data_2202264
_journal_name_full  'Acta Crystallographica, Section E'
_journal_year  2003
_journal_volume  59
_journal_page_first  o1004
_journal_page_last  o1005
_publ_section_title
;
o-Methoxy-N-phenylbenzohydroxamic acid
;
loop_
_publ_author_name
  'Elhadi Elbay Saad'
  'Yang Farina'
  'Bohari M. Yamin'
_chemical_formula_moiety  'C14 H13 N O3'
_chemical_formula_sum  'C14 H13 N O3'
_chemical_formula_iupac  'C14 H13 N O3'
_chemical_formula_weight  243.25
_symmetry_cell_setting  Monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, y, -z+1/2'
  'x+1/2, y+1/2, z'
  '-x+1/2, y+1/2, -z+1/2'
  '-x, -y, -z'
  'x, -y, z-1/2'
  '-x+1/2, -y+1/2, -z'
  'x+1/2, -y+1/2, z-1/2'
_cell_length_a  22.451(3)
_cell_length_b  8.3709(13)
_cell_length_c  14.921(2)
_cell_angle_alpha  90.00
_cell_angle_beta  118.531(3)
_cell_angle_gamma  90.00
_cell_volume  2463.6(6)
_cell_formula_units_Z  8
_cell_measurement_temperature  293(2)
_exptl_crystal_density_diffrn  1.312
_diffrn_ambient_temperature  293(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  O1 0.26350(6) 0.88494(14) 0.12891(7) 0.0727(4) Uani d . 1 . . O
  H1A 0.2451 0.8431 0.0724 0.109 Uiso calc R 1 . . H
  O2 0.31734(5) 0.65663(14) 0.07502(7) 0.0606(3) Uani d . 1 . . O
  O3 0.45786(5) 0.77742(14) 0.31765(8) 0.0679(3) Uani d . 1 . . O
  N1 0.30728(6) 0.77572(14) 0.20054(8) 0.0486(3) Uani d . 1 . . N
  C1 0.31973(7) 0.68471(17) 0.36362(10) 0.0490(3) Uani d . 1 . . C
  H1B 0.3165 0.5792 0.3422 0.059 Uiso calc R 1 . . H
  C2 0.32723(8) 0.7194(2) 0.45915(11) 0.0597(4) Uani d . 1 . . C
  H2A 0.3298 0.6369 0.5026 0.072 Uiso calc R 1 . . H
  C3 0.33084(8) 0.8751(2) 0.49009(11) 0.0653(4) Uani d . 1 . . C
  H3A 0.3358 0.8977 0.5543 0.078 Uiso calc R 1 . . H
  C4 0.32725(7) 0.9970(2) 0.42680(11) 0.0616(4) Uani d . 1 . . C
  H4A 0.3294 1.1023 0.4480 0.074 Uiso calc R 1 . . H
  C5 0.32045(7) 0.96475(17) 0.33104(11) 0.0529(3) Uani d . 1 . . C
  H5A 0.3181 1.0478 0.2881 0.064 Uiso calc R 1 . . H
  C6 0.31715(6) 0.80803(16) 0.30051(9) 0.0437(3) Uani d . 1 . . C
  C7 0.33543(6) 0.66695(16) 0.16711(9) 0.0453(3) Uani d . 1 . . C
  C8 0.38821(6) 0.55763(17) 0.24190(9) 0.0453(3) Uani d . 1 . . C
  C9 0.37689(7) 0.39490(19) 0.23187(11) 0.0552(4) Uani d . 1 . . C
  H9A 0.3352 0.3559 0.1826 0.066 Uiso calc R 1 . . H
  C10 0.42684(9) 0.2898(2) 0.29427(14) 0.0684(4) Uani d . 1 . . C
  H10A 0.4191 0.1802 0.2877 0.082 Uiso calc R 1 . . H
  C11 0.48836(9) 0.3493(2) 0.36647(13) 0.0722(5) Uani d . 1 . . C
