Crystallography Open Database

Information card for entry 2104120

Preview

Coordinates	2104120.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	azidobis(di-2-pyridylamine)copper(II) perchlorate
Formula	C20 H18 Cl Cu N9 O4
Calculated formula	C20 H18 Cl Cu N9 O4
Title of publication	Five-coordinate copper(II) complexes: crystal structures, spectroscopic properties and new extended structural pathways of [Cu(chelate)~2~<i>X</i>]<i>Y</i>, where chelate = dpyam, phen and bipy; <i>X</i> = pseudohalide ligands
Authors of publication	Youngme, Sujittra; Phuengphai, Pongthipun; Pakawatchai, Chaveng; Kongsaeree, Palangpon; Chaichit, Narongsak
Journal of publication	Acta Crystallographica Section B
Year of publication	2008
Journal volume	64
Journal issue	3
Pages of publication	318 - 329
a	13.436 ± 0.0005 Å
b	8.388 ± 0.0003 Å
c	22.575 ± 0.0005 Å
α	90°
β	118.147 ± 0.0019°
γ	90°
Cell volume	2243.35 ± 0.13 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0627
Residual factor for significantly intense reflections	0.0446
Weighted residual factors for significantly intense reflections	0.1115
Weighted residual factors for all reflections included in the refinement	0.1254
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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