#------------------------------------------------------------------------------ #$Date: 2011-09-16 16:46:08 +0100 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: svn://www.crystallography.net/cod/hkl/2/2200338.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200338_Fobs loop_ _publ_author_name 'Fronczek, Frank R.' 'Johnson, Rolanda J.' 'Strongin, Robert M.' _publ_section_title ; Trimethylsulfonium methanesulfonate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o447 _journal_page_last o448 _journal_volume 57 _journal_year 2001 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.6157 _cell_length_b 8.2419 _cell_length_c 7.5397 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.7097 _[local]_cod_data_source_file om6021Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rjohnson1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 234.36 186.55 11.09 o 4 0 0 44.12 50.91 5.78 o 6 0 0 2570.14 2447.59 71.53 o 8 0 0 1836.84 1795.59 61.09 o 10 0 0 25.06 -2.94 8.81 o 12 0 0 438.49 517.75 32.72 o 14 0 0 136.29 161.35 20.66 o 16 0 0 49.79 32.40 27.41 o 2 1 0 3905.34 3899.65 79.46 o 4 1 0 1506.12 1415.47 28.40 o 6 1 0 73.66 78.43 4.99 o 8 1 0 0.02 2.94 4.01 o 10 1 0 5883.87 6162.21 138.41 o 12 1 0 120.36 125.52 10.48 o 14 1 0 91.52 97.80 13.02 o 16 1 0 315.84 288.70 37.21 o 0 2 0 18392.92 18471.24 1135.08 o 2 2 0 76.45 99.69 4.99 o 4 2 0 81.57 81.17 3.92 o 6 2 0 1292.95 1167.83 25.75 o 8 2 0 31.12 24.47 5.87 o 10 2 0 39.08 41.90 5.68 o 12 2 0 341.91 344.38 15.08 o 14 2 0 94.70 99.66 14.39 o 16 2 0 35.35 -12.73 25.45 o 2 3 0 1024.17 1104.69 22.91 o 4 3 0 520.57 505.53 12.65 o 6 3 0 1072.15 1086.65 22.68 o 8 3 0 10.53 2.94 4.99 o 10 3 0 1761.24 1819.64 69.55 o 12 3 0 137.25 122.68 9.69 o 14 3 0 15.21 10.77 16.64 o 16 3 0 177.42 148.14 24.38 o 0 4 0 4680.39 4497.36 152.34 o 2 4 0 852.12 860.03 18.36 o 4 4 0 159.36 176.86 7.54 o 6 4 0 610.30 567.74 14.90 o 8 4 0 189.50 174.40 7.44 o 10 4 0 6.59 3.92 4.89 o 12 4 0 203.68 169.50 13.02 o 14 4 0 40.65 11.84 13.80 o 16 4 0 50.49 34.26 22.32 o 2 5 0 540.86 502.60 14.02 o 4 5 0 325.09 311.63 11.07 o 6 5 0 6.37 8.81 3.92 o 8 5 0 0.49 -4.89 4.89 o 10 5 0 2407.98 2557.89 104.70 o 12 5 0 166.58 142.17 13.41 o 14 5 0 25.10 5.78 14.59 o 16 5 0 175.59 286.58 72.06 o 0 6 0 10081.39 10542.60 312.06 o 2 6 0 74.37 77.34 6.56 o 4 6 0 14.25 10.77 5.97 o 6 6 0 693.03 716.55 21.76 o 8 6 0 428.72 450.33 18.61 o 10 6 0 1.03 5.78 6.75 o 12 6 0 162.23 157.44 20.46 o 14 6 0 48.83 37.98 18.50 o 2 7 0 757.38 740.37 25.59 o 4 7 0 741.67 730.11 35.49 o 6 7 0 21.92 13.61 6.95 o 8 7 0 9.61 5.78 5.87 o 10 7 0 1869.41 2087.06 108.78 o 12 7 0 14.83 32.40 14.58 o 14 7 0 24.81 54.03 54.72 o 0 8 0 2498.90 2644.94 109.65 o 2 8 0 3.63 7.73 6.75 o 4 8 0 15.68 22.61 8.91 o 6 8 0 630.44 709.63 33.32 o 8 8 0 7.86 6.95 10.87 o 10 8 0 30.63 7.73 45.81 o 12 8 0 109.81 113.86 34.07 o 2 9 0 0.84 4.89 10.87 o 4 9 0 323.92 359.62 29.67 o 6 9 0 96.28 84.00 18.40 o 8 9 0 2.34 15.56 12.63 o 10 9 0 416.15 542.11 71.40 o 0 10 0 532.29 510.69 65.05 o 2 10 0 9.42 33.18 14.78 o 4 10 0 7.93 22.61 17.52 o 6 10 0 133.05 126.20 21.83 o 8 10 0 14.21 16.54 34.06 o 2 11 0 30.57 11.84 19.58 o 4 11 0 17.24 -3.92 22.42 o 1 0 1 211.54 228.89 6.67 o 2 0 1 6670.18 6833.10 148.62 o 3 0 1 732.03 763.26 17.31 o 4 0 1 3995.49 3811.07 70.17 o 5 0 1 4202.02 4249.74 90.50 o 6 0 1 378.13 367.06 10.78 o 7 0 