Crystallography Open Database

Information card for entry 2200052

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Coordinates	2200052.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	[(1RS,4RS)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca- 7,12-diene-N^1^,N^4^,N^8^,N^12^]nickel(II) diperchlorate
Formula	C17 H34 Cl2 N4 Ni O8
Calculated formula	C17 H34 Cl2 N4 Ni O8
Title of publication	[(1<i>RS</i>,4<i>RS</i>)-5,5,7,13,15,15-Hexamethyl-1,4,8,12-tetraazacyclopentadeca-7,12-diene-<i>N</i>^1^,<i>N</i>^4^,<i>N</i>^8^,<i>N</i>^12^]nickel(II) diperchlorate
Authors of publication	Curtis, Neil F.; Waters, Joyce M.; Rickard, Clifton E.
Journal of publication	Acta Crystallographica Section E
Year of publication	2001
Journal volume	57
Journal issue	1
Pages of publication	m48 - m50
a	10.3529 ± 0.0001 Å
b	16.1128 ± 0.0001 Å
c	15.04 ± 0.0001 Å
α	90°
β	107.025 ± 0.001°
γ	90°
Cell volume	2398.94 ± 0.03 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.051
Residual factor for significantly intense reflections	0.042
Weighted residual factors for all reflections	0.112
Weighted residual factors for all reflections included in the refinement	0.105
Goodness-of-fit parameter for all reflections	1.044
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

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