#------------------------------------------------------------------------------ #$Date: 2012-02-03 17:16:24 +0000 (Fri, 03 Feb 2012) $ #$Revision: 32112 $ #$URL: svn://www.crystallography.net/cod/cif/2/10/40/2104064.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104064 loop_ _publ_author_name 'van Mechelen, Jan B.' 'Peschar, Rene' 'Schenk, Henk' _publ_section_title ; Structures of mono-unsaturated triacylglycerols. III. The \b-2 polymorphs of trans-mono-unsaturated triacylglycerols and related fully saturated triacylglycerols ; _journal_coeditor_code DR5018 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 240 _journal_page_last 248 _journal_volume 64 _journal_year 2008 _chemical_formula_moiety 'C47 H90 O6' _chemical_formula_structural 'C47 H90 O6' _chemical_formula_sum 'C47 H90 O6' _chemical_formula_weight 751.23 _chemical_melting_point 327 _chemical_name_common '\b-2 MMP' _chemical_name_systematic 1,2-dimeristoyl-3-palmitoylglycerol _space_group_IT_number 2 _symmetry_cell_setting triclinic _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _audit_creation_method 'from EXP file using GSAS2CIF' _cell_angle_alpha 92.323(5) _cell_angle_beta 89.791(5) _cell_angle_gamma 100.448(3) _cell_formula_units_Z 2 _cell_length_a 5.45706(15) _cell_length_b 12.1401(5) _cell_length_c 37.369(2) _cell_measurement_temperature 295 _cell_volume 2432.60(18) _computing_structure_refinement GSAS _diffrn_ambient_temperature 295 _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.79948 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_crystal_colour white _exptl_crystal_density_diffrn 1.03 _exptl_crystal_description powder _refine_ls_extinction_method none _refine_ls_goodness_of_fit_all 3.82 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 467 _refine_ls_number_restraints 474 _refine_ls_shift/su_max 0.34 _refine_ls_shift/su_mean 0.01 _reflns_number_total 2663 _[local]_cod_data_source_file dr5018.cif _[local]_cod_data_source_block PMM-B2-TRANS2 _cod_depositor_comments ; The following automatic conversions were performed: '_geom_bond_publ_flag' value 'N' changed to 'n' according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (284 times). '_geom_angle_publ_flag' value 'N' changed to 'n' according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (276 times). Automatic conversion script Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius The following automatic conversions were performed: '_geom_bond_publ_flag' value 'N' changed to 'n' according to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (284 times). '_geom_angle_publ_flag' value 'N' changed to 'n' according to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29 (276 times). Automatic conversion script Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana ; _cod_original_cell_volume 2432.58(19) _cod_database_code 2104064 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z -1 -x,-y,-z loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_thermal_displace_type _atom_site_occupancy O O1a 1.0030(5) 0.1288(3) 0.45003(6) 0.0253 Uiso 1.0 C C1a 0.9145(3) 0.0620(2) 0.42226(5) 0.0253 Uiso 1.0 C C2a 1.1212(4) 0.01735(19) 0.40330(5) 0.0253 Uiso 1.0 O O2a 0.6968(4) 0.0311(5) 0.41605(12) 0.0253 Uiso 1.0 C C3a 1.0242(4) -0.0504(2) 0.36943(5) 0.0253 Uiso 1.0 C C4a 1.2295(4) -0.04344(19) 0.34138(5) 0.0253 Uiso 1.0 C C5a 1.1440(4) -0.12324(19) 0.30950(5) 0.0253 Uiso 1.0 C C6a 1.3540(4) -0.1233(2) 0.28253(5) 0.0253 Uiso 1.0 C C7a 1.2603(4) -0.1999(2) 0.25028(5) 0.0253 Uiso 1.0 C C8a 1.4713(4) -0.2111(2) 0.22443(5) 0.0253 Uiso 1.0 C C9a 1.3657(4) -0.2793(2) 0.19115(5) 0.0253 Uiso 1.0 C C10a 1.5719(4) -0.2954(2) 0.16504(5) 0.0253 Uiso 1.0 C C11a 1.4613(4) -0.3730(2) 0.13389(5) 0.0253 Uiso 1.0 C C12a 1.6579(4) -0.38356(19) 0.10566(5) 0.0253 Uiso 1.0 C C13a 1.5440(4) -0.4647(2) 0.07553(5) 0.0253 Uiso 1.0 C C14a 1.7366(4) -0.4745(2) 0.04664(6) 0.0253 Uiso 1.0 C C1 0.8508(4) 0.12292(18) 0.48227(5) 0.0253 Uiso 1.0 C C2 0.9687(4) 0.21151(14) 0.50911(5) 0.0253 Uiso 1.0 O O1b 0.8622(7) 0.19031(18) 0.54451(5) 0.0253 Uiso 1.0 C C1b 0.9138(3) 0.27398(12) 0.56893(5) 0.0253 Uiso 1.0 C C2b 0.6963(4) 0.27553(17) 0.59353(6) 0.0253 Uiso 1.0 O O2b 1.0915(5) 0.3482(2) 0.56769(12) 0.0253 Uiso 1.0 C C3b 0.7504(4) 0.37466(17) 0.62046(5) 0.0253 Uiso 1.0 C C4b 0.5463(4) 0.36437(18) 0.64871(5) 0.0253 Uiso 1.0 C C5b 0.6060(4) 0.45726(18) 0.67770(5) 0.0253 Uiso 1.0 C C6b 0.4172(4) 0.43711(17) 0.70797(5) 0.0253 Uiso 1.0 C C7b 0.4711(4) 0.53183(17) 0.73647(5) 0.0253 Uiso 1.0 C C8b 0.2816(4) 0.51351(17) 0.76665(5) 0.0253 Uiso 1.0 C C9b 0.3387(4) 0.60998(17) 0.79440(5) 0.0253 Uiso 1.0 C C10b 0.1494(4) 0.59589(17) 0.82460(5) 0.0253 Uiso 1.0 C C11b 0.2189(4) 0.69154(18) 0.85237(5) 0.0253 Uiso 1.0 C C12b 0.0239(4) 0.68485(18) 0.88171(5) 0.0253 Uiso 1.0 C C13b 0.0978(4) 0.78189(18) 0.90881(5) 0.0253 Uiso 1.0 C C14b -0.0893(4) 0.7740(2) 0.93922(6) 0.0253 Uiso 1.0 C C3 0.8825(4) 0.32024(16) 0.50373(5) 0.0253 Uiso 1.0 O O1c 0.8917(4) 0.3460(2) 0.46591(5) 0.0253 Uiso 1.0 C C1c 0.7381(3) 0.41203(11) 0.45531(4) 0.0253 Uiso 1.0 C C2c 0.6198(3) 0.3701(2) 0.41993(5) 0.0253 Uiso 1.0 O O2c 0.6716(6) 0.4834(2) 0.47423(9) 0.0253 Uiso 1.0 C C3c 0.8165(4) 0.3434(2) 0.39366(5) 0.0253 Uiso 1.0 C C4c 0.6949(4) 0.2899(2) 0.35905(5) 0.0253 Uiso 1.0 C C5c 0.8941(4) 0.2735(2) 0.33180(5) 0.0253 Uiso 1.0 C C6c 0.7790(4) 0.2025(2) 0.29950(5) 0.0253 Uiso 1.0 C C7c 0.9822(4) 0.1875(2) 0.27280(5) 0.0253 Uiso 1.0 C C8c 0.8741(4) 0.1217(2) 0.23922(5) 0.0253 Uiso 1.0 C C9c 1.0874(4) 0.0972(2) 0.21578(5) 0.0253 Uiso 1.0 C C10c 0.9937(4) 0.0441(2) 0.17976(5) 0.0253 Uiso 1.0 C C11c 1.2163(4) 0.0329(2) 0.15624(5) 0.0253 Uiso 1.0 C C12c 1.1332(4) -0.0361(2) 0.12217(5) 0.0253 Uiso 1.0 C C13c 1.3597(4) -0.0453(2) 0.09919(5) 0.0253 Uiso 1.0 C C14c 1.2807(4) -0.1087(2) 0.06395(5) 0.0253 Uiso 1.0 C C15c 1.5054(4) -0.1055(2) 0.03949(5) 0.0253 Uiso 1.0 C C16c 1.4357(5) -0.1822(2) 0.00649(6) 0.0253 Uiso 1.0 H H141a 1.6903(12) -0.4398(5) 0.02438(14) 0.0506 Uiso 1.0 H H142a 1.7423(13) -0.5554(4) 0.04134(18) 0.0506 Uiso 1.0 H H143a 1.9040(9) -0.4346(6) 0.05515(18) 0.0506 Uiso 1.0 H H131a 1.4000(10) -0.4368(5) 0.06486(17) 0.0506 