1 17.80 26.33 4.80 o 8 0 1 1806.05 1745.10 39.34 o 9 0 1 0.04 -0.98 4.99 o 10 0 1 170.84 179.39 9.20 o 11 0 1 55.14 63.63 8.03 o 12 0 1 1640.64 1626.35 58.13 o 13 0 1 7.91 11.84 8.81 o 14 0 1 467.91 504.98 28.11 o 15 0 1 38.24 17.62 17.62 o 16 0 1 0.16 41.11 21.63 o 17 0 1 0.05 37.98 21.63 o 0 1 1 596.70 673.20 12.99 o 1 1 1 113.18 120.71 3.42 o 2 1 1 11387.71 11061.95 149.06 o 3 1 1 8.16 14.70 1.86 o 4 1 1 1386.25 1301.66 19.20 o 5 1 1 1676.91 1725.79 26.44 o 6 1 1 140.81 127.60 4.20 o 7 1 1 35.51 36.63 3.42 o 8 1 1 2528.34 2522.15 44.67 o 9 1 1 98.76 101.83 15.52 o 10 1 1 31.84 28.65 4.22 o 11 1 1 6.57 8.33 7.29 o 12 1 1 546.51 550.28 16.00 o 13 1 1 0.13 1.13 7.27 o 14 1 1 71.99 53.78 8.55 o 15 1 1 165.27 154.27 14.15 o 16 1 1 1.30 7.97 13.83 o 17 1 1 5.25 8.63 15.18 o 1 2 1 2.07 12.41 4.40 o 2 2 1 6821.20 6667.46 97.37 o 3 2 1 246.10 269.60 7.20 o 4 2 1 721.04 794.26 15.26 o 5 2 1 748.88 781.57 12.54 o 6 2 1 552.17 560.44 23.48 o 7 2 1 55.78 60.27 3.65 o 8 2 1 1508.58 1443.14 25.12 o 9 2 1 34.38 24.01 8.27 o 10 2 1 84.79 83.49 7.24 o 11 2 1 4.51 6.24 4.90 o 12 2 1 355.02 367.97 24.73 o 13 2 1 12.82 15.99 11.31 o 14 2 1 254.74 252.46 28.01 o 15 2 1 34.47 26.69 10.67 o 16 2 1 0.12 -6.93 13.91 o 17 2 1 3.04 -20.12 21.14 o 0 3 1 725.24 683.07 17.97 o 1 3 1 835.05 939.32 15.58 o 2 3 1 426.62 370.27 7.54 o 3 3 1 83.90 91.53 8.76 o 4 3 1 1267.46 1260.93 17.34 o 5 3 1 114.10 118.77 4.11 o 6 3 1 747.27 753.40 12.70 o 7 3 1 359.21 354.78 22.00 o 8 3 1 1828.88 1767.76 36.62 o 9 3 1 12.01 15.13 4.40 o 10 3 1 573.21 575.16 13.16 o 11 3 1 29.16 30.51 5.82 o 12 3 1 318.82 308.63 31.34 o 13 3 1 28.40 28.66 6.79 o 14 3 1 9.91 10.59 12.03 o 15 3 1 37.35 19.09 10.01 o 16 3 1 14.14 14.48 13.41 o 17 3 1 19.93 3.61 19.80 o 1 4 1 9.58 11.20 4.40 o 2 4 1 2042.35 2045.72 33.10 o 3 4 1 487.54 499.15 8.74 o 4 4 1 621.14 671.22 12.45 o 5 4 1 101.79 93.44 4.31 o 6 4 1 169.35 176.25 8.27 o 7 4 1 75.93 77.51 3.51 o 8 4 1 854.92 846.05 17.09 o 9 4 1 44.77 41.54 4.45 o 10 4 1 32.26 24.11 6.36 o 11 4 1 22.56 18.22 3.56 o 12 4 1 171.30 206.65 17.97 o 13 4 1 27.17 18.28 11.75 o 14 4 1 211.52 203.17 20.42 o 15 4 1 27.21 11.78 11.02 o 16 4 1 0.25 6.07 20.81 o 0 5 1 46.95 51.79 5.87 o 1 5 1 12.42 19.84 4.01 o 2 5 1 2090.67 2140.03 38.83 o 3 5 1 1.90 -0.58 3.33 o 4 5 1 685.28 649.70 12.26 o 5 5 1 204.40 209.86 6.07 o 6 5 1 24.69 31.43 3.05 o 7 5 1 36.95 33.43 3.43 o 8 5 1 834.53 786.83 21.86 o 9 5 1 5.75 11.11 7.29 o 10 5 1 43.64 35.83 11.21 o 11 5 1 7.27 10.00 6.59 o 12 5 1 310.39 312.24 19.05 o 13 5 1 4.20 -8.89 8.89 o 14 5 1 25.43 47.04 13.66 o 15 5 1 56.07 31.88 13.54 o 1 6 1 49.38 41.36 5.38 o 2 6 1 1056.18 1044.04 21.47 o 3 6 1 27.90 27.25 4.21 o 4 6 1 517.19 485.20 11.57 o 5 6 1 533.05 524.76 22.83 o 6 6 1 112.36 118.71 6.03 o 7 6 1 13.71 16.73 3.03 o 8 6 1 676.52 752.06 17.31 o 9 6 1 0.01 12.41 6.36 o 10 6 1 31.12 17.48 6.92 o 11 6 1 13.86 11.04 8.61 o 12 6 1 674.91 727.29 48.26 o 13 6 1 0.40 -12.96 12.96 o 14 6 1 220.86 243.41 22.01 o 15 6 1 16.80 10.20 26.97 o 0 7 1 205.36 200.94 9.79 o 1 7 1 55.02 43.76 4.67 o 2 7 1 1599.78 1606.41 38.89 o 3 7 1 15.29 22.65 5.41 o 4 7 1 377.48 365.15 12.62 o 5 7 1 224.89 214.11 21.15 o 6 7 1 121.21 112.25 7.27 o 7 7 1 13.47 12.21 5.10 o 8 7 1 731.77 729.99 20.69 o 9 7 1 43.54 41.46 8.58 o 10 7 1 6.87 15.80 9.15 o 11 7 1 2.24 -1.91 11.06 o 12 7 1 199.47 190.30 21.86 o 13 7 1 