#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:32:49 +0100 (Sat, 02 Apr 2016) $ #$Revision: 181065 $ #$URL: svn://www.crystallography.net/cod/hkl/2/21/45/2214507.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214507_Fobs loop_ _publ_author_name 'Grigoriev, Mikhail S.' 'Pisareva, Svetlana A.' 'Safiulina, Alfiya M.' 'Nifant'ev, Eduard E.' _publ_section_title ; 1,1,1-Tris[(diphenylphosphoryl)methyl]propane monohydrate ; _journal_coeditor_code BH2120 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3441 _journal_page_last o3442 _journal_volume 63 _journal_year 2007 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.143 _cell_angle_gamma 90.000 _cell_length_a 9.5303 _cell_length_b 10.4028 _cell_length_c 18.0951 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.7109 _cod_data_source_file bh2120Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pp in Pc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l 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101.24 117.33 49.71 o -5 0 -22 27.85 15.01 41.61 o -4 0 -22 845.17 799.71 53.92 o -3 0 -22 174.69 203.19 35.74 o -2 0 -22 501.93 505.84 44.21 o -1 0 -22 235.62 211.07 34.20 o 0 0 -22 387.47 362.75 38.66 o 1 0 -22 420.41 419.63 39.74 o 2 0 -22 109.00 128.85 30.55 o 3 0 -22 962.98 952.61 51.97 o 4 0 -22 302.29 339.09 35.84 o 5 0 -22 88.43 95.18 41.08 o 6 0 -22 53.09 51.85 38.06 o -6 1 -22 87.12 68.98 32.48 o -5 1 -22 128.62 68.73 31.94 o -4 1 -22 144.87 133.81 24.77 o -3 1 -22 81.27 79.99 22.16 o -2 1 -22 71.54 67.60 20.76 o -1 1 -22 384.51 406.39 28.23 o 0 1 -22 472.07 501.72 30.40 o 1 1 -22 3.40 1.76 17.45 o 2 1 -22 62.31 76.42 19.65 o 3 1 -22 97.16 120.89 20.96 o 4 1 -22 78.00 83.51 23.17 o 5 1 -22 101.35 107.03 30.31 o 6 1 -22 58.48 70.40 19.89 o -6 2 -22 0.14 -25.56 28.46 o -5 2 -22 22.86 19.38 24.08 o -4 2 -22 66.89 45.96 25.48 o -3 2 -22 48.75 49.85 21.59 o -2 2 -22 11.35 5.20 18.70 o -1 2 -22 126.46 156.88 23.25 o 0 2 -22 159.48 181.98 23.50 o 1 2 -22 69.67 85.82 20.44 o 2 2 -22 9.57 11.62 17.05 o 3 2 -22 17.55 27.09 18.14 o 4 2 -22 37.46 46.00 21.86 o 5 2 -22 68.57 75.35 28.66 o 6 2 -22 139.68 156.57 31.35 o -6 3 -22 10.59 39.35 31.81 o -5 3 -22 25.51 42.23 25.55 o -4 3 -22 37.37 24.88 24.94 o -3 3 -22 43.98 59.28 21.83 o -2 3 -22 112.25 84.98 22.14 o -1 3 -22 92.48 105.67 21.99 o 0 3 -22 22.78 24.53 19.00 o 1 3 -22 63.49 67.85 20.52 o 2 3 -22 52.49 44.69 19.38 o 3 3 -22 14.74 10.84 21.27 o 4 3 -22 58.82 60.11 23.15 o 5 3 -22 185.17 198.48 27.23 o 6 3 -22 197.77 195.88 40.16 o -5 4 -22 52.06 