#------------------------------------------------------------------------------ #$Date: 2016-04-06 14:49:50 +0100 (Wed, 06 Apr 2016) $ #$Revision: 181890 $ #$URL: svn://www.crystallography.net/cod/hkl/2/23/90/2239082.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239082 _cell_angle_alpha 90.000 _cell_angle_beta 101.211 _cell_angle_gamma 90.000 _cell_length_a 21.8068 _cell_length_b 7.3521 _cell_length_c 18.6016 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.8525 _cod_data_source_file hb7188Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sreenivas_SB22_0m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8257.39 7740.80 312.51 o 4 0 0 9627.57 8934.69 322.99 o 6 0 0 11025.32 10258.84 422.27 o 8 0 0 1256.25 971.12 52.52 o 10 0 0 1689.21 1879.39 125.11 o 12 0 0 5120.63 5888.76 159.53 o 14 0 0 28.64 37.74 3.64 o 16 0 0 2286.44 2546.15 61.79 o 18 0 0 2424.10 2602.34 56.90 o 20 0 0 2333.00 2503.35 61.43 o 22 0 0 1534.37 1589.89 41.49 o 24 0 0 1466.85 1237.53 85.10 o 1 1 0 283.87 283.59 10.81 o 3 1 0 5593.26 5876.96 145.09 o 5 1 0 18597.73 18279.54 448.73 o 7 1 0 63618.36 55820.59 1691.92 o 9 1 0 9329.51 8286.52 259.87 o 13 1 0 253.23 264.05 6.07 o 15 1 0 170.58 215.62 5.09 o 17 1 0 180.67 295.56 6.84 o 19 1 0 1347.89 1284.71 22.00 o 21 1 0 262.09 250.13 5.45 o 23 1 0 17.29 16.28 2.90 o 0 2 0 65954.20 46563.50 1888.21 o 2 2 0 101501.23 59044.78 1589.03 o 4 2 0 236.16 217.07 6.20 o 6 2 0 117.65 102.03 3.80 o 8 2 0 2559.45 2179.25 86.29 o 10 2 0 1220.01 204.24 574.16 o 12 2 0 3883.37 3981.68 86.52 o 14 2 0 869.04 937.85 25.31 o 16 2 0 922.33 957.27 34.95 o 18 2 0 1412.08 1546.94 40.03 o 20 2 0 1251.68 1319.46 39.04 o 22 2 0 980.12 918.51 38.26 o 24 2 0 119.17 106.31 3.26 o 1 3 0 3116.51 3608.35 101.97 o 3 3 0 4651.34 4466.39 126.56 o 5 3 0 128.72 138.36 6.67 o 7 3 0 4853.64 4580.83 479.15 o 9 3 0 1872.62 1861.59 109.91 o 11 3 0 719.91 807.02 43.77 o 13 3 0 186.74 0.00 855.50 o 15 3 0 104.33 0.00 614.06 o 17 3 0 1730.20 1768.91 49.50 o 19 3 0 618.98 679.71 31.99 o 21 3 0 1125.82 1092.09 53.45 o 23 3 0 105.09 78.70 3.49 o 0 4 0 9786.79 8447.45 411.90 o 2 4 0 3439.16 3336.83 105.69 o 4 4 0 8940.23 8399.69 192.70 o 6 4 0 4342.06 4209.30 101.00 o 8 4 0 1368.24 1414.84 121.67 o 10 4 0 519.19 610.18 23.19 o 12 4 0 395.37 403.80 22.44 o 14 4 0 204.99 200.02 18.25 o 16 4 0 184.38 188.88 9.15 o 18 4 0 581.82 583.70 10.33 o 20 4 0 540.14 477.21 