.00000 0.05 0.62
Q5 1 0.8776 0.3571 0.5199 11.00000 0.05 0.61
;
_shelx_res_checksum 30600
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C C1 1.08876(9) 0.26717(5) 0.67740(8) 0.01280(19) Uani d 1 . .
C C2 1.16248(10) 0.24855(5) 0.77116(9) 0.0143(2) Uani d 1 . .
C C3 1.21656(10) 0.19627(6) 0.78313(9) 0.0168(2) Uani d 1 . .
H H3 1.265479 0.184681 0.846347 0.020 Uiso calc 1 . .
C C4 1.19921(11) 0.16026(6) 0.70187(10) 0.0181(2) Uani d 1 . .
H H4 1.236234 0.124227 0.710186 0.022 Uiso calc 1 . .
C C5 1.12871(11) 0.17703(6) 0.61019(9) 0.0172(2) Uani d 1 . .
H H5 1.116761 0.152104 0.555782 0.021 Uiso calc 1 . .
C C6 1.07372(10) 0.23083(5) 0.59571(9) 0.01344(19) Uani d 1 . .
C C7 1.01093(10) 0.24828(5) 0.49648(9) 0.0143(2) Uani d 1 . .
H H7 1.006415 0.221706 0.445933 0.017 Uiso calc 1 . .
C C8 0.90690(9) 0.31284(5) 0.37006(8) 0.01228(19) Uani d 1 . .
C C9 0.89805(10) 0.27744(6) 0.29048(9) 0.0158(2) Uani d 1 . .
H H9 0.929948 0.239845 0.301535 0.019 Uiso calc 1 . .
C C10 0.84288(11) 0.29712(6) 0.19561(9) 0.0177(2) Uani d 1 . .
H H10 0.838676 0.273414 0.141756 0.021 Uiso calc 1 . .
C C11 0.79343(11) 0.35170(6) 0.17892(9) 0.0180(2) Uani d 1 . .
H H11 0.753453 0.364358 0.113722 0.022 Uiso calc 1 . .
C C12 0.80232(10) 0.38753(6) 0.25697(9) 0.0165(2) Uani d 1 . .
H H12 0.768362 0.424589 0.245216 0.020 Uiso calc 1 . .
C C13 0.86130(9) 0.36908(5) 0.35292(8) 0.01261(19) Uani d 1 . .
C C14 0.86585(9) 0.45908(5) 0.43142(8) 0.01299(19) Uani d 1 . .
H H14 0.842477 0.476080 0.368075 0.016 Uiso calc 1 . .
C C15 0.88340(9) 0.49758(5) 0.51263(9) 0.01227(19) Uani d 1 . .
C C16 0.85687(10) 0.55718(5) 0.49079(9) 0.0149(2) Uani d 1 . .
H H16 0.828358 0.569966 0.424586 0.018 Uiso calc 1 . .
C C17 0.87220(10) 0.59651(5) 0.56485(10) 0.0171(2) Uani d 1 . .
H H17 0.853918 0.636313 0.549479 0.020 Uiso calc 1 . .
C C18 0.91454(10) 0.57844(6) 0.66279(10) 0.0179(2) Uani d 1 . .
H H18 0.924599 0.605938 0.713507 0.021 Uiso calc 1 . .
C C19 0.94174(10) 0.52068(5) 0.68585(9) 0.0159(2) Uani d 1 . .
C C20 0.92776(9) 0.47886(5) 0.61106(9) 0.01308(19) Uani d 1 . .
C C21 1.24369(11) 0.27202(6) 0.94121(9) 0.0186(2) Uani d 1 . .
H H21A 1.315565 0.264844 0.943232 0.028 Uiso calc 1 . .
H H21B 1.217041 0.236589 0.960896 0.028 Uiso calc 1 . .
H H21C 1.246519 0.303823 0.986232 0.028 Uiso calc 1 . .
C C22 0.99273(16) 0.53626(7) 0.85697(11) 0.0332(4) Uani d 1 . .
H H22A 1.024290 0.515325 0.919384 0.050 Uiso calc 1 . .
H H22B 0.921502 0.550476 0.847949 0.050 Uiso calc 1 . .
H H22C 1.038435 0.569379 0.857384 0.050 Uiso calc 1 . .
C C23 0.52840(9) 0.25172(5) 0.44578(8) 0.01176(18) Uani d 1 . .
C C24 0.46778(9) 0.22290(5) 0.35609(8) 0.01268(19) Uani d 1 . .
C C25 0.43012(11) 0.16688(6) 0.35462(9) 0.0172(2) Uani d 1 . .
H H25 0.390311 0.148472 0.293762 0.021 Uiso calc 1 . .
C C26 0.45041(12) 0.13691(6) 0.44277(10) 0.0194(2) Uani d 1 . .
H H26 0.425375 0.098106 0.441344 0.023 Uiso calc 1 . .
C C27 0.50633(11) 0.16367(6) 0.53081(9) 0.0169(2) Uani d 1 . .
H H27 0.518748 0.143494 0.590172 0.020 Uiso calc 1 . .
C C28 0.54589(9) 0.22136(5) 0.53402(8) 0.01287(19) Uani d 1 . .
C C29 0.59648(9) 0.24760(5) 0.62881(8) 0.01302(19) Uani d 1 . .
H H29 0.599779 0.225325 0.683861 0.016 Uiso calc 1 . .
C C30 0.68372(9) 0.32289(5) 0.74144(8) 0.01303(19) Uani d 1 . .
C C31 0.70575(10) 0.29133(6) 0.82799(9) 0.0170(2) Uani d 1 . .
