#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:00:52 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180899 $ #$URL: svn://www.crystallography.net/cod/hkl/2/10/39/2103937.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103937_Fobs loop_ _publ_author_name 'Salmer\'on-Valverde, Amparo' 'Bern\`es, Sylvain' 'Robles-Mart\'inez, Juan Gerardo' _publ_section_title ; Structure and degree of charge transfer of two polymorphs of a 1:1 molecular complex: [2,2'-bis-1,3-dithiole][9-dicyanomethylene-4,5,7-trinitrofluorene-2-carboxylic acid methyl ester] (TTF-MeDC2TNF) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 505 _journal_page_last 511 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.304 _cell_angle_gamma 90.000 _cell_length_a 6.7816 _cell_length_b 30.5723 _cell_length_c 12.4381 _exptl_crystal_F_000 1272.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file sn5000cdc2tnfsup2.hkl _cod_data_source_block cdc2tnf #BEGIN Tags that were not found in dictionaries: _shelx_title ' cdc2tnf in P2(1)/n LAST, para Acta B. Fase ordenada' _shelx_refln_list_code 4 _shelx_f_calc_maximum 652.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 426139.34 428497.84 1016.44 o 4 0 0 32731.03 32217.12 338.27 o 6 0 0 631.07 776.80 40.76 o 8 0 0 220.92 580.36 65.21 o 1 1 0 2.72 4.95 3.72 o 2 1 0 32090.36 32312.00 2026.76 o 3 1 0 147.80 91.78 22.01 o 4 1 0 20401.86 21855.29 249.02 o 5 1 0 449.41 450.42 19.83 o 6 1 0 6031.24 6046.46 93.07 o 7 1 0 139.72 203.35 28.17 o 8 1 0 1119.35 1055.59 46.01 o 1 2 0 774.40 804.19 18.99 o 2 2 0 0.48 88.85 14.67 o 3 2 0 4690.03 5096.05 134.49 o 5 2 0 104.83 152.43 26.90 o 7 2 0 21.73 64.39 30.16 o 8 2 0 1.82 165.47 44.02 o 1 3 0 29.22 27.18 13.86 o 2 3 0 221.42 160.58 16.30 o 3 3 0 63.24 64.39 14.67 o 4 3 0 866.08 963.46 40.76 o 5 3 0 145.69 174.43 20.38 o 6 3 0 550.91 722.19 35.05 o 7 3 0 25.52 32.60 25.27 o 8 3 0 128.72 141.01 41.57 o 1 4 0 484.75 439.16 36.68 o 2 4 0 22.14 35.05 12.23 o 3 4 0 382.32 398.59 22.82 o 4 4 0 91.45 100.26 18.75 o 5 4 0 30.42 32.60 16.30 o 6 4 0 23.96 34.23 20.38 o 7 4 0 21.13 52.17 39.13 o 1 5 0 1118.96 932.61 24.19 o 2 5 0 1782.48 1533.22 76.62 o 3 5 0 107.41 107.59 15.49 o 4 5 0 185.72 242.09 22.82 o 5 5 0 0.08 0.00 17.12 o 6 5 0 8.98 -0.82 21.19 o 7 5 0 0.04 -24.45 24.45 o 0 6 0 0.39 21.19 6.52 o 1 6 0 3511.90 3395.92 67.95 o 2 6 0 196.79 208.67 17.12 o 3 6 0 0.03 3.26 11.41 o 4 6 0 71.96 118.19 17.12 o 5 6 0 25.07 16.30 22.82 o 6 6 0 54.53 88.03 19.56 o 7 6 0 71.45 