0.35 -1.62 13.21 o 14 7 1 44.98 23.85 39.60 o 1 8 1 22.83 15.36 4.85 o 2 8 1 871.71 874.78 28.14 o 3 8 1 0.56 -5.36 5.36 o 4 8 1 6.83 5.64 5.85 o 5 8 1 189.80 169.73 9.76 o 6 8 1 154.26 156.72 16.79 o 7 8 1 2.78 5.05 8.39 o 8 8 1 387.64 386.49 31.24 o 9 8 1 0.05 -7.45 8.66 o 10 8 1 73.72 51.67 14.22 o 11 8 1 2.73 -0.75 18.06 o 12 8 1 118.41 100.78 31.62 o 0 9 1 149.98 128.26 16.35 o 1 9 1 9.15 12.68 8.31 o 2 9 1 172.78 163.55 24.48 o 3 9 1 1.55 5.28 10.23 o 4 9 1 143.97 157.85 17.28 o 5 9 1 42.32 70.74 11.84 o 6 9 1 10.57 15.66 8.24 o 7 9 1 9.11 -6.90 9.07 o 8 9 1 422.81 465.34 39.23 o 9 9 1 0.48 -13.05 13.05 o 10 9 1 91.09 93.82 21.38 o 11 9 1 4.43 8.07 19.64 o 1 10 1 0.36 0.30 9.32 o 2 10 1 238.36 213.67 18.39 o 3 10 1 26.27 48.23 13.66 o 4 10 1 8.35 9.31 9.39 o 5 10 1 15.19 32.38 14.45 o 6 10 1 24.33 40.06 11.77 o 7 10 1 3.79 1.10 13.30 o 8 10 1 157.14 119.35 20.83 o 0 11 1 0.99 17.62 25.45 o 1 11 1 8.49 9.62 12.78 o 2 11 1 184.32 142.32 19.65 o 3 11 1 0.97 -24.52 24.52 o 4 11 1 57.95 52.25 19.09 o 5 11 1 15.55 13.27 15.60 o 0 0 2 20866.97 21066.63 472.37 o 1 0 2 241.19 284.78 6.37 o 2 0 2 2136.73 2237.22 44.67 o 3 0 2 284.38 330.91 9.12 o 4 0 2 8.81 10.77 3.92 o 5 0 2 225.35 218.26 7.45 o 6 0 2 1428.21 1390.06 28.02 o 7 0 2 3353.15 3458.94 77.66 o 8 0 2 583.13 587.29 21.27 o 9 0 2 0.10 3.92 4.89 o 10 0 2 47.10 56.88 10.87 o 11 0 2 128.60 119.25 8.91 o 12 0 2 323.47 324.97 15.77 o 13 0 2 579.29 630.22 29.88 o 14 0 2 66.03 58.74 10.57 o 15 0 2 0.04 -2.94 12.82 o 16 0 2 12.44 43.17 27.51 o 17 0 2 43.24 46.11 32.30 o 1 1 2 181.58 194.95 4.18 o 2 1 2 2175.47 2079.52 33.04 o 3 1 2 7265.74 7308.99 93.65 o 4 1 2 697.79 631.66 10.96 o 5 1 2 186.27 206.38 6.66 o 6 1 2 9.30 13.42 3.92 o 7 1 2 64.92 65.01 4.27 o 8 1 2 13.04 15.46 3.60 o 9 1 2 28.86 32.76 3.91 o 10 1 2 1966.69 1942.32 47.56 o 11 1 2 0.94 -0.89 4.59 o 12 1 2 166.43 162.20 7.79 o 13 1 2 54.32 61.70 7.71 o 14 1 2 13.01 9.60 9.10 o 15 1 2 13.21 9.79 10.38 o 16 1 2 303.99 281.25 39.17 o 17 1 2 101.41 58.69 26.38 o 0 2 2 4368.29 4121.03 85.22 o 1 2 2 1070.89 1174.62 15.91 o 2 2 2 1.42 -1.75 1.75 o 3 2 2 13.96 14.83 6.31 o 4 2 2 1.14 5.66 4.40 o 5 2 2 1.06 2.26 8.27 o 6 2 2 2194.51 2113.60 52.90 o 7 2 2 625.31 663.41 11.57 o 8 2 2 25.24 24.73 7.24 o 9 2 2 408.16 389.86 12.25 o 10 2 2 18.12 14.46 6.85 o 11 2 2 101.60 96.02 6.89 o 12 2 2 357.48 348.01 21.79 o 13 2 2 319.12 295.34 14.70 o 14 2 2 165.21 169.29 14.10 o 15 2 2 39.80 19.70 13.65 o 16 2 2 13.93 5.07 20.02 o 17 2 2 5.86 13.69 33.82 o 1 3 2 1631.64 1670.28 25.17 o 2 3 2 136.25 123.55 4.35 o 3 3 2 338.38 313.28 6.64 o 4 3 2 2574.69 2540.79 38.69 o 5 3 2 622.43 609.81 11.41 o 6 3 2 196.15 202.94 7.64 o 7 3 2 18.60 12.66 4.15 o 8 3 2 4.22 14.07 4.70 o 9 3 2 75.94 65.86 6.09 o 10 3 2 1048.29 1055.00 25.87 o 11 3 2 261.73 237.44 20.61 o 12 3 2 0.19 -7.05 7.05 o 13 3 2 0.09 -0.01 9.83 o 14 3 2 16.12 3.81 10.02 o 15 3 2 21.36 31.83 11.02 o 16 3 2 218.68 194.03 22.56 o 0 4 2 3409.73 3440.83 73.80 o 1 4 2 1021.17 1093.77 18.88 o 2 4 2 9.90 10.38 5.33 o 3 4 2 0.39 -1.14 3.87 o 4 4 2 38.52 38.20 3.34 o 5 4 2 19.88 31.56 13.80 o 6 4 2 1617.67 1631.68 28.54 o 7 4 2 159.43 170.83 8.52 o 8 4 2 17.44 13.14 7.29 o 9 4 2 503.75 511.52 14.77 o 10 4 2 17.06 3.68 7.29 o 11 4 2 49.80 52.40 7.15 o 12 4 2 269.03 268.90 14.95 o 13 4 2 174.78 181.11 14.86 o 14 4 2 140.59 135.87 15.31 o 15 4 2 59.45 