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Information card for entry 2203630
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| Coordinates | 2203630.cif |
|---|---|
| Structure factors | 2203630.hkl |
| Original IUCr paper | HTML |
| Chemical name | (1R,2R)-1,3-Bis(tert-butyldimethylsilyloxy)-2-(4-hydroxybutanamido)- 1-(4-nitrophenyl)propane |
|---|---|
| Formula | C25 H46 N2 O6 Si2 |
| Calculated formula | C25 H46 N2 O6 Si2 |
| Title of publication | (1<i>R</i>,2<i>R</i>)-1,3-Bis(<i>tert</i>-butyldimethylsilyloxy)-2-(4-hydroxybutanamido)-1-(4-nitrophenyl)propane |
| Authors of publication | Johansson, Dorte; Larsen, Frank B.; Bond, Andrew D.; Nielsen, Poul |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2004 |
| Journal volume | 60 |
| Journal issue | 5 |
| Pages of publication | o907 - o908 |
| a | 14.9014 ± 0.0012 Å |
| b | 12.0241 ± 0.001 Å |
| c | 17.2103 ± 0.0014 Å |
| α | 90° |
| β | 91.288 ± 0.002° |
| γ | 90° |
| Cell volume | 3082.9 ± 0.4 Å3 |
| Cell temperature | 180 ± 2 K |
| Ambient diffraction temperature | 180 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.1012 |
| Residual factor for significantly intense reflections | 0.0564 |
| Weighted residual factors for significantly intense reflections | 0.1284 |
| Weighted residual factors for all reflections included in the refinement | 0.148 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
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