H H31 0.688947 0.250992 0.825223 0.020 Uiso calc 1 . .
C C32 0.75210(11) 0.31921(7) 0.91752(9) 0.0213(3) Uani d 1 . .
H H32 0.766979 0.297903 0.976298 0.026 Uiso calc 1 . .
C C33 0.77717(12) 0.37847(7) 0.92208(9) 0.0236(3) Uani d 1 . .
H H33 0.809004 0.397159 0.983975 0.028 Uiso calc 1 . .
C C34 0.75600(11) 0.41032(6) 0.83700(9) 0.0197(2) Uani d 1 . .
H H34 0.773706 0.450562 0.840548 0.024 Uiso calc 1 . .
C C35 0.70840(10) 0.38273(5) 0.74597(8) 0.0142(2) Uani d 1 . .
C C36 0.66511(9) 0.46648(5) 0.64641(9) 0.0137(2) Uani d 1 . .
H H36 0.669278 0.486802 0.703553 0.016 Uiso calc 1 . .
C C37 0.63824(9) 0.49964(5) 0.55805(9) 0.01299(19) Uani d 1 . .
C C38 0.61599(10) 0.55999(5) 0.56164(10) 0.0161(2) Uani d 1 . .
H H38 0.620872 0.576832 0.621696 0.019 Uiso calc 1 . .
C C39 0.58763(10) 0.59411(5) 0.47960(10) 0.0173(2) Uani d 1 . .
H H39 0.572358 0.634290 0.482858 0.021 Uiso calc 1 . .
C C40 0.58109(10) 0.56966(5) 0.39037(10) 0.0165(2) Uani d 1 . .
H H40 0.561737 0.593468 0.333634 0.020 Uiso calc 1 . .
C C41 0.60270(9) 0.51128(5) 0.38511(9) 0.0138(2) Uani d 1 . .
C C42 0.62963(9) 0.47407(5) 0.46857(9) 0.01229(19) Uani d 1 . .
C C43 0.38309(10) 0.23312(6) 0.18210(9) 0.0171(2) Uani d 1 . .
H H43A 0.372500 0.262585 0.131329 0.026 Uiso calc 1 . .
H H43B 0.313892 0.222924 0.183858 0.026 Uiso calc 1 . .
H H43C 0.415559 0.198218 0.167304 0.026 Uiso calc 1 . .
C C44 0.57068(12) 0.51586(6) 0.21474(10) 0.0216(3) Uani d 1 . .
H H44A 0.567734 0.489983 0.161224 0.032 Uiso calc 1 . .
H H44B 0.623386 0.546720 0.223027 0.032 Uiso calc 1 . .
H H44C 0.500134 0.533374 0.199164 0.032 Uiso calc 1 . .
Fe Fe1 0.92344(2) 0.35310(2) 0.56529(2) 0.01038(4) Uani d 1 . .
Fe Fe2 0.66903(2) 0.35162(2) 0.54108(2) 0.00972(4) Uani d 1 . .
N N1 0.95992(8) 0.29733(4) 0.47026(7) 0.01231(17) Uani d 1 . .
N N2 0.87934(8) 0.40288(4) 0.43754(7) 0.01174(17) Uani d 1 . .
N N3 0.63825(8) 0.29959(4) 0.64536(7) 0.01168(16) Uani d 1 . .
N N4 0.68429(8) 0.41050(4) 0.65444(7) 0.01255(17) Uani d 1 . .
O O1 1.17380(8) 0.28770(4) 0.84418(6) 0.01919(18) Uani d 1 . .
O O2 1.04159(7) 0.31752(4) 0.67200(6) 0.01700(17) Uani d 1 . .
O O3 0.95949(8) 0.42490(4) 0.63837(6) 0.01651(17) Uani d 1 . .
O O4 0.98394(9) 0.49786(4) 0.77871(7) 0.0236(2) Uani d 1 . .
O O5 0.45184(7) 0.25582(4) 0.27481(6) 0.01544(16) Uani d 1 . .
O O6 0.56115(7) 0.30521(4) 0.44185(6) 0.01348(15) Uani d 1 . .
O O7 0.64462(7) 0.41871(4) 0.45718(6) 0.01361(15) Uani d 1 . .
O O8 0.60097(8) 0.48307(4) 0.30340(7) 0.01774(17) Uani d 1 . .
O O9 0.79937(7) 0.32477(4) 0.56055(6) 0.01312(15) Uani d 1 . .
O O10 1.01072(10) 0.37077(5) 0.84647(8) 0.0260(2) Uani d 1 . .
H H10A 1.033811 0.344794 0.816773 0.039 Uiso d 1 . .
H H10B 0.989409 0.399583 0.805018 0.039 Uiso d 1 . .
O O11 1.19078(9) 0.42012(6) 0.76496(9) 0.0321(3) Uani d 1 . .
H H11A 1.124104 0.426667 0.727741 0.048 Uiso d 1 . .
H H11B 1.194509 0.382485 0.773752 0.048 Uiso d 1 . .
O O12 1.19790(12) 0.43386(7) 0.96466(9) 0.0438(3) Uani d 1 . .
H H12A 1.135376 0.418501 0.932145 0.066 Uiso d 1 . .
H H12B 1.221847 0.442892 0.920136 0.066 Uiso d 1 . .
O O13 0.51035(11) 0.37150(5) 0.25280(8) 0.0295(3) Uani d 1 . .
H H13A 0.502313 0.343602 0.288940 0.044 Uiso d 1 . .
H H13B 0.552296 0.396394 0.294381 0.044 Uiso d 1 . .