76.83 14.06 o 16 4 2 9.66 50.02 33.18 o 1 5 2 326.21 331.38 7.98 o 2 5 2 789.56 785.07 23.64 o 3 5 2 837.12 781.54 16.46 o 4 5 2 496.91 539.82 11.80 o 5 5 2 27.84 29.21 6.41 o 6 5 2 1.05 6.54 6.16 o 7 5 2 13.68 14.59 5.89 o 8 5 2 0.90 3.29 5.22 o 9 5 2 0.03 -4.00 7.52 o 10 5 2 1187.65 1245.69 37.47 o 11 5 2 35.70 32.83 8.16 o 12 5 2 71.52 80.77 14.29 o 13 5 2 7.63 7.96 22.51 o 14 5 2 7.59 12.70 13.78 o 15 5 2 7.51 37.98 22.42 o 0 6 2 3448.32 3565.08 71.23 o 1 6 2 61.52 53.53 4.61 o 2 6 2 133.65 103.74 6.33 o 3 6 2 23.52 18.18 4.65 o 4 6 2 5.16 7.87 4.19 o 5 6 2 27.97 25.11 4.63 o 6 6 2 466.50 489.49 18.43 o 7 6 2 795.85 796.56 24.34 o 8 6 2 260.90 286.24 12.68 o 9 6 2 11.81 16.28 6.64 o 10 6 2 21.30 23.04 9.25 o 11 6 2 32.77 43.93 11.07 o 12 6 2 150.16 158.35 22.08 o 13 6 2 218.18 237.02 29.62 o 14 6 2 33.72 35.31 18.21 o 1 7 2 28.32 28.55 5.87 o 2 7 2 362.94 369.67 11.84 o 3 7 2 1131.60 1134.49 29.75 o 4 7 2 280.94 304.89 12.86 o 5 7 2 34.89 33.09 6.23 o 6 7 2 0.36 -1.94 4.75 o 7 7 2 30.64 54.79 23.15 o 8 7 2 1.45 4.74 11.26 o 9 7 2 16.66 4.43 10.57 o 10 7 2 651.04 743.08 35.18 o 11 7 2 2.13 5.75 10.06 o 12 7 2 41.80 32.56 13.03 o 13 7 2 26.74 20.83 22.02 o 0 8 2 724.92 750.38 42.93 o 1 8 2 0.92 -1.75 7.39 o 2 8 2 0.36 -2.63 3.92 o 3 8 2 2.77 0.70 6.59 o 4 8 2 1.48 5.31 11.70 o 5 8 2 11.32 5.38 6.99 o 6 8 2 506.93 522.90 25.99 o 7 8 2 280.00 245.79 40.30 o 8 8 2 4.89 -1.03 9.76 o 9 8 2 20.49 26.93 20.51 o 10 8 2 4.40 -15.17 15.17 o 11 8 2 17.67 -3.55 12.57 o 12 8 2 103.93 65.46 14.90 o 1 9 2 70.12 75.80 33.38 o 2 9 2 32.69 13.20 8.34 o 3 9 2 151.54 143.04 11.70 o 4 9 2 449.84 504.10 23.61 o 5 9 2 17.82 18.96 8.25 o 6 9 2 35.20 35.37 10.33 o 7 9 2 0.67 -9.82 15.58 o 8 9 2 0.55 -3.92 14.68 o 9 9 2 1.98 24.56 21.58 o 10 9 2 178.08 137.66 26.44 o 0 10 2 333.60 338.56 35.75 o 1 10 2 53.50 16.19 16.47 o 2 10 2 0.92 -10.75 10.75 o 3 10 2 3.72 -6.05 17.23 o 4 10 2 0.00 -3.43 11.07 o 5 10 2 1.85 -11.06 11.06 o 6 10 2 248.56 305.09 79.46 o 7 10 2 25.72 19.48 22.32 o 8 10 2 5.58 14.24 19.81 o 1 11 2 21.38 -7.66 34.70 o 2 11 2 94.71 86.93 16.26 o 3 11 2 42.82 25.46 14.02 o 4 11 2 73.33 61.57 15.74 o 1 0 3 872.51 820.74 17.98 o 2 0 3 7.69 13.61 3.92 o 3 0 3 42.00 43.17 4.89 o 4 0 3 717.77 702.26 16.58 o 5 0 3 4848.11 4962.25 93.28 o 6 0 3 4.48 13.61 3.92 o 7 0 3 534.94 551.35 16.17 o 8 0 3 297.01 255.75 9.99 o 9 0 3 0.11 -0.98 4.99 o 10 0 3 14.03 12.73 9.79 o 11 0 3 198.89 234.13 16.25 o 12 0 3 120.32 108.58 11.75 o 13 0 3 25.10 23.49 10.96 o 14 0 3 512.86 526.36 35.85 o 15 0 3 138.45 128.25 22.71 o 16 0 3 18.98 20.56 20.46 o 17 0 3 1.54 0.00 9.79 o 0 1 3 186.21 202.78 6.27 o 1 1 3 311.22 295.93 5.34 o 2 1 3 453.84 399.77 7.11 o 3 1 3 732.01 750.54 12.11 o 4 1 3 1423.85 1396.15 21.52 o 5 1 3 2773.12 2756.75 38.04 o 6 1 3 303.16 285.56 7.07 o 7 1 3 7.49 1.82 7.88 o 8 1 3 89.55 86.81 5.57 o 9 1 3 227.85 236.62 8.16 o 10 1 3 26.47 22.29 4.44 o 11 1 3 127.05 140.82 8.09 o 12 1 3 187.17 166.53 12.19 o 13 1 3 23.54 17.43 7.12 o 14 1 3 137.39 130.32 17.13 o 15 1 3 438.31 464.32 25.73 o 16 1 3 0.64 17.41 14.69 o 1 2 3 281.07 252.37 4.92 o 2 2 3 1729.13 1656.74 28.11 o 3 2 3 558.44 551.42 14.61 o 4 2 3 499.16 521.06 14.31 o 5 2 3 1766.76 1793.90 29.89 o 6 2 3 952.62 957.67 17.55 o 7 2 3 460.09 486.68 16.07 o 8 2 3 533.05 514.71 12.05 o 9 2 3 18.45 10.57 2.70 o 10 2 3 145.68 145.64 6.78 o 11 2 3 21.98 22.71 