Uiso 1.0 H H132a 1.4838(12) -0.5401(4) 0.08542(17) 0.0506 Uiso 1.0 H H121a 1.7991(10) -0.4124(5) 0.11676(17) 0.0506 Uiso 1.0 H H122a 1.7212(12) -0.3084(4) 0.09579(17) 0.0506 Uiso 1.0 H H111a 1.3233(10) -0.3418(5) 0.12285(17) 0.0506 Uiso 1.0 H H112a 1.3935(11) -0.4488(4) 0.14295(17) 0.0506 Uiso 1.0 H H101a 1.7001(10) -0.3294(5) 0.17752(17) 0.0506 Uiso 1.0 H H102a 1.6512(11) -0.2212(4) 0.15582(17) 0.0506 Uiso 1.0 H H91a 1.2468(11) -0.2389(5) 0.17911(17) 0.0506 Uiso 1.0 H H92a 1.2753(11) -0.3543(4) 0.19825(18) 0.0506 Uiso 1.0 H H81a 1.5941(11) -0.2499(5) 0.23622(17) 0.0506 Uiso 1.0 H H82a 1.5561(11) -0.1349(4) 0.21748(18) 0.0506 Uiso 1.0 H H71a 1.1304(10) -0.1678(5) 0.23749(16) 0.0506 Uiso 1.0 H H72a 1.1851(11) -0.2757(4) 0.25864(17) 0.0506 Uiso 1.0 H H61a 1.4957(10) -0.1508(5) 0.29401(17) 0.0506 Uiso 1.0 H H62a 1.4121(12) -0.0454(4) 0.27449(17) 0.0506 Uiso 1.0 H H51a 1.0005(10) -0.0987(5) 0.29753(17) 0.0506 Uiso 1.0 H H52a 1.0896(12) -0.2007(4) 0.31809(17) 0.0506 Uiso 1.0 H H41a 1.3814(10) -0.0641(5) 0.35230(17) 0.0506 Uiso 1.0 H H42a 1.2708(12) 0.0350(4) 0.33304(17) 0.0506 Uiso 1.0 H H31a 0.9663(12) -0.1304(4) 0.37538(18) 0.0506 Uiso 1.0 H H32a 0.8813(10) -0.0197(5) 0.35958(17) 0.0506 Uiso 1.0 H H21a 1.2539(10) 0.0815(5) 0.39684(18) 0.0506 Uiso 1.0 H H22a 1.1934(12) -0.0317(4) 0.41972(16) 0.0506 Uiso 1.0 H H11 0.6799(9) 0.1352(5) 0.47622(18) 0.0506 Uiso 1.0 H H12 0.8398(13) 0.0474(4) 0.49258(17) 0.0506 Uiso 1.0 H H141b -0.2574(9) 0.7786(5) 0.92945(17) 0.0506 Uiso 1.0 H H142b -0.0970(13) 0.7011(4) 0.95109(17) 0.0506 Uiso 1.0 H H143b -0.0364(11) 0.8373(5) 0.95710(15) 0.0506 Uiso 1.0 H H131b 0.1033(13) 0.8542(4) 0.89668(16) 0.0506 Uiso 1.0 H H132b 0.2662(9) 0.7791(6) 0.91871(17) 0.0506 Uiso 1.0 H H121b 0.0124(13) 0.6124(4) 0.89395(17) 0.0506 Uiso 1.0 H H122b -0.1414(9) 0.6893(5) 0.87094(17) 0.0506 Uiso 1.0 H H111b 0.3836(9) 0.6869(6) 0.86326(17) 0.0506 Uiso 1.0 H H112b 0.2316(13) 0.7646(4) 0.84046(17) 0.0506 Uiso 1.0 H H101b -0.0201(9) 0.5973(6) 0.81481(17) 0.0506 Uiso 1.0 H H102b 0.1494(13) 0.5228(4) 0.83605(17) 0.0506 Uiso 1.0 H H91b 0.3344(13) 0.6820(4) 0.78264(17) 0.0506 Uiso 1.0 H H92b 0.5087(9) 0.6121(6) 0.80459(17) 0.0506 Uiso 1.0 H H81b 0.2907(13) 0.4414(4) 0.77816(17) 0.0506 Uiso 1.0 H H82b 0.1105(9) 0.5103(6) 0.75673(17) 0.0506 Uiso 1.0 H H71b 0.4637(13) 0.6047(4) 0.72539(17) 0.0506 Uiso 1.0 H H72b 0.6417(9) 0.5345(6) 0.74657(17) 0.0506 Uiso 1.0 H H61b 0.4267(13) 0.3643(4) 0.71896(17) 0.0506 Uiso 1.0 H H62b 0.2460(9) 0.4340(6) 0.69807(17) 0.0506 Uiso 1.0 H H51b 0.5995(13) 0.5311(4) 0.66715(17) 0.0506 Uiso 1.0 H H52b 0.7772(9) 0.4582(6) 0.68743(17) 0.0506 Uiso 1.0 H H41b 0.3851(9) 0.3701(5) 0.63692(17) 0.0506 Uiso 1.0 H H42b 0.5303(13) 0.2900(4) 0.65986(17) 0.0506 Uiso 1.0 H H31b 0.9147(9) 0.3752(6) 0.63234(17) 0.0506 Uiso 1.0 H H32b 0.7563(13) 0.4460(4) 0.60771(16) 0.0506 Uiso 1.0 H H21b 0.5461(9) 0.2815(5) 0.57900(16) 0.0506 Uiso 1.0 H H22b 0.6634(12) 0.2042(4) 0.60665(16) 0.0506 Uiso 1.0 H H21 1.1545(8) 0.2206(6) 0.50940(19) 0.0506 Uiso 1.0 H H161c 1.3654(11) -0.2596(4) 0.01403(18) 0.0506 Uiso 1.0 H H162c 1.3083(10) -0.1533(5) -0.00790(16) 0.0506 Uiso 1.0 H H163c 1.5876(9) -0.1840(6) -0.00844(16) 0.0506 Uiso 1.0 H H151c 1.6430(10) -0.1309(5) 0.05273(16) 0.0506 Uiso 1.0 H H152c 1.5635(12) -0.0270(4) 0.03190(18) 0.0506 Uiso 1.0 H H141c 1.1527(10) -0.0731(5) 0.05204(17) 0.0506 Uiso 1.0 H H142c 1.2079(11) -0.1884(4) 0.06875(18) 0.0506 Uiso 1.0 H H131c 1.4724(11) -0.0861(5) 0.11244(16) 0.0506 Uiso 1.0 H H132c 1.4509(11) 0.0317(4) 0.09422(18) 0.0506 Uiso 1.0 H H121c 1.0159(11) 0.0013(5) 0.10862(16) 0.0506 Uiso 1.0 H H122c 1.0476(11) -0.1128(4) 0.12847(18) 0.0506 Uiso 1.0 H H111c 1.3337(11) -0.0047(5) 0.16976(16) 0.0506 Uiso 1.0 H H112c 1.3036(11) 0.1092(4) 0.14982(18) 0.0506 Uiso 1.0 H H101c 0.8905(11) 0.0928(4) 0.16811(17) 0.0506 Uiso 1.0 H H102c 0.8910(10) -0.0317(5) 0.18319(18) 0.0506 Uiso 1.0 H H91c 1.1770(12) 0.0446(4) 0.22821(17) 0.0506 Uiso 1.0 H H92c 1.2056(10) 0.1688(5) 0.21183(18) 0.0506 Uiso 1.0 H H81c 0.7716(11) 0.1668(5) 0.22583(16) 0.0506 Uiso 1.0 H H82c 0.7677(10) 0.0496(5) 0.24600(18) 0.0506 Uiso 1.0 H H71c 1.1019(11) 0.1462(5) 0.28425(17) 0.0506 Uiso 1.0 H H72c 1.0727(11) 0.2628(4) 0.26596(18) 0.0506 Uiso 1.0 H H61c 0.6545(11) 0.2408(5) 0.28789(17) 0.0506 Uiso 1.0 H H62c 0.6945(11) 0.1275(4) 0.30746(18) 0.0506 Uiso 1.0 H H51c 1.0191(11) 0.2351(5) 0.34327(17) 0.0506 Uiso 1.0 H H52c 0.9790(11) 0.3482(4) 0.32371(17) 0.0506 Uiso 1.0 H H41c 0.5872(11) 0.3399(4) 0.34916(17) 0.0506 Uiso 1.0 H H42c 0.5908(10) 0.2156(5) 0.36405(18) 0.0506 Uiso 1.0 H H31c 0.9336(10) 0.4140(5) 0.38829(18) 0.0506 Uiso 1.0 H H32c 0.9113(12) 0.2901(4) 0.40468(17) 0.0506 Uiso 1.0 H H21c 0.4932(10) 0.3008(5) 0.42348(18) 0.0506 Uiso 1.0 H H22c 0.5361(12) 0.4291(4) 0.41003(17) 0.0506 Uiso 1.0 H H31 0.9928(10) 0.3819(5) 0.51761(16) 0.0506 Uiso 1.0 H H32 0.7076(9) 0.3143(6) 0.51250(18) 0.0506 Uiso 1.0 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O 0.000 0.000 International_Tables_Vol_C C 0.000 0.000 International_Tables_Vol_C H 0.000 0.000 International_Tables_Vol_C loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1a O1a C1 1_555 1_555 117.1(2) n O1a C1a C2a 1_555 1_555 110.55(17) n O1a C1a O2a 1_555 1_555 124.1(3) n C2a C1a O2a 1_555 1_555 124.7(3) n C1a C2a C3a 1_555 1_555 110.65(16) n C1a C2a H21a 1_555 1_555 109.1(4) n C1a C2a H22a 1_555 1_555 109.1(4) n C3a C2a H21a 1_555 1_555 109.4(4) n C3a C2a H22a 1_555 1_555 109.4(4) n H21a C2a H22a 1_555 1_555 109.1(5) n C2a C3a C4a 1_555 1_555 110.29(16) n C2a C3a H31a 1_555 1_555 109.3(4) n C2a C3a H32a 1_555 1_555 109.3(4) n C4a C3a H31a 1_555 1_555 109.4(4) n C4a C3a H32a 1_555 1_555 109.2(4) n H31a C3a H32a 1_555 1_555 109.4(5) n C3a C4a C5a 1_555 1_555 110.35(16) n C3a C4a H41a 1_555 1_555 109.3(4) n C3a C4a H42a 1_555 1_555 109.2(4) n C5a C4a H41a 1_555 1_555 109.3(4) n C5a C4a H42a 1_555 1_555 109.3(4) n H41a C4a H42a 1_555 1_555 109.4(5) n C4a C5a C6a 1_555 1_555 110.83(16) n C4a C5a H51a 1_555 1_555 109.1(4) n C4a C5a H52a 1_555 1_555 109.3(4) n C6a C5a H51a 1_555 1_555 109.0(4) n C6a C5a H52a 1_555 1_555 109.3(4) n H51a C5a H52a 1_555 1_555 109.3(5) n