40.51 o 22 4 0 78.63 62.96 4.38 o 1 5 0 4935.57 4719.73 82.56 o 3 5 0 375.94 317.29 21.53 o 5 5 0 444.77 410.15 21.60 o 7 5 0 238.45 234.60 14.44 o 9 5 0 5.63 12.88 15.46 o 11 5 0 72.57 0.00 541.70 o 13 5 0 628.29 636.36 14.15 o 15 5 0 1484.62 1368.75 30.10 o 17 5 0 174.44 151.48 25.82 o 19 5 0 259.81 261.11 33.37 o 0 6 0 1909.69 2006.57 87.77 o 2 6 0 6.90 319.91 407.76 o 4 6 0 838.04 872.06 69.37 o 6 6 0 183.40 199.31 5.50 o 8 6 0 240.32 280.13 17.95 o 10 6 0 193.68 0.00 816.95 o 12 6 0 149.36 144.42 10.48 o 14 6 0 99.80 101.62 9.99 o 16 6 0 12.41 14.75 62.67 o 1 7 0 355.52 431.38 46.42 o 3 7 0 356.91 437.36 41.92 o 5 7 0 132.25 0.00 390.10 o 7 7 0 384.85 453.64 47.37 o 9 7 0 0.19 1.30 50.96 o 11 7 0 181.30 157.25 21.41 o 13 7 0 66.03 0.00 451.76 o 0 8 0 346.34 0.00 519.38 o 2 8 0 592.28 586.80 92.82 o 4 8 0 35.76 62.76 41.40 o 6 8 0 349.08 277.65 42.44 o 8 8 0 53.95 37.55 5.07 o -25 1 1 382.98 314.75 12.19 o -23 1 1 810.66 819.13 13.51 o -21 1 1 1377.16 1430.77 25.62 o -19 1 1 1136.17 1178.91 100.17 o -17 1 1 417.73 410.67 7.75 o -15 1 1 2.43 1.41 1.14 o -13 1 1 108.79 107.56 3.05 o -9 1 1 2039.76 1513.74 48.86 o -7 1 1 14179.98 12878.16 315.70 o -5 1 1 31049.67 28115.04 686.80 o -3 1 1 10852.81 11022.02 260.35 o -1 1 1 56661.56 31455.54 1143.35 o 1 1 1 10874.96 10350.33 244.79 o 3 1 1 1293.97 1327.22 33.11 o 5 1 1 3.29 0.26 0.73 o 7 1 1 581.44 575.32 15.28 o 9 1 1 239.72 226.61 10.33 o 11 1 1 8.23 26.56 4.67 o 13 1 1 102.41 73.58 2.60 o 15 1 1 3109.82 3227.83 51.23 o 17 1 1 3828.85 4180.99 70.81 o 19 1 1 1907.76 1979.48 43.41 o 21 1 1 565.69 555.00 18.14 o 23 1 1 31.89 31.66 6.95 o -24 2 1 157.83 147.51 4.75 o -22 2 1 71.21 83.92 11.79 o -20 2 1 345.81 355.67 7.09 o -18 2 1 554.03 629.96 31.54 o -16 2 1 6.26 7.84 3.43 o -14 2 1 1822.21 1932.61 80.04 o -12 2 1 5339.00 5143.85 126.82 o -10 2 1 271.05 33.14 774.34 o -8 2 1 1592.12 1323.88 53.02 o -6 2 1 280.12 355.07 9.73 o -4 2 1 294.85 396.41 10.15 o -2 2 1 33688.59 26936.79 657.40 o 0 2 1 17254.88 15605.54 400.39 o 2 2 1 8.60 3.43 0.72 o 4 2 1 8393.48 7743.30 184.48 o 6 2 1 776.13 794.89 23.52 o 8 2 1 5063.15 4538.02 169.80 o 10 2 1 2295.87 2476.56 169.07 o 12 2 1 205.24 228.81 27.75 o 14 2 1 535.66 546.21 31.44 o 16 2 1 516.81 544.10 20.00 o 18 2 1 715.57 699.73 13.50 o 20 2 1 58.54 0.00 919.07 o 22 2 1 30.19 24.52 30.65 o 24 2 1 99.03 86.66 3.81 o -23 3 1 712.59 568.26 15.45 o -21 3 1 429.32 