Crystallography Open Database

Information card for entry 2238949

Preview

Coordinates	2238949.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Di-μ-oxido-bis[bis(diisopropylacetamidinato)-κ<i>N</i>;κ^2^<i>N</i>,<i>N</i>'-germanium(IV)]
Formula	C32 H68 Ge2 N8 O2
Calculated formula	C32 H68 Ge2 N8 O2
Title of publication	Di-μ-oxido-bis[bis(diisopropylacetamidinato)-κ<i>N</i>;κ^2^<i>N</i>,<i>N</i>'-germanium(IV)]
Authors of publication	Syre, Ronny; Frenzel, Nancy; Hrib, Cristian G.; Burte, Edmund P.; Jones, Peter G.; Edelmann, Frank T.
Journal of publication	Acta Crystallographica Section E
Year of publication	2013
Journal volume	69
Journal issue	12
Pages of publication	m686 - m687
a	20.1934 ± 0.0002 Å
b	12.7424 ± 0.0001 Å
c	15.9008 ± 0.0001 Å
α	90°
β	100.038 ± 0.001°
γ	90°
Cell volume	4028.84 ± 0.06 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0209
Residual factor for significantly intense reflections	0.0202
Weighted residual factors for significantly intense reflections	0.0558
Weighted residual factors for all reflections included in the refinement	0.0565
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176798 (current)	2016-02-21	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23.	2238949.cif
92405	2014-01-12	cif/ Adding structures of 2238949 via cif-deposit CGI script.	2238949.cif