#------------------------------------------------------------------------------ #$Date: 2016-04-06 14:49:50 +0100 (Wed, 06 Apr 2016) $ #$Revision: 181890 $ #$URL: svn://www.crystallography.net/cod/hkl/2/23/90/2239001.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239001 _cell_angle_alpha 90.000 _cell_angle_beta 92.892 _cell_angle_gamma 90.000 _cell_length_a 11.2858 _cell_length_b 17.5442 _cell_length_c 24.7745 _exptl_crystal_F_000 2088.00 _reflns_d_resolution_high 0.7893 _cod_data_source_file hg5379Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CO-TEBa in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 484.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2880.59 2268.29 96.50 o 3 0 0 2539.46 2007.32 74.73 o 4 0 0 7389.20 6346.25 175.77 o 5 0 0 1200.67 1697.47 59.83 o 6 0 0 7391.40 8694.56 568.08 o 7 0 0 773.58 1021.76 75.60 o 8 0 0 160.39 128.83 30.34 o 9 0 0 2122.23 1807.19 79.59 o 10 0 0 2400.93 2103.50 88.35 o 11 0 0 566.72 542.11 50.74 o 12 0 0 239.98 187.01 32.18 o 13 0 0 551.55 570.16 45.30 o 1 1 0 20963.76 15759.34 341.12 o 2 1 0 2948.78 2909.63 54.04 o 3 1 0 2609.50 2408.54 73.75 o 4 1 0 53.63 99.03 8.97 o 5 1 0 9526.50 10463.35 194.64 o 6 1 0 3927.86 5810.71 329.29 o 7 1 0 1273.50 1075.16 81.83 o 8 1 0 433.59 502.66 49.05 o 9 1 0 262.37 254.22 21.97 o 10 1 0 2248.83 1972.99 60.51 o 11 1 0 726.84 734.95 31.97 o 12 1 0 141.18 178.32 21.53 o 13 1 0 410.79 433.81 28.02 o 0 2 0 27333.48 29479.65 536.22 o 1 2 0 2008.99 1564.75 32.03 o 2 2 0 2484.69 2631.20 89.93 o 3 2 0 678.74 468.41 22.06 o 4 2 0 176.89 119.85 9.59 o 5 2 0 150.33 239.58 25.07 o 6 2 0 14436.35 16527.67 527.80 o 7 2 0 597.93 726.92 45.20 o 8 2 0 8299.83 8381.17 190.33 o 9 2 0 2993.59 2794.65 71.60 o 10 2 0 466.10 468.31 28.70 o 11 2 0 803.81 846.54 33.38 o 12 2 0 34.13 62.10 22.52 o 13 2 0 96.04 75.74 11.76 o 1 3 0 1944.62 2193.93 177.57 o 2 3 0 12306.84 17295.51 464.63 o 3 3 0 12142.76 12034.20 558.08 o 4 3 0 56.14 34.48 9.17 o 5 3 0 12.81 13.08 6.94 o 6 3 0 1808.86 1542.97 59.22 o 7 3 0 3583.57 3749.54 255.83 o 8 3 0 1021.92 1098.65 62.21 o 9 3 0 281.28 392.13 38.13 o 10 3 0 751.96 721.39 39.13 o 12 3 0 122.12 235.52 23.62 o 13 3 0 58.64 56.29 10.43 o 0 4 0 5894.84 7114.35 187.06 o 1 4 0 2163.02 2429.52 81.42 o 2 4 0 103.53 128.46 17.31 o 3 4 0 8419.85 9018.60 245.23 o 4 4 0 1433.27 1618.39 62.65 o 5 4 0 427.53 623.16 35.68 o 6 4 0 2379.00 2470.82 80.18 o 7 4 0 1493.32 1697.73 