#------------------------------------------------------------------------------ #$Date: 2011-09-16 16:46:08 +0100 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: svn://www.crystallography.net/cod/hkl/2/2214466.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214466_Fobs loop_ _publ_author_name 'Li, Zong-Sheng' 'Chai, Jian-She' _publ_section_title ; Bis[diaquahydrogen(1+)] naphthalene-1,5-disulfonate ; _journal_coeditor_code ZL2026 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3258 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.362 _cell_angle_gamma 90.000 _cell_length_a 11.4131 _cell_length_b 9.0543 _cell_length_c 7.1957 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file zl2026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.30 0.00 0.92 o 2 0 0 1757.76 2135.70 95.42 o 4 0 0 125.79 86.74 4.32 o 5 0 0 8561.41 11725.52 462.41 o 6 0 0 40.72 61.31 4.22 o 7 0 0 13.14 20.92 1.67 o 8 0 0 77.30 58.70 3.39 o 9 0 0 129.58 109.11 5.64 o 10 0 0 179.37 166.76 12.20 o 11 0 0 321.52 357.04 28.87 o 12 0 0 0.77 3.05 1.37 o 13 0 0 381.97 392.40 26.82 o 14 0 0 2.88 2.76 1.02 o 1 1 0 2134.58 0.76 0.71 o 2 1 0 21.70 33.01 1.10 o 3 1 0 2098.29 2224.12 62.20 o 4 1 0 1330.05 1391.59 42.88 o 5 1 0 242.43 290.31 9.55 o 6 1 0 553.97 573.32 14.83 o 7 1 0 296.65 328.64 10.66 o 8 1 0 172.88 183.15 6.27 o 9 1 0 168.82 176.96 6.08 o 10 1 0 20.40 17.43 1.24 o 11 1 0 83.80 71.94 3.48 o 12 1 0 10.06 10.30 2.09 o 13 1 0 41.68 40.33 2.10 o 14 1 0 26.32 19.03 1.77 o 0 2 0 165.44 64.16 8.90 o 1 2 0 223.25 212.92 17.19 o 2 2 0 6230.51 8052.59 174.89 o 3 2 0 1975.52 2128.70 43.99 o 4 2 0 3.82 2.60 0.33 o 5 2 0 59.18 59.43 1.68 o 6 2 0 275.25 286.88 7.42 o 7 2 0 18.10 16.72 0.84 o 8 2 0 263.96 267.95 7.20 o 9 2 0 319.01 353.80 10.30 o 10 2 0 384.30 357.42 11.72 o 11 2 0 115.52 116.49 4.78 o 12 2 0 0.80 0.76 0.58 o 13 2 0 192.51 170.29 7.80 o 14 2 0 138.78 144.61 6.51 o 1 3 0 215.84 182.76 3.89 o 2 3 0 217.41 229.97 4.10 o 3 3 0 1146.68 1162.02 25.04 o 4 3 0 330.99 399.60 7.47 o 5 3 0 1826.93 1917.28 42.08 o 6 3 0 790.94 811.70 19.93 o 7 3 0 221.58 206.54 11.38 o 8 3 0 1260.22 1330.59 41.62 o 9 3 0 684.57 710.89 21.41 o 10 3 0 355.22 370.85 11.19 o 11 3 0 150.33 158.00 4.77 o 12 3 0 285.91 333.51 11.83 o 13 3 0 99.68 106.07 4.86 o 14 3 0 203.85 205.39 23.20 o 0 4 0 1918.03 2518.99 71.69 o 1 4 0 85.93 97.19 2.00 o 2 4 0 436.89 431.11 9.89 o 3 4 0 1035.64 1244.93 