#------------------------------------------------------------------------------ #$Date: 2016-02-21 00:03:34 +0000 (Sun, 21 Feb 2016) $ #$Revision: 176798 $ #$URL: svn://www.crystallography.net/cod/cif/2/23/91/2239109.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2239109 loop_ _publ_author_name 'Ezzedinloo, Lida' 'Shrestha, Sumi' 'Bhadbhade, Mohan' 'Colbran, Stephen' _publ_section_title ; Tri-\m-chlorido-bis[(\h^5^-pentamethylcyclopentadienyl)rhodium(III)] hexafluoridophosphate from synchrotron radiation ; _journal_coeditor_code TK5276 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m14 _journal_page_last m15 _journal_paper_doi 10.1107/S1600536813032480 _journal_volume 70 _journal_year 2014 _chemical_formula_iupac '[Rh2 (C10 H15)2 Cl3] P F6' _chemical_formula_moiety 'C20 H30 Cl3 Rh2 +, F6 P -' _chemical_formula_sum 'C20 H30 Cl3 F6 P Rh2' _chemical_formula_weight 727.58 _chemical_name_common '[Cp*RuCl3RuCp*][PF6]' _chemical_name_systematic ; Tri-\m-chlorido-bis[(\h^5^-pentamethylcyclopentadienyl)rhodium(III)] hexafluoridophosphate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2013 _cell_angle_alpha 64.28(3) _cell_angle_beta 82.42(3) _cell_angle_gamma 86.70(3) _cell_formula_units_Z 2 _cell_length_a 8.0970(16) _cell_length_b 12.604(3) _cell_length_c 14.441(3) _cell_measurement_reflns_used 9980 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 22.5 _cell_measurement_theta_min 2.5 _cell_volume 1316.2(6) _computing_cell_refinement 'XDS (Kabsch, 1993)' _computing_data_collection 'BLU-ICE (McPhillips et al., 2002)' _computing_data_reduction 'XDS (Kabsch, 1993)' _computing_molecular_graphics 'CrystalMaker (CrystalMaker, 2013)' _computing_publication_material 'publCIF (Westrip, 2010)' _computing_structure_refinement 'SHELXL2013 (Sheldrick, 2008)' _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) and OLEX-2 (Dolomanov et al., 2009) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.871 _diffrn_measured_fraction_theta_max 0.896 _diffrn_measurement_device_type '3-BM1 Australian Synchrotron' _diffrn_measurement_method 'Phi Scan' _diffrn_radiation_monochromator Si<111> _diffrn_radiation_type Synchrotron _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0211 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 15787 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 24.998 _diffrn_reflns_theta_min 1.807 _diffrn_standards_decay_% 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.669 _exptl_absorpt_correction_type none _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.836 _exptl_crystal_description plate _exptl_crystal_F_000 720 _exptl_crystal_size_max 0.015 _exptl_crystal_size_mid 0.015 _exptl_crystal_size_min 0.010 _refine_diff_density_max 1.026 _refine_diff_density_min -0.565 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.094 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 299 _refine_ls_number_reflns 4158 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.094 _refine_ls_R_factor_all 0.0254 _refine_ls_R_factor_gt 0.0250 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0180P)^2^+3.0381P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0593 _refine_ls_wR_factor_ref 0.0595 _reflns_number_gt 4064 _reflns_number_total 4158 _reflns_threshold_expression I>2\s(I) _cod_data_source_file tk5276sup1.cf _cod_data_source_block I _cod_original_cell_volume 1316.1(6) _cod_database_code 2239109 _cod_database_fobs_code 2239109 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.975 _shelx_estimated_absorpt_t_max 0.984 _shelx_hkl_checksum 17045 _shelx_hkl_file ; 0 0 3 62.14 1.80 0 0 3 64.87 1.88 0 0 -5 180.60 5.21 0 0 -5 192.40 5.54 0 0 6 723.60 20.77 0 0 6 674.40 19.36 0 0 -7 6.90 0.28 0 0 -7 6.38 0.30 0 0 7 7.11 0.27 0 0 7 7.11 0.30 0 0 -8 814.90 23.42 0 0 -8 746.00 21.43 0 0 8 770.60 22.15 0 0 -9 353.00 10.19 0 0 -9 332.60 9.58 0 0 9 338.30 9.74 0 0 9 333.60 9.62 0 0 -10 835.30 24.03 0 0 -10 874.30 25.17 0 0 10 819.30 23.56 0 0 10 867.80 24.98 0 0 -11 104.90 3.08 0 0 -11 109.00 3.22 0 0 11 103.60 3.02 0 0 11 108.70 3.22 0 0 -12 580.40 16.76 0 0 -12 622.30 17.99 0 0 12 623.00 17.99 0 0 12 599.00 17.27 0 0 -13 7.91 0.50 0 0 -13 6.96 0.45 0 0 13 9.18 0.56 0 0 13 8.01 0.42 0 0 14 396.30 11.52 0 0 14 437.80 12.75 0 -1 14 3.58 0.42 0 -1 14 4.81 0.60 0 1 -14 2.51 0.49 0 1 -14 3.55 0.52 0 -1 13 96.72 2.91 0 -1 13 93.01 2.74 0 -1 12 4.87 0.36 0 -1 12 5.11 0.51 0 1 -12 4.01 0.44 0 1 -12 5.32 0.48 0 -1 11 114.20 3.33 0 -1 11 110.30 3.28 0 1 -11 107.80 3.17 0 1 -11 112.00 3.31 0 -1 10 98.15 2.92 0 -1 10 93.41 2.73 0 1 -10 94.80 2.79 0 1 -10 95.27 2.83 0 -1 9 18.86 0.68 0 -1 9 20.09 0.66 0 1 -9 20.13 0.66 0 1 -9 19.63 0.70 0 1 -8 13.79 0.47 0 1 -8 14.47 0.54 0 -1 7 3.25 0.21 0 -1 7 3.48 0.22 0 -1 7 2.76 0.23 0 1 -7 2.91 0.25 0 1 -7 3.17 0.22 0 -1 6 357.30 10.28 0 -1 6 354.40 10.18 0 1 -6 368.50 10.60 0 1 -6 367.20 10.56 0 -1 5 416.00 11.95 0 -1 5 413.30 11.87 0 1 -5 444.40 12.76 0 1 -5 444.70 12.78 0 -1 4 144.50 4.18 0 -1 4 149.80 4.32 0 1 -4 147.50 4.26 0 1 -4 146.80 4.24 0 -1 3 468.90 13.45 0 -1 2 234.90 6.75 0 1 -2 247.60 7.12 0 1 -2 245.00 7.04 0 -1 1 37.69 1.11 0 -1 1 37.06 1.10 0 1 -1 37.44 1.10 0 1 -1 38.07 1.12 0 -1 -1 12.68 0.38 0 -1 -1 12.77 0.39 0 1 1 12.91 0.39 0 1 1 12.75 0.39 0 -1 -5 