#------------------------------------------------------------------------------ #$Date: 2023-03-16 03:03:16 +0000 (Thu, 16 Mar 2023) $ #$Revision: 281906 $ #$URL: svn://www.crystallography.net/cod/cif/2/10/90/2109099.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2109099 loop_ _publ_author_name 'Yakubovich, Olga V.' 'Kiriukhina, Galina V.' 'Simonov, Sergey V.' 'Volkov, Anatoly S.' 'Dimitrova, Olga V.' _publ_section_title ; (Na,Li)~3~(Cl,OH)[Cu~3~OAl(PO~4~)~3~]: a first salt-inclusion aluminophosphate oxocuprate with a new type of crystal structure ; _journal_coeditor_code JE5049 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 24 _journal_page_last 31 _journal_paper_doi 10.1107/S2052520622011696 _journal_volume 79 _journal_year 2023 _chemical_formula_sum 'Al8 Cl7 Cu24 Li4.19 Na19.81 O105 P24' _chemical_formula_weight 4896.74 _chemical_name_common 'aluminophosphate oxocuprate' _chemical_name_systematic 'sodium alumonophosphate oxocuprate chloride' _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-C 2y' _space_group_name_H-M_alt 'C 1 2/m 1' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90.361(2) _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 13.3428(4) _cell_length_b 18.9320(5) _cell_length_c 8.9404(2) _cell_measurement_reflns_used 6699 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 37.154 _cell_measurement_theta_min 1.869 _cell_volume 2258.35(10) _computing_cell_refinement 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_molecular_graphics 'Diamond (Brandenburg, 2006)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2015b)' _computing_structure_solution 'SHELXT (Sheldrick, 2015a)' _diffrn_ambient_temperature 423(2) _diffrn_detector_area_resol_mean 5.2283 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'Xcalibur, AtlasS2, Gemini' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0206 _diffrn_reflns_av_unetI/netI 0.0194 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 7934 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.489 _diffrn_reflns_theta_min 1.867 _diffrn_source 'fine-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 6.485 _exptl_absorpt_correction_T_max 1.295 _exptl_absorpt_correction_T_min 0.778 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.67a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour light-green _exptl_crystal_density_diffrn 3.601 _exptl_crystal_description prism _exptl_crystal_F_000 2349 _exptl_crystal_size_max 0.100 _exptl_crystal_size_mid 0.045 _exptl_crystal_size_min 0.040 _exptl_transmission_factor_max 1.000 _exptl_transmission_factor_min 0.780 _refine_diff_density_max 1.698 _refine_diff_density_min -1.739 _refine_diff_density_rms 0.191 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.165 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 247 _refine_ls_number_reflns 2646 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.165 _refine_ls_R_factor_all 0.0405 _refine_ls_R_factor_gt 0.0390 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+30.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1089 _refine_ls_wR_factor_ref 0.1097 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2542 _reflns_number_total 2646 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file je5049sup1.cif _cod_data_source_block I _cod_depositor_comments ; The following automatic conversions were performed: data item '_atom_sites_solution_primary' value 'Direct' was changed to 'direct' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. data item '_atom_sites_solution_secondary' value 'Diffmap' was changed to 'difmap'. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_original_sg_symbol_H-M 'C 2/m' _cod_database_code 2109099 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.563 _shelx_estimated_absorpt_t_max 0.781 _exptl_absorpt_special_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _shelx_res_file ; TITL shelxt_a.res in C2/m shelx.res created by SHELXL-2018/3 at 12:09:26 on 31-Oct-2022 CELL 0.71073 13.3428 18.9320 8.9404 90.000 90.361 90.000 ZERR 1.00 0.0004 0.0005 0.0002 0.000 0.002 0.000 LATT 7 SYMM - X, Y, - Z SFAC O NA AL P CU CL LI UNIT 105 19.81 8 24 24 7 4.19 MERG 2 FMAP 2 PLAN 20 OMIT -3 55 TEMP 150(2) ACTA SIZE 0.04*0.045*0.10 EADP CL2 O15 EADP NA3 LI1 EXYZ NA4 LI2 EADP NA4 LI2 OMIT 4 0 3 OMIT 2 0 1 OMIT 2 0 2 OMIT -4 0 3 TWIN 1 0 0 0 -1 0 0 0 -1 2 BOND LIST 6 L.S. 3 WGHT 0.050000 30.000000 BASF 0.14483 FVAR 0.45046 0.74933 0.55617 0.84056 CU1 5 0.250000 0.250000 0.500000 10.50000 0.01205 0.01204 = 0.00859 0.00191 0.00232 0.00096 CU2 5 0.127051 0.416711 0.310495 11.00000 0.01060 0.01208 = 0.01101 -0.00566 0.00131 0.00025 CU3 5 0.000000 0.248350 0.500000 10.50000 0.01557 0.01471 = 0.01121 0.00000 0.00033 0.00000 CU4 5 0.625544 0.745189 0.828964 11.00000 0.04806 0.00518 = 0.00703 -0.00056 -0.00034 0.00340 P1 4 0.125728 0.263034 0.195259 11.00000 0.01604 0.01034 = 0.00736 -0.00062 0.00021 0.00129 P2 4 0.119050 0.619187 0.667275 11.00000 0.01132 0.00471 = 0.00447 -0.00025 0.00089 -0.00090 P3 4 0.632420 0.617157 0.654540 11.00000 0.01148 0.00661 = 0.00585 -0.00151 0.00184 0.00005 AL1 3 0.246643 0.500000 0.526087 10.50000 0.00771 0.00774 = 0.00649 0.00000 0.00082 0.00000 AL2 3 0.000000 0.500000 0.500000 10.25000 0.00660 0.00631 = 0.00522 0.00000 0.00087 0.00000 AL3 3 0.500000 0.500000 0.500000 10.25000 0.00841 0.00983 = 0.00755 0.00000 0.00219 0.00000 NA1 2 0.000000 0.607984 1.000000 10.50000 0.01125 0.01320 = 0.01026 0.00000 0.00010 0.00000 NA2 2 0.749738 0.614039 1.012327 11.00000 0.01568 0.02655 = 0.02717 -0.00159 -0.00277 0.00056 NA3 2 0.618821 0.618520 0.311958 31.00000 0.01135 0.01497 = 0.01241 0.00523 0.00482 0.00109 LI1 7 0.622179 0.575723 0.300194 -31.00000 0.01135 0.01497 = 0.01241 0.00523 0.00482 0.00109 NA4 2 0.504408 0.618963 1.034793 40.50000 0.01729 0.08335 = 0.09113 -0.01981 0.01554 0.00071 LI2 7 0.504408 0.618963 1.034793 -40.50000 0.01729 0.08335 = 0.09113 -0.01981 0.01554 0.00071 CL2 6 0.619065 0.510231 1.067873 20.50000 0.02179 0.01333 = 0.00903 0.00412 0.00379 -0.00099 O15 1 0.541120 0.500000 0.847352 -20.50000 0.02179 0.01333 = 0.00903 0.00412 0.00379 -0.00099 CL1 6 0.131336 0.500000 0.068024 10.50000 0.02248 0.01146 = 0.00971 0.00000 -0.00035 0.00000 O1 1 0.375241 0.500000 0.592568 10.50000 0.00650 0.01014 = 0.00973 0.00000 0.00156 0.00000 O2 1 0.125218 0.500000 0.432600 10.50000 0.00891 0.00589 = 0.00449 0.00000 0.00159 0.00000 O3 1 0.211887 0.571581 0.661622 11.00000 0.01178 0.00939 = 0.01277 -0.00479 0.00245 0.00043 O4 1 0.727193 0.572209 0.628668 11.00000 0.01004 0.01008 = 0.01422 -0.00568 0.00436 -0.00062 O5 1 0.023381 0.572424 0.651370 11.00000 0.00881 0.00822 = 0.00745 -0.00215 -0.00112 0.00023 O6 1 0.116726 0.654881 0.822303 11.00000 0.01442 0.00597 = 0.00492 -0.00106 0.00049 -0.00117 O7 1 0.630781 0.679293 0.544209 11.00000 0.02967 0.01428 = 0.01064 0.00491 0.00324 -0.00050 O8 1 0.119051 0.672796 0.540150 11.00000 0.02682 0.01214 = 0.00782 0.00274 -0.00044 -0.00580 O9 1 0.540520 0.571078 0.636206 11.00000 0.01094 0.01491 = 0.01501 -0.00725 0.00309 -0.00231 O10 1 0.635797 0.645780 0.814697 11.00000 0.01594 0.00758 = 0.00573 -0.00203 0.00184 0.00038 O11 1 0.221214 0.243394 0.285490 11.00000 0.01576 0.01632 = 0.01215 0.00416 0.00369 0.00689 O12 1 0.030533 0.241224 0.281553 11.00000 0.01947 0.01791 = 0.01801 0.00751 -0.00246 -0.00614 O13 1 0.124807 0.343391 0.167625 11.00000 0.01265 0.01063 = 0.00739 -0.00262 0.00179 -0.00001 O14 1 0.127344 0.224753 0.048364 11.00000 0.08138 0.01508 = 0.01154 -0.00322 -0.00325 0.00858 HKLF 4 REM shelxt_a.res in C2/m REM wR2 = 0.1097, GooF = S = 1.165, Restrained GooF = 1.165 for all data REM R1 = 0.0390 for 2542 Fo > 4sig(Fo) and 0.0405 for all 2646 data REM 247 parameters refined using 0 restraints END WGHT 0.0591 31.4071 REM Highest difference peak 1.698, deepest hole -1.739, 1-sigma level 0.191 Q1 1 0.5821 0.7458 0.8670 11.00000 0.05 1.66 Q2 1 0.6668 0.7501 0.8734 11.00000 0.05 1.48 Q3 1 0.5371 0.5222 0.8544 11.00000 0.05 1.18 Q4 1 0.6221 0.5622 0.1628 11.00000 0.05 1.03 Q5 1 0.6240 0.7570 0.7971 11.00000 0.05 0.97 Q6 1 0.1719 0.2437 0.0060 11.00000 0.05 0.97 Q7 1 0.1207 0.2252 0.1974 11.00000 0.05 0.84 Q8 1 0.0767 0.2388 0.0093 11.00000 0.05 0.77 Q9 1 0.0448 0.2187 0.2221 11.00000 0.05 0.71 Q10 1 0.5751 0.5000 1.0442 10.50000 0.05 0.71 Q11 1 0.6185 0.5000 1.2278 10.50000 0.05 0.69 Q12 1 0.1227 0.2781 0.0497 11.00000 0.05 0.62 Q13 1 0.3815 0.4799 0.6672 11.00000 0.05 0.62 Q14 1 0.1762 0.5000 0.0488 10.50000 0.05 0.61 Q15 1 0.1209 0.4814 0.0810 11.00000 0.05 0.59 Q16 1 0.1914 0.2183 0.2460 11.00000 0.05 0.59 Q17 1 0.1221 0.6383 0.7403 11.00000 0.05 0.57 Q18 1 0.6192 0.6457 0.1664 11.00000 0.05 0.57 Q19 1 0.6288 0.6334 0.7247 11.00000 0.05 0.57 Q20 1 0.1050 0.6493 0.6142 11.00000 0.05 0.56 ; _shelx_res_checksum 48860 _shelx_hkl_file ; 0 -30 0 2806.17 134.269 4 0 -30 -1 421.173 58.9628 4 0 -30 1 378.755 55.6022 4 0 -30 -2 569.238 68.6700 4 0 -30 2 434.454 58.6530 4 0 -30 3 103.446 38.7907 4 0 -30 4 47.4791 34.7341 4 0 -30 5 902.613 78.6006 4 0 -28 0 2328.84 117.894 4 0 -28 -1 572.703 62.6096 4 0 -28 1 730.901 68.1811 4 0 -28 2 2260.93 116.221 4 0 -28 -2 2318.73 119.721 4 0 -28 -3 1599.91 100.310 4 0 -28 3 1676.74 100.190 4 0 -28 4 435.459 56.1930 4 0 -28 5 196.944 42.1916 4 0 -28 6 383.858 52.9908 4 0 -26 0 2576.63 116.859 4 0 -26 1 96.0788 33.9461 4 0 -26 -1 32.1877 30.0704 4 0 -26 -2 915.745 73.8312 4 0 -26 2 1019.75 76.3354 4 0 -26 3 5426.02 167.788 4 0 -26 -3 5263.22 168.796 4 0 -26 4 796.877 68.9009 4 0 -26 5 71.1753 32.3782 4 0 -26 6 102.069 36.3960 4 0 -26 7 61.2998 29.8809 4 0 -26 -8 778.106 68.8782 2 0 -26 -9 1132.62 83.0132 2 0 -24 0 11052.0 225.702 4 0 -24 -1 3285.31 124.710 4 0 -24 1 3396.50 126.504 4 0 -24 -2 8.04675 25.8464 4 0 -24 2 64.3911 29.9128 4 0 -24 3 158.945 36.5315 4 0 -24 -3 96.0863 30.9214 4 0 -24 -4 151.279 36.4168 4 0 -24 4 275.205 43.1620 4 0 -24 5 4489.71 144.713 4 0 -24 6 3612.47 130.154 4 0 -24 7 284.680 43.2983 4 0 -24 -8 164.747 41.6169 2 0 -24 -9 918.692 74.3148 2 0 -24 -10 569.527 62.2926 2 0 -22 0 5432.41 149.915 4 0 -22 -1 277.661 39.9055 4 0 -22 1 304.035 40.8366 4 0 -22 2 581.932 52.8075 4 0 -22 -2 521.880 50.5285 4 0 -22 -3 61.3899 27.0667 4 0 -22 3 68.4368 27.2958 4 0 -22 -4 316.417 43.3107 4 0 -22 4 305.437 42.5630 4 0 -22 5 14.7797 25.6367 4 0 -22 6 7892.96 181.283 4 0 -22 7 357.972 44.8480 4 0 -22 -8 764.530 63.8221 2 0 -22 -9 569.721 59.2645 2 0 -22 -10 91.9582 36.4557 2 0 -22 -11 180.883 41.9333 2 0 -20 0 1325.87 71.8022 4 0 -20 -1 370.354 41.7008 4 0 -20 1 339.070 39.6571 4 0 -20 2 2923.21 103.005 4 0 -20 -2 2871.56 103.786 4 0 -20 3 20798.0 272.393 4 0 -20 -3 20630.0 281.186 4 0 -20 4 2510.66 97.8356 4 0 -20 -4 2485.28 100.846 4 0 -20 5 8.89064 21.7118 4 0 -20 6 648.650 53.4625 4 0 -20 7 69.1789 26.3669 4 0 -20 -8 260.593 40.7119 2 0 -20 8 292.033 38.9393 4 0 -20 -9 7376.13 185.683 2 0 -20 -10 1240.73 83.2948 2 0 -20 -11-15.3324 30.8713 2 0 -20 -12 2014.47 110.290 2 0 -18 0 1533.68 70.9104 4 0 -18 -1 948.141 58.1182 4 0 -18 1 883.975 54.8083 4 0 -18 -2 3802.25 111.775 4 0 -18 2 3977.66 112.437 4 0 -18 -3 3722.72 111.614 4 0 -18 3 3991.28 113.572 4 0 -18 4 161.950 30.9755 4 0 -18 -4 122.264 28.0703 4 0 -18 5 943.349 58.6186 4 0 -18 6 2845.63 97.8689 4 0 -18 7 386.511 40.6393 4 0 -18 -7 325.015 39.4789 2 0 -18 8 69.6577 24.4133 4 0 -18 -8 79.6748 27.9183 2 0 -18 -9 3105.58 118.218 2 0 -18 -10 2679.82 114.670 2 0 -18 -11 141.876 36.8976 2 0 -18 -12 114.772 37.5666 2 0 -16 0 34581.4 304.132 4 0 -16 1 5968.72 127.325 4 0 -16 -1 5836.81 128.049 4 0 -16 -2 2417.60 84.3546 4 0 -16 2 2471.84 83.5517 4 0 -16 -3 2070.89 79.5222 4 0 -16 3 2100.77 77.4579 4 0 -16 4 518.597 41.2913 4 0 -16 -4 447.780 40.5408 4 0 -16 5 1841.87 71.7101 6 0 -16 5 1976.22 76.0599 4 0 -16 6 7442.18 147.188 4 0 -16 6 7280.86 141.796 6 0 -16 7 3837.46 104.908 6 0 -16 7 3878.76 107.835 4 0 -16 -7 3753.58 112.150 2 0 -16 8 402.144 38.2826 6 0 -16 8 385.728 38.4696 4 0 -16 -8 449.896 44.5089 2 0 -16 -9 1259.01 74.5702 2 0 -16 -10-51.2627 29.7981 2 0 -16 -11 26.0656 27.3126 2 0 -16 -12 2352.89 114.078 2 0 -16 -13 870.579 75.7983 2 0 -14 0 3312.86 88.3178 4 0 -14 -1 45.3550 18.6373 4 0 -14 1 4.83016 17.9982 4 0 -14 -2 523.916 39.2489 4 0 -14 2 474.552 35.9898 4 0 -14 -3 6885.58 132.268 4 0 -14 3 7031.79 127.751 4 0 -14 -4 3085.81 92.2277 4 0 -14 4 3172.26 85.7185 6 0 -14 4 3147.79 87.6099 4 0 -14 5 93.3567 21.3087 4 0 -14 5 85.1089 21.1748 6 0 -14 6 7649.14 134.973 6 0 -14 6 7640.48 137.942 4 0 -14 7 92.8979 22.2225 4 0 -14 7 102.563 23.8396 6 0 -14 -7 135.976 25.8017 2 0 -14 8 672.817 44.4389 6 0 -14 8 686.574 45.6945 4 0 -14 -8 746.919 53.8559 2 0 -14 9 197.685 27.6023 6 0 -14 9 158.789 26.1015 4 0 -14 -9 173.861 32.3296 2 0 -14 -10 238.928 38.8845 2 0 -14 -11 97.5447 30.4128 2 0 -14 -12 1320.75 85.9827 2 0 -14 -13 649.043 66.0482 2 0 -12 1 8361.28 126.980 4 0 -12 -1 8239.65 127.715 4 0 -12 2 42.0246 16.4669 4 0 -12 -2 28.9606 15.9098 4 0 -12 3 24486.7 211.773 6 0 -12 -3 24824.0 230.951 4 0 -12 3 24902.9 219.870 4 0 -12 4 2693.30 72.3063 6 0 -12 -4 2817.92 81.4925 4 0 -12 4 2778.74 75.7003 4 0 -12 5 4597.32 97.9547 4 0 -12 5 4460.20 94.7629 6 0 -12 6 7556.25 126.220 6 0 -12 6 7516.60 127.563 4 0 -12 7 344.059 31.2945 6 0 -12 -7 354.556 34.6694 2 0 -12 8 1480.34 60.2732 6 0 -12 -8 1466.21 70.0435 2 0 -12 9 12991.4 175.839 6 0 -12 -9 12824.8 213.563 2 0 -12 -10 3523.63 120.155 2 0 -12 -11 68.0601 28.5639 2 0 -12 -12 429.717 52.4814 2 0 -12 -13 196.503 41.3980 2 0 -12 -14 43.0208 33.1002 2 0 -10 0 5785.68 96.3060 4 0 -10 1 103.438 17.5700 4 0 -10 -1 111.418 18.1091 4 0 -10 2 6561.23 98.6253 6 0 -10 -2 6643.21 107.017 4 0 -10 2 6562.13 101.562 4 0 -10 -3 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63.6681 2 0 -8 -11 66.6464 27.5569 2 0 -8 -12 6767.83 173.411 2 0 -8 -13 2396.92 114.459 2 0 -8 -14 596.440 66.1669 2 0 -6 1 4031.24 59.2924 6 0 -6 1 4171.94 61.7159 4 0 -6 -1 4161.92 64.7226 4 0 -6 2 25680.1 150.102 6 0 -6 -3 14798.1 133.657 4 0 -6 3 14565.8 118.513 1 0 -6 4 107.141 14.4345 1 0 -6 5 3322.12 63.2121 1 0 -6 -5 3528.03 77.2779 2 0 -6 -6 36292.4 267.740 2 0 -6 6 35597.3 215.261 1 0 -6 7 129.800 22.8555 8 0 -6 -7 146.099 24.1682 2 0 -6 7 154.159 18.9474 1 0 -6 8 90.1864 23.1411 8 0 -6 8 59.9064 17.1251 1 0 -6 -8 56.1417 18.9160 2 0 -6 9 955.806 58.6713 8 0 -6 -9 1017.82 58.8823 2 0 -6 9 913.546 41.7636 1 0 -6 -10 4035.31 121.621 2 0 -6 -11 520.381 47.7337 2 0 -6 -12 945.611 70.0788 2 0 -6 -13 617.950 61.4904 2 0 -6 -14 2.10672 30.1506 2 0 -4 0 10847.7 75.0186 3 0 -4 -1 387.617 18.1626 4 0 -4 1 384.097 16.9052 6 0 -4 1 386.060 14.7974 3 0 -4 2 11894.9 86.4156 1 0 -4 3 102540. 