26.59 o 4 4 0 5.34 13.68 0.60 o 5 4 0 1.15 0.90 0.19 o 6 4 0 208.33 199.38 3.68 o 7 4 0 1100.70 1084.05 20.27 o 8 4 0 324.97 322.08 7.36 o 9 4 0 77.84 70.83 3.50 o 10 4 0 127.42 130.04 9.70 o 11 4 0 72.09 66.42 2.56 o 12 4 0 125.36 111.90 5.02 o 13 4 0 64.99 65.70 5.30 o 1 5 0 529.76 554.06 13.82 o 2 5 0 0.19 0.79 0.51 o 3 5 0 66.45 65.65 1.84 o 4 5 0 364.57 375.36 8.09 o 5 5 0 0.10 0.13 0.34 o 6 5 0 231.41 226.59 5.52 o 7 5 0 88.44 83.79 3.46 o 8 5 0 50.70 54.75 4.34 o 9 5 0 179.97 172.80 4.48 o 10 5 0 21.92 20.82 0.67 o 11 5 0 4.98 5.34 0.43 o 12 5 0 37.14 39.10 1.86 o 13 5 0 39.39 38.66 5.14 o 0 6 0 617.16 642.35 19.34 o 1 6 0 49.42 43.54 1.14 o 2 6 0 407.58 381.98 7.59 o 3 6 0 288.17 275.11 7.10 o 4 6 0 185.05 201.38 5.20 o 5 6 0 294.65 288.82 9.52 o 6 6 0 1.28 2.95 0.51 o 7 6 0 399.00 403.99 13.48 o 8 6 0 2.76 5.32 0.74 o 9 6 0 110.89 107.85 4.95 o 10 6 0 20.11 20.22 4.12 o 11 6 0 48.43 46.79 2.94 o 12 6 0 20.32 11.66 2.03 o 1 7 0 829.87 881.02 16.31 o 2 7 0 47.29 46.48 1.18 o 3 7 0 1.27 3.40 0.18 o 4 7 0 316.83 293.62 8.77 o 5 7 0 70.43 67.71 2.50 o 6 7 0 397.39 380.45 13.80 o 7 7 0 88.13 82.10 3.47 o 8 7 0 25.67 29.40 1.52 o 9 7 0 20.32 13.95 0.94 o 10 7 0 85.10 90.55 4.48 o 11 7 0 8.05 7.98 1.44 o 0 8 0 385.08 407.84 16.05 o 1 8 0 102.81 97.57 2.47 o 2 8 0 14.13 8.87 0.46 o 3 8 0 86.97 89.84 2.19 o 4 8 0 31.82 31.51 1.40 o 5 8 0 74.17 55.90 2.31 o 6 8 0 4.84 2.84 0.67 o 7 8 0 7.82 8.27 1.14 o 8 8 0 22.92 22.28 1.21 o 9 8 0 9.20 9.12 1.06 o 10 8 0 23.20 25.05 3.95 o 1 9 0 18.51 19.70 0.85 o 2 9 0 13.34 11.69 0.66 o 3 9 0 147.98 149.91 6.13 o 4 9 0 7.97 4.63 0.66 o 5 9 0 183.45 193.72 7.25 o 6 9 0 33.71 31.25 1.59 o 7 9 0 67.66 81.18 3.37 o 8 9 0 279.48 279.47 12.12 o 9 9 0 1.84 -0.25 0.95 o 0 10 0 240.13 256.85 10.83 o 1 10 0 33.30 28.76 1.14 o 2 10 0 107.02 112.88 3.68 o 3 10 0 13.36 13.40 1.13 o 4 10 0 195.78 220.36 7.73 o 5 10 0 31.60 28.65 1.54 o 6 10 0 2.88 2.95 0.82 o 7 10 0 75.07 70.00 3.70 o 1 11 0 6.25 6.73 0.75 o 2 11 0 0.24 1.94 0.75 o 3 11 0 2.25 2.13 0.84 o 4 11 0 5.23 7.55 1.11 o 5 11 0 53.92 52.95 3.35 o -14 1 1 115.69 126.09 6.89 o -13 1 1 47.86 48.04 1.84 o -12 1 1 162.69 188.80 5.76 o -11 1 1 32.73 29.57 1.52 o -10 1 1 432.61 440.90 12.35 o -9 1 1 390.31 395.97 9.27 o -8 1 1 96.80 87.06 2.20 o -7 1 1 986.73 1074.75 26.53 o -6 1 1 314.28 322.45 7.00 o -5 1 1 597.03 571.87 12.15 o -4 1 1 449.45 500.42 10.88 o -3 1 1 547.05 483.89 9.87 