175.50 5.06 0 -1 -5 195.20 5.63 0 -1 -5 183.30 5.28 0 1 5 188.20 5.42 0 1 5 189.40 5.45 0 -1 -7 39.46 1.18 0 -1 -7 36.96 1.10 0 1 7 37.73 1.13 0 1 7 38.66 1.14 0 -1 -8 464.60 13.38 0 -1 -8 448.90 12.92 0 1 8 453.70 13.06 0 1 8 462.90 13.30 0 -1 -9 20.73 0.68 0 -1 -9 22.87 0.71 0 1 9 20.02 0.66 0 1 9 20.88 0.64 0 -1 -10 637.20 18.37 0 -1 -10 592.80 17.07 0 -1 -11 15.28 0.54 0 -1 -11 16.68 0.61 0 1 11 17.52 0.66 0 1 11 16.84 0.57 0 -1 -12 845.30 24.44 0 -1 -12 837.30 24.20 0 1 12 787.10 22.70 0 1 12 847.20 24.45 0 -1 -13 76.81 2.29 0 -1 -13 84.63 2.53 0 1 13 87.24 2.57 0 1 13 86.94 2.60 0 1 14 857.90 24.96 0 1 14 934.30 27.19 0 -2 14 63.30 1.92 0 -2 14 64.20 2.02 0 2 -14 66.47 2.08 0 2 -14 62.33 1.94 0 -2 13 20.97 0.93 0 -2 13 20.64 0.79 0 2 -13 19.68 0.82 0 2 -13 20.76 0.89 0 -2 12 75.26 2.33 0 -2 12 73.42 2.19 0 2 -12 74.16 2.28 0 2 -12 69.01 2.10 0 -2 11 87.51 2.64 0 -2 11 91.11 2.69 0 2 -11 93.65 2.81 0 2 -11 93.95 2.80 0 -2 10 243.20 7.04 0 -2 10 230.50 6.71 0 2 -10 227.80 6.63 0 2 -10 225.50 6.53 0 -2 9 340.50 9.82 0 -2 9 340.40 9.84 0 -2 8 209.50 6.07 0 -2 8 203.60 5.88 0 2 -8 207.60 6.03 0 2 -8 208.60 6.03 0 -2 7 168.40 4.88 0 -2 7 162.90 4.71 0 2 -7 175.70 5.08 0 2 -7 170.80 4.97 0 -2 6 86.85 2.55 0 -2 6 86.50 2.53 0 2 -6 85.82 2.53 0 2 -6 88.47 2.59 0 -2 5 37.19 1.14 0 -2 5 37.91 1.16 0 2 -5 37.26 1.13 0 2 -5 38.86 1.19 0 -2 4 549.30 15.76 0 2 -4 555.60 15.94 0 -2 3 17.39 0.57 0 -2 3 17.19 0.56 0 2 -3 17.35 0.57 0 2 -3 16.99 0.56 0 -2 2 111.00 3.23 0 -2 2 113.00 3.28 0 2 -2 108.80 3.16 0 2 -2 105.30 3.06 0 -2 1 1.07 0.15 0 -2 1 1.05 0.13 0 2 -1 1.18 0.16 0 2 -1 0.93 0.15 0 -2 0 14.97 0.50 0 -2 0 14.90 0.49 0 2 0 15.89 0.51 0 2 0 15.68 0.51 0 -2 -1 22.73 0.70 0 -2 -1 23.91 0.74 0 2 1 23.71 0.73 0 2 1 24.30 0.74 0 -2 -2 339.80 9.75 0 2 2 375.20 10.76 0 -2 -3 8.33 0.29 0 -2 -3 7.45 0.27 0 -2 -6 270.30 7.77 0 -2 -6 267.00 7.68 0 2 6 262.10 7.54 0 2 6 266.50 7.66 0 -2 -7 145.60 4.20 0 -2 -7 150.90 4.36 0 2 7 151.60 4.38 0 2 7 144.70 4.17 0 -2 -9 181.10 5.24 0 -2 -9 182.00 5.25 0 2 9 185.50 5.35 0 2 9 184.00 5.32 0 -2 -10 436.00 12.57 0 -2 -10 416.30 11.98 0 2 10 426.00 12.26 0 2 10 429.10 12.37 0 -2 -11 73.49 2.19 0 -2 -11 69.09 2.04 0 2 11 72.90 2.17 0 2 11 72.88 2.14 0 -2 -12 389.60 11.29 0 -2 -12 396.00 11.46 0 2 12 377.30 10.90 0 2 12 394.00 11.40 0 -2 -13 0.11 0.35 0 -2 -13 0.33 0.33 0 2 13 1.20 0.38 0 2 13 -0.02 0.30 0 -2 -14 711.10 20.87 0 -2 -14 699.70 20.55 0 2 14 718.90 20.90 0 2 14 705.40 20.51 0 -3 15 28.51 1.20 0 -3 15 27.90 1.06 0 -3 14 102.50 3.03 0 -3 14 108.90 3.31 0 3 -14 106.70 3.20 0 3 -14 109.90 3.34 0 -3 13 8.88 0.73 0 -3 13 9.79 0.61 0 3 -13 8.59 0.73 0 3 -13 9.36 0.69 0 -3 12 344.10 9.94 0 -3 12 336.00 9.75 0 3 -12 340.20 9.85 0 3 -12 331.40 9.61 0 -3 11 17.09 0.82 0 -3 11 19.17 0.80 0 3 -11 17.58 0.78 0 3 -11 17.04 0.72 0 -3 10 785.50 22.57 0 -3 10 829.40 23.85 0 -3 10 881.30 25.32 0 3 -10 825.10 23.72 0 3 -10 855.90 24.59 0 -3 9 88.88 2.67 0 -3 9 85.79 2.55 0 3 -9 88.59 2.65 0 3 -9 81.70 2.48 0 -3 8 793.20 22.78 0 -3 8 770.70 22.12 0 3 -8 820.00 23.53 0 3 -8 802.50 23.06 0 -3 7 159.80 4.65 0 -3 7 163.70 4.76 0 3 -7 163.00 4.76 0 3 -7 162.00 4.70 0 3 -6 1693.00 48.48 0 3 -6 1619.00 46.39 0 -3 5 2.79 0.27 0 -3 5 2.56 0.28 0 3 -5 2.47 0.25 0 3 -5 2.65 0.28 0 -3 3 158.00 4.58 0 -3 3 155.20 4.51 0 3 -3 160.70 4.66 0 3 -3 157.00 4.56 0 -3 1 25.38 0.80 0 -3 1 25.69 0.81 0 3 -1 24.44 0.78 0 3 -1 24.89 0.79 0 -3 -1 41.13 1.24 0 -3 -1 41.06 1.24 0 3 1 41.28 1.25 0 3 1 40.73 1.23 0 -3 -3 37.26 1.12 0 -3 -3 34.31 1.04 0 3 3 34.42 1.04 0 3 3 37.42 1.12 0 -3 -8 106.60 3.09 0 -3 -8 110.10 3.19 0 3 8 103.70 3.01 0 3 8 99.89 2.90 0 -3 -9 6.46 0.29 0 -3 -9 6.30 0.28 0 3 9 6.58 0.28 0 3 9 6.20 0.29 0 -3 -10 24.50 0.78 0 -3 -10 24.57 0.77 0 3 10 22.08 0.70 0 3 10 24.44 0.78 0 -3 -11 31.33 0.98 0 -3 -11 30.50 0.97 0 3 11 31.33 1.00 0 3 11 31.27 0.98 0 -3 -12 37.15 1.17 0 -3 -12 37.64 1.19 0 3 12 37.45 1.17 0 3 12 37.89 1.20 0 -3 -13 54.28 1.67 0 -3 -13 50.49 1.55 0 3 13 57.62 1.76 0 3 13 54.85 1.67 0 -3 -14 48.22 1.50 0 -3 -14 52.71 1.62 0 3 14 52.22 1.62 0 3 14 47.83 1.47 0 3 15 13.33 0.61 0 3 15 11.95 0.57 0 3 16 175.50 6.16 0 -4 15 76.48 2.38 0 -4 15 70.06 2.34 0 4 -15 77.25 2.49 0 4 -15 78.92 2.55 0 -4 14 100.50 3.12 0 -4 14 99.37 2.99 0 4 -14 99.35 3.10 0 4 -14 90.31 2.76 0 -4 13 53.22 1.81 0 -4 13 53.70 1.72 0 4 -13 57.53 1.91 0 4 -13 58.57 1.92 0 4 -12 86.80 2.67 0 4 -12 84.60 2.59 0 -4 11 12.67 0.75 0 -4 11 11.30 0.67 0 4 -11 12.62 0.80 0 4 -11 12.07 0.70 0 -4 10 308.90 8.98 0 -4 10 302.90 8.76 0 4 -10 308.80 8.95 0 4 -10 318.50 9.24 0 -4 9 75.46 2.28 0 -4 9 78.00 2.41 0 4 -9 79.38 2.41 0 4 -9 78.82 2.41 0 -4 8 398.30 11.51 0 -4 8 427.20 12.32 0 4 -8 387.40 11.17 0 4 -8 393.10 11.35 0 -4 7 215.10 6.24 0 -4 7 222.20 6.45 0 4 -7 222.40 6.46 0 4 -7 220.20 6.38 0 -4 6 632.60 18.17 0 -4 6 606.80 17.43 0 4 -6 607.30 17.46 0 4 -6 624.80 17.94 0 -4 5 98.13 2.90 0 -4 5 95.07 2.82 0 4 -5 98.79 2.93 0 4 -5 100.60 2.97 0 -4 4 1082.00 31.02 0 -4 4 1067.00 30.57 0 4 -4 1079.00 30.92 0 4 -4 1033.00 29.60 0 -4 3 66.01 1.97 0 -4 3 68.00 2.03 0 4 -3 65.49 1.96 0 4 -3 68.18 2.04 0 -4 1 24.51 0.79 0 -4 1 26.60 0.85 0 4 -1 26.12 0.84 0 4 -1 25.78 0.84 0 -4 -1 30.76 0.96 0 -4 -1 32.55 1.01 0 4 1 30.88 0.97 0 4 1 33.20 1.03 0 4 2 116.60 