4.71 o 12 2 3 58.19 48.96 7.93 o 13 2 3 4.10 21.26 10.77 o 14 2 3 155.73 173.75 15.05 o 15 2 3 113.11 98.45 14.88 o 16 2 3 41.32 41.33 15.49 o 0 3 3 2642.93 2632.35 51.63 o 1 3 3 390.36 425.64 8.25 o 2 3 3 634.51 617.65 21.87 o 3 3 3 63.44 56.99 3.74 o 4 3 3 971.88 970.93 15.46 o 5 3 3 752.29 754.92 14.34 o 6 3 3 413.75 426.53 16.12 o 7 3 3 394.64 360.52 21.11 o 8 3 3 1511.85 1461.21 31.68 o 9 3 3 23.36 18.83 5.82 o 10 3 3 69.81 73.31 13.31 o 11 3 3 195.69 217.89 11.98 o 12 3 3 167.04 161.55 12.64 o 13 3 3 85.39 97.90 13.75 o 14 3 3 124.32 133.38 15.26 o 15 3 3 195.73 206.12 32.46 o 16 3 3 112.88 86.97 25.84 o 1 4 3 184.93 168.48 12.49 o 2 4 3 1508.91 1556.39 28.45 o 3 4 3 519.40 535.43 33.86 o 4 4 3 867.50 863.11 18.21 o 5 4 3 851.99 779.76 22.75 o 6 4 3 749.30 753.67 21.37 o 7 4 3 355.75 365.59 23.61 o 8 4 3 418.36 429.53 13.19 o 9 4 3 28.97 17.20 13.17 o 10 4 3 240.88 232.77 11.54 o 11 4 3 2.99 14.84 6.85 o 12 4 3 87.35 85.94 10.87 o 13 4 3 12.78 1.33 24.91 o 14 4 3 93.85 86.46 14.15 o 15 4 3 92.13 68.80 24.78 o 0 5 3 83.90 101.53 7.54 o 1 5 3 0.05 1.76 4.50 o 2 5 3 661.58 676.64 13.87 o 3 5 3 129.22 125.50 7.93 o 4 5 3 536.67 536.65 11.30 o 5 5 3 864.29 890.22 20.17 o 6 5 3 400.54 390.19 13.67 o 7 5 3 56.20 54.61 4.81 o 8 5 3 184.40 163.31 10.05 o 9 5 3 80.66 83.77 9.69 o 10 5 3 1.37 7.05 6.90 o 11 5 3 76.86 75.96 9.71 o 12 5 3 139.65 128.45 12.96 o 13 5 3 19.14 24.21 12.28 o 14 5 3 132.97 123.87 21.64 o 15 5 3 203.29 203.64 38.92 o 1 6 3 294.62 280.05 8.73 o 2 6 3 50.98 57.56 4.85 o 3 6 3 2.29 6.33 4.40 o 4 6 3 404.16 410.81 36.98 o 5 6 3 1260.25 1250.89 38.96 o 6 6 3 18.59 25.76 7.75 o 7 6 3 166.49 169.37 38.19 o 8 6 3 194.79 197.64 13.00 o 9 6 3 0.02 -5.24 6.80 o 10 6 3 0.10 19.48 15.76 o 11 6 3 68.42 87.34 13.72 o 12 6 3 91.97 86.47 14.73 o 13 6 3 4.50 -7.34 10.28 o 14 6 3 226.20 207.64 25.87 o 0 7 3 8.87 3.92 3.92 o 1 7 3 79.50 68.40 5.35 o 2 7 3 139.34 143.82 7.68 o 3 7 3 96.47 87.65 6.75 o 4 7 3 287.58 278.99 15.38 o 5 7 3 569.60 565.09 32.09 o 6 7 3 89.67 84.85 31.67 o 7 7 3 0.31 -1.95 8.16 o 8 7 3 21.45 14.91 9.22 o 9 7 3 105.06 91.02 13.25 o 10 7 3 13.47 18.35 9.98 o 11 7 3 42.32 11.55 13.51 o 12 7 3 67.94 59.48 13.91 o 13 7 3 2.59 -15.71 15.71 o 1 8 3 135.85 124.52 15.67 o 2 8 3 202.92 208.43 11.75 o 3 8 3 16.32 26.70 7.78 o 4 8 3 40.11 56.24 11.45 o 5 8 3 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568.78 580.28 11.58 o 2 3 5 51.75 53.73 4.05 o 3 3 5 481.66 449.83 9.84 o 4 3 5 33.99 38.21 4.01 o 5 3 5 601.57 617.75 13.44 o 6 3 5 896.74 914.62 24.62 o 7 3 5 22.77 10.02 5.84 o 8 3 5 215.65 225.42 13.08 o 9 3 5 452.83 480.92 19.52 o 10 3 5 3.75 3.30 8.42 o 11 3 5 323.43 337.70 21.06 o 12 3 5 39.55 46.94 14.29 o 13 3 5 11.68 24.47 16.74 o 14 3 5 142.27 186.93 67.85 o 1 4 5 866.87 866.68 16.80 o 2 4 5 215.23 229.76 7.04 o 3 4 5 7.54 11.09 3.98 o 4 4 5 990.52 978.14 23.39 o 5 4 5 908.85 906.74 33.00 o 6 4 5 113.99 100.84 4.76 o 7 4 5 367.92 395.74 14.23 o 8 4 5 73.10 77.09 19.63 o 9 4 5 52.65 40.34 8.69 o 10 4 5 355.00 367.31 18.81 o 11 4 5 235.27 271.45 19.03 o 12 4 5 0.53 -13.18 13.18 o 13 4 5 32.42 16.88 15.15 o 14 4 5 1.46 -16.54 27.21 o 0 5 5 169.81 187.02 13.71 o 1 5 5 168.04 159.71 9.20 o 2 5 5 43.48 48.06 5.58 o 3 5 5 294.06 286.43 9.95 o 4 5 5 31.31 22.80 9.25 o 5 5 5 403.56 394.30 14.87 o 6 5 5 612.99 691.99 26.06 o 7 5 5 0.55 -7.08 11.57 o 8 5 5 10.31 