273.403 1 0 -4 4 11872.2 127.430 8 0 -4 -4 12146.0 124.087 2 0 -4 4 11865.1 102.702 1 0 -4 5 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45.7940 7 -2 2 2 2070.78 31.8772 4 -2 2 2 2125.66 31.8917 6 2 2 -2 2008.88 35.8559 2 2 2 -1 8232.48 68.3994 8 2 2 -1 8051.42 46.7512 4 -2 2 1 8002.11 70.9058 7 -2 2 1 8127.95 58.4706 1 2 2 0 66.8774 8.80693 5 -2 2 0 78.5485 10.0894 3 2 2 1 7491.60 74.7593 5 -2 2 -2 1650.08 31.3723 8 2 2 2 1582.83 34.0812 7 2 2 2 1701.95 30.6697 2 2 2 3 3770.84 62.3541 7 -2 2 -3 3669.63 60.5960 2 2 2 4 1613.73 48.2607 7 -2 2 -4 1534.48 45.2391 2 2 2 5 113.721 18.3981 7 -2 2 -5 155.834 19.8035 5 -2 2 -5 126.153 19.5431 2 -2 2 -6 3301.65 76.8695 5 -2 2 -6 3268.01 81.6709 2 2 2 7 4319.30 103.460 8 -2 2 -7 4148.72 93.2332 5 -2 2 -7 4270.21 101.668 2 2 2 8 1091.83 59.2444 8 -2 2 -8 1052.32 52.7874 5 -2 2 -8 1045.03 56.9933 2 2 2 9 630.542 50.8997 8 -2 2 -9 677.298 49.5866 2 2 2 10 1680.02 82.4051 8 -2 2 -10 1642.03 80.0977 2 2 2 11 1140.45 72.3453 8 -2 2 -11 1121.46 73.3194 2 2 2 12 1107.10 76.3408 8 -2 2 -12 1219.59 81.5299 2 2 2 13 1143.53 83.1962 8 2 2 14 738.211 71.7231 8 2 2 15 96.9064 87.2177 8 -2 4 14 3087.11 143.891 8 -2 4 13 992.328 80.7247 8 2 4 -13 1177.41 83.8882 2 -2 4 12 1015.13 77.7073 8 2 4 -12 942.916 73.0471 2 -2 4 11 472.860 52.0865 8 2 4 -11 478.759 50.8960 2 -2 4 10 449.066 49.6491 8 2 4 -10 433.221 44.9226 2 -2 4 9 92.3006 28.6341 8 2 4 -9 49.7113 22.2792 2 -2 4 8 6103.70 141.737 8 2 4 -8 6375.67 135.634 2 2 4 -7 147.397 16.7858 5 2 4 -7 123.235 22.9162 2 2 4 -6 7192.12 83.0227 5 -2 4 6 7144.24 136.022 7 2 4 -6 7192.98 121.602 2 -2 4 5 4115.90 96.3444 7 2 4 -5 3968.34 82.7137 2 -2 4 4 2974.06 73.8523 7 2 4 -4 3027.09 65.5231 2 -2 4 3 6122.77 94.6001 7 2 4 -3 5946.27 80.0132 2 -2 4 2 4294.46 70.8296 7 2 4 -2 4360.19 58.6621 2 2 4 -1 3488.97 44.6393 4 -2 4 1 3490.09 56.9380 3 -2 4 0 22.9745 8.95534 3 -2 4 -1 2592.66 48.0613 3 2 4 3 5778.36 84.2256 7 2 4 4 2488.13 62.5583 7 2 4 5 3117.90 77.5101 7 2 4 6 5133.45 108.399 7 -2 4 -6 4884.20 101.648 2 -2 4 -7 99.7029 19.7368 5 2 4 7 111.238 24.1372 7 -2 4 -7 82.5167 20.5075 2 -2 4 -8 8838.48 144.824 5 -2 4 -8 8910.37 161.951 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10 12 275.238 52.3085 8 -2 10 10 756.601 67.4088 7 -2 10 9 2099.56 101.419 7 -2 10 8 2420.64 102.925 7 -2 10 7 2157.31 92.3775 7 -2 10 6 60.7573 24.5073 7 -2 10 5 509.940 42.7341 7 2 10 -5 518.826 28.2852 3 -2 10 4 429.875 37.4620 7 2 10 -4 367.077 21.7140 3 2 10 -3 352.489 19.4784 3 2 10 -2 2893.78 49.3076 3 -2 10 0 26.1917 13.1867 3 -2 10 -1 7367.68 107.621 3 -2 10 -2 3267.00 73.8090 3 -2 10 -3 837.855 39.8556 3 -2 10 -4 559.778 35.4060 3 2 10 5 218.927 29.7531 7 -2 10 -5 233.697 26.4764 3 2 10 6 101.938 24.6435 7 -2 10 -6 85.2430 21.1463 3 2 10 7 2563.07 94.8325 7 2 10 8 1582.26 80.4440 7 2 10 9 1013.22 69.0846 7 2 10 10 1809.33 94.4722 7 -2 10 -10 1797.18 77.2262 5 2 10 12 765.411 70.1075 8 2 10 13 632.542 70.7376 8 2 10 14 257.115 50.7828 8 -2 12 13 397.923 59.1853 8 -2 12 12 277.019 51.7960 8 -2 12 10 3114.94 135.075 7 -2 12 9 2009.32 103.925 7 2 12 -9 2053.67 77.2385 3 -2 12 8 1443.30 85.3953 7 2 12 -8 1388.92 59.6521 3 -2 12 7 217.026 36.4088 7 2 12 -7 190.554 22.8783 3 -2 12 6 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5 235.321 37.2025 7 2 14 -5 228.759 22.9697 3 2 14 -4 156.188 17.0187 3 2 14 -3 1314.84 43.6876 3 -2 14 -1 5991.96 114.098 3 -2 14 -2 36.9405 15.4820 3 -2 14 -3 1441.84 58.2232 3 -2 14 -4 87.0598 20.3655 3 -2 14 -5 150.568 25.2144 3 2 14 6 754.531 58.3067 7 -2 14 -6 814.669 51.0246 3 2 14 7 4583.20 140.991 7 -2 14 -7 4897.99 126.005 3 2 14 8 69.7308 30.7786 7 -2 14 -8 75.9505 26.3292 3 2 14 9 77.0907 31.1877 7 -2 14 -9 87.4862 27.1982 3 2 14 10 233.438 44.5382 7 -2 14 -10 265.599 41.5047 3 2 14 11 1270.98 92.2414 7 -2 14 -11 1317.51 81.1486 3 2 14 13 519.209 66.2657 8 -2 16 11 816.949 82.9967 7 -2 16 10 15.1423 34.4331 7 -2 16 9 461.420 58.8282 7 -2 16 8 142.001 38.4770 7 -2 16 7 5046.48 162.790 7 -2 16 6 76.6447 31.5587 7 2 16 -6 80.5589 19.6448 3 -2 16 5 6203.05 166.319 7 2 16 -5 5993.91 102.781 3 2 16 -4 111.104 17.8232 3 -2 16 -1 5054.81 112.390 3 -2 16 -2 737.053 45.2063 3 -2 16 -3 117.909 21.2090 3 -2 16 -4 32.9905 19.2160 3 -2 16 -5 7422.21 145.778 3 2 16 6 71.7939 29.8917 7 -2 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680.280 66.1658 4 -3 -27 0 56.2839 32.0136 4 3 -27 0 58.7101 32.9202 4 3 -27 1 118.472 36.3809 4 3 -27 2 339.782 50.6675 4 3 -27 3 36.4303 31.0194 4 3 -27 4 106.057 35.9344 4 3 -27 5 189.399 43.5757 4 3 -27 6 132.492 38.5620 4 3 -27 7-34.8133 37.3232 4 3 -25 -9 121.052 39.8534 2 3 -25 -8 947.026 76.4497 2 -3 -25 6 26.9107 26.8546 4 -3 -25 5 194.794 37.8980 4 3 -25 -5 259.971 44.8732 4 -3 -25 4 517.930 54.6832 4 3 -25 -4 490.600 55.4666 4 -3 -25 3 82.1250 32.0155 4 3 -25 -3 66.1007 31.7622 4 3 -25 -2 322.673 47.6928 4 -3 -25 2 388.290 49.7476 4 3 -25 -1 950.582 72.1874 4 -3 -25 1 913.979 71.4188 4 -3 -25 0 769.340 66.9100 4 3 -25 0 883.871 70.3538 4 3 -25 1 892.806 70.2928 4 -3 -25 -1 977.482 74.4749 4 3 -25 2 208.638 41.4536 4 3 -25 3 24.3664 28.4834 4 3 -25 4 83.7807 33.6429 4 3 -25 5 221.806 41.3707 4 3 -25 6 7.06241 28.4405 4 3 -25 7 524.322 59.5846 4 -3 -25 -7 564.900 54.4657 2 3 -25 8 161.829 103.307 4 3 -23 -10 423.931 60.2118 2 3 -23 -9 90.4204 36.1649 2 3 -23 -8 106.308 36.8631 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4 5 -7 -4 2348.81 56.6757 4 5 -7 -3 1863.46 51.7446 4 5 -7 -2 2308.06 56.1476 4 5 -7 -2 2271.17 54.8274 6 5 -7 -1 1011.92 39.8738 6 5 -7 0 47.9479 14.6679 1 5 -7 1 4726.95 85.2410 1 5 -7 2 461.707 30.6713 1 -5 -7 -2 405.363 16.8067 2 -5 -7 -3 6117.97 72.3029 2 5 -7 3 6410.46 108.400 1 -5 -7 -4 601.039 27.7197 2 5 -7 4 613.135 39.0042 1 5 -7 5 387.816 35.1263 1 -5 -7 -5 352.368 25.2672 2 5 -7 6 971.790 51.3484 1 -5 -7 -6 1030.67 45.3712 2 5 -7 7 490.020 40.2398 1 -5 -7 -7 432.178 33.3006 2 -5 -7 -8 138.320 22.4110 2 5 -7 8 151.073 28.9162 1 -5 -7 -9 1628.96 71.7847 2 5 -7 9 1660.32 74.5362 1 -5 -7 -10 520.830 47.8557 2 5 -7 10 557.965 50.9901 1 5 -7 11 284.427 38.4888 1 -5 -7 -11 220.336 36.9456 2 -5 -7 -12 257.167 42.6115 2 -5 -7 -13 43.5218 30.1625 2 -5 -7 -14 50.7219 35.0032 2 5 -5 -14 201.381 45.5897 2 5 -5 -13 346.242 50.0977 2 -5 -5 12 67.8153 35.3266 8 5 -5 -12-43.2635 29.5303 2 -5 -5 11 871.995 69.3823 8 5 -5 -11 976.598 69.1364 2 -5 -5 10 1394.03 80.4802 8 5 -5 -10 1212.76 71.8149 2 -5 -5 9 164.378 31.4303 8 5 -5 -9 137.301 28.7544 2 -5 -5 8 425.664 43.9228 8 5 -5 -8 398.688 38.8137 2 -5 -5 7 323.526 35.2655 8 5 -5 -7 429.193 37.1183 2 -5 -5 6 27.0566 18.8477 8 5 -5 -6 13.7403 14.8774 2 -5 -5 5 2801.52 78.2780 8 5 -5 -5 3027.64 55.8176 4 5 -5 -5 2901.92 76.6464 2 5 -5 -4 3669.28 61.8399 4 -5 -5 4 3668.70 82.1163 8 5 -5 -3 473.778 23.8948 4 5 -5 -2 1495.86 40.0350 6 -5 -5 1 256.063 12.6346 2 5 -5 -1 280.175 21.4386 1 -5 -5 1 238.669 8.46263 3 5 -5 0 319.778 22.3801 1 -5 -5 0 291.626 8.52138 2 5 -5 1 723.205 33.5965 1 -5 -5 -2 387.636 14.1837 2 -5 -5 -3 1533.21 35.2467 2 -5 -5 -4 5978.74 81.7797 2 -5 -5 -5 494.331 28.5327 2 -5 -5 -6 28.3743 12.7147 2 -5 -5 -7 116.173 20.9842 2 -5 -5 -8 1101.57 55.1678 2 -5 -5 -9 60.2476 21.7552 2 -5 -5 -10 704.087 53.6679 2 -5 -5 -11 732.303 59.1826 2 5 -5 11 670.096 53.4752 1 5 -5 12-11.3791 26.0349 1 -5 -5 -12 55.9455 30.1911 2 -5 -5 -13 216.282 42.8689 2 -5 -5 -14 535.131 63.2868 2 -5 -3 14 95.0681 42.8145 8 5 -3 -14 74.8833 37.7275 2 -5 -3 13 58.8564 36.0102 8 5 -3 -13 60.4504 34.0133 2 -5 -3 12 706.982 66.6208 8 5 -3 -12 674.147 60.9842 2 -5 -3 11 16.7696 27.8794 8 5 -3 -11 52.3654 26.5483 2 -5 -3 10 34.4584 26.4222 8 5 -3 -10-7.20229 22.1851 2 -5 -3 9 4.34021 20.8929 8 5 -3 -9 8.80438 18.2723 2 -5 -3 8 81.7031 28.3986 8 5 -3 -8 66.3091 21.8455 2 -5 -3 7 84.0702 22.8760 8 5 -3 -7 64.5323 18.3095 2 -5 -3 6 1417.57 61.4174 8 5 -3 -6 1390.26 56.8839 2 -5 -3 5 1025.76 48.9436 8 5 -3 -5 1040.81 45.6444 2 5 -3 -4 872.880 25.1567 4 -5 -3 4 880.530 40.9448 8 5 -3 -4 847.686 37.4740 2 5 -3 -3 685.413 23.1137 4 -5 -3 3 693.355 32.7083 8 5 -3 -2 119.666 12.6855 6 -5 -3 2 125.553 14.7241 8 5 -3 -2 139.900 13.6195 1 5 -3 -1 1014.68 31.1944 1 -5 -3 1 1031.31 22.5146 3 -5 -3 0 1330.44 39.0490 5 -5 -3 -1 1112.06 39.5987 5 -5 -3 -2 598.438 33.0539 5 -5 -3 -2 606.703 17.1720 2 -5 -3 -3 148.653 21.4695 5 -5 -3 -3 181.523 13.6532 2 -5 -3 -4 431.444 32.7885 5 -5 -3 -4 441.754 23.6650 2 5 -3 5 874.518 34.4685 8 -5 -3 -5 939.909 49.5442 5 -5 -3 -5 932.543 38.2320 2 5 -3 6 300.042 25.4917 8 -5 -3 -6 334.602 28.2069 2 5 -3 7 22.7685 13.9660 8 -5 -3 -7 48.5104 16.8211 2 5 -3 8 585.661 39.4772 8 -5 -3 -8 577.856 42.3981 2 5 -3 9 18.6474 18.0655 8 -5 -3 -9 29.8328 20.4677 2 5 -3 10 11.8147 18.2503 8 -5 -3 -10-22.3867 22.1798 2 5 -3 11 47.1972 24.4244 8 -5 -3 -11-4.60442 21.5708 2 -5 -3 -12 174.231 38.5092 2 -5 -3 -13 62.8979 36.5387 2 -5 -1 14 241.465 52.6154 8 5 -1 -14 189.130 47.2074 2 -5 -1 13 370.380 56.1491 8 5 -1 -13 355.886 51.4264 2 -5 -1 12 149.783 39.9503 8 5 -1 -12 85.7691 32.5538 2 -5 -1 11 204.184 41.4019 8 5 -1 -11 130.283 32.3380 2 -5 -1 10 288.648 42.2630 8 5 -1 -10 298.224 36.1970 2 -5 -1 9 175.091 32.8282 8 5 -1 -9 135.185 26.5952 2 -5 -1 8 1795.81 80.0862 8 5 -1 -8 1713.23 70.9600 2 -5 -1 7 4774.23 119.341 8 5 -1 -7 4472.39 104.666 2 -5 -1 6 351.508 34.9795 8 5 -1 -6 364.311 30.9959 2 -5 -1 5 505.225 36.0391 8 5 -1 -5 472.448 30.8834 2 -5 -1 4 1274.84 48.7441 8 5 -1 -4 1314.58 44.6589 2 -5 -1 3 51.4633 12.8977 8 5 -1 -3 67.0183 7.37482 4 5 -1 -3 71.0068 13.1980 2 -5 -1 2 1421.96 40.0870 8 -5 -1 2 1458.91 26.6412 5 5 -1 -2 1465.60 29.5835 1 -5 -1 1 2582.56 43.5104 8 -5 -1 1 2671.13 44.1399 5 -5 -1 1 2529.21 43.1718 3 -5 -1 0 1224.21 34.6145 5 -5 -1 0 1249.08 32.0496 3 -5 -1 -1 4535.24 72.0775 5 -5 -1 -2 508.892 29.1051 5 5 -1 3 137.012 10.1509 8 -5 -1 -3 109.201 17.9532 5 5 -1 4 1292.72 35.1015 8 -5 -1 -4 1280.79 51.8923 5 -5 -1 -4 1426.09 42.1948 2 5 -1 5 900.604 35.1372 8 -5 -1 -5 976.037 47.9295 5 -5 -1 -5 948.754 39.8555 2 -5 -1 -6 1171.97 56.7844 5 5 -1 6 1105.75 43.7488 8 -5 -1 -6 1203.76 49.8334 2 5 -1 7 2016.99 65.3591 8 -5 -1 -7 2241.14 81.1538 5 -5 -1 -7 2179.95 72.5765 2 5 -1 8 445.730 36.7423 8 -5 -1 -8 495.471 41.3123 2 5 -1 9 145.950 26.8722 8 -5 -1 -9 76.6361 23.3136 2 5 -1 10 45.5355 21.8217 8 -5 -1 -10 66.4985 25.9679 2 5 -1 11 335.285 40.6770 8 -5 -1 -11 296.403 41.8359 2 5 -1 12 42.8084 26.5101 8 5 -1 13 130.436 36.7019 8 -5 1 14 238.087 51.2010 8 5 1 -14 189.535 44.5588 2 -5 1 13 409.602 59.5779 8 5 1 -13 322.306 50.4131 2 -5 1 12 61.2817 34.4841 8 5 1 -12 95.1869 32.8207 2 -5 1 11 149.436 36.0880 8 5 1 -11 202.423 37.6642 2 -5 1 10 281.001 40.4311 8 5 1 -10 311.843 38.7942 2 -5 1 9 143.093 30.3590 8 5 1 -9 162.517 28.2192 2 -5 1 8 1746.68 80.4029 8 5 1 -8 1658.34 66.8698 2 -5 1 7 4647.55 120.587 8 5 1 -7 4442.33 104.314 2 -5 1 6 399.780 38.4602 8 5 1 -6 390.103 31.5517 2 -5 1 5 503.649 36.6861 8 -5 1 5 472.784 13.9299 5 5 1 -5 469.722 30.8653 2 -5 1 4 1280.26 49.5265 8 5 1 -4 1299.92 43.1153 2 -5 1 3 75.7372 15.1931 8 5 1 -3 57.8290 11.4209 2 -5 1 2 1435.36 40.3475 8 5 1 -2 1471.54 34.8892 2 -5 1 1 2470.81 43.4454 8 -5 1 1 2528.55 49.8657 3 5 1 -1 2508.46 35.9780 2 5 1 0 1184.90 23.0551 8 -5 1 0 1140.42 20.9629 8 -5 1 0 1246.35 35.8104 3 -5 1 -1 4658.41 72.4119 3 5 1 1 4585.11 37.8113 2 5 1 2 454.146 14.0657 7 5 1 2 488.298 16.8216 2 -5 1 -3 116.396 10.7433 7 5 1 4 1254.76 36.2677 8 -5 1 -4 1316.43 51.0462 5 5 1 5 912.816 37.2997 8 -5 1 -5 915.940 45.5071 5 5 1 6 1162.32 48.1782 8 -5 1 -6 1157.63 55.3082 5 5 1 7 2084.96 68.8988 8 -5 1 -7 2290.00 81.0564 5 -5 1 -7 2268.29 75.7117 2 -5 1 -8 532.789 45.6496 5 5 1 8 477.528 38.3025 8 -5 1 -8 493.550 41.4542 2 5 1 9 76.6472 22.1041 8 -5 1 -9 106.851 29.7084 5 -5 1 -9 85.6697 24.7318 2 5 1 10 69.5529 24.8055 8 5 1 11 308.705 41.6460 8 5 1 12 48.6432 26.7855 8 5 1 13 143.496 38.0353 8 -5 3 14 84.9198 42.7754 8 5 3 -14 87.2348 209.147 2 -5 3 13-40.7450 34.3946 8 5 3 -13 0.77022 27.4589 2 -5 3 12 745.646 69.7278 8 5 3 -12 710.227 63.6367 2 -5 3 11 44.3232 28.8839 8 5 3 -11 20.5889 24.5202 2 -5 3 10-36.1451 30.2079 8 5 3 -10 10.9725 21.4213 2 -5 3 9 2.16004 22.9423 8 5 3 -9 26.6467 20.4888 2 -5 3 8 81.6177 28.2598 8 5 3 -8 107.046 25.5383 2 -5 3 7 121.744 25.9435 8 5 3 -7 121.706 22.9180 2 -5 3 6 1391.43 62.8360 8 5 3 -6 1375.32 53.5455 2 5 3 -5 1006.24 41.4536 2 -5 3 4 847.044 42.5770 7 5 3 -4 813.941 33.6315 2 5 3 -3 681.917 13.2443 4 -5 3 3 690.648 35.0817 7 5 3 -3 644.969 26.8915 2 5 3 -3 685.734 22.6252 3 -5 3 2 109.145 16.2361 7 5 3 -2 96.0855 9.25144 4 5 3 -2 131.208 11.9391 2 5 3 -2 117.392 9.25048 3 -5 3 1 1017.78 31.2807 7 5 3 -1 1048.28 21.8396 2 -5 3 1 1034.51 36.5028 3 -5 3 0 1350.31 29.2933 7 -5 3 0 1441.56 42.6356 3 -5 3 -1 1140.73 39.6479 3 -5 3 -2 597.365 16.9279 8 -5 3 -2 639.897 32.9343 3 5 3 3 165.123 14.8864 7 5 3 4 457.511 25.8960 7 5 3 5 966.876 40.6562 7 -5 3 -6 306.668 31.6367 5 -5 3 -7 40.0441 20.9137 5 5 3 7 53.4475 18.7270 8 -5 3 -8 458.479 41.6357 5 5 3 8 551.380 41.5760 8 5 3 9 23.4272 19.4569 8 -5 3 -9 57.5600 23.5554 5 5 3 10 8.92530 20.5767 8 -5 3 -10 65.7148 28.5559 5 5 3 11 21.4954 22.0070 8 5 3 12 94.5657 30.6978 8 5 3 13 40.7471 31.2123 8 -5 5 14 241.601 50.1274 8 -5 5 13 357.417 55.8995 8 5 5 -13 287.894 50.9466 2 -5 5 12-37.0973 37.8199 8 5 5 -12-11.9986 25.9711 2 -5 5 11 925.476 74.4650 8 5 5 -11 916.894 67.8356 2 -5 5 10 1411.62 86.5099 8 5 5 -10 1294.77 73.7602 2 -5 5 9 172.368 35.4480 8 5 5 -9 167.291 30.0327 2 -5 5 8 414.349 45.5257 8 5 5 -8 425.386 40.2327 2 5 5 -7 357.534 33.5577 2 -5 5 6 11.5331 19.1608 7 5 5 -6 3.74060 13.7684 2 -5 5 5 2887.96 85.9686 7 5 5 -5 2970.61 73.5684 2 -5 5 4 3684.23 90.5302 7 5 5 -4 3830.01 75.5307 2 5 5 -3 421.681 15.2098 6 5 5 -3 426.919 16.7043 4 5 5 -3 463.547 17.9879 5 -5 5 3 439.394 31.1228 7 5 5 -3 398.139 13.2519 3 5 5 -3 474.581 24.7668 2 -5 5 2 1525.49 47.6642 7 5 5 -2 1534.36 36.2644 2 -5 5 1 324.406 21.6522 7 -5 5 1 256.412 22.6473 3 -5 5 0 327.649 23.8758 3 -5 5 -1 741.909 34.0618 3 -5 5 -2 367.372 27.5639 3 -5 5 -3 1595.75 55.6112 3 5 5 4 5784.01 92.1585 7 5 5 5 535.554 33.9944 7 5 5 6 49.6156 16.3703 7 5 5 7 129.328 23.6000 7 -5 5 -7 139.040 27.4849 5 -5 5 -8 1140.91 62.3464 5 -5 5 -9 1.74968 19.9070 5 5 5 9 73.6832 24.1801 8 5 5 10 755.492 58.6015 8 -5 5 -10 809.369 59.7631 5 -5 5 -11 810.980 64.1610 5 5 5 11 699.712 59.1419 8 5 5 12 39.9281 28.6446 8 5 5 13 161.488 38.3027 8 -5 7 14 11.9491 37.9745 8 -5 7 13 427.010 59.9884 8 -5 7 12 1105.37 86.6665 8 -5 7 11 33.3014 30.0266 8 5 7 -11 38.8769 26.2172 2 -5 7 10 3378.51 128.981 8 5 7 -10 3658.21 123.058 2 5 7 -9 2005.12 86.2599 2 -5 7 8 86.8228 27.6363 7 5 7 -8 53.7796 20.4321 2 -5 7 7 944.388 60.6653 7 5 7 -7 969.998 53.3522 2 -5 7 6 1861.73 78.4919 7 5 7 -6 1893.02 66.9942 2 -5 7 5 2105.58 76.3534 7 5 7 -5 2108.23 64.7198 2 -5 7 4 2218.27 73.3722 7 -5 7 3 1803.74 63.8587 7 -5 7 2 2362.57 64.3015 7 -5 7 1 997.275 45.8820 3 -5 7 0 56.0860 15.0056 3 -5 7 -1 4775.37 91.6254 3 -5 7 -2 425.989 32.1000 3 -5 7 -3 5994.41 108.787 3 5 7 4 596.477 34.6769 7 -5 7 -4 561.689 39.1100 3 5 7 5 353.704 30.4706 7 5 7 6 1019.63 51.7204 7 5 7 7 490.906 40.7227 7 5 7 8 160.946 27.2630 7 -5 7 -8 221.637 33.7512 5 -5 7 -9 1604.38 77.0763 5 5 7 10 529.864 51.1133 8 -5 7 -10 645.232 56.5125 5 5 7 11 285.147 42.6378 8 -5 7 -11 294.933 43.6784 5 5 7 12 90.4019 31.4409 8 -5 7 -12 305.329 46.5059 5 5 7 13 5.56792 26.3271 8 -5 9 13 336.711 58.1725 8 -5 9 12 240.034 50.7539 8 -5 9 11 161.816 41.4010 8 -5 9 9 1052.65 75.3927 7 -5 9 8 715.761 59.8102 7 -5 9 7 227.684 37.1824 7 -5 9 6 172.191 31.0224 7 -5 9 5 442.110 40.5993 7 5 9 -5 413.704 16.7572 3 -5 9 4 172.213 27.4841 7 -5 9 3 697.375 43.1188 7 -5 9 1 515.090 37.3530 3 -5 9 0 228.541 24.4903 3 -5 9 -1 2354.16 69.2315 3 -5 9 -2 278.107 27.8488 3 -5 9 -3 152.247 25.3299 3 -5 9 -4 372.472 33.5666 3 5 9 5 574.427 40.0826 7 -5 9 -5 557.425 41.9197 3 5 9 6 618.079 43.5113 7 -5 9 -6 523.236 43.6168 3 5 9 7 1013.03 57.3948 7 5 9 8 123.318 29.9383 7 5 9 9 182.313 