3.40 0 4 2 120.90 3.52 0 -4 -3 8.17 0.35 0 -4 -3 9.03 0.37 0 4 3 9.39 0.36 0 4 3 8.40 0.34 0 -4 -5 1.29 0.18 0 -4 -5 1.56 0.21 0 4 5 1.43 0.22 0 4 5 1.41 0.19 0 -4 -7 143.10 4.14 0 -4 -7 150.20 4.34 0 4 7 151.20 4.37 0 4 7 139.10 4.03 0 -4 -8 631.60 18.11 0 -4 -8 641.90 18.41 0 -4 -9 198.60 5.73 0 -4 -9 196.60 5.66 0 4 9 192.60 5.56 0 4 9 190.20 5.49 0 -4 -10 636.60 18.28 0 -4 -10 595.80 17.11 0 4 10 594.60 17.07 0 4 10 609.60 17.50 0 -4 -11 244.40 7.06 0 -4 -11 246.30 7.12 0 4 11 239.50 6.92 0 4 11 226.30 6.54 0 -4 -12 475.10 13.70 0 -4 -12 508.70 14.66 0 -4 -12 513.30 14.80 0 4 12 469.10 13.51 0 4 12 497.00 14.32 0 -4 -13 2.51 0.37 0 -4 -13 3.42 0.41 0 4 13 2.42 0.39 0 4 13 2.56 0.38 0 -4 -14 180.30 5.27 0 -4 -14 178.20 5.22 0 4 14 182.30 5.32 0 4 14 184.20 5.38 0 -4 -15 0.32 0.42 0 -4 -15 -0.05 0.45 0 4 15 0.61 0.47 0 4 15 0.47 0.50 0 -5 14 5.90 1.26 0 -5 14 4.26 0.82 0 5 -14 6.45 1.11 0 5 -14 6.03 1.00 0 -5 13 2.25 0.95 0 -5 13 2.37 0.78 0 5 -13 3.57 0.95 0 5 -13 3.13 0.81 0 5 -12 25.43 1.12 0 5 -12 24.85 1.14 0 -5 11 5.42 0.65 0 -5 11 5.46 0.66 0 -5 11 4.48 0.70 0 5 -11 5.01 0.73 0 5 -11 4.48 0.72 0 -5 10 50.71 1.69 0 -5 10 49.07 1.61 0 -5 9 28.74 1.13 0 -5 9 29.24 1.10 0 5 -9 29.24 1.12 0 5 -9 29.22 1.12 0 -5 8 211.80 6.18 0 -5 8 202.70 5.95 0 5 -8 209.70 6.14 0 5 -8 201.70 5.92 0 -5 7 81.52 2.48 0 -5 7 77.99 2.38 0 5 -7 84.10 2.53 0 5 -7 82.06 2.49 0 -5 6 155.40 4.55 0 -5 6 159.80 4.68 0 5 -6 155.80 4.57 0 5 -6 157.80 4.62 0 -5 5 4.03 0.42 0 -5 5 4.24 0.39 0 5 -5 3.89 0.39 0 5 -5 3.85 0.36 0 -5 4 755.10 21.67 0 -5 4 756.70 21.71 0 5 -4 765.00 21.95 0 5 -4 739.10 21.22 0 -5 3 48.19 1.49 0 -5 3 45.06 1.40 0 5 -3 46.19 1.43 0 5 -3 46.84 1.46 0 -5 1 316.60 9.13 0 -5 1 339.10 9.77 0 5 -1 336.50 9.70 0 5 -1 333.70 9.62 0 -5 -1 212.00 6.13 0 -5 -1 215.00 6.23 0 5 1 209.90 6.08 0 5 1 213.40 6.18 0 -5 -2 955.80 27.37 0 5 2 991.90 28.40 0 -5 -3 3.33 0.27 0 -5 -3 4.25 0.27 0 -5 -5 130.60 3.80 0 -5 -5 122.50 3.57 0 -5 -7 459.20 13.19 0 -5 -7 506.60 14.53 0 5 7 470.20 13.51 0 5 7 474.90 13.62 0 -5 -9 269.00 7.74 0 -5 -9 264.10 7.61 0 5 9 254.10 7.33 0 5 9 252.40 7.27 0 5 10 1966.00 56.32 0 -5 -11 9.24 0.42 0 -5 -11 10.68 0.44 0 5 11 9.19 0.44 0 5 11 9.81 0.49 0 -5 -12 1206.00 34.61 0 -5 -12 1174.00 33.73 0 5 12 1226.00 35.21 0 5 12 1206.00 34.62 0 -5 -13 52.47 1.63 0 -5 -13 50.57 1.59 0 5 13 53.09 1.65 0 5 13 51.25 1.60 0 -5 -14 425.70 12.30 0 -5 -14 456.80 13.20 0 5 14 441.90 12.76 0 5 14 438.10 12.65 0 -5 -15 17.11 0.71 0 -5 -15 16.49 0.74 0 -5 -16 191.30 5.64 0 -5 -16 206.70 6.09 0 5 16 184.80 5.43 0 5 16 195.40 5.74 0 -6 14 104.70 3.36 0 -6 14 96.95 3.09 0 6 -14 106.30 3.43 0 6 -14 111.10 3.51 0 -6 13 1.47 1.00 0 -6 13 -0.10 1.07 0 6 -13 2.13 0.84 0 6 -13 0.80 0.83 0 -6 12 140.80 4.25 0 -6 12 140.60 4.19 0 6 -12 148.40 4.42 0 6 -12 139.90 4.17 0 -6 11 21.92 1.13 0 -6 11 19.40 0.96 0 6 -11 21.70 1.01 0 6 -11 23.77 1.11 0 -6 10 23.03 1.09 0 -6 10 22.31 0.95 0 6 -10 25.52 1.09 0 6 -10 25.70 1.08 0 -6 9 36.76 1.40 0 6 -9 33.49 1.26 0 6 -9 36.85 1.35 0 -6 8 1.97 0.57 0 6 -8 2.28 0.69 0 -6 7 6.63 0.64 0 -6 7 5.92 0.69 0 6 -7 6.05 0.62 0 6 -7 7.13 0.61 0 -6 6 199.60 5.83 0 -6 6 206.00 6.02 0 6 -6 209.20 6.10 0 6 -6 204.50 5.98 0 -6 5 10.66 0.56 0 -6 5 12.37 0.61 0 6 -5 12.18 0.58 0 6 -5 12.50 0.61 0 -6 4 910.30 26.11 0 -6 4 901.00 25.85 0 6 -4 932.20 26.74 0 6 -4 911.90 26.16 0 -6 3 0.55 0.34 0 -6 3 -0.02 0.34 0 6 -3 0.17 0.28 0 6 -3 0.39 0.35 0 -6 2 406.80 11.71 0 -6 2 394.30 11.37 0 6 -2 402.60 11.60 0 6 -2 420.70 12.12 0 -6 1 105.20 3.11 0 -6 1 105.70 3.12 0 6 -1 108.90 3.22 0 6 -1 112.90 3.33 0 -6 0 21.82 0.76 0 -6 0 22.14 0.78 0 6 0 22.16 0.80 0 6 0 24.35 0.84 0 -6 -1 41.31 1.28 0 -6 -1 41.45 1.30 0 6 1 40.40 1.28 0 6 1 42.89 1.34 0 6 2 179.40 5.20 0 6 2 173.60 5.05 0 -6 -3 7.98 0.40 0 -6 -3 9.26 0.43 0 6 3 7.78 0.39 0 6 3 8.62 0.39 0 -6 -4 521.00 14.97 0 -6 -4 546.70 15.68 0 6 4 542.00 15.55 0 6 4 550.60 15.81 0 -6 -5 220.30 6.38 0 -6 -5 232.20 6.71 0 6 5 228.60 6.59 0 6 5 223.80 6.48 0 -6 -6 397.40 11.42 0 -6 -6 404.50 11.64 0 6 6 396.70 11.41 0 6 6 403.90 11.59 0 -6 -7 122.70 3.57 0 -6 -7 128.90 3.76 0 6 7 122.20 3.58 0 6 7 125.00 3.63 0 -6 -8 37.19 1.16 0 -6 -8 41.50 1.27 0 6 8 37.93 1.16 0 6 8 35.12 1.11 0 -6 -9 181.70 5.27 0 -6 -9 183.90 5.31 0 6 9 188.40 5.44 0 6 9 182.80 5.31 0 -6 -10 58.47 1.74 0 -6 -10 53.38 1.62 0 6 10 52.96 1.62 0 6 10 55.16 1.65 0 -6 -11 153.30 4.47 0 -6 -11 149.00 4.32 0 6 11 150.90 4.41 0 6 11 143.70 4.18 0 -6 -12 538.60 15.48 0 -6 -12 542.50 15.63 0 6 12 547.30 15.75 0 6 12 510.20 14.68 0 -6 -13 0.67 0.49 0 -6 -13 0.26 0.40 0 -6 -14 601.50 17.32 0 -6 -14 585.90 16.90 0 6 14 561.50 16.17 0 6 14 554.80 15.99 0 -6 -15 9.44 0.55 0 -6 -15 9.51 0.65 0 -6 -15 8.98 0.56 0 6 15 9.32 0.63 0 6 15 10.29 0.63 0 -6 -16 263.60 7.70 0 -6 -16 267.30 7.79 0 6 16 270.90 7.89 0 6 16 253.10 7.39 0 6 17 23.45 0.97 0 6 17 21.89 0.94 0 -7 13 23.45 1.41 0 -7 13 18.86 1.27 0 -7 12 207.00 6.09 0 -7 12 202.10 5.98 0 -7 12 197.10 5.81 0 7 -12 201.30 5.91 0 7 -12 210.00 6.18 0 -7 11 137.50 4.18 0 -7 11 131.80 3.93 0 7 -11 137.80 4.13 0 7 -11 135.50 4.06 0 -7 10 107.60 3.28 0 -7 10 105.80 3.30 0 7 -10 111.50 3.38 0 7 -10 106.60 3.25 0 -7 9 239.50 7.02 0 -7 9 254.30 7.41 0 7 -9 272.30 7.93 0 7 -9 264.20 7.69 0 -7 8 130.00 3.89 