97.81 29.34 o 1 7 0 85.71 63.02 21.19 o 2 7 0 3447.53 2795.00 105.15 o 3 7 0 424.67 469.50 25.27 o 4 7 0 186.82 202.15 20.38 o 5 7 0 169.00 194.81 26.08 o 6 7 0 120.53 155.69 21.19 o 7 7 0 45.71 39.94 27.71 o 1 8 0 3533.13 3751.88 81.43 o 2 8 0 13460.53 13384.06 216.82 o 3 8 0 1317.85 1330.26 48.09 o 4 8 0 47.81 40.76 21.19 o 5 8 0 4.20 29.34 20.38 o 6 8 0 112.80 176.88 23.64 o 7 8 0 14.99 28.53 23.64 o 1 9 0 1665.18 1211.12 33.37 o 2 9 0 345.95 397.77 27.71 o 3 9 0 130.60 96.18 17.12 o 4 9 0 174.65 225.78 23.64 o 5 9 0 3.12 5.71 16.30 o 6 9 0 15.71 26.08 16.30 o 7 9 0 0.00 -8.15 26.08 o 0 10 0 2023.25 1598.43 60.32 o 1 10 0 2966.20 3039.31 131.23 o 2 10 0 1556.93 1520.99 57.06 o 3 10 0 854.83 806.96 33.42 o 4 10 0 3.21 17.93 22.01 o 5 10 0 2.88 21.19 17.12 o 6 10 0 66.83 124.71 23.64 o 7 10 0 13.59 14.67 24.45 o 1 11 0 28.80 -111.31 162.61 o 2 11 0 616.52 532.27 29.34 o 3 11 0 603.91 580.36 30.16 o 4 11 0 2116.82 1992.12 88.03 o 5 11 0 63.87 51.35 17.12 o 6 11 0 313.44 295.88 27.71 o 7 11 0 2.74 30.97 26.08 o 0 12 0 17157.17 16449.68 272.25 o 1 12 0 6653.96 6406.29 320.34 o 2 12 0 8033.52 8376.04 185.03 o 3 12 0 477.73 387.18 26.08 o 4 12 0 2119.96 2055.70 96.18 o 5 12 0 2.11 32.60 16.30 o 6 12 0 152.80 174.43 22.82 o 7 12 0 171.84 180.14 35.86 o 2 13 0 36.75 193.18 22.82 o 3 13 0 610.11 524.11 30.16 o 4 13 0 4.18 18.75 19.56 o 5 13 0 863.85 835.48 38.31 o 6 13 0 5.64 23.64 16.30 o 7 13 0 358.50 293.44 46.46 o 0 14 0 7107.51 7835.63 200.52 o 1 14 0 8136.03 8574.09 569.76 o 2 14 0 3934.35 4379.57 136.94 o 3 14 0 3819.24 3579.14 125.53 o 4 14 0 155.80 167.10 22.01 o 5 14 0 619.70 619.48 33.42 o 6 14 0 22.06 61.13 30.16 o 7 14 0 62.03 127.16 44.83 o 1 15 0 272.96 499.81 503.33 o 3 15 0 15.39 -17.12 17.12 o 4 15 0 2600.83 2596.93 96.18 o 5 15 0 89.39 141.01 28.53 o 6 15 0 392.47 457.28 44.02 o 7 15 0 114.90 116.56 35.05 o 0 16 0 161.73 126.34 15.49 o 1 16 0 167.52 118.28 30.57 o 2 16 0 105.57 98.63 21.19 o 3 16 0 22.61 13.04 12.23 o 4 16 0 68.31 81.51 25.27 o 5 16 0 81.92 102.70 22.82 o 6 16 0 1.31 -2.45 33.42 o 7 16 0 66.14 18.75 35.86 o 1 17 0 116.41 49.50 12.92 o 2 17 0 10.91 23.64 20.38 o 3 17 0 92.41 97.00 21.19 o 4 17 0 30.15 21.19 22.01 o 5 17 0 62.82 70.91 19.56 o 6 17 0 7.77 25.27 32.60 o 7 17 0 8.86 15.49 29.34 o 0 18 0 5043.50 4905.32 155.69 o 1 18 0 1629.93 1713.92 43.79 o 2 18 0 2281.38 2423.31 116.56 o 3 18 0 274.72 176.88 22.82 o 4 18 0 444.74 390.44 29.34 o 5 18 0 0.23 -13.86 15.49 o 6 18 0 46.95 28.53 30.97 o 1 19 0 14.83 -5.55 143.05 o 3 19 0 200.07 105.96 22.82 o 4 19 0 547.18 505.37 31.79 o 5 19 0 13.69 50.54 18.75 o 6 19 0 449.20 542.86 45.65 o 0 20 0 2367.98 2513.79 111.67 o 1 20 0 5464.61 5819.75 110.50 o 2 20 0 1468.49 1118.33 47.28 o 3 20 0 1684.54 1325.36 52.17 o 4 20 0 166.27 138.57 24.45 o 5 20 0 295.13 332.56 26.90 o 6 20 0 0.19 38.31 34.23 o 1 21 0 121.17 172.73 133.68 o 2 21 0 106.34 -28.53 28.53 o 4 21 0 19.02 -18.75 18.75 o 5 21 0 1011.02 893.36 58.69 o 6 21 0 0.28 -19.56 30.16 o 0 22 0 4472.49 4532.81 138.57 o 1 22 0 1227.19 1112.31 33.37 o 2 22 0 2367.74 1882.90 60.32 o 4 22 0 220.57 179.32 25.27 o 5 22 0 104.48 207.85 47.28 o 6 22 0 11.01 62.76 35.86 o 1 23 0 36.40 -31.59 40.76 o 2 23 0 1509.47 1091.43 63.58 o 3 23 0 6.57 -20.38 20.38 o 4 23 0 1606.18 1625.32 77.44 o 5 23 0 10.56 -11.41 32.60 o 6 23 0 609.61 701.81 61.13 o 0 24 0 5.48 15.49 19.56 o 1 24 0 1106.55 1126.16 70.91 o 2 24 0 7.51 57.87 31.79 o 3 24 0 691.35 573.84 35.86 o 4 24 0 2.81 -25.27 60.32 o 5 24 0 375.10 490.69 51.35 o 6 24 0 13.40 6.52 40.76 o 1 25 0 63.79 27.42 34.23 o 2 25 0 141.00 28.53 25.27 o 3 25 0 164.20 -39.94 39.94 o 4 25 0 529.17 658.61 52.98 o 5 25 0 35.98 103.52 42.39 o 0 26 0 1964.98 1948.11 81.51 o 1 26 0 173.50 172.46 16.82 o 2 26 0 1290.36 1371.83 52.17 o 3 26 0 9.72 -22.82 22.82 o 4 26 0 201.48 216.82 39.94 o 5 26 0 1.37 -13.04 21.19 o 1 27 0 5.30 -11.23 11.23 o 2 27 0 44.50 145.09 28.53 o 3 27 0 262.24 228.23 41.57 o 4 27 0 51.74 18.75 30.97 o 5 27 0 237.72 299.96 45.65 o 0 28 0 91.84 121.45 22.82 o 1 28 0 227.51 223.91 17.52 o 2 28 0 11.33 -0.82 15.49 o 3 28 0 16.00 -25.27 25.27 o 4 28 0 7.63 -9.78 21.19 o 5 28 0 33.96 12.23 39.13 o 1 29 0 0.01 -10.91 10.91 o 2 29 0 2.64 4.08 19.56 o 3 29 0 3.21 -14.67 22.01 o 4 29 0 38.31 -8.15 26.90 o 0 30 0 81.26 113.30 26.90 o 1 30 0 84.17 150.86 22.72 o 2 30 0 68.15 156.50 34.23 o 3 30 0 0.70 -5.71 19.56 o 4 30 0 19.90 50.54 26.08 o 1 31 0 0.72 -4.24 14.10 o 2 31 0 4.99 -13.86 17.93 o 3 31 0 2.91 -13.04 17.93 o 4 31 0 8.82 -6.52 21.19 o 0 32 0 5.73 4.08 24.45 o 1 32 0 389.30 560.27 33.63 o 2 32 0 14.65 -21.19 21.19 o 3 32 0 188.16 276.32 46.46 o 1 33 0 21.18 -16.33 19.58 o 2 33 0 119.87 83.96 50.54 o 3 33 0 109.77 -13.04 54.61 o 0 34 0 1578.30 2143.73 83.14 o 1 34 0 22.05 26.50 23.64 o 2 34 0 1101.27 1201.47 80.70 o 1 35 0 85.81 93.09 29.12 o 2 35 0 208.50 198.89 61.95 o 0 36 0 4.64 10.60 34.23 o 1 36 0 542.27 730.35 70.10 o -7 0 1 59.65 28.53 26.90 o -5 0 1 734.40 678.98 30.16 o -3 0 1 40.78 30.16 14.67 