82.07 o 8 4 0 1351.09 1339.89 96.11 o 9 4 0 2933.94 3021.91 89.81 o 10 4 0 96.48 129.47 26.89 o 11 4 0 1867.99 2347.91 91.66 o 12 4 0 524.30 677.99 40.30 o 13 4 0 93.57 148.72 16.02 o 1 5 0 2939.45 3608.45 75.43 o 2 5 0 5743.68 6877.56 174.58 o 3 5 0 4703.29 4883.27 115.28 o 4 5 0 3898.77 3592.54 169.14 o 5 5 0 665.47 895.62 45.13 o 6 5 0 192.83 212.50 24.07 o 7 5 0 106.98 92.54 23.50 o 8 5 0 439.11 753.93 79.84 o 9 5 0 96.85 142.96 20.26 o 10 5 0 722.86 754.28 47.23 o 11 5 0 74.66 201.06 84.57 o 12 5 0 171.30 255.03 25.01 o 13 5 0 19.08 24.05 10.14 o 0 6 0 8025.77 10336.85 278.01 o 1 6 0 462.56 671.38 26.94 o 2 6 0 12556.14 15840.48 954.99 o 3 6 0 1579.27 1661.32 112.77 o 4 6 0 658.04 677.63 74.84 o 5 6 0 875.63 986.02 50.45 o 6 6 0 132.82 150.98 22.25 o 7 6 0 18.36 26.31 12.71 o 8 6 0 21.73 12.98 13.20 o 9 6 0 22.08 38.80 17.96 o 10 6 0 91.38 78.90 21.48 o 11 6 0 75.16 147.58 34.64 o 12 6 0 238.78 263.76 34.54 o 13 6 0 177.69 152.28 35.28 o 1 7 0 753.66 760.21 31.03 o 2 7 0 69.55 106.77 14.66 o 3 7 0 13438.89 14148.44 1166.31 o 4 7 0 601.66 469.87 65.76 o 5 7 0 187.87 137.71 28.13 o 6 7 0 471.24 451.91 54.27 o 7 7 0 3146.39 3248.26 221.69 o 8 7 0 15.86 635.02 552.78 o 9 7 0 2036.50 2153.34 77.44 o 10 7 0 291.36 270.56 29.87 o 11 7 0 635.41 736.75 62.50 o 13 7 0 13.83 61.60 28.19 o 0 8 0 266.57 287.81 45.78 o 1 8 0 1167.99 1083.36 40.70 o 2 8 0 7489.29 8834.48 241.41 o 3 8 0 5277.72 5764.68 141.88 o 4 8 0 1339.74 900.59 100.44 o 5 8 0 64.09 39.73 14.18 o 6 8 0 526.97 490.58 58.74 o 7 8 0 243.21 262.32 62.54 o 8 8 0 1448.99 1452.36 80.30 o 9 8 0 48.65 9.58 22.61 o 10 8 0 391.22 404.66 37.77 o 11 8 0 90.30 162.08 35.89 o 12 8 0 40.67 55.24 16.51 o 13 8 0 211.58 205.02 74.61 o 1 9 0 8102.97 9371.85 192.46 o 2 9 0 1572.18 2066.27 73.78 o 3 9 0 5235.36 4921.10 311.05 o 4 9 0 6718.27 7326.92 228.81 o 5 9 0 834.10 599.32 65.73 o 6 9 0 2830.18 2524.21 209.67 o 7 9 0 1515.63 1567.59 84.04 o 8 9 0 1113.82 1165.92 169.23 o 9 9 0 49.73 74.32 24.79 o 10 9 0 1783.84 1778.95 102.48 o 11 9 0 536.65 607.80 52.95 o 12 9 0 43.23 191.16 25.92 o 0 10 0 10555.70 11606.89 309.20 o 1 10 0 3811.34 4326.15 148.41 o 2 10 0 19.80 19.27 8.88 o 3 10 0 188.09 107.30 32.28 o 4 10 0 1508.30 1179.87 89.69 o 5 10 0 108.03 13.49 15.53 o 6 10 0 1162.42 991.45 129.06 o 7 10 0 37.71 61.39 13.74 o 8 10 0 1976.71 1708.91 91.04 o 9 10 0 143.65 125.04 28.44 o 10 10 0 38.86 53.50 24.91 o 11 10 0 24.73 84.15 23.59 