0 -7 8 131.00 3.95 0 7 -8 136.80 4.06 0 7 -8 133.20 3.98 0 -7 7 247.50 7.25 0 -7 7 261.10 7.64 0 7 -7 259.00 7.59 0 7 -7 276.60 8.04 0 -7 6 338.80 9.83 0 7 -6 391.00 11.32 0 -7 4 354.40 10.25 0 -7 4 348.90 10.08 0 7 -4 362.70 10.48 0 7 -4 375.60 10.86 0 -7 3 147.30 4.32 0 -7 3 153.30 4.52 0 7 -3 155.90 4.59 0 7 -3 155.90 4.58 0 -7 2 113.80 3.36 0 -7 2 117.90 3.50 0 7 -2 120.10 3.56 0 7 -2 119.20 3.53 0 -7 1 4.26 0.39 0 -7 1 4.01 0.41 0 7 -1 4.89 0.43 0 7 -1 4.15 0.41 0 -7 0 71.17 2.15 0 -7 0 70.69 2.15 0 7 0 76.42 2.31 0 7 0 73.69 2.23 0 -7 -1 155.70 4.55 0 -7 -1 147.50 4.32 0 7 1 156.50 4.59 0 7 1 155.50 4.55 0 -7 -2 231.00 6.69 0 -7 -2 224.40 6.52 0 7 2 220.80 6.42 0 7 2 220.20 6.38 0 -7 -3 12.47 0.55 0 -7 -3 12.31 0.52 0 7 3 13.63 0.53 0 7 3 13.04 0.56 0 -7 -4 67.15 2.02 0 -7 -4 65.75 1.99 0 7 4 68.76 2.09 0 7 4 69.13 2.07 0 -7 -5 185.00 5.37 0 -7 -5 184.20 5.36 0 7 5 187.80 5.46 0 7 5 195.80 5.67 0 -7 -6 41.72 1.31 0 -7 -6 45.11 1.40 0 7 6 45.42 1.39 0 7 6 44.27 1.39 0 -7 -7 -0.12 0.30 0 -7 -7 0.27 0.25 0 -7 -8 3.26 0.30 0 -7 -8 3.09 0.34 0 -7 -9 161.80 4.71 0 -7 -9 168.00 4.87 0 7 9 159.40 4.65 0 7 9 157.30 4.56 0 -7 -10 105.00 3.07 0 -7 -10 108.40 3.20 0 7 10 97.70 2.89 0 7 10 99.91 2.93 0 -7 -11 70.90 2.15 0 -7 -11 70.80 2.10 0 7 11 69.63 2.09 0 7 11 62.71 1.94 0 -7 -12 23.20 0.80 0 -7 -12 21.07 0.88 0 7 12 22.26 0.86 0 7 12 22.55 0.87 0 -7 -13 230.00 6.72 0 -7 -13 220.70 6.38 0 7 13 216.80 6.32 0 7 13 220.30 6.40 0 -7 -14 187.00 5.50 0 -7 -14 182.20 5.31 0 7 14 171.50 5.02 0 7 14 178.60 5.24 0 -7 -15 80.43 2.49 0 -7 -15 76.29 2.34 0 7 15 79.42 2.44 0 7 15 82.18 2.53 0 -7 -16 92.84 2.86 0 -7 -16 92.88 2.80 0 7 16 93.17 2.83 0 7 16 91.80 2.84 0 -7 -17 1.13 0.68 0 -7 -17 0.84 0.66 0 7 17 1.01 0.62 0 7 17 0.92 0.71 0 -7 -18 23.23 0.99 0 -7 -18 24.90 1.05 0 7 18 27.14 1.14 0 7 18 25.11 1.07 0 -8 12 130.10 3.99 0 -8 12 139.60 4.21 0 8 -12 142.40 4.30 0 8 -12 138.50 4.18 0 -8 11 27.11 1.36 0 -8 11 25.49 1.12 0 8 -11 28.47 1.26 0 8 -11 26.34 1.23 0 -8 10 159.90 4.77 0 -8 10 169.90 5.09 0 8 -10 162.00 4.81 0 8 -10 159.00 4.71 0 -8 9 117.40 3.63 0 -8 9 114.00 3.48 0 8 -9 113.60 3.44 0 8 -9 118.40 3.58 0 -8 8 111.60 3.44 0 -8 8 103.20 3.14 0 8 -8 109.10 3.31 0 8 -8 104.50 3.16 0 -8 7 213.80 6.29 0 -8 7 223.80 6.57 0 8 -7 226.40 6.64 0 8 -7 222.20 6.50 0 -8 6 360.30 10.46 0 -8 6 375.80 10.91 0 8 -6 460.00 13.34 0 8 -6 449.10 12.98 0 -8 5 230.90 6.75 0 -8 5 238.50 7.00 0 8 -5 245.60 7.20 0 8 -5 243.90 7.10 0 -8 4 1005.00 28.83 0 -8 4 1023.00 29.37 0 8 -4 1029.00 29.56 0 8 -4 1066.00 30.58 0 -8 3 204.20 5.97 0 -8 3 209.30 6.16 0 8 -3 212.30 6.23 0 8 -3 213.00 6.22 0 -8 2 1340.00 38.42 0 -8 2 1424.00 40.80 0 8 -2 1403.00 40.20 0 8 -2 1399.00 40.09 0 -8 1 150.00 4.42 0 8 -1 149.30 4.41 0 -8 0 1602.00 45.86 0 -8 0 1556.00 44.56 0 8 0 1584.00 45.38 0 8 0 1561.00 44.68 0 -8 -1 50.43 1.58 0 -8 -1 48.83 1.55 0 8 1 49.69 1.59 0 8 1 50.90 1.60 0 -8 -2 1438.00 41.18 0 -8 -2 1433.00 41.04 0 8 2 1445.00 41.39 0 -8 -3 113.60 3.37 0 -8 -3 114.80 3.39 0 8 3 108.30 3.22 0 8 3 109.50 3.23 0 -8 -4 813.90 23.35 0 -8 -4 789.40 22.64 0 8 4 791.50 22.71 0 8 4 817.80 23.45 0 -8 -5 559.10 16.07 0 -8 -5 544.40 15.64 0 8 5 569.30 16.36 0 8 5 562.30 16.14 0 -8 -6 649.60 18.64 0 -8 -6 659.20 18.93 0 8 6 655.10 18.82 0 8 6 647.70 18.57 0 -8 -7 206.00 5.98 0 -8 -7 198.10 5.77 0 8 7 204.10 5.95 0 8 7 204.90 5.93 0 -8 -8 976.20 27.98 0 -8 -8 950.20 27.22 0 8 8 989.40 28.37 0 8 8 1009.00 28.89 0 -8 -9 188.70 5.48 0 -8 -9 180.10 5.25 0 8 9 176.70 5.17 0 8 9 176.90 5.13 0 -8 -10 1080.00 30.96 0 -8 -10 1042.00 29.86 0 8 10 1128.00 32.34 0 8 10 1127.00 32.27 0 -8 -11 78.91 2.40 0 -8 -11 75.45 2.25 0 8 11 72.87 2.25 0 8 11 75.00 2.25 0 -8 -12 493.80 14.20 0 -8 -12 485.40 14.02 0 8 12 430.80 12.45 0 8 12 405.20 11.69 0 -8 -13 1.75 0.61 0 -8 -13 2.60 0.47 0 8 13 2.15 0.56 0 8 13 2.25 0.55 0 -8 -14 66.36 2.11 0 -8 -14 62.98 1.91 0 8 14 63.34 2.00 0 8 14 61.58 2.00 0 -8 -15 9.00 0.65 0 -8 -15 8.87 0.82 0 8 15 8.81 0.71 0 8 15 8.44 0.83 0 -8 -16 35.24 1.39 0 -8 -16 35.21 1.26 0 8 16 37.03 1.36 0 8 16 36.71 1.43 0 -8 -17 8.14 0.85 0 -8 -17 11.39 0.94 0 8 17 9.85 0.82 0 8 17 10.68 0.94 0 -8 -18 13.40 0.94 0 -8 -18 12.67 0.93 0 8 18 12.94 0.94 0 8 18 11.04 0.92 0 8 19 33.82 1.49 0 8 19 32.98 1.38 0 -9 12 2.31 0.92 0 -9 11 -0.08 1.02 0 -9 11 0.37 0.97 0 9 -11 0.25 0.91 0 9 -11 -1.20 1.01 0 -9 10 1.35 1.01 0 -9 10 1.25 0.83 0 9 -10 0.55 0.82 0 9 -10 -0.18 0.79 0 -9 9 29.16 1.39 0 -9 9 28.89 1.24 0 9 -9 28.65 1.24 0 9 -9 29.25 1.21 0 -9 8 5.09 0.87 0 -9 8 2.83 0.76 0 9 -8 2.58 0.76 0 9 -8 2.27 0.69 0 -9 7 15.95 0.99 0 -9 7 15.78 0.93 0 9 -7 15.21 0.93 0 9 -7 16.16 0.87 0 -9 6 69.26 2.27 0 -9 6 68.79 2.24 0 9 -6 69.98 2.27 0 9 -6 65.38 2.08 0 -9 5 73.31 2.34 0 -9 5 66.74 2.16 0 9 -5 71.40 2.31 0 9 -5 71.77 2.26 0 -9 4 613.20 17.65 0 -9 4 607.20 17.50 0 9 -4 625.80 18.03 0 9 -4 637.00 18.31 0 -9 3 226.10 6.61 0 -9 3 230.10 6.74 0 9 -3 225.70 6.58 0 9 -3 228.60 6.70 0 -9 2 722.90 20.77 0 -9 2 733.00 21.11 0 9 -2 726.30 20.90 0 9 -2 712.20 20.46 0 -9 1 19.31 0.89 0 -9 1 19.26 0.83 0 9 -1 20.03 0.86 0 9 -1 18.04 0.77 0 -9 0 397.40 11.48 0 -9 0 375.90 10.90 0 9 0 383.20 11.09 0 9 0 381.10 10.99 0 -9 -1 48.43 1.59 0 -9 -1 48.64 1.58 0 9 1 47.68 1.58 0 9 1 46.63 1.49 0 -9 -2 497.30 14.33 