34.4370 7 -5 9 -9 251.704 37.8510 5 -5 9 -10 605.160 53.2320 5 -5 9 -11 262.092 40.5838 5 5 9 11 333.343 46.4912 8 5 9 12 177.550 39.5303 8 5 9 13 19.0043 29.9909 8 -5 11 13 382.161 63.5126 8 -5 11 12 1026.93 89.1267 8 -5 11 11 185.782 45.5975 8 -5 11 9 63.9121 34.0574 7 -5 11 8 1577.28 89.2211 7 -5 11 7 1391.63 80.3542 7 -5 11 6 1167.99 70.1414 7 -5 11 5 324.114 39.2312 7 5 11 -5 120.673 7.42852 3 -5 11 4 3281.17 102.241 7 -5 11 3 997.994 55.1470 7 -5 11 1 47.6716 19.7250 3 -5 11 0 365.871 32.3195 3 -5 11 -1 67.6695 18.7259 3 -5 11 -2 1332.45 58.4886 3 -5 11 -3 152.772 25.9072 3 -5 11 -4 5546.94 122.972 3 5 11 5 1592.42 67.7757 7 -5 11 -5 1489.33 68.0788 3 5 11 6 2134.98 82.0888 7 -5 11 -6 2243.76 86.8092 3 5 11 7 213.292 34.5336 7 -5 11 -7 251.518 36.4572 3 5 11 8 245.136 37.1964 7 -5 11 -8 257.047 39.8374 3 5 11 9-13.8688 21.8827 7 -5 11 -9 34.9296 26.5673 3 5 11 10 636.274 58.5643 7 -5 11 -10 695.375 57.6915 5 -5 11 -10 571.704 58.1407 3 -5 11 -11 78.5089 32.0956 5 -5 11 -11 60.2199 34.5936 3 5 11 12 940.180 76.0104 8 -5 11 -12 806.217 75.1832 3 5 11 13 274.176 50.9396 8 -5 11 -13 383.621 58.3109 3 -5 11 -14 325.597 59.8676 3 -5 13 13 563.585 73.5177 8 -5 13 12 1099.07 94.6538 8 -5 13 10 775.986 75.4477 7 -5 13 9 2692.54 125.318 7 -5 13 8 166.820 40.2316 7 -5 13 7 4047.93 138.506 7 -5 13 6 1049.64 71.6145 7 -5 13 5 146.469 31.2586 7 -5 13 4 476.268 44.9858 7 -5 13 1 3689.80 100.750 3 -5 13 0 2150.45 76.5463 3 -5 13 -1 5461.68 119.485 3 -5 13 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0 28.9659 16.8622 6 6 -10 1 5322.31 103.923 1 6 -10 2 1751.99 63.0069 1 6 -10 3 20.3827 18.8422 1 -6 -10 -3 34.5321 10.1215 2 6 -10 4 69.1211 23.5138 1 -6 -10 -4 100.333 15.0216 2 -6 -10 -5 90.3072 16.4505 2 6 -10 5 78.0733 23.4289 1 6 -10 6 421.568 40.0794 1 -6 -10 -6 446.780 31.0501 2 6 -10 7 1156.87 62.9612 1 -6 -10 -7 1123.01 52.3825 2 6 -10 8 3050.71 101.815 1 -6 -10 -8 2967.64 88.2625 2 6 -10 9 1834.78 82.9384 1 -6 -10 -9 1742.01 73.9228 2 6 -10 10 1056.18 66.5748 1 -6 -10 -10 1037.10 62.7550 2 -6 -10 -11 174.159 33.3297 2 6 -10 11 180.322 36.9798 1 -6 -10 -12 195.654 39.0436 2 -6 -10 -13 152.610 38.2172 2 6 -8 -13 632.209 66.2264 2 6 -8 -12 489.546 56.8157 2 6 -8 -11 755.885 64.2121 2 6 -8 -10 10.4837 23.2680 2 6 -8 -9 92.5087 28.4090 2 6 -8 -8 155.888 29.6369 2 6 -8 -7 2433.32 88.8048 2 6 -8 -6 63.1180 14.4874 4 6 -8 -6 65.9174 21.5596 2 6 -8 -5 17952.8 168.813 4 6 -8 -4 2712.79 66.2519 4 6 -8 -3 3298.33 72.3711 4 6 -8 -2 4646.41 86.3335 4 6 -8 -2 4668.27 85.2603 6 6 -8 -1 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49.0980 2 -7 5 11 800.623 71.3686 8 7 5 -11 693.233 60.1745 2 -7 5 10 822.061 68.5594 8 7 5 -10 835.983 61.0377 2 -7 5 9 12.2546 23.1669 8 7 5 -9 23.1281 54.2895 2 -7 5 8 68.2936 28.3318 8 7 5 -8 65.6003 22.4119 2 -7 5 7 604.754 50.9170 8 7 5 -7 701.157 45.4516 2 7 5 -6 1514.22 58.8285 2 -7 5 5 599.504 42.4824 7 7 5 -5 634.701 36.0761 2 -7 5 4 147.848 24.3618 7 7 5 -4 131.892 12.4060 3 7 5 -4 170.243 19.4104 2 -7 5 3 753.600 41.4100 7 7 5 -3 816.318 32.4056 2 -7 5 2 547.604 30.9260 7 -7 5 2 610.411 36.2753 3 7 5 -2 596.343 23.6414 2 -7 5 1 723.099 31.7631 7 -7 5 1 787.987 39.7293 3 -7 5 0 1029.48 32.2459 7 -7 5 0 1088.93 45.4946 3 -7 5 -1 194.737 22.0970 3 -7 5 -2 912.409 45.1272 3 7 5 3 1540.08 41.9390 7 -7 5 -3 1560.92 59.4154 3 7 5 4 683.677 31.9290 7 -7 5 -4 737.448 45.9082 3 7 5 5 364.365 26.8025 7 7 5 6 248.683 26.6878 7 -7 5 -7 1274.01 66.5820 5 -7 5 -8 249.210 35.2741 5 7 5 8 244.848 29.6018 8 -7 5 -9 66.0514 28.0368 5 7 5 9 41.4379 19.8967 8 -7 5 -10 325.193 44.9027 5 7 5 10 282.378 36.6307 8 7 5 11 144.262 32.4155 8 -7 5 -11 193.024 40.4206 5 -7 7 13 113.048 42.2317 8 -7 7 11 147.521 40.3297 8 7 7 -11 185.362 38.1356 2 -7 7 10 569.605 59.4636 8 7 7 -10 562.081 54.1437 2 -7 7 9 760.168 62.0368 8 7 7 -9 727.845 54.1571 2 7 7 -8 49.8250 22.5148 2 -7 7 7 2195.65 92.2882 7 7 7 -7 2072.39 76.8386 2 -7 7 6 1640.22 75.8731 7 7 7 -6 1598.16 62.3320 2 -7 7 5 163.911 29.4500 7 7 7 -5 185.270 23.0933 2 -7 7 4 546.610 40.3480 7 7 7 -4 524.178 30.5686 2 -7 7 3 3365.23 85.3681 7 -7 7 2 1037.60 46.4996 7 -7 7 2 1015.76 51.1597 3 -7 7 1 9265.62 119.931 7 -7 7 1 9503.20 140.859 3 -7 7 0 2388.54 71.4944 3 -7 7 -1 3013.47 82.6655 3 -7 7 -2 4881.14 105.181 3 -7 7 -3 1194.14 57.8006 3 7 7 4 304.044 25.0544 7 -7 7 -4 305.004 32.9074 3 7 7 5 664.350 37.9143 7 -7 7 -5 623.844 47.1199 3 7 7 6 220.730 27.0089 7 7 7 7 2126.95 76.2035 7 -7 7 -8 298.698 38.8329 5 -7 7 -9 162.920 34.6691 5 7 7 9 118.030 27.0039 8 7 7 10 877.925 60.2829 8 -7 7 -10 923.437 68.5665 5 7 7 11 54.9080 26.6364 8 -7 7 -11 117.305 38.6316 5 -7 7 -12 768.254 69.5023 5 -7 9 13 189.918 44.3329 8 -7 9 12 472.439 65.5268 8 -7 9 11 16.3651 30.9189 8 -7 9 10 1068.50 80.3748 8 -7 9 8 320.367 43.0776 7 -7 9 7 363.632 42.9243 7 -7 9 6 594.276 51.2246 7 -7 9 5 114.597 25.7102 7 -7 9 4 3638.29 101.202 7 -7 9 3 128.498 23.6391 7 -7 9 2 562.931 38.1104 7 -7 9 2 617.568 43.0532 3 -7 9 1 257.784 28.9115 3 -7 9 0 152.722 23.9786 3 -7 9 -1 294.261 29.8902 3 -7 9 -2 733.064 45.4809 3 -7 9 -3 237.406 30.0030 3 -7 9 -4 759.088 50.5854 3 7 9 5 33.1132 15.9644 7 -7 9 -5 18.2039 20.1472 3 7 9 6 77.6895 22.3877 7 -7 9 -6 91.2397 27.1617 3 7 9 7 87.4636 23.5534 7 -7 9 -7 100.055 29.1518 3 7 9 8 126.396 27.2354 7 -7 9 -8 112.306 32.0963 3 -7 9 -9 158.933 35.0175 5 -7 9 -9 54.4125 30.2837 3 -7 9 -10 148.023 36.8583 5 7 9 10 113.022 31.6226 8 -7 9 -11 14.4829 28.9458 5 7 9 11 49.9656 27.2487 8 -7 9 -12 345.273 51.8926 5 -7 9 -12 394.421 60.5513 3 -7 9 -13 48.7846 35.3358 3 -7 11 13 157.865 47.1250 8 -7 11 12 442.968 65.1153 8 -7 11 11 44.6063 36.6023 8 -7 11 9 90.2184 37.2499 7 -7 11 8 378.802 50.8527 7 -7 11 7 6.07551 22.4335 7 -7 11 6 1469.35 77.4641 7 -7 11 5 346.199 42.0728 7 -7 11 4 4422.53 119.500 7 -7 11 3 1592.43 68.6204 7 -7 11 2 1174.29 57.0962 7 -7 11 1 31.2872 20.0499 3 -7 11 0 2936.35 88.9619 3 -7 11 -1 141.143 24.9704 3 -7 11 -2 1872.19 74.3015 3 -7 11 -3 1159.39 62.2840 3 -7 11 -4 3369.81 104.744 3 7 11 5 1335.25 61.5232 7 -7 11 -5 1283.14 69.0000 3 7 11 6 213.254 30.0431 7 -7 11 -6 258.773 37.9657 3 7 11 7 129.948 26.5595 7 -7 11 -7 143.898 32.0474 3 7 11 8 470.520 46.0068 7 -7 11 -8 486.193 51.3827 3 7 11 9 307.815 41.1587 7 -7 11 -9 354.318 47.7510 3 -7 11 -10 964.426 71.4959 5 -7 11 -10 828.240 70.6722 3 -7 11 -11 295.951 46.2033 5 7 11 11 338.406 46.3507 8 -7 11 -11 352.745 53.4421 3 -7 11 -12 32.2021 35.1181 5 -7 11 -12 85.9893 38.7572 3 -7 11 -13 103.729 42.8083 3 -7 13 12 331.400 61.0341 8 -7 13 11 39.0425 36.5207 8 -7 13 9 1496.36 97.6229 7 -7 13 8 1044.85 79.4022 7 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268.238 45.6532 3 7 17 9 26.7408 27.6669 7 -7 17 -9 0.12953 28.2980 3 7 17 10 337.241 53.0033 7 -7 17 -10 338.750 53.8207 3 7 17 11 85.7228 36.0894 7 -7 17 -11 167.531 45.9135 5 -7 17 -11 105.493 40.5075 3 -7 17 -12 378.466 63.4810 3 -7 19 11 832.940 93.5465 7 -7 19 10 946.763 94.7528 7 -7 19 9 826.299 87.6717 7 -7 19 8 263.920 51.8322 7 -7 19 7 1054.40 87.4280 7 -7 19 6 23.6811 29.5033 7 -7 19 5 66.0838 33.0984 7 -7 19 4 74.0327 34.7383 7 -7 19 -1 1264.24 77.0726 3 -7 19 -2 1116.14 72.7741 3 -7 19 -3 426.041 50.3857 3 -7 19 -4 31.2085 25.6655 3 -7 19 -5 458.741 51.7607 3 7 19 6 49.3371 32.0294 7 -7 19 -6 55.0575 29.5373 3 7 19 7 1056.11 79.1948 7 -7 19 -7 1005.90 77.0722 3 7 19 8 55.5578 33.1156 7 -7 19 -8 14.9717 30.8131 3 7 19 9 100.983 38.4310 7 -7 19 -9 68.2810 36.9982 3 7 19 10 252.903 51.8668 7 -7 19 -10 234.275 50.6170 3 -7 19 -11 36.1966 39.4189 3 -7 21 10 35.8056 43.2575 7 -7 21 9 1207.87 106.236 7 -7 21 8 150.583 48.4962 7 -7 21 7 1574.33 110.025 7 -7 21 6 243.301 51.8378 7 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25 4 53.0182 35.4775 7 -7 25 -4 12.3014 33.1734 3 -7 25 -5 386.101 58.3011 3 7 25 6 241.800 60.5131 7 -7 25 -6 86.0195 41.5919 3 7 25 7 197.261 50.4610 7 -7 25 -7 240.228 53.2975 3 7 25 8 364.307 61.9440 7 -7 27 6 19.2652 43.5102 7 -7 27 5 57.2963 40.6004 7 -7 27 4 277.077 57.6769 7 -7 27 3 276.446 59.6293 7 -7 27 -5 91.3316 40.3116 3 7 27 6 147.245 51.5740 7 7 27 7 135.109 49.3084 7 -7 29 4 120.067 51.2828 7 -7 29 3 278.968 67.3454 7 8 -28 -5 81.0467 35.9072 4 8 -28 -4 996.894 82.6554 4 8 -28 -3 1408.32 96.9461 4 8 -28 -2 1827.39 109.865 4 8 -28 -1 440.068 72.2142 4 8 -28 0 673.598 71.5246 4 8 -28 1 101.516 38.2256 4 8 -28 2 1629.33 105.360 4 8 -28 3 1905.64 114.724 4 8 -28 4 671.857 74.5707 4 8 -26 -6-4.30336 29.3040 4 8 -26 -5 23.2992 28.8889 4 8 -26 -4 371.607 53.9957 4 8 -26 -3 2615.42 123.848 4 8 -26 -2 563.902 62.9576 4 8 -26 -1 140.669 40.4343 4 8 -26 0 1160.75 86.1872 4 8 -26 1-17.3385 35.8145 4 8 -26 2 906.907 78.7254 4 8 -26 3 2484.05 124.177 4 8 -26 4 397.601 59.9214 4 8 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6 8 -22 3 200.134 40.7423 4 8 -22 3 255.819 45.4301 6 8 -22 4 80.8464 36.4849 6 8 -22 4 100.272 37.0406 4 8 -22 5 63.4036 36.7651 6 8 -22 5 91.4808 38.7730 4 8 -22 6 3709.08 141.038 6 8 -22 6 3570.43 141.315 4 8 -22 7 134.167 41.0610 4 8 -22 7 117.812 40.1951 6 8 -22 8 462.973 60.3775 6 8 -22 8 355.228 54.5744 4 8 -22 9 398.823 57.3585 6 8 -22 9 329.100 55.6203 4 8 -22 10 46.0668 41.1047 4 8 -20 -10 549.936 66.9508 2 8 -20 -9 3579.47 146.212 2 8 -20 -8 417.624 55.5484 2 8 -20 -7 725.815 59.3087 4 8 -20 -6 638.868 55.4945 4 8 -20 -5 38.9080 24.1061 4 8 -20 -4 1093.88 69.4915 4 8 -20 -3 9262.44 194.428 4 8 -20 -2 2181.39 97.4499 4 8 -20 -1 29.7934 24.1207 4 8 -20 0 1399.93 79.5230 4 8 -20 1 20.5585 26.4545 4 8 -20 1 14.3838 25.8773 6 8 -20 2 2085.14 95.9278 6 8 -20 2 2010.45 95.4211 4 8 -20 3 10509.5 210.918 6 8 -20 3 10289.4 213.044 4 8 -20 4 886.760 69.2171 4 8 -20 4 841.513 67.3838 6 8 -20 5 78.4471 33.7905 4 8 -20 5 85.1883 33.8007 6 8 -20 6 528.096 56.8215 6 8 -20 6 469.905 54.9723 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744.620 52.3910 4 8 -16 -4 846.378 54.8697 4 8 -16 -3 2024.75 82.3197 4 8 -16 -2 2885.59 97.1820 4 8 -16 -1 3234.87 101.563 6 8 -16 -1 3225.50 103.498 4 8 -16 0 12562.4 198.914 6 8 -16 0 12075.2 198.053 4 8 -16 1 2372.94 92.0200 4 8 -16 1 2398.07 90.8925 6 8 -16 2 2464.64 94.2293 6 8 -16 3 2377.43 93.8367 6 8 -16 4 698.486 56.2466 6 8 -16 5 1267.12 73.8990 6 8 -16 6 2911.17 111.722 6 8 -16 6 2981.92 111.515 1 8 -16 7 2438.42 106.089 6 8 -16 7 2478.30 105.311 1 8 -16 8 370.833 49.0005 6 8 -16 8 520.225 55.4726 1 8 -16 9 573.345 60.5703 6 8 -16 9 639.887 61.7886 1 8 -16 10 28.6024 32.5189 6 8 -16 11 70.5454 36.2076 6 8 -14 -12 1398.67 97.4771 2 8 -14 -11 76.0082 36.1668 2 8 -14 -10 149.114 41.5269 2 8 -14 -9 73.1130 33.2911 2 8 -14 -8 1007.71 71.1210 2 8 -14 -7 541.276 42.4566 4 8 -14 -6 6437.56 135.878 4 8 -14 -5 165.086 27.0944 4 8 -14 -4 261.415 32.3878 4 8 -14 -3 1717.90 71.1734 4 8 -14 -2 426.824 38.1154 6 8 -14 -2 452.417 39.7601 4 8 -14 -1 457.454 39.8984 6 8 -14 -1 517.836 42.0600 4 8 -14 0 3222.50 96.5875 6 8 -14 1 239.244 33.6357 6 8 -14 2 237.303 33.0505 6 8 -14 3 1505.74 72.1816 6 -8 -14 -3 1505.09 40.8997 2 8 -14 3 1561.14 72.9541 1 8 -14 4 630.038 50.6326 1 -8 -14 -4 629.773 29.7503 2 8 -14 5 267.272 39.2573 1 8 -14 6 5622.35 146.253 1 8 -14 7 434.782 48.2635 1 8 -14 8 950.668 69.0640 1 8 -14 9 52.7857 32.6430 1 8 -14 10 77.1269 34.3930 1 8 -14 11 136.317 40.6534 1 8 -12 -12 323.593 51.2129 2 8 -12 -11 246.281 46.7812 2 8 -12 -10 3287.49 131.210 2 8 -12 -9 7261.55 184.461 2 8 -12 -8 1059.39 69.7213 2 8 -12 -7 201.927 26.0722 4 8 -12 -7 197.870 33.2512 2 8 -12 -6 3036.01 86.9960 4 8 -12 -5 3030.73 86.2192 4 8 -12 -4 3854.21 98.0765 4 8 -12 -3 16681.2 199.882 4 8 -12 -2 364.966 33.4729 6 8 -12 -2 335.639 32.9462 4 8 -12 -1 2659.19 81.9055 6 8 -12 0 22319.0 235.137 6 8 -12 1 3494.81 97.5830 6 8 -12 1 3529.16 96.3125 1 -8 -12 -2 576.126 19.6630 2 8 -12 2 676.641 47.0269 1 8 -12 3 16602.5 217.718 1 -8 -12 -3 16562.4 117.977 2 8 -12 4 2926.07 96.4255 1 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110.490 1 -8 -8 -4 1265.19 35.8363 2 8 -8 4 1185.94 58.9863 1 -8 -8 -5 79.1510 14.8564 2 8 -8 5 43.2540 21.1475 1 -8 -8 -6 13999.3 156.430 2 8 -8 6 13256.6 205.260 1 -8 -8 -7 7283.79 126.929 2 8 -8 7 7015.91 156.264 1 -8 -8 -8 111.970 23.3697 2 8 -8 8 107.725 30.7463 1 -8 -8 -9 2055.79 81.6649 2 8 -8 9 1923.65 90.5450 1 8 -8 10 345.353 58.7010 1 -8 -8 -10 340.003 39.2589 2 8 -8 11-16.9997 31.2484 1 -8 -8 -11 20.9116 24.5302 2 8 -8 12 5039.28 154.489 1 8 -6 -13 219.747 44.0462 2 8 -6 -12 490.589 58.2928 2 8 -6 -11 886.436 70.2239 2 8 -6 -10 4495.09 141.067 2 8 -6 -9 476.326 47.2512 2 8 -6 -8 109.225 28.0930 2 8 -6 -7 62.6010 24.1413 2 8 -6 -6 14980.8 133.777 4 8 -6 -6 15000.8 201.248 2 8 -6 -5 1463.81 44.3899 4 8 -6 -4 1144.70 41.2384 4 8 -6 -3 305.588 24.1307 6 8 -6 -2 4989.32 86.8361 6 8 -6 -2 4924.84 86.2398 1 8 -6 -1 336.217 26.5318 1 -8 -6 1 279.057 14.7107 3 8 -6 0 14950.2 161.164 1 -8 -6 0 14226.3 116.105 3 8 -6 1 418.385 32.5255 1 8 -6 2 4594.22 99.4290 1 -8 -6 -4 894.188 30.3170 2 -8 -6 -5 1295.28 43.1447 2 -8 -6 -6 16021.9 170.882 2 -8 -6 -7 26.4070 16.1442 2 -8 -6 -8 275.330 31.1845 2 -8 -6 -9 210.898 30.8206 2 -8 -6 -10 3203.64 109.390 2 -8 -6 -11 1149.95 72.5531 2 8 -6 11 1164.51 77.2513 1 8 -6 12 796.386 67.4247 1 8 -4 -13 1013.31 81.0457 2 -8 -4 12 451.067 57.5964 8 8 -4 -12 307.119 44.7859 2 -8 -4 11 121.554 38.8036 8 8 -4 -11 99.5413 32.5477 2 -8 -4 10 1487.94 86.6229 8 8 -4 -10 1482.35 81.7729 2 -8 -4 9 12676.9 230.155 8 8 -4 -9 12808.7 218.040 2 -8 -4 8 270.037 37.8160 8 8 -4 -8 278.085 35.2088 2 -8 -4 7 5173.51 131.113 8 8 -4 -7 5322.81 124.429 2 -8 -4 6 141.364 25.8399 8 8 -4 -6 163.925 26.1542 2 8 -4 -5 154.795 14.1856 4 -8 -4 5 144.077 23.0126 8 8 -4 -5 151.360 22.4678 2 -8 -4 4 3662.55 86.4950 8 8 -4 -4 3883.18 64.9324 4 8 -4 -3 52586.3 245.393 6 8 -4 -2 7844.62 100.210 1 -8 -4 1 1449.31 36.4696 3 8 -4 -1 1423.54 46.9258 1 -8 -4 0 1199.29 36.7737 3 8 -4 0 1288.98 46.9494 1 -8 -4 -1 1516.84 56.3625 5 -8 -4 -2 7806.47 131.752 5 -8 -4 -3 49595.4 349.720 5 -8 -4 -4 3515.02 101.871 5 -8 -4 -7 4872.67 107.006 2 -8 -4 -8 484.935 39.9629 2 8 -4 13 614.076 63.4692 1 8 -2 -14 128.936 43.9211 2 -8 -2 13 1971.98 114.525 8 8 -2 -13 1839.49 104.889 2 -8 -2 12 651.929 67.7295 8 8 -2 -12 661.604 62.5100 2 -8 -2 11 366.006 51.6749 8 8 -2 -11 178.752 34.3547 2 -8 -2 10 504.124 53.6822 8 8 -2 -10 426.411 47.5328 2 -8 -2 9 2507.44 105.509 8 8 -2 -9 2574.87 98.5441 2 -8 -2 8 145.590 30.6212 8 8 -2 -8 141.872 27.2736 2 -8 -2 7 1156.00 64.0864 8 8 -2 -7 1121.58 57.1262 2 -8 -2 6 8142.52 152.674 8 8 -2 -6 8044.63 139.289 2 8 -2 -5 1968.71 31.2142 4 -8 -2 5 2100.30 72.9150 8 8 -2 -5 2214.91 69.1742 2 -8 -2 4 617.367 37.6266 8 8 -2 -4 610.782 22.9947 4 8 -2 -4 641.758 35.8731 2 8 -2 -3 26912.5 155.141 6 -8 -2 3 26754.8 207.646 8 8 -2 -3 26832.3 158.620 1 -8 -2 2 59.5831 12.3149 8 -8 -2 2 67.8947 13.3219 5 -8 -2 2 51.1840 11.3208 3 8 -2 -2 40.7810 11.4214 1 -8 -2 1 60.1435 14.4319 5 -8 -2 1 97.3286 13.7222 3 -8 -2 0 4362.87 83.3514 5 -8 -2 0 4196.17 72.3329 3 -8 -2 -1 22.1431 14.1989 5 -8 -2 -1 27.4590 11.8418 3 -8 -2 -2 112.333 20.6375 5 -8 -2 -3 25460.0 242.605 5 -8 -2 -4 769.004 48.8127 5 -8 -2 -5 2391.42 85.2703 5 -8 -2 -6 6537.36 146.496 5 -8 -2 -7 735.008 55.7548 5 8 0 -14 60.8091 37.1388 2 -8 0 13 148.083 46.2010 8 8 0 -13 117.530 41.1081 2 -8 0 12 3024.19 136.721 8 8 0 -12 3059.46 126.529 2 -8 0 11 170.857 41.9312 8 8 0 -11 116.091 31.5348 2 -8 0 10 2524.31 112.950 8 8 0 -10 2561.46 100.611 2 -8 0 9 1737.87 87.8902 8 8 0 -9 1757.64 78.8220 2 -8 0 8 5060.35 139.516 8 8 0 -8 5147.62 126.784 2 -8 0 7 2478.25 66.2669 8 8 0 -7 2941.66 89.8388 2 -8 0 6 41173.0 344.196 8 -8 0 5 2879.61 84.7061 8 8 0 -5 2984.85 76.6066 2 8 0 -4 4504.95 46.4807 4 -8 0 4 4468.31 96.1143 8 -8 0 4 4358.32 44.8889 5 8 0 -4 4591.64 86.4500 2 -8 0 3 1262.04 47.2950 8 -8 0 3 1211.89 32.2050 5 8 0 -3 1284.62 42.7123 2 8 0 -3 1247.17 31.7906 1 -8 0 2 472.915 25.9955 8 8 0 -2 456.675 23.2236 2 -8 0 2 502.929 27.8301 3 -8 0 1 3895.27 58.1821 8 -8 0 1 3994.13 73.6884 3 8 0 0 205235. 