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Information card for entry 2203288
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| Coordinates | 2203288.cif |
|---|---|
| Structure factors | 2203288.hkl |
| Original IUCr paper | HTML |
| Chemical name | [1,8-Di-2-n-propyl-1,3,6,8,10,13-hexaazacyclotetradecane]nickel(II) diperchlorate |
|---|---|
| Formula | C14 H34 Cl2 N6 Ni O8 |
| Calculated formula | C14 H34 Cl2 N6 Ni O8 |
| Title of publication | (1,8-Di-<i>n</i>-propyl-1,3,6,8,10,13-hexaazacyclotetradecane)nickel(II) diperchlorate |
| Authors of publication | Li, Yan-Wu; Xiang, Hua; Lu, Tong-Bu; Ng, Seik Weng |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2004 |
| Journal volume | 60 |
| Journal issue | 3 |
| Pages of publication | m312 - m313 |
| a | 8.1634 ± 0.0006 Å |
| b | 12.411 ± 0.001 Å |
| c | 12.518 ± 0.001 Å |
| α | 77.094 ± 0.001° |
| β | 83.348 ± 0.001° |
| γ | 71.882 ± 0.001° |
| Cell volume | 1173.47 ± 0.16 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0532 |
| Residual factor for significantly intense reflections | 0.0438 |
| Weighted residual factors for significantly intense reflections | 0.1238 |
| Weighted residual factors for all reflections included in the refinement | 0.1305 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.083 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
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