0 9 2 497.10 14.30 0 -9 -3 10.40 0.58 0 -9 -3 10.32 0.62 0 9 3 9.76 0.62 0 9 3 10.41 0.57 0 -9 -4 333.60 9.65 0 -9 -4 314.40 9.09 0 9 4 324.80 9.40 0 9 4 337.60 9.76 0 -9 -5 119.70 3.55 0 -9 -5 114.50 3.41 0 -9 -6 215.20 6.27 0 9 6 218.40 6.37 0 9 7 11.99 0.63 0 9 7 12.67 0.62 0 -9 -8 725.10 20.82 0 -9 -8 678.80 19.51 0 9 8 705.00 20.26 0 9 8 773.00 22.18 0 -9 -9 3.03 0.39 0 -9 -9 2.38 0.43 0 9 9 1.41 0.47 0 9 9 2.44 0.40 0 9 10 1276.00 36.59 0 9 10 1395.00 39.97 0 -9 -11 19.12 0.82 0 9 11 17.94 0.85 0 9 12 1130.00 32.47 0 -9 -13 12.81 0.87 0 9 13 13.40 0.83 0 9 13 12.81 0.82 0 -9 -14 487.10 14.09 0 -9 -14 517.70 14.89 0 9 14 500.00 14.44 0 9 14 469.90 13.56 0 -9 -15 21.71 0.86 0 -9 -15 22.97 1.07 0 9 15 24.39 1.14 0 9 15 21.40 1.08 0 -9 -16 290.10 8.48 0 9 16 271.80 7.94 0 9 16 284.60 8.32 0 -9 -17 35.40 1.37 0 -9 -17 38.04 1.58 0 9 17 33.76 1.41 0 -9 -18 166.70 4.98 0 -9 -18 159.00 4.77 0 9 18 181.20 5.40 0 9 18 170.50 5.09 0 -9 -19 3.78 1.01 0 -9 -19 6.73 1.07 0 9 19 5.19 1.12 0 9 19 3.89 1.12 0 -10 11 42.19 1.68 0 -10 11 43.30 1.96 0 -10 10 6.25 1.24 0 -10 10 8.37 1.11 0 10 -10 7.58 1.04 0 10 -10 9.29 0.91 0 -10 9 10.26 0.97 0 -10 9 8.64 1.07 0 10 -9 9.88 0.87 0 10 -9 9.14 0.96 0 -10 8 43.18 1.60 0 -10 8 44.51 1.66 0 10 -8 48.53 1.70 0 10 -8 44.74 1.64 0 -10 7 7.14 0.89 0 -10 7 6.68 0.85 0 10 -7 6.83 0.87 0 10 -7 6.02 0.76 0 -10 6 6.78 0.74 0 -10 6 7.49 0.87 0 10 -6 5.17 0.71 0 10 -6 6.65 0.73 0 -10 5 17.30 1.01 0 -10 5 14.95 0.83 0 10 -5 17.87 0.98 0 10 -5 15.85 0.86 0 -10 4 120.10 3.67 0 -10 4 122.40 3.68 0 10 -4 129.20 3.91 0 10 -4 126.40 3.75 0 -10 3 57.90 1.95 0 -10 3 56.42 1.84 0 10 -3 57.25 1.84 0 10 -3 60.44 1.98 0 -10 2 235.50 6.91 0 -10 2 241.90 7.05 0 10 -2 240.00 7.03 0 10 -2 232.20 6.76 0 -10 1 13.44 0.72 0 -10 1 13.95 0.80 0 10 -1 14.97 0.77 0 10 -1 13.44 0.64 0 -10 0 98.08 2.96 0 -10 0 99.28 3.05 0 10 0 102.40 3.12 0 10 0 98.61 2.96 0 -10 -1 9.82 0.72 0 -10 -1 9.96 0.60 0 10 1 10.51 0.72 0 10 1 10.25 0.60 0 -10 -2 95.76 2.93 0 -10 -2 99.65 3.00 0 10 2 99.00 2.97 0 10 2 100.00 3.06 0 -10 -3 9.63 0.63 0 -10 -3 10.20 0.58 0 10 3 9.34 0.56 0 10 3 10.01 0.63 0 -10 -4 328.20 9.51 0 -10 -4 299.90 8.67 0 10 4 326.30 9.43 0 10 4 326.00 9.47 0 -10 -5 171.10 5.05 0 -10 -5 168.00 4.91 0 10 5 171.30 5.01 0 10 5 176.00 5.19 0 -10 -6 187.80 5.53 0 -10 -6 182.90 5.33 0 10 6 180.50 5.27 0 10 6 183.20 5.41 0 -10 -7 735.00 21.15 0 -10 -7 753.40 21.62 0 10 7 741.50 21.27 0 10 7 730.20 21.00 0 -10 -8 326.10 9.41 0 -10 -8 334.80 9.72 0 10 8 336.60 9.79 0 10 8 314.80 9.10 0 -10 -9 287.70 8.38 0 -10 -9 278.20 8.03 0 10 9 276.80 8.01 0 10 9 281.10 8.21 0 -10 -10 1064.00 30.54 0 -10 -10 1089.00 31.18 0 10 10 1088.00 31.17 0 10 10 1105.00 31.72 0 10 11 60.39 1.89 0 10 11 58.28 1.94 0 -10 -12 908.90 26.06 0 -10 -12 850.40 24.47 0 10 12 788.10 22.71 0 10 12 809.10 23.23 0 10 13 29.24 1.12 0 10 13 27.95 1.17 0 -10 -14 374.20 10.77 0 -10 -14 367.60 10.66 0 10 14 355.90 10.34 0 10 14 344.70 9.98 0 -10 -15 1.18 0.51 0 -10 -15 0.75 0.72 0 10 15 1.75 0.77 0 10 15 0.88 0.84 0 -10 -16 193.50 5.64 0 -10 -16 198.10 5.87 0 10 16 186.80 5.53 0 10 16 186.50 5.53 0 -10 -17 6.24 0.79 0 -10 -17 4.97 0.94 0 10 17 3.95 0.91 0 10 17 5.80 0.94 0 -10 -18 138.30 4.20 0 -10 -18 148.90 4.44 0 10 18 137.20 4.18 0 10 18 132.90 4.07 0 -10 -19 38.56 1.67 0 -10 -19 34.06 1.52 0 -11 10 89.62 2.93 0 -11 10 86.43 2.96 0 11 -10 90.73 2.85 0 11 -10 91.54 3.07 0 -11 9 44.24 1.71 0 -11 9 42.09 1.80 0 11 -9 45.98 1.70 0 11 -9 47.31 1.86 0 -11 8 239.60 7.05 0 -11 8 229.20 6.72 0 11 -8 228.10 6.67 0 11 -8 229.20 6.74 0 -11 7 19.70 1.10 0 -11 7 18.58 1.12 0 11 -7 20.51 1.07 0 11 -7 21.60 1.19 0 -11 6 401.50 11.63 0 -11 6 382.80 11.11 0 11 -6 409.30 11.82 0 11 -6 410.70 11.88 0 -11 5 4.26 0.84 0 -11 5 5.50 0.86 0 11 -5 5.55 0.72 0 11 -5 5.92 0.74 0 -11 4 226.70 6.68 0 -11 4 236.70 6.94 0 -11 3 6.82 0.71 0 -11 3 7.27 0.73 0 11 -3 7.92 0.68 0 11 -3 7.47 0.81 0 -11 2 54.59 1.85 0 -11 2 55.12 1.81 0 11 -2 58.65 1.92 0 11 -2 57.88 1.84 0 -11 1 11.02 0.71 0 -11 1 10.23 0.77 0 11 -1 12.62 0.74 0 11 -1 10.79 0.66 0 -11 0 47.20 1.56 0 -11 0 48.26 1.67 0 11 0 46.30 1.52 0 11 0 48.52 1.65 0 -11 -1 169.10 4.97 0 -11 -1 164.90 4.90 0 11 1 173.70 5.14 0 11 1 178.30 5.22 0 -11 -2 111.10 3.38 0 -11 -2 108.90 3.26 0 11 2 114.50 3.41 0 11 2 115.10 3.47 0 -11 -3 266.70 7.74 0 -11 -3 271.70 7.93 0 11 3 277.80 8.10 0 11 3 285.40 8.27 0 -11 -4 242.50 7.08 0 -11 -4 222.80 6.48 0 11 4 233.00 6.78 0 11 4 246.60 7.21 0 -11 -5 160.30 4.75 0 -11 -5 154.80 4.53 0 11 5 164.80 4.83 0 11 5 163.70 4.86 0 -11 -6 277.30 8.02 0 -11 -6 278.70 8.11 0 11 6 273.70 7.93 0 11 6 278.60 8.13 0 -11 -7 13.12 0.78 0 -11 -7 13.14 0.62 0 11 7 13.02 0.65 0 11 7 12.36 0.79 0 -11 -8 76.09 2.39 0 -11 -8 78.94 2.38 0 11 8 75.78 2.40 0 11 8 78.59 2.39 0 -11 -9 12.47 0.61 0 -11 -9 12.90 0.79 0 11 9 14.24 0.70 0 11 9 12.70 0.80 0 -11 -10 168.40 4.90 0 -11 -10 179.70 5.30 0 11 10 166.40 4.87 0 11 10 170.50 5.06 0 -11 -11 30.59 1.17 0 -11 -11 34.49 1.18 0 11 11 29.15 1.07 0 11 11 27.61 1.16 0 -11 -12 157.70 4.61 0 -11 -12 162.90 4.87 0 11 12 163.40 4.90 0 11 12 162.80 4.80 0 -11 -13 0.52 0.48 0 -11 -13 0.44 0.67 0 11 13 0.48 0.80 0 11 13 1.23 0.65 0 -11 -14 22.39 1.05 0 -11 -14 21.80 0.86 0 11 14 20.00 0.99 0 11 14 21.16 1.05 0 -11 -15 131.80 3.88 0 -11 -15 139.20 4.19 0 11 15 133.20 4.02 0 11 15 132.90 4.01 0 -11 -16 75.19 2.29 0 -11 -16 76.38 2.50 0 11 16 77.59 2.49 0 11 16 75.88 2.49 0 -11 -17 98.57 3.11 0 -11 -17 92.45 2.81 0 11 17 96.02 3.04 0 11 17 99.32 3.10 0 -11 -18 86.11 2.68 0 -11 -18 85.65 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1.19 2 12 -7 11.15 0.86 -2 -12 6 0.58 1.09 -2 -12 6 3.52 0.81 2 12 -6 2.17 1.00 2 12 -6 2.35 0.86 -2 -12 5 35.16 1.37 -2 -12 5 34.93 1.49 2 12 -5 37.92 1.60 2 12 -5 34.35 1.32 -2 -12 4 24.07 1.22 -2 -12 4 27.35 1.22 2 12 -4 27.04 1.31 2 12 -4 26.93 1.12 -2 -12 3 21.01 1.14 -2 -12 3 21.33 1.08 2 12 -3 20.78 1.14 2 12 -3 20.87 0.89 -2 -12 2 2.19 0.65 -2 -12 2 0.45 0.71 2 12 -2 2.24 0.85 2 12 -2 2.32 0.67 2 12 -1 38.67 1.44 2 12 -1 37.14 1.30 -2 -12 0 148.20 4.44 -2 -12 0 153.00 4.50 2 12 0 153.50 4.60 2 12 0 153.60 4.52 -2 -12 -1 7.74 0.73 -2 -12 -1 7.65 0.62 2 12 1 7.64 0.77 2 12 1 9.01 0.58 -2 -12 -2 98.46 2.95 -2 -12 -2 101.50 3.11 2 12 2 102.10 3.13 2 12 2 105.90 3.15 -2 -12 -3 68.31 2.19 -2 -12 -3 64.19 1.98 2 12 3 64.45 2.08 2 12 3 64.17 1.99 -2 -12 -4 2.69 0.69 -2 -12 -4 2.56 0.42 2 12 4 2.51 0.67 2 12 4 3.74 0.45 -2 -12 -5 428.80 12.40 -2 -12 -5 398.60 11.47 2 12 5 423.40 12.24 2 12 5 396.20 11.41 -2 -12 -6 12.18 0.78 -2 -12 -6 11.60 0.61 2 12 6 12.55 0.83 2 12 6 11.14 0.58 -2 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4.01 2 12 19 130.60 4.03 -2 -12 -20 50.58 1.88 -2 -12 -20 52.34 2.07 2 12 20 54.07 2.09 2 12 20 53.59 2.26 -2 -13 7 96.82 3.37 -2 -13 7 93.36 2.95 2 13 -7 99.19 3.08 2 13 -7 104.40 3.39 -2 -13 6 1.86 0.86 -2 -13 6 2.07 1.37 2 13 -6 0.80 0.83 2 13 -6 2.61 1.12 -2 -13 5 220.40 6.54 -2 -13 5 209.60 6.13 2 13 -5 232.50 6.86 2 13 -5 222.10 6.48 -2 -13 4 1.80 0.79 -2 -13 4 3.22 1.00 2 13 -4 0.65 1.04 2 13 -4 2.29 0.80 -2 -13 3 486.50 14.01 -2 -13 3 512.10 14.79 2 13 -3 498.60 14.34 2 13 -3 511.50 14.77 -2 -13 2 12.19 0.85 -2 -13 2 10.69 1.00 2 13 -2 11.79 0.74 2 13 -2 11.41 1.01 -2 -13 1 447.20 12.96 -2 -13 1 457.20 13.20 2 13 -1 498.50 14.41 2 13 -1 509.70 14.68 -2 -13 0 3.00 0.67 -2 -13 0 3.59 0.76 2 13 0 3.99 0.85 2 13 0 4.31 0.68 -2 -13 -1 534.50 15.43 -2 -13 -1 526.80 15.14 2 13 1 537.30 15.51 2 13 1 552.30 15.87 -2 -13 -2 76.99 2.36 -2 -13 -2 82.41 2.59 2 13 2 82.42 2.62 2 13 2 80.78 2.46 -2 -13 -3 270.30 7.90 -2 -13 -3 255.70 7.41 2 13 3 286.70 8.30 2 13 3 281.30 8.22 -2 -13 -4 22.18 1.00 -2 -13 -4 20.10 0.79 2 13 4 19.81 0.99 2 13 4 21.82 0.89 -2 -13 -5 60.62 1.98 -2 -13 -5 57.07 1.79 2 13 5 56.27 1.78 2 13 5 59.01 1.92 -2 -13 -6 10.66 0.57 -2 -13 -6 11.86 0.77 2 13 6 10.72 0.74 2 13 6 10.73 0.58 -2 -13 -7 93.23 2.86 -2 -13 -7 95.51 2.85 2 13 7 96.23 2.97 2 13 7 95.79 2.87 2 13 8 36.04 1.37 2 13 8 34.11 1.17 -2 -13 -9 173.00 5.12 -2 -13 -9 179.60 5.24 2 13 9 166.20 4.86 2 13 9 174.20 5.17 -2 -13 -10 60.19 1.86 -2 -13 -10 57.32 1.88 2 13 10 58.07 1.82 2 13 10 58.21 1.95 -2 -13 -11 157.40 4.59 -2 -13 -11 163.60 4.86 2 13 11 153.40 4.50 2 13 11 158.80 4.73 -2 -13 -12 0.51 0.47 -2 -13 -12 0.29 0.72 2 13 12 0.70 0.66 2 13 12 -0.21 0.81 -2 -13 -13 33.34 1.32 -2 -13 -13 34.05 1.19 2 13 13 34.09 1.40 2 13 13 29.42 1.19 -2 -13 -14 49.77 1.74 -2 -13 -14 51.82 1.65 2 13 14 49.41 1.71 2 13 14 47.42 1.72 -2 -13 -15 2.08 0.81 -2 -13 -15 2.18 0.64 2 13 15 3.37 0.85 2 13 15 2.00 0.88 -2 -13 -16 5.92 0.92 -2 -13 -16 5.83 0.72 2 13 16 4.13 0.93 2 13 16 3.77 0.97 -2 -13 -17 19.31 0.90 -2 -13 -17 20.65 1.20 2 13 17 19.00 1.11 2 13 17 21.21 1.25 -2 -13 -18 7.96 1.13 -2 -13 -18 7.06 0.79 2 13 18 7.17 0.93 2 13 18 6.54 1.25 -2 -13 -19 36.58 1.43 -2 -13 -19 33.99 1.55 2 13 19 34.58 1.82 2 13 19 36.28 1.57 -2 -13 -20 20.32 1.21 -2 -13 -20 21.19 1.46 2 13 20 21.62 1.94 2 13 20 25.43 1.55 -2 -14 5 86.89 2.72 -2 -14 5 91.52 3.11 2 14 -5 93.41 3.03 2 14 -5 89.15 2.74 -2 -14 4 4.41 1.21 -2 -14 4 3.51 0.83 2 14 -4 2.25 0.85 2 14 -4 3.40 1.17 -2 -14 3 167.40 5.00 -2 -14 3 160.50 4.73 2 14 -3 179.00 5.26 2 14 -3 177.30 5.31 -2 -14 2 0.03 0.98 -2 -14 2 -0.83 0.63 2 14 -2 -0.86 0.86 2 14 -2 -0.14 0.77 -2 -14 1 221.30 6.52 -2 -14 1 209.50 6.12 2 14 -1 218.20 6.45 2 14 -1 225.20 6.56 -2 -14 0 26.78 1.24 2 14 0 27.50 1.10 2 14 0 28.27 1.30 -2 -14 -1 274.60 7.95 -2 -14 -1 285.30 8.32 2 14 1 282.30 8.23 2 14 1 293.60 8.51 -2 -14 -2 57.81 1.85 -2 -14 -2 64.98 2.15 2 14 2 64.63 2.15 2 14 2 65.92 2.08 -2 -14 -3 276.40 8.06 -2 -14 -3 270.10 7.82 2 14 3 293.90 8.56 2 14 3 293.60 8.50 -2 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0.51 -2 -15 -6 3.25 0.75 2 15 6 2.54 0.80 2 15 6 2.19 0.58 -2 -15 -7 131.90 3.90 -2 -15 -7 136.20 4.09 2 15 7 130.00 3.91 2 15 7 136.40 4.04 -2 -15 -8 5.60 0.84 -2 -15 -8 5.52 0.63 2 15 8 4.06 0.65 2 15 8 2.91 0.81 -2 -15 -9 315.40 9.16 -2 -15 -9 333.00 9.61 2 15 9 305.50 8.88 2 15 9 306.00 8.85 -2 -15 -10 1.46 0.67 -2 -15 -10 0.33 0.58 2 15 10 -0.79 0.80 2 15 10 1.14 0.62 -2 -15 -11 420.90 12.11 -2 -15 -11 455.90 13.16 2 15 11 442.30 12.74 2 15 11 457.30 13.21 -2 -15 -12 0.90 0.62 -2 -15 -12 2.04 0.83 2 15 12 1.72 0.73 2 15 12 -0.09 0.73 -2 -15 -13 340.90 9.83 -2 -15 -13 334.00 9.70 2 15 13 330.10 9.55 2 15 13 338.70 9.85 -2 -15 -14 5.31 0.71 -2 -15 -14 4.40 0.94 2 15 14 4.73 0.80 2 15 14 2.62 1.01 -2 -15 -15 186.40 5.43 -2 -15 -15 176.40 5.26 2 15 15 177.40 5.23 2 15 15 175.70 5.25 -2 -15 -16 57.74 1.99 -2 -15 -16 55.15 1.81 2 15 16 53.77 1.91 2 15 16 55.45 2.02 -2 -15 -17 126.40 3.89 -2 -15 -17 128.50 3.82 2 15 17 123.10 3.84 2 15 17 125.10 3.79 -2 -15 -18 23.23 0.98 -2 -15 -18 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36.86 1.52 5 -10 7 35.70 1.34 -5 10 -8 35.71 1.44 -5 10 -8 34.76 1.48 5 -10 8 31.68 1.24 5 -10 8 34.50 1.54 -5 9 14 210.90 6.17 -5 9 14 220.10 6.43 5 -9 -14 223.90 6.56 5 -9 -14 210.90 6.18 -5 9 13 32.49 1.22 -5 9 13 31.46 1.21 5 -9 -13 35.83 1.25 5 -9 -13 31.46 1.17 -5 9 12 180.30 5.31 -5 9 12 182.00 5.36 -5 9 11 0.42 0.69 5 -9 -11 0.77 0.66 5 -9 -11 -0.40 0.56 -5 9 10 194.60 5.73 -5 9 10 194.60 5.71 5 -9 -10 196.50 5.75 5 -9 -10 190.00 5.58 -5 9 9 0.58 0.64 -5 9 9 0.53 0.65 5 -9 -9 0.60 0.57 5 -9 -9 -0.61 0.53 -5 9 8 270.90 7.92 -5 9 8 269.60 7.85 5 -9 -8 263.60 7.68 5 -9 -8 259.60 7.56 -5 9 7 3.10 0.62 -5 9 7 2.82 0.64 5 -9 -7 2.90 0.59 5 -9 -7 3.32 0.60 -5 9 6 501.60 14.49 -5 9 6 482.60 13.94 5 -9 -6 508.80 14.68 5 -9 -6 486.30 14.03 -5 9 5 145.50 4.33 -5 9 5 139.30 4.17 5 -9 -5 143.50 4.26 5 -9 -5 147.80 4.38 -5 9 4 702.50 20.21 -5 9 4 709.60 20.41 5 -9 -4 701.50 20.19 5 -9 -4 695.20 19.99 -5 9 3 0.80 0.61 -5 9 3 1.24 0.59 5 -9 -3 0.30 0.50 5 -9 -3 1.51 0.50 -5 9 2 697.20 20.07 -5 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508.80 14.68 6 -8 -4 487.80 14.05 -6 8 3 483.10 13.94 -6 8 3 496.10 14.33 6 -8 -3 458.90 13.22 6 -8 -3 493.00 14.24 -6 8 2 116.40 3.54 -6 8 2 123.30 3.70 6 -8 -2 116.40 3.53 6 -8 -2 117.10 3.49 -6 8 1 805.70 23.16 -6 8 1 816.70 23.45 6 -8 -1 795.60 22.88 6 -8 -1 749.70 21.52 -6 8 0 22.44 1.04 -6 8 0 24.58 1.01 6 -8 0 20.92 0.92 6 -8 0 21.68 0.90 -6 8 -1 821.10 23.60 -6 8 -1 850.80 24.43 6 -8 1 810.00 23.24 6 -8 1 853.90 24.53 -6 8 -2 41.53 1.43 -6 8 -2 41.56 1.47 6 -8 2 42.04 1.47 6 -8 2 40.94 1.37 -6 8 -3 449.20 12.98 -6 8 -3 445.20 12.83 6 -8 3 424.20 12.24 6 -8 3 447.20 12.94 -6 8 -4 5.76 0.62 -6 8 -4 4.53 0.64 6 -8 4 7.45 0.72 6 -8 4 6.26 0.62 -6 8 -5 173.40 5.15 -6 8 -5 175.80 5.16 6 -8 5 175.80 5.23 6 -8 5 172.80 5.07 -6 8 -6 1.10 0.65 -6 8 -6 0.00 0.80 6 -8 6 0.93 0.67 6 -8 6 -0.24 0.53 -6 8 -7 285.30 8.27 -6 8 -7 287.20 8.38 6 -8 7 297.90 8.63 6 -8 7 281.50 8.23 6 -8 7 283.60 8.22 -6 8 -8 40.08 1.57 -6 8 -8 44.01 1.54 6 -8 8 37.91 1.46 6 -8 8 36.39 1.32 6 -8 8 41.37 1.43 -6 8 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10.33 7 -8 -5 364.30 10.52 7 -8 -5 357.10 10.37 -7 8 4 204.00 6.05 -7 8 4 195.00 5.73 -7 8 3 207.90 6.11 -7 8 3 189.40 5.56 7 -8 -3 205.40 5.99 7 -8 -3 193.80 5.72 -7 8 2 92.12 2.80 -7 8 2 96.42 2.98 7 -8 -2 100.10 3.08 7 -8 -2 93.88 2.82 -7 8 1 93.97 2.86 -7 8 1 99.54 3.07 7 -8 -1 100.50 3.10 7 -8 -1 98.37 2.96 -7 8 0 118.70 3.60 -7 8 0 123.20 3.68 7 -8 0 117.30 3.50 7 -8 0 121.80 3.69 -7 8 -1 178.90 5.29 -7 8 -1 187.30 5.50 7 -8 1 182.50 5.39 7 -8 1 180.90 5.30 -7 8 -2 67.83 2.23 -7 8 -2 63.76 2.03 7 -8 2 63.41 2.06 7 -8 2 64.63 2.02 -7 8 -3 231.50 6.81 -7 8 -3 223.70 6.52 7 -8 3 232.00 6.81 7 -8 3 236.20 6.87 7 -8 3 215.40 6.27 -7 8 -4 9.57 0.78 -7 8 -4 10.66 0.75 7 -8 4 11.81 0.69 7 -8 4 11.63 0.84 7 -8 4 10.45 0.69 -7 8 -5 48.48 1.69 -7 8 -5 52.55 1.71 7 -8 5 50.51 1.66 7 -8 5 49.26 1.72 7 -8 5 45.83 1.53 -7 8 -6 127.50 3.87 -7 8 -6 134.30 3.98 7 -8 6 128.30 3.91 7 -8 6 129.30 3.86 -7 8 -7 12.29 1.07 -7 8 -7 11.81 0.81 7 -8 7 13.15 0.89 7 -8 7 11.79 1.00 -7 8 -8 103.90 3.16 7 -8 8 101.10 3.07 -7 7 12 13.03 0.85 -7 7 12 11.97 0.88 -7 7 11 123.00 3.66 -7 7 11 120.90 3.67 7 -7 -11 124.50 3.79 7 -7 -11 116.50 3.45 -7 7 10 26.41 1.09 7 -7 -10 24.37 0.96 7 -7 -10 24.30 1.14 -7 7 9 88.31 2.79 -7 7 9 89.63 2.73 7 -7 -9 94.86 2.95 7 -7 -9 93.28 2.83 -7 7 8 64.56 2.17 -7 7 8 63.84 2.01 7 -7 -8 65.77 2.07 7 -7 -8 64.27 2.09 -7 7 7 139.20 4.12 -7 7 7 131.60 4.00 7 -7 -7 136.80 4.05 7 -7 -7 133.30 3.99 -7 7 6 444.50 12.82 -7 7 6 443.20 12.85 7 -7 -6 444.50 12.86 7 -7 -6 445.70 12.85 -7 7 5 319.80 9.34 -7 7 5 322.70 9.35 7 -7 -5 335.90 9.72 7 -7 -5 338.90 9.85 7 -7 -5 322.00 9.31 -7 7 4 352.60 10.20 -7 7 4 338.10 9.86 -7 7 3 249.70 7.27 -7 7 3 248.20 7.27 7 -7 -3 238.80 6.94 7 -7 -3 257.70 7.49 7 -7 -3 250.40 7.32 -7 7 2 131.00 3.94 -7 7 2 127.60 3.80 7 -7 -2 135.60 4.01 7 -7 -2 132.70 3.99 7 -7 -2 122.90 3.64 -7 7 1 247.70 7.25 -7 7 1 242.80 7.08 7 -7 -1 248.50 7.21 7 -7 -1 243.00 7.11 7 -7 -1 237.90 6.91 -7 7 0 207.20 6.06 -7 7 0 213.30 6.27 7 -7 0 206.30 6.01 7 -7 0 208.90 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79.14 2.55 8 -9 1 85.75 2.62 8 -9 1 80.50 2.46 -8 9 -2 2.61 0.71 -8 9 -2 2.63 0.77 8 -9 2 2.03 0.66 8 -9 2 2.28 0.72 8 -9 2 3.01 0.79 -8 9 -3 98.26 3.00 -8 9 -3 99.19 3.09 8 -9 3 102.30 3.08 8 -9 3 95.80 2.98 8 -9 3 94.33 2.88 -8 9 -4 3.80 0.78 8 -9 4 4.57 0.77 -8 8 11 25.79 1.41 -8 8 11 24.91 1.36 8 -8 -11 23.50 1.45 8 -8 -11 25.10 1.20 -8 8 10 234.30 6.86 -8 8 10 229.70 6.77 8 -8 -10 215.20 6.32 8 -8 -10 227.90 6.63 -8 8 9 6.91 0.85 -8 8 9 4.97 0.95 8 -8 -9 7.20 0.94 8 -8 -9 5.91 0.68 -8 8 8 245.00 7.13 -8 8 8 254.10 7.49 8 -8 -8 240.50 7.06 8 -8 -8 260.00 7.55 -8 8 7 158.10 4.67 -8 8 7 151.40 4.58 8 -8 -7 156.40 4.61 8 -8 -7 155.80 4.66 -8 8 6 146.20 4.33 -8 8 6 144.90 4.42 8 -8 -6 141.50 4.18 8 -8 -6 143.90 4.34 -8 8 5 144.30 4.27 -8 8 5 135.20 4.11 8 -8 -5 141.70 4.26 8 -8 -5 141.40 4.19 -8 8 