Crystallography Open Database

Information card for entry 2202576

2202575 << 2202576 >> 2202577

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Coordinates	Coordinates are not available: file is not found.
Structure factors	2202576.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	trans-μ-But-2-ene-1,4-diyl-dichlorobis(tri-tert- butylsilyl)digermanium(Ge‒Ge)
Formula	C28 H60 Cl2 Ge2 Si2
Calculated formula	C28 H60 Cl2 Ge2 Si2
Title of publication	<i>trans</i>-μ-But-2-ene-1,4-diyldichlorobis(tri-<i>tert</i>-butylsilyl)digermanium(Ge‒Ge)
Authors of publication	Lerner, Hans-Wolfram; Dürner, Gerd; Bolte, Michael
Journal of publication	Acta Crystallographica Section E
Year of publication	2003
Journal volume	59
Journal issue	9
Pages of publication	m816 - m817
a	25.236 ± 0.001 Å
b	9.6427 ± 0.0005 Å
c	14.0761 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	3425.3 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.046
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.055
Weighted residual factors for all reflections included in the refinement	0.059
Goodness-of-fit parameter for all reflections included in the refinement	0.867
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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