o -2 1 1 829.98 885.21 18.29 o 0 1 1 758.58 734.78 28.55 o 1 1 1 2332.45 16.84 3.33 o 2 1 1 409.92 399.06 56.92 o 3 1 1 1621.83 1681.19 43.63 o 4 1 1 4249.27 5278.57 141.23 o 5 1 1 1232.82 1285.68 30.37 o 6 1 1 1709.95 1810.52 44.80 o 7 1 1 1.44 4.31 0.48 o 8 1 1 577.28 588.66 17.24 o 9 1 1 13.16 7.51 0.64 o 10 1 1 218.57 243.05 9.64 o 11 1 1 15.36 11.99 0.89 o 12 1 1 295.75 328.38 11.35 o 13 1 1 17.20 19.47 1.44 o 14 1 1 284.61 321.20 20.75 o -14 2 1 120.50 109.08 5.12 o -13 2 1 95.90 97.82 3.76 o -12 2 1 3.10 3.02 0.47 o -11 2 1 113.38 109.90 2.98 o -10 2 1 81.42 75.79 2.10 o -9 2 1 637.65 652.25 12.67 o -8 2 1 22.20 19.38 0.70 o -7 2 1 312.51 297.61 6.22 o -6 2 1 72.74 61.77 1.60 o -5 2 1 429.38 399.13 7.32 o -4 2 1 250.11 225.61 4.20 o -3 2 1 1963.68 2042.59 32.63 o -2 2 1 4437.83 5290.95 91.13 o -1 2 1 10.06 9.54 0.40 o 0 2 1 3941.22 4757.05 103.80 o 1 2 1 209.89 181.60 3.15 o 2 2 1 4259.09 5085.73 99.72 o 3 2 1 2165.79 2303.48 46.88 o 4 2 1 2.31 0.09 0.22 o 5 2 1 501.11 521.41 12.81 o 6 2 1 60.55 51.21 1.48 o 7 2 1 906.27 902.15 20.87 o 8 2 1 190.08 180.76 4.39 o 9 2 1 65.20 62.47 2.53 o 10 2 1 0.85 -0.44 0.44 o 11 2 1 178.29 179.69 7.93 o 12 2 1 72.16 64.51 4.57 o 13 2 1 268.39 259.93 13.98 o -14 3 1 12.77 8.47 1.57 o -13 3 1 0.07 0.21 0.57 o -12 3 1 0.08 0.73 0.46 o -11 3 1 265.95 283.65 8.60 o -10 3 1 33.74 31.42 1.09 o -9 3 1 9.98 9.98 0.62 o -8 3 1 203.17 204.69 4.27 o -7 3 1 327.46 317.75 6.07 o -6 3 1 1258.67 1365.25 24.23 o -5 3 1 13.33 17.01 1.59 o -4 3 1 73.20 84.76 1.62 o -3 3 1 208.61 211.03 4.17 o -2 3 1 458.79 481.86 9.68 o -1 3 1 17.77 18.21 0.52 o 0 3 1 60.53 51.80 1.22 o 1 3 1 52.31 51.82 1.14 o 2 3 1 1425.23 1604.67 26.67 o 3 3 1 945.13 1096.38 20.32 o 4 3 1 186.83 196.69 3.84 o 5 3 1 139.39 147.29 3.10 o 6 3 1 7.91 11.42 0.95 o 7 3 1 252.16 249.78 9.24 o 8 3 1 196.63 193.27 5.81 o 9 3 1 12.16 15.14 1.06 o 10 3 1 118.37 127.24 4.47 o 11 3 1 18.09 18.21 1.12 o 12 3 1 5.29 7.15 0.86 o 13 3 1 6.73 4.88 1.65 o -13 4 1 98.74 84.13 5.38 o -12 4 1 44.56 46.32 1.66 o -11 4 1 242.23 252.93 6.51 o -10 4 1 16.74 12.39 2.17 o -9 4 1 40.40 44.47 1.26 o -8 4 1 362.51 358.55 8.02 o -7 4 1 319.38 330.61 6.71 o -6 4 1 8.65 7.24 0.50 o -5 4 1 98.46 80.97 3.12 o -4 4 1 218.94 219.53 4.24 o -3 4 1 13.71 7.22 0.66 o -2 4 1 621.81 625.94 12.08 o -1 4 1 631.35 651.49 16.10 o 0 4 1 4369.50 5508.53 132.98 o 1 4 1 343.22 311.02 5.68 o 2 4 1 116.85 112.05 