O O14 0.33696(10) 0.45164(5) 0.16404(9) 0.0301(2) Uani d 1 . .
H H14A 0.303822 0.446857 0.101121 0.045 Uiso d 1 . .
H H14B 0.385680 0.424467 0.182002 0.045 Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
C1 0.0127(4) 0.0134(5) 0.0128(5) 0.0020(4) 0.0055(4) 0.0002(4)
C2 0.0140(5) 0.0171(5) 0.0122(5) 0.0019(4) 0.0054(4) 0.0004(4)
C3 0.0170(5) 0.0182(5) 0.0163(5) 0.0034(4) 0.0076(4) 0.0042(4)
C4 0.0218(6) 0.0149(5) 0.0203(6) 0.0039(4) 0.0112(5) 0.0034(4)
C5 0.0227(6) 0.0135(5) 0.0180(5) 0.0035(4) 0.0108(5) 0.0008(4)
C6 0.0145(5) 0.0142(5) 0.0129(5) 0.0009(4) 0.0069(4) 0.0002(4)
C7 0.0170(5) 0.0137(5) 0.0137(5) -0.0001(4) 0.0076(4) -0.0012(4)
C8 0.0134(4) 0.0145(5) 0.0099(4) -0.0012(4) 0.0055(4) -0.0012(4)
C9 0.0180(5) 0.0165(5) 0.0134(5) -0.0001(4) 0.0067(4) -0.0029(4)
C10 0.0204(6) 0.0214(6) 0.0110(5) -0.0031(4) 0.0059(4) -0.0036(4)
C11 0.0194(5) 0.0224(6) 0.0105(5) -0.0018(4) 0.0042(4) -0.0001(4)
C12 0.0188(5) 0.0175(5) 0.0117(5) -0.0003(4) 0.0045(4) 0.0004(4)
C13 0.0132(5) 0.0146(5) 0.0106(4) -0.0016(4) 0.0053(4) -0.0016(4)
C14 0.0124(4) 0.0146(5) 0.0125(5) 0.0000(4) 0.0054(4) 0.0006(4)
C15 0.0111(4) 0.0125(5) 0.0142(5) -0.0008(4) 0.0060(4) -0.0013(4)
C16 0.0138(5) 0.0137(5) 0.0182(5) 0.0001(4) 0.0076(4) 0.0007(4)
C17 0.0171(5) 0.0133(5) 0.0225(6) 0.0003(4) 0.0095(5) -0.0010(4)
C18 0.0188(5) 0.0156(5) 0.0203(6) 0.0000(4) 0.0089(5) -0.0041(4)
C19 0.0165(5) 0.0153(5) 0.0148(5) 0.0000(4) 0.0051(4) -0.0037(4)
C20 0.0123(4) 0.0122(5) 0.0149(5) -0.0004(4) 0.0055(4) -0.0019(4)
C21 0.0178(5) 0.0251(6) 0.0114(5) 0.0030(5) 0.0040(4) 0.0026(4)
C22 0.0543(11) 0.0246(7) 0.0157(6) 0.0062(7) 0.0085(7) -0.0060(5)
C23 0.0125(4) 0.0116(4) 0.0118(4) -0.0001(4) 0.0055(4) -0.0001(4)
C24 0.0153(5) 0.0124(5) 0.0114(4) -0.0004(4) 0.0064(4) -0.0009(4)
C25 0.0226(6) 0.0138(5) 0.0157(5) -0.0038(4) 0.0082(4) -0.0026(4)
C26 0.0280(6) 0.0132(5) 0.0179(5) -0.0043(4) 0.0100(5) -0.0011(4)
C27 0.0234(6) 0.0136(5) 0.0147(5) -0.0017(4) 0.0088(4) 0.0017(4)
C28 0.0145(5) 0.0132(5) 0.0116(4) -0.0002(4) 0.0058(4) 0.0002(4)
C29 0.0141(5) 0.0143(5) 0.0111(4) 0.0013(4) 0.0055(4) 0.0026(4)
C30 0.0124(4) 0.0177(5) 0.0095(4) 0.0008(4) 0.0049(4) 0.0002(4)
C31 0.0177(5) 0.0229(6) 0.0113(5) 0.0005(4) 0.0067(4) 0.0024(4)
C32 0.0237(6) 0.0307(7) 0.0092(5) -0.0010(5) 0.0062(4) 0.0017(5)
C33 0.0274(7) 0.0312(7) 0.0106(5) -0.0046(6) 0.0055(5) -0.0031(5)
C34 0.0232(6) 0.0222(6) 0.0123(5) -0.0044(5) 0.0054(4) -0.0033(4)
C35 0.0140(5) 0.0185(5) 0.0105(4) 0.0002(4) 0.0053(4) -0.0003(4)
C36 0.0131(5) 0.0153(5) 0.0135(5) -0.0014(4) 0.0061(4) -0.0026(4)
C37 0.0115(4) 0.0125(5) 0.0154(5) -0.0009(4) 0.0057(4) -0.0017(4)
C38 0.0146(5) 0.0134(5) 0.0212(6) -0.0012(4) 0.0081(4) -0.0036(4)
C39 0.0151(5) 0.0123(5) 0.0250(6) -0.0006(4) 0.0085(5) -0.0011(4)
C40 0.0152(5) 0.0131(5) 0.0216(6) 0.0006(4) 0.0075(4) 0.0039(4)
C41 0.0135(5) 0.0127(5) 0.0157(5) -0.0010(4) 0.0062(4) 0.0010(4)