347.971 7 -8 0 0 206361. 535.952 3 -8 0 -1 3607.63 79.9704 5 -8 0 -1 3406.31 74.0175 3 -8 0 -2 451.456 33.7214 5 -8 0 -3 1210.73 53.9587 5 -8 0 -4 3169.87 92.0534 5 8 0 5 4045.59 59.3324 8 -8 0 -5 3969.21 107.203 5 8 0 6 40866.2 226.530 8 -8 0 -6 41376.2 361.922 5 8 0 7 3150.72 72.7260 8 -8 0 -7 3215.90 107.591 5 8 0 8 5015.93 101.357 8 -8 0 -8 5089.57 142.283 5 8 0 9 1007.02 51.5116 8 -8 0 -9 1102.88 72.9210 5 8 2 -14 77.9783 43.4238 2 -8 2 13 1975.22 117.316 8 8 2 -13 1852.19 105.763 2 -8 2 12 636.064 67.4462 8 8 2 -12 590.749 60.4211 2 -8 2 11 308.542 47.4345 8 8 2 -11 289.936 43.8916 2 -8 2 10 416.098 50.5623 8 8 2 -10 443.192 46.6786 2 -8 2 9 2413.23 104.798 8 8 2 -9 2422.56 103.830 2 -8 2 8 181.476 32.5506 8 8 2 -8 169.161 27.9678 2 -8 2 7 1148.68 64.5845 8 8 2 -7 997.667 51.3180 2 -8 2 6 8437.38 160.420 8 8 2 -6 7835.77 132.370 2 -8 2 5 2162.57 76.7057 8 8 2 -5 2118.96 64.0131 2 -8 2 4 689.689 40.7699 8 8 2 -4 546.334 13.0288 4 8 2 -4 650.113 33.0751 2 -8 2 2 58.2439 13.1610 8 8 2 -2 45.6762 9.85945 2 -8 2 2 61.6514 15.0669 3 -8 2 1 43.9352 9.96765 8 -8 2 1 59.2749 19.2704 3 8 2 -1 52.3224 7.90151 2 -8 2 0 3870.57 44.5832 8 8 2 0 3953.76 36.6674 2 -8 2 0 4376.56 85.4627 3 8 2 1 33.7121 4.34649 2 -8 2 -1 16.7351 12.5026 3 8 2 2 130.024 8.82069 2 -8 2 -2 150.300 21.0461 3 8 2 3 22962.9 88.1905 8 8 2 4 771.787 24.4469 8 -8 2 -4 882.554 50.5412 5 8 2 5 2418.45 51.3217 8 -8 2 -5 2466.41 83.9505 5 8 2 6 6365.43 95.5699 8 -8 2 -6 6759.00 145.524 5 8 2 7 748.644 38.4330 8 -8 2 -7 827.084 57.8129 5 -8 2 -8 160.104 33.9939 5 8 2 8 136.769 22.2167 8 8 2 9 3074.65 90.0808 8 -8 2 -9 3207.53 118.950 5 -8 2 -10 386.049 50.0300 5 8 4 -14 795.732 78.1918 2 -8 4 13 938.050 85.0434 8 8 4 -13 1013.71 81.6896 2 -8 4 12 265.056 48.5774 8 8 4 -12 313.101 48.4444 2 -8 4 11 78.4207 30.6261 8 8 4 -11 114.574 32.7591 2 -8 4 10 1377.28 85.9456 8 8 4 -10 1516.61 80.8583 2 -8 4 9 12773.0 240.510 8 8 4 -9 12660.3 211.646 2 -8 4 8 251.637 39.1514 8 8 4 -8 309.390 35.6035 2 -8 4 7 5118.46 133.530 8 8 4 -7 5157.71 116.303 2 -8 4 6 118.315 26.1590 8 8 4 -6 135.442 21.3669 2 -8 4 5 144.653 24.7077 8 8 4 -5 158.364 20.8536 2 8 4 -4 3474.52 34.7626 4 8 4 -4 3857.61 75.4866 2 -8 4 3 51540.0 313.488 7 8 4 -3 50808.0 238.949 2 -8 4 2 7908.79 110.548 7 8 4 -2 7826.71 79.1362 2 -8 4 2 8007.79 124.930 3 -8 4 1 1412.09 41.3317 7 -8 4 1 1342.95 50.6731 3 8 4 -1 1401.27 25.1701 2 -8 4 0 1179.22 32.0971 7 -8 4 0 1221.92 48.9384 3 -8 4 -1 1468.61 26.0038 7 -8 4 -1 1544.78 56.1661 3 -8 4 -2 7694.19 127.464 3 8 4 3 48794.9 202.089 7 -8 4 -3 47591.8 327.999 3 8 4 4 3529.57 63.0412 7 8 4 5 178.998 18.5979 7 8 4 6 338.898 26.3353 8 -8 4 -6 287.162 35.8348 5 8 4 7 4561.00 96.8175 8 -8 4 -7 4699.24 129.204 5 8 4 8 501.585 38.0205 8 -8 4 -8 490.250 48.8200 5 8 4 9 13005.4 189.762 8 -8 4 -9 13856.2 245.172 5 8 4 10 1744.09 76.1832 8 -8 4 -10 1881.00 97.0295 5 -8 4 -11 158.840 42.6073 5 -8 6 13 305.629 53.9073 8 -8 6 12 440.834 60.0867 8 8 6 -12 474.426 56.5626 2 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1895.96 112.529 5 -8 8 13 2416.30 134.100 8 -8 8 12 5281.06 189.989 8 -8 8 11 130.792 42.8414 8 -8 8 10 347.762 49.0008 8 -8 8 9 1562.66 89.7710 8 8 8 -9 1631.80 80.2887 2 8 8 -8 52.3629 22.3831 2 -8 8 7 7800.10 177.252 7 8 8 -7 8058.22 151.256 2 -8 8 6 14428.3 226.031 7 8 8 -6 14929.1 189.929 2 -8 8 5 49.7326 20.9575 7 -8 8 4 1244.98 60.6687 7 -8 8 3 3936.70 97.1344 7 -8 8 2 3720.61 87.0775 7 -8 8 2 3781.57 98.5922 3 -8 8 1 522.436 32.0792 7 -8 8 1 564.806 39.9121 3 -8 8 -1 143.630 24.7751 3 -8 8 -2 3019.44 89.2523 3 -8 8 -3 4656.80 114.379 3 8 8 4 1185.49 47.7189 7 -8 8 -4 1131.68 61.4557 3 8 8 5 80.0043 18.5290 7 -8 8 -5 65.8792 24.8600 3 8 8 6 13169.5 174.006 7 -8 8 -6 13192.5 217.225 3 8 8 7 6767.78 134.897 7 -8 8 -7 6540.52 162.847 3 8 8 8 98.2304 25.8169 7 -8 8 -8 87.9972 27.9462 3 8 8 9 1888.06 80.1152 8 -8 8 -9 2003.12 96.3058 5 -8 8 -10 416.931 50.9940 5 8 8 10 382.373 42.3052 8 -8 8 -11 44.8022 34.1941 5 -8 8 -12 5050.05 171.256 5 -8 8 -13 2484.21 136.899 3 -8 10 13 1266.62 103.561 8 -8 10 12 494.036 68.3793 8 -8 10 11 322.107 54.2182 8 -8 10 10 879.695 77.2920 8 -8 10 8 274.419 44.1680 7 -8 10 7 381.472 45.2140 7 -8 10 6 3209.97 113.776 7 -8 10 5 1540.43 74.3418 7 -8 10 4 233.338 31.9914 7 -8 10 3 27042.1 267.284 7 -8 10 2 994.543 50.3314 7 -8 10 2 1025.83 56.6960 3 -8 10 1 54.4590 17.3227 7 -8 10 1 33.7712 18.6463 3 -8 10 0 258.357 30.4069 3 -8 10 -1 60.4292 22.7742 3 -8 10 -2 865.015 53.3091 3 -8 10 -3 25223.5 272.892 3 -8 10 -4 171.886 30.7189 3 8 10 5 1687.92 66.0710 7 -8 10 -5 1740.39 81.6399 3 8 10 6 2947.00 89.9712 7 -8 10 -6 2887.31 106.809 3 8 10 7 252.778 31.6941 7 -8 10 -7 248.939 38.4514 3 8 10 8 162.176 30.1995 7 -8 10 -8 145.624 33.8393 3 8 10 9 5305.71 141.511 7 -8 10 -9 5736.75 163.991 5 -8 10 -9 5220.53 163.120 3 8 10 10 665.127 55.7193 8 -8 10 -10 718.933 65.2840 5 -8 10 -10 611.774 64.5704 3 -8 10 -11 445.756 56.3478 5 -8 10 -11 489.993 62.1360 3 -8 10 -12 436.861 58.6772 5 -8 10 -12 396.475 60.1726 3 -8 10 -13 982.432 88.5200 3 -8 12 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676.766 51.0367 5 9 1 6 2096.43 49.0516 8 -9 1 -6 2006.75 85.9318 5 -9 1 -7 205.622 35.9052 5 9 1 7 148.217 18.9673 8 -9 1 -8 404.641 47.1786 5 -9 1 -9 1895.49 96.6856 5 -9 1 -10 46.1248 34.0990 5 -9 3 13 157.816 46.9161 8 9 3 -13 135.580 42.5227 2 -9 3 12 281.246 50.5875 8 9 3 -12 288.798 46.1734 2 -9 3 11 124.605 39.9129 8 9 3 -11 46.3910 28.9337 2 -9 3 10 126.155 36.1959 8 9 3 -10 118.665 30.6332 2 -9 3 9 78.4478 29.3306 8 9 3 -9 84.7400 26.9368 2 -9 3 8 388.674 43.9959 8 9 3 -8 442.401 39.6608 2 -9 3 7 131.644 29.5218 8 9 3 -7 123.859 23.2423 2 -9 3 6 170.029 29.8680 8 9 3 -6 124.119 20.4983 2 -9 3 5 92.5575 23.6822 8 9 3 -5 112.242 19.4350 2 -9 3 4 1709.88 63.6695 8 9 3 -4 1726.11 52.7202 2 9 3 -4 1614.86 27.8522 1 -9 3 3 153.621 20.6763 8 9 3 -3 131.545 15.2709 2 -9 3 2 208.351 19.9551 8 -9 3 2 212.147 24.4432 3 9 3 -2 210.009 15.4386 2 -9 3 1 450.358 22.9298 8 9 3 -1 439.655 15.9175 2 -9 3 1 475.587 32.2751 3 -9 3 0 365.580 15.9387 8 -9 3 0 393.679 30.2981 3 9 3 1 183.411 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5 2 4905.76 91.5235 7 -9 5 2 4991.58 105.966 3 9 5 -2 4831.29 62.8570 2 -9 5 1 785.666 33.6961 7 -9 5 1 751.360 42.9580 3 -9 5 0 1418.54 38.0587 7 -9 5 0 1442.01 58.0518 3 -9 5 -1 1146.00 26.6217 7 -9 5 -1 1321.76 56.8252 3 -9 5 -2 1449.78 20.0631 8 -9 5 -2 1371.27 22.2062 7 -9 5 -2 2108.06 74.6572 3 9 5 3 3182.32 55.3849 7 -9 5 -3 3215.37 94.0682 3 9 5 4 1220.99 38.1859 7 -9 5 -4 1273.90 63.2221 3 9 5 5 351.643 25.1263 7 -9 5 -5 305.029 37.9347 3 -9 5 -7 127.140 30.8984 5 9 5 7 120.314 20.7721 8 -9 5 -8 162.690 34.7701 5 9 5 8 127.223 23.2501 8 -9 5 -9 177.596 37.9636 5 -9 5 -10 73.8079 34.7930 5 -9 5 -11 713.799 69.7529 5 -9 5 -12 957.654 83.6936 5 -9 7 13 146.045 44.9168 8 -9 7 12 699.663 72.8355 8 -9 7 11 145.983 42.1569 8 9 7 -11 376.971 49.9578 2 -9 7 10 688.171 65.8528 8 9 7 -10 603.246 55.3565 2 -9 7 9 108.013 35.4678 8 9 7 -9 158.312 33.7365 2 -9 7 8 345.117 43.8868 8 9 7 -8 264.700 34.2756 2 9 7 -7 693.512 46.9348 2 9 7 -6 575.959 40.0614 2 -9 7 5 738.356 50.3802 7 9 7 -5 690.554 39.1918 2 -9 7 4 298.383 31.3093 7 9 7 -4 308.098 24.2858 2 -9 7 3 1273.42 57.3029 7 -9 7 2 2723.35 72.6942 7 -9 7 2 2850.04 86.0362 3 -9 7 1 795.327 37.3939 7 -9 7 1 778.304 47.3940 3 -9 7 0 217.424 19.1918 7 -9 7 0 226.902 29.4571 3 -9 7 -1 1483.81 39.9640 7 -9 7 -1 1524.29 63.6357 3 -9 7 -2 633.623 44.6792 3 -9 7 -3 3358.29 99.5521 3 9 7 4 158.488 18.7726 7 -9 7 -4 90.6930 24.4673 3 9 7 5 186.655 21.3312 7 -9 7 -5 231.937 34.1943 3 9 7 6 657.406 38.9163 7 -9 7 -6 678.676 54.4684 3 9 7 7 690.656 43.0360 7 -9 7 -7 647.915 56.2802 3 -9 7 -8 130.564 32.8711 5 9 7 8 165.884 26.6277 8 -9 7 -8 191.342 39.5918 3 -9 7 -9 911.747 69.3147 5 -9 7 -10 86.7345 34.1531 5 -9 7 -11 1482.57 94.7081 5 -9 7 -12 236.932 51.4074 5 -9 7 -13 90.5719 46.3284 3 -9 9 13 52.9779 39.8746 8 -9 9 12 250.516 53.2042 8 -9 9 11 488.437 62.9296 8 -9 9 10 76.9861 33.4043 8 -9 9 9 487.733 58.1987 8 -9 9 7 31.7717 23.9199 7 -9 9 6 475.654 46.7748 7 -9 9 5 313.420 37.5715 7 -9 9 4 2.16005 17.1059 7 -9 9 3 140.530 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77.9138 2 -10 4 7 131.281 30.8948 8 10 4 -7 166.730 26.5077 2 -10 4 6 1894.45 82.1464 8 10 4 -6 1835.46 66.3092 2 -10 4 5 396.005 36.6806 8 10 4 -5 401.562 30.0348 2 -10 4 4 726.035 44.1642 8 10 4 -4 688.391 34.4557 2 -10 4 3 1024.96 46.3544 8 10 4 -3 928.844 34.4723 2 -10 4 2 1254.63 45.4555 8 10 4 -2 1168.16 31.9382 2 -10 4 2 1263.58 55.8827 3 -10 4 1 1076.57 36.1902 8 -10 4 1 1037.59 50.0818 3 10 4 -1 980.376 19.6342 2 -10 4 0 15.8569 6.98989 8 -10 4 0 24.2327 15.3145 3 -10 4 -1 1225.92 56.2825 3 10 4 2 1089.57 24.5717 8 10 4 2 1188.20 24.3301 7 -10 4 -2 1251.26 57.9363 3 10 4 3 454.480 14.3048 7 -10 4 -3 472.483 40.1385 3 -10 4 -4 650.058 47.7927 3 10 4 5 156.800 14.3378 8 -10 4 -5 177.458 31.4797 3 -10 4 -6 1261.42 71.7557 5 -10 4 -7 53.2393 26.8508 5 -10 4 -8 3112.21 121.690 5 -10 4 -9 69.8042 32.4925 5 -10 4 -10 48.7224 33.1591 5 -10 4 -11 186.730 46.5913 5 -10 6 13 63.0392 38.5834 8 -10 6 12 414.628 60.7304 8 10 6 -12 471.980 58.0006 2 -10 6 11 4160.87 159.270 8 10 6 -11 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71.8015 5 -10 8 -11 715.377 75.7490 3 -10 8 -12 82.8917 42.0865 5 -10 8 -12 100.855 43.8121 3 -10 8 -13 1406.05 104.055 5 -10 10 12-2.98624 37.2356 8 -10 10 11 314.287 53.5268 8 -10 10 10 65.2783 36.5035 8 -10 10 9 1075.26 80.0755 8 -10 10 7 478.924 51.7103 7 -10 10 6 53.3903 23.0562 7 -10 10 5 43.9337 22.8696 7 -10 10 4 49.6049 23.1479 7 -10 10 3 265.173 31.3800 7 -10 10 2 464.871 35.9249 7 -10 10 2 489.501 44.0425 3 -10 10 1 849.898 44.0553 7 -10 10 1 842.449 54.3961 3 -10 10 0-8.48723 12.4643 7 -10 10 0 0.30780 19.0913 3 -10 10 -1 981.535 58.6437 3 -10 10 -2 500.936 44.7015 3 -10 10 -3 586.296 49.8092 3 10 10 4 91.6044 20.2311 7 -10 10 -4 81.9206 26.2373 3 10 10 5 38.8953 16.5749 7 -10 10 -5 76.7547 27.7121 3 10 10 6 22.3067 14.3988 7 -10 10 -6-3.34372 22.7165 3 -10 10 -7 696.142 62.0751 3 -10 10 -8 228.246 43.3438 3 -10 10 -9 470.282 56.3087 5 -10 10 -9 407.704 55.3604 3 -10 10 -10 413.067 55.0679 5 -10 10 -10 464.831 61.1585 3 -10 10 -11 218.830 48.2872 5 -10 10 -11 330.211 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101.701 42.6113 3 -10 18 -10 1441.62 106.179 3 -10 20 9 614.161 80.4155 7 -10 20 8 355.367 64.0912 7 -10 20 7 225.790 51.6896 7 -10 20 6 68.5931 37.0991 7 -10 20 5 16.5629 28.3120 7 -10 20 4 627.156 64.1080 7 -10 20 3 1088.11 78.6374 7 -10 20 2 1329.30 84.5353 7 -10 20 -1 107.290 38.0935 3 -10 20 -2 1600.87 95.6153 3 -10 20 -3 872.506 74.2189 3 -10 20 -4 403.126 52.7811 3 -10 20 -5 13.1539 29.0120 3 10 20 6 51.0653 31.0931 7 -10 20 -6 54.3019 35.7087 3 -10 20 -7 245.464 49.9752 3 -10 20 -8 1562.59 106.712 3 -10 20 -9 846.696 83.8536 3 -10 22 8 214.372 56.5380 7 -10 22 7 789.708 85.0213 7 -10 22 6 657.254 72.7641 7 -10 22 5 1177.99 92.9729 7 -10 22 4 310.905 52.9486 7 -10 22 3 146.228 40.7755 7 -10 22 2 223.668 47.3042 7 -10 22 -1 2758.77 127.710 3 -10 22 -2 412.298 56.5110 3 -10 22 -3 156.684 42.2660 3 -10 22 -4 396.312 58.5569 3 -10 22 -5 1386.32 96.6660 3 10 22 6 513.631 61.8819 7 -10 22 -6 355.979 57.8642 3 -10 22 -7 1095.32 90.6109 3 -10 22 -8 681.989 78.3545 3 -10 22 -9 34.0042 39.3682 3 -10 24 7 115.203 45.3589 7 -10 24 6 536.327 72.6652 7 -10 24 5 124.252 46.1736 7 -10 24 4 1055.22 90.7679 7 -10 24 3-7.19006 32.3600 7 -10 24 2 580.481 67.7975 7 -10 24 -2 395.945 58.4512 3 -10 24 -3-20.2749 33.8729 3 -10 24 -4 1139.40 92.2348 3 -10 24 -5 149.243 45.8022 3 -10 24 -6 505.565 67.5332 3 -10 24 -7-70.9452 45.7819 3 -10 26 6 57.3917 44.7377 7 -10 26 5 357.378 63.4133 7 -10 26 4 451.866 68.3312 7 -10 26 3 149.548 49.2972 7 -10 26 2 701.088 75.1784 7 -10 26 -4 591.118 73.8902 3 -10 26 -5 364.639 61.2651 3 -10 26 -6 239.356 55.4926 3 -10 28 3 166.548 49.7175 7 -10 28 2 92.4742 42.8561 7 -10 28 1 873.865 90.4124 7 11 -27 -4 77.8689 37.7873 4 11 -27 -3 56.5948 35.3273 4 11 -27 -2 29.4751 33.1145 4 11 -27 -1 376.338 55.7689 4 11 -27 0 5.43542 33.3601 4 11 -27 1 113.054 44.5506 4 11 -27 2 29.7141 35.9318 4 11 -25 -6 15.5961 30.0225 4 11 -25 -5 195.555 42.2528 4 11 -25 -4 682.322 67.6446 4 11 -25 -3 76.5398 34.3679 4 11 -25 -2 72.3947 34.1268 4 11 -25 -1 61.9892 32.2433 4 11 -25 0 410.195 57.7420 4 11 -25 1 138.898 42.2666 4 11 -25 2 140.101 43.3993 4 11 -25 3 97.2888 39.3620 4 11 -25 4 110.510 43.3677 4 11 -25 4 137.078 46.6706 6 11 -25 5 106.258 45.3535 4 11 -25 5 70.7230 39.6312 6 11 -23 -6 755.414 65.8279 4 11 -23 -5 365.314 51.3248 4 11 -23 -4 913.878 71.5726 4 11 -23 -3 750.250 67.6573 4 11 -23 -2 145.519 38.4917 4 11 -23 -1 78.8787 34.2700 4 11 -23 0 740.116 69.0548 4 11 -23 1-1.60800 30.2132 4 11 -23 2 840.217 74.3715 6 11 -23 2 967.181 80.1151 4 11 -23 3 629.405 67.3491 6 11 -23 3 589.549 66.1379 4 11 -23 4 537.990 65.8424 4 11 -23 4 552.016 64.0992 6 11 -23 5 260.855 51.6561 6 11 -23 5 163.153 44.1903 4 11 -23 6 119.521 42.7925 6 11 -23 6 202.874 50.7987 4 11 -23 7 180.054 48.5227 6 11 -23 7 54.9095 34.4733 4 11 -21 -8 769.679 70.9752 2 11 -21 -6 18.4588 24.1162 4 11 -21 -5 320.405 44.8863 4 11 -21 -4 54.4369 29.8326 4 11 -21 -3 54.7933 29.8557 4 11 -21 -2 221.954 42.2713 4 11 -21 -1 1204.80 79.8927 4 11 -21 0 251.778 44.8036 4 11 -21 0 255.837 43.0867 6 11 -21 1 591.515 60.4017 6 11 -21 1 592.007 61.2890 4 11 -21 2 58.6880 31.7239 6 11 -21 2 24.1044 27.7567 4 11 -21 3 203.763 43.2500 6 11 -21 3 198.185 43.3023 4 11 -21 4 153.412 39.8574 4 11 -21 4 234.718 47.0200 6 11 -21 5 243.861 47.4408 4 11 -21 5 110.127 38.5762 6 11 -21 6 7.39789 33.4459 6 11 -21 7 565.237 69.1725 6 11 -21 8 270.715 55.1333 6 11 -19 -9 1319.28 91.5962 2 11 -19 -8 305.425 47.4534 2 11 -19 -6 143.556 32.5134 4 11 -19 -5 4.46303 21.7089 4 11 -19 -4 191.361 39.8019 4 11 -19 -3 849.477 65.8682 4 11 -19 -2 686.272 58.4715 4 11 -19 -1 511.629 52.1777 6 11 -19 -1 502.215 52.7733 4 11 -19 0 102.831 33.8478 6 11 -19 0 122.541 33.3596 4 11 -19 1 241.929 41.6411 6 11 -19 1 301.359 44.9533 4 11 -19 2 109.152 35.3584 4 11 -19 2 118.775 36.4492 6 11 -19 3 150.241 38.8020 6 11 -19 4 79.7005 37.0184 6 11 -19 5 271.536 49.8592 6 11 -19 6 394.804 55.2847 6 11 -19 7 203.466 45.5120 6 11 -19 8 26.0278 34.8869 6 11 -19 9 160.332 48.1700 6 11 -17 -10 918.473 78.4752 2 11 -17 -9 307.933 49.8792 2 11 -17 -8 35.4375 28.2720 2 11 -17 -6 1912.79 85.6114 4 11 -17 -5 231.182 36.5466 4 11 -17 -4 3267.27 112.383 4 11 -17 -3 2027.89 89.9113 4 11 -17 -2 710.721 57.7292 4 11 -17 -1 1152.22 68.7204 6 11 -17 -1 988.486 65.3149 4 11 -17 0 639.813 54.2358 6 11 -17 0 607.542 53.8531 4 11 -17 1 