36.13 26.29 o -4 4 -22 228.55 268.99 33.00 o -3 4 -22 81.18 63.93 26.34 o -2 4 -22 91.19 144.08 23.84 o -1 4 -22 55.52 55.47 20.69 o 0 4 -22 2.56 -4.04 18.91 o 1 4 -22 160.27 181.56 24.47 o 2 4 -22 17.89 38.47 22.76 o 3 4 -22 248.84 263.81 30.33 o 4 4 -22 91.19 89.07 23.74 o 5 4 -22 181.68 211.14 28.81 o -4 5 -22 268.95 282.05 33.88 o -3 5 -22 118.54 104.82 28.39 o -2 5 -22 89.93 105.93 27.04 o -1 5 -22 305.39 289.49 27.50 o 0 5 -22 474.68 486.54 37.76 o 1 5 -22 16.78 32.89 19.31 o 2 5 -22 155.62 155.57 27.15 o 3 5 -22 23.40 28.81 21.82 o 4 5 -22 53.25 53.44 23.29 o -3 6 -22 116.67 111.32 28.60 o -2 6 -22 75.65 62.20 24.83 o -1 6 -22 139.08 153.33 24.18 o 0 6 -22 94.92 97.52 23.10 o 1 6 -22 275.00 239.11 30.88 o 2 6 -22 63.47 49.30 24.06 o 3 6 -22 407.60 372.45 33.64 o -2 7 -22 86.16 94.21 27.41 o -1 7 -22 14.99 7.28 23.30 o 0 7 -22 1.34 -3.27 21.34 o 1 7 -22 46.93 44.68 24.59 o 2 7 -22 24.24 9.72 22.02 o -7 1 -21 113.12 86.91 33.76 o -6 1 -21 314.76 295.31 40.72 o -5 1 -21 178.84 169.66 28.67 o -4 1 -21 159.46 165.32 23.65 o -3 1 -21 58.17 58.88 19.82 o -2 1 -21 226.59 251.92 24.37 o -1 1 -21 299.08 305.47 24.93 o 0 1 -21 99.85 102.20 19.45 o 1 1 -21 119.53 115.42 19.87 o 2 1 -21 3.59 16.68 15.79 o 3 1 -21 237.08 274.40 22.93 o 4 1 -21 114.09 121.19 23.23 o 5 1 -21 145.29 120.14 29.75 o 6 1 -21 67.30 53.26 18.58 o 7 1 -21 4.98 2.32 16.34 o -7 2 -21 45.67 15.24 24.97 o -6 2 -21 365.64 357.73 42.93 o -5 2 -21 664.61 634.92 41.69 o -4 2 -21 86.87 78.88 25.37 o -3 2 -21 175.22 180.75 23.86 o -2 2 -21 4.74 30.22 17.93 o -1 2 -21 744.70 793.09 48.28 o 0 2 -21 177.83 179.39 22.30 o 1 2 -21 33.01 32.60 16.95 o 2 2 -21 116.62 115.20 19.57 o 3 2 -21 229.59 256.56 23.06 o 4 2 -21 42.89 28.06 21.02 o 5 2 -21 157.57 159.86 24.44 o 6 2 -21 209.38 219.27 33.74 o 7 2 -21 138.94 175.63 31.53 o -7 3 -21 6.75 -23.35 23.82 o -6 3 -21 167.32 163.36 30.00 o -5 3 -21 162.84 168.84 29.42 o -4 3 -21 199.64 161.63 28.50 o -3 3 -21 154.96 179.93 23.72 o -2 3 -21 451.86 463.44 29.58 o -1 3 -21 1201.63 1220.87 41.05 o 0 3 -21 225.56 272.37 24.72 o 1 3 -21 130.68 153.42 21.02 o 2 3 -21 201.68 204.96 22.70 o 3 3 -21 143.30 131.06 24.46 o 4 3 -21 388.97 422.14 31.74 o 5 3 -21 135.28 134.25 24.41 o 6 3 -21 526.99 473.96 42.52 o 7 3 -21 18.81 39.48 26.60 o -6 4 -21 137.56 104.47 24.57 o -5 4 -21 171.39 181.13 29.73 o -4 4 -21 51.39 34.91 24.97 o -3 4 -21 11.61 -11.99 21.51 o -2 4 -21 54.64 39.89 19.29 o -1 4 -21 332.25 337.24 28.12 o 0 4 -21 148.11 179.51 22.73 o 1 4 -21 16.72 15.73 18.18 o 2 4 -21 28.36 28.55 