1.92 o 3 4 1 123.67 102.67 2.16 o 4 4 1 178.26 178.46 3.44 o 5 4 1 1403.96 1434.95 26.20 o 6 4 1 98.35 98.37 2.24 o 7 4 1 0.06 0.79 0.59 o 8 4 1 26.45 22.29 0.83 o 9 4 1 310.57 331.04 8.46 o 10 4 1 0.21 0.87 0.55 o 11 4 1 216.82 218.34 6.19 o 12 4 1 3.27 2.86 0.58 o 13 4 1 69.66 63.39 6.58 o -13 5 1 111.05 118.75 6.41 o -12 5 1 75.31 81.34 3.82 o -11 5 1 14.32 14.10 0.95 o -10 5 1 114.39 130.66 2.77 o -9 5 1 3.69 0.88 0.46 o -8 5 1 1718.41 1853.73 55.85 o -7 5 1 94.56 95.49 4.35 o -6 5 1 366.70 352.03 7.30 o -5 5 1 233.74 236.39 5.06 o -4 5 1 292.21 278.43 6.34 o -3 5 1 1069.08 1153.80 23.56 o -2 5 1 133.62 130.13 3.06 o -1 5 1 33.82 24.96 2.18 o 0 5 1 114.95 107.86 3.00 o 1 5 1 52.69 56.61 1.44 o 2 5 1 357.21 396.70 8.11 o 3 5 1 238.10 232.71 5.60 o 4 5 1 117.21 130.23 2.84 o 5 5 1 347.41 336.70 6.89 o 6 5 1 321.69 308.91 6.23 o 7 5 1 1164.67 1208.71 27.26 o 8 5 1 391.65 406.35 11.60 o 9 5 1 3.13 3.25 0.42 o 10 5 1 135.86 140.59 5.33 o 11 5 1 54.50 61.70 2.48 o 12 5 1 199.36 211.82 12.93 o -12 6 1 0.53 0.86 1.24 o -11 6 1 40.04 34.76 2.04 o -10 6 1 0.47 -0.43 0.56 o -9 6 1 12.99 9.69 0.81 o -8 6 1 7.98 6.76 1.16 o -7 6 1 200.30 178.50 5.36 o -6 6 1 0.16 -0.02 0.40 o -5 6 1 71.06 62.39 3.60 o -4 6 1 174.87 173.48 4.70 o -3 6 1 182.90 189.17 4.66 o -2 6 1 0.13 0.46 0.37 o -1 6 1 23.21 22.72 0.91 o 0 6 1 127.80 117.85 3.14 o 1 6 1 15.59 18.20 0.82 o 2 6 1 111.99 129.04 3.29 o 3 6 1 262.79 275.57 6.42 o 4 6 1 234.85 225.92 7.65 o 5 6 1 191.06 153.22 5.32 o 6 6 1 57.37 43.07 3.39 o 7 6 1 4.28 3.59 0.49 o 8 6 1 21.55 22.20 1.26 o 9 6 1 96.08 89.44 3.22 o 10 6 1 0.00 0.47 0.32 o 11 6 1 2.42 1.79 0.86 o 12 6 1 65.48 52.61 3.98 o -11 7 1 70.75 57.57 4.22 o -10 7 1 63.25 69.35 2.94 o -9 7 1 2.90 2.83 0.65 o -8 7 1 195.02 188.53 6.99 o -7 7 1 56.13 44.66 1.93 o -6 7 1 411.92 427.56 11.76 o -5 7 1 406.58 385.30 12.03 o -4 7 1 9.39 7.49 1.00 o -3 7 1 359.28 370.38 10.08 o -2 7 1 251.87 274.49 6.08 o -1 7 1 21.65 19.88 0.78 o 0 7 1 306.04 310.75 8.87 o 1 7 1 127.22 131.71 3.09 o 2 7 1 141.17 148.90 3.53 o 3 7 1 63.78 55.00 1.57 o 4 7 1 45.46 41.38 1.73 o 5 7 1 124.40 130.44 4.35 o 6 7 1 123.30 107.30 3.78 o 7 7 1 30.02 25.31 1.57 o 8 7 1 34.69 34.08 1.89 o 9 7 1 6.99 8.56 1.85 o 10 7 1 116.62 116.79 7.07 o 11 7 1 11.39 8.13 1.79 o -10 8 1 0.06 -0.95 0.95 o -9 8 1 158.32 164.22 8.12 o -8 8 1 0.04 0.62 0.61 o -7 8 1 232.25 239.28 9.38 o -6 8 1 75.30 76.76 2.88 o -5 8 1 