135.564 35.6611 6 11 -17 2 2781.91 109.588 6 11 -17 3 1101.80 74.4664 6 11 -17 4 1611.33 90.1875 6 11 -17 5 844.604 68.1159 6 11 -17 6 303.845 50.3813 6 11 -17 7 322.476 50.6755 6 11 -17 7 360.102 53.9945 1 11 -17 8 34.2813 32.8150 6 11 -17 8 41.4241 40.7065 1 11 -17 9 43.0688 35.6276 6 11 -17 10 384.620 61.3333 6 11 -15 -11 141.555 40.2495 2 11 -15 -10 68.2059 36.7523 2 11 -15 -9 88.3322 34.9416 2 11 -15 -8 106.813 34.2487 2 11 -15 -6 222.048 33.1436 4 11 -15 -5 1707.32 76.1510 4 11 -15 -4 148.596 29.7204 4 11 -15 -3 77.3942 27.2214 4 11 -15 -2 267.822 35.9744 6 11 -15 -2 221.565 33.9452 4 11 -15 -1 1021.33 68.6929 6 11 -15 -1 948.234 60.5539 4 11 -15 0 40.5992 24.8238 6 11 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182.601 45.0383 1 11 -13 11 67.6307 40.9360 1 11 -11 -12 360.035 52.5842 2 11 -11 -11 158.436 39.3370 2 11 -11 -10 145.238 37.9551 2 11 -11 -9 65.5398 30.7073 2 11 -11 -8 561.713 55.3604 2 11 -11 -7 65.4468 27.2729 2 11 -11 -6 1416.63 59.4333 4 11 -11 -5 1237.73 57.1862 4 11 -11 -4 1555.15 64.7414 4 11 -11 -3 1104.88 55.0858 6 11 -11 -3 1048.20 54.6333 4 11 -11 -2 402.583 38.8068 6 11 -11 -1 306.010 33.4885 6 11 -11 0 1026.69 57.3655 6 11 -11 0 1034.87 57.4131 1 11 -11 1 158.175 29.8965 1 11 -11 2 2163.08 85.7488 1 11 -11 3 652.109 52.4000 1 11 -11 4 985.939 64.0614 1 11 -11 5 1111.50 69.3018 1 11 -11 6 438.166 49.3265 1 11 -11 7 250.053 41.2269 1 11 -11 8 749.061 65.2240 1 11 -11 9 48.9718 32.4876 1 11 -11 10 117.946 40.2000 1 11 -11 11 47.7008 38.8093 1 11 -11 12 272.424 52.7270 1 11 -9 -12 509.522 60.6618 2 11 -9 -11 84.1134 33.6300 2 11 -9 -10 414.481 50.7504 2 11 -9 -9 224.825 39.1134 2 11 -9 -8 70.2629 28.5440 2 11 -9 -7 710.935 54.8206 2 11 -9 -6 433.422 41.4592 2 11 -9 -5 10.4282 14.3223 4 11 -9 -4 1748.75 63.9276 4 11 -9 -3 514.724 36.6304 6 11 -9 -3 529.742 37.5123 4 11 -9 -2 55.5344 20.8099 6 11 -9 -1 14.5710 16.3980 6 11 -9 -1 37.1898 20.6237 1 11 -9 0 4.31692 18.3720 1 -11 -9 0 26.9958 10.0612 3 -11 -9 -1-2.44909 10.3050 3 11 -9 1 20.4288 20.6123 1 11 -9 2 394.767 38.6591 1 11 -9 3 166.660 31.0602 1 11 -9 4 1023.92 62.7523 1 11 -9 5 55.2761 25.5710 1 11 -9 6 82.3034 29.9711 1 11 -9 7 83.1561 33.6181 1 11 -9 8 202.395 40.4606 1 11 -9 9 106.973 37.2364 1 11 -9 10 74.7873 37.0436 1 11 -9 11 76.1068 39.7803 1 11 -9 12 34.8323 36.5629 1 11 -7 -12 93.0806 37.4916 2 11 -7 -11 589.118 61.1750 2 11 -7 -10 328.043 46.9834 2 11 -7 -9 2205.35 99.0086 2 11 -7 -8 862.284 60.9904 2 11 -7 -7 153.278 31.5730 2 11 -7 -6 772.341 52.0844 2 11 -7 -5 124.806 19.8443 4 11 -7 -5 134.743 26.9350 2 11 -7 -4 128.124 20.4681 6 11 -7 -4 88.6911 18.6794 4 11 -7 -3 901.503 43.3728 6 11 -7 -2 1433.73 57.0073 6 11 -7 -2 1483.27 57.6329 1 11 -7 -1 1393.64 57.5723 1 -11 -7 1 1481.77 39.1629 3 11 -7 0 302.174 31.3754 1 -11 -7 0 328.012 23.3120 3 -11 -7 -1 443.767 30.0317 3 11 -7 1 455.978 39.5583 1 11 -7 2 1339.96 64.5629 1 11 -7 3 94.8480 26.0255 1 11 -7 4 224.823 34.2713 1 11 -7 8 287.692 46.0622 1 11 -7 9 450.351 55.5217 1 11 -7 10 845.594 72.3359 1 11 -7 11 44.2218 37.3618 1 11 -7 12 35.9296 39.8424 1 11 -7 13-0.93900 41.3923 1 11 -5 -13 609.172 65.6228 2 11 -5 -12 0.52289 30.2494 2 11 -5 -11 1199.56 81.2594 2 11 -5 -10 137.892 33.9027 2 11 -5 -9 107.023 28.8170 2 11 -5 -8 2135.40 90.4005 2 11 -5 -7 1511.18 72.9077 2 11 -5 -6 77.1827 23.6509 2 11 -5 -5 2300.92 57.0747 4 11 -5 -5 2087.53 74.6243 2 11 -5 -4 214.037 21.9932 6 11 -5 -4 175.276 20.9486 4 11 -5 -3 221.244 23.1319 6 11 -5 -2 764.544 40.1787 1 -11 -5 2 727.052 29.0329 3 11 -5 -1 25.5911 17.1676 1 -11 -5 1 48.2224 12.6619 3 11 -5 0-16.1867 19.2676 1 -11 -5 0 17.3610 11.9706 3 -11 -5 -1 175.188 21.2693 3 11 -5 1 147.694 25.5751 1 11 -5 12 102.839 41.9926 1 11 -5 13 49.5788 39.8746 1 11 -3 -13 106.613 38.6549 2 11 -3 -12 43.0095 33.4554 2 -11 -3 11 73.8235 36.0594 8 11 -3 -11-12.0619 25.5183 2 -11 -3 10 87.3510 34.3564 8 11 -3 -10 109.248 31.7086 2 -11 -3 9 66.7699 30.5255 8 11 -3 -9 32.7590 24.1518 2 -11 -3 8 51.6805 25.3337 8 11 -3 -8 98.0572 27.6019 2 -11 -3 7 550.653 47.7696 8 11 -3 -7 548.213 44.7137 2 -11 -3 6 431.336 40.0372 8 11 -3 -6 415.157 37.6011 2 -11 -3 5 93.9487 21.6053 8 11 -3 -5 135.200 23.9943 2 11 -3 -4 17.3429 11.7473 6 11 -3 -4 15.0305 14.5004 2 11 -3 -3 134.039 19.1784 1 11 -3 -2 579.396 33.8306 1 -11 -3 2 545.985 29.5546 3 -11 -3 1 189.989 24.8900 5 11 -3 -1 111.332 19.4970 1 -11 -3 1 146.722 18.6523 3 -11 -3 0 328.297 31.0936 5 -11 -3 0 358.216 27.5350 3 -11 -3 -1 72.6358 22.1059 5 -11 -3 -1 66.2537 17.3571 3 -11 -3 -2 189.658 28.8153 5 -11 -3 -2 174.658 25.0371 3 -11 -3 -3 93.4966 25.0825 5 -11 -3 -4 10.6187 20.9176 5 -11 -3 -5 48.4060 26.8249 5 -11 -3 -6 427.145 48.7055 5 -11 -1 13 432.424 63.3086 8 11 -1 -13 448.172 58.9407 2 -11 -1 12 97.9161 37.1252 8 11 -1 -12 143.631 39.7181 2 -11 -1 11 1971.27 107.533 8 11 -1 -11 1946.69 98.5879 2 -11 -1 10 349.268 49.1543 8 11 -1 -10 335.198 42.1966 2 -11 -1 9 36.9823 29.9796 8 11 -1 -9 1.22347 22.1329 2 -11 -1 8 2409.32 100.742 8 11 -1 -8 2498.35 94.1390 2 -11 -1 7 153.066 31.5520 8 11 -1 -7 185.894 29.0114 2 -11 -1 6 417.032 40.8894 8 11 -1 -6 427.811 36.8915 2 -11 -1 5 3251.45 94.1627 8 11 -1 -5 3173.91 85.4807 2 11 -1 -4 780.988 28.7979 6 -11 -1 4 766.041 43.4455 8 11 -1 -4 733.276 39.7579 2 -11 -1 3 172.897 21.1240 8 -11 -1 3 180.504 19.0200 5 11 -1 -3 132.823 17.1288 1 11 -1 -3 163.549 19.5671 2 -11 -1 2 311.883 25.8333 5 11 -1 -2 317.788 22.7877 2 -11 -1 2 350.085 26.8252 3 11 -1 -2 294.423 25.3297 1 -11 -1 1 78.3954 18.2514 5 -11 -1 1 95.9267 18.3660 3 -11 -1 0 223.927 26.7666 5 -11 -1 0 200.452 23.5928 3 -11 -1 -1 31.0674 18.3417 5 -11 -1 -1 4.01485 13.5539 3 -11 -1 -2 124.132 25.1566 5 -11 -1 -2 110.216 21.8299 3 -11 -1 -3 61.9289 23.3283 5 -11 -1 -3 60.5741 20.3721 3 -11 -1 -4 171.109 31.4042 5 -11 -1 -5 1089.60 66.8525 5 -11 -1 -6 283.506 41.7415 5 -11 -1 -7 471.134 51.8560 5 -11 -1 -8 909.993 72.4482 5 -11 1 13 436.217 62.5605 8 11 1 -13 325.927 52.4227 2 -11 1 12 213.486 49.2197 8 11 1 -12 119.447 37.1564 2 -11 1 11 2036.68 110.143 8 11 1 -11 1959.10 99.6730 2 -11 1 10 390.030 52.1312 8 11 1 -10 372.131 44.4377 2 -11 1 9-2.43782 23.4854 8 11 1 -9 8.34465 21.5111 2 -11 1 8 2303.03 100.649 8 11 1 -8 2237.13 85.0894 2 -11 1 7 166.920 32.6899 8 11 1 -7 168.539 27.3038 2 -11 1 6 411.584 40.4263 8 11 1 -6 430.899 35.9018 2 -11 1 5 3222.45 95.2868 8 11 1 -5 3087.82 81.6459 2 11 1 -4 756.013 24.6929 6 -11 1 4 718.723 43.1069 8 -11 1 4 710.671 29.5139 5 11 1 -4 770.278 27.4441 1 11 1 -4 691.802 36.5448 2 -11 1 3 171.191 19.1551 5 -11 1 3 159.365 20.7762 8 11 1 -3 148.562 18.0553 1 11 1 -3 150.901 17.7809 2 -11 1 2 310.092 22.7789 8 -11 1 2 312.530 26.7649 5 11 1 -2 328.813 21.3122 2 -11 1 2 356.858 30.5111 3 -11 1 1 99.4070 20.0271 5 11 1 -1 85.4955 11.6141 2 -11 1 1 101.932 20.1480 3 -11 1 0 193.538 25.1782 5 11 1 0 169.471 12.1082 2 -11 1 0 160.964 23.5768 3 -11 1 -1 2.30894 17.1685 5 -11 1 -1 21.9106 15.7641 3 -11 1 -2 115.320 25.4254 5 -11 1 -2 142.166 24.9115 3 -11 1 -3 61.3920 22.4703 5 -11 1 -3 39.1054 18.5415 3 -11 1 -4 175.253 31.9034 5 -11 1 -4 199.179 31.2072 3 -11 1 -5 1129.63 68.1070 5 -11 1 -6 302.005 41.4285 5 -11 1 -7 407.280 49.0697 5 -11 1 -8 977.679 75.0029 5 -11 1 -9 15.6408 29.5347 5 -11 1 -10 203.504 45.0232 5 -11 3 13 73.5928 37.7896 8 11 3 -13 132.306 42.0355 2 -11 3 12 35.0150 34.5393 8 11 3 -12 10.2308 31.0621 2 -11 3 11 5.46303 29.2301 8 11 3 -11 50.7959 30.9974 2 -11 3 10 38.1937 27.3205 8 11 3 -10 107.616 29.9365 2 -11 3 9 20.2341 24.8455 8 11 3 -9 64.2874 27.0410 2 -11 3 8 102.808 32.0480 8 11 3 -8 88.5290 26.1224 2 -11 3 7 488.379 46.8489 8 11 3 -7 557.151 42.3546 2 -11 3 6 442.869 42.5043 8 11 3 -6 453.861 35.0030 2 -11 3 5 102.579 23.2421 8 11 3 -5 84.7709 17.1975 2 -11 3 4 18.0380 15.9858 8 11 3 -4 16.0874 9.43634 1 11 3 -4 1.95303 10.6531 2 -11 3 3 87.2223 17.9185 8 11 3 -3 88.9278 14.0173 2 -11 3 2 548.592 30.2427 8 11 3 -2 551.513 23.3745 2 -11 3 2 608.751 39.8790 3 -11 3 1 133.402 13.8491 8 11 3 -1 132.904 9.42962 2 -11 3 1 160.933 23.5402 3 -11 3 0 297.934 30.4265 3 -11 3 -1 58.0834 20.0509 3 -11 3 -2 180.293 28.6776 3 -11 3 -3 130.686 25.6086 3 -11 3 -4 67.0765 25.2168 5 -11 3 -4 5.84455 18.3959 3 -11 3 -5 40.2076 23.5720 5 -11 3 -5 50.9460 25.1656 3 -11 3 -6 513.425 51.3914 5 -11 3 -7 126.734 34.9279 5 -11 3 -8 312.683 47.2920 5 -11 3 -9 74.9110 34.4675 5 -11 3 -10 120.241 39.7677 5 -11 3 -11 176.457 48.7081 5 11 5 -13 687.868 69.9437 2 -11 5 12 14.5248 31.4213 8 11 5 -12 87.2595 35.4904 2 -11 5 11 1074.21 83.3765 8 11 5 -11 1214.15 80.8837 2 -11 5 10 205.490 41.7134 8 11 5 -10 213.136 38.9702 2 -11 5 9 98.2565 32.9917 8 11 5 -9 176.958 33.0998 2 -11 5 8 2161.55 99.9368 8 11 5 -8 2080.20 85.0141 2 -11 5 7 1537.64 80.6494 8 11 5 -7 1550.11 68.5542 2 -11 5 6 1.45886 19.6228 8 11 5 -6 11.7006 16.1550 2 -11 5 5 2229.22 83.0519 8 11 5 -5 2173.11 66.8292 2 -11 5 4 216.920 28.9717 8 11 5 -4 211.812 22.0247 2 -11 5 3 202.971 24.6026 8 11 5 -3 212.026 18.6443 2 -11 5 2 745.519 37.1799 8 -11 5 2 716.882 46.2129 3 11 5 -2 735.433 24.2332 2 -11 5 1 70.3503 13.6415 8 -11 5 1 50.0656 18.5642 3 -11 5 0 11.1984 7.62477 8 -11 5 0 18.2241 17.6194 3 -11 5 -1 206.619 29.5974 3 -11 5 -2 533.619 43.5595 3 -11 5 -3 81.1051 24.8208 3 -11 5 -4 767.193 54.2857 3 -11 5 -5 641.105 53.7178 3 -11 5 -6 29.7494 26.0613 5 -11 5 -6 17.9601 24.1196 3 -11 5 -7 577.363 55.3457 5 -11 5 -7 529.702 56.8778 3 -11 5 -8 274.586 46.6387 5 -11 5 -8 237.906 43.5145 3 -11 5 -9 51.6708 31.0505 5 -11 5 -10 291.533 51.2978 5 -11 5 -11 459.510 66.1094 5 -11 5 -12 240.872 54.8419 5 -11 7 12 107.553 41.7348 8 -11 7 11 448.821 58.7325 8 -11 7 10 284.719 48.4627 8 11 7 -10 398.115 49.7430 2 -11 7 9 2142.66 107.588 8 11 7 -9 2263.21 96.1343 2 -11 7 8 865.260 66.9928 8 11 7 -8 912.230 58.2662 2 -11 7 7 127.387 32.4163 8 11 7 -7 125.986 25.3618 2 -11 7 6 764.137 55.3596 8 11 7 -6 851.904 47.9713 2 11 7 -5 157.616 23.4362 2 -11 7 3 907.325 48.3092 7 -11 7 2 1453.10 55.7760 7 -11 7 2 1388.38 65.8276 3 -11 7 1 1502.73 50.3013 7 -11 7 1 1449.25 66.9105 3 -11 7 0 289.916 20.9714 7 -11 7 0 272.048 32.7075 3 -11 7 -1 465.278 21.0730 7 -11 7 -1 477.929 42.5788 3 -11 7 -2 1460.26 70.3270 3 11 7 3 145.939 16.1490 7 -11 7 -3 149.166 28.3766 3 -11 7 -4 308.264 38.9455 3 -11 7 -5 843.740 60.6172 3 -11 7 -6 581.648 55.7617 3 -11 7 -7 591.491 57.3122 5 -11 7 -7 495.681 53.8442 3 -11 7 -8 365.558 49.8055 5 -11 7 -8 278.509 47.7633 3 -11 7 -9 419.649 56.7516 5 -11 7 -9 391.506 55.9977 3 -11 7 -10 870.377 77.5316 5 -11 7 -10 880.559 80.9594 3 -11 7 -11 343.623 59.3539 5 -11 7 -11 68.3065 40.9913 3 -11 7 -12 141.180 46.4993 5 -11 7 -12 85.4771 43.6448 3 -11 9 12 517.927 67.3433 8 -11 9 11 141.328 41.8723 8 -11 9 10 382.672 54.4742 8 -11 9 9 102.155 34.9750 8 -11 9 8 131.982 37.4286 8 -11 9 7 668.924 56.8844 8 -11 9 5-0.50896 18.2400 7 -11 9 4 1581.54 71.5488 7 -11 9 3 557.646 41.1160 7 -11 9 2 77.2341 19.4607 7 -11 9 2 65.4437 43.0251 3 -11 9 1 43.4777 15.1102 7 -11 9 1 18.6832 19.3496 3 -11 9 0 21.9456 12.3751 7 -11 9 0-13.8782 20.9971 3 -11 9 -1 7.13936 9.72562 7 -11 9 -1 20.6843 20.5446 3 -11 9 -2 417.795 22.7963 7 -11 9 -2 414.989 42.4854 3 -11 9 -3 157.671 30.6118 3 11 9 4 1042.84 44.5187 7 -11 9 -4 1017.77 65.9785 3 -11 9 -5 44.9775 25.8821 3 -11 9 -6 75.0210 28.9401 3 -11 9 -7 57.7831 29.7634 3 -11 9 -8 253.039 45.5582 5 -11 9 -8 242.270 46.5773 3 -11 9 -9 57.2242 34.8964 5 -11 9 -9 59.9796 32.6406 3 -11 9 -10 104.226 39.6560 5 -11 9 -10 93.8213 40.1489 3 -11 9 -11 35.6114 38.1145 5 -11 9 -11 65.0698 38.9604 3 -11 9 -12 137.651 48.7550 5 -11 9 -12 58.8713 44.3515 3 -11 11 12 334.131 57.9642 8 -11 11 11 119.137 44.8701 8 -11 11 10 105.828 37.5653 8 -11 11 9 7.24565 29.5749 8 -11 11 6 1323.69 77.0479 7 -11 11 5 1309.30 72.6880 7 -11 11 4 1496.07 74.2001 7 -11 11 3 1102.71 59.6305 7 -11 11 2 434.403 38.2197 7 -11 11 2 387.100 43.2559 3 -11 11 1 328.914 30.0721 7 -11 11 1 363.482 40.4172 3 -11 11 0 974.819 45.6913 7 -11 11 0 895.390 59.7981 3 -11 11 -1 111.267 17.9153 7 -11 11 -1 118.143 29.6294 3 -11 11 -2 2142.11 90.7050 3 -11 11 -3 699.733 57.9320 3 11 11 4 1043.12 50.4771 7 -11 11 -4 1007.99 68.9803 3 -11 11 -5 1042.23 72.2564 3 -11 11 -6 457.267 53.8213 3 -11 11 -7 328.508 49.8935 3 -11 11 -8 719.897 69.3702 3 -11 11 -9 14.9473 29.5971 5 -11 11 -9 64.1006 36.0822 3 -11 11 -10 228.650 48.5230 5 -11 11 -10 158.442 46.7948 3 -11 11 -11 37.9286 36.9531 5 -11 11 -11 53.6691 41.4329 3 -11 11 -12 141.707 49.6284 5 -11 11 -12 185.163 55.7180 3 -11 13 11 271.109 54.3226 8 -11 13 10 219.716 50.6689 8 -11 13 9 1386.67 93.4701 8 -11 13 7 1343.71 86.4945 7 -11 13 6 1603.48 88.4069 7 -11 13 5 232.071 39.2471 7 -11 13 4-4.41257 19.0626 7 -11 13 3 919.222 58.0713 7 -11 13 2 36.6364 18.3752 7 -11 13 1 1570.93 66.8202 7 -11 13 1 1505.71 79.4804 3 -11 13 0 2003.65 72.3156 7 -11 13 0 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31.6647 33.1858 3 -11 15 -9 36.3663 35.0588 3 -11 15 -10 112.064 42.2109 5 -11 15 -10 176.942 49.0927 3 -11 15 -11-63.2661 41.4876 5 -11 15 -11 90.3933 46.7473 3 -11 17 9 270.561 55.0996 7 -11 17 8 10.7751 31.5448 7 -11 17 7 181.108 44.6554 7 -11 17 6 1831.57 103.731 7 -11 17 5 171.870 39.7711 7 -11 17 4 3329.46 125.883 7 -11 17 3 2088.82 97.0275 7 -11 17 2 707.786 58.0834 7 -11 17 1 1123.39 66.8486 7 -11 17 0 650.899 59.9193 3 -11 17 -1 152.604 39.3876 3 -11 17 -2 2946.17 121.643 3 -11 17 -3 1038.76 75.9527 3 -11 17 -4 1682.79 97.9337 3 11 17 5 864.660 63.9312 7 -11 17 -5 747.094 68.6562 3 -11 17 -6 294.900 52.6169 3 -11 17 -7 333.054 54.5703 3 -11 17 -8 63.0028 37.7063 3 -11 17 -9 65.7288 42.0725 3 -11 17 -10 340.926 61.0085 3 -11 19 9 1509.06 110.519 7 -11 19 8 345.239 59.7495 7 -11 19 7 174.790 45.3732 7 -11 19 6 201.353 45.1082 7 -11 19 5 83.0733 35.7094 7 -11 19 4 320.665 48.7533 7 -11 19 3 829.743 66.8587 7 -11 19 2 702.913 60.3185 7 -11 19 1 448.551 48.6898 7 -11 19 0 142.771 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1078.53 70.2493 6 12 -16 2 2329.65 100.843 6 12 -16 3 1943.81 95.8373 6 12 -16 4 3226.80 123.291 6 12 -16 4 3501.03 127.474 1 12 -16 5 1124.80 78.1378 6 12 -16 5 1177.08 80.3728 1 12 -16 6 675.120 65.6430 1 12 -16 7 241.540 47.6743 1 12 -16 8 1266.04 89.5071 1 12 -16 9 864.916 77.9168 1 12 -16 10 1507.04 101.218 1 12 -14 -10 878.607 74.8920 2 12 -14 -9 523.925 58.4916 2 12 -14 -8 311.922 45.5786 2 12 -14 -7 27.4296 25.3888 2 12 -14 -5 677.372 48.6025 4 12 -14 -4 980.045 59.2032 4 12 -14 -3 328.942 39.6871 4 12 -14 -2 1360.06 69.3584 6 12 -14 -2 1331.80 70.1906 4 12 -14 -1 24.0445 22.7326 6 12 -14 0 1009.68 64.0352 6 12 -14 1 63.5849 26.4463 6 12 -14 2 1391.23 76.8540 6 12 -14 2 1568.25 80.3910 1 12 -14 3 368.990 46.7520 1 12 -14 4 380.862 48.7818 1 12 -14 5 554.339 57.2423 1 12 -14 6 33.9294 32.5210 1 12 -14 7 110.001 37.6935 1 12 -14 8 478.957 59.1769 1 12 -14 9 382.547 56.2999 1 12 -14 10 688.099 72.8282 1 12 -14 11 693.759 74.2357 1 12 -12 -11 1012.37 80.6688 2 12 -12 -10 2.82132 25.4961 2 12 -12 -9 45.0808 28.8139 2 12 -12 -8 5657.52 159.548 2 12 -12 -7 3687.74 121.729 2 12 -12 -5 1943.59 75.9900 4 12 -12 -4 538.513 43.2497 4 12 -12 -3 862.221 52.3678 6 12 -12 -3 900.431 54.0184 4 12 -12 -2 4503.25 116.028 6 12 -12 -1 5535.86 131.195 6 12 -12 0 1278.47 67.2717 6 12 -12 1 3700.51 112.459 1 12 -12 2 3660.08 115.848 1 12 -12 3 906.666 62.9894 1 12 -12 4 1376.23 77.6317 