17.93 o 3 4 -21 176.61 170.14 25.77 o 4 4 -21 245.85 244.90 28.18 o 5 4 -21 161.28 153.24 25.46 o 6 4 -21 123.87 130.11 30.86 o -6 5 -21 303.57 250.38 33.43 o -5 5 -21 40.54 63.09 26.84 o -4 5 -21 31.59 20.00 24.32 o -3 5 -21 30.00 15.50 23.15 o -2 5 -21 19.58 1.49 18.53 o -1 5 -21 180.43 193.79 23.54 o 0 5 -21 169.33 175.41 24.12 o 1 5 -21 26.75 40.57 19.31 o 2 5 -21 53.60 41.13 21.88 o 3 5 -21 22.22 21.29 20.90 o 4 5 -21 125.71 126.66 24.63 o 5 5 -21 24.42 1.38 20.22 o 6 5 -21 0.19 -0.51 19.65 o -5 6 -21 61.05 54.84 26.74 o -4 6 -21 66.79 65.83 26.01 o -3 6 -21 369.29 336.99 34.24 o -2 6 -21 497.97 458.77 36.39 o -1 6 -21 6.84 8.37 18.78 o 0 6 -21 208.22 205.13 25.22 o 1 6 -21 137.77 147.13 22.96 o 2 6 -21 122.38 126.35 25.64 o 3 6 -21 329.50 357.11 32.71 o 4 6 -21 13.84 9.23 20.81 o 5 6 -21 356.29 356.29 31.69 o -4 7 -21 171.95 162.45 29.95 o -3 7 -21 2.31 11.48 23.47 o -2 7 -21 291.96 246.05 31.73 o -1 7 -21 515.93 531.46 38.77 o 0 7 -21 38.91 17.71 19.96 o 1 7 -21 58.12 97.51 25.26 o 2 7 -21 18.66 17.53 21.18 o 3 7 -21 89.07 85.50 24.58 o 4 7 -21 141.65 132.94 26.54 o -1 8 -21 17.38 12.87 23.74 o 0 8 -21 131.39 139.44 34.47 o 1 8 -21 76.57 89.91 25.16 o -8 0 -20 445.53 394.88 51.53 o -7 0 -20 312.74 279.73 39.07 o -6 0 -20 888.40 818.17 75.69 o -5 0 -20 242.62 237.60 35.71 o -4 0 -20 6.51 0.15 23.16 o -3 0 -20 141.45 138.98 30.55 o -2 0 -20 658.30 634.56 52.89 o -1 0 -20 587.01 566.58 42.69 o 0 0 -20 305.16 281.19 32.56 o 1 0 -20 700.17 704.06 44.25 o 2 0 -20 157.56 164.85 28.75 o 3 0 -20 33.68 19.44 21.92 o 4 0 -20 16.09 24.00 21.81 o 5 0 -20 116.76 75.70 35.79 o 6 0 -20 699.73 751.43 64.60 o 7 0 -20 453.49 465.55 29.50 o 8 0 -20 32.08 48.11 26.67 o -8 1 -20 137.82 106.36 27.89 o -7 1 -20 230.00 218.56 29.95 o -6 1 -20 189.32 188.30 28.64 o -5 1 -20 282.99 252.39 29.97 o -4 1 -20 452.69 453.67 28.96 o -3 1 -20 51.16 64.83 19.10 o -2 1 -20 267.96 282.94 24.66 o -1 1 -20 77.78 50.33 17.61 o 0 1 -20 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76.77 63.01 17.51 o 2 3 -20 53.05 58.58 17.25 o 3 3 -20 58.32 49.94 16.80 o 4 3 -20 258.61 251.55 26.13 o 5 3 -20 73.04 69.98 20.72 o 6 3 -20 68.74 54.21 25.91 o 7 3 -20 90.16 97.60 27.86 o -7 4 -20 99.99 75.02 26.82 o -6 4 -20 98.73 91.71 23.55 o -5 4 -20 45.30 56.80 21.40 o -4 4 -20 26.89 13.82 22.24 o -3 4 -20 44.05 33.76 18.53 o -2 4 -20 300.74 323.70 25.77 o -1 4 -20 734.27 735.52 36.91 o 0 4 -20 85.04 93.00 20.04 o 1 4 -20 196.13 226.95 22.91 o 2 4 -20 257.16 307.06 24.03 o 3 4 -20 110.04 91.03 21.87 o 4 4 -20 32.10 