  H11A 0.5221 0.2786 0.4086 0.087 Uiso calc R 1 . . H
  C12 0.50103(7) 0.5099(2) 0.37769(11) 0.0638(4) Uani d . 1 . . C
  H12A 0.5430 0.5475 0.4268 0.077 Uiso calc R 1 . . H
  C13 0.45093(7) 0.61640(19) 0.31543(9) 0.0506(3) Uani d . 1 . . C
  C14 0.52019(9) 0.8451(2) 0.39225(15) 0.0855(6) Uani d . 1 . . C
  H14A 0.5183 0.9592 0.3850 0.128 Uiso calc R 1 . . H
  H14B 0.5568 0.8043 0.3828 0.128 Uiso calc R 1 . . H
  H14C 0.5275 0.8174 0.4592 0.128 Uiso calc R 1 . . H
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  O1 0.0888(8) 0.0716(7) 0.0385(5) 0.0328(6) 0.0149(5) 0.0087(5)
  O2 0.0616(6) 0.0812(7) 0.0329(5) 0.0130(5) 0.0176(4) 0.0033(4)
  O3 0.0464(6) 0.0718(8) 0.0695(7) -0.0063(5) 0.0149(5) -0.0083(5)
  N1 0.0502(6) 0.0547(7) 0.0347(5) 0.0101(5) 0.0154(5) 0.0065(5)
  C1 0.0468(7) 0.0557(8) 0.0441(7) -0.0014(6) 0.0213(6) -0.0010(6)
  C2 0.0601(9) 0.0766(11) 0.0448(7) 0.0012(7) 0.0270(7) 0.0041(7)
  C3 0.0599(9) 0.0905(12) 0.0415(7) 0.0036(8) 0.0211(7) -0.0098(8)
  C4 0.0504(8) 0.0654(9) 0.0540(8) 0.0007(7) 0.0129(6) -0.0177(7)
  C5 0.0456(7) 0.0552(8) 0.0480(7) -0.0008(6) 0.0143(6) -0.0001(6)
  C6 0.0348(6) 0.0550(8) 0.0362(6) 0.0003(5) 0.0128(5) -0.0007(5)
  C7 0.0398(6) 0.0575(8) 0.0341(6) -0.0006(5) 0.0141(5) 0.0009(5)
  C8 0.0411(6) 0.0613(8) 0.0345(6) 0.0052(5) 0.0188(5) 0.0027(5)
  C9 0.0497(7) 0.0635(9) 0.0501(7) 0.0028(6) 0.0221(6) 0.0019(6)
  C10 0.0670(10) 0.0629(10) 0.0756(10) 0.0119(8) 0.0343(9) 0.0151(8)
  C11 0.0574(9) 0.0854(13) 0.0658(10) 0.0233(8) 0.0230(8) 0.0234(9)
  C12 0.0439(8) 0.0914(12) 0.0471(7) 0.0090(7) 0.0145(6) 0.0038(8)
  C13 0.0421(6) 0.0695(9) 0.0397(6) 0.0024(6) 0.0190(5) -0.0009(6)
  C14 0.0601(10) 0.0968(14) 0.0812(12) -0.0163(9) 0.0188(9) -0.0276(11)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  O1 N1 . 1.3931(14) yes
  O1 H1A . 0.8200 ?
  O2 C7 . 1.2359(15) yes
  O3 C13 . 1.3554(19) yes
  O3 C14 . 1.4251(19) yes
  N1 C7 . 1.3335(17) yes
  N1 C6 . 1.4252(16) yes
  C1 C6 . 1.3797(19) ?
  C1 C2 . 1.384(2) ?
  C1 H1B . 0.9300 ?
  C2 C3 . 1.372(2) ?
  C2 H2A . 0.9300 ?
  C3 C4 . 1.367(2) ?
  C3 H3A . 0.9300 ?
  C4 C5 . 1.389(2) ?
  C4 H4A . 0.9300 ?
  C5 C6 . 1.3791(19) ?
  C5 H5A . 0.9300 ?
  C7 C8 . 1.4912(17) ?
  C8 C9 . 1.381(2) ?
  C8 C13 . 1.3975(18) ?
  C9 C10 . 1.379(2) ?
  C9 H9A . 0.9300 ?
  C10 C11 . 1.377(3) ?
  C10 H10A . 0.9300 ?
  C11 C12 . 1.368(2) ?
  C11 H11A . 0.9300 ?
  C12 C13 . 1.387(2) ?
  C12 H12A . 0.9300 ?
  C14 H14A . 0.9600 ?
  C14 H14B . 0.9600 ?
  C14 H14C . 0.9600 ?