Crystallography Open Database

Information card for entry 2214274

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Structure parameters

Chemical name	Chlorido(1-pyrrolidinecarbodithioato-κ^2^S,S')(triphenylphosphine- κP)nickel(II) chloroform hemisolvate
Formula	C47 H47 Cl5 N2 Ni2 P2 S4
Calculated formula	C47 H47 Cl5 N2 Ni2 P2 S4
Title of publication	Chlorido(1-pyrrolidinecarbodithioato-κ^2^<i>S</i>,<i>S</i>')(triphenylphosphine-κ<i>P</i>)nickel(II) chloroform hemisolvate
Authors of publication	Kropidłowska, Anna; Janczak, Jan; Gołaszewska, Jolanta; Becker, Barbara
Journal of publication	Acta Crystallographica Section E
Year of publication	2007
Journal volume	63
Journal issue	7
Pages of publication	m1947 - m1947
a	9.713 ± 0.002 Å
b	10.076 ± 0.002 Å
c	14.509 ± 0.003 Å
α	90.37 ± 0.02°
β	91.21 ± 0.02°
γ	117.39 ± 0.02°
Cell volume	1260.3 ± 0.5 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1597
Residual factor for significantly intense reflections	0.0577
Weighted residual factors for significantly intense reflections	0.1072
Weighted residual factors for all reflections included in the refinement	0.119
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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