448.47 22.36 o -19 3 1 188.27 189.58 18.15 o -17 3 1 128.71 120.58 6.21 o -15 3 1 694.97 688.90 22.02 o -13 3 1 557.83 556.74 21.91 o -11 3 1 1099.18 1049.96 18.45 o -9 3 1 798.13 913.46 34.64 o -7 3 1 38.40 0.00 547.79 o -5 3 1 802.60 682.94 29.29 o -3 3 1 29601.50 24099.04 678.93 o -1 3 1 987.80 925.63 25.92 o 1 3 1 6909.47 6011.96 160.24 o 3 3 1 2933.61 2759.83 87.00 o 5 3 1 1269.56 1260.52 45.57 o 7 3 1 207.27 216.98 46.17 o 9 3 1 139.96 198.09 9.19 o 11 3 1 2.61 5.21 14.54 o 13 3 1 1056.34 1037.27 76.21 o 15 3 1 147.80 0.00 870.37 o 17 3 1 651.43 694.44 38.28 o 19 3 1 959.29 1021.05 17.69 o 21 3 1 164.26 172.42 4.32 o 23 3 1 13.70 7.73 1.84 o -22 4 1 494.10 412.70 15.98 o -20 4 1 917.03 921.69 54.88 o -18 4 1 884.45 918.71 27.79 o -16 4 1 248.75 289.18 9.63 o -14 4 1 33.26 36.87 2.62 o -12 4 1 613.24 678.54 52.98 o -10 4 1 4925.48 5153.49 90.92 o -8 4 1 168.03 129.04 35.08 o -6 4 1 36.80 27.91 12.65 o -4 4 1 4573.85 3875.22 108.78 o -2 4 1 521.35 643.21 41.70 o 0 4 1 17.40 0.00 436.88 o 2 4 1 409.17 496.27 34.93 o 4 4 1 1211.05 1328.27 29.70 o 6 4 1 7092.97 6656.35 163.14 o 8 4 1 21.47 68.60 270.17 o 10 4 1 1446.68 1424.26 99.05 o 12 4 1 4595.65 4856.76 80.31 o 14 4 1 1801.01 1963.28 106.14 o 16 4 1 470.69 439.50 26.32 o 18 4 1 9.46 12.19 6.73 o 20 4 1 0.76 216.41 739.18 o -19 5 1 1.74 254.96 467.99 o -17 5 1 57.66 61.57 5.09 o -15 5 1 0.37 2.40 4.83 o -13 5 1 726.30 791.82 47.08 o -11 5 1 2.81 2.14 13.91 o -9 5 1 1326.45 1501.73 98.13 o -7 5 1 770.06 812.19 52.87 o -5 5 1 527.42 473.27 60.60 o -3 5 1 2674.47 2796.82 106.49 o -1 5 1 3247.97 3230.34 159.49 o 1 5 1 233.05 246.60 10.94 o 3 5 1 1.39 3.57 14.49 o 5 5 1 4201.04 4387.14 113.16 o 7 5 1 1597.73 1787.07 85.77 o 9 5 1 46.67 52.43 27.03 o 11 5 1 590.43 666.60 76.67 o 13 5 1 255.08 251.26 16.94 o 15 5 1 352.20 368.19 66.69 o 17 5 1 33.56 28.93 104.54 o 19 5 1 142.26 126.79 4.16 o -16 6 1 0.80 463.25 477.45 o -14 6 1 265.03 263.34 8.60 o -12 6 1 681.15 673.24 86.26 o -10 6 1 179.26 0.00 601.89 o -8 6 1 3184.63 3377.86 179.81 o -6 6 1 3855.95 4164.71 73.69 o -4 6 1 173.85 189.61 22.91 o -2 6 1 1893.28 2187.01 165.06 o 0 6 1 939.49 1065.54 67.30 o 2 6 1 130.32 178.06 20.96 o 4 6 1 290.52 362.23 35.86 o 6 6 1 84.07 119.95 19.39 o 8 6 1 2085.67 2331.82 45.74 o 10 6 1 841.45 912.49 23.93 o 12 6 1 223.18 229.77 29.97 o 14 6 1 886.92 825.45 95.86 o 16 6 1 596.68 545.92 37.91 o -13 7 1 320.96 241.72 