Crystallography Open Database

Information card for entry 2214510

Preview

Coordinates	2214510.cif
Structure factors	2214510.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	cyclo-Tetrakis[μ-<i>N</i>-(2-hydroxybenzoyl)-<i>N</i>'-(2-hydroxy-3-\ methoxybenzylidene)hydrazinate(2-)]tetracobalt(II)} <i>N</i>,<i>N</i>-dimethylformamide tetrasolvate
Formula	C72 H76 Co4 N12 O20
Calculated formula	C72 H76 Co4 N12 O20
SMILES	CN(C=O)C.C[O]1c2c3[O]4[Co]56(OC(=N[N]5=Cc3ccc2)c2c(O)cccc2)[O](C)c2cccc3c2[O]6[Co]25(OC(=N[N]5=C3)c3c(O)cccc3)[O](C)c3cccc5c3[O]2[Co]23(OC(=N[N]2=C5)c2c(O)cccc2)[O](C)c2cccc5c2[O]3[Co]214OC(=N[N]2=C5)c1c(O)cccc1.CN(C)C=O.CN(C)C=O.CN(C)C=O
Title of publication	<i>cyclo</i>-Tetrakis[μ-<i>N</i>-(2-hydroxybenzoyl)-<i>N</i>'-(2-hydroxy-3-methoxybenzylidene)hydrazinate(2–)]tetracobalt(II) <i>N</i>,<i>N</i>-dimethylformamide tetrasolvate
Authors of publication	Gao, Yu-Xiang; Wang, Li-Bin; Niu, Yan-Ling; Hao, Lu-Jiang
Journal of publication	Acta Crystallographica Section E
Year of publication	2007
Journal volume	63
Journal issue	8
Pages of publication	m2128 - m2128
a	23.996 ± 0.002 Å
b	23.996 ± 0.002 Å
c	13.1605 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	7577.9 ± 1.1 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	88
Hermann-Mauguin space group symbol	I 41/a :2
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.0845
Residual factor for significantly intense reflections	0.0407
Weighted residual factors for significantly intense reflections	0.1009
Weighted residual factors for all reflections included in the refinement	0.1356
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

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