Crystallography Open Database

Information card for entry 2205238

2205237 << 2205238 >> 2205239

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Structure parameters

Chemical name	bis(2-oxidonaphthalene-1-carbaldehyde benzoylhydrazonato)vanadium(IV) dichloromethane hexane hemisolvate
Formula	C40 H33 Cl2 N4 O4 V
Calculated formula	C40 H33 Cl2 N4 O4 V
Title of publication	A trigonal prismatic coordination geometry for vanadium in bis(2-oxidonaphthalene-1-carbaldehyde benzoylhydrazonato)vanadium(IV) dichloromethane hexane hemisolvate
Authors of publication	Gao, Shan; Huo, Li-Hua; Zhao, Hui; Ng, Seik Weng
Journal of publication	Acta Crystallographica Section E
Year of publication	2005
Journal volume	61
Journal issue	3
Pages of publication	m519 - m521
a	12.598 ± 0.003 Å
b	13.021 ± 0.003 Å
c	13.652 ± 0.003 Å
α	116.04 ± 0.03°
β	101.84 ± 0.03°
γ	106.21 ± 0.03°
Cell volume	1787.3 ± 1.2 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.077
Residual factor for significantly intense reflections	0.056
Weighted residual factors for significantly intense reflections	0.16
Weighted residual factors for all reflections included in the refinement	0.174
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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