o -1 0 1 23.39 40.27 5.68 o 1 0 1 23.73 31.74 6.52 o 3 0 1 473.00 795.54 33.42 o 5 0 1 1.72 -1.63 15.49 o 7 0 1 118.39 111.67 37.49 o -7 1 1 48.27 92.41 22.72 o -6 1 1 6353.53 5628.10 89.59 o -5 1 1 3.05 -5.71 14.41 o -4 1 1 20277.04 18430.15 251.46 o -3 1 1 10.30 32.23 9.50 o -2 1 1 35983.37 32215.77 381.06 o -1 1 1 6631.83 6472.55 53.28 o 0 1 1 9223.83 9786.55 99.87 o 1 1 1 7675.99 7763.19 162.00 o 2 1 1 12501.82 12606.93 242.09 o 3 1 1 213.51 213.55 19.56 o 4 1 1 5187.07 5916.24 109.97 o 5 1 1 252.94 201.29 15.84 o 6 1 1 1098.14 1197.04 32.20 o 7 1 1 10.09 67.82 21.41 o -7 2 1 3.41 55.43 30.16 o -6 2 1 83.91 278.77 27.71 o -5 2 1 44.97 61.13 17.93 o -4 2 1 6915.03 6834.67 161.39 o -3 2 1 240.27 377.39 22.01 o -2 2 1 42704.37 38604.30 317.89 o -1 2 1 2.02 37.02 6.26 o 0 2 1 20081.22 20737.97 169.13 o 1 2 1 662.60 587.63 31.38 o 2 2 1 12009.85 11178.38 173.62 o 3 2 1 600.97 540.42 24.45 o 4 2 1 1299.49 1543.81 50.54 o 5 2 1 39.07 61.95 25.27 o 6 2 1 18.62 44.83 23.64 o 7 2 1 3.85 -15.49 30.97 o -7 3 1 62.16 56.24 33.42 o -6 3 1 994.59 1055.56 43.20 o -5 3 1 155.40 182.58 22.82 o -4 3 1 1359.60 1401.17 56.24 o -3 3 1 979.02 951.23 35.86 o -2 3 1 26.81 76.62 15.49 o -1 3 1 285.55 299.08 9.17 o 0 3 1 3955.94 3919.40 80.29 o 1 3 1 1000.23 1150.32 34.23 o 2 3 1 1.68 3.26 12.23 o 3 3 1 151.54 171.17 21.19 o 4 3 1 8.53 31.79 17.12 o 5 3 1 300.07 345.61 23.64 o 6 3 1 59.96 80.70 19.56 o 7 3 1 64.72 31.79 34.23 o -8 4 1 73.73 124.71 32.60 o -7 4 1 9.05 -2.45 26.90 o -6 4 1 648.97 754.79 33.42 o -5 4 1 0.05 15.49 19.56 o -4 4 1 2432.30 2638.50 101.89 o -3 4 1 363.20 417.33 21.19 o -2 4 1 4418.65 3852.20 111.67 o -1 4 1 393.20 542.67 37.90 o 0 4 1 30.64 65.22 5.45 o 1 4 1 4743.01 4774.89 132.86 o 2 4 1 3226.89 3343.57 103.52 o 3 4 1 446.50 425.49 22.82 o 4 4 1 658.09 670.02 30.97 o 5 4 1 584.46 551.01 29.34 o 6 4 1 204.08 163.84 23.64 o 7 4 1 64.03 54.61 27.71 o -7 5 1 14.47 -19.56 33.42 o -6 5 1 7.66 41.57 19.56 o -5 5 1 0.08 16.30 17.93 o -4 5 1 92.50 114.12 23.64 o -3 5 1 1239.41 1264.23 48.91 o -2 5 1 84.58 202.15 17.12 o -1 5 1 2210.46 1875.22 66.84 o 0 5 1 1519.01 1451.68 68.47 o 1 5 1 4580.34 4707.43 76.63 o 2 5 1 5002.75 4915.91 123.08 o 3 5 1 4307.67 4644.48 135.31 o 4 5 1 13.48 52.17 18.75 o 5 5 1 345.67 330.12 28.53 o 6 5 1 108.68 158.95 21.19 o 7 5 1 83.34 79.88 33.42 o -7 6 1 6.71 17.93 28.53 o -6 6 1 5.40 32.60 21.19 o -5 6 1 0.32 2.45 20.38 o -4 6 1 0.72 -14.67 14.67 o -3 6 1 8.98 44.02 19.56 o -2 6 1 2932.81 2371.96 97.00 o -1 6 1 622.05 313.30 35.46 o 0 6 1 1737.95 1684.65 86.81 o 1 6 1 874.90 829.19 40.35 o 2 6 1 2484.02 2856.14 100.26 o 3 6 1 263.41 271.43 20.38 o 4 6 1 57.43 44.83 21.19 o 5 6 1 100.48 137.75 19.56 o 6 6 1 0.02 50.54 22.01 o 7 6 1 6.40 56.24 25.27 o -7 7 1 82.44 49.72 27.71 o -6 7 1 11.46 40.76 16.30 o -5 7 1 493.95 451.57 27.71 o -4 7 1 22.93 12.23 13.04 o -3 7 1 1618.58 1578.05 52.17 o -2 7 1 1698.74 1654.67 57.06 o -1 7 1 4451.68 4497.35 150.79 o 0 7 1 1057.41 902.59 52.98 o 1 7 1 236.63 154.50 23.64 o 2 7 1 508.66 374.95 19.56 o 3 7 1 1013.82 959.38 41.57 o 4 7 1 693.91 709.14 29.34 o 5 7 1 628.30 689.58 30.97 o 6 7 1 138.38 147.53 24.45 o 7 7 1 233.24 240.46 37.49 o -7 8 1 15.76 2.45 23.64 o -6 8 1 40.68 71.73 18.75 o -5 8 1 54.12 85.59 22.82 o -4 8 1 0.22 14.67 13.86 o -3 8 1 50.79 122.27 17.12 o -2 8 1 120.63 127.16 16.30 o -1 8 1 654.70 730.47 20.53 o 0 8 1 1662.16 1391.17 78.66 o 1 8 1 143.34 257.75 31.38 o 2 8 1 4771.20 4737.40 132.05 o 3 8 1 967.66 1140.34 48.09 o 4 8 1 641.38 629.26 30.16 o 5 8 1 1.18 48.91 20.38 o 6 8 1 193.39 195.63 25.27 o 7 8 1 24.45 19.56 39.13 o -7 9 1 0.93 -4.08 24.45 o -6 9 1 0.02 -16.30 16.30 o -5 9 1 4.41 38.31 19.56 o -4 9 1 232.26 264.91 25.27 o -3 9 1 1534.50 1401.98 53.80 o -2 9 1 0.12 21.19 10.60 o -1 9 1 2654.23 2499.93 69.63 o 0 9 1 25.60 7.63 10.19 o 1 9 1 2543.75 2370.17 171.17 o 2 9 1 90.79 79.88 15.49 o 3 9 1 881.34 812.66 35.86 o 4 9 1 202.32 190.74 24.45 o 5 9 1 31.24 18.75 16.30 o 6 9 1 19.42 32.60 18.75 o 7 9 1 16.63 3.26 29.34 o -7 10 1 0.60 0.00 26.08 o -6 10 1 6.13 34.23 19.56 o -5 10 1 49.62 79.88 22.01 o -4 10 1 104.19 119.82 20.38 o -3 10 1 783.17 771.09 30.97 o -2 10 1 1711.39 1529.14 55.43 o -1 10 1 278.17 317.83 47.68 o 0 10 1 4391.98 3687.15 91.35 o 1 10 1 732.99 790.57 23.91 o 2 10 1 3332.58 3327.27 118.19 o 3 10 1 116.22 88.85 17.12 o 4 10 1 1027.39 973.24 34.23 o 5 10 1 918.13 1039.26 43.20 o 6 10 1 110.79 71.73 19.56 o 7 10 1 230.86 290.18 40.76 o -7 11 1 97.35 83.96 29.34 o -6 11 1 316.43 396.96 26.90 o -5 11 1 478.62 477.65 29.34 o -4 11 1 1938.38 1886.16 91.29 o -3 11 1 481.16 502.92 27.71 o -2 11 1 5317.75 4674.64 143.46 o -1 11 1 426.86 350.73 14.04 o 0 11 1 9581.63 8384.44 537.97 o 1 11 1 720.04 855.36 23.61 o 2 11 1 1122.28 823.26 37.49 o 3 11 1 2553.54 2565.14 103.52 o 4 11 1 285.94 332.56 25.27 o 5 11 1 573.39 554.27 30.97 o 6 11 1 0.01 37.49 18.75 o 7 11 1 47.88 83.14 35.05 o -7 12 1 44.09 57.06 30.97 o -6 12 1 132.65 175.25 22.01 o -5 12 1 19.38 74.99 22.01 