38.36 o -11 7 1 22.89 291.48 526.15 o -9 7 1 271.33 0.00 534.26 o -7 7 1 411.58 427.20 61.07 o -5 7 1 1103.04 1145.62 87.80 o -3 7 1 13.91 32.87 37.36 o -1 7 1 2449.50 2745.93 98.01 o 1 7 1 207.38 236.88 30.12 o 3 7 1 3.68 1.59 19.81 o 5 7 1 16.49 24.63 16.12 o 7 7 1 233.41 263.58 43.71 o 9 7 1 590.11 621.78 61.23 o 11 7 1 139.14 166.55 9.12 o 13 7 1 52.78 36.91 3.33 o -8 8 1 457.14 293.51 16.91 o -6 8 1 5.89 8.48 39.40 o -4 8 1 117.28 132.11 25.35 o -2 8 1 56.91 45.70 34.93 o 0 8 1 1.45 703.76 533.44 o 2 8 1 52.50 52.43 14.41 o 4 8 1 183.11 181.85 43.63 o 6 8 1 92.62 0.00 427.41 o 8 8 1 68.34 70.33 6.76 o -24 0 2 218.97 214.06 9.21 o -22 0 2 24.74 30.90 2.24 o -20 0 2 202.35 185.48 5.77 o -18 0 2 41.98 37.74 3.38 o -16 0 2 2359.44 2562.78 55.82 o -14 0 2 2121.54 1928.32 42.29 o -12 0 2 3209.16 3353.46 112.30 o -10 0 2 16.41 16.91 4.06 o -8 0 2 5689.60 5402.36 197.99 o -6 0 2 72875.28 60266.27 2195.02 o -4 0 2 42110.15 36359.03 1325.02 o -2 0 2 319.26 356.34 13.77 o 0 0 2 478.25 488.38 19.86 o 2 0 2 107430.88 61082.05 5478.90 o 4 0 2 29.15 109.85 7.13 o 6 0 2 3963.60 3641.75 217.48 o 8 0 2 1800.60 1608.30 94.68 o 12 0 2 2039.80 2754.52 65.39 o 14 0 2 2700.56 2939.27 68.81 o 16 0 2 3411.28 3550.83 87.85 o 18 0 2 1539.00 1667.91 48.16 o 20 0 2 1104.77 1061.58 27.82 o 22 0 2 1092.49 934.08 101.59 o 24 0 2 300.60 326.10 9.44 o -25 1 2 37.27 25.60 2.34 o -23 1 2 39.24 0.00 614.06 o -21 1 2 76.36 88.31 10.72 o -19 1 2 282.42 321.39 6.01 o -17 1 2 166.85 169.38 4.18 o -15 1 2 735.12 844.35 14.66 o -13 1 2 4340.29 4741.50 79.23 o -9 1 2 5180.38 4616.09 155.28 o -7 1 2 213.90 252.59 7.13 o -5 1 2 39585.72 35302.77 855.42 o -3 1 2 122.92 107.70 4.15 o -1 1 2 7485.17 7005.97 172.12 o 1 1 2 18877.31 16360.63 387.18 o 3 1 2 40343.16 33591.77 821.55 o 5 1 2 504.03 483.04 12.90 o 7 1 2 2652.65 2482.24 67.79 o 9 1 2 11773.47 10655.38 393.74 o 11 1 2 147.30 101.11 3.71 o 13 1 2 2701.61 2775.64 41.78 o 15 1 2 1387.02 1519.43 23.72 o 17 1 2 278.29 254.18 6.19 o 19 1 2 130.79 0.00 957.62 o 21 1 2 463.57 389.81 8.30 o 23 1 2 116.39 0.00 762.17 o -24 2 2 12.40 13.77 11.99 o -22 2 2 394.86 402.22 37.31 o -20 2 2 384.53 419.04 27.96 o -18 2 2 215.30 239.19 11.03 o -16 2 2 659.58 741.61 13.93 o -14 2 2 50.95 59.24 4.41 o -12 2 2 2922.91 2904.31 56.67 o -10 2 2 503.14 675.91 405.09 o -8 2 2 1021.11 911.98 31.96 o -6 2 2 240.85 186.81 5.99 o -4 2 2 3888.60 3691.57 91.01 