C5a C6a C7a 1_555 1_555 109.69(16) n C5a C6a H61a 1_555 1_555 109.5(4) n C5a C6a H62a 1_555 1_555 109.3(4) n C7a C6a H61a 1_555 1_555 109.5(4) n C7a C6a H62a 1_555 1_555 109.3(4) n H61a C6a H62a 1_555 1_555 109.5(5) n C6a C7a C8a 1_555 1_555 111.15(16) n C6a C7a H71a 1_555 1_555 109.1(4) n C6a C7a H72a 1_555 1_555 109.3(4) n C8a C7a H71a 1_555 1_555 108.9(4) n C8a C7a H72a 1_555 1_555 109.2(4) n H71a C7a H72a 1_555 1_555 109.2(5) n C7a C8a C9a 1_555 1_555 109.33(15) n C7a C8a H81a 1_555 1_555 109.5(4) n C7a C8a H82a 1_555 1_555 109.5(4) n C9a C8a H81a 1_555 1_555 109.4(4) n C9a C8a H82a 1_555 1_555 109.5(4) n H81a C8a H82a 1_555 1_555 109.6(5) n C8a C9a C10a 1_555 1_555 111.03(16) n C8a C9a H91a 1_555 1_555 109.0(4) n C8a C9a H92a 1_555 1_555 109.4(4) n C10a C9a H91a 1_555 1_555 109.0(4) n C10a C9a H92a 1_555 1_555 109.2(4) n H91a C9a H92a 1_555 1_555 109.3(5) n C9a C10a C11a 1_555 1_555 109.25(16) n C9a C10a H101a 1_555 1_555 109.5(4) n C9a C10a H102a 1_555 1_555 109.5(4) n C11a C10a H101a 1_555 1_555 109.5(4) n C11a C10a H102a 1_555 1_555 109.5(4) n H101a C10a H102a 1_555 1_555 109.5(5) n C10a C11a C12a 1_555 1_555 110.84(16) n C10a C11a H111a 1_555 1_555 109.1(4) n C10a C11a H112a 1_555 1_555 109.3(4) n C12a C11a H111a 1_555 1_555 109.1(4) n C12a C11a H112a 1_555 1_555 109.2(4) n H111a C11a H112a 1_555 1_555 109.3(5) n C11a C12a C13a 1_555 1_555 109.57(16) n C11a C12a H121a 1_555 1_555 109.4(4) n C11a C12a H122a 1_555 1_555 109.5(4) n C13a C12a H121a 1_555 1_555 109.4(4) n C13a C12a H122a 1_555 1_555 109.5(4) n H121a C12a H122a 1_555 1_555 109.4(5) n C12a C13a C14a 1_555 1_555 110.31(16) n C12a C13a H131a 1_555 1_555 109.4(4) n C12a C13a H132a 1_555 1_555 109.2(4) n C14a C13a H131a 1_555 1_555 109.3(4) n C14a C13a H132a 1_555 1_555 109.3(4) n H131a C13a H132a 1_555 1_555 109.3(5) n C13a C14a H141a 1_555 1_555 109.5(4) n C13a C14a H142a 1_555 1_555 109.4(4) n C13a C14a H143a 1_555 1_555 109.5(4) n H141a C14a H142a 1_555 1_555 109.4(6) n H141a C14a H143a 1_555 1_555 109.4(6) n H142a C14a H143a 1_555 1_555 109.5(6) n O1a C1 C2 1_555 1_555 109.20(18) n O1a C1 H11 1_555 1_555 109.7(4) n O1a C1 H12 1_555 1_555 109.4(4) n C2 C1 H11 1_555 1_555 109.6(4) n C2 C1 H12 1_555 1_555 109.5(4) n H11 C1 H12 1_555 1_555 109.5(6) n C1 C2 O1b 1_555 1_555 110.77(17) n C1 C2 C3 1_555 1_555 111.03(17) n C1 C2 H21 1_555 1_555 112.4(4) n O1b C2 C3 1_555 1_555 97.63(18) n O1b C2 H21 1_555 1_555 112.0(5) n C3 C2 H21 1_555 1_555 112.2(4) n C2 O1b C1b 1_555 1_555 116.3(2) n O1b C1b C2b 1_555 1_555 110.52(19) n O1b C1b O2b 1_555 1_555 124.1(3) n C2b C1b O2b 1_555 1_555 124.3(2) n C1b C2b C3b 1_555 1_555 110.65(15) n C1b C2b H21b 1_555 1_555 109.1(4) n C1b C2b H22b 1_555 1_555 109.1(4) n C3b C2b H21b 1_555 1_555 109.4(4) n C3b C2b H22b 1_555 1_555 109.3(4) n H21b C2b H22b 1_555 1_555 109.3(5) n C2b C3b C4b 1_555 1_555 109.73(16) n C2b C3b H31b 1_555 1_555 109.3(4) n C2b C3b H32b 1_555 1_555 109.4(4) n C4b C3b H31b 1_555 1_555 109.4(4) n C4b C3b H32b 1_555 1_555 109.5(4) n H31b C3b H32b 1_555 1_555 109.5(6) n C3b C4b C5b 1_555 1_555 110.93(16) n C3b C4b H41b 1_555 1_555 108.9(4) n C3b C4b H42b 1_555 1_555 109.4(4) n C5b C4b H41b 1_555 1_555 109.0(4) n C5b C4b H42b 1_555 1_555 109.3(4) n H41b C4b H42b 1_555 1_555 109.3(6) n C4b C5b C6b 1_555 1_555 110.03(16) n C4b C5b H51b 1_555 1_555 109.3(4) n C4b C5b H52b 1_555 1_555 109.4(4) n C6b C5b H51b 1_555 1_555 109.4(4) n C6b C5b H52b 1_555 1_555 109.3(4) n H51b C5b H52b 1_555 1_555 109.3(6) n C5b C6b C7b 1_555 1_555 110.22(16) n C5b C6b H61b 1_555 1_555 109.4(4) n C5b C6b H62b 1_555 1_555 109.2(4) n C7b C6b H61b 1_555 1_555 109.5(4) n C7b C6b H62b 1_555 1_555 109.2(4) n H61b C6b H62b 1_555 1_555 109.3(6) n C6b C7b C8b 1_555 1_555 110.76(16) n C6b C7b H71b 1_555 1_555 109.4(4) n C6b C7b H72b 1_555 1_555 109.2(4) n C8b C7b H71b 1_555 1_555 109.2(4) n C8b C7b H72b 1_555 1_555 109.0(4) n H71b C7b H72b 1_555 1_555 109.2(6) n C7b C8b C9b 1_555 1_555 109.47(16) n C7b C8b H81b 1_555 1_555 109.5(4) n C7b C8b H82b 1_555 1_555 109.4(4) n C9b C8b H81b 1_555 1_555 109.5(4) n C9b C8b H82b 1_555 1_555 109.4(4) n H81b C8b H82b 1_555 1_555 109.5(6) n C8b C9b C10b 1_555 1_555 110.98(16) n C8b C9b H91b 1_555 1_555 109.2(4) n C8b C9b H92b 1_555 1_555 109.2(4) n C10b C9b H91b 1_555 1_555 109.2(4) n C10b C9b H92b 1_555 1_555 109.0(4) n H91b C9b H92b 1_555 1_555 109.2(6) n C9b C10b C11b 1_555 1_555 109.23(16) n C9b C10b H101b 1_555 1_555 109.5(4) n C9b C10b H102b 1_555 1_555 109.6(4) n C11b C10b H101b 1_555 1_555 109.4(4) n C11b C10b H102b 1_555 1_555 109.5(4) n H101b C10b H102b 1_555 1_555 109.6(6) n C10b C11b C12b 1_555 1_555 110.76(16) n C10b C11b H111b 1_555 1_555 109.2(4) n C10b C11b H112b 1_555 1_555 109.3(4) n C12b C11b H111b 1_555 1_555 109.1(4) n C12b C11b H112b 1_555 1_555 109.3(4) n H111b C11b H112b 1_555 1_555 109.3(6) n C11b C12b C13b 1_555 1_555 109.42(16) n C11b C12b H121b 1_555 1_555 109.5(4) n C11b C12b H122b 1_555 1_555 109.4(4) n C13b C12b H121b 1_555 1_555 109.5(4) n C13b C12b H122b 1_555 1_555 109.4(4) n H121b C12b H122b 1_555 1_555 109.5(6) n C12b C13b C14b 1_555 1_555 110.24(17) n C12b C13b H131b 1_555 1_555 109.3(4) n C12b C13b H132b 1_555 1_555 109.2(4) n C14b C13b H131b 1_555 1_555 109.5(4) n C14b C13b H132b 1_555 1_555 109.2(4) n H131b C13b H132b 1_555 1_555 109.4(6) n C13b C14b H141b 1_555 1_555 109.4(4) n C13b C14b H142b 1_555 1_555 109.5(4) n C13b C14b H143b 1_555 1_555 109.4(4) n H141b C14b H142b 1_555 1_555 109.6(6) n H141b C14b H143b 1_555 1_555 109.5(6) n H142b C14b H143b 1_555 1_555 109.4(5) n C2 C3 O1c 1_555 1_555 110.59(18) n C2 C3 H31 1_555 1_555 109.4(4) n C2 C3 H32 1_555 1_555 109.2(4) n O1c C3 H31 1_555 1_555 109.1(4) n O1c C3 H32 1_555 1_555 109.3(4) n H31 C3 H32 1_555 1_555 109.3(5) n C3 O1c C1c 1_555 1_555 116.4(2) n O1c C1c C2c 1_555 1_555 110.87(16) n O1c C1c O2c 1_555 1_555 123.9(2) n C2c C1c O2c 1_555 1_555 124.1(2) n C1c C2c C3c 1_555 1_555 110.25(14) n C1c C2c H21c 1_555 1_555 109.3(4) n C1c C2c H22c 1_555 1_555 109.2(4) n C3c C2c H21c 1_555 1_555 109.4(4) n C3c C2c H22c 1_555 1_555 109.3(4) n H21c C2c H22c 1_555 1_555 109.3(5) n C2c C3c C4c 1_555 1_555 