#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:20 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180989 $ #$URL: svn://www.crystallography.net/cod/hkl/2/20/69/2206920.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206920_Fobs loop_ _publ_author_name 'Anjum, Shazia' 'Choudhary, M. Iqbal' 'Ali, Shamsher' 'Fun, Hoong-Kun' Atta-ur-Rahman _publ_section_title ; 2-(Methoxycarbonyl)succinanilic acid ; _journal_coeditor_code CI6655 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3520 _journal_page_last o3522 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.001 _cell_angle_gamma 90.000 _cell_length_a 18.3008 _cell_length_b 12.1788 _cell_length_c 10.8967 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.7965 _cod_data_source_file ci6655Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ncr1pm in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 234.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1809.90 1651.74 24.27 o 4 0 0 26973.53 22023.48 465.20 o 6 0 0 34210.81 26724.00 1470.61 o 8 0 0 2657.90 2673.28 38.81 o 10 0 0 513.00 560.39 9.17 o 12 0 0 1980.44 2073.38 30.87 o 14 0 0 25.85 22.76 1.40 o 16 0 0 0.08 0.00 1.15 o 18 0 0 25.11 26.75 2.76 o 20 0 0 32.16 39.82 3.50 o 22 0 0 11.57 7.75 2.18 o 1 1 0 775.82 804.67 7.47 o 3 1 0 11190.11 10559.32 247.16 o 5 1 0 1813.79 1893.06 15.64 o 7 1 0 3037.37 3331.92 30.12 o 9 1 0 302.77 307.90 3.33 o 11 1 0 620.75 648.62 7.35 o 13 1 0 628.23 626.47 8.73 o 15 1 0 434.92 408.96 6.37 o 17 1 0 0.17 0.74 0.79 o 19 1 0 1.29 0.66 1.32 o 21 1 0 128.83 126.85 6.64 o 2 2 0 4823.54 4577.52 45.65 o 4 2 0 4838.08 4631.32 41.86 o 6 2 0 3889.39 4039.70 36.37 o 8 2 0 1009.02 1051.29 9.90 o 10 2 0 61.29 62.40 1.45 o 12 2 0 305.86 287.82 5.04 o 14 2 0 474.07 538.21 7.84 o 16 2 0 14.73 15.77 1.17 o 18 2 0 35.64 37.35 2.22 o 20 2 0 84.86 95.43 7.11 o 22 2 0 25.54 17.57 2.08 o 1 3 0 30503.97 31211.95 1173.64 o 3 3 0 262.70 269.26 3.09 o 5 3 0 12914.42 12794.81 115.58 o 7 3 0 989.02 963.45 9.11 o 9 3 0 2538.35 2743.96 25.04 o 11 3 0 375.07 395.87 4.82 o 13 3 0 417.85 419.84 6.32 o 15 3 0 27.27 30.48 1.46 o 17 3 0 10.77 14.22 1.29 o 19 3 0 3.37 3.61 1.18 o 21 3 0 26.30 25.78 3.03 o 0 4 0 5470.59 5710.32 269.24 o 2 4 0 2732.73 3004.89 27.19 o 4 4 0 352.49 361.34 3.67 o 6 4 0 7.57 4.65 0.37 o 8 4 0 163.75 132.57 1.89 o 10 4 0 23.12 26.39 1.04 o 12 4 0 570.01 563.15 6.73 o 14 4 0 185.89 168.84 3.36 o 16 4 0 217.16 245.09 4.54 o 18 4 0 93.06 96.13 2.73 o 20 4 0 225.47 