o 12 10 0 509.10 370.18 32.56 o 1 11 0 4238.75 4503.82 235.81 o 2 11 0 3057.84 2684.18 94.54 o 3 11 0 306.53 156.16 43.87 o 4 11 0 122.58 95.20 25.77 o 5 11 0 132.50 165.88 52.74 o 6 11 0 556.82 599.75 54.57 o 7 11 0 1941.15 1909.74 80.13 o 8 11 0 293.95 301.89 32.51 o 9 11 0 85.58 111.39 18.97 o 10 11 0 167.45 131.43 27.49 o 11 11 0 247.74 226.29 35.38 o 12 11 0 811.32 598.50 37.29 o 0 12 0 9107.21 10001.08 266.07 o 1 12 0 2526.07 2634.91 81.73 o 2 12 0 2646.48 2808.86 123.93 o 3 12 0 33.20 31.93 26.67 o 4 12 0 1105.07 901.68 127.63 o 5 12 0 2105.63 1833.61 70.85 o 6 12 0 1065.69 999.98 57.39 o 7 12 0 37.89 60.59 14.72 o 8 12 0 2268.36 2278.91 99.03 o 9 12 0 568.06 596.07 40.07 o 10 12 0 123.12 138.80 27.13 o 11 12 0 80.45 79.16 16.86 o 1 13 0 763.56 727.50 117.60 o 2 13 0 1912.79 1870.49 71.43 o 3 13 0 2156.75 2269.04 75.18 o 4 13 0 1577.09 1580.69 63.86 o 5 13 0 25.41 12.20 11.31 o 6 13 0 2998.84 2834.70 144.67 o 7 13 0 2572.20 2452.29 156.38 o 8 13 0 337.05 407.37 56.45 o 9 13 0 257.56 314.69 45.07 o 10 13 0 1165.11 1278.26 71.63 o 11 13 0 44.01 135.41 21.58 o 0 14 0 54.98 13.26 11.74 o 1 14 0 671.27 667.39 79.05 o 2 14 0 871.78 793.34 56.22 o 3 14 0 535.15 566.07 30.21 o 4 14 0 172.73 128.06 58.97 o 5 14 0 491.88 414.74 35.02 o 6 14 0 1010.97 876.06 52.62 o 7 14 0 55.27 70.69 16.26 o 8 14 0 724.12 722.02 43.64 o 9 14 0 458.39 489.72 31.66 o 10 14 0 52.24 129.14 27.14 o 11 14 0 29.13 23.62 6.96 o 1 15 0 506.67 515.02 94.27 o 2 15 0 2749.35 2599.13 159.04 o 3 15 0 16.91 18.55 28.66 o 4 15 0 89.74 110.56 37.86 o 5 15 0 369.58 383.41 33.12 o 6 15 0 357.42 349.85 46.37 o 7 15 0 545.58 446.22 35.74 o 8 15 0 246.36 281.39 27.16 o 9 15 0 9.84 24.88 12.88 o 10 15 0 45.63 56.67 12.36 o 0 16 0 6.85 10.33 13.47 o 1 16 0 8.70 15.93 9.03 o 2 16 0 633.46 583.26 64.30 o 3 16 0 57.72 103.72 39.67 o 4 16 0 227.04 297.66 43.12 o 5 16 0 1065.91 1041.57 90.42 o 6 16 0 734.68 741.60 45.59 o 7 16 0 0.22 10.29 11.92 o 8 16 0 1.20 33.74 10.14 o 9 16 0 31.30 127.52 45.59 o 1 17 0 299.15 370.84 52.06 o 2 17 0 49.93 70.54 24.67 o 3 17 0 191.04 170.86 35.16 o 4 17 0 71.08 85.50 22.17 o 5 17 0 307.56 335.25 30.65 o 6 17 0 15.06 16.90 10.08 o 7 17 0 489.90 544.74 32.90 o 8 17 0 8.29 56.52 21.80 o 0 18 0 26.66 29.21 14.11 o 1 18 0 51.02 45.84 13.69 o 2 18 0 372.54 389.72 53.51 o 3 18 0 188.67 215.17 36.76 o 4 18 0 113.46 139.36 28.87 o 5 18 0 251.66 233.70 21.58 o 6 18 0 6.44 9.99 7.69 o 7 18 0 