110.47(15) n C2c C3c H31c 1_555 1_555 109.4(4) n C2c C3c H32c 1_555 1_555 109.0(4) n C4c C3c H31c 1_555 1_555 109.4(4) n C4c C3c H32c 1_555 1_555 109.1(4) n H31c C3c H32c 1_555 1_555 109.4(5) n C3c C4c C5c 1_555 1_555 109.96(15) n C3c C4c H41c 1_555 1_555 109.4(4) n C3c C4c H42c 1_555 1_555 109.4(4) n C5c C4c H41c 1_555 1_555 109.3(4) n C5c C4c H42c 1_555 1_555 109.3(4) n H41c C4c H42c 1_555 1_555 109.5(5) n C4c C5c C6c 1_555 1_555 110.69(16) n C4c C5c H51c 1_555 1_555 109.1(4) n C4c C5c H52c 1_555 1_555 109.2(4) n C6c C5c H51c 1_555 1_555 109.3(4) n C6c C5c H52c 1_555 1_555 109.2(4) n H51c C5c H52c 1_555 1_555 109.3(5) n C5c C6c C7c 1_555 1_555 109.46(15) n C5c C6c H61c 1_555 1_555 109.5(4) n C5c C6c H62c 1_555 1_555 109.4(4) n C7c C6c H61c 1_555 1_555 109.4(4) n C7c C6c H62c 1_555 1_555 109.5(4) n H61c C6c H62c 1_555 1_555 109.6(5) n C6c C7c C8c 1_555 1_555 111.31(15) n C6c C7c H71c 1_555 1_555 108.9(4) n C6c C7c H72c 1_555 1_555 109.2(4) n C8c C7c H71c 1_555 1_555 109.0(4) n C8c C7c H72c 1_555 1_555 109.0(4) n H71c C7c H72c 1_555 1_555 109.3(5) n C7c C8c C9c 1_555 1_555 108.69(15) n C7c C8c H81c 1_555 1_555 109.7(4) n C7c C8c H82c 1_555 1_555 109.7(4) n C9c C8c H81c 1_555 1_555 109.6(4) n C9c C8c H82c 1_555 1_555 109.6(4) n H81c C8c H82c 1_555 1_555 109.6(5) n C8c C9c C10c 1_555 1_555 111.39(15) n C8c C9c H91c 1_555 1_555 109.1(4) n C8c C9c H92c 1_555 1_555 109.1(4) n C10c C9c H91c 1_555 1_555 108.9(4) n C10c C9c H92c 1_555 1_555 109.0(4) n H91c C9c H92c 1_555 1_555 109.3(5) n C9c C10c C11c 1_555 1_555 108.82(15) n C9c C10c H101c 1_555 1_555 109.5(4) n C9c C10c H102c 1_555 1_555 109.7(4) n C11c C10c H101c 1_555 1_555 109.5(4) n C11c C10c H102c 1_555 1_555 109.6(4) n H101c C10c H102c 1_555 1_555 109.7(5) n C10c C11c C12c 1_555 1_555 110.66(15) n C10c C11c H111c 1_555 1_555 109.2(4) n C10c C11c H112c 1_555 1_555 109.2(4) n C12c C11c H111c 1_555 1_555 109.3(4) n C12c C11c H112c 1_555 1_555 109.2(4) n H111c C11c H112c 1_555 1_555 109.3(5) n C11c C12c C13c 1_555 1_555 109.35(15) n C11c C12c H121c 1_555 1_555 109.4(4) n C11c C12c H122c 1_555 1_555 109.5(4) n C13c C12c H121c 1_555 1_555 109.5(4) n C13c C12c H122c 1_555 1_555 109.4(4) n H121c C12c H122c 1_555 1_555 109.6(5) n C12c C13c C14c 1_555 1_555 110.53(15) n C12c C13c H131c 1_555 1_555 109.1(4) n C12c C13c H132c 1_555 1_555 109.2(4) n C14c C13c H131c 1_555 1_555 109.3(4) n C14c C13c H132c 1_555 1_555 109.4(4) n H131c C13c H132c 1_555 1_555 109.3(5) n C13c C14c C15c 1_555 1_555 109.91(16) n C13c C14c H141c 1_555 1_555 109.3(4) n C13c C14c H142c 1_555 1_555 109.4(4) n C15c C14c H141c 1_555 1_555 109.5(4) n C15c C14c H142c 1_555 1_555 109.4(4) n H141c C14c H142c 1_555 1_555 109.4(5) n C14c C15c C16c 1_555 1_555 110.13(17) n C14c C15c H151c 1_555 1_555 109.4(4) n C14c C15c H152c 1_555 1_555 109.4(4) n C16c C15c H151c 1_555 1_555 109.3(4) n C16c C15c H152c 1_555 1_555 109.3(4) n H151c C15c H152c 1_555 1_555 109.3(5) n C15c C16c H161c 1_555 1_555 109.5(4) n C15c C16c H162c 1_555 1_555 109.6(4) n C15c C16c H163c 1_555 1_555 109.4(4) n H161c C16c H162c 1_555 1_555 109.4(5) n H161c C16c H163c 1_555 1_555 109.5(6) n H162c C16c H163c 1_555 1_555 109.4(5) n loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1a C1a 1_555 1.327(3) n O1a C1 1_555 1.458(3) n C1a O1a 1_555 1.327(3) n C1a C2a 1_555 1.501(3) n C1a O2a 1_555 1.200(3) n C2a C1a 1_555 1.501(3) n C2a C3a 1_555 1.524(3) n C2a H21a 1_555 1.000(6) n C2a H22a 1_555 1.001(7) n O2a C1a 1_555 1.200(3) n C3a C2a 1_555 1.524(3) n C3a C4a 1_555 1.525(3) n C3a H31a 1_555 1.000(6) n C3a H32a 1_555 1.000(6) n C4a C3a 1_555 1.525(3) n C4a C5a 1_555 1.524(3) n C4a H41a 1_555 1.001(6) n C4a H42a 1_555 1.000(6) n C5a C4a 1_555 1.524(3) n C5a C6a 1_555 1.524(3) n C5a H51a 1_555 1.000(6) n C5a H52a 1_555 0.999(6) n C6a C5a 1_555 1.524(3) n C6a C7a 1_555 1.523(3) n C6a H61a 1_555 1.000(6) n C6a H62a 1_555 1.000(6) n C7a C6a 1_555 1.523(3) n C7a C8a 1_555 1.522(3) n C7a H71a 1_555 1.000(7) n C7a H72a 1_555 0.999(6) n C8a C7a 1_555 1.522(3) n C8a C9a 1_555 1.521(3) n C8a H81a 1_555 1.000(7) n C8a H82a 1_555 1.000(6) n C9a C8a 1_555 1.521(3) n C9a C10a 1_555 1.520(3) n C9a H91a 1_555 1.000(7) n C9a H92a 1_555 0.999(6) n C10a C9a 1_555 1.520(3) n C10a C11a 1_555 1.522(3) n C10a H101a 1_555 1.000(7) n C10a H102a 1_555 1.001(6) n C11a C10a 1_555 1.522(3) n C11a C12a 1_555 1.520(3) n C11a H111a 1_555 1.000(6) n C11a H112a 1_555 1.000(6) n C12a C11a 1_555 1.520(3) n C12a C13a 1_555 1.522(3) n C12a H121a 1_555 1.000(6) n C12a H122a 1_555 1.000(6) n C13a C12a 1_555 1.522(3) n C13a C14a 1_555 1.520(3) n C13a H131a 1_555 1.000(6) n C13a H132a 1_555 1.001(6) n C14a C13a 1_555 1.520(3) n C14a H141a 1_555 1.000(6) n C14a H142a 1_555 1.000(6) n C14a H143a 1_555 1.000(5) n C1 O1a 1_555 1.458(3) n C1 C2 1_555 1.498(3) n C1 H11 1_555 0.999(6) n C1 H12 1_555 1.001(6) n C2 C1 1_555 1.498(3) n C2 O1b 1_555 1.457(3) n C2 C3 1_555 1.500(3) n C2 H21 1_555 1.000(5) n O1b C2 1_555 1.457(3) n O1b C1b 1_555 1.329(3) n C1b O1b 1_555 1.329(3) n C1b C2b 1_555 1.501(3) n C1b O2b 1_555 1.200(3) n C2b C1b 1_555 1.501(3) n C2b C3b 1_555 1.524(3) n C2b H21b 1_555 1.000(6) n C2b H22b 1_555 1.000(6) n O2b C1b 1_555 1.200(3) n C3b C2b 1_555 1.524(3) n C3b C4b 1_555 1.524(3) n C3b H31b 1_555 1.001(6) n C3b H32b 1_555 1.001(6) n C4b C3b 1_555 1.524(3) n C4b C5b 1_555 1.524(3) n C4b H41b 1_555 1.000(6) n C4b H42b 1_555 0.999(6) n C5b C4b 1_555 1.524(3) n C5b C6b 1_555 1.524(3) n C5b H51b 1_555 1.001(6) n C5b H52b 1_555 1.001(6) n C6b C5b 1_555 1.524(3) n C6b C7b 1_555 1.524(3) n C6b H61b 1_555 0.999(6) n C6b H62b 1_555 1.000(6) n C7b C6b 1_555 1.524(3) n C7b C8b 1_555 1.523(3) n C7b H71b 1_555 0.999(6) n C7b H72b 1_555 1.000(6) n C8b C7b 1_555 1.523(3) n C8b C9b 1_555 1.522(3) n C8b H81b 1_555 1.000(6) n C8b H82b 1_555 0.999(6) n C9b C8b 1_555 1.522(3) n C9b C10b 1_555 1.521(3) n C9b H91b 1_555 0.999(6) n C9b H92b 1_555 1.000(6) n C10b C9b 1_555 1.521(3) n C10b C11b 1_555 1.521(3) n C10b H101b 1_555 1.000(6) n C10b H102b 1_555 1.001(6) n C11b C10b 1_555 1.521(3) n C11b C12b 1_555 1.519(3) n C11b H111b 1_555 1.000(6) n C11b H112b 1_555 0.999(6) n C12b C11b 1_555 