226.83 6.13 o 22 4 0 0.06 -0.85 2.84 o 1 5 0 129.57 91.20 1.23 o 3 5 0 12335.74 13222.18 164.01 o 5 5 0 3872.36 4357.70 39.32 o 7 5 0 138.29 140.91 1.83 o 9 5 0 2024.29 2153.74 19.92 o 11 5 0 435.59 479.59 5.24 o 13 5 0 67.23 56.26 1.77 o 15 5 0 10.99 10.84 1.01 o 17 5 0 35.27 39.55 1.73 o 19 5 0 42.89 45.11 3.10 o 21 5 0 32.14 36.91 2.52 o 0 6 0 342.49 311.18 7.02 o 2 6 0 87.02 54.22 0.96 o 4 6 0 294.30 341.12 3.64 o 6 6 0 242.19 230.69 2.70 o 8 6 0 0.03 0.65 0.32 o 10 6 0 25.49 18.07 0.75 o 12 6 0 243.36 220.94 3.33 o 14 6 0 296.09 300.54 5.16 o 16 6 0 201.18 213.11 4.24 o 18 6 0 66.24 62.18 3.92 o 20 6 0 161.91 183.52 4.28 o 1 7 0 90.84 107.20 1.50 o 3 7 0 828.87 915.63 8.83 o 5 7 0 113.95 129.60 2.97 o 7 7 0 374.70 415.83 4.49 o 9 7 0 297.63 319.29 3.70 o 11 7 0 0.72 0.65 0.41 o 13 7 0 27.86 21.73 1.06 o 15 7 0 6.06 8.98 1.03 o 17 7 0 74.78 72.42 2.66 o 19 7 0 14.97 15.35 1.39 o 0 8 0 359.39 325.54 4.55 o 2 8 0 0.87 3.97 0.58 o 4 8 0 1383.21 1459.43 13.80 o 6 8 0 1470.69 1539.59 14.57 o 8 8 0 169.93 189.52 2.53 o 10 8 0 7.42 6.69 0.58 o 12 8 0 968.93 995.51 11.43 o 14 8 0 36.59 32.61 1.63 o 16 8 0 439.01 454.24 7.41 o 18 8 0 1.45 3.36 1.38 o 1 9 0 18.30 19.24 0.88 o 3 9 0 3.92 2.97 0.53 o 5 9 0 609.74 575.89 6.93 o 7 9 0 39.00 38.37 1.29 o 9 9 0 332.07 347.50 4.12 o 11 9 0 250.56 240.10 3.22 o 13 9 0 242.02 255.64 4.53 o 15 9 0 48.01 46.20 2.27 o 17 9 0 0.47 2.08 1.00 o 0 10 0 365.83 372.68 9.03 o 2 10 0 876.13 905.51 10.32 o 4 10 0 920.96 919.57 11.93 o 6 10 0 468.01 451.38 6.58 o 8 10 0 441.82 428.19 6.40 o 10 10 0 36.88 35.46 1.52 o 12 10 0 160.06 168.06 4.49 o 14 10 0 88.19 87.35 5.07 o 16 10 0 7.82 12.45 2.47 o 1 11 0 168.91 142.98 3.42 o 3 11 0 105.67 94.27 2.68 o 5 11 0 368.99 323.51 6.11 o 7 11 0 5.17 4.72 0.94 o 9 11 0 4.28 3.65 0.77 o 11 11 0 481.68 483.35 9.42 o 13 11 0 24.34 29.93 2.04 o 15 11 0 3.96 4.86 2.02 o 0 12 0 675.66 612.50 14.57 o 2 12 0 286.20 303.34 5.96 o 4 12 0 28.16 37.74 1.80 o 6 12 0 16.78 20.59 1.41 o 8 12 0 21.96 22.48 1.51 o 10 12 0 125.80 146.83 3.80 o 12 12 0 22.46 21.68 2.39 o 1 13 0 18.91 12.03 1.25 o 3 13 0 4.98 4.14 0.93 o 5 13 0 36.50 26.75 1.90 o 7 13 0 10.32 17.44 1.48 o 9 13 0 42.69 48.23 5.94 o 11 13 0 8.74 7.30 1.73 o 0 14 0 99.16 108.01 4.74 o 2 14 0 0.01 1.89 0.89 o 4 14 0 51.66 53.33 2.38 o 6 14 0 18.17 8.18 2.16 o 8 14 0 33.71 40.74 2.41 o 1 15 0 3.00 3.82 1.17 o 3 15 0 7.59 6.99 1.30 o -21 1 1 24.32 23.58 2.14 o -19 1 1 68.71 76.72 4.70 o -17 1 1 75.80 77.01 3.65 o -15 