o -4 12 1 499.89 495.59 30.97 o -3 12 1 240.43 178.51 23.64 o -2 12 1 765.50 620.30 34.23 o -1 12 1 86.74 58.94 10.33 o 0 12 1 168.49 138.53 123.49 o 1 12 1 2614.59 2107.82 61.81 o 2 12 1 382.49 317.89 22.01 o 3 12 1 761.30 749.90 32.60 o 4 12 1 89.90 92.11 22.01 o 5 12 1 727.84 805.33 38.31 o 6 12 1 134.81 135.31 26.90 o 7 12 1 174.35 148.35 37.49 o -7 13 1 48.69 19.56 30.97 o -6 13 1 687.34 670.02 32.60 o -5 13 1 275.46 262.46 25.27 o -4 13 1 764.11 731.97 34.23 o -3 13 1 3985.05 3612.56 125.53 o -2 13 1 906.16 851.79 35.86 o -1 13 1 14152.93 14894.08 926.78 o 0 13 1 113.79 96.80 10.18 o 1 13 1 22234.62 22026.63 216.96 o 2 13 1 955.62 1119.96 43.20 o 3 13 1 5512.41 5299.01 146.72 o 4 13 1 414.55 438.53 27.71 o 5 13 1 331.38 326.04 29.34 o 6 13 1 383.95 358.65 26.90 o 7 13 1 0.70 0.00 35.86 o -7 14 1 77.81 97.81 31.79 o -6 14 1 28.86 50.54 21.19 o -5 14 1 705.63 758.05 34.23 o -4 14 1 238.11 237.20 28.53 o -3 14 1 2304.44 2034.51 74.17 o -2 14 1 173.45 138.57 21.19 o -1 14 1 176.10 104.47 21.60 o 0 14 1 377.52 312.64 14.69 o 1 14 1 1222.94 2087.79 1122.00 o 2 14 1 249.40 211.93 20.38 o 3 14 1 2124.39 2094.01 64.39 o 4 14 1 444.74 467.06 33.42 o 5 14 1 1494.20 1461.49 50.54 o 6 14 1 11.23 78.25 33.42 o 7 14 1 488.19 492.32 44.83 o -7 15 1 104.13 148.35 39.13 o -6 15 1 11.99 37.49 31.79 o -5 15 1 485.09 559.98 32.60 o -4 15 1 21.70 41.57 22.82 o -3 15 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2581.44 110.85 o 2 17 1 4.71 0.00 19.56 o 3 17 1 668.46 591.77 30.97 o 4 17 1 6.30 35.86 18.75 o 5 17 1 86.35 71.73 19.56 o 6 17 1 21.25 12.23 34.23 o 7 17 1 4.18 2.45 29.34 o -7 18 1 9.60 7.34 31.79 o -6 18 1 30.55 53.80 27.71 o -5 18 1 0.95 -12.23 15.49 o -4 18 1 473.84 435.27 30.97 o -3 18 1 0.01 -7.34 14.67 o -2 18 1 97.86 97.00 19.56 o -1 18 1 16.85 13.19 9.01 o 0 18 1 1.15 -7.55 9.60 o 1 18 1 106.80 -29.02 136.94 o 2 18 1 53.49 41.57 16.30 o 3 18 1 301.28 253.50 27.71 o 4 18 1 270.10 187.47 23.64 o 5 18 1 174.62 156.50 23.64 o 6 18 1 31.57 50.54 38.31 o -6 19 1 128.32 77.44 41.57 o -5 19 1 590.05 623.56 35.05 o -4 19 1 423.55 318.71 26.08 o -3 19 1 619.18 502.92 29.34 o -2 19 1 1716.63 1608.21 61.13 o -1 19 1 181.85 162.81 14.95 o 0 19 1 1401.61 1254.73 124.30 o 1 19 1 854.31 825.32 69.69 o 2 19 1 283.98 269.80 28.53 o 3 19 1 855.51 838.75 36.68 o 4 19 1 136.93 87.22 22.01 o 5 19 1 304.77 268.17 27.71 o 6 19 1 2.19 1.63 26.08 o -6 20 1 3.44 48.09 30.16 o -5 20 1 176.86 218.45 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