3.99 8.97 5.32 o 1 19 0 50.26 59.09 15.25 o 2 19 0 1821.83 1919.59 103.95 o 3 19 0 809.08 1016.43 70.75 o 4 19 0 1026.75 994.69 68.13 o 5 19 0 183.03 141.89 26.14 o 6 19 0 264.76 339.81 32.13 o 7 19 0 613.76 641.21 34.84 o 0 20 0 4447.89 6116.32 177.85 o 1 20 0 2163.92 2752.68 177.59 o 2 20 0 182.16 217.32 29.69 o 3 20 0 421.39 419.76 40.06 o 4 20 0 213.07 177.05 25.19 o 5 20 0 97.29 67.52 15.07 o 6 20 0 84.02 119.18 14.68 o 1 21 0 965.54 1220.60 60.76 o 2 21 0 1022.92 1165.01 59.20 o 3 21 0 116.75 153.84 19.38 o 4 21 0 97.65 95.09 14.76 o -13 1 1 57.43 147.12 18.54 o -12 1 1 189.50 277.76 26.54 o -11 1 1 494.54 700.29 41.85 o -9 1 1 708.55 753.05 35.42 o -8 1 1 431.68 481.26 39.61 o -7 1 1 1324.85 1396.30 72.71 o -6 1 1 301.41 344.39 25.47 o -5 1 1 2440.92 2524.50 72.67 o -4 1 1 78.82 73.17 7.75 o -3 1 1 33484.14 33074.33 594.74 o -2 1 1 2392.41 2096.56 88.04 o -1 1 1 17.91 18.06 2.67 o 1 1 1 1212.04 988.63 32.96 o 2 1 1 3050.52 2615.62 72.29 o 3 1 1 6069.94 5866.96 123.25 o 4 1 1 1598.93 1480.00 30.03 o 5 1 1 1244.02 1244.77 62.91 o 6 1 1 712.13 803.08 92.65 o 7 1 1 253.89 215.78 24.19 o 8 1 1 341.83 352.41 43.54 o 9 1 1 215.97 254.96 35.20 o 11 1 1 155.55 350.77 48.45 o 12 1 1 29.71 71.78 23.53 o 13 1 1 152.02 292.24 23.54 o 14 1 1 97.55 81.81 11.55 o -13 2 1 693.75 745.73 35.76 o -12 2 1 499.75 499.54 28.45 o -11 2 1 1433.22 1416.10 43.81 o -10 2 1 326.49 427.29 52.80 o -9 2 1 1380.84 1714.68 138.01 o -8 2 1 730.48 1600.68 446.82 o -7 2 1 4263.53 4809.48 167.74 o -6 2 1 916.67 1108.77 76.46 o -5 2 1 5651.90 6351.40 119.96 o -4 2 1 322.48 497.80 26.12 o -3 2 1 639.07 463.61 17.98 o -2 2 1 1235.01 1211.87 59.92 o -1 2 1 2521.62 2162.76 83.77 o 0 2 1 3124.75 3445.87 58.53 o 1 2 1 4993.47 4503.72 113.11 o 2 2 1 370.31 418.83 42.83 o 3 2 1 209.81 139.15 26.77 o 4 2 1 940.89 1090.51 31.32 o 5 2 1 723.25 716.53 34.01 o 6 2 1 7180.78 8885.93 290.38 o 7 2 1 56.49 53.55 23.81 o 8 2 1 1019.77 1056.79 58.50 o 9 2 1 230.09 285.93 24.46 o 11 2 1 591.81 599.19 28.61 o 12 2 1 23.80 38.57 17.09 o 13 2 1 16.38 17.38 7.90 o -13 3 1 7.49 15.97 7.24 o -12 3 1 251.35 303.62 26.72 o -11 3 1 702.20 775.59 35.95 o -10 3 1 3400.34 3441.90 81.79 o -9 3 1 3083.25 3089.32 66.68 o -8 3 1 2632.25 3054.26 103.96 o -7 3 1 100.70 110.99 29.89 o -6 3 1 11360.02 12227.71 432.29 o -5 3 1 187.97 320.12 24.16 o -4 3 1 2555.11 2598.77 105.19 o -3 3 1 31.93 58.03 8.69 o -2 3 1 43435.30 41994.18 1980.91 o -1 3 