507.66 502.31 19.38 o -4 8 1 17.00 21.70 2.07 o -3 8 1 19.38 17.55 1.04 o -2 8 1 1187.98 1298.11 30.54 o -1 8 1 0.14 0.73 0.36 o 0 8 1 438.56 438.28 10.15 o 1 8 1 71.96 77.48 2.37 o 2 8 1 147.22 164.51 4.45 o 3 8 1 456.57 426.54 10.82 o 4 8 1 117.89 121.12 5.72 o 5 8 1 46.62 44.26 2.56 o 6 8 1 88.56 83.70 3.29 o 7 8 1 216.19 222.81 10.28 o 8 8 1 19.12 21.37 1.39 o 9 8 1 28.04 25.17 4.45 o 10 8 1 10.26 8.81 2.49 o -9 9 1 39.72 41.46 3.71 o -8 9 1 0.33 0.53 0.64 o -7 9 1 0.04 -0.25 0.66 o -6 9 1 13.96 12.04 1.94 o -5 9 1 4.15 3.88 0.63 o -4 9 1 0.49 2.13 0.73 o -3 9 1 28.53 27.22 1.51 o -2 9 1 97.31 94.48 2.81 o -1 9 1 194.35 197.68 4.61 o 0 9 1 25.43 25.16 0.96 o 1 9 1 316.46 342.38 8.22 o 2 9 1 38.15 37.49 1.17 o 3 9 1 7.28 7.55 0.47 o 4 9 1 145.58 150.11 4.95 o 5 9 1 0.78 0.65 0.75 o 6 9 1 88.94 87.25 3.95 o 7 9 1 5.73 3.13 1.01 o 8 9 1 10.53 13.48 2.39 o -7 10 1 11.27 12.43 1.28 o -6 10 1 25.12 24.59 1.52 o -5 10 1 20.17 30.30 1.59 o -4 10 1 68.50 78.44 3.40 o -3 10 1 27.57 29.37 1.56 o -2 10 1 0.54 1.28 0.37 o -1 10 1 0.89 0.73 0.46 o 0 10 1 22.62 25.16 0.96 o 1 10 1 24.15 25.35 0.97 o 2 10 1 17.05 17.63 0.80 o 3 10 1 4.90 3.23 0.73 o 4 10 1 64.54 71.43 3.58 o 5 10 1 0.29 0.46 0.75 o 6 10 1 12.03 9.33 1.41 o 7 10 1 6.38 5.81 1.30 o -5 11 1 50.67 41.98 5.23 o -4 11 1 27.84 27.42 1.71 o -3 11 1 19.43 17.39 1.37 o -2 11 1 10.54 9.57 1.01 o -1 11 1 207.85 243.27 8.12 o 0 11 1 37.27 43.34 2.53 o 1 11 1 46.86 46.97 1.85 o 2 11 1 40.85 41.35 1.98 o 3 11 1 156.50 154.58 6.95 o 4 11 1 47.37 45.79 2.48 o -14 0 2 52.42 50.33 3.69 o -13 0 2 4.17 2.31 0.93 o -12 0 2 40.56 44.25 2.81 o -11 0 2 373.22 387.39 13.72 o -10 0 2 27.11 25.56 1.55 o -9 0 2 15.30 11.05 0.90 o -8 0 2 303.48 312.84 10.62 o -7 0 2 1024.95 1078.75 30.58 o -6 0 2 91.69 120.67 4.23 o -5 0 2 7.83 5.81 0.37 o -4 0 2 45.19 68.20 1.91 o -3 0 2 1132.16 1316.63 33.95 o 0 0 2 3741.84 4332.62 128.70 o 1 0 2 7504.89 10873.33 447.97 o 2 0 2 84.35 81.04 3.65 o 3 0 2 6328.08 8425.93 356.58 o 4 0 2 1090.21 1062.80 48.93 o 5 0 2 3213.28 3366.71 149.41 o 6 0 2 778.83 843.43 36.55 o 7 0 2 127.87 135.79 6.51 o 8 0 2 62.00 77.13 4.23 o 9 0 2 198.98 219.34 13.72 o 10 0 2 51.23 61.85 3.93 o 11 0 2 130.86 140.73 6.63 o 12 0 2 3.04 3.58 0.84 o 13 0 2 166.14 154.88 15.35 o -14 1 2 0.06 0.59 0.79 o -13 1 2 4.85 3.84 0.93 o -12 1 2 81.58 87.75 2.87 o -11 1 2 18.84 22.44 2.49 o -10 1 2 1.02 1.44 0.48 o -9 1 2 12.32 12.70 1.33 