1.519(3) n C12b C13b 1_555 1.520(3) n C12b H121b 1_555 1.000(6) n C12b H122b 1_555 1.001(6) n C13b C12b 1_555 1.520(3) n C13b C14b 1_555 1.519(3) n C13b H131b 1_555 1.000(6) n C13b H132b 1_555 0.999(6) n C14b C13b 1_555 1.519(3) n C14b H141b 1_555 1.000(6) n C14b H142b 1_555 1.000(6) n C14b H143b 1_555 1.000(6) n C3 C2 1_555 1.500(3) n C3 O1c 1_555 1.459(3) n C3 H31 1_555 1.000(6) n C3 H32 1_555 0.999(5) n O1c C3 1_555 1.459(3) n O1c C1c 1_555 1.331(3) n C1c O1c 1_555 1.331(3) n C1c C2c 1_555 1.502(2) n C1c O2c 1_555 1.202(3) n C2c C1c 1_555 1.502(2) n C2c C3c 1_555 1.521(3) n C2c H21c 1_555 1.000(6) n C2c H22c 1_555 1.000(7) n O2c C1c 1_555 1.202(3) n C3c C2c 1_555 1.521(3) n C3c C4c 1_555 1.522(3) n C3c H31c 1_555 0.999(6) n C3c H32c 1_555 1.000(7) n C4c C3c 1_555 1.522(3) n C4c C5c 1_555 1.521(3) n C4c H41c 1_555 0.999(7) n C4c H42c 1_555 0.999(6) n C5c C4c 1_555 1.521(3) n C5c C6c 1_555 1.522(3) n C5c H51c 1_555 1.000(7) n C5c H52c 1_555 0.999(6) n C6c C5c 1_555 1.522(3) n C6c C7c 1_555 1.520(3) n C6c H61c 1_555 1.000(7) n C6c H62c 1_555 0.999(6) n C7c C6c 1_555 1.520(3) n C7c C8c 1_555 1.521(3) n C7c H71c 1_555 1.000(7) n C7c H72c 1_555 1.000(6) n C8c C7c 1_555 1.521(3) n C8c C9c 1_555 1.519(3) n C8c H81c 1_555 0.999(7) n C8c H82c 1_555 1.000(6) n C9c C8c 1_555 1.519(3) n C9c C10c 1_555 1.518(3) n C9c H91c 1_555 1.000(7) n C9c H92c 1_555 1.000(6) n C10c C9c 1_555 1.518(3) n C10c C11c 1_555 1.520(3) n C10c H101c 1_555 1.000(7) n C10c H102c 1_555 1.000(6) n C11c C10c 1_555 1.520(3) n C11c C12c 1_555 1.519(3) n C11c H111c 1_555 1.000(7) n C11c H112c 1_555 1.000(6) n C12c C11c 1_555 1.519(3) n C12c C13c 1_555 1.520(3) n C12c H121c 1_555 0.999(7) n C12c H122c 1_555 1.000(6) n C13c C12c 1_555 1.520(3) n C13c C14c 1_555 1.521(3) n C13c H131c 1_555 1.001(7) n C13c H132c 1_555 1.000(6) n C14c C13c 1_555 1.521(3) n C14c C15c 1_555 1.522(3) n C14c H141c 1_555 1.000(7) n C14c H142c 1_555 1.000(6) n C15c C14c 1_555 1.522(3) n C15c C16c 1_555 1.521(3) n C15c H151c 1_555 1.001(6) n C15c H152c 1_555 1.000(6) n C16c C15c 1_555 1.521(3) n C16c H161c 1_555 1.000(6) n C16c H162c 1_555 1.000(7) n C16c H163c 1_555 1.001(6) n H141a C14a 1_555 1.000(6) n H142a C14a 1_555 1.000(6) n H143a C14a 1_555 1.000(5) n H131a C13a 1_555 1.000(6) n H132a C13a 1_555 1.001(6) n H121a C12a 1_555 1.000(6) n H122a C12a 1_555 1.000(6) n H111a C11a 1_555 1.000(6) n H112a C11a 1_555 1.000(6) n H101a C10a 1_555 1.000(7) n H102a C10a 1_555 1.001(6) n H91a C9a 1_555 1.000(7) n H92a C9a 1_555 0.999(6) n H81a C8a 1_555 1.000(7) n H82a C8a 1_555 1.000(6) n H71a C7a 1_555 1.000(7) n H72a C7a 1_555 0.999(6) n H61a C6a 1_555 1.000(6) n H62a C6a 1_555 1.000(6) n H51a C5a 1_555 1.000(6) n H52a C5a 1_555 0.999(6) n H41a C4a 1_555 1.001(6) n H42a C4a 1_555 1.000(6) n H31a C3a 1_555 1.000(6) n H32a C3a 1_555 1.000(6) n H21a C2a 1_555 1.000(6) n H22a C2a 1_555 1.001(7) n H11 C1 1_555 0.999(6) n H12 C1 1_555 1.001(6) n H141b C14b 1_555 1.000(6) n H142b C14b 1_555 1.000(6) n H143b C14b 1_555 1.000(6) n H131b C13b 1_555 1.000(6) n H132b C13b 1_555 0.999(6) n H121b C12b 1_555 1.000(6) n H122b C12b 1_555 1.001(6) n H111b C11b 1_555 1.000(6) n H112b C11b 1_555 0.999(6) n H101b C10b 1_555 1.000(6) n H102b C10b 1_555 1.001(6) n H91b C9b 1_555 0.999(6) n H92b C9b 1_555 1.000(6) n H81b C8b 1_555 1.000(6) n H82b C8b 1_555 0.999(6) n H71b C7b 1_555 0.999(6) n H72b C7b 1_555 1.000(6) n H61b C6b 1_555 0.999(6) n H62b C6b 1_555 1.000(6) n H51b C5b 1_555 1.001(6) n H52b C5b 1_555 1.001(6) n H41b C4b 1_555 1.000(6) n H42b C4b 1_555 0.999(6) n H31b C3b 1_555 1.001(6) n H32b C3b 1_555 1.001(6) n H21b C2b 1_555 1.000(6) n H22b C2b 1_555 1.000(6) n H21 C2 1_555 1.000(5) n H161c C16c 1_555 1.000(6) n H162c C16c 1_555 1.000(7) n H163c C16c 1_555 1.001(6) n H151c C15c 1_555 1.001(6) n H152c C15c 1_555 1.000(6) n H141c C14c 1_555 1.000(7) n H142c C14c 1_555 1.000(6) n H131c C13c 1_555 1.001(7) n H132c C13c 1_555 1.000(6) n H121c C12c 1_555 0.999(7) n H122c C12c 1_555 1.000(6) n H111c C11c 1_555 1.000(7) n H112c C11c 1_555 1.000(6) n H101c C10c 1_555 1.000(7) n H102c C10c 1_555 1.000(6) n H91c C9c 1_555 1.000(7) n H92c C9c 1_555 1.000(6) n H81c C8c 1_555 0.999(7) n H82c C8c 1_555 1.000(6) n H71c C7c 1_555 1.000(7) n H72c C7c 1_555 1.000(6) n H61c C6c 1_555 1.000(7) n H62c C6c 1_555 0.999(6) n H51c C5c 1_555 1.000(7) n H52c C5c 1_555 0.999(6) n H41c C4c 1_555 0.999(7) n H42c C4c 1_555 0.999(6) n H31c C3c 1_555 0.999(6) n H32c C3c 1_555 1.000(7) n H21c C2c 1_555 1.000(6) n H22c C2c 1_555 1.000(7) n H31 C3 1_555 1.000(6) n H32 C3 1_555 0.999(5) n loop_ _refln_index_h _refln_index_k _refln_index_l 0 0 1 0 0 2 0 0 3 0 1 0 0 1 1 0 1 -1 0 1 -2 0 1 2 0 1 -3 0 0 4 0 1 3 0 1 -4 0 0 5 0 1 4 0 1 -5 0 1 5 0 0 6 0 2 1 0 2 0 0 2 -1 0 2 -2 0 2 2 0 1 -6 0 2 -3 0 1 6 0 2 3 1 0 -1 1 0 0 1 -1 0 0 0 7 0 2 -4 1 -1 1 1 -1 -1 0 1 -7 1 0 -2 0 2 4 1 -1 -2 1 0 1 1 -1 2 1 0 2 0 2 -5 1 0 -3 1 -1 -3 0 1 7 1 -1 3 1 0 3 0 2 5 1 0 -4 1 -1 4 1 0 4 1 -1 -4 0 0 8 0 1 -8 0 2 -6 1 1 -2 1 1 0 1 0 -5 1 -2 -1 1 1 -1 1 1 1 1 -1 5 1 -2 0 1 -2 1 0 2 6 0 1 8 1 -1 -5 1 0 5 1 -2 -2 1 1 -3 1 -2 2 1 1 2 0 2 -7 1 1 3 1 -2 -3 1 1 -4 1 -1 6 1 -2 3 0 0 9 1 0 -6 1 -1 -6 1 0 6 0 1 -9 1 -2 4 1 1 4 1 -2 -4 0 2 7 1 1 -5 0 3 1 0 3 0 1 -2 5 0 3 -1 0 2 -8 1 1 5 0 1 9 0 3 -2 0 3 2 1 -1 7 0 3 -3 1 -2 -5 0 3 3 1 1 -6 1 0 -7 1 -1 -7 0 3 -4 1 0 7 0 3 4 0 2 8 1 -2 6 0 0 10 0 1 -10 1 1 6 0 3 -5 1 -2 -6 1 2 -1 0 2 -9 1 2 1 1 2 2 1 -1 8 1 0 8 1 2 0 0 3 5 1 1 -7 1 2 -2 1 -2 7 1 2 -3 0 3 -6 1 0 -8 1 -1 -8 0 1 10 1 1 7 1 2 3 1 -2 -7 0 2 9 1 2 -4 1 -3 -1 1 2 4 1 -3 -2 1 -3 -3 0 3 6 0 2 -10 1 -1 9 1 -3 0 1 2 -5 1 -3 1 0 3 -7 1 1 -8 1 -2 8 0 1 -11 1 -3 2 0 0 11 1 0 9 1 -3 4 1 -3 3 1 2 5 1 -3 -4 1 1 8 1 0 -9 1 -1 -9 0 3 7 1 -3 5 1 -2 -8 1 2 -6 0 3 -8 1 -3 -5 0 1 11 0 2 10 1 2 6 1 -1 10 1 2 -7 1 -2 9 1 1 -9 1 -3 6 0 2 -11 0 1 -12 0 3 8 1 -3 -6 1 0 10 1 1 9 1 2 7 0 0 12 1 0 -10 1 -2 -9 1 -3 7 1 -1 -10 0 3 -9 1 -2 10 1 2 -8 0 4 1 0 2 11 0 4 0 0 1 12 1 -3 -7 0 4 2 1 1 -10 0 4 -2 0 4 3 1 -1 11 1 1 10 1 3 0 1 3 -1 0 4 -1 1 0 11 0 3 9 1 3 2 1 -3 8 1 3 1 0 2 -12 1 3 -3 1 2 8 1 3 -2 0 4 -3 0 4 -4 0 3 -10 0 1 -13 1 -2 -10 1 3 3 0 4 4 1 -3 -8 1 3 -4 1 0 -11 0 0 13 1 2 -9 1 3 4 0 4 5 0 4 -5 1 -3 9 1 -2 11 1 -1 -11 1 1 -11 1 -1 12 1 3 -5 0 4 -6 0 3 -11 1 -4 -2 0 2 12 1 3 5 1 2 9 0 3 10 1 1 11 1 -4 -3 1 3 -6 2 -1 -2 0 1 13 1 2 -10 0 4 -7 2 -1 0 1 -4 -1 0 4 6 1 0 12 1 -4 -4 2 -1 1 2 -1 -1 1 -4 0 1 -3 -9 0 2 -13 2 -1 2 1 -4 1 2 -1 -3 1 -2 -11 1 -4 2 1 -3 10 0 4 7 1 -4 3 1 3 6 1 0 -12 0 1 -14 2 -2 -1 2 0 -2 1 2 10 1 -4 -5 1 3 -7 1 -4 4 2 0 0 1 -4 5 2 -1 -4 1 -2 12 2 0 -1 2 -2 -2 0 0 14 2 -1 3 1 1 -12 0 4 -8 2 -2 0 1 -1 -12 2 -2 1 2 0 -3 2 -1 4 1 3 7 1 -4 6 2 0 1 1 -4 -6 2 -2 2 0 3 -12 1 -1 13 2 -2 -3 0 3 11 1 3 -8 1 2 -11 2 0 2 1 -3 11 2 -1 -5 1 1 12 1 -3 -10 2 -2 3 2 0 -4 0 2 13 0 2 -14 0 4 -9 1 -4 7 0 4 8 2 -1 5 1 0 13 2 0 -5 2 -2 -4 0 1 14 2 -2 4 1 -2 -12 2 0 3 1 -2 13 2 -2 -5 1 -4 -7 1 -4 8 1 2 11 1 3 8 2 -1 -6 2 0 4 1 0 -13 1 3 -9 0 3 12 2 -1 6 2 0 -6 2 -2 5 2 0 5 0 1 -15 1 1 -13 2 -1 -7 1 -4 -8 1 -1 -13 0 4 -10 2 -2 -6 0 4 9 0 3 -13 1 2 -12 2 -3 0 2 -2 6 1 -3 12 1 -3 -11 0 0 15 2 -3 -1 1 -1 14 2 1 -2 2 1 -3 2 1 0 1 1 13 2 1 -1 1 -4 9 2 1 -4 2 -3 -2 2 1 1 2 -3 1 2 0 6 2 -1 7 2 0 -7 1 3 9 0 2 14 1 4 -1 1 4 0 0 2 -15 1 4 2 2 -3 2 2 1 2 1 4 -2 1 4 1 1 0 14 2 -3 -3 1 3 -10 2 -1 -8 2 -3 -4 2 -2 -7 1 -2 -13 2 -3 3 2 -2 7 1 2 12 1 -2 14 2 1 -5 1 4 -3 1 4 -4 1 4 3 2 1 3 2 0 7 1 -4 -9 0 1 15 1 -4 10 1 4 4 2 -1 8 0 5 0 0 5 2 0 3 -14 0 4 -11 0 4 10 2 1 -6 0 3 13 0 5 1 2 -3 4 1 3 10 1 0 -14 0 5 -1 2 -3 -5 2 -3 5 1 4 -5 2 0 -8 2 1 4 0 5 3 0 5 -2 1 1 -14 1 3 -11 1 2 -13 1 -3 13 1 -3 -12 0 5 4 1 1 14 1 4 5 1 -1 -14 0 5 -3 2 -2 -8 0 1 -16 0 5 -4 2 -2 8 2 -1 -9 0 5 -5 2 0 8 1 -1 15 2 1 -7 0 4 -12 1 4 -6 0 4 11 1 -5 -2 2 -3 6 1 -5 -3 2 1 5 2 0 -9 2 -1 9 1 0 15 2 -3 -6 0 0 16 1 -4 -10 2 1 6 0 5 5 1 -4 11 1 4 -7 2 -2 9 0 2 15 1 4 6 0 2 -16 1 2 13 0 5 -6 0 5 6 1 -2 -14 1 -5 -4 1 -2 15 2 0 9 1 3 11 1 -3 14 1 -5 -1 2 1 7 1 -5 -5 0 5 -7 1 -5 0 1 4 7 0 3 -15 2 -3 7 2 -2 -9 1 3 -12 0 3 14 2 1 -8 2 -3 -7 1 -5 1 0 1 16 2 -1 -10 1 -4 12 1 -5 2 2 2 -3 1 -5 3 1 -3 -13 2 2 -4 1 2 -14 1 0 -15 1 4 -8 2 0 -10 2 2 0 2 2 -1 2 -3 8 2 -1 10 1 -5 4 1 1 -15 2 2 1 0 1 -17 0 5 7 2 2 -2 1 1 15 2 -3 -8 1 -5 6 2 -4 -1 0 4 -13 0 4 12 1 -5 5 2 1 -9 1 -5 -6 2 -2 10 1 -4 -11 1 -1 -15 2 2 2 0 5 -8 2 -4 -3 2 1 8 2 2 -5 2 -4 -2 1 4 -9 2 -4 0 2 -4 1 1 4 8 1 -5 7 2 0 10 0 5 8 0 0 17 2 -4 2 1 -1 16 1 -5 -7 2 2 -6 2 2 3 2 -2 -10 1 0 16 1 3 12 0 5 -9 2 -4 -4 2 -1 11 2 -4 3 1 2 14 1 -5 8 2 -3 9 2 -1 -11 1 -3 15 0 2 16 2 1 9 1 3 -13 1 -3 -14 1 -2 -15 0 2 -17 1 2 -15 2 2 4 2 2 5 1 -2 16 1 -4 13 2 -3 -9 2 -4 4 2 0 -11 0 3 -16 2 1 -10 2 2 -7 0 3 15 2 -4 -5 2 -2 11 2 2 6 1 4 -10 2 -2 -11 1 4 9 1 -5 -8 0 5 9 2 -4 -6 1 -4 -12 0 4 -14 2 -4 5 0 4 13 0 1 17 2 0 11 1 0 -16 1 -5 9 0 5 -10 1 1 -16 2 -4 6 1 1 16 1 -1 17 1 3 -14 2 -3 10 1 -5 -9 1 2 15 0 1 -18 2 -1 12 1 4 10 2 1 10 2 2 -8 1 3 13 2 2 7 2 -2 12 2 -3 -10 2 -1 -12 1 -5 10 2 -4 -7 0 5 -11 1 -2 17 2 1 -11 2 0 -12 2 -4 7 1 -4 -13 1 4 -11 1 0 17 0 0 18 1 -4 14 2 0 12 0 4 -15 1 5 2 2 -3 11 2 2 -9 1 -1 -16 1 5 -1 1 -3 16 0 5 10 1 -3 -15 1 5 0 2 2 8 2 -2 -12 1 5 -2 1 2 -16 1 -2 -16 1 5 1 2 -4 8 0 2 17 1 5 -3 0 2 -18 1 5 3 0 3 -17 0 3 16 1 -5 -10 0 4 14 2 -4 -8 1 4 -12 1 5 -5 1 5 -4 1 4 11 2 1 11 1 -5 11 1 5 4 2 -3 -11 2 -1 13 1 3 -15 0 5 -12 1 5 5 1 -4 15 2 3 -4 2 -2 13 2 3 -3 1 0 -17 1 1 -17 2 2 -10 2 -1 -13 2 2 9 2 1 -12 1 3 14 0 1 18 0 6 2 1 2 16 2 -4 9 1 1 17 2 3 0 2 3 -1 1 5 -6 2 0 -13 2 3 3 0 5 11 2 -3 12 1 -1 18 2 3 1 2 3 -2 0 6 1 2 3 4 2 0 13 2 3 -5 1 -4 -14 1 -5 12 0 1 -19 0 6 4 0 6 3 2 3 2 2 -2 -13 0 6 -1 2 1 12 0 6 0 2 -4 -9 2 3 -6 0 4 -16 1 5 6 0 6 -2 2 -4 10 1 -2 18 1 -5 -11 2 2 10 1 -3 -16 1 -3 17 2 -5 -3 0 6 -3 1 5 -7 2 -1 14 1 0 18 2 3 5 1 4 -13 2 -5 -2 1 2 -17 1 -1 -17 1 -6 -3 1 4 12 0 5 12 1 -6 -4 1 -6 -2 0 0 19 1 -2 -17 0 6 5 2 -5 -1 1 5 -8 2 -3 -12 0 6 -4 2 -4 -10 0 6 -5 2 3 6 0 4 15 2 2 -11 0 5 -13 1 3 15 0 3 -18 2 3 -7 2 -5 -4 0 2 18 2 -5 0 0 3 17 0 2 -19 1 5 7 2 -2 14 2 1 -13 1 1 -18 1 3 -16 1 -4 16 2 -1 -14 2 -3 13 1 -6 -5 1 -6 0 2 3 -8 0 6 -6 2 0 -14 1 -5 13 1 -6 -1 1 5 8 0 6 6 2 -4 11 1 -6 -6 1 -6 1 2 -5 -5 0 6 -7 2 0 14 1 -6 2 2 -5 1 2 2 11 2 2 -12 2 3 7 2 1 13 1 2 17 1 5 -9 1 0 -18 2 -5 -6 0 6 7 1 -5 -12 0 5 -14 2 -5 2 2 -2 -14 1 -4 -15 1 -3 18 1 -6 3 0 6 -8 1 1 18 1 -6 4 0 1 19 2 -5 3 1 -1 19 0 4 -17 1 4 -14 2 -4 -11 2 3 8 1 -6 7 1 5 -10 1 4 13 0 5 13 2 -5 5 2 -2 15 2 -4 12 2 -1 15 2 -3 14 2 3 -9 2 -3 -13 1 -6 6 1 -5 14 1 -6 -7 2 -5 4 2 -5 6 1 -6 5 0 1 -20 1 -3 -17 0 3 -19 1 -2 19 1 -6 8 1 5 9 2 -5 -7 1 2 -18 2 -5 7 1 -5 -13 0 6 8 0 2 19 0 4 16 0 2 -20 2 1 -14 1 3 16 1 -6 -8 1 0 19 0 6 -9 2 0 15 1 -1 -18 2 3 -10 1 -2 -18 2 -5 -8 2 -5 8 2 -1 -15 1 4 -15 2 2 12 0 0 20 1 -4 17 1 3 -17 2 2 -13 0 3 18 2 0 -15 0 6 9 2 3 9 0 6 -10 1 5 -11 2 1 14 0 5 -15 1 1 -19 1 -6 9 2 -4 -12 3 -1 -1 2 -2 -15 2 -4 13 1 -4 -16 3 -1 -2 1 5 10 3 -2 0 3 -2 1 0 5 14 1 2 18 3 -2 -3 1 4 14 1 -6 -9 2 3 10 3 -2 -1 2 1 -15 1 -6 10 1 -3 19 1 -5 15 2 -3 15 2 -5 9 3 -1 0 2 -3 -14 3 -2 2 3 -1 -3 3 -1 1 2 -2 16 2 3 -11 2 4 -2 2 -5 -9 2 4 1 0 4 -18 2 -1 16 2 2 13 3 -2 -2 1 1 19 2 4 -4 3 -1 2 2 4 3 2 4 -3 3 -2 3 3 -2 -4 2 4 2 1 -5 -14 2 4 -1 2 4 0 1 -1 20 0 6 10 0 6 -11 1 5 11 1 0 -19 3 -1 -5 0 1 20 3 -1 -4 2 -5 10 1 -6 11 3 -1 3 1 0 20 2 1 15 1 -3 -18 1 5 -12 2 4 -5 2 0 16 0 3 -20 2 2 -14 2 4 4 2 4 -6 1 -2 20 0 4 17 1 3 17 2 4 5 1 2 -19 1 4 -16 3 -2 -5 3 -3 -1 3 0 -1 0 1 -21 3 -1 4 2 -1 -16 1 4 15 1 6 -1 2 0 -16 3 0 -2 2 -4 -13 3 -3 -2 1 6 0 1 -6 -10 3 -1 -6 1 -4 18 1 6 -2 0 2 20 2 -3 -15 0 5 -16 0 2 -21 1 3 -18 1 -1 -19 1 -2 -19 2 3 11 2 -4 14 3 -2 4 3 0 -4 1 6 1 2 -5 -10 3 0 0 1 6 3 3 -3 0 1 6 -3 3 0 -3 3 -3 1 2 3 -12 3 0 1 1 5 -13 3 -3 -3 0 3 19 2 -2 -16 2 4 -7 0 4 -19 3 -1 5 3 -3 2 1 6 2 3 -2 -6 2 4 6 0 5 15 0 0 21 2 -5 11 1 6 -4 0 6 -12 1 -4 -17 1 -5 16 0 6 11 1 -6 -11 2 2 14 3 -2 5 2 -3 16 3 0 -5 2 1 -16 3 -3 3 1 -6 12 1 1 -20 1 5 12 1 6 4 3 -2 6 3 -3 -4 3 -1 -7 1 1 20 2 -2 17 3 0 2 2 -1 17 1 2 19 1 -5 -15 1 6 -5 3 -1 6 3 -3 4 2 -4 15 1 -3 20 2 -6 -2 0 4 18 0 5 -17 2 4 -8 3 0 3 3 -2 -7 2 -5 12 0 6 -13 2 4 7 2 2 -15 3 0 -6 3 -3 -5 2 1 16 1 6 5 1 -6 13 1 -4 19 1 2 -20 3 -3 -6 2 -5 -11 2 -6 -4 1 6 6 2 -6 -3 1 3 -19 3 0 -7 2 3 12 3 -2 -8 2 -6 -5 3 -2 7 3 -3 5 2 0 17 2 4 -9 1 6 -6 2 -4 -14 1 4 -17 1 6 -7 2 4 8 3 -1 -8 2 3 -13 1 -1 21 1 -5 17 1 -3 -19 1 4 16 2 -6 -1 1 5 -14 1 3 18 3 -1 7 2 -1 -17 2 -3 17 0 1 21 2 -3 -16 1 0 21 2 0 -17 0 3 -21 1 -2 21 0 6 12 3 0 4 0 7 1 1 -6 -12 1 0 -20 0 7 3 3 -3 6 2 -5 -12 3 -3 -7 2 -6 -6 1 5 13 2 -2 -17 2 -6 1 0 7 2 2 -6 0 3 -4 0 1 6 7 0 7 -1 0 1 -22 2 -1 18 3 0 -8 3 -2 8 2 2 15 0 5 16 2 -6 2 0 7 0 3 1 -2 3 -4 -1 2 -6 -7 1 -2 -20 1 6 -8 1 -1 -20 0 2 21 3 -2 -9 0 4 -20 0 2 -22 3 0 5 2 1 -17 2 3 -14 2 4 -10 1 6 8 3 1 -4 2 -6 3 2 -5 13 0 0 22 0 7 5 0 7 4 3 -4 -2 0 3 20 3 -1 -9 3 -1 8 3 1 -3 1 -4 -18 1 6 -9 2 4 9 0 6 -14 2 -4 16 0 6 13 1 -7 -4 1 -7 -3 1 -6 14 1 -5 -16 1 -7 -5 3 0 6 2 -2 18 3 -3 7 0 7 -2 3 -4 1 1 -7 -2 0 7 -4 2 -6 4 3 -4 -3 2 3 13 3 -4 2 0 5 -18 2 2 -16 3 -3 -8 1 1 -21 3 1 -1 0 7 -3 3 1 -5 3 -1 -10 3 1 -6 3 0 7 1 1 21 3 -4 3 0 4 19 2 1 17 1 2 20 2 -4 -15 1 5 -15 3 0 -9 0 7 -5 3 -2 9 0 7 -6 0 7 6 2 -6 -8 3 -4 -5 3 1 0 1 -3 21 2 -6 5 2 -5 14 3 -4 -4 3 1 1 2 -6 7 1 -4 20 1 4 -18 1 -6 -13 0 6 -15 1 -1 22 1 -7 1 1 -7 -6 0 5 17 2 0 18 1 -5 18 3 -2 -10 1 -7 0 3 -4 4 2 -6 6 1 6 9 2 -5 -13 1 4 17 1 3 -20 3 1 2 3 -1 9 1 2 -21 1 6 -10 3 -3 8 2 4 -11 1 -2 22 1 -7 -1 1 -7 -7 2 -6 8 2 -3 18 2 -3 -17 1 5 14 2 -1 -18 2 4 10 3 1 -7 1 3 19 1 -7 2 2 0 -18 2 3 14 3 1 3 0 7 -7 0 1 22 1 -3 -20 3 -4 -6 3 -3 -9 3 -3 9 3 -4 5 3 0 8 1 -7 3 1 -7 4 0 7 -8 2 -6 9 2 3 -15 1 0 -21 2 2 16 0 7 7 3 -1 10 2 -2 19 2 2 -17 0 3 -22 2 -2 -18 3 -1 -11 0 1 -23 2 4 -12 1 -6 15 1 -7 8 1 0 22 0 6 14 1 -6 -14 3 0 -10 2 -6 -9 3 -2 10 3 1 4 2 -1 19 0 7 8 2 4 11 2 5 -1 2 1 -18 2 5 0 2 -4 17 1 -7 5 2 -6 10 3 0 9 1 -7 7 2 5 -2 3 -4 6 2 5 1 1 -7 -8 0 4 -21 1 -5 -17 3 1 -8 1 6 10 2 5 3 1 6 -11 1 5 15 3 -2 -11 3 -4 -7 1 -4 -19 2 5 -3 2 -6 -10 2 -5 15 1 -1 -21 2 5 2 1 5 -16 3 1 5 1 -3 22 3 -2 11 0 2 22 0 5 -19 0 7 -9 0 3 21 0 2 -23 2 0 19 2 5 -5 1 -7 -9 3 1 -9 2 -4 -16 3 -3 10 1 -7 6 0 6 -16 3 -3 -10 2 5 -4 2 -5 -14 0 0 23 1 -7 9 1 -6 16 2 5 4 2 5 5 2 1 18 1 6 -12 1 -2 -21 0 7 -10 3 -4 7 3 -1 11 2 2 17 0 7 9 0 4 20 1 1 -22 1 4 -19 1 -5 19 0 5 18 3 -4 8 3 0 -11 3 -1 -12 2 5 -6 2 3 15 1 -7 10 1 2 21 3 1 6 1 4 18 2 4 -13 3 -3 -11 1 1 22 2 5 -7 2 -6 11 3 0 10 3 -4 -8 1 -4 21 2 -4 18 2 -3 -18 2 -3 19 2 4 12 2 3 -16 1 3 -21 2 5 6 2 -1 -19 1 5 -17 3 -4 -9 1 6 11 2 0 -19 0 6 15 1 -1 23 1 -6 -15 1 2 -22 1 -7 11 3 2 -5 3 1 7 3 2 -4 3 -2 -12 3 -5 -1 2 -6 -11 3 1 -10 1 3 20 2 2 -18 3 0 -12 1 -2 23 1 -7 -10 2 -6 12 3 -3 11 3 -2 12 0 5 -20 2 -4 -17 3 -5 -2 1 -3 -21 3 0 11 2 -2 20 2 -2 -19 0 7 -11 2 5 -8 3 -4 9 3 -5 -4 3 2 0 3 2 -1 1 5 16 3 -5 1 3 2 -3 3 -5 0 2 -5 16 1 6 -13 3 1 8 2 -1 20 3 2 1 2 1 -19 0 1 23 0 7 10 1 6 12 3 2 -2 3 2 -6 3 -5 2 3 -5 -3 1 0 -22 3 -1 12 2 1 19 0 3 -23 1 -5 -18 2 5 7 3 2 2 1 -5 20 3 2 -7 1 4 -20 2 -5 -15 0 6 -17 3 -5 3 0 7 -12 1 0 23 0 1 -24 3 -3 -12 1 -6 17 3 -1 -13 0 4 -22 2 5 8 3 -5 -5 1 -4 -20 3 -4 -10 2 4 -14 0 7 11 3 1 9 3 2 3 1 7 0 2 0 20 3 -5 4 1 -7 12 2 4 13 3 1 -11 2 5 -9 1 7 1 2 3 16 1 -3 23 2 2 18 1 2 22 2 -6 -12 1 -1 -22 1 -7 -11 0 3 22 3 -4 10 3 -2 -13 3 -3 12 3 -1 13 2 -6 13 0 2 23 2 -5 17 3 2 4 3 0 -13 0 2 -24 1 7 2 3 2 -8 2 3 -17 0 5 19 3 -2 13 2 5 -10 3 -5 5 3 0 12 2 -4 19 3 -5 -6 1 4 19 1 7 -1 3 1 10 0 4 21 1 5 -18 1 7 -2 0 6 16 1 -6 -16 1 -2 -22 1 -7 13 1 7 4 0 6 -18 2 -3 -19 2 -7 -5 2 -7 -4 0 0 24 2 -3 20 2 4 -15 3 2 -9 2 -7 -3 1 6 -14 1 7 -3 1 -4 22 1 7 3 1 1 -23 2 5 9 1 -7 -12 1 6 13 1 7 -5 2 -7 -2 2 4 14 3 2 5 0 7 -13 2 -1 -20 1 3 -22 2 2 -19 3 -3 13 1 1 23 3 -5 6 2 0 -20 2 -4 -18 2 -6 14 1 7 -4 3 -4 -11 3 -3 -13 0 5 -21 1 5 17 1 7 5 1 3 21 3 -2 14 0 7 12 3 -5 -7 3 -1 -14 0 3 -24 1 2 -23 3 1 -12 1 7 -6 2 -2 21 2 -7 -6 3 -4 11 2 -2 -20 2 -5 -16 1 -1 24 3 -5 -8 2 -7 -1 1 6 -15 2 5 -11 2 -7 -7 2 1 -20 1 -2 24 0 7 -14 1 -6 18 1 -3 -22 2 3 -18 3 2 6 1 -5 -19 2 -7 1 2 -1 21 2 -7 0 2 -6 -13 3 -5 7 2 1 20 2 -7 2 1 -5 21 3 1 11 3 2 -10 3 -1 14 3 -2 -14 1 4 -21 3 -5 8 3 0 -14 3 0 13 1 7 6 2 5 10 3 -4 12 1 7 -7 1 -7 14 1 7 7 3 1 -13 3 2 7 2 3 17 1 7 -8 1 0 -23 0 1 24 2 -3 21 0 3 23 1 -4 -21 0 4 -23 2 -5 18 2 -7 3 2 -7 4 2 0 21 2 2 19 1 -7 -13 1 0 24 1 -4 23 2 4 -16 3 -4 -12 1 6 14 3 -5 -9 2 -6 -14 3 -3 14 0 6 17 2 -7 -8 0 1 -25 1 -6 -17 2 5 11 3 1 12 1 5 -19 3 2 8 2 -4 20 2 -6 15 0 6 -19 2 4 15 0 5 20 2 -7 5 3 -3 -14 1 -6 19 1 -3 24 3 -2 -15 0 7 13 1 4 20 1 -7 15 2 5 -12 3 -5 9 1 2 23 3 0 14 2 -7 -9 2 -7 8 0 8 2 3 -2 15 2 -3 -20 1 -1 -23 3 2 -11 3 -1 -15 1 -8 -4 1 7 -9 1 3 22 1 7 8 0 4 22 0 8 0 1 -8 -3 0 2 24 1 -5 -20 0 7 -15 0 8 4 0 2 -25 3 2 9 1 6 -16 2 2 -20 2 -7 9 2 -4 -19 2 -7 6 1 5 18 0 8 1 1 -8 -2 1 -2 -23 0 8 3 2 -1 -21 2 -5 -17 2 -1 22 2 5 -13 3 -4 13 2 3 18 2 0 -21 2 -6 16 1 3 -23 3 -1 15 3 3 -5 0 7 14 3 3 -4 1 1 -24 0 5 -22 3 0 -15 2 -7 7 0 0 25 2 -7 10 3 3 -6 3 3 -3 1 -8 -5 3 3 0 3 3 -1 3 1 -14 0 8 -1 3 -5 -10 1 -8 -6 0 8 -2 2 3 -19 3 -6 -1 3 3 -7 0 6 18 3 3 1 3 3 -2 1 1 24 0 8 6 0 8 5 3 2 10 2 -2 -21 2 -2 22 3 -5 10 0 8 -3 2 6 -1 2 6 0 3 -4 -13 2 5 12 2 1 -21 3 -6 -2 0 4 -24 2 6 -2 3 3 2 1 7 -10 1 -7 -14 1 2 -24 0 3 -25 2 -7 -10 3 1 13 2 6 1 2 6 3 3 -6 -4 2 1 21 1 -5 22 1 7 9 0 8 -4 2 6 -3 3 -3 15 3 -6 1 1 6 15 1 4 -22 3 -6 0 2 -6 -15 2 4 -17 1 -1 25 1 -3 -23 3 2 -12 2 -5 19 3 -5 11 3 -6 2 1 7 -11 3 -6 -3 3 3 3 2 6 2 1 -2 25 1 4 21 3 -3 -15 1 -7 16 1 -8 -1 0 8 -7 3 2 11 2 4 16 2 6 -4 1 7 10 0 8 -6 1 0 25 1 -8 -7 3 3 -8 3 0 15 3 -2 -16 0 8 -5 2 6 4 2 -3 22 3 -1 16 1 -6 -18 1 -8 1 2 -5 -18 2 2 20 0 8 7 1 -8 0 1 -8 2 3 -2 16 3 -6 -5 2 -7 11 1 5 -20 1 -8 -8 0 6 -20 1 -4 -22 3 -1 -16 2 6 -6 0 7 -16 3 3 4 2 0 22 3 3 -9 1 -8 3 1 -6 20 2 5 -14 2 -4 21 3 -4 14 2 6 -5 3 -5 -11 1 0 -24 0 3 24 3 2 -13 1 6 -17 1 -4 24 3 1 14 3 3 5 0 1 25 0 5 21 3 -6 3 3 -3 16 1 -8 4 1 6 16 2 6 5 2 6 6 2 -7 12 0 8 -8 0 7 15 3 1 -15 2 -6 17 0 2 -26 2 -7 -11 3 0 -16 2 -3 -21 0 8 -9 3 -6 -6 1 5 19 2 5 13 3 -6 4 2 6 -7 3 -6 -7 0 1 -26 2 -4 -20 1 -3 25 3 -4 -14 1 -5 -21 1 7 -12 2 -5 20 2 2 -21 3 -5 12 1 2 24 2 3 19 1 -8 5 0 8 8 3 3 7 1 3 23 1 -8 8 0 7 -17 0 4 23 1 -7 -15 1 -8 6 3 3 6 3 -4 15 1 7 11 1 -1 -24 1 -8 -9 3 -6 6 0 8 9 3 2 12 3 3 -10 2 3 -20 0 6 19 3 -6 5 2 -1 -22 2 -7 -12 2 0 -22 1 -8 9 1 -8 7 2 -1 23 1 6 -18 0 5 -23 3 3 8 0 2 25 2 6 7 1 5 -21 2 -6 -16 1 3 -24 1 -8 -10 2 4 -18 1 -7 17 2 6 -8 2 2 21 3 -3 -16 1 -8 10 3 -5 -12 2 -2 -22 0 8 -10 3 0 16 2 -4 22 2 -2 23 3 -6 -8 2 6 -9 1 1 -25 2 1 -22 2 4 17 2 5 -15 3 -2 -17 3 2 -14 3 -1 17 3 -6 7 2 -7 13 1 -5 23 3 -2 17 0 0 26 2 1 22 2 0 