1 1 48.09 40.80 1.59 o -13 1 1 114.72 122.35 2.19 o -11 1 1 1000.34 1069.68 11.65 o -9 1 1 557.98 552.34 5.47 o -7 1 1 37.55 50.98 0.82 o -5 1 1 255.09 270.11 2.44 o -3 1 1 756.88 655.00 5.52 o -1 1 1 510.02 569.71 5.89 o 1 1 1 2.08 -0.78 0.39 o 3 1 1 409.04 507.55 8.45 o 5 1 1 1836.99 1827.58 18.86 o 7 1 1 526.10 476.92 5.44 o 9 1 1 31.54 21.32 0.76 o 11 1 1 11.93 22.06 3.11 o 13 1 1 27.94 28.56 1.83 o 15 1 1 229.77 223.58 5.35 o 17 1 1 5.31 6.26 1.18 o 19 1 1 6.47 4.71 1.16 o 21 1 1 29.74 36.09 2.36 o -22 2 1 40.15 51.55 4.06 o -20 2 1 144.00 140.82 3.52 o -18 2 1 5.19 4.75 1.64 o -16 2 1 230.48 199.52 3.88 o -14 2 1 259.48 228.24 4.03 o -12 2 1 1512.76 1591.79 17.00 o -10 2 1 801.23 722.03 7.05 o -8 2 1 1175.38 1324.36 11.13 o -6 2 1 1372.27 1300.62 10.86 o -4 2 1 52.74 25.98 0.73 o -2 2 1 12822.65 12387.51 304.63 o 0 2 1 752.46 705.77 7.44 o 2 2 1 849.69 868.58 8.07 o 4 2 1 186.97 210.97 2.26 o 6 2 1 2282.22 2364.95 21.58 o 8 2 1 935.02 905.34 9.83 o 10 2 1 1776.00 1782.45 18.77 o 12 2 1 858.19 925.27 10.33 o 14 2 1 51.22 52.87 2.29 o 16 2 1 317.26 292.01 6.59 o 18 2 1 8.67 8.92 1.37 o 20 2 1 1.15 0.43 0.99 o 22 2 1 4.08 4.29 1.35 o -21 3 1 96.45 98.41 3.00 o -19 3 1 0.40 0.38 0.76 o -17 3 1 10.90 9.04 1.20 o -15 3 1 498.03 490.82 7.35 o -13 3 1 170.99 180.92 3.36 o -11 3 1 10.73 8.41 0.58 o -9 3 1 6208.34 6480.19 64.49 o -7 3 1 64.20 53.99 1.48 o -5 3 1 359.52 338.51 3.40 o -3 3 1 15249.48 15295.40 267.77 o -1 3 1 562.88 528.71 5.71 o 1 3 1 3937.86 3763.64 34.08 o 3 3 1 317.52 376.36 3.74 o 5 3 1 2.83 2.32 0.30 o 7 3 1 712.71 715.21 6.98 o 9 3 1 325.20 305.94 4.88 o 11 3 1 0.46 2.28 0.45 o 13 3 1 266.46 281.03 5.47 o 15 3 1 155.26 134.04 3.91 o 17 3 1 1.82 3.28 1.02 o 19 3 1 31.49 27.76 2.05 o 21 3 1 25.02 25.28 2.20 o -22 4 1 1.40 1.78 2.02 o -20 4 1 5.19 4.55 0.97 o -18 4 1 43.31 44.03 1.95 o -16 4 1 16.15 14.33 1.14 o -14 4 1 274.51 265.42 4.56 o -12 4 1 20.56 18.99 1.67 o -10 4 1 34.44 43.95 1.40 o -8 4 1 1053.46 1026.59 10.08 o -6 4 1 2599.86 2956.21 26.83 o -4 4 1 5295.33 5536.74 50.00 o -2 4 1 5043.71 5265.75 47.54 o 0 4 1 2007.28 2211.31 20.18 o 2 4 1 2200.18 2265.86 20.60 o 4 4 1 158.44 150.65 1.80 o 6 4 1 12.81 3.47 0.32 o 8 4 1 0.46 0.27 0.28 o 10 4 1 1295.11 1308.21 12.48 o 12 4 1 34.44 40.19 1.18 o 14 4 1 627.58 604.25 11.46 o 16 4 1 32.31 33.81 3.59 o 18 4 1 2.81 5.56 1.21 o 20 4 1 13.92 24.31 2.51 o -21 5 1 76.48 84.16 2.76 o -19 5 1 15.72 19.57 1.44 o -17 5 1 16.60 15.95 1.24 o -15 5 1 678.50 671.35 