Crystallography Open Database

Information card for entry 2214518

Preview

Coordinates	2214518.cif
Structure factors	2214518.hkl
Original IUCr paper	HTML

Structure parameters

Common name	(18-Crown-6)bis(tetrahydrofuran-κO)potassium(I) [1,2-bis(fluoren-9-ylcarbonyl)benzene(2-)]bis(η^5^-\ cyclopentadienyl)dysprosate(III)
Formula	C64 H70 Dy K O10
Calculated formula	C64 H70 Dy K O10
SMILES	[K]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)([O]1CCCC1)[O]1CCCC1.[Dy]123456789(OC(=C%10c%11ccccc%11c%11ccccc%10%11)c%10ccccc%10C(=C%10c%11ccccc%11c%11ccccc%10%11)O1)([cH]1[cH]5[cH]4[cH]3[cH]21)[cH]1[cH]6[cH]7[cH]8[cH]91
Title of publication	(18-Crown-6)bis(tetrahydrofuran-κ<i>O</i>)potassium(I) [1,2-bis(fluoren-9-ylcarbonyl)benzene(2{-})]bis(η^5^-cyclopentadienyl)dysprosate(III)
Authors of publication	Zaeni, Ahmad; Olbrich, Falk; Blaurock, Steffen; Edelmann, Frank T.
Journal of publication	Acta Crystallographica Section E
Year of publication	2007
Journal volume	63
Journal issue	8
Pages of publication	m2218 - m2218
a	12.0798 ± 0.0002 Å
b	13.0513 ± 0.0002 Å
c	19.3154 ± 0.0003 Å
α	85.17 ± 0.0008°
β	73.148 ± 0.0007°
γ	74.5617 ± 0.0008°
Cell volume	2809.2 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0288
Residual factor for significantly intense reflections	0.0255
Weighted residual factors for significantly intense reflections	0.0653
Weighted residual factors for all reflections included in the refinement	0.0669
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

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