1 12 -12 5 2177.63 99.3592 1 12 -12 6 397.895 50.3119 1 12 -12 7 2813.55 119.266 1 12 -12 8 5166.42 164.396 1 12 -12 9 12.8373 33.4348 1 12 -12 10 15.0510 34.6317 1 12 -12 11 1158.83 88.6350 1 12 -10 -11 2933.71 129.163 2 12 -10 -10 13.9310 27.0523 2 12 -10 -9 124.282 37.3265 2 12 -10 -8 290.535 41.3127 2 12 -10 -7 1046.56 66.3544 2 12 -10 -6 59.1266 23.5858 2 12 -10 -5 6002.45 120.774 4 12 -10 -4 73.3609 22.8054 4 12 -10 -3 1719.01 67.2739 6 12 -10 -3 1623.77 66.7907 4 12 -10 -2 1544.10 66.0202 6 12 -10 -1 3356.28 97.8502 6 12 -10 -1 3224.31 95.4419 1 12 -10 0 90.3829 26.3916 1 12 -10 1 3292.33 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1 19 -9 6 64.8215 41.4557 1 19 -7 -1 682.853 58.2921 6 19 -7 -1 795.360 63.2070 1 19 -7 0 415.655 51.2019 1 19 -7 1 236.893 46.7908 1 19 -7 2 593.620 62.9702 1 19 -7 3 90.9197 37.4152 1 19 -7 4 145.261 46.6564 1 19 -7 5 125.105 43.7837 1 19 -7 6 273.036 56.6890 1 19 -7 7 108.465 45.6003 1 19 -5 -1 120.122 34.2588 1 19 -5 0-20.7672 28.8225 1 19 -5 1 77.4468 33.1248 1 19 -5 2 22.5116 30.9730 1 19 -5 3 36.5460 35.8729 1 19 -5 4 20.4823 34.2272 1 19 -5 5 65.2638 43.5103 1 -19 -5 -6-18.2452 36.1048 3 19 -5 6-38.5847 39.9556 1 -19 -5 -7 143.481 51.1671 3 19 -5 7 81.4901 43.3426 1 -19 -5 -8-25.5346 46.9629 3 19 -3 -1 98.6063 30.2566 1 19 -3 0 124.722 34.3270 1 19 -3 1-9.91255 28.7375 1 19 -3 2 44.3669 33.9312 1 19 -3 3 23.4790 32.8481 1 19 -3 4-45.5931 37.3828 1 -19 -3 -4 3.06013 29.0797 3 19 -3 5 65.9601 38.1198 1 -19 -3 -5 53.7436 35.8829 3 -19 -3 -6-23.8168 38.9626 3 -19 -3 -7 86.0878 45.1027 3 -19 -3 -8 125.430 52.8466 3 19 -1 0 110.182 33.0821 1 19 -1 1-17.7716 33.7328 1 -19 -1 -2 73.9968 29.9629 3 -19 -1 -3 39.9782 30.8367 3 -19 -1 -4 43.7089 31.9053 3 -19 -1 -5 146.651 42.8300 3 -19 -1 -6 125.163 46.3312 3 -19 -1 -7-2.95864 37.6522 3 -19 -1 -8 163.375 54.8578 3 -19 1 0 191.517 39.7399 5 19 1 0 80.6350 29.2409 1 -19 1 0 132.051 33.9886 3 -19 1 -1 121.005 37.9873 5 -19 1 -1 31.0260 25.0929 3 -19 1 -2 39.5006 32.5550 5 -19 1 -2 43.1271 31.1561 3 -19 1 -3 16.2986 33.4116 5 -19 1 -3 32.4139 31.0751 3 -19 1 -4 133.666 45.4886 5 -19 1 -4 25.6537 32.4569 3 -19 1 -5 277.358 55.5094 5 -19 1 -5 252.633 51.9379 3 -19 1 -6 243.346 54.0539 5 -19 1 -6 92.2435 44.4107 3 -19 1 -7 138.083 50.8623 3 -19 1 -8 109.971 53.0046 3 -19 3 1 151.286 37.2674 3 -19 3 0 256.160 43.8199 5 -19 3 0 184.727 39.7484 3 -19 3 -1 39.5417 30.8454 5 -19 3 -1 8.16159 25.3521 3 -19 3 -2 220.941 47.4171 5 -19 3 -2 90.0549 33.8092 3 -19 3 -3 57.3442 37.8437 5 -19 3 -3 34.9066 31.2756 3 -19 3 -4 83.9321 39.7489 5 -19 3 -4 111.378 39.9957 3 -19 3 -5 167.721 51.6953 5 -19 3 -5 37.0276 35.9002 3 -19 3 -6 81.2535 41.6813 5 -19 3 -6 64.5359 41.6633 3 -19 3 -7 142.413 52.0939 5 -19 3 -7 91.1821 46.2458 3 -19 5 1 72.8493 33.0550 3 -19 5 0-23.4891 29.7007 5 -19 5 0 51.5799 31.9497 3 -19 5 -1 136.038 38.6586 5 -19 5 -1 12.6952 30.7842 3 -19 5 -2 34.3888 32.1014 5 -19 5 -2 58.3962 33.1950 3 -19 5 -3 38.1807 33.8631 5 -19 5 -3 86.4878 36.3235 3 -19 5 -4 25.7034 34.7619 5 -19 5 -4 51.1853 35.8070 3 -19 5 -5 45.5735 37.0283 5 -19 5 -5 118.345 45.0530 3 -19 5 -6 127.360 47.9587 5 -19 5 -6 91.7079 44.8420 3 -19 5 -7 270.469 60.4479 5 -19 5 -7 100.740 46.0777 3 -19 7 1 667.847 61.3698 5 -19 7 1 765.343 69.7134 3 -19 7 0 306.139 46.0981 5 -19 7 0 313.445 50.7188 3 -19 7 -1 128.165 39.2376 5 -19 7 -1 146.918 38.9821 3 -19 7 -2 538.825 63.1062 5 -19 7 -2 611.450 64.8643 3 -19 7 -3 120.012 43.2540 5 -19 7 -3 96.7923 37.2415 3 -19 7 -4 78.5972 41.6501 5 -19 7 -4 99.8923 43.1600 3 -19 7 -5 241.420 54.8555 5 -19 7 -5 251.950 52.8043 3 -19 7 -6 237.007 54.1696 5 -19 7 -6 246.147 60.3334 3 -19 7 -7 298.878 60.3148 5 -19 7 -7 195.236 55.5515 3 -19 9 1 66.0451 32.6071 5 -19 9 1 123.844 40.3408 3 -19 9 0-6.65229 29.0274 5 -19 9 0 32.5848 32.8874 3 -19 9 -1 11.9347 30.6199 5 -19 9 -1 62.2777 36.0037 3 -19 9 -2 83.3670 37.4527 5 -19 9 -2 24.8440 31.4787 3 -19 9 -3 269.823 52.8699 5 -19 9 -3 272.244 52.4421 3 -19 9 -4 252.034 53.1599 5 -19 9 -4 301.825 57.5626 3 -19 9 -5 32.6217 38.0155 5 -19 9 -5 142.177 46.1975 3 -19 9 -6 12.0476 37.3806 5 -19 9 -6 102.880 47.2305 3 -19 11 0 261.561 50.7375 3 -19 11 -1 62.7923 36.9918 3 -19 11 -2 301.425 51.7352 3 -19 11 -3 381.883 62.0421 5 -19 11 -3 129.491 42.7463 3 -19 11 -4 132.609 47.0908 5 -19 11 -4 89.8256 41.1078 3 -19 11 -5 597.398 75.1874 5 -19 11 -5 601.829 75.3270 3 -19 13 0 1036.21 87.1238 3 -19 13 -1 221.313 50.5812 3 -19 13 -2 450.521 64.4639 3 -19 13 -3 85.5563 41.3827 3 -19 13 -4 132.177 48.4000 5 -19 13 -4-26.7369 42.4540 3 -19 15 0 96.6928 44.2768 3 -19 15 -1 53.0492 37.7589 3 -19 15 -2 75.3797 41.4385 3 -19 15 -3 67.0667 41.0724 3 20 -16 0 184.907 47.7998 4 20 -14 0 498.728 60.6796 6 20 -14 1 165.417 45.0048 6 20 -14 2 358.800 61.7973 6 20 -12 0 176.197 42.8070 6 20 -12 1 438.633 58.1819 6 20 -12 2 926.745 78.5737 6 20 -12 2 1214.41 90.3956 1 20 -12 3 1041.61 87.4564 1 20 -10 0 149.621 39.1632 6 20 -10 1 611.001 64.4417 6 20 -10 1 647.543 66.4443 1 20 -10 2 285.578 53.1887 1 20 -10 3 131.309 44.9930 1 20 -10 4 34.1250 37.7935 1 20 -8 0 301.094 48.5918 1 20 -8 1 827.684 71.0507 1 20 -8 2 1639.70 101.665 1 20 -8 3 251.484 51.0753 1 20 -8 4 969.581 85.3562 1 20 -8 5 699.663 75.6003 1 20 -6 0 283.294 46.2673 1 20 -6 1 43.6235 35.0982 1 20 -6 2 2305.66 115.299 1 20 -6 3 1541.13 98.2780 1 20 -6 4 268.610 54.3714 1 20 -6 5 21.9677 40.5136 1 20 -6 6 174.794 52.4606 1 20 -4 0 859.625 67.5266 1 20 -4 1 2848.80 120.975 1 20 -4 2 144.730 41.0167 1 20 -4 3 80.5357 37.9493 1 20 -4 4 7.66886 36.6436 1 20 -4 5 2356.31 128.837 1 20 -4 6 2345.53 131.761 1 20 -2 0 317.565 45.1327 1 20 -2 1 415.847 53.3252 1 20 -2 2 362.064 53.9927 1 20 -2 3 129.535 42.0301 1 20 -2 4-19.7254 36.7645 1 -20 -2 -5 954.172 84.1015 3 -20 -2 -6 142.959 45.5555 3 -20 -2 -7 223.244 56.9460 3 20 0 0 1495.97 85.4330 1 20 0 1 40.1287 34.9083 1 -20 0 -3 2526.39 129.718 5 -20 0 -3 2428.34 117.694 3 -20 0 -4 2265.34 120.319 3 -20 0 -5 96.4836 47.7113 3 -20 0 -6 42.5596 40.2763 3 -20 0 -7 145.268 51.6173 3 -20 2 -1 594.638 64.5523 5 -20 2 -1 529.330 56.7399 3 -20 2 -2 344.620 54.7281 5 -20 2 -2 338.189 51.4933 3 -20 2 -3 236.880 54.2155 5 -20 2 -3 119.149 39.2994 3 -20 2 -4 127.503 47.5494 5 -20 2 -4 14.7810 35.2155 3 -20 2 -5 912.861 89.6636 5 -20 2 -5 898.364 85.5760 3 -20 2 -6 109.892 48.9750 5 -20 2 -6 120.482 49.6512 3 -20 2 -7 217.008 56.8019 3 -20 4 1 2643.36 118.404 3 -20 4 0 922.210 74.3678 5 -20 4 0 741.792 68.4360 3 -20 4 -1 2825.34 128.712 5 -20 4 -1 2572.73 120.422 3 -20 4 -2 248.520 51.5513 5 -20 4 -2 77.9760 38.6620 3 -20 4 -3 142.527 46.2668 5 -20 4 -3 191.362 45.2083 3 -20 4 -4 189.052 48.9146 5 -20 4 -4 46.0759 37.4302 3 -20 4 -5 2486.97 139.518 5 -20 4 -5 2350.04 133.411 3 -20 4 -6 2727.90 148.526 5 -20 4 -6 2532.41 143.621 3 -20 6 1 62.6547 35.5301 3 -20 6 0 217.867 44.3683 5 -20 6 0 277.385 49.8023 3 -20 6 -1 24.8064 31.3471 5 -20 6 -1 83.8069 36.7900 3 -20 6 -2 2222.00 121.579 5 -20 6 -2 1923.25 110.861 3 -20 6 -3 1517.80 105.668 5 -20 6 -3 1443.51 99.7700 3 -20 6 -4 297.603 58.4032 5 -20 6 -4 217.472 50.0881 3 -20 6 -5 78.8441 45.6171 5 -20 6 -5 112.712 51.2926 3 -20 6 -6 388.041 68.0128 5 -20 6 -6 207.190 56.7254 3 -20 8 1 476.655 60.7793 3 -20 8 0 200.694 45.0144 5 -20 8 0 406.982 58.9418 3 -20 8 -1 932.677 80.5803 5 -20 8 -1 888.311 79.9426 3 -20 8 -2 1518.21 103.629 5 -20 8 -2 1368.19 96.8343 3 -20 8 -3 273.141 53.9365 5 -20 8 -3 209.699 49.0173 3 -20 8 -4 972.329 90.8243 5 -20 8 -4 959.993 88.6191 3 -20 8 -5 616.576 77.0023 5 -20 8 -5 661.161 80.0458 3 -20 10 0 157.093 41.9730 5 -20 10 0 196.149 47.0266 3 -20 10 -1 654.590 72.1213 5 -20 10 -1 661.013 74.0476 3 -20 10 -2 103.982 41.3789 5 -20 10 -2 166.984 46.0357 3 -20 10 -3 124.648 46.2345 5 -20 10 -3 17.7425 36.8901 3 -20 10 -4 7.85327 35.8617 5 -20 10 -4-25.5582 40.3930 3 -20 12 0 158.170 47.1886 3 -20 12 -1 554.448 70.3825 5 -20 12 -1 513.690 67.1249 3 -20 12 -2 1065.58 93.8934 5 -20 12 -2 1039.65 91.8921 3 -20 12 -3 1010.24 93.0352 5 -20 12 -3 836.389 83.5556 3 -20 14 0 561.095 71.1453 3 -20 14 -1 220.847 56.7711 3 21 -11 1 188.469 46.0468 6 21 -11 2 122.759 86.8764 6 21 -11 2 127.789 47.1235 1 21 -9 1 31.3855 34.0571 6 21 -9 1 82.2057 42.0999 1 21 -9 2 87.5619 43.2636 1 21 -9 3 40.3541 39.8697 1 21 -7 1 308.492 52.7371 1 21 -7 2 268.212 52.3932 1 21 -7 3 241.525 51.7313 1 21 -7 4 187.295 50.2857 1 21 -5 1 864.496 73.7972 1 21 -5 2 342.609 56.2519 1 21 -5 3 586.628 68.8320 1 21 -5 4 1205.55 94.7161 1 21 -3 1 121.980 40.9348 1 21 -3 2 10.2139 35.7703 1 21 -3 3 5.12958 38.5320 1 21 -3 4 5.19632 38.9783 1 21 -3 5 72.2059 44.6584 1 21 -1 1 1610.08 96.1177 1 21 -1 2 143.780 45.6107 1 21 -1 3 144.690 45.7441 1 21 -1 4 774.336 80.3547 1 21 -1 5 28.8751 38.9067 1 21 1 1 1560.18 95.1862 1 -21 1 -4 740.013 77.3684 3 -21 1 -5 60.8435 40.1070 3 -21 1 -6 489.136 75.0049 3 -21 3 -1 130.444 42.5762 5 -21 3 -2 130.610 45.5547 5 -21 3 -2-59.0411 42.6472 3 -21 3 -3 88.9966 45.7131 5 -21 3 -3 80.8562 39.8659 3 -21 3 -4 89.8381 44.0108 5 -21 3 -4 41.8378 37.9090 3 -21 3 -5 165.080 50.0202 5 -21 3 -5 84.0347 44.3589 3 -21 5 0 427.993 59.3236 3 -21 5 -1 951.507 82.9462 5 -21 5 -1 749.717 73.9759 3 -21 5 -2 317.356 57.6239 5 -21 5 -2 102.818 45.4490 3 -21 5 -3 724.462 79.3035 5 -21 5 -3 682.560 74.2389 3 -21 5 -4 1318.41 104.748 5 -21 5 -4 1104.68 94.4344 3 -21 5 -5 171.697 54.3877 3 -21 7 0 95.9587 37.9184 3 -21 7 -1 416.294 61.2818 5 -21 7 -1 335.576 57.7088 3 -21 7 -2 194.411 51.6983 5 -21 7 -2 171.525 42.8837 3 -21 7 -3 327.141 59.8722 5 -21 7 -3 241.935 51.7602 3 -21 7 -4 169.345 50.1608 5 -21 7 -4 233.470 53.8495 3 -21 9 0 23.5936 34.0248 3 -21 9 -1 73.9283 42.5632 5 -21 9 -1 22.2462 34.7148 3 -21 9 -2 43.5390 41.2476 5 -21 9 -2 57.9987 39.9731 3 -21 9 -3 35.0786 38.1637 5 -21 9 -3-29.3863 38.0777 3 -21 11 0 14.7769 37.4871 3 -21 11 -1 56.2903 35.9289 5 -21 11 -1 154.415 47.1141 3 -21 11 -2 55.3716 40.5506 5 -21 11 -2 124.528 49.6528 3 22 -8 2 149.107 52.4339 1 22 -6 2 74.0815 44.0176 1 22 -4 2 3.57233 37.7519 1 22 -4 3 32.1904 37.8526 1 22 -2 2 58.1789 44.2004 1 22 -2 3 121.078 105.818 1 22 0 2-31.0879 41.1203 1 22 0 3 0.64008 41.0243 1 22 2 2-45.5508 43.2847 1 -22 4 -2 168.910 54.3085 5 -22 4 -3 128.153 49.9470 5 -22 6 -2 289.341 62.7077 5 -22 6 -2 204.153 52.8936 3 -22 6 -3 165.732 46.7648 3 -22 8 -1 102.022 47.0273 3 -22 8 -2 99.9699 48.1066 3 0 0 0 0.00 0.00 0 TITL 2man075_C2 in C2 REM C2 (#5 in standard setting) CELL 0.71073 13.342760 18.931951 8.940431 90.0000 90.3613 90.0000 ZERR 23.00 0.000374 0.000489 0.000204 0.0000 0.0023 0.0000 LATT -7 SYMM -x, y,-z SFAC O Na Al P Cu UNIT 23.00 23.00 23.00 23.00 23.00 TREF HKLF 4 END ; _shelx_hkl_checksum 32329 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.250000 0.250000 0.500000 0.0109(2) Uani 1 2 d S . P . . Cu2 Cu 0.12705(5) 0.41671(3) 0.31049(7) 0.01122(16) Uani 1 1 d . . . . . Cu3 Cu 0.000000 0.24835(5) 0.500000 0.0138(2) Uani 1 2 d S T P . . Cu4 Cu 0.62554(8) 0.74519(3) 0.82896(7) 0.02009(19) Uani 1 1 d . . . . . P1 P 0.12573(12) 0.26303(7) 0.19526(14) 0.0112(3) Uani 1 1 d . . . . . P2 P 0.11905(10) 0.61919(6) 0.66727(13) 0.0068(2) Uani 1 1 d . . . . . P3 P 0.63242(10) 0.61716(7) 0.65454(13) 0.0080(3) Uani 1 1 d . . . . . Al1 Al 0.24664(16) 0.500000 0.5261(2) 0.0073(4) Uani 1 2 d S T P . . Al2 Al 0.000000 0.500000 0.500000 0.0060(6) Uani 1 4 d S T P . . Al3 Al 0.500000 0.500000 0.500000 0.0086(6) Uani 1 4 d S T P . . Na1 Na 0.000000 0.60798(18) 1.000000 0.0116(6) Uani 1 2 d S T P . . Na2 Na 0.74974(18) 0.61404(16) 1.0123(3) 0.0231(6) Uani 1 1 d . . . . . Na3 Na 0.6188(3) 0.6185(2) 0.3120(4) 0.0129(12) Uani 0.556(10) 1 d . . P . . Li1 Li 0.6222(17) 0.5757(14) 0.300(2) 0.0129(12) Uani 0.444(10) 1 d . . P . . Na4 Na 0.504(2) 0.6190(6) 1.0348(16) 0.064(6) Uani 0.420(15) 1 d . . P . . Li2 Li 0.504(2) 0.6190(6) 1.0348(16) 0.064(6) Uani 0.080(15) 1 d . . P . . Cl2 Cl 0.6191(3) 0.5102(4) 1.0679(3) 0.0147(17) Uani 0.375(4) 1 d . . P . . O15 O 0.5411(17) 0.500000 0.847(2) 0.0147(17) Uani 0.251(8) 2 d S T P . . Cl1 Cl 0.13134(16) 0.500000 0.06802(19) 0.0146(4) Uani 1 2 d S T P . . O1 O 0.3752(4) 0.500000 0.5926(5) 0.0088(9) Uani 1 2 d S T P . . O2 O 0.1252(4) 0.500000 0.4326(5) 0.0064(9) Uani 1 2 d S T P . . O3 O 0.2119(3) 0.5716(2) 0.6616(4) 0.0113(7) Uani 1 1 d . . . . . O4 O 0.7272(3) 0.5722(2) 0.6287(4) 0.0114(8) Uani 1 1 d . . . . . O5 O 0.0234(3) 0.5724(2) 0.6514(4) 0.0082(7) Uani 1 1 d . . . . . O6 O 0.1167(3) 0.65488(18) 0.8223(4) 0.0084(7) Uani 1 1 d . . . . . O7 O 0.6308(3) 0.6793(2) 0.5442(4) 0.0182(8) Uani 1 1 d . . . . . O8 O 0.1191(3) 0.6728(2) 0.5402(4) 0.0156(8) Uani 1 1 d . . . . . O9 O 0.5405(3) 0.5711(2) 0.6362(4) 0.0136(8) Uani 1 1 d . . . . . O10 O 0.6358(3) 0.64578(18) 0.8147(4) 0.0097(7) Uani 1 1 d . . . . . O11 O 0.2212(3) 0.2434(2) 0.2855(5) 0.0147(8) Uani 1 1 d . . . . . O12 O 0.0305(3) 0.2412(2) 0.2816(5) 0.0185(9) Uani 1 1 d . . . . . O13 O 0.1248(3) 0.34339(19) 0.1676(4) 0.0102(7) Uani 1 1 d . . . . . O14 O 0.1273(5) 0.2248(2) 0.0484(5) 0.0360(12) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.0121(4) 0.0120(5) 0.0086(4) 0.0019(3) 0.0023(4) 0.0010(3) Cu2 0.0106(3) 0.0121(3) 0.0110(3) -0.0057(2) 0.0013(3) 0.0003(3) Cu3 0.0156(5) 0.0147(5) 0.0112(5) 0.000 0.0003(4) 0.000 Cu4 0.0481(5) 0.0052(3) 0.0070(3) -0.0006(2) -0.0003(4) 0.0034(3) P1 0.0160(6) 0.0103(6) 0.0074(5) -0.0006(4) 0.0002(6) 0.0013(6) P2 0.0113(6) 0.0047(5) 0.0045(5) -0.0002(4) 0.0009(5) -0.0009(5) P3 0.0115(6) 0.0066(6) 0.0059(5) -0.0015(4) 0.0018(5) 0.0000(5) Al1 0.0077(10) 0.0077(10) 0.0065(9) 0.000 0.0008(8) 0.000 Al2 0.0066(13) 0.0063(14) 0.0052(13) 0.000 0.0009(11) 0.000 Al3 0.0084(14) 0.0098(15) 0.0076(14) 0.000 0.0022(11) 0.000 Na1 0.0112(14) 0.0132(15) 0.0103(13) 0.000 0.0001(12) 0.000 Na2 0.0157(11) 0.0266(15) 0.0272(14) -0.0016(10) -0.0028(11) 0.0006(10) Na3 0.0114(18) 0.015(2) 0.0124(18) 0.0052(16) 0.0048(15) 0.0011(17) Li1 0.0114(18) 0.015(2) 0.0124(18) 0.0052(16) 0.0048(15) 0.0011(17) Na4 0.017(5) 0.083(7) 0.091(16) -0.020(6) 0.016(11) 0.001(6) Li2 0.017(5) 0.083(7) 0.091(16) -0.020(6) 0.016(11) 0.001(6) Cl2 0.0218(14) 0.013(5) 0.0090(12) 0.0041(14) 0.0038(11) -0.0010(16) O15 0.0218(14) 0.013(5) 0.0090(12) 0.0041(14) 0.0038(11) -0.0010(16) Cl1 0.0225(9) 0.0115(8) 0.0097(7) 0.000 -0.0004(7) 0.000 O1 0.006(2) 0.010(2) 0.010(2) 0.000 0.002(2) 0.000 O2 0.009(2) 0.006(2) 0.004(2) 0.000 0.0016(19) 0.000 O3 0.0118(17) 0.0094(17) 0.0128(18) -0.0048(14) 0.0025(14) 0.0004(14) O4 0.0100(17) 0.0101(18) 0.0142(18) -0.0057(15) 0.0044(14) -0.0006(14) O5 0.0088(16) 0.0082(17) 0.0075(16) -0.0022(14) -0.0011(13) 0.0002(13) O6 0.0144(17) 0.0060(15) 0.0049(15) -0.0011(12) 0.0005(14) -0.0012(14) O7 0.030(2) 0.0143(19) 0.0106(17) 0.0049(15) 0.0032(17) -0.0005(19) O8 0.027(2) 0.0121(18) 0.0078(16) 0.0027(14) -0.0004(16) -0.0058(18) O9 0.0109(17) 0.0149(19) 0.0150(18) -0.0072(16) 0.0031(14) -0.0023(15) O10 0.0159(17) 0.0076(16) 0.0057(15) -0.0020(13) 0.0018(14) 0.0004(15) O11 0.0158(19) 0.016(2) 0.0121(19) 0.0042(15) 0.0037(15) 0.0069(15) O12 0.019(2) 0.018(2) 0.018(2) 0.0075(16) -0.0025(17) -0.0061(17) O13 0.0126(16) 0.0106(17) 0.0074(15) -0.0026(13) 0.0018(15) 0.0000(15) O14 0.081(4) 0.015(2) 0.0115(19) -0.0032(16) -0.003(3) 0.009(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O11 Cu1 O11 180.0 7_556 . ? O11 Cu1 O7 89.97(16) 7_556 5_666 ? O11 Cu1 O7 90.03(16) . 