o -2 2 2 10569.31 9552.93 234.97 o 0 2 2 7503.87 7167.29 176.25 o 2 2 2 20255.86 19164.18 471.06 o 4 2 2 1954.69 1807.41 45.16 o 6 2 2 1114.05 1250.91 34.58 o 8 2 2 33.55 13.53 2.95 o 10 2 2 1405.41 1768.73 29.72 o 12 2 2 3986.97 4714.12 133.12 o 14 2 2 20.21 1822.58 919.74 o 16 2 2 18.14 18.49 14.18 o 18 2 2 42.26 32.17 3.15 o 20 2 2 283.27 272.88 31.23 o 22 2 2 115.92 70.65 2.76 o -23 3 2 509.80 435.72 17.46 o -21 3 2 869.27 891.32 32.42 o -19 3 2 16.12 20.80 27.23 o -17 3 2 440.67 486.06 21.45 o -15 3 2 1399.36 1533.67 56.90 o -13 3 2 2188.30 2094.40 62.15 o -11 3 2 3353.34 2921.98 93.85 o -9 3 2 933.38 757.16 55.56 o -7 3 2 312.52 0.00 357.17 o -5 3 2 260.69 240.80 11.90 o -3 3 2 2974.43 2765.07 78.97 o -1 3 2 6707.08 6553.77 176.32 o 1 3 2 175.03 137.53 5.20 o 3 3 2 6.30 9.31 1.67 o 5 3 2 10594.75 9446.78 327.66 o 7 3 2 5858.76 5801.56 146.35 o 9 3 2 15.49 23.72 94.00 o 11 3 2 1432.04 1456.77 26.83 o 13 3 2 502.86 503.85 54.99 o 15 3 2 252.67 0.00 854.14 o 17 3 2 716.75 679.26 23.44 o 19 3 2 741.02 733.04 40.35 o 21 3 2 140.03 149.75 3.91 o -22 4 2 17.76 11.05 1.51 o -20 4 2 204.09 0.00 575.52 o -18 4 2 23.93 26.09 30.36 o -16 4 2 17.58 15.16 50.58 o -14 4 2 23.62 30.78 7.59 o -12 4 2 680.20 697.48 13.07 o -10 4 2 1120.05 1069.21 35.89 o -8 4 2 393.73 386.75 25.86 o -6 4 2 60.71 65.64 29.62 o -4 4 2 6.09 74.51 110.01 o -2 4 2 3101.37 2509.64 93.12 o 0 4 2 5845.79 5857.57 101.85 o 2 4 2 1175.75 1013.01 46.95 o 4 4 2 219.49 218.91 24.17 o 6 4 2 103.15 137.70 5.25 o 8 4 2 496.68 490.17 21.34 o 10 4 2 1433.55 1583.80 81.35 o 12 4 2 439.79 370.55 52.23 o 14 4 2 2756.59 2815.65 154.39 o 16 4 2 80.28 0.00 802.07 o 18 4 2 133.08 0.00 770.96 o 20 4 2 0.71 2.41 1.33 o -19 5 2 27.65 24.12 2.64 o -17 5 2 232.50 0.00 741.20 o -15 5 2 1914.23 1864.74 203.34 o -13 5 2 2567.49 2502.20 216.41 o -11 5 2 1915.66 1875.30 104.16 o -9 5 2 568.89 483.84 63.24 o -7 5 2 2804.60 2780.15 49.45 o -5 5 2 4944.13 4725.90 230.04 o -3 5 2 182.83 182.04 7.54 o -1 5 2 41.01 72.03 38.85 o 1 5 2 50.69 56.13 11.95 o 3 5 2 1488.01 1559.94 63.40 o 5 5 2 6026.28 5778.16 100.44 o 7 5 2 5555.64 5551.18 182.66 o 9 5 2 6784.34 7126.04 124.59 o 11 5 2 1103.95 1111.90 95.60 o 13 5 2 199.72 189.87 25.28 o 15 5 2 281.58 271.32 8.42 o 17 5 2 14.26 20.76 1.95 o 19 5 2 434.15 363.58 10.70 o -18 6 2 20.61 11.94 2.87 o -16 6 2 28.77 0.00 641.79 o -14 6 2 121.16 125.57 14.92 o -12 6 2 731.58 