Crystallography Open Database

Information card for entry 2203477

2203476 << 2203477 >> 2203478

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Coordinates	2203477.cif
Original IUCr paper	HTML

Structure parameters

Common name	Bis(pyridine-2-carbaldehyde thiosemicarbazonato)cobalt(III) perchlorate
Formula	C14 H14 Cl Co N8 O4 S2
Calculated formula	C14 H14 Cl Co N8 O4 S2
SMILES	[Co]1234(SC(=N[N]2=Cc2[n]1cccc2)N)SC(=N[N]4=Cc1[n]3cccc1)N.Cl(=O)(=O)(=O)[O-]
Title of publication	Bis(pyridine-2-carbaldehyde thiosemicarbazonato)cobalt(III) perchlorate
Authors of publication	Wang, Heng-Shan; Huang, Ling; Chen, Zhen-Feng; Wang, Xian-Wen; Zhou, Jian; Shi, Shao-Ming; Liang, Hong; Yu, Kai-Bei
Journal of publication	Acta Crystallographica Section E
Year of publication	2004
Journal volume	60
Journal issue	4
Pages of publication	m354 - m356
a	8.568 ± 0.001 Å
b	10.352 ± 0.001 Å
c	12.44 ± 0.002 Å
α	103.73 ± 0.01°
β	102.42 ± 0.01°
γ	100.16 ± 0.01°
Cell volume	1016.2 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0473
Residual factor for significantly intense reflections	0.035
Weighted residual factors for significantly intense reflections	0.0879
Weighted residual factors for all reflections included in the refinement	0.0916
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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