9.63 o -13 5 1 257.76 267.93 4.54 o -11 5 1 704.98 733.56 8.38 o -9 5 1 1343.88 1370.28 12.90 o -7 5 1 53.58 50.61 0.94 o -5 5 1 1682.85 1839.01 16.92 o -3 5 1 1222.85 1191.82 11.14 o -1 5 1 8837.36 9205.13 93.69 o 1 5 1 139.81 134.94 1.81 o 3 5 1 4383.89 4589.59 41.42 o 5 5 1 4054.35 4534.26 40.94 o 7 5 1 770.08 755.84 7.44 o 9 5 1 2467.58 2519.89 23.28 o 11 5 1 83.36 85.46 1.52 o 13 5 1 65.58 63.75 1.92 o 15 5 1 2.59 2.60 0.70 o 17 5 1 0.03 1.69 0.99 o 19 5 1 7.68 7.87 1.43 o 21 5 1 4.67 9.46 1.63 o -20 6 1 5.80 8.06 1.16 o -18 6 1 49.86 47.26 2.06 o -16 6 1 1.57 3.02 0.80 o -14 6 1 900.73 944.85 12.80 o -12 6 1 163.19 172.92 3.64 o -10 6 1 246.89 227.39 2.78 o -8 6 1 18.10 13.74 0.87 o -6 6 1 32.89 24.89 0.71 o -4 6 1 1405.84 1480.55 13.80 o -2 6 1 81.21 94.84 1.38 o 0 6 1 4451.86 5166.67 46.51 o 2 6 1 503.11 502.82 5.06 o 4 6 1 2430.51 2808.85 25.62 o 6 6 1 845.58 829.95 8.12 o 8 6 1 7.21 5.91 0.50 o 10 6 1 0.15 1.32 0.39 o 12 6 1 287.74 300.57 3.67 o 14 6 1 54.43 51.91 1.84 o 16 6 1 69.55 85.66 2.53 o 18 6 1 25.63 31.53 3.32 o 20 6 1 35.24 48.74 2.81 o -19 7 1 0.00 -0.29 0.89 o -17 7 1 216.06 212.79 4.37 o -15 7 1 46.73 49.42 1.88 o -13 7 1 88.50 84.06 2.29 o -11 7 1 130.46 149.40 2.53 o -9 7 1 1266.63 1196.61 11.52 o -7 7 1 1825.89 1865.31 17.40 o -5 7 1 576.40 587.51 5.96 o -3 7 1 2049.34 2042.17 18.89 o -1 7 1 2329.79 2593.20 26.20 o 1 7 1 289.59 235.86 2.65 o 3 7 1 842.65 936.16 9.01 o 5 7 1 740.64 794.34 7.84 o 7 7 1 40.96 54.77 1.14 o 9 7 1 65.57 57.10 1.88 o 11 7 1 145.87 148.03 2.24 o 13 7 1 0.43 0.93 0.57 o 15 7 1 240.31 261.17 4.85 o 17 7 1 11.73 13.03 1.82 o 19 7 1 144.86 157.76 5.06 o -18 8 1 48.11 43.72 2.42 o -16 8 1 37.04 38.39 2.43 o -14 8 1 1048.32 1112.95 18.14 o -12 8 1 5.12 3.68 0.70 o -10 8 1 295.61 297.80 3.59 o -8 8 1 634.05 691.56 7.07 o -6 8 1 410.21 412.75 4.50 o -4 8 1 695.57 688.01 6.93 o -2 8 1 992.06 984.86 9.58 o 0 8 1 366.52 392.15 4.83 o 2 8 1 299.64 305.89 4.01 o 4 8 1 649.06 634.53 6.45 o 6 8 1 26.21 21.85 0.79 o 8 8 1 63.72 55.30 1.23 o 10 8 1 309.43 297.32 3.68 o 12 8 1 35.63 27.46 1.05 o 14 8 1 0.96 1.67 0.78 o 16 8 1 0.06 0.29 0.95 o 18 8 1 52.49 56.30 5.48 o -17 9 1 17.67 21.36 1.79 o -15 9 1 4.25 3.65 1.09 o -13 9 1 6.54 7.21 1.20 o -11 9 1 2.55 4.87 0.91 o -9 9 1 18.03 13.80 0.80 o -7 9 1 832.74 812.05 10.63 o -5 9 1 72.20 63.90 1.45 o -3 9 1 792.66 810.67 8.96 o -1 9 1 95.64 82.01 1.49 o 1 9 1 40.86 45.12 1.27 o 3 9 1 0.89 3.85 0.56 o 5 9 1 278.26 281.47 3.97 o 7 9 1 