8.16 18.95 o 5 4 -20 28.33 30.62 19.76 o 6 4 -20 122.09 139.75 23.81 o 7 4 -20 128.26 167.25 24.67 o -6 5 -20 260.95 242.01 27.90 o -5 5 -20 472.68 491.84 37.48 o -4 5 -20 220.46 227.94 30.31 o -3 5 -20 586.61 537.34 37.12 o -2 5 -20 516.38 493.27 30.48 o -1 5 -20 346.00 296.23 25.31 o 0 5 -20 207.09 218.57 23.23 o 1 5 -20 112.66 84.56 19.38 o 2 5 -20 603.51 564.40 35.95 o 3 5 -20 532.21 557.76 34.69 o 4 5 -20 16.81 16.04 20.20 o 5 5 -20 150.09 142.84 24.35 o 6 5 -20 212.23 218.91 22.39 o -6 6 -20 111.79 126.64 28.94 o -5 6 -20 178.83 191.60 29.95 o -4 6 -20 62.32 40.91 24.90 o -3 6 -20 30.31 13.63 22.25 o -2 6 -20 163.64 193.41 28.11 o -1 6 -20 110.83 122.21 21.83 o 0 6 -20 12.30 -4.74 16.92 o 1 6 -20 207.11 201.30 23.45 o 2 6 -20 183.99 169.12 26.34 o 3 6 -20 211.98 216.11 27.94 o 4 6 -20 33.60 47.68 21.54 o 5 6 -20 100.17 122.27 20.34 o 6 6 -20 184.54 193.12 21.98 o -5 7 -20 87.01 115.51 28.06 o -4 7 -20 67.29 45.01 24.79 o -3 7 -20 35.45 44.51 24.22 o -2 7 -20 134.96 140.91 27.47 o -1 7 -20 64.92 56.52 22.95 o 0 7 -20 1.83 5.34 18.25 o 1 7 -20 23.01 21.23 21.52 o 2 7 -20 28.67 34.87 22.08 o 3 7 -20 22.66 33.65 21.70 o 4 7 -20 14.89 16.78 16.47 o 5 7 -20 81.02 90.98 19.76 o -3 8 -20 58.99 60.66 25.03 o -2 8 -20 28.56 46.88 24.56 o -1 8 -20 246.62 289.25 31.42 o 0 8 -20 80.34 79.36 49.00 o 1 8 -20 135.15 167.50 28.05 o 2 8 -20 35.87 39.45 22.77 o 3 8 -20 6.67 13.54 16.23 o 0 9 -20 156.40 159.57 35.13 o -8 1 -19 100.95 97.52 22.62 o -7 1 -19 149.38 135.32 22.86 o -6 1 -19 212.35 189.11 26.48 o -5 1 -19 70.73 52.34 19.14 o -4 1 -19 132.43 130.47 18.46 o -3 1 -19 17.74 5.21 15.87 o -2 1 -19 92.27 85.72 18.87 o -1 1 -19 104.73 115.44 18.65 o 0 1 -19 128.61 141.09 19.77 o 1 1 -19 346.73 341.37 23.51 o 2 1 -19 63.90 64.44 16.48 o 3 1 -19 191.18 200.27 20.06 o 4 1 -19 268.19 291.98 21.32 o 5 1 -19 0.76 -0.11 13.75 o 6 1 -19 34.75 39.88 14.60 o 7 1 -19 28.26 12.65 14.32 o 8 1 -19 111.00 136.85 20.56 o -8 2 -19 17.77 53.98 24.59 o -7 2 -19 111.48 139.68 27.27 o -6 2 -19 185.60 152.50 25.93 o -5 2 -19 296.71 289.80 24.56 o -4 2 -19 51.58 39.49 15.95 o -3 2 -19 1351.34 1323.35 43.48 o -2 2 -19 959.49 925.65 41.62 o -1 2 -19 140.24 131.90 19.66 o 0 2 -19 413.96 411.97 25.48 o 1 2 -19 138.81 147.47 19.82 o 2 2 -19 305.20 317.21 22.85 o 3 2 -19 575.55 609.92 28.24 o 4 2 -19 109.53 109.25 19.99 o 5 2 -19 895.28 942.08 29.82 o 6 2 -19 328.53 334.90 27.26 o 7 2 -19 14.11 18.67 18.98 o 8 2 -19 81.82 98.08 16.11 o -8 3 -19 35.65 9.04 24.06 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