5_666 ? O11 Cu1 O7 90.03(16) 7_556 3_445 ? O11 Cu1 O7 89.97(16) . 3_445 ? O7 Cu1 O7 180.00(17) 5_666 3_445 ? O11 Cu1 O8 87.20(14) 7_556 6_565 ? O11 Cu1 O8 92.80(14) . 6_565 ? O7 Cu1 O8 101.48(16) 5_666 6_565 ? O7 Cu1 O8 78.52(16) 3_445 6_565 ? O11 Cu1 O8 92.80(14) 7_556 4_546 ? O11 Cu1 O8 87.20(14) . 4_546 ? O7 Cu1 O8 78.52(16) 5_666 4_546 ? O7 Cu1 O8 101.48(16) 3_445 4_546 ? O8 Cu1 O8 180.0 6_565 4_546 ? O11 Cu1 Na3 127.99(14) 7_556 3_445 ? O11 Cu1 Na3 52.01(14) . 3_445 ? O7 Cu1 Na3 137.72(12) 5_666 3_445 ? O7 Cu1 Na3 42.28(12) 3_445 3_445 ? O8 Cu1 Na3 98.60(12) 6_565 3_445 ? O8 Cu1 Na3 81.40(12) 4_546 3_445 ? O11 Cu1 Na3 52.01(14) 7_556 5_666 ? O11 Cu1 Na3 127.99(14) . 5_666 ? O7 Cu1 Na3 42.28(12) 5_666 5_666 ? O7 Cu1 Na3 137.72(12) 3_445 5_666 ? O8 Cu1 Na3 81.40(12) 6_565 5_666 ? O8 Cu1 Na3 98.60(12) 4_546 5_666 ? Na3 Cu1 Na3 180.00(9) 3_445 5_666 ? O13 Cu2 O2 171.92(16) . . ? O13 Cu2 O4 105.60(16) . 5_666 ? O2 Cu2 O4 77.17(19) . 5_666 ? O13 Cu2 O5 100.09(15) . 5_566 ? O2 Cu2 O5 78.85(19) . 5_566 ? O4 Cu2 O5 152.18(14) 5_666 5_566 ? O13 Cu2 Cl1 83.43(11) . . ? O2 Cu2 Cl1 88.69(11) . . ? O4 Cu2 Cl1 97.51(12) 5_666 . ? O5 Cu2 Cl1 95.82(11) 5_566 . ? O13 Cu2 Al2 142.71(12) . . ? O2 Cu2 Al2 37.26(16) . . ? O4 Cu2 Al2 110.70(11) 5_666 . ? O5 Cu2 Al2 42.68(10) 5_566 . ? Cl1 Cu2 Al2 99.76(4) . . ? O13 Cu2 Al1 147.31(12) . . ? O2 Cu2 Al1 36.66(16) . . ? O4 Cu2 Al1 41.89(11) 5_666 . ? O5 Cu2 Al1 111.35(11) 5_566 . ? Cl1 Cu2 Al1 101.51(5) . . ? Al2 Cu2 Al1 68.93(4) . . ? O13 Cu2 Na1 46.81(12) . 5_566 ? O2 Cu2 Na1 126.23(15) . 5_566 ? O4 Cu2 Na1 137.09(11) 5_666 5_566 ? O5 Cu2 Na1 69.70(10) 5_566 5_566 ? Cl1 Cu2 Na1 54.03(6) . 5_566 ? Al2 Cu2 Na1 105.88(4) . 5_566 ? Al1 Cu2 Na1 154.72(6) . 5_566 ? O13 Cu2 Na2 45.66(12) . 5_666 ? O2 Cu2 Na2 129.45(14) . 5_666 ? O4 Cu2 Na2 77.06(11) 5_666 5_666 ? O5 Cu2 Na2 129.91(11) 5_566 5_666 ? Cl1 Cu2 Na2 53.00(6) . 5_666 ? Al2 Cu2 Na2 152.76(5) . 5_666 ? Al1 Cu2 Na2 112.69(6) . 5_666 ? Na1 Cu2 Na2 60.27(4) 5_566 5_666 ? O12 Cu3 O12 172.3(3) 2_556 . ? O12 Cu3 O8 92.15(16) 2_556 6_565 ? O12 Cu3 O8 93.07(15) . 6_565 ? O12 Cu3 O8 93.07(15) 2_556 5_566 ? O12 Cu3 O8 92.15(16) . 5_566 ? O8 Cu3 O8 94.9(2) 6_565 5_566 ? O12 Cu3 O7 88.25(16) 2_556 4_546 ? O12 Cu3 O7 87.19(16) . 4_546 ? O8 Cu3 O7 173.64(16) 6_565 4_546 ? O8 Cu3 O7 78.74(16) 5_566 4_546 ? O12 Cu3 O7 87.19(16) 2_556 3_445 ? O12 Cu3 O7 88.24(16) . 3_445 ? O8 Cu3 O7 78.74(16) 6_565 3_445 ? O8 Cu3 O7 173.64(16) 5_566 3_445 ? O7 Cu3 O7 107.6(2) 4_546 3_445 ? O12 Cu3 Na3 122.37(14) 2_556 3_445 ? O12 Cu3 Na3 50.70(14) . 3_445 ? O8 Cu3 Na3 103.50(12) 6_565 3_445 ? O8 Cu3 Na3 138.63(12) 5_566 3_445 ? O7 Cu3 Na3 81.57(13) 4_546 3_445 ? O7 Cu3 Na3 44.56(12) 3_445 3_445 ? O12 Cu3 Na3 50.70(14) 2_556 4_546 ? O12 Cu3 Na3 122.37(14) . 4_546 ? O8 Cu3 Na3 138.63(12) 6_565 4_546 ? O8 Cu3 Na3 103.50(12) 5_566 4_546 ? O7 Cu3 Na3 44.56(12) 4_546 4_546 ? O7 Cu3 Na3 81.57(13) 3_445 4_546 ? Na3 Cu3 Na3 86.65(13) 3_445 4_546 ? O10 Cu4 O6 174.30(14) . 8_565 ? O10 Cu4 O14 82.72(17) . 3_556 ? O6 Cu4 O14 102.96(17) 8_565 3_556 ? O10 Cu4 O12 90.24(16) . 4_556 ? O6 Cu4 O12 87.89(16) 8_565 4_556 ? O14 Cu4 O12 114.9(2) 3_556 4_556 ? O10 Cu4 O11 89.92(15) . 5_666 ? O6 Cu4 O11 86.99(15) 8_565 5_666 ? O14 Cu4 O11 116.7(2) 3_556 5_666 ? O12 Cu4 O11 128.04(14) 4_556 5_666 ? O10 Cu4 Na4 47.3(4) . 2_657 ? O6 Cu4 Na4 136.4(4) 8_565 2_657 ? O14 Cu4 Na4 59.0(3) 3_556 2_657 ? O12 Cu4 Na4 69.4(4) 4_556 2_657 ? O11 Cu4 Na4 136.4(4) 5_666 2_657 ? O10 Cu4 Na2 43.18(12) . . ? O6 Cu4 Na2 140.67(13) 8_565 . ? O14 Cu4 Na2 51.90(16) 3_556 . ? O12 Cu4 Na2 128.34(13) 4_556 . ? O11 Cu4 Na2 81.45(11) 5_666 . ? Na4 Cu4 Na2 62.3(4) 2_657 . ? O10 Cu4 Na4 51.5(3) . . ? O6 Cu4 Na4 133.1(3) 8_565 . ? O14 Cu4 Na4 48.8(3) 3_556 . ? O12 Cu4 Na4 77.2(4) 4_556 . ? O11 Cu4 Na4 136.7(4) 5_666 . ? Na4 Cu4 Na4 10.2(5) 2_657 . ? Na2 Cu4 Na4 57.5(4) . . ? O10 Cu4 Na2 139.73(13) . 7_667 ? O6 Cu4 Na2 43.15(12) 8_565 7_667 ? O14 Cu4 Na2 75.09(17) 3_556 7_667 ? O12 Cu4 Na2 129.50(12) 4_556 7_667 ? O11 Cu4 Na2 71.47(12) 5_666 7_667 ? Na4 Cu4 Na2 133.1(3) 2_657 7_667 ? Na2 Cu4 Na2 97.69(7) . 7_667 ? Na4 Cu4 Na2 123.1(2) . 7_667 ? O10 Cu4 Na1 146.39(12) . 7_567 ? O6 Cu4 Na1 38.04(11) 8_565 7_567 ? O14 Cu4 Na1 74.62(15) 3_556 7_567 ? O12 Cu4 Na1 77.57(11) 4_556 7_567 ? O11 Cu4 Na1 122.30(11) 5_666 7_567 ? Na4 Cu4 Na1 99.2(4) 2_657 7_567 ? Na2 Cu4 Na1 125.94(5) . 7_567 ? Na4 Cu4 Na1 95.1(3) . 7_567 ? Na2 Cu4 Na1 56.71(5) 7_667 7_567 ? O14 P1 O13 109.7(2) . . ? O14 P1 O12 108.9(3) . . ? O13 P1 O12 109.7(2) . . ? O14 P1 O11 108.9(3) . . ? O13 P1 O11 109.0(2) . . ? O12 P1 O11 110.6(2) . . ? O14 P1 Na3 82.0(2) . 3_445 ? O13 P1 Na3 168.12(16) . 3_445 ? O12 P1 Na3 62.95(19) . 3_445 ? O11 P1 Na3 67.54(18) . 3_445 ? O14 P1 Na2 81.0(2) . 5_666 ? O13 P1 Na2 40.85(14) . 5_666 ? O12 P1 Na2 149.00(18) . 5_666 ? O11 P1 Na2 92.59(17) . 5_666 ? Na3 P1 Na2 147.83(10) 3_445 5_666 ? O14 P1 Na1 84.7(2) . 5_566 ? O13 P1 Na1 38.10(15) . 5_566 ? O12 P1 Na1 92.48(17) . 5_566 ? O11 P1 Na1 146.43(17) . 5_566 ? Na3 P1 Na1 145.98(10) 3_445 5_566 ? Na2 P1 Na1 58.45(5) 5_666 5_566 ? O8 P2 O3 111.3(2) . . ? O8 P2 O6 112.2(2) . . ? O3 P2 O6 107.9(2) . . ? O8 P2 O5 108.3(2) . . ? O3 P2 O5 108.9(2) . . ? O6 P2 O5 108.0(2) . . ? O8 P2 Na2 130.91(17) . 2_657 ? O3 P2 Na2 65.98(16) . 2_657 ? O6 P2 Na2 42.06(15) . 2_657 ? O5 P2 Na2 118.99(15) . 2_657 ? O8 P2 Na1 134.34(18) . . ? O3 P2 Na1 112.06(16) . . ? O6 P2 Na1 39.30(14) . . ? O5 P2 Na1 69.90(14) . . ? Na2 P2 Na1 59.51(5) 2_657 . ? O9 P3 O10 108.9(2) . . ? O9 P3 O7 111.3(3) . . ? O10 P3 O7 109.3(2) . . ? O9 P3 O4 109.3(2) . . ? O10 P3 O4 108.4(2) . . ? O7 P3 O4 109.6(2) . . ? O9 P3 Na3 81.60(18) . . ? O10 P3 Na3 158.74(17) . . ? O7 P3 Na3 49.57(17) . . ? O4 P3 Na3 84.16(17) . . ? O9 P3 Na4 69.4(4) . 2_657 ? O10 P3 Na4 39.7(4) . 2_657 ? O7 P3 Na4 121.5(3) . 2_657 ? O4 P3 Na4 125.8(4) . 2_657 ? Na3 P3 Na4 143.4(4) . 2_657 ? O9 P3 Na3 37.58(17) . 2_656 ? O10 P3 Na3 86.42(17) . 2_656 ? O7 P3 Na3 92.4(2) . 2_656 ? O4 P3 Na3 146.60(17) . 2_656 ? Na3 P3 Na3 92.07(10) . 2_656 ? Na4 P3 Na3 51.3(4) 2_657 2_656 ? O1 Al1 O2 171.8(3) . . ? O1 Al1 O3 91.46(18) . 6_565 ? O2 Al1 O3 94.22(17) . 6_565 ? O1 Al1 O3 91.46(18) . . ? O2 Al1 O3 94.22(17) . . ? O3 Al1 O3 92.4(3) 6_565 . ? O1 Al1 O4 93.36(18) . 5_666 ? O2 Al1 O4 80.74(17) . 5_666 ? O3 Al1 O4 89.88(17) 6_565 5_666 ? O3 Al1 O4 174.6(2) . 5_666 ? O1 Al1 O4 93.35(18) . 2_656 ? O2 Al1 O4 80.74(17) . 2_656 ? O3 Al1 O4 174.6(2) 6_565 2_656 ? O3 Al1 O4 89.88(17) . 2_656 ? O4 Al1 O4 87.5(2) 5_666 2_656 ? O1 Al1 Li1 38.1(5) . 2_656 ? O2 Al1 Li1 145.6(5) . 2_656 ? O3 Al1 Li1 99.9(5) 6_565 2_656 ? O3 Al1 Li1 54.3(5) . 2_656 ? O4 Al1 Li1 130.1(5) 5_666 2_656 ? O4 Al1 Li1 85.4(5) 2_656 2_656 ? O1 Al1 Li1 38.1(5) . 5_666 ? O2 Al1 Li1 145.6(5) . 5_666 ? O3 Al1 Li1 54.3(5) 6_565 5_666 ? O3 Al1 Li1 99.9(5) . 5_666 ? O4 Al1 Li1 85.4(5) 5_666 5_666 ? O4 Al1 Li1 130.1(5) 2_656 5_666 ? Li1 Al1 Li1 63.1(11) 2_656 5_666 ? O1 Al1 Cu2 136.15(12) . . ? O2 Al1 Cu2 39.04(8) . . ? O3 Al1 Cu2 84.33(13) 6_565 . ? O3 Al1 Cu2 132.24(15) . . ? O4 Al1 Cu2 43.18(12) 5_666 . ? O4 Al1 Cu2 90.55(14) 2_656 . ? Li1 Al1 Cu2 172.5(4) 2_656 . ? Li1 Al1 Cu2 115.6(5) 5_666 . ? O1 Al1 Cu2 136.15(12) . 6_565 ? O2 Al1 Cu2 39.04(8) . 6_565 ? O3 Al1 Cu2 132.24(15) 6_565 6_565 ? O3 Al1 Cu2 84.33(13) . 6_565 ? O4 Al1 Cu2 90.55(14) 5_666 6_565 ? O4 Al1 Cu2 43.18(12) 2_656 6_565 ? Li1 Al1 Cu2 115.6(5) 2_656 6_565 ? Li1 Al1 Cu2 172.5(4) 5_666 6_565 ? Cu2 Al1 Cu2 64.60(5) . 6_565 ? O1 Al1 Na3 47.70(9) . 2_656 ? O2 Al1 Na3 134.50(9) . 2_656 ? O3 Al1 Na3 110.66(17) 6_565 2_656 ? O3 Al1 Na3 49.06(14) . 2_656 ? O4 Al1 Na3 134.23(15) 5_666 2_656 ? O4 Al1 Na3 74.45(14) 2_656 2_656 ? Li1 Al1 Na3 12.9(5) 2_656 2_656 ? Li1 Al1 Na3 75.9(6) 5_666 2_656 ? Cu2 Al1 Na3 164.98(10) . 2_656 ? Cu2 Al1 Na3 102.68(8) 6_565 2_656 ? O1 Al1 Na3 47.70(9) . 5_666 ? O2 Al1 Na3 134.50(9) . 5_666 ? O3 Al1 Na3 49.06(14) 6_565 5_666 ? O3 Al1 Na3 110.66(16) . 5_666 ? O4 Al1 Na3 74.45(14) 5_666 5_666 ? O4 Al1 Na3 134.23(15) 2_656 5_666 ? Li1 Al1 Na3 75.9(6) 2_656 5_666 ? Li1 Al1 Na3 12.9(5) 5_666 5_666 ? Cu2 Al1 Na3 102.68(8) . 5_666 ? Cu2 Al1 Na3 164.98(10) 6_565 5_666 ? Na3 Al1 Na3 88.61(16) 2_656 5_666 ? O2 Al2 O2 180.0 . 5_566 ? O2 Al2 O5 95.08(15) . . ? O2 Al2 O5 84.92(15) 5_566 . ? O2 Al2 O5 84.92(15) . 5_566 ? O2 Al2 O5 95.08(15) 5_566 5_566 ? O5 Al2 O5 180.0 . 5_566 ? O2 Al2 O5 95.08(15) . 6_565 ? O2 Al2 O5 84.92(15) 5_566 6_565 ? O5 Al2 O5 89.3(2) . 6_565 ? O5 Al2 O5 90.7(2) 5_566 6_565 ? O2 Al2 O5 84.92(15) . 2_556 ? O2 Al2 O5 95.08(15) 5_566 2_556 ? O5 Al2 O5 90.7(2) . 2_556 ? O5 Al2 O5 89.3(2) 5_566 2_556 ? O5 Al2 O5 180.0 6_565 2_556 ? O2 Al2 Cu2 40.73(8) . . ? O2 Al2 Cu2 139.27(8) 5_566 . ? O5 Al2 Cu2 134.60(10) . . ? O5 Al2 Cu2 45.40(10) 5_566 . ? O5 Al2 Cu2 86.04(11) 6_565 . ? O5 Al2 Cu2 93.96(11) 2_556 . ? O2 Al2 Cu2 139.27(8) . 2_556 ? O2 Al2 Cu2 40.73(8) 5_566 2_556 ? O5 Al2 Cu2 93.96(11) . 2_556 ? O5 Al2 Cu2 86.04(11) 5_566 2_556 ? O5 Al2 Cu2 45.40(10) 6_565 2_556 ? O5 Al2 Cu2 134.60(10) 2_556 2_556 ? Cu2 Al2 Cu2 113.48(3) . 2_556 ? O2 Al2 Cu2 139.27(8) . 5_566 ? O2 Al2 Cu2 40.73(8) 5_566 5_566 ? O5 Al2 Cu2 45.40(10) . 5_566 ? O5 Al2 Cu2 134.60(10) 5_566 5_566 ? O5 Al2 Cu2 93.96(11) 6_565 5_566 ? O5 Al2 Cu2 86.04(11) 2_556 5_566 ? Cu2 Al2 Cu2 180.00(2) . 5_566 ? Cu2 Al2 Cu2 66.52(3) 2_556 5_566 ? O2 Al2 Cu2 40.73(8) . 6_565 ? O2 Al2 Cu2 139.27(8) 5_566 6_565 ? O5 Al2 Cu2 86.04(11) . 6_565 ? O5 Al2 Cu2 93.96(11) 5_566 6_565 ? O5 Al2 Cu2 134.60(10) 6_565 6_565 ? O5 Al2 Cu2 45.40(10) 2_556 6_565 ? Cu2 Al2 Cu2 66.52(3) . 6_565 ? Cu2 Al2 Cu2 180.00(2) 2_556 6_565 ? Cu2 Al2 Cu2 113.48(3) 5_566 6_565 ? O1 Al3 O1 180.0 5_666 . ? O1 Al3 O9 88.09(16) 5_666 5_666 ? O1 Al3 O9 91.91(16) . 5_666 ? O1 Al3 O9 91.91(16) 5_666 6_565 ? O1 Al3 O9 88.09(16) . 6_565 ? O9 Al3 O9 89.3(3) 5_666 6_565 ? O1 Al3 O9 88.09(16) 5_666 2_656 ? O1 Al3 O9 91.91(16) . 2_656 ? O9 Al3 O9 90.7(3) 5_666 2_656 ? O9 Al3 O9 180.0 6_565 2_656 ? O1 Al3 O9 91.91(16) 5_666 . ? O1 Al3 O9 88.09(16) . . ? O9 Al3 O9 180.0 5_666 . ? O9 Al3 O9 90.7(3) 6_565 . ? O9 Al3 O9 89.3(3) 2_656 . ? O1 Al3 Li1 36.5(5) 5_666 6_565 ? O1 Al3 Li1 143.5(5) . 6_565 ? O9 Al3 Li1 52.7(5) 5_666 6_565 ? O9 Al3 Li1 83.2(5) 6_565 6_565 ? O9 Al3 Li1 96.8(5) 2_656 6_565 ? O9 Al3 Li1 127.3(5) . 6_565 ? O1 Al3 Li1 143.5(5) 5_666 2_656 ? O1 Al3 Li1 36.5(5) . 2_656 ? O9 Al3 Li1 127.3(5) 5_666 2_656 ? O9 Al3 Li1 96.8(5) 6_565 2_656 ? O9 Al3 Li1 83.2(5) 2_656 2_656 ? O9 Al3 Li1 52.7(5) . 2_656 ? Li1 Al3 Li1 180.0 6_565 2_656 ? O1 Al3 Li1 143.5(5) 5_666 5_666 ? O1 Al3 Li1 36.5(5) . 5_666 ? O9 Al3 Li1 83.2(5) 5_666 5_666 ? O9 Al3 Li1 52.7(5) 6_565 5_666 ? O9 Al3 Li1 127.3(5) 2_656 5_666 ? O9 Al3 Li1 96.8(5) . 5_666 ? Li1 Al3 Li1 118.8(10) 6_565 5_666 ? Li1 Al3 Li1 61.2(10) 2_656 5_666 ? O1 Al3 Li1 36.5(5) 5_666 . ? O1 Al3 Li1 143.5(5) . . ? O9 Al3 Li1 96.8(5) 5_666 . ? O9 Al3 Li1 127.3(5) 6_565 . ? O9 Al3 Li1 52.7(5) 2_656 . ? O9 Al3 Li1 83.2(5) . . ? Li1 Al3 Li1 61.2(10) 6_565 . ? Li1 Al3 Li1 118.8(10) 2_656 . ? Li1 Al3 Li1 180.0 5_666 . ? O1 Al3 Na3 47.57(9) 5_666 . ? O1 Al3 Na3 132.43(9) . . ? O9 Al3 Na3 107.38(14) 5_666 . ? O9 Al3 Na3 133.70(14) 6_565 . ? O9 Al3 Na3 46.30(14) 2_656 . ? O9 Al3 Na3 72.62(14) . . ? Li1 Al3 Na3 74.7(5) 6_565 . ? Li1 Al3 Na3 105.3(5) 2_656 . ? Li1 Al3 Na3 166.5(5) 5_666 . ? Li1 Al3 Na3 13.5(5) . . ? O1 Al3 Na3 132.43(9) 5_666 2_656 ? O1 Al3 Na3 47.57(9) . 2_656 ? O9 Al3 Na3 133.70(14) 5_666 2_656 ? O9 Al3 Na3 107.38(14) 6_565 2_656 ? O9 Al3 Na3 72.62(14) 2_656 2_656 ? O9 Al3 Na3 46.30(14) . 2_656 ? Li1 Al3 Na3 166.5(5) 6_565 2_656 ? Li1 Al3 Na3 13.5(5) 2_656 2_656 ? Li1 Al3 Na3 74.7(5) 5_666 2_656 ? Li1 Al3 Na3 105.3(5) . 2_656 ? Na3 Al3 Na3 91.86(14) . 2_656 ? O6 Na1 O6 136.6(2) . 2_557 ? O6 Na1 O13 79.75(12) . 6_566 ? O6 Na1 O13 84.04(13) 2_557 6_566 ? O6 Na1 O13 84.04(13) . 5_566 ? O6 Na1 O13 79.75(12) 2_557 5_566 ? O13 Na1 O13 135.2(2) 6_566 5_566 ? O6 Na1 Cl1 122.81(10) . 5_566 ? O6 Na1 Cl1 90.35(10) 2_557 5_566 ? O13 Na1 Cl1 148.63(13) 6_566 5_566 ? O13 Na1 Cl1 73.21(10) 5_566 5_566 ? O6 Na1 Cl1 90.35(10) . 1_556 ? O6 Na1 Cl1 122.81(10) 2_557 1_556 ? O13 Na1 Cl1 73.21(10) 6_566 1_556 ? O13 Na1 Cl1 148.63(13) 5_566 1_556 ? Cl1 Na1 Cl1 84.32(11) 5_566 1_556 ? O6 Na1 Cu2 80.01(9) . 5_566 ? O6 Na1 Cu2 106.19(9) 2_557 5_566 ? O13 Na1 Cu2 158.56(12) 6_566 5_566 ? O13 Na1 Cu2 34.70(8) 5_566 5_566 ? Cl1 Na1 Cu2 51.89(4) 5_566 5_566 ? Cl1 Na1 Cu2 113.93(9) 1_556 5_566 ? O6 Na1 Cu2 106.19(9) . 6_566 ? O6 Na1 Cu2 80.01(9) 2_557 6_566 ? O13 Na1 Cu2 34.70(8) 6_566 6_566 ? O13 Na1 Cu2 158.56(12) 5_566 6_566 ? Cl1 Na1 Cu2 113.93(9) 5_566 6_566 ? Cl1 Na1 Cu2 51.89(4) 1_556 6_566 ? Cu2 Na1 Cu2 163.60(12) 5_566 6_566 ? O6 Na1 Na2 46.66(10) . 2_657 ? O6 Na1 Na2 131.38(12) 2_557 2_657 ? O13 Na1 Na2 47.37(10) 6_566 2_657 ? O13 Na1 Na2 130.63(11) 5_566 2_657 ? Cl1 Na1 Na2 130.65(12) 5_566 2_657 ? Cl1 Na1 Na2 53.09(6) 1_556 2_657 ? Cu2 Na1 Na2 119.23(5) 5_566 2_657 ? Cu2 Na1 Na2 61.41(5) 6_566 2_657 ? O6 Na1 Na2 131.38(12) . 1_455 ? O6 Na1 Na2 46.66(10) 2_557 1_455 ? O13 Na1 Na2 130.63(11) 6_566 1_455 ? O13 Na1 Na2 47.37(10) 5_566 1_455 ? Cl1 Na1 Na2 53.09(6) 5_566 1_455 ? Cl1 Na1 Na2 130.65(12) 1_556 1_455 ? Cu2 Na1 Na2 61.41(5) 5_566 1_455 ? Cu2 Na1 Na2 119.23(5) 6_566 1_455 ? Na2 Na1 Na2 176.07(16) 2_657 1_455 ? O6 Na1 P2 150.14(14) . 2_557 ? O6 Na1 P2 24.01(8) 2_557 2_557 ? O13 Na1 P2 75.91(9) 6_566 2_557 ? O13 Na1 P2 101.28(9) 5_566 2_557 ? Cl1 Na1 P2 86.52(6) 5_566 2_557 ? Cl1 Na1 P2 98.83(6) 1_556 2_557 ? Cu2 Na1 P2 120.65(3) 5_566 2_557 ? Cu2 Na1 P2 60.53(2) 6_566 2_557 ? Na2 Na1 P2 120.05(5) 2_657 2_557 ? Na2 Na1 P2 59.67(5) 1_455 2_557 ? O6 Na1 P2 24.00(8) . . ? O6 Na1 P2 150.14(14) 2_557 . ? O13 Na1 P2 101.28(9) 6_566 . ? O13 Na1 P2 75.91(9) 5_566 . ? Cl1 Na1 P2 98.83(6) 5_566 . ? Cl1 Na1 P2 86.52(6) 1_556 . ? Cu2 Na1 P2 60.53(2) 5_566 . ? Cu2 Na1 P2 120.65(3) 6_566 . ? Na2 Na1 P2 59.67(5) 2_657 . ? Na2 Na1 P2 120.05(5) 1_455 . ? P2 Na1 P2 172.82(12) 2_557 . ? O10 Na2 O6 145.63(18) . 2_657 ? O10 Na2 O13 82.37(15) . 5_666 ? O6 Na2 O13 78.17(13) 2_657 5_666 ? O10 Na2 Cl2 84.84(14) . . ? O6 Na2 Cl2 126.58(15) 2_657 . ? O13 Na2 Cl2 143.84(17) 5_666 . ? O10 Na2 O14 60.57(15) . 3_556 ? O6 Na2 O14 97.06(18) 2_657 3_556 ? O13 Na2 O14 103.87(18) 5_666 3_556 ? Cl2 Na2 O14 98.9(2) . 3_556 ? O10 Na2 Cl1 111.38(13) . 5_666 ? O6 Na2 Cl1 89.25(12) 2_657 5_666 ? O13 Na2 Cl1 72.17(11) 5_666 5_666 ? Cl2 Na2 Cl1 81.43(16) . 5_666 ? O14 Na2 Cl1 171.77(15) 3_556 5_666 ? O10 Na2 Cl2 87.23(14) . 6_565 ? O6 Na2 Cl2 125.31(15) 2_657 6_565 ? O13 Na2 Cl2 140.31(16) 5_666 6_565 ? Cl2 Na2 Cl2 5.1(2) . 6_565 ? O14 Na2 Cl2 103.93(19) 3_556 6_565 ? Cl1 Na2 Cl2 76.38(14) 5_666 6_565 ? O10 Na2 Li1 108.3(4) . 1_556 ? O6 Na2 Li1 88.5(4) 2_657 1_556 ? O13 Na2 Li1 166.6(5) 5_666 1_556 ? Cl2 Na2 Li1 47.9(5) . 1_556 ? O14 Na2 Li1 75.6(5) 3_556 1_556 ? Cl1 Na2 Li1 110.0(5) 5_666 1_556 ? Cl2 Na2 Li1 50.7(5) 6_565 1_556 ? O10 Na2 Na3 105.21(14) . 1_556 ? O6 Na2 Na3 83.38(13) 2_657 1_556 ? O13 Na2 Na3 155.79(16) 5_666 1_556 ? Cl2 Na2 Na3 60.37(13) . 1_556 ? O14 Na2 Na3 62.82(14) 3_556 1_556 ? Cl1 Na2 Na3 123.48(12) 5_666 1_556 ? Cl2 Na2 Na3 63.79(12) 6_565 1_556 ? Li1 Na2 Na3 14.7(5) 1_556 1_556 ? O10 Na2 Na4 53.9(3) . . ? O6 Na2 Na4 132.9(3) 2_657 . ? O13 Na2 Na4 135.4(3) 5_666 . ? Cl2 Na2 Na4 50.1(2) . . ? O14 Na2 Na4 50.3(2) 3_556 . ? Cl1 Na2 Na4 127.6(2) 5_666 . ? Cl2 Na2 Na4 55.0(2) 6_565 . ? Li1 Na2 Na4 54.4(5) 1_556 . ? Na3 Na2 Na4 53.1(3) 1_556 . ? O10 Na2 Na1 127.76(13) . 