C42 0.0112(4) 0.0111(5) 0.0150(5) -0.0006(3) 0.0057(4) 0.0005(4)
C43 0.0179(5) 0.0214(6) 0.0106(5) -0.0021(4) 0.0042(4) -0.0030(4)
C44 0.0274(7) 0.0201(6) 0.0177(6) -0.0007(5) 0.0095(5) 0.0065(5)
Fe1 0.01062(7) 0.01160(7) 0.00918(7) 0.00124(5) 0.00416(5) -0.00053(5)
Fe2 0.01054(7) 0.01061(7) 0.00868(7) -0.00008(5) 0.00452(5) 0.00020(5)
N1 0.0128(4) 0.0142(4) 0.0109(4) 0.0003(3) 0.0056(3) -0.0008(3)
N2 0.0119(4) 0.0137(4) 0.0099(4) -0.0004(3) 0.0046(3) -0.0015(3)
N3 0.0117(4) 0.0147(4) 0.0091(4) -0.0003(3) 0.0045(3) -0.0001(3)
N4 0.0130(4) 0.0142(4) 0.0108(4) -0.0005(3) 0.0050(3) -0.0007(3)
O1 0.0199(4) 0.0220(5) 0.0120(4) 0.0066(3) 0.0023(3) -0.0010(3)
O2 0.0167(4) 0.0185(4) 0.0124(4) 0.0071(3) 0.0021(3) -0.0019(3)
O3 0.0212(4) 0.0133(4) 0.0125(4) 0.0016(3) 0.0039(3) -0.0011(3)
O4 0.0348(6) 0.0193(5) 0.0120(4) 0.0060(4) 0.0042(4) -0.0036(3)
O5 0.0195(4) 0.0157(4) 0.0092(3) -0.0034(3) 0.0037(3) -0.0003(3)
O6 0.0165(4) 0.0121(4) 0.0108(3) -0.0029(3) 0.0043(3) 0.0008(3)
O7 0.0183(4) 0.0111(4) 0.0130(4) 0.0019(3) 0.0077(3) 0.0009(3)
O8 0.0267(5) 0.0136(4) 0.0138(4) 0.0006(3) 0.0089(3) 0.0034(3)
O9 0.0125(4) 0.0141(4) 0.0141(4) 0.0020(3) 0.0067(3) 0.0027(3)
O10 0.0333(6) 0.0250(5) 0.0253(5) 0.0070(4) 0.0174(5) 0.0052(4)
O11 0.0225(5) 0.0417(7) 0.0297(6) -0.0074(5) 0.0078(5) 0.0043(5)
O12 0.0428(8) 0.0570(9) 0.0246(6) -0.0005(7) 0.0058(6) 0.0004(6)
O13 0.0514(7) 0.0186(5) 0.0158(4) -0.0107(5) 0.0103(5) -0.0012(4)
O14 0.0358(6) 0.0269(6) 0.0267(5) -0.0038(5) 0.0116(5) -0.0049(4)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-1 0 0 0.0100
1 0 0 0.0100
0 -1 0 0.0700
0 1 0 0.0600
1 -2 -2 0.0850
1 2 -2 0.0750
-1 0 2 0.0400
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C6 C1 C2 . . 117.96(11) ?
O2 C1 C2 . . 117.67(10) ?
O2 C1 C6 . . 124.34(10) ?
C3 C2 C1 . . 121.37(11) ?
O1 C2 C1 . . 113.20(10) ?
O1 C2 C3 . . 125.42(11) ?
C2 C3 H3 . . 120.0 ?
C2 C3 C4 . . 119.98(11) ?
C4 C3 H3 . . 120.0 ?
C3 C4 H4 . . 119.9 ?
C5 C4 C3 . . 120.13(12) ?
C5 C4 H4 . . 119.9 ?
C4 C5 H5 . . 119.5 ?
C4 C5 C6 . . 121.00(12) ?
C6 C5 H5 . . 119.5 ?
C1 C6 C7 . . 122.68(11) ?
C5 C6 C1 . . 119.53(11) ?
C5 C6 C7 . . 117.61(11) ?
C6 C7 H7 . . 117.3 ?
N1 C7 C6 . . 125.44(11) ?
N1 C7 H7 . . 117.3 ?
C9 C8 C13 . . 119.53(10) ?
C9 C8 N1 . . 125.39(11) ?
C13 C8 N1 . . 115.09(10) ?
C8 C9 H9 . . 119.9 ?
C10 C9 C8 . . 120.12(12) ?
C10 C9 H9 . . 119.9 ?
C9 C10 H10 . . 119.9 ?
C9 C10 C11 . . 120.19(12) ?
C11 C10 H10 . . 119.9 ?
C10 C11 H11 . . 119.8 ?
C12 C11 C10 . . 120.37(11) ?
C12 C11 H11 . . 119.8 ?
C11 C12 H12 . . 120.0 ?
C11 C12 C13 . . 119.93(12) ?
C13 C12 H12 . . 120.0 ?
C8 C13 N2 . . 115.54(10) ?
C12 C13 C8 . . 119.74(11) ?
C12 C13 N2 . . 124.71(11) ?
C15 C14 H14 . . 117.3 ?
N2 C14 H14 . . 117.3 ?
N2 C14 C15 . . 125.35(11) ?
C16 C15 C14 . . 117.21(11) ?
C20 C15 C14 . . 122.99(10) ?
C20 C15 C16 . . 119.78(11) ?
C15 C16 H16 . . 119.8 ?
C17 C16 C15 . . 120.34(12) ?
C17 C16 H16 . . 119.8 ?
C16 C17 H17 . . 119.7 ?