7.79 14.14 o 9 5 5 179.79 193.58 24.92 o 10 5 5 3.79 5.03 8.66 o 11 5 5 178.71 158.55 25.95 o 12 5 5 32.88 36.77 14.90 o 13 5 5 5.76 3.28 21.94 o 1 6 5 280.74 285.75 11.14 o 2 6 5 16.86 10.32 5.46 o 3 6 5 54.57 67.67 6.81 o 4 6 5 488.00 532.11 17.35 o 5 6 5 215.48 204.76 11.60 o 6 6 5 23.04 24.82 13.07 o 7 6 5 344.05 350.07 20.51 o 8 6 5 25.29 52.98 12.89 o 9 6 5 1.70 25.74 11.47 o 10 6 5 26.80 29.51 12.53 o 11 6 5 53.69 69.51 16.33 o 12 6 5 3.69 14.18 16.12 o 0 7 5 35.96 39.16 14.88 o 1 7 5 9.74 6.89 7.76 o 2 7 5 4.63 -1.30 5.33 o 3 7 5 86.13 85.75 11.89 o 4 7 5 17.30 16.02 5.92 o 5 7 5 122.79 127.02 13.44 o 6 7 5 241.12 272.15 46.46 o 7 7 5 29.25 28.29 11.77 o 8 7 5 27.72 20.22 11.50 o 9 7 5 37.74 25.65 13.38 o 10 7 5 0.05 -7.66 12.80 o 11 7 5 122.52 123.21 38.28 o 1 8 5 186.28 191.33 16.82 o 2 8 5 34.58 46.85 9.92 o 3 8 5 34.25 35.20 10.26 o 4 8 5 147.03 154.97 21.63 o 5 8 5 87.72 81.30 19.45 o 6 8 5 17.74 23.19 17.51 o 7 8 5 130.18 133.07 21.33 o 8 8 5 24.15 55.29 19.26 o 9 8 5 6.91 -11.31 17.03 o 0 9 5 378.62 360.81 36.83 o 1 9 5 63.27 115.75 57.22 o 2 9 5 2.80 -7.18 12.30 o 3 9 5 49.07 24.23 14.19 o 4 9 5 10.57 -4.89 18.54 o 5 9 5 77.65 81.66 26.73 o 6 9 5 136.67 190.84 24.51 o 7 9 5 0.42 12.51 20.80 o 1 10 5 109.31 89.43 17.28 o 2 10 5 55.30 55.35 16.84 o 3 10 5 3.66 -3.61 29.27 o 0 0 6 0.75 -9.89 9.89 o 1 0 6 99.46 100.84 7.54 o 2 0 6 562.99 520.79 15.68 o 3 0 6 107.86 94.68 7.93 o 4 0 6 98.77 101.53 7.54 o 5 0 6 42.77 35.34 5.97 o 6 0 6 26.38 21.44 5.78 o 7 0 6 126.23 130.41 9.99 o 8 0 6 384.11 383.87 23.31 o 9 0 6 239.93 251.66 26.83 o 10 0 6 105.10 127.56 16.94 o 11 0 6 28.44 6.95 17.72 o 12 0 6 31.96 -37.98 38.18 o 13 0 6 142.66 209.91 34.46 o 14 0 6 34.13 -4.89 29.46 o 1 1 6 317.68 315.45 8.66 o 2 1 6 333.09 336.96 8.93 o 3 1 6 439.17 454.11 27.33 o 4 1 6 133.25 122.87 6.12 o 5 1 6 130.39 118.68 6.85 o 6 1 6 72.44 62.10 5.18 o 7 1 6 9.14 6.70 4.46 o 8 1 6 537.71 564.23 17.15 o 9 1 6 438.17 461.83 19.49 o 10 1 6 0.67 12.13 10.06 o 11 1 6 30.22 25.09 15.09 o 12 1 6 159.97 197.51 21.29 o 13 1 6 15.48 42.16 21.51 o 14 1 6 34.39 41.10 19.66 o 0 2 6 115.92 115.83 8.13 o 1 2 6 783.06 769.77 15.33 o 2 2 6 1190.06 1241.99 21.86 o 3 2 6 1.42 7.30 5.82 o 4 2 6 156.70 163.32 13.12 o 5 2 6 13.54 18.98 4.46 o 6 2 6 159.30 145.56 6.92 o 7 2 6 508.32 510.11 16.26 o 8 2 6 103.78 108.48 13.61 o 9 2 6 57.28 64.82 19.09 o 10 2 6 8.55 25.89 10.35 o 11 2 6 74.65 56.94 13.69 o 12 2 6 43.88 28.36 14.08 o 13 2 6 265.68 305.73 38.34 o 14 2 6 81.40 62.65 39.16 o 1 3 6 76.61 65.84 4.81 o 2 3 6 78.54 63.18 8.17 o 3 3 6 1541.48 1589.85 30.90 o 4 3 6 479.37 463.50 11.89 o 5 3 6 35.40 41.24 5.23 o 6 3 6 0.05 -1.43 6.95 o 7 3 6 13.72 7.84 5.92 o 8 3 6 388.90 414.83 16.57 o 9 3 6 566.81 618.02 31.00 o 10 3 6 29.90 17.58 9.77 o 11 3 6 200.37 264.40 20.81 o 12 3 6 328.40 346.75 35.07 o 13 3 6 8.19 14.03 23.39 o 0 4 6 79.92 71.37 7.93 o 1 4 6 975.82 991.40 21.60 o 2 4 6 724.37 728.30 20.20 o 3 4 6 1.09 2.87 7.88 o 4 4 6 107.29 111.20 6.22 o 5 4 6 29.70 26.27 3.22 o 6 4 6 113.87 103.41 4.92 o 7 4 6 580.46 615.30 22.57 o 8 4 6 57.61 64.40 9.35 o 9 4 6 9.19 34.98 14.30 o 10 4 6 10.18 5.55 13.61 o 11 4 6 54.71 51.68 14.54 o 12 4 6 33.27 28.85 25.45 o 13 4 6 235.67 191.33 61.49 o 1 5 6 71.80 81.19 7.73 o 2 5 6 140.11 141.55 8.91 o 3 5 6 506.45 517.61 42.81 o 4 5 6 32.76 39.85 7.43 o 5 5 6 8.68 8.94 9.74 o 6 5 