1 1613.94 1116.75 48.38 o 0 3 1 4306.12 5012.78 112.49 o 1 3 1 304.94 292.37 29.47 o 2 3 1 793.16 760.27 146.45 o 3 3 1 535.20 632.56 41.98 o 4 3 1 481.13 549.46 28.73 o 5 3 1 6.54 5.62 5.63 o 6 3 1 5634.14 5796.29 170.52 o 7 3 1 1073.77 885.65 72.90 o 8 3 1 1747.71 1630.26 76.08 o 9 3 1 961.22 1171.13 139.78 o 10 3 1 507.87 536.95 52.13 o 11 3 1 1561.73 1732.96 54.87 o 12 3 1 257.34 295.31 37.78 o 13 3 1 31.96 99.20 27.46 o -13 4 1 46.05 51.32 11.63 o -12 4 1 181.68 338.44 28.71 o -11 4 1 217.74 441.39 42.38 o -10 4 1 781.48 727.94 35.49 o -9 4 1 1427.35 1763.54 287.54 o -8 4 1 2005.53 1963.31 86.34 o -7 4 1 3610.71 3712.96 172.56 o -6 4 1 1823.21 1839.78 81.99 o -5 4 1 324.66 367.60 27.27 o -3 4 1 5291.96 4351.35 162.98 o -2 4 1 17610.56 20501.56 289.57 o -1 4 1 3668.21 4650.47 134.61 o 0 4 1 237.89 133.03 14.18 o 1 4 1 234976.16 295670.41 12824.60 o 2 4 1 476.84 293.58 25.29 o 3 4 1 3802.00 3466.99 246.90 o 4 4 1 2693.70 2972.77 87.71 o 5 4 1 1167.52 786.06 48.24 o 6 4 1 799.15 664.76 40.25 o 7 4 1 504.96 533.88 37.72 o 8 4 1 139.02 116.68 31.13 o 9 4 1 2895.72 2813.39 69.24 o 10 4 1 1931.37 1869.56 52.08 o 11 4 1 3222.38 3235.15 111.70 o 12 4 1 433.42 446.81 38.94 o 13 4 1 135.78 113.96 13.75 o -13 5 1 14.20 12.62 4.19 o -12 5 1 763.79 833.89 44.65 o -11 5 1 1612.02 1808.95 103.09 o -10 5 1 3407.31 3665.54 95.32 o -9 5 1 7526.62 7178.13 124.32 o -8 5 1 131.74 133.44 37.22 o -7 5 1 1135.44 977.86 68.54 o -6 5 1 2852.03 2962.16 109.94 o -5 5 1 307.06 454.62 31.33 o -4 5 1 6437.34 6598.25 415.04 o -3 5 1 3886.70 3545.63 89.96 o -2 5 1 192.79 259.88 14.82 o 0 5 1 6071.35 6823.10 270.94 o 1 5 1 7.91 22.39 10.26 o 2 5 1 44324.09 55969.89 760.00 o 3 5 1 317.73 153.42 55.01 o 4 5 1 11354.24 10803.78 646.69 o 5 5 1 766.76 741.79 41.12 o 6 5 1 781.19 633.18 41.64 o 7 5 1 2620.21 2402.37 87.03 o 8 5 1 2385.71 2405.60 136.39 o 9 5 1 190.51 214.97 25.89 o 10 5 1 33.07 45.74 10.92 o 11 5 1 365.13 479.39 41.04 o 12 5 1 253.65 399.22 30.75 o 13 5 1 42.39 7.77 12.20 o -13 6 1 94.02 143.08 11.06 o -12 6 1 219.82 347.79 38.97 o -11 6 1 292.73 345.90 44.42 o -10 6 1 29.17 36.73 12.94 o -9 6 1 72.80 56.09 11.36 o -8 6 1 2162.23 2069.90 82.41 o -7 6 1 1322.65 1243.70 74.78 o -6 6 1 449.79 390.71 41.33 o -5 6 1 4619.38 4446.84 130.59 o -4 6 1 994.06 1272.06 75.71 o -3 6 1 930.61 570.51 83.45 o -2 6 1 258.09 459.85 22.61 o -1 6 1 245.38 284.07 25.35 o 0 6 1 2807.52 4172.93 379.25 o 1 6 1 