1196.28 1231.96 13.70 o 9 9 1 88.51 65.77 1.72 o 11 9 1 1212.20 1385.18 15.44 o 13 9 1 146.35 137.89 3.37 o 15 9 1 0.00 0.82 1.02 o 17 9 1 82.80 96.36 3.83 o -16 10 1 0.00 1.28 1.40 o -14 10 1 19.01 18.71 2.80 o -12 10 1 268.08 281.51 9.48 o -10 10 1 9.01 3.44 0.78 o -8 10 1 1637.92 1693.85 20.94 o -6 10 1 26.17 39.03 1.94 o -4 10 1 1313.46 1260.22 15.89 o -2 10 1 0.00 -0.21 0.55 o 0 10 1 80.65 71.50 1.86 o 2 10 1 41.79 29.74 1.31 o 4 10 1 149.35 117.57 2.59 o 6 10 1 181.09 159.34 3.15 o 8 10 1 253.71 247.64 3.82 o 10 10 1 0.01 0.62 0.65 o 12 10 1 174.59 155.88 4.37 o 14 10 1 3.64 7.13 2.02 o 16 10 1 64.10 77.54 4.99 o -15 11 1 32.04 37.35 3.71 o -13 11 1 5.72 4.16 1.73 o -11 11 1 55.11 64.37 2.71 o -9 11 1 151.16 153.85 4.69 o -7 11 1 9.18 10.20 0.93 o -5 11 1 158.66 146.31 3.02 o -3 11 1 381.61 302.81 4.93 o -1 11 1 9.05 7.62 0.83 o 1 11 1 1.93 0.21 0.60 o 3 11 1 0.04 0.41 0.62 o 5 11 1 0.03 0.11 1.36 o 7 11 1 38.99 39.80 3.52 o 9 11 1 185.65 185.06 9.90 o 11 11 1 79.16 89.99 5.13 o 13 11 1 0.46 -0.66 1.07 o -14 12 1 0.37 -1.11 1.20 o -12 12 1 0.25 -1.11 0.84 o -10 12 1 0.55 -0.21 0.64 o -8 12 1 0.75 1.15 0.74 o -6 12 1 47.01 43.39 1.94 o -4 12 1 21.50 24.14 4.18 o -2 12 1 305.44 250.63 7.69 o 0 12 1 212.67 194.92 4.39 o 2 12 1 1.26 1.10 0.84 o 4 12 1 179.09 145.18 3.71 o 6 12 1 347.36 325.52 6.41 o 8 12 1 28.06 23.84 1.57 o 10 12 1 88.52 95.89 3.07 o 12 12 1 23.23 27.37 2.72 o -11 13 1 75.69 88.71 4.45 o -9 13 1 133.55 133.03 3.70 o -7 13 1 16.50 17.03 1.44 o -5 13 1 47.30 54.14 2.76 o -3 13 1 42.97 35.15 1.79 o -1 13 1 1.73 3.72 1.96 o 1 13 1 1.50 3.11 0.86 o 3 13 1 0.79 -0.54 0.70 o 5 13 1 5.92 8.22 1.17 o 7 13 1 0.20 0.45 0.74 o 9 13 1 4.43 5.69 1.67 o 11 13 1 51.64 61.05 3.79 o -8 14 1 33.30 46.27 5.54 o -6 14 1 2.11 4.13 1.10 o -4 14 1 23.50 26.01 1.75 o -2 14 1 70.26 69.82 3.63 o 0 14 1 6.35 6.81 1.13 o 2 14 1 7.65 9.64 1.28 o 4 14 1 17.63 26.15 1.73 o 6 14 1 32.79 39.97 3.87 o 8 14 1 38.09 49.77 5.11 o -3 15 1 0.51 3.58 1.11 o -1 15 1 37.03 52.37 2.51 o 1 15 1 0.86 0.74 1.02 o 3 15 1 17.64 19.52 1.66 o -22 0 2 119.22 147.26 7.01 o -20 0 2 57.21 46.33 2.40 o -18 0 2 1230.74 1245.10 20.08 o -16 0 2 1617.66 1685.88 25.98 o -14 0 2 36.14 44.88 1.81 o -12 0 2 3272.01 3346.13 48.77 o -10 0 2 1202.37 1146.73 17.42 o -8 0 2 3259.21 3424.40 49.43 o -6 0 2 10587.13 11436.89 164.44 o -4 0 2 4.02 -0.47 0.24 o -2 0 2 3917.98 3948.41 83.85 o 0 0 2 717.28 742.62 16.23 o 2 0 2 10193.86 9760.11 207.93 o 6 0 2 30794.72 31375.56 