C16 C17 C18 . . 120.55(12) ?
C18 C17 H17 . . 119.7 ?
C17 C18 H18 . . 119.9 ?
C19 C18 C17 . . 120.12(12) ?
C19 C18 H18 . . 119.9 ?
C18 C19 C20 . . 120.83(12) ?
O4 C19 C18 . . 125.46(11) ?
O4 C19 C20 . . 113.71(11) ?
C15 C20 C19 . . 118.36(11) ?
O3 C20 C15 . . 123.91(11) ?
O3 C20 C19 . . 117.71(11) ?
H21A C21 H21B . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
O1 C21 H21A . . 109.5 ?
O1 C21 H21B . . 109.5 ?
O1 C21 H21C . . 109.5 ?
H22A C22 H22B . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
O4 C22 H22A . . 109.5 ?
O4 C22 H22B . . 109.5 ?
O4 C22 H22C . . 109.5 ?
C28 C23 C24 . . 117.46(10) ?
O6 C23 C24 . . 118.26(10) ?
O6 C23 C28 . . 124.23(10) ?
C25 C24 C23 . . 121.45(11) ?
O5 C24 C23 . . 113.70(10) ?
O5 C24 C25 . . 124.86(11) ?
C24 C25 H25 . . 119.8 ?
C24 C25 C26 . . 120.31(11) ?
C26 C25 H25 . . 119.8 ?
C25 C26 H26 . . 120.0 ?
C27 C26 C25 . . 120.02(12) ?
C27 C26 H26 . . 120.0 ?
C26 C27 H27 . . 119.7 ?
C26 C27 C28 . . 120.58(11) ?
C28 C27 H27 . . 119.7 ?
C23 C28 C27 . . 120.14(11) ?
C23 C28 C29 . . 122.82(11) ?
C27 C28 C29 . . 116.91(10) ?
C28 C29 H29 . . 117.5 ?
N3 C29 C28 . . 125.10(11) ?
N3 C29 H29 . . 117.5 ?
C31 C30 C35 . . 119.93(11) ?
C31 C30 N3 . . 125.43(11) ?
C35 C30 N3 . . 114.64(10) ?
C30 C31 H31 . . 120.2 ?
C32 C31 C30 . . 119.66(13) ?
C32 C31 H31 . . 120.2 ?
C31 C32 H32 . . 119.8 ?
C31 C32 C33 . . 120.44(12) ?
C33 C32 H32 . . 119.8 ?
C32 C33 H33 . . 119.7 ?
C34 C33 C32 . . 120.60(12) ?
C34 C33 H33 . . 119.7 ?
C33 C34 H34 . . 120.2 ?
C33 C34 C35 . . 119.52(13) ?
C35 C34 H34 . . 120.2 ?
C30 C35 N4 . . 115.56(10) ?
C34 C35 C30 . . 119.85(11) ?
C34 C35 N4 . . 124.57(11) ?
C37 C36 H36 . . 117.5 ?
N4 C36 H36 . . 117.5 ?
N4 C36 C37 . . 125.07(11) ?
C38 C37 C36 . . 117.59(11) ?
C42 C37 C36 . . 122.47(10) ?
C42 C37 C38 . . 119.90(11) ?
C37 C38 H38 . . 119.6 ?
C39 C38 C37 . . 120.82(12) ?
C39 C38 H38 . . 119.6 ?
C38 C39 H39 . . 120.0 ?
C38 C39 C40 . . 120.04(12) ?
C40 C39 H39 . . 120.0 ?
C39 C40 H40 . . 119.9 ?
C41 C40 C39 . . 120.23(12) ?
C41 C40 H40 . . 119.9 ?
C40 C41 C42 . . 121.20(11) ?
O8 C41 C40 . . 125.45(11) ?
O8 C41 C42 . . 113.35(10) ?
C37 C42 C41 . . 117.75(10) ?
O7 C42 C37 . . 124.38(11) ?
O7 C42 C41 . . 117.87(11) ?
H43A C43 H43B . . 109.5 ?
H43A C43 H43C . . 109.5 ?
H43B C43 H43C . . 109.5 ?
O5 C43 H43A . . 109.5 ?
O5 C43 H43B . . 109.5 ?
O5 C43 H43C . . 109.5 ?
H44A C44 H44B . . 109.5 ?
H44A C44 H44C . . 109.5 ?
H44B C44 H44C . . 109.5 ?
O8 C44 H44A . . 109.5 ?
O8 C44 H44B . . 109.5 ?
O8 C44 H44C . . 109.5 ?
N2 Fe1 N1 . . 77.43(4) ?
O2 Fe1 N1 . . 87.35(4) ?
O2 Fe1 N2 . . 145.27(4) ?
O3 Fe1 N1 . . 145.37(4) ?
O3 Fe1 N2 . . 87.87(4) ?
O3 Fe1 O2 . . 87.38(4) ?
O9 Fe1 N1 . . 102.80(4) ?
O9 Fe1 N2 . . 103.56(4) ?
O9 Fe1 O2 . . 110.23(4) ?
O9 Fe1 O3 . . 111.13(4) ?
N4 Fe2 N3 . . 76.28(4) ?
O6 Fe2 N3 . . 86.45(4) ?
O6 Fe2 N4 . . 140.16(4) ?
O7 Fe2 N3 . . 152.65(4) ?
O7 Fe2 N4 . . 86.70(4) ?
O7 Fe2 O6 . . 93.50(4) ?
O9 Fe2 N3 . . 98.98(4) ?
O9 Fe2 N4 . . 108.21(4) ?