10182.47 11328.29 642.11 o 2 6 1 487.90 270.25 21.22 o 3 6 1 176.41 178.07 35.34 o 4 6 1 3132.65 2730.09 91.25 o 5 6 1 3755.86 3190.94 94.06 o 6 6 1 5361.21 5134.38 165.65 o 7 6 1 444.64 524.98 44.53 o 8 6 1 41.24 40.47 13.54 o 9 6 1 1846.38 1962.08 68.96 o 10 6 1 1640.46 1667.98 62.34 o 11 6 1 506.84 625.62 42.74 o 12 6 1 102.90 101.93 22.59 o 13 6 1 86.81 59.07 16.10 o -13 7 1 30.21 20.78 5.03 o -12 7 1 99.59 147.42 24.46 o -11 7 1 576.40 752.98 65.27 o -10 7 1 1349.11 1509.86 56.92 o -9 7 1 531.97 516.48 43.05 o -8 7 1 1128.76 1121.99 68.25 o -7 7 1 995.60 1039.89 128.80 o -6 7 1 8771.92 8310.97 366.69 o -5 7 1 2363.09 2044.44 108.55 o -4 7 1 3937.58 4168.32 152.75 o -3 7 1 42.56 40.20 11.58 o -2 7 1 1248.46 1781.99 50.61 o -1 7 1 3463.41 3863.39 154.63 o 0 7 1 227.40 128.17 19.58 o 1 7 1 864.42 1090.99 42.38 o 2 7 1 5830.43 6297.83 313.83 o 3 7 1 923.08 1007.85 91.35 o 4 7 1 2095.62 1342.54 108.90 o 5 7 1 9.28 -10.29 16.86 o 6 7 1 36.20 19.26 13.73 o 7 7 1 504.82 507.07 59.35 o 8 7 1 5761.30 5730.48 165.67 o 9 7 1 288.44 306.81 30.78 o 10 7 1 887.96 962.72 45.71 o 11 7 1 63.17 319.10 107.65 o 12 7 1 1014.82 1274.67 73.07 o 13 7 1 226.47 260.86 67.01 o -13 8 1 184.95 135.60 16.02 o -12 8 1 121.42 79.70 17.42 o -11 8 1 89.60 69.68 19.93 o -10 8 1 2.35 6.23 11.42 o -9 8 1 528.23 480.63 40.08 o -8 8 1 888.13 875.83 72.37 o -7 8 1 1351.54 1137.17 131.65 o -6 8 1 76.44 106.35 30.37 o -5 8 1 24.94 30.32 13.53 o -4 8 1 404.63 183.58 32.43 o -3 8 1 466.39 319.16 46.80 o -2 8 1 4651.97 5209.21 154.91 o -1 8 1 133.71 203.75 17.75 o 0 8 1 728.46 737.72 32.40 o 1 8 1 131.07 63.14 9.91 o 2 8 1 730.77 574.81 35.21 o 3 8 1 2705.72 3167.75 173.60 o 4 8 1 2307.50 2528.76 175.33 o 5 8 1 2711.99 2567.69 127.51 o 6 8 1 93.38 15.30 14.09 o 7 8 1 95.14 88.06 44.41 o 8 8 1 647.09 618.33 60.82 o 9 8 1 1263.63 1187.87 61.22 o 10 8 1 406.95 470.86 39.91 o 11 8 1 592.88 580.99 55.17 o 12 8 1 15.30 76.50 17.17 o 13 8 1 137.91 138.11 39.20 o -12 9 1 1.66 13.89 9.88 o -11 9 1 824.93 1024.99 70.18 o -10 9 1 108.35 116.67 28.98 o -9 9 1 1247.55 1246.58 107.82 o -8 9 1 2031.98 2000.67 113.94 o -7 9 1 91.12 65.57 27.96 o -6 9 1 51.49 22.94 32.28 o -5 9 1 2350.04 2219.25 182.65 o -4 9 1 980.85 1007.51 78.74 o -3 9 1 189.88 270.82 29.91 o -2 9 1 5383.38 5944.28 203.67 o -1 9 1 622.56 538.92 31.67 o 0 9 1 474.55 601.66 35.63 o 1 9 1 750.37 946.97 47.55 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