6 30.32 27.86 12.92 o 7 5 6 10.64 2.55 10.04 o 8 5 6 282.59 268.36 34.57 o 9 5 6 366.22 398.22 26.05 o 10 5 6 1.61 -6.87 14.38 o 11 5 6 61.80 60.54 21.88 o 12 5 6 70.88 71.36 31.23 o 0 6 6 3.31 12.72 11.84 o 1 6 6 136.49 133.24 10.38 o 2 6 6 204.46 211.75 13.78 o 3 6 6 26.84 38.14 10.08 o 4 6 6 62.41 61.85 13.41 o 5 6 6 7.42 14.94 8.60 o 6 6 6 7.52 35.11 11.39 o 7 6 6 89.53 87.79 12.77 o 8 6 6 168.09 168.76 17.51 o 9 6 6 70.27 62.92 16.34 o 10 6 6 58.50 46.41 14.94 o 11 6 6 8.97 14.95 16.59 o 1 7 6 98.39 74.90 11.69 o 2 7 6 129.34 121.33 14.16 o 3 7 6 104.72 91.97 13.77 o 4 7 6 40.42 60.37 16.27 o 5 7 6 55.69 66.81 17.08 o 6 7 6 26.91 16.80 21.44 o 7 7 6 0.06 18.11 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25.51 16.31 7.97 o 8 1 7 17.04 23.19 8.75 o 9 1 7 123.60 135.99 14.86 o 10 1 7 32.05 37.59 13.91 o 11 1 7 226.26 253.54 45.29 o 12 1 7 30.12 26.05 19.93 o 13 1 7 5.96 -20.56 25.55 o 1 2 7 644.97 663.44 16.50 o 2 2 7 5.14 16.41 5.86 o 3 2 7 106.95 95.70 12.19 o 4 2 7 259.49 244.82 9.31 o 5 2 7 160.16 165.98 12.14 o 6 2 7 100.07 89.52 8.95 o 7 2 7 64.93 72.98 11.40 o 8 2 7 0.65 -11.23 11.23 o 9 2 7 86.47 76.37 16.81 o 10 2 7 348.48 406.50 26.55 o 11 2 7 109.10 127.14 19.68 o 12 2 7 19.81 26.33 26.33 o 13 2 7 1.52 -17.62 27.31 o 0 3 7 737.56 831.37 32.54 o 1 3 7 426.60 404.07 13.23 o 2 3 7 130.27 123.90 8.49 o 3 3 7 51.01 36.72 5.93 o 4 3 7 202.48 182.44 8.47 o 5 3 7 169.31 166.48 14.69 o 6 3 7 217.47 232.47 14.77 o 7 3 7 180.67 199.63 17.30 o 8 3 7 9.88 18.20 11.89 o 9 3 7 289.26 346.37 87.50 o 10 3 7 9.31 -0.01 22.46 o 11 3 7 216.19 253.92 24.68 o 12 3 7 10.46 7.73 20.36 o 1 4 7 498.10 523.33 17.72 o 2 4 7 1.20 4.89 5.93 o 3 4 7 126.69 112.30 7.32 o 4 4 7 85.55 76.67 13.22 o 5 4 7 169.63 165.49 32.36 o 6 4 7 130.36 124.89 10.37 o 7 4 7 51.00 48.15 13.18 o 8 4 7 0.05 3.53 12.07 o 9 4 7 77.65 66.23 16.66 o 10 4 7 212.12 218.14 19.95 o 11 4 7 110.97 108.57 25.45 o 0 5 7 339.10 332.89 33.10 o 1 5 7 94.48 81.31 17.57 o 2 5 7 1.00 -3.03 11.31 o 3 5 7 39.01 32.96 12.68 o 4 5 7 114.22 110.18 11.77 o 5 5 7 106.67 119.02 10.75 o 6 5 7 344.49 336.20 20.66 o 7 5 7 35.86 55.98 26.97 o 8 5 7 43.73 52.43 32.70 o 9 5 7 86.39 96.61 36.71 o 10 5 7 7.18 -5.31 18.07 o 1 6 7 147.03 154.55 41.56 o 2 6 7 0.17 2.31 17.67 o 3 6 7 3.84 4.81 22.95 o 4 6 7 452.11 467.70 36.53 o 5 6 7 20.74 34.19 20.64 o 6 6 7 97.39 116.25 15.96 o 7 6 7 81.67 80.51 13.48 o 8 6 7 0.91 16.04 27.95 o 9 6 7 10.64 8.48 16.05 o 0 7 7 401.23 442.31 39.47 o 1 7 7 24.02 24.81 14.25 o 2 7 7 16.17 3.94 13.91 o 3 7 7 9.88 -9.53 11.09 o 4 7 7 52.87 43.22 16.50 o 5 7 7 37.40 80.07 26.33 o 6 7 7 336.39 348.42 39.22 o 7 7 7 8.20 -7.46 17.13 o 1 8 7 145.22 155.79 18.91 o 2 8 7 23.99 10.07 22.42 o 3 8 7 19.85 5.39 17.36 o 4 8 7 125.12 125.16 49.24 o 5 8 7 26.88 61.84 25.14 o 0 0 8 85.48 41.12 17.62 o 1 0 8 305.14 298.41 18.41 o 2 0 8 775.00 764.21 32.93 o 3 0 8 74.79 89.28 11.85 o 4 0 8 281.36 288.70 21.25 o 5 0 8 59.90 43.17 12.73 o 6 0 8 1.08 0.98 12.92 o 7 0 8 171.03 213.54 31.14 o 8 0 8 367.80 381.37 48.87 o 9 0 8 16.20 -8.81 17.62 o 10 0 8 14.07 13.61 30.25 o 11 0 8 40.05 46.11 36.12 o 1 1 8 58.07 42.49 7.20 o 2 1 8 161.98 163.25 14.39 o 3 1 8 249.68 257.67 22.82 o 4 1 8 12.26 13.55 8.99 o 5 1 8 45.79 42.56 11.84 o 6 1 8 205.29 205.04 16.39 o 7 1 8 16.59 0.63 11.78 o 8 1 8 424.74 434.42 27.14 o 9 1 8 177.48 194.00 21.97 o 10 1 8 