O9 Fe2 O6 . . 109.82(4) ?
O9 Fe2 O7 . . 106.68(4) ?
C7 N1 C8 . . 121.48(10) ?
C7 N1 Fe1 . . 124.40(8) ?
C8 N1 Fe1 . . 113.22(7) ?
C13 N2 Fe1 . . 113.26(8) ?
C14 N2 C13 . . 120.76(10) ?
C14 N2 Fe1 . . 125.96(8) ?
C29 N3 C30 . . 121.35(10) ?
C29 N3 Fe2 . . 125.02(8) ?
C30 N3 Fe2 . . 112.90(7) ?
C35 N4 Fe2 . . 113.05(8) ?
C36 N4 C35 . . 119.45(10) ?
C36 N4 Fe2 . . 127.21(8) ?
C2 O1 C21 . . 117.22(10) ?
C1 O2 Fe1 . . 130.60(8) ?
C20 O3 Fe1 . . 130.40(8) ?
C19 O4 C22 . . 116.84(11) ?
C24 O5 C43 . . 117.86(10) ?
C23 O6 Fe2 . . 130.35(7) ?
C42 O7 Fe2 . . 133.51(8) ?
C41 O8 C44 . . 117.82(10) ?
Fe1 O9 Fe2 . . 137.97(5) ?
H10A O10 H10B . . 104.3 ?
H11A O11 H11B . . 104.5 ?
H12A O12 H12B . . 104.6 ?
H13A O13 H13B . . 104.6 ?
H14A O14 H14B . . 104.4 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
C1 C2 . 1.4235(16) ?
C1 C6 . 1.4187(16) ?
C1 O2 . 1.3080(14) ?
C2 C3 . 1.3810(17) ?
C2 O1 . 1.3690(15) ?
C3 H3 . 0.9500 ?
C3 C4 . 1.4035(19) ?
C4 H4 . 0.9500 ?
C4 C5 . 1.3756(18) ?
C5 H5 . 0.9500 ?
C5 C6 . 1.4147(17) ?
C6 C7 . 1.4385(17) ?
C7 H7 . 0.9500 ?
C7 N1 . 1.2983(16) ?
C8 C9 . 1.3994(16) ?
C8 C13 . 1.4102(17) ?
C8 N1 . 1.4196(15) ?
C9 H9 . 0.9500 ?
C9 C10 . 1.3851(17) ?
C10 H10 . 0.9500 ?
C10 C11 . 1.3961(19) ?
C11 H11 . 0.9500 ?
C11 C12 . 1.3867(18) ?
C12 H12 . 0.9500 ?
C12 C13 . 1.3972(16) ?
C13 N2 . 1.4132(15) ?
C14 H14 . 0.9500 ?
C14 C15 . 1.4367(16) ?
C14 N2 . 1.3000(16) ?
C15 C16 . 1.4184(17) ?
C15 C20 . 1.4107(17) ?
C16 H16 . 0.9500 ?
C16 C17 . 1.3733(18) ?
C17 H17 . 0.9500 ?
C17 C18 . 1.3996(19) ?
C18 H18 . 0.9500 ?
C18 C19 . 1.3817(18) ?
C19 C20 . 1.4224(17) ?
C19 O4 . 1.3716(16) ?
C20 O3 . 1.3208(15) ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C21 O1 . 1.4248(15) ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C22 O4 . 1.4252(17) ?
C23 C24 . 1.4231(16) ?
C23 C28 . 1.4187(16) ?
C23 O6 . 1.3143(14) ?
C24 C25 . 1.3801(17) ?
C24 O5 . 1.3667(14) ?
C25 H25 . 0.9500 ?
C25 C26 . 1.4064(18) ?
C26 H26 . 0.9500 ?
C26 C27 . 1.3715(18) ?
C27 H27 . 0.9500 ?
C27 C28 . 1.4219(17) ?
C28 C29 . 1.4332(16) ?
C29 H29 . 0.9500 ?
C29 N3 . 1.3017(16) ?
C30 C31 . 1.4008(17) ?
C30 C35 . 1.4081(18) ?
C30 N3 . 1.4173(15) ?
C31 H31 . 0.9500 ?
C31 C32 . 1.3833(18) ?
C32 H32 . 0.9500 ?
C32 C33 . 1.396(2) ?
C33 H33 . 0.9500 ?
C33 C34 . 1.3878(19) ?
C34 H34 . 0.9500 ?
C34 C35 . 1.3991(17) ?
C35 N4 . 1.4175(15) ?
C36 H36 . 0.9500 ?
C36 C37 . 1.4339(17) ?
C36 N4 . 1.3061(16) ?
C37 C38 . 1.4221(17) ?
C37 C42 . 1.4144(17) ?
C38 H38 . 0.9500 ?
C38 C39 . 1.3694(18) ?
C39 H39 . 0.9500 ?
C39 C40 . 1.4090(19) ?
C40 H40 . 0.9500 ?
C40 C41 . 1.3798(17) ?
C41 C42 . 1.4285(17) ?
C41 O8 . 1.3671(15) ?
C42 O7 . 1.3075(14) ?
C43 H43A . 0.9800 ?
C43 H43B . 0.9800 ?
C43 H43C . 0.9800 ?
C43 O5 . 1.4236(14) ?
C44 H44A . 0.9800 ?
C44 H44B . 0.9800 ?
C44 H44C . 0.9800 ?
C44 O8 . 1.4288(15) ?