664.97 o 8 0 2 12877.19 13380.26 283.94 o 10 0 2 640.88 637.04 15.65 o 12 0 2 731.31 699.99 17.30 o 14 0 2 333.28 420.04 11.80 o 16 0 2 614.97 625.41 16.55 o 18 0 2 0.52 1.98 1.40 o 20 0 2 31.61 38.95 3.38 o 22 0 2 0.14 0.74 1.61 o -21 1 2 170.74 180.22 4.16 o -19 1 2 3.65 4.33 0.80 o -17 1 2 114.17 114.23 2.40 o -15 1 2 419.37 417.76 5.45 o -13 1 2 605.81 577.66 6.88 o -11 1 2 250.74 237.26 4.12 o -9 1 2 2449.43 2691.63 27.66 o -7 1 2 2332.80 2371.70 21.56 o -5 1 2 77.61 80.47 1.20 o -3 1 2 2374.13 2192.23 19.98 o -1 1 2 29447.29 25903.69 1674.03 o 1 1 2 11120.14 11592.39 139.04 o 3 1 2 54860.60 51448.09 2716.12 o 5 1 2 24751.56 25235.08 300.57 o 7 1 2 62.36 80.49 1.81 o 9 1 2 2795.88 2953.56 35.81 o 11 1 2 840.14 777.88 11.97 o 13 1 2 385.09 361.46 5.66 o 15 1 2 90.56 91.33 3.13 o 17 1 2 202.48 163.88 7.24 o 19 1 2 39.41 39.53 2.32 o 21 1 2 10.54 8.79 1.53 o -22 2 2 118.44 128.85 4.51 o -20 2 2 3.52 4.71 1.16 o -18 2 2 1080.89 1075.20 14.70 o -16 2 2 117.64 109.87 2.27 o -14 2 2 18.56 18.73 0.91 o -12 2 2 367.62 346.99 4.46 o -10 2 2 514.81 621.93 6.17 o -8 2 2 1264.35 1300.80 10.95 o -6 2 2 900.30 964.64 8.16 o -4 2 2 634.30 538.27 4.65 o -2 2 2 2161.68 1933.43 17.70 o 0 2 2 13250.08 13606.03 235.84 o 2 2 2 27842.22 27501.67 319.33 o 4 2 2 197.91 163.98 2.61 o 6 2 2 15904.35 16312.61 210.33 o 8 2 2 831.10 764.22 10.06 o 10 2 2 142.05 155.71 3.42 o 12 2 2 748.66 720.07 9.84 o 14 2 2 167.07 155.66 4.20 o 16 2 2 67.42 46.23 2.34 o 18 2 2 52.39 59.09 4.53 o 20 2 2 1.07 0.71 0.97 o 22 2 2 0.02 0.73 1.08 o -21 3 2 20.36 19.18 1.50 o -19 3 2 10.77 12.74 1.22 o -17 3 2 514.68 543.89 10.65 o -15 3 2 489.03 472.07 7.15 o -13 3 2 8.59 6.28 0.62 o -11 3 2 1021.70 960.28 10.59 o -9 3 2 2215.43 2411.62 20.00 o -7 3 2 391.99 384.81 3.52 o -5 3 2 4635.86 5088.22 41.61 o -3 3 2 4317.34 4303.33 35.31 o -1 3 2 1045.08 1044.22 12.51 o 1 3 2 15.60 13.07 0.48 o 3 3 2 86.21 105.00 1.57 o 5 3 2 57.34 55.33 1.22 o 7 3 2 1402.40 1401.89 17.48 o 9 3 2 1291.81 1270.05 16.11 o 11 3 2 264.11 256.99 4.26 o 13 3 2 15.90 14.22 1.28 o 15 3 2 338.85 338.75 7.31 o 17 3 2 137.82 121.03 4.12 o 19 3 2 14.75 19.79 1.87 o 21 3 2 10.09 9.66 2.56 o -22 4 2 0.00 1.58 0.91 o -20 4 2 44.63 51.11 2.12 o -18 4 2 286.60 303.80 5.47 o -16 4 2 15.32 12.72 1.06 o -14 4 2 510.56 518.17 8.82 o -12 4 2 891.59 973.20 12.78 o -10 4 2 1.80 4.14 0.43 o -8 4 2 1232.01 1467.11 12.37 o -6 4 2 1071.98 1138.33 9.64 o -4 4 2 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