744.47 109.49 o -10 6 2 16.36 18.67 35.18 o -8 6 2 19.01 0.00 555.57 o -6 6 2 101.23 0.00 532.61 o -4 6 2 1756.27 1817.10 45.63 o -2 6 2 444.46 494.25 44.52 o 0 6 2 552.80 631.51 59.53 o 2 6 2 942.35 960.40 55.56 o 4 6 2 1194.81 1271.04 64.29 o 6 6 2 501.14 505.59 39.09 o 8 6 2 309.60 358.05 41.34 o 10 6 2 66.40 74.56 13.42 o 12 6 2 36.20 45.71 11.74 o 14 6 2 368.40 365.22 18.61 o 16 6 2 2.44 1.81 1.56 o -13 7 2 262.73 255.48 31.63 o -11 7 2 291.41 333.26 58.15 o -9 7 2 1223.12 1358.64 91.69 o -7 7 2 708.68 766.14 68.50 o -5 7 2 50.78 62.10 28.64 o -3 7 2 824.46 905.93 114.32 o -1 7 2 82.01 71.04 26.91 o 1 7 2 834.01 925.83 79.16 o 3 7 2 828.29 925.19 36.30 o 5 7 2 73.94 67.54 33.88 o 7 7 2 971.95 1059.41 81.76 o 9 7 2 637.26 681.70 40.90 o 11 7 2 548.93 548.49 67.95 o 13 7 2 329.81 316.38 15.89 o -8 8 2 326.91 293.17 79.80 o -6 8 2 215.23 0.00 409.15 o -4 8 2 71.43 56.91 21.83 o -2 8 2 411.42 436.10 65.31 o 0 8 2 120.66 110.83 11.47 o 2 8 2 34.94 0.00 338.46 o 4 8 2 0.79 2.63 36.20 o 6 8 2 30.42 32.91 2.37 o -25 1 3 28.11 24.40 2.34 o -23 1 3 49.78 54.55 6.15 o -21 1 3 1.06 3.06 8.87 o -19 1 3 23.51 32.28 1.87 o -17 1 3 63.40 81.71 2.57 o -15 1 3 1060.04 1198.64 18.24 o -13 1 3 3571.60 3702.90 58.73 o -11 1 3 7055.90 6114.23 490.64 o -7 1 3 7743.12 7758.65 190.18 o -5 1 3 12392.13 12013.77 294.23 o -3 1 3 2020.43 2087.59 56.91 o -1 1 3 97.07 78.96 3.96 o 1 1 3 11524.81 10300.79 242.90 o 3 1 3 3253.74 2733.79 67.98 o 5 1 3 1889.07 1544.38 38.82 o 7 1 3 462.50 326.10 13.85 o 9 1 3 339.12 194.88 15.17 o 11 1 3 48.20 27.00 1.96 o 13 1 3 140.01 116.68 2.65 o 15 1 3 0.11 22.11 7.05 o 17 1 3 343.31 376.00 38.47 o 19 1 3 612.45 646.67 21.09 o 21 1 3 942.36 935.73 18.51 o 23 1 3 547.35 485.79 12.81 o -24 2 3 63.74 51.97 8.26 o -22 2 3 41.42 0.00 672.22 o -20 2 3 7.06 6.82 1.95 o -18 2 3 4206.42 4502.53 64.97 o -16 2 3 4009.65 4301.85 64.69 o -14 2 3 626.68 542.91 10.41 o -12 2 3 969.20 1125.32 25.56 o -10 2 3 400.21 503.92 108.09 o -8 2 3 1962.13 1661.79 74.90 o -6 2 3 817.08 848.46 23.39 o -4 2 3 6926.19 6693.76 164.35 o -2 2 3 32.44 47.82 2.12 o 0 2 3 2732.35 2983.57 73.99 o 2 2 3 23521.98 20666.95 505.69 o 4 2 3 9639.11 9308.79 229.36 o 6 2 3 12005.98 10215.58 272.46 o 8 2 3 7197.84 6182.69 328.67 o 10 2 3 3.39 246.17 734.44 o 12 2 3 5.08 3.60 20.09 o 14 2 3 110.70 104.67 15.77 o 16 2 3 12.94 17.50 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