Fe1 N1 . 2.1035(10) y
Fe1 N2 . 2.0893(10) y
Fe1 O2 . 1.9373(9) y
Fe1 O3 . 1.9262(9) y
Fe1 O9 . 1.7835(9) y
Fe2 N3 . 2.1232(10) y
Fe2 N4 . 2.1036(10) y
Fe2 O6 . 1.9374(8) y
Fe2 O7 . 1.9246(9) y
Fe2 O9 . 1.7893(8) y
O10 H10A . 0.8701 ?
O10 H10B . 0.8712 ?
O11 H11A . 0.8692 ?
O11 H11B . 0.8713 ?
O12 H12A . 0.8699 ?
O12 H12B . 0.8693 ?
O13 H13A . 0.8693 ?
O13 H13B . 0.8689 ?
O14 H14A . 0.8697 ?
O14 H14B . 0.8713 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C7 H7 O10 4_565 0.95 2.60 3.5233(16) 164.6 yes
C36 H36 O14 3_666 0.95 2.45 3.3930(17) 172.4 yes
C44 H44B O11 3_766 0.98 2.58 3.4643(19) 150.5 yes
O10 H10A O1 . 0.87 2.21 2.9342(15) 140.2 yes
O10 H10A O2 . 0.87 2.28 3.0393(14) 145.6 yes
O10 H10B O3 . 0.87 2.42 3.1432(14) 141.4 yes
O10 H10B O4 . 0.87 2.28 3.0579(15) 148.1 yes
O11 H11A O3 . 0.87 2.11 2.9635(15) 168.9 yes
O11 H11B O1 . 0.87 2.48 3.2974(16) 157.4 yes
O11 H11B O2 . 0.87 2.52 3.0582(15) 120.7 yes
O12 H12A O10 . 0.87 2.00 2.8520(19) 166.9 yes
O12 H12B O11 . 0.87 2.23 2.9457(19) 138.9 yes
O13 H13A O5 . 0.87 2.11 2.8255(14) 139.1 yes
O13 H13A O6 . 0.87 2.27 3.0237(13) 145.4 yes
O13 H13B O7 . 0.87 2.30 3.0580(14) 145.8 yes
O13 H13B O8 . 0.87 2.08 2.8108(14) 140.9 yes
O14 H14A O12 1_454 0.87 1.99 2.8457(17) 166.5 yes
O14 H14B O13 . 0.87 2.01 2.8683(18) 166.9 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C1 C2 C3 C4 . . . . -0.1(2) ?
C1 C2 O1 C21 . . . . 178.19(11) ?
C1 C6 C7 N1 . . . . -1.6(2) ?
C2 C1 C6 C5 . . . . 2.23(18) ?
C2 C1 C6 C7 . . . . -172.67(12) ?
C2 C1 O2 Fe1 . . . . -169.87(9) ?
C2 C3 C4 C5 . . . . 0.2(2) ?
C3 C2 O1 C21 . . . . -2.89(19) ?
C3 C4 C5 C6 . . . . 0.9(2) ?
C4 C5 C6 C1 . . . . -2.1(2) ?
C4 C5 C6 C7 . . . . 173.03(12) ?
C5 C6 C7 N1 . . . . -176.54(12) ?
C6 C1 C2 C3 . . . . -1.17(18) ?
C6 C1 C2 O1 . . . . 177.79(11) ?
C6 C1 O2 Fe1 . . . . 12.13(19) ?
C6 C7 N1 C8 . . . . 174.88(11) ?
C6 C7 N1 Fe1 . . . . -16.72(18) ?
C8 C9 C10 C11 . . . . -1.7(2) ?
C8 C13 N2 C14 . . . . 162.34(11) ?
C8 C13 N2 Fe1 . . . . -19.29(13) ?
C9 C8 C13 C12 . . . . 3.85(18) ?
C9 C8 C13 N2 . . . . -176.60(11) ?
C9 C8 N1 C7 . . . . 3.76(18) ?
C9 C8 N1 Fe1 . . . . -165.84(10) ?
C9 C10 C11 C12 . . . . 2.3(2) ?
C10 C11 C12 C13 . . . . 0.2(2) ?
C11 C12 C13 C8 . . . . -3.25(19) ?
C11 C12 C13 N2 . . . . 177.25(12) ?
C12 C13 N2 C14 . . . . -18.13(18) ?
C12 C13 N2 Fe1 . . . . 160.24(10) ?
C13 C8 C9 C10 . . . . -1.37(18) ?
C13 C8 N1 C7 . . . . -175.78(11) ?
C13 C8 N1 Fe1 . . . . 14.62(13) ?
C14 C15 C16 C17 . . . . -179.59(11) ?
C14 C15 C20 C19 . . . . 179.96(11) ?
C14 C15 C20 O3 . . . . 1.53(18) ?
C15 C14 N2 C13 . . . . -179.02(11) ?
C15 C14 N2 Fe1 . . . . 2.83(17) ?
C15 C16 C17 C18 . . . . 0.26(19) ?
C15 C20 O3 Fe1 . . . . -19.60(18) ?
C16 C15 C20 C19 . . . . 1.76(17) ?
C16 C15 C20 O3 . . . . -176.67(11) ?
C16 C17 C18 C19 . . . . 0.2(2) ?
C17 C18 C19 C20 . . . . 0.3(2) ?
C17 C18 C19 O4 . . . . 179.85(13) ?
C18 C19 C20 C15 . . . . -1.27(18) ?
C18 C19 C20 O3 . . . . 177.26(12) ?
C18 C19 O4 C22 . . . . 5.0(2) ?
C19 C20 O3 Fe1 . . . . 161.96(9) ?
C20 C15 C16 C17 . . . . -1.28(18) ?