o -8 1 2 791.54 860.53 18.61 o -7 1 2 22.40 26.56 1.19 o -6 1 2 76.94 64.90 1.30 o -5 1 2 11.13 9.97 0.39 o -4 1 2 1630.30 1753.49 29.78 o -3 1 2 2185.09 2490.15 41.60 o -2 1 2 996.68 968.87 15.78 o -1 1 2 1093.00 1214.92 20.93 o 0 1 2 424.62 395.11 6.87 o 1 1 2 1422.82 1438.54 23.90 o 2 1 2 482.77 480.60 10.50 o 3 1 2 3.45 9.02 0.55 o 4 1 2 1387.50 1538.58 40.87 o 5 1 2 202.21 206.55 7.23 o 6 1 2 19.02 17.66 0.81 o 7 1 2 7.02 7.50 1.47 o 8 1 2 180.91 183.75 5.22 o 9 1 2 0.38 0.42 0.37 o 10 1 2 16.42 11.19 0.88 o 11 1 2 1.10 0.09 1.01 o 12 1 2 147.99 151.79 7.81 o 13 1 2 6.97 8.03 1.37 o -14 2 2 100.55 94.54 4.24 o -13 2 2 34.36 33.27 2.45 o -12 2 2 7.94 5.56 0.62 o -11 2 2 167.77 176.05 5.10 o -10 2 2 22.16 17.11 0.71 o -9 2 2 149.77 154.26 3.82 o -8 2 2 507.36 541.47 9.12 o -7 2 2 544.80 570.00 11.08 o -6 2 2 139.12 129.47 2.78 o -5 2 2 1010.87 1123.42 19.07 o -4 2 2 179.73 195.80 3.81 o -3 2 2 10.23 6.64 0.28 o -2 2 2 875.34 996.96 14.75 o -1 2 2 440.69 398.17 6.82 o 0 2 2 3.77 4.61 0.26 o 1 2 2 493.77 468.85 11.14 o 2 2 2 1598.55 1619.95 31.14 o 3 2 2 898.40 920.50 17.95 o 4 2 2 9.02 8.67 0.51 o 5 2 2 138.82 127.38 3.17 o 6 2 2 3.47 4.57 0.54 o 7 2 2 1143.50 1161.73 28.43 o 8 2 2 0.22 0.03 0.26 o 9 2 2 0.38 0.49 0.55 o 10 2 2 93.45 97.22 4.69 o 11 2 2 85.86 80.00 3.37 o 12 2 2 96.26 115.71 4.87 o 13 2 2 122.45 132.06 14.15 o -13 3 2 121.96 126.73 4.36 o -12 3 2 79.07 94.28 3.14 o -11 3 2 48.12 52.20 2.63 o -10 3 2 1149.90 1250.15 30.71 o -9 3 2 99.15 102.05 4.45 o -8 3 2 406.82 412.50 8.70 o -7 3 2 271.86 287.02 5.70 o -6 3 2 127.17 111.94 2.34 o -5 3 2 1707.46 1932.76 31.46 o -4 3 2 536.13 600.31 8.99 o -3 3 2 108.42 96.80 1.89 o -2 3 2 38.81 30.09 0.79 o -1 3 2 44.75 29.94 0.85 o 0 3 2 3.19 5.52 0.80 o 1 3 2 245.09 209.43 4.17 o 2 3 2 1007.62 1175.34 18.35 o 3 3 2 1340.19 1283.40 21.91 o 4 3 2 147.30 142.34 2.71 o 5 3 2 988.01 1024.74 23.00 o 6 3 2 1792.58 1926.89 40.66 o 7 3 2 772.40 751.95 17.03 o 8 3 2 215.12 216.91 5.77 o 9 3 2 24.18 27.61 1.54 o 10 3 2 653.11 716.23 25.37 o 11 3 2 132.47 133.47 4.81 o 12 3 2 226.69 242.68 10.97 o 13 3 2 22.46 21.98 2.34 o -13 4 2 126.69 123.21 8.29 o -12 4 2 3.18 1.56 0.49 o -11 4 2 1.95 2.68 0.52 o -10 4 2 165.77 177.91 4.98 o -9 4 2 953.75 956.80 23.62 o -8 4 2 12.58 14.13 1.47 o -7 4 2 423.81 433.29 9.03 o -6 4 2 2.05 1.09 0.24 o -5 4 2 91.27 72.14 1.65 o 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