1_655 ? O6 Na2 Na1 45.86(10) 2_657 1_655 ? O13 Na2 Na1 46.14(10) 5_666 1_655 ? Cl2 Na2 Na1 129.27(17) . 1_655 ? O14 Na2 Na1 129.84(18) 3_556 1_655 ? Cl1 Na2 Na1 52.58(8) 5_666 1_655 ? Cl2 Na2 Na1 124.43(16) 6_565 1_655 ? Li1 Na2 Na1 124.0(4) 1_556 1_655 ? Na3 Na2 Na1 125.28(11) 1_556 1_655 ? Na4 Na2 Na1 178.3(3) . 1_655 ? Li1 Na3 O9 72.4(16) . 2_656 ? Li1 Na3 O7 126.0(16) . . ? O9 Na3 O7 93.9(2) 2_656 . ? Li1 Na3 O1 28.2(15) . 5_666 ? O9 Na3 O1 66.54(19) 2_656 5_666 ? O7 Na3 O1 98.0(2) . 5_666 ? Li1 Na3 O3 66.4(17) . 2_656 ? O9 Na3 O3 132.7(2) 2_656 2_656 ? O7 Na3 O3 92.0(2) . 2_656 ? O1 Na3 O3 66.20(19) 5_666 2_656 ? Li1 Na3 O12 152.9(17) . 3 ? O9 Na3 O12 87.29(19) 2_656 3 ? O7 Na3 O12 71.88(18) . 3 ? O1 Na3 O12 151.6(2) 5_666 3 ? O3 Na3 O12 138.6(2) 2_656 3 ? Li1 Na3 O11 144.6(16) . 3 ? O9 Na3 O11 142.8(2) 2_656 3 ? O7 Na3 O11 68.13(17) . 3 ? O1 Na3 O11 145.2(2) 5_666 3 ? O3 Na3 O11 81.99(17) 2_656 3 ? O12 Na3 O11 56.63(14) 3 3 ? Li1 Na3 Na4 85.5(17) . 1_554 ? O9 Na3 Na4 72.5(5) 2_656 1_554 ? O7 Na3 Na4 140.9(4) . 1_554 ? O1 Na3 Na4 108.8(3) 5_666 1_554 ? O3 Na3 Na4 124.5(5) 2_656 1_554 ? O12 Na3 Na4 71.0(3) 3 1_554 ? O11 Na3 Na4 100.6(4) 3 1_554 ? Li1 Na3 P1 151.3(15) . 3 ? O9 Na3 P1 117.15(18) 2_656 3 ? O7 Na3 P1 81.78(15) . 3 ? O1 Na3 P1 176.3(2) 5_666 3 ? O3 Na3 P1 110.11(17) 2_656 3 ? O12 Na3 P1 31.74(11) 3 3 ? O11 Na3 P1 31.48(10) 3 3 ? Na4 Na3 P1 73.2(3) 1_554 3 ? Li1 Na3 Cl2 39.5(15) . 1_554 ? O9 Na3 Cl2 83.54(18) 2_656 1_554 ? O7 Na3 Cl2 165.3(2) . 1_554 ? O1 Na3 Cl2 67.62(19) 5_666 1_554 ? O3 Na3 Cl2 79.38(16) 2_656 1_554 ? O12 Na3 Cl2 122.3(2) 3 1_554 ? O11 Na3 Cl2 121.65(19) 3 1_554 ? Na4 Na3 Cl2 51.9(3) 1_554 1_554 ? P1 Na3 Cl2 112.31(17) 3 1_554 ? Li1 Na3 P3 96.7(15) . . ? O9 Na3 P3 81.27(15) 2_656 . ? O7 Na3 P3 29.43(11) . . ? O1 Na3 P3 68.63(15) 5_666 . ? O3 Na3 P3 81.44(15) 2_656 . ? O12 Na3 P3 97.75(16) 3 . ? O11 Na3 P3 93.85(15) 3 . ? Na4 Na3 P3 151.7(5) 1_554 . ? P1 Na3 P3 111.20(14) 3 . ? Cl2 Na3 P3 136.19(19) 1_554 . ? Li1 Na3 Na2 80.6(15) . 1_554 ? O9 Na3 Na2 130.6(2) 2_656 1_554 ? O7 Na3 Na2 135.06(19) . 1_554 ? O1 Na3 Na2 104.78(18) 5_666 1_554 ? O3 Na3 Na2 64.03(13) 2_656 1_554 ? O12 Na3 Na2 100.59(16) 3 1_554 ? O11 Na3 Na2 71.13(13) 3 1_554 ? Na4 Na3 Na2 64.7(5) 1_554 1_554 ? P1 Na3 Na2 73.07(10) 3 1_554 ? Cl2 Na3 Na2 50.97(13) 1_554 1_554 ? P3 Na3 Na2 143.56(15) . 1_554 ? Na3 Li1 O1 139(2) . 5_666 ? Na3 Li1 O3 94.0(18) . 2_656 ? O1 Li1 O3 82.5(9) 5_666 2_656 ? Na3 Li1 O9 87.3(17) . 2_656 ? O1 Li1 O9 81.0(9) 5_666 2_656 ? O3 Li1 O9 156.2(11) 2_656 2_656 ? Na3 Li1 Cl2 128.1(19) . 1_554 ? O1 Li1 Cl2 92.9(11) 5_666 1_554 ? O3 Li1 Cl2 97.2(8) 2_656 1_554 ? O9 Li1 Cl2 100.7(9) 2_656 1_554 ? Na3 Li1 Cl2 135.3(19) . 6_564 ? O1 Li1 Cl2 85.7(10) 5_666 6_564 ? O3 Li1 Cl2 96.3(8) 2_656 6_564 ? O9 Li1 Cl2 99.5(9) 2_656 6_564 ? Cl2 Li1 Cl2 7.2(3) 1_554 6_564 ? Na3 Li1 Al1 119(2) . 5_666 ? O1 Li1 Al1 40.5(5) 5_666 5_666 ? O3 Li1 Al1 42.9(4) 2_656 5_666 ? O9 Li1 Al1 116.8(9) 2_656 5_666 ? Cl2 Li1 Al1 103.1(9) 1_554 5_666 ? Cl2 Li1 Al1 97.5(8) 6_564 5_666 ? Na3 Li1 Al3 112.9(18) . . ? O1 Li1 Al3 40.0(5) 5_666 . ? O3 Li1 Al3 117.4(9) 2_656 . ? O9 Li1 Al3 42.0(4) 2_656 . ? Cl2 Li1 Al3 106.1(9) 1_554 . ? Cl2 Li1 Al3 100.3(8) 6_564 . ? Al1 Li1 Al3 75.2(6) 5_666 . ? Na3 Li1 Li1 172.0(15) . 6_565 ? O1 Li1 Li1 33.8(8) 5_666 6_565 ? O3 Li1 Li1 88.0(7) 2_656 6_565 ? O9 Li1 Li1 87.8(7) 2_656 6_565 ? Cl2 Li1 Li1 59.2(6) 1_554 6_565 ? Cl2 Li1 Li1 51.9(5) 6_564 6_565 ? Al1 Li1 Li1 58.4(5) 5_666 6_565 ? Al3 Li1 Li1 59.4(5) . 6_565 ? Na3 Li1 Na4 78.4(16) . 1_554 ? O1 Li1 Na4 133.3(13) 5_666 1_554 ? O3 Li1 Na4 130.7(10) 2_656 1_554 ? O9 Li1 Na4 72.8(8) 2_656 1_554 ? Cl2 Li1 Na4 56.4(6) 1_554 1_554 ? Cl2 Li1 Na4 62.2(6) 6_564 1_554 ? Al1 Li1 Na4 159.4(10) 5_666 1_554 ? Al3 Li1 Na4 110.1(9) . 1_554 ? Li1 Li1 Na4 106.1(6) 6_565 1_554 ? Na3 Li1 Na2 84.7(15) . 1_554 ? O1 Li1 Na2 129.1(11) 5_666 1_554 ? O3 Li1 Na2 66.3(5) 2_656 1_554 ? O9 Li1 Na2 137.4(9) 2_656 1_554 ? Cl2 Li1 Na2 55.1(4) 1_554 1_554 ? Cl2 Li1 Na2 60.6(4) 6_564 1_554 ? Al1 Li1 Na2 103.6(7) 5_666 1_554 ? Al3 Li1 Na2 160.8(10) . 1_554 ? Li1 Li1 Na2 103.2(5) 6_565 1_554 ? Na4 Li1 Na2 64.6(7) 1_554 1_554 ? Na3 Li1 Na4 81.5(16) . 2_656 ? O1 Li1 Na4 132.3(12) 5_666 2_656 ? O3 Li1 Na4 127.3(9) 2_656 2_656 ? O9 Li1 Na4 76.5(7) 2_656 2_656 ? Cl2 Li1 Na4 52.0(5) 1_554 2_656 ? Cl2 Li1 Na4 58.0(5) 6_564 2_656 ? Al1 Li1 Na4 154.8(9) 5_666 2_656 ? Al3 Li1 Na4 112.4(8) . 2_656 ? Li1 Li1 Na4 103.4(5) 6_565 2_656 ? Na4 Li1 Na4 4.8(7) 1_554 2_656 ? Na2 Li1 Na4 61.0(6) 1_554 2_656 ? Na4 Na4 O10 115(5) 2_657 2_657 ? Na4 Na4 O15 111.2(18) 2_657 5_667 ? O10 Na4 O15 76.4(8) 2_657 5_667 ? Na4 Na4 Cl2 103(3) 2_657 . ? O10 Na4 Cl2 125.2(6) 2_657 . ? O15 Na4 Cl2 52.7(5) 5_667 . ? Na4 Na4 O14 99(3) 2_657 3_556 ? O10 Na4 O14 108.1(5) 2_657 3_556 ? O15 Na4 O14 144.3(9) 5_667 3_556 ? Cl2 Na4 O14 103.7(9) . 3_556 ? Na4 Na4 O10 53(4) 2_657 . ? O10 Na4 O10 153.6(6) 2_657 . ? O15 Na4 O10 128.6(8) 5_667 . ? Cl2 Na4 O10 81.1(7) . . ? O14 Na4 O10 58.2(5) 3_556 . ? Na4 Na4 O14 68(3) 2_657 4_556 ? O10 Na4 O14 59.6(5) 2_657 4_556 ? O15 Na4 O14 126.6(12) 5_667 4_556 ? Cl2 Na4 O14 169.9(6) . 4_556 ? O14 Na4 O14 81.6(4) 3_556 4_556 ? O10 Na4 O14 94.7(4) . 4_556 ? Na4 Na4 Cl2 65(3) 2_657 2_657 ? O10 Na4 Cl2 83.0(8) 2_657 2_657 ? O15 Na4 Cl2 49.1(6) 5_667 2_657 ? Cl2 Na4 Cl2 78.3(4) . 2_657 ? O14 Na4 Cl2 163.4(7) 3_556 2_657 ? O10 Na4 Cl2 106.5(5) . 2_657 ? O14 Na4 Cl2 94.2(7) 4_556 2_657 ? Na4 Na4 O15 56.9(16) 2_657 . ? O10 Na4 O15 130.0(9) 2_657 . ? O15 Na4 O15 65.8(8) 5_667 . ? Cl2 Na4 O15 48.2(5) . . ? O14 Na4 O15 121.8(10) 3_556 . ? O10 Na4 O15 66.7(6) . . ? O14 Na4 O15 121.7(7) 4_556 . ? Cl2 Na4 O15 47.7(5) 2_657 . ? Na4 Na4 Cl2 101(3) 2_657 6_565 ? O10 Na4 Cl2 122.8(6) 2_657 6_565 ? O15 Na4 Cl2 48.9(5) 5_667 6_565 ? Cl2 Na4 Cl2 4.6(2) . 6_565 ? O14 Na4 Cl2 108.3(9) 3_556 6_565 ? O10 Na4 Cl2 83.6(6) . 6_565 ? O14 Na4 Cl2 166.7(7) 4_556 6_565 ? Cl2 Na4 Cl2 73.8(3) 2_657 6_565 ? O15 Na4 Cl2 45.7(5) . 6_565 ? Na4 Na4 Na3 159(5) 2_657 1_556 ? O10 Na4 Na3 85.9(5) 2_657 1_556 ? O15 Na4 Na3 76.8(6) 5_667 1_556 ? Cl2 Na4 Na3 65.9(4) . 1_556 ? O14 Na4 Na3 68.5(5) 3_556 1_556 ? O10 Na4 Na3 106.5(9) . 1_556 ? O14 Na4 Na3 124.2(5) 4_556 1_556 ? Cl2 Na4 Na3 125.8(5) 2_657 1_556 ? O15 Na4 Na3 114.1(7) . 1_556 ? Cl2 Na4 Na3 68.7(4) 6_565 1_556 ? Na4 Na4 Li1 152(4) 2_657 1_556 ? O10 Na4 Li1 91.2(6) 2_657 1_556 ? O15 Na4 Li1 63.4(8) 5_667 1_556 ? Cl2 Na4 Li1 51.3(6) . 1_556 ? O14 Na4 Li1 81.0(8) 3_556 1_556 ? O10 Na4 Li1 107.1(10) . 1_556 ? O14 Na4 Li1 138.7(7) 4_556 1_556 ? Cl2 Na4 Li1 111.7(6) 2_657 1_556 ? O15 Na4 Li1 99.2(8) . 1_556 ? Cl2 Na4 Li1 53.6(6) 6_565 1_556 ? Na3 Na4 Li1 16.0(5) 1_556 1_556 ? Cl2 Cl2 Li1 120.8(6) 6_565 1_556 ? Cl2 Cl2 Na4 142.9(5) 6_565 . ? Li1 Cl2 Na4 72.3(7) 1_556 . ? Cl2 Cl2 Li1 51.9(5) 6_565 6_566 ? Li1 Cl2 Li1 68.9(11) 1_556 6_566 ? Na4 Cl2 Li1 126.1(6) . 6_566 ? Cl2 Cl2 Na2 137.26(14) 6_565 . ? Li1 Cl2 Na2 77.0(6) 1_556 . ? Na4 Cl2 Na2 77.3(6) . . ? Li1 Cl2 Na2 126.3(5) 6_566 . ? Cl2 Cl2 Na4 137.6(4) 6_565 2_657 ? Li1 Cl2 Na4 84.9(7) 1_556 2_657 ? Na4 Cl2 Na4 12.8(6) . 2_657 ? Li1 Cl2 Na4 136.1(7) 6_566 2_657 ? Na2 Cl2 Na4 77.4(5) . 2_657 ? Cl2 Cl2 Na4 32.5(5) 6_565 6_565 ? Li1 Cl2 Na4 121.7(7) 1_556 6_565 ? Na4 Cl2 Na4 110.4(10) . 6_565 ? Li1 Cl2 Na4 64.3(6) 6_566 6_565 ? Na2 Cl2 Na4 160.9(4) . 6_565 ? Na4 Cl2 Na4 106.2(3) 2_657 6_565 ? Cl2 Cl2 Na2 37.66(12) 6_565 6_565 ? Li1 Cl2 Na2 122.8(6) 1_556 6_565 ? Na4 Cl2 Na2 163.8(4) . 6_565 ? Li1 Cl2 Na2 68.7(5) 6_566 6_565 ? Na2 Cl2 Na2 99.60(15) . 6_565 ? Na4 Cl2 Na2 151.1(3) 2_657 6_565 ? Na4 Cl2 Na2 68.0(5) 6_565 6_565 ? Cl2 Cl2 Na3 133.22(14) 6_565 1_556 ? Li1 Cl2 Na3 12.4(6) 1_556 1_556 ? Na4 Cl2 Na3 62.2(4) . 1_556 ? Li1 Cl2 Na3 81.3(5) 6_566 1_556 ? Na2 Cl2 Na3 68.66(19) . 1_556 ? Na4 Cl2 Na3 74.4(3) 2_657 1_556 ? Na4 Cl2 Na3 130.5(4) 6_565 1_556 ? Na2 Cl2 Na3 131.85(16) 6_565 1_556 ? Cl2 Cl2 Na4 37.6(4) 6_565 5_667 ? Li1 Cl2 Na4 131.9(7) 1_556 5_667 ? Na4 Cl2 Na4 106.5(3) . 5_667 ? Li1 Cl2 Na4 75.6(6) 6_566 5_667 ? Na2 Cl2 Na4 151.0(4) . 5_667 ? Na4 Cl2 Na4 100.0(7) 2_657 5_667 ? Na4 Cl2 Na4 11.6(5) 6_565 5_667 ? Na2 Cl2 Na4 68.6(5) 6_565 5_667 ? Na3 Cl2 Na4 139.2(4) 1_556 5_667 ? Cl2 Cl2 Na3 41.84(12) 6_565 6_566 ? Li1 Cl2 Na3 79.0(6) 1_556 6_566 ? Na4 Cl2 Na3 131.9(5) . 6_566 ? Li1 Cl2 Na3 10.1(5) 6_566 6_566 ? Na2 Cl2 Na3 132.41(16) . 6_566 ? Na4 Cl2 Na3 140.0(5) 2_657 6_566 ? Na4 Cl2 Na3 55.7(3) 6_565 6_566 ? Na2 Cl2 Na3 61.62(16) 6_565 6_566 ? Na3 Cl2 Na3 91.38(16) 1_556 6_566 ? Na4 Cl2 Na3 66.7(3) 5_667 6_566 ? Na4 O15 Na4 123.1(11) 2_657 5_667 ? Na4 O15 Na4 11.9(6) 2_657 . ? Na4 O15 Na4 114.2(8) 5_667 . ? Na4 O15 Na4 114.2(8) 2_657 6_565 ? Na4 O15 Na4 11.9(6) 5_667 6_565 ? Na4 O15 Na4 104.3(9) . 6_565 ? Cu2 Cl1 Cu2 72.04(5) 6_565 . ? Cu2 Cl1 Na1 126.68(7) 6_565 5_566 ? Cu2 Cl1 Na1 74.08(4) . 5_566 ? Cu2 Cl1 Na1 74.08(4) 6_565 1_554 ? Cu2 Cl1 Na1 126.68(7) . 1_554 ? Na1 Cl1 Na1 95.68(11) 5_566 1_554 ? Cu2 Cl1 Na2 76.53(6) 6_565 2_656 ? Cu2 Cl1 Na2 132.96(9) . 2_656 ? Na1 Cl1 Na2 151.96(9) 5_566 2_656 ? Na1 Cl1 Na2 74.33(7) 1_554 2_656 ? Cu2 Cl1 Na2 132.96(9) 6_565 5_666 ? Cu2 Cl1 Na2 76.53(6) . 5_666 ? Na1 Cl1 Na2 74.33(7) 5_566 5_666 ? Na1 Cl1 Na2 151.96(9) 1_554 5_666 ? Na2 Cl1 Na2 102.08(13) 2_656 5_666 ? Li1 O1 Li1 112.4(16) 2_656 5_666 ? Li1 O1 Al1 101.4(8) 2_656 . ? Li1 O1 Al1 101.4(8) 5_666 . ? Li1 O1 Al3 103.4(8) 2_656 . ? Li1 O1 Al3 103.4(8) 5_666 . ? Al1 O1 Al3 134.5(3) . . ? Li1 O1 Na3 13.0(8) 2_656 2_656 ? Li1 O1 Na3 125.3(9) 5_666 2_656 ? Al1 O1 Na3 98.37(17) . 2_656 ? Al3 O1 Na3 97.48(17) . 2_656 ? Li1 O1 Na3 125.3(9) 2_656 5_666 ? Li1 O1 Na3 13.0(8) 5_666 5_666 ? Al1 O1 Na3 98.37(17) . 5_666 ? Al3 O1 Na3 97.48(17) . 5_666 ? Na3 O1 Na3 138.2(3) 2_656 5_666 ? Al2 O2 Al1 132.8(3) . . ? Al2 O2 Cu2 102.01(19) . . ? Al1 O2 Cu2 104.31(19) . . ? Al2 O2 Cu2 102.01(19) . 6_565 ? Al1 O2 Cu2 104.30(19) . 6_565 ? Cu2 O2 Cu2 110.6(2) . 6_565 ? P2 O3 Al1 130.4(2) . . ? P2 O3 Li1 140.6(7) . 2_656 ? Al1 O3 Li1 82.9(6) . 2_656 ? P2 O3 Na3 122.1(2) . 2_656 ? Al1 O3 Na3 95.35(18) . 2_656 ? Li1 O3 Na3 19.6(6) 2_656 2_656 ? P3 O4 Al1 129.4(2) . 5_666 ? P3 O4 Cu2 133.5(2) . 5_666 ? Al1 O4 Cu2 94.93(16) 5_666 5_666 ? P2 O5 Al2 126.1(2) . . ? P2 O5 Cu2 136.9(2) . 5_566 ? Al2 O5 Cu2 91.92(15) . 5_566 ? P2 O6 Cu4 117.6(2) . 8_465 ? P2 O6 Na1 116.7(2) . . ? Cu4 O6 Na1 112.85(17) 8_465 . ? P2 O6 Na2 112.8(2) . 2_657 ? Cu4 O6 Na2 104.64(17) 8_465 2_657 ? Na1 O6 Na2 87.48(13) . 2_657 ? P3 O7 Cu1 126.6(3) . 3 ? P3 O7 Cu3 125.1(3) . 3 ? Cu1 O7 Cu3 100.69(16) 3 3 ? P3 O7 Na3 101.0(2) . . ? Cu1 O7 Na3 100.90(18) 3 . ? Cu3 O7 Na3 94.67(18) 3 . ? P2 O8 Cu3 124.6(2) . 5_566 ? P2 O8 Cu1 122.8(2) . 4_556 ? Cu3 O8 Cu1 95.23(15) 5_566 4_556 ? P3 O9 Al3 135.1(2) . . ? P3 O9 Li1 137.1(7) . 2_656 ? Al3 O9 Li1 85.3(6) . 2_656 ? P3 O9 Na3 119.4(2) . 2_656 ? Al3 O9 Na3 98.23(19) . 2_656 ? Li1 O9 Na3 20.3(6) 2_656 2_656 ? P3 O10 Cu4 114.4(2) . . ? P3 O10 Na4 115.9(4) . 2_657 ? Cu4 O10 Na4 96.7(3) . 2_657 ? P3 O10 Na2 127.9(2) . . ? Cu4 O10 Na2 104.20(17) . . ? Na4 O10 Na2 91.5(5) 2_657 . ? P3 O10 Na4 127.0(4) . . ? Cu4 O10 Na4 95.2(3) . . ? Na4 O10 Na4 12.3(9) 2_657 . ? Na2 O10 Na4 80.0(4) . . ? P1 O11 Cu1 130.6(2) . . ? P1 O11 Cu4 118.4(2) . 5_666 ? Cu1 O11 Cu4 105.08(18) . 5_666 ? P1 O11 Na3 80.98(19) . 3_445 ? Cu1 O11 Na3 93.75(17) . 3_445 ? Cu4 O11 Na3 124.32(18) 5_666 3_445 ? P1 O12 Cu3 129.9(3) . . ? P1 O12 Cu4 121.4(2) . 4_546 ? Cu3 O12 Cu4 103.15(19) . 4_546 ? P1 O12 Na3 85.3(2) . 3_445 ? Cu3 O12 Na3 93.02(18) . 3_445 ? Cu4 O12 Na3 118.6(2) 4_546 3_445 ? P1 O13 Cu2 128.1(2) . . ? P1 O13 Na1 118.7(2) . 5_566 ? Cu2 O13 Na1 98.49(17) . 5_566 ? P1 O13 Na2 115.0(2) . 5_666 ? Cu2 O13 Na2 101.15(17) . 5_666 ? Na1 O13 Na2 86.49(13) 5_566 5_666 ? P1 O14 Cu4 139.9(3) . 3_444 ? P1 O14 Na4 113.7(5) . 3_444 ? Cu4 O14 Na4 95.7(4) 3_444 3_444 ? P1 O14 Na2 119.7(3) . 3_444 ? Cu4 O14 Na2 92.12(19) 3_444 3_444 ? Na4 O14 Na2 77.0(5) 3_444 3_444 ? P1 O14 Na4 125.0(5) . 4_546 ? Cu4 O14 Na4 82.7(4) 3_444 4_546 ? Na4 O14 Na4 13.1(6) 3_444 4_546 ? Na2 O14 Na4 77.7(5) 3_444 4_546 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O11 1.957(4) 7_556 ? Cu1 O11 1.958(4) . ? Cu1 O7 2.118(4) 5_666 ? Cu1 O7 2.118(4) 3_445 ? Cu1 O8 2.308(4) 6_565 ? Cu1 O8 2.308(4) 4_546 ? Cu1 Na3 3.471(4) 3_445 ? Cu1 Na3 3.471(4) 5_666 ? Cu2 O13 1.886(3) . ? Cu2 O2 1.918(3) . ? Cu2 O4 2.027(4) 5_666 ? Cu2 O5 2.048(4) 5_566 ? Cu2 Cl1 2.6815(15) . ? Cu2 Al2 2.8752(6) . ? Cu2 Al1 2.951(2) . ? Cu2 Na1 3.2770(8) 5_566 ? Cu2 Na2 3.381(3) 5_666 ? Cu3 O12 2.002(5) 2_556 ? Cu3 O12 2.002(5) . ? Cu3 O8 2.208(4) 6_565 ? Cu3 O8 2.208(4) 5_566 ? Cu3 O7 2.214(5) 4_546 ? Cu3 O7 2.214(4) 3_445 ? Cu3 Na3 3.379(4) 3_445 ? Cu3 Na3 3.379(4) 4_546 ? Cu4 O10 1.891(4) . ? Cu4 O6 1.896(3) 8_565 ? Cu4 O14 1.999(4) 3_556 ? Cu4 O12 2.301(4) 4_556 ? Cu4 O11 2.302(4) 5_666 ? Cu4 Na4 3.198(18) 2_657 ? Cu4 Na2 3.401(3) . ? Cu4 Na4 3.427(18) . ? Cu4 Na2 3.443(3) 7_667 ? Cu4 Na1 3.592(3) 7_567 ? P1 O14 1.500(4) . ? P1 O13 1.541(4) . ? P1 O12 1.546(4) . ? P1 O11 1.549(4) . ? P1 Na3 2.930(4) 3_445 ? P1 Na2 3.415(3) 5_666 ? P1 Na1 3.433(3) 5_566 ? P2 O8 1.524(4) . ? P2 O3 1.533(4) . ? P2 O6 1.542(3) . ? P2 O5 1.559(4) . ? P2 Na2 3.349(3) 2_657 ? P2 Na1 3.3877(12) . ? P3 O9 1.513(4) . ? P3 O10 1.531(4) . ? P3 O7 1.535(4) . ? P3 O4 1.543(4) . ? P3 Na3 3.067(4) . ? P3 Na4 3.33(2) 2_657 ? P3 Na3 3.368(4) 2_656 ? Al1 O1 1.812(6) . ? Al1 O2 1.818(6) . ? Al1 O3 1.878(4) 6_565 ? Al1 O3 1.878(4) . ? Al1 O4 1.978(4) 5_666 ? Al1 O4 1.978(4) 2_656 ? Al1 Li1 2.74(2) 2_656 ? Al1 Li1 2.74(2) 5_666 ? Al1 Na3 3.213(4) 2_656 ? Al1 Na3 3.213(4) 5_666 ? Al2 O2 1.780(5) . ? Al2 O2 1.780(5) 5_566 ? Al2 O5 1.950(4) . ? Al2 O5 1.950(4) 5_566 ? Al2 O5 1.950(4) 6_565 ? Al2 O5 1.950(4) 2_556 ? Al3 O1 1.864(5) 5_666 ? Al3 O1 1.864(5) . ? Al3 O9 1.891(4) 5_666 ? Al3 O9 1.891(4) 6_565 ? Al3 O9 1.891(4) 2_656 ? Al3 O9 1.891(4) . ? Al3 Li1 2.82(2) 6_565 ? Al3 Li1 2.82(2) 2_656 ? Al3 Li1 2.82(2) 5_666 ? Al3 Li1 2.82(2) . ? Al3 Na3 3.226(4) . ? Al3 Na3 3.226(4) 2_656 ? Na1 O6 2.402(4) . ? Na1 O6 2.402(4) 2_557 ? Na1 O13 2.416(4) 6_566 ? Na1 O13 2.416(4) 5_566 ? Na1 Cl1 2.758(3) 5_566 ? Na1 Cl1 2.758(3) 1_556 ? Na1 Na2 3.344(2) 2_657 ? Na1 Na2 3.344(2) 1_455 ? Na2 O10 2.400(4) . ? Na2 O6 2.434(4) 2_657 ? Na2 O13 2.464(4) 5_666 ? Na2 Cl2 2.676(7) . ? Na2 O14 2.678(6) 3_556 ? Na2 Cl1 2.777(3) 5_666 ? Na2 Cl2 2.972(7) 6_565 ? Na2 Li1 3.18(2) 1_556 ? Na2 Na3 3.208(5) 1_556 ? Na2 Na4 3.28(3) . ? Na3 Li1 0.82(3) . ? Na3 O9 2.357(6) 2_656 ? Na3 O7 2.378(6) . ? Na3 O1 2.402(4) 5_666 ? Na3 O3 2.437(6) 2_656 ? Na3 O12 2.618(6) 3 ? Na3 O11 2.741(6) 3 ? Na3 Na4 2.902(18) 1_554 ? Na3 Cl2 2.994(7) 1_554 ? Li1 O1 1.72(2) 5_666 ? Li1 O3 2.24(2) 2_656 ? Li1 O9 2.25(2) 2_656 ? Li1 Cl2 2.42(2) 1_554 ? Li1 Cl2 2.64(2) 6_564 ? Li1 Li1 2.87(5) 6_565 ? Li1 Na4 2.95(3) 1_554 ? Li1 Na4 3.53(3) 2_656 ? Na4 Na4 0.63(3) 2_657 ? Na4 O10 2.37(2) 2_657 ? Na4 O15 2.561(17) 5_667 ? Na4 Cl2 2.581(18) . ? Na4 O14 2.59(2) 3_556 ? Na4 O10 2.69(2) . ? Na4 O14 2.764(19) 4_556 ? Na4 Cl2 2.788(19) 2_657 ? Na4 O15 2.851(18) . ? Na4 Cl2 2.899(17) 6_565 ? Cl2 Cl2 0.387(16) 6_565 ? _cod_database_fobs_code 2109099