C20 C19 O4 C22 . . . . -175.42(13) ?
C23 C24 C25 C26 . . . . 0.5(2) ?
C23 C24 O5 C43 . . . . -173.78(11) ?
C23 C28 C29 N3 . . . . -5.11(19) ?
C24 C23 C28 C27 . . . . 1.92(17) ?
C24 C23 C28 C29 . . . . -173.76(11) ?
C24 C23 O6 Fe2 . . . . -164.34(8) ?
C24 C25 C26 C27 . . . . 1.1(2) ?
C25 C24 O5 C43 . . . . 6.24(18) ?
C25 C26 C27 C28 . . . . -1.1(2) ?
C26 C27 C28 C23 . . . . -0.4(2) ?
C26 C27 C28 C29 . . . . 175.50(13) ?
C27 C28 C29 N3 . . . . 179.08(12) ?
C28 C23 C24 C25 . . . . -1.96(18) ?
C28 C23 C24 O5 . . . . 178.06(10) ?
C28 C23 O6 Fe2 . . . . 18.26(18) ?
C28 C29 N3 C30 . . . . 177.92(11) ?
C28 C29 N3 Fe2 . . . . -12.57(17) ?
C30 C31 C32 C33 . . . . -0.1(2) ?
C30 C35 N4 C36 . . . . 154.03(11) ?
C30 C35 N4 Fe2 . . . . -20.17(13) ?
C31 C30 C35 C34 . . . . 0.74(18) ?
C31 C30 C35 N4 . . . . 179.21(11) ?
C31 C30 N3 C29 . . . . 11.48(18) ?
C31 C30 N3 Fe2 . . . . -159.20(10) ?
C31 C32 C33 C34 . . . . 0.0(2) ?
C32 C33 C34 C35 . . . . 0.5(2) ?
C33 C34 C35 C30 . . . . -0.8(2) ?
C33 C34 C35 N4 . . . . -179.16(13) ?
C34 C35 N4 C36 . . . . -27.58(18) ?
C34 C35 N4 Fe2 . . . . 158.22(11) ?
C35 C30 C31 C32 . . . . -0.26(19) ?
C35 C30 N3 C29 . . . . -169.33(11) ?
C35 C30 N3 Fe2 . . . . 19.99(12) ?
C36 C37 C38 C39 . . . . -178.65(11) ?
C36 C37 C42 C41 . . . . -179.83(11) ?
C36 C37 C42 O7 . . . . 0.22(19) ?
C37 C36 N4 C35 . . . . -179.01(11) ?
C37 C36 N4 Fe2 . . . . -5.72(18) ?
C37 C38 C39 C40 . . . . -0.56(19) ?
C37 C42 O7 Fe2 . . . . 6.29(18) ?
C38 C37 C42 C41 . . . . 2.55(17) ?
C38 C37 C42 O7 . . . . -177.41(11) ?
C38 C39 C40 C41 . . . . 0.30(19) ?
C39 C40 C41 C42 . . . . 1.44(18) ?
C39 C40 C41 O8 . . . . -178.67(12) ?
C40 C41 C42 C37 . . . . -2.84(17) ?
C40 C41 C42 O7 . . . . 177.12(11) ?
C40 C41 O8 C44 . . . . -2.36(18) ?
C41 C42 O7 Fe2 . . . . -173.67(8) ?
C42 C37 C38 C39 . . . . -0.91(18) ?
C42 C41 O8 C44 . . . . 177.53(11) ?
N1 C8 C9 C10 . . . . 179.10(12) ?
N1 C8 C13 C12 . . . . -176.57(11) ?
N1 C8 C13 N2 . . . . 2.98(15) ?
N1 Fe1 O9 Fe2 . . . . -129.67(7) ?
N2 C14 C15 C16 . . . . -175.49(11) ?
N2 C14 C15 C20 . . . . 6.27(19) ?
N2 Fe1 O9 Fe2 . . . . -49.74(8) ?
N3 C30 C31 C32 . . . . 178.89(12) ?
N3 C30 C35 C34 . . . . -178.50(11) ?
N3 C30 C35 N4 . . . . -0.02(15) ?
N3 Fe2 O9 Fe1 . . . . -141.18(7) ?
N4 C36 C37 C38 . . . . 177.73(12) ?
N4 C36 C37 C42 . . . . 0.06(19) ?
N4 Fe2 O9 Fe1 . . . . -62.77(8) ?
O1 C2 C3 C4 . . . . -178.89(12) ?
O2 C1 C2 C3 . . . . -179.31(12) ?
O2 C1 C2 O1 . . . . -0.35(17) ?
O2 C1 C6 C5 . . . . -179.77(12) ?
O2 C1 C6 C7 . . . . 5.33(19) ?
O2 Fe1 O9 Fe2 . . . . 138.43(7) ?
O3 Fe1 O9 Fe2 . . . . 43.26(8) ?
O4 C19 C20 C15 . . . . 179.11(11) ?
O4 C19 C20 O3 . . . . -2.36(17) ?
O5 C24 C25 C26 . . . . -179.53(12) ?
O6 C23 C24 C25 . . . . -179.54(12) ?
O6 C23 C24 O5 . . . . 0.47(16) ?
O6 C23 C28 C27 . . . . 179.34(12) ?
O6 C23 C28 C29 . . . . 3.66(19) ?
O6 Fe2 O9 Fe1 . . . . 129.37(7) ?
O7 Fe2 O9 Fe1 . . . . 29.25(8) ?
O8 C41 C42 C37 . . . . 177.26(10) ?
O8 C41 C42 O7 . . . . -2.78(16) ?