0.58 -4.19 16.13 o 11 1 8 70.47 47.77 33.28 o 0 2 8 108.29 86.35 11.65 o 1 2 8 266.50 254.80 13.77 o 2 2 8 644.13 659.31 42.09 o 3 2 8 25.82 24.39 7.48 o 4 2 8 257.55 257.77 20.96 o 5 2 8 101.84 76.83 13.26 o 6 2 8 13.31 -12.33 15.81 o 7 2 8 171.40 174.98 22.42 o 8 2 8 24.81 40.01 15.15 o 9 2 8 9.89 -5.50 15.92 o 10 2 8 7.26 27.31 15.58 o 11 2 8 15.80 28.29 21.63 o 1 3 8 22.75 10.19 7.24 o 2 3 8 6.96 1.07 12.03 o 3 3 8 248.91 231.13 14.73 o 4 3 8 1.17 8.33 10.78 o 5 3 8 65.97 54.38 11.87 o 6 3 8 2.52 26.57 13.83 o 7 3 8 2.56 2.41 14.19 o 8 3 8 285.38 279.35 21.43 o 9 3 8 118.41 102.97 30.30 o 10 3 8 60.32 69.31 22.42 o 0 4 8 154.62 171.05 36.03 o 1 4 8 157.67 199.25 28.57 o 2 4 8 366.60 386.98 27.07 o 3 4 8 26.84 24.20 18.65 o 4 4 8 170.06 195.62 15.71 o 5 4 8 65.01 60.63 10.68 o 6 4 8 28.14 16.28 8.44 o 7 4 8 108.87 107.84 17.79 o 8 4 8 1.63 -9.52 29.85 o 9 4 8 4.04 8.81 19.48 o 1 5 8 30.18 36.37 12.11 o 2 5 8 38.27 61.18 31.86 o 3 5 8 110.86 119.81 35.00 o 4 5 8 2.05 0.89 8.98 o 5 5 8 15.68 0.70 11.87 o 6 5 8 69.90 81.62 16.34 o 7 5 8 7.68 13.39 17.84 o 8 5 8 232.95 208.16 36.13 o 0 6 8 36.86 56.87 21.73 o 1 6 8 106.61 146.23 16.47 o 2 6 8 301.94 315.03 46.27 o 3 6 8 36.30 3.15 14.85 o 4 6 8 113.31 121.61 22.95 o 5 6 8 25.61 23.18 33.18 o 6 6 8 1.65 2.22 28.78 o 7 6 8 67.20 82.06 26.92 o 1 7 8 20.73 10.19 20.95 o 2 7 8 83.32 67.14 15.84 o 3 7 8 104.58 111.09 32.50 o 4 7 8 15.73 33.52 27.90 o 1 0 9 64.51 83.99 23.49 o 2 0 9 18.92 -22.71 22.71 o 3 0 9 493.30 488.22 33.21 o 4 0 9 364.23 330.64 27.32 o 5 0 9 94.43 150.47 25.36 o 6 0 9 113.44 107.89 38.38 o 7 0 9 6.92 32.40 21.73 o 8 0 9 33.21 21.44 24.37 o 9 0 9 112.05 139.11 56.88 o 0 1 9 371.03 354.94 42.41 o 1 1 9 183.45 168.62 19.76 o 2 1 9 36.58 39.11 14.49 o 3 1 9 12.11 15.56 12.35 o 4 1 9 143.34 155.49 17.58 o 5 1 9 78.78 85.98 15.29 o 6 1 9 288.89 308.42 44.02 o 7 1 9 238.85 255.81 25.46 o 8 1 9 0.54 -16.52 16.52 o 9 1 9 30.27 22.44 27.75 o 1 2 9 62.97 65.81 26.87 o 2 2 9 10.83 27.14 13.83 o 3 2 9 255.06 294.28 23.05 o 4 2 9 41.41 33.15 15.27 o 5 2 9 15.99 -1.47 14.19 o 6 2 9 86.94 89.92 23.40 o 7 2 9 13.91 20.49 21.16 o 8 2 9 29.27 5.85 19.05 o 0 3 9 256.32 250.68 31.73 o 1 3 9 54.58 25.35 22.42 o 2 3 9 201.18 206.39 25.47 o 3 3 9 57.34 63.08 16.38 o 4 3 9 135.32 115.96 16.70 o 5 3 9 16.14 4.73 13.10 o 6 3 9 61.98 66.44 22.11 o 7 3 9 95.38 56.88 18.40 o 8 3 9 0.77 16.54 23.39 o 1 4 9 29.24 -0.34 9.59 o 2 4 9 4.66 22.99 17.30 o 3 4 9 121.97 126.97 20.40 o 4 4 9 19.08 34.52 17.60 o 5 4 9 1.47 2.81 21.97 o 6 4 9 75.48 98.06 24.96 o 7 4 9 5.93 -5.78 27.31 o 0 5 9 178.88 112.50 25.26 o 1 5 9 46.06 45.44 14.90 o 2 5 9 24.23 21.25 16.74 o 3 5 9 13.51 22.18 14.31 o 4 5 9 76.82 86.98 25.40 o 5 5 9 36.82 50.73 32.40 o 1 6 9 23.47 49.70 36.71 o 2 6 9 9.91 12.75 14.99 o 0 0 10 2.62 8.81 25.45 o 1 0 10 193.11 104.08 34.46 o 2 0 10 51.04 12.73 31.23 o 3 0 10 0.05 21.44 33.28 o 4 0 10 146.32 140.59 30.45 o 5 0 10 144.13 104.07 30.64 o 6 0 10 30.82 2.94 29.46 o 1 1 10 293.32 275.46 47.84 o 2 1 10 33.85 -14.00 22.32 o 3 1 10 83.37 42.21 37.42 o 4 1 10 14.17 36.47 22.76 o 5 1 10 168.19 121.63 24.31 o 0 2 10 47.25 11.84 34.46 o 1 2 10 41.31 -13.75 27.60 o 2 2 10 87.44 119.40 37.74 o 3 2 10 0.05 -18.62 30.39 o 4 2 10 143.15 86.42 66.28 o 5 2 10 108.97 122.00 24.13 o 1 3 10 118.34 187.74 42.76 o 2 3 10 5.86 -36.92 36.92 o 3 3 10 5.65 6.86 34.77 o