23 1 -2 -24 1 1 25 1 -8 11 0 4 -25 0 8 -11 1 -7 -16 3 -1 -17 3 2 13 1 4 -23 3 1 15 1 -6 -19 2 -5 -19 1 2 -25 1 7 -13 1 4 22 0 3 -26 3 -5 13 3 -5 -13 0 6 -21 3 -3 17 2 6 8 3 3 -11 3 1 -16 1 -3 -24 0 8 10 2 5 14 3 3 9 1 -6 21 1 6 17 2 -3 23 0 7 16 1 7 12 1 -1 26 2 -6 18 1 -7 18 3 -4 -15 2 -7 14 3 0 -17 1 -2 26 2 5 -16 2 6 9 3 -6 8 2 4 -19 1 -4 -23 2 6 -10 2 -7 -13 1 7 -14 3 -6 -9 1 0 26 3 -4 16 1 -8 -11 0 7 -18 3 0 17 3 -6 9 3 3 -12 0 5 22 3 3 10 3 -5 14 2 4 18 1 -4 25 1 5 20 2 -5 21 3 -2 18 1 7 13 0 3 25 1 -8 12 2 3 20 0 8 -12 2 -3 -22 1 0 -25 2 -4 -21 2 5 15 1 6 -19 2 2 -22 1 -5 -22 2 -6 -17 1 3 -25 3 2 -15 0 1 26 1 -6 -20 0 6 20 2 3 -21 3 -3 -17 1 -5 24 3 -4 -16 2 -2 24 3 3 11 2 -6 19 3 2 14 0 2 -27 0 6 -22 0 8 11 1 -3 26 1 -8 13 3 4 -5 2 -8 -5 2 -8 -6 1 3 24 1 2 25 1 5 -22 2 1 23 2 -8 -4 1 -6 22 0 4 24 2 6 10 3 -2 -18 3 -1 18 2 6 -11 2 -8 -3 3 -5 -14 3 1 16 2 -1 -23 0 1 -27 2 0 -23 0 5 -24 3 -6 10 3 -6 -10 2 -1 24 1 -7 -17 1 8 2 1 1 -26 3 -1 -18 2 2 22 3 4 -1 1 -1 -25 3 4 0 2 -7 15 2 -4 23 0 8 12 1 1 26 1 8 -1 3 4 -2 1 -8 -12 3 4 1 3 1 -17 1 8 -2 1 8 0 2 6 -12 3 4 -6 4 -2 -1 3 -3 18 3 3 -13 1 7 -15 3 -6 11 2 -2 -23 3 4 -4 3 4 -7 2 1 -23 3 -6 -11 0 2 26 2 -7 -14 2 -5 -20 0 7 17 1 8 3 2 5 -17 1 8 -3 3 4 -3 1 8 1 4 -2 -2 1 6 18 3 4 2 0 8 -13 1 -7 19 1 5 21 3 -5 15 2 -8 -7 3 0 -18 1 4 -24 3 -4 17 2 0 24 2 -8 -1 1 -2 27 1 8 -4 2 -8 -8 1 7 14 1 -1 27 1 8 5 4 -2 -3 0 4 -26 1 4 23 1 -8 -13 0 7 -19 2 4 -20 3 4 3 2 -8 1 3 0 18 1 8 4 2 -7 16 3 3 12 2 -8 0 4 -2 0 4 -2 1 2 -8 -2 0 0 27 1 2 -26 0 8 -14 3 1 17 2 2 -23 2 -3 24 4 -1 0 2 6 11 3 4 6 2 5 16 1 8 -5 1 -8 14 2 4 19 3 -1 19 3 4 -8 4 -1 -1 4 -2 2 0 3 -27 3 2 -16 3 -2 19 4 -2 -4 4 -3 0 4 -3 1 1 -3 -25 4 -1 -4 2 -8 2 4 -3 -1 4 -1 -2 3 -7 -2 3 4 4 3 2 15 1 -2 -25 3 4 -9 1 6 -20 2 -6 -18 3 -4 -17 4 -2 3 2 -5 22 4 -3 -4 3 -7 -4 1 -4 -24 3 4 5 1 8 6 4 -3 -2 1 8 -7 3 -3 -18 0 5 23 3 -6 12 4 -2 -6 2 3 21 3 -5 -15 0 5 -25 2 6 -13 3 -7 0 4 -1 -3 2 6 12 1 8 -6 0 8 13 3 -4 18 1 -3 27 3 -7 -3 3 -6 -12 2 -4 -22 2 -6 20 4 -2 -5 3 -7 -1 2 -8 3 2 -8 4 1 -8 15 4 -1 -5 3 3 -14 1 -4 26 2 -8 -9 4 -2 4 2 -3 -23 4 -3 -3 4 -1 1 1 0 27 2 -8 5 1 -6 -21 0 6 21 2 3 -22 0 7 -20 3 4 7 1 7 -16 3 -2 -19 1 -5 -23 4 -3 -5 4 -1 2 1 -7 -18 0 6 -23 3 -7 -5 3 -6 13 2 -7 -15 2 -8 -10 4 -3 2 0 3 26 1 -5 25 3 -1 -19 1 -6 23 1 5 -23 1 3 -26 3 -7 1 3 2 -17 3 1 -18 3 4 8 1 8 -8 3 -5 16 1 0 -26 2 -2 25 2 1 -24 4 -1 3 2 5 -18 4 -2 5 4 -2 -7 1 8 7 3 -3 19 4 -3 3 1 4 -25 2 -8 6 3 4 -10 3 2 16 4 -1 -6 3 3 13 1 -8 -14 1 8 8 2 1 24 0 7 18 1 7 15 1 3 25 0 8 -15 3 3 -15 3 4 9 0 1 27 1 -7 20 2 0 -24 2 -1 -24 0 4 25 1 6 19 4 -3 -6 2 -8 7 2 2 23 3 0 -19 2 -7 17 4 -1 4 1 2 26 2 -8 9 2 -1 25 0 2 -28 2 -4 24 4 -3 4 1 7 -17 2 -5 -21 3 4 -11 3 -7 -6 3 -7 -7 4 0 -3 2 -3 25 2 7 -1 3 -7 2 2 7 0 2 7 -2 4 -2 6 2 7 3 2 -7 -16 1 5 22 3 0 19 2 6 -14 2 5 17 4 0 0 0 1 -28 1 1 -27 2 7 1 2 -8 10 3 1 18 3 -7 3 4 0 -1 1 8 -9 2 7 -3 2 4 -21 2 6 13 4 -4 -3 4 -1 -7 1 -1 -26 3 -5 17 4 -2 -8 4 -1 -8 1 2 -27 3 -6 -13 4 0 -4 4 -1 5 1 8 -10 1 1 27 4 -3 5 4 0 -2 0 8 -16 3 3 14 0 8 14 4 -4 0 4 -4 1 2 7 2 3 -1 20 3 -5 -16 2 4 20 3 -2 20 2 7 -4 4 -3 -7 2 -8 -11 1 -8 16 2 -8 8 4 -4 -1 2 0 25 3 -4 -18 1 -9 -5 4 -4 2 2 -8 11 0 2 27 2 7 4 3 1 -19 2 3 -23 1 -4 -25 1 8 9 1 4 24 3 -6 14 1 -9 -4 4 0 -6 2 -6 -19 1 6 -21 0 9 3 0 0 28 4 -4 -4 0 7 19 2 -7 18 0 9 1 3 -3 20 4 -4 -2 3 -3 -19 4 -2 7 2 2 -24 0 4 -27 4 -4 3 2 6 -15 4 0 -5 3 -4 19 1 -9 -3 3 -7 -8 3 4 10 2 -2 -24 4 0 1 1 -7 21 1 -2 28 3 -7 6 2 7 -5 3 -7 5 4 -3 6 4 -1 6 1 -1 28 2 -5 23 2 -8 12 3 -7 4 0 9 5 0 9 2 2 -6 21 4 0 2 1 -9 -2 2 7 6 3 4 -12 4 -4 4 2 3 22 0 9 -1 0 7 -21 2 7 5 0 9 4 0 9 -2 0 9 0 4 -4 -5 4 -1 -9 4 -2 -9 1 -8 -15 1 -7 -19 3 2 -18 3 -2 -20 2 7 -7 1 -9 -6 1 -8 17 0 3 -28 1 -3 -26 1 -9 -7 0 5 24 3 3 -16 1 7 16 4 -3 -8 4 0 -7 2 5 -19 1 8 -11 0 5 -26 2 7 -6 2 -4 -23 3 2 17 1 -6 -22 0 6 22 4 -3 -9 2 -8 13 3 -1 -20 1 -2 -26 3 0 20 3 -7 7 4 -2 8 4 -4 5 2 -3 -24 0 9 -4 0 6 -24 4 -3 7 3 -7 8 4 -1 7 1 7 -18 0 9 7 1 -5 -24 0 9 6 1 -6 24 1 8 10 1 -4 27 2 -1 26 2 6 14 1 -3 28 1 5 -24 3 -7 9 3 -2 21 3 -7 -9 3 -6 -14 2 -8 -12 4 -4 -6 4 0 3 2 7 7 1 6 -22 2 -6 -20 1 -5 26 1 6 20 3 0 -20 0 9 -3 2 -7 -17 0 9 -5 2 7 -8 3 3 15 0 8 -17 1 0 28 3 4 11 0 8 15 1 8 11 2 1 -25 3 -7 -10 3 -5 18 1 -9 0 2 5 18 3 -6 15 4 -4 6 2 -2 26 1 3 -27 4 0 -8 1 4 -26 0 3 27 3 1 19 1 -9 -8 4 -1 -10 2 1 25 2 -5 -22 4 -2 -10 4 0 4 1 -9 -1 3 -5 -17 0 9 -7 2 2 24 2 6 -16 2 -8 -13 1 0 -27 3 4 -13 4 -3 8 1 -9 -9 2 -4 25 1 -9 1 0 9 -6 2 0 -25 2 5 -20 2 4 -22 2 -1 -25 4 -1 8 4 -2 9 1 -9 2 1 3 26 4 -3 -10 1 8 -12 0 1 -29 3 -4 -19 1 5 23 0 4 26 2 -7 19 4 -4 -8 4 -4 -7 0 9 8 3 4 12 1 -9 3 2 -3 26 3 -1 21 3 1 -20 3 5 -4 3 -7 10 2 4 21 2 3 23 1 2 27 4 -4 7 2 7 -9 2 -8 14 2 7 8 0 1 28 3 -6 16 4 1 -3 3 -4 20 1 8 -13 3 -1 -21 3 -3 -20 3 -3 21 1 -9 4 2 7 -10 0 2 -29 2 7 9 1 -8 -16 3 4 -14 4 1 -5 1 -8 18 3 5 -6 4 -5 -2 0 9 -8 3 -7 11 3 3 -17 2 3 -24 4 0 -9 0 9 -9 3 5 -5 1 -9 8 1 1 -28 3 2 -19 4 1 -4 4 1 -2 1 2 -28 1 -9 5 1 -1 -27 3 5 5 2 0 26 1 4 25 4 0 -10 4 -3 9 3 -7 -11 4 0 5 1 -9 9 3 2 18 3 0 -21 3 5 4 1 1 28 4 -5 -3 1 -9 6 2 2 -25 4 -1 -11 2 -8 15 2 6 15 4 -1 9 1 -4 -26 4 -2 -11 3 5 3 3 -6 -15 3 -2 -21 3 5 -3 4 -2 10 4 -5 1 4 -5 0 4 -4 -9 1 -9 -10 1 -9 10 4 -3 10 4 -4 8 3 1 20 2 -2 -25 4 1 -6 4 -5 2 4 -5 -1 0 2 28 4 -3 -11 0 9 9 3 5 -1 3 5 -7 4 1 -1 3 5 0 3 0 21 3 5 -8 3 3 16 3 5 -2 4 -5 -4 4 -2 -12 4 -5 3 1 -9 11 3 5 1 0 0 29 1 -2 29 4 0 6 2 7 -11 3 5 6 2 -4 -24 1 -9 7 1 -1 29 0 5 25 0 9 -10 3 -5 19 3 4 13 3 5 7 3 5 2 4 -5 4 3 -7 12 0 9 -11 1 -3 -27 4 1 -7 2 -3 -25 4 1 -8 4 -5 -5 4 0 -11 4 -4 9 4 -1 10 1 -2 -27 3 4 -15 3 2 19 3 5 -9 4 -5 5 4 -2 11 4 -1 -12 4 1 0 3 -7 13 4 -3 11 4 0 7 2 -9 -4 4 1 1 3 3 17 3 5 -10 2 1 -26 3 1 -21 4 -1 11 4 1 2 1 -9 12 3 5 8 4 0 8 1 0 29 4 -5 6 4 1 -9 3 5 9 4 1 3 0 3 28 2 0 -26 2 -9 -6 2 -9 -5 4 0 9 3 -8 -4 4 -4 10 1 0 -28 2 -9 -3 3 4 14 4 1 4 3 -8 -3 0 1 -30 4 -2 12 2 -1 -26 1 -1 -28 0 1 29 3 -8 -2 4 -1 12 4 1 5 1 1 -29 2 -2 -26 3 -8 -1 4 0 10 2 -9 -1 2 -9 1 2 -9 0 2 -9 -2 0 2 29 4 1 6 3 -8 0 4 0 11 4 2 -5 2 -9 2 0 0 30 4 2 -4 2 -9 3 4 1 7 1 -2 -28 2 -9 4 3 -8 1 2 -9 5 3 -8 2 4 2 -3 2 -9 6 3 -8 3 4 2 0 4 2 -1 4 2 1 4 2 -2 3 -8 4 4 2 2 4 1 8 2 -9 7 1 0 -29 4 2 3 3 -8 5 2 -9 8 4 2 4 1 -1 -29 3 -8 6 4 1 9