4 77.24 2.40 -8 8 4 77.59 2.53 8 -8 -4 70.78 2.22 8 -8 -4 73.11 2.37 -8 8 3 28.69 1.30 -8 8 3 28.21 1.14 8 -8 -3 27.93 1.17 8 -8 -3 30.12 1.11 8 -8 -2 0.71 0.80 8 -8 -2 0.35 0.52 8 -8 -2 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6 16 53.37 1.81 8 7 -6 29.00 1.55 8 7 -6 25.60 1.63 -8 -7 5 16.48 1.25 -8 -7 5 15.95 1.28 8 7 -5 14.77 1.33 8 7 -5 13.99 1.21 -8 -7 4 52.02 1.81 -8 -7 4 54.84 1.97 8 7 -4 44.82 1.68 8 7 -4 50.23 1.82 -8 -7 3 -0.19 0.77 -8 -7 3 0.41 0.85 8 7 -3 0.03 0.93 8 7 -3 0.58 0.82 -8 -7 2 75.68 2.41 -8 -7 2 76.45 2.46 8 7 -2 73.64 2.36 8 7 -2 72.41 2.37 -8 -7 1 6.63 0.86 -8 -7 1 6.53 0.76 8 7 -1 6.08 0.86 8 7 -1 7.70 0.76 -8 -7 0 88.10 2.72 -8 -7 0 93.68 2.86 8 7 0 86.71 2.67 8 7 0 88.23 2.71 -8 -7 -1 0.38 0.56 -8 -7 -1 0.35 0.74 8 7 1 -0.60 0.72 8 7 1 -0.26 0.77 -8 -7 -2 248.30 7.24 -8 -7 -2 252.10 7.34 8 7 2 264.20 7.72 8 7 2 287.00 8.35 -8 -7 -3 14.03 0.74 -8 -7 -3 14.94 0.78 8 7 3 13.29 0.76 8 7 3 14.16 0.89 -8 -7 -4 340.00 9.83 -8 -7 -4 342.20 9.90 8 7 4 345.70 10.00 8 7 4 339.70 9.79 -8 -7 -5 16.44 0.79 -8 -7 -5 18.13 0.84 8 7 5 16.57 0.91 8 7 5 18.28 0.79 -8 -7 -6 327.70 9.47 -8 -7 -6 325.10 9.40 8 7 6 320.90 9.26 8 7 6 311.70 9.03 -8 -7 -7 3.38 0.64 -8 -7 -7 1.96 0.62 8 7 7 3.44 0.60 8 7 7 1.83 0.68 -8 -7 -8 293.60 8.50 -8 -7 -8 295.90 8.58 8 7 8 287.50 8.34 8 7 8 310.00 8.96 -8 -7 -9 1.18 0.60 -8 -7 -9 1.00 0.64 8 7 9 2.32 0.63 8 7 9 2.28 0.60 -8 -7 -10 435.00 12.55 -8 -7 -10 411.20 11.84 8 7 10 392.30 11.34 8 7 10 429.00 12.35 8 7 11 0.43 0.77 8 7 11 0.58 0.63 -8 -7 -12 429.50 12.36 -8 -7 -12 435.80 12.58 8 7 12 444.70 12.79 8 7 12 447.50 12.93 -8 -7 -13 14.68 0.87 -8 -7 -13 14.74 0.83 -8 -7 -13 12.50 0.89 8 7 13 14.17 0.83 8 7 13 13.50 1.03 -8 -7 -14 139.30 4.18 -8 -7 -14 135.00 4.00 -8 -7 -14 131.00 3.95 8 7 14 134.70 3.98 8 7 14 130.70 3.96 -8 -7 -15 13.18 0.89 -8 -7 -15 15.02 1.05 8 7 15 13.28 0.90 8 7 15 13.45 1.10 -8 -7 -16 113.10 3.43 8 7 16 120.40 3.61 -8 -8 5 30.07 1.57 -8 -8 5 31.20 1.71 8 8 -5 26.40 1.50 8 8 -5 27.60 1.61 -8 -8 4 3.54 0.96 -8 -8 4 3.97 1.15 8 8 -4 4.33 1.09 8 8 -4 4.20 1.17 -8 -8 3 18.05 1.23 -8 -8 3 17.78 1.05 8 8 -3 18.82 1.09 8 8 -3 17.52 1.14 -8 -8 2 11.53 1.07 -8 -8 2 12.76 1.01 8 8 -2 12.93 1.06 8 8 -2 10.81 1.05 -8 -8 1 1.26 0.79 -8 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277.60 8.04 -9 7 4 21.84 1.16 -9 7 4 19.04 0.96 9 -7 -4 20.73 1.16 9 -7 -4 20.30 0.91 -9 7 3 297.10 8.61 -9 7 3 303.50 8.85 9 -7 -3 293.40 8.57 9 -7 -3 295.40 8.55 -9 7 2 3.32 0.68 -9 7 2 3.80 0.87 9 -7 -2 3.51 0.90 9 -7 -2 2.03 0.63 -9 7 1 122.10 3.73 -9 7 1 121.20 3.62 9 -7 -1 118.20 3.63 9 -7 -1 121.20 3.61 -9 7 0 4.22 0.84 -9 7 0 4.91 0.66 9 -7 0 4.50 0.71 9 -7 0 3.72 0.91 -9 7 -1 116.70 3.49 -9 7 -1 114.20 3.52 9 -7 1 119.50 3.65 9 -7 1 121.90 3.63 -9 7 -2 6.74 0.84 -9 7 -2 6.72 0.64 9 -7 2 7.64 0.73 9 -7 2 6.66 0.97 -9 7 -3 191.80 5.61 -9 7 -3 198.70 5.90 9 -7 3 189.70 5.64 9 -7 3 198.20 5.78 -9 7 -4 4.28 0.86 -9 7 -4 2.70 0.61 9 -7 4 4.17 1.01 9 -7 4 3.48 0.59 -9 6 9 142.20 4.39 -9 6 9 146.10 4.43 9 -6 -9 139.50 4.13 9 -6 -9 142.60 4.38 -9 6 8 39.37 1.52 -9 6 8 40.69 1.69 9 -6 -8 38.45 1.63 9 -6 -8 37.71 1.35 -9 6 7 151.20 4.56 -9 6 7 146.80 4.37 9 -6 -7 152.80 4.48 9 -6 -7 158.80 4.79 -9 6 6 77.51 2.43 -9 6 6 75.25 2.48 9 -6 -6 76.28 2.54 9 -6 -6 81.02 2.50 -9 6 5 211.40 6.28 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9 -3 2.55 1.12 -9 -9 2 65.78 2.21 -9 -9 2 73.86 2.63 9 9 -2 64.77 2.16 9 9 -2 64.49 2.30 -9 -9 1 11.31 1.40 -9 -9 1 11.00 1.02 9 9 -1 10.19 0.86 9 9 -1 10.59 1.05 -9 -9 0 32.52 1.54 -9 -9 0 30.75 1.34 9 9 0 31.12 1.50 9 9 0 29.40 1.39 -9 -9 -1 26.80 1.22 -9 -9 -1 30.42 1.33 9 9 1 27.75 1.27 9 9 1 24.84 1.21 -9 -9 -2 0.53 0.84 -9 -9 -2 1.12 0.90 9 9 2 2.15 0.83 9 9 2 0.04 0.98 -9 -9 -3 25.16 1.19 -9 -9 -3 22.94 1.15 9 9 3 25.32 1.28 9 9 3 22.61 1.00 -9 -9 -4 33.97 1.29 -9 -9 -4 33.23 1.34 9 9 4 32.76 1.41 9 9 4 33.96 1.34 -9 -9 -5 7.11 0.92 9 9 5 8.47 0.82 9 9 5 7.67 1.08 -9 -9 -6 74.06 2.33 -9 -9 -6 74.00 2.32 9 9 6 79.32 2.46 9 9 6 72.92 2.32 -9 -9 -7 63.05 2.01 -9 -9 -7 61.62 2.01 9 9 7 61.42 1.97 9 9 7 57.15 1.91 -9 -9 -8 1.63 0.75 -9 -9 -8 3.19 0.70 9 9 8 1.36 0.63 9 9 8 3.11 0.78 -9 -9 -9 48.40 1.64 -9 -9 -9 47.41 1.63 9 9 9 46.61 1.63 9 9 9 43.61 1.46 -9 -9 -10 0.48 0.65 -9 -9 -10 0.93 0.74 9 9 10 0.41 0.62 9 9 10 0.32 0.72 -9 -9 -11 19.93 0.91 -9 -9 -11 23.60 1.18 9 9 11 20.46 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13.30 1.28 10 -8 -6 16.05 0.96 10 -8 -6 15.23 1.32 -10 8 5 2.25 1.05 -10 8 5 2.63 1.13 10 -8 -5 0.61 0.79 10 -8 -5 1.61 1.01 -10 8 4 44.07 1.70 -10 8 4 40.43 1.65 10 -8 -4 43.54 1.71 10 -8 -4 43.11 1.50 -10 8 3 4.16 1.01 -10 8 3 2.80 0.89 10 -8 -3 2.90 0.80 10 -8 -3 3.53 1.16 -10 8 2 39.19 1.63 -10 8 2 38.86 1.48 10 -8 -2 39.75 1.72 10 -8 -2 40.71 1.47 -10 7 7 29.51 1.47 -10 7 7 28.81 1.50 10 -7 -7 30.30 1.53 10 -7 -7 29.18 1.24 -10 7 6 14.60 1.16 -10 7 6 14.43 1.24 10 -7 -6 14.14 0.87 10 -7 -6 14.54 1.26 -10 7 5 48.44 1.82 -10 7 5 53.92 1.96 10 -7 -5 54.78 1.79 10 -7 -5 50.48 1.92 -10 7 4 10.80 1.06 -10 7 4 10.00 1.06 10 -7 -4 11.23 1.14 10 -7 -4 9.85 0.81 -10 7 3 103.30 3.18 -10 7 3 95.38 3.02 10 -7 -3 100.20 3.02 10 -7 -3 103.10 3.29 -10 7 2 1.66 0.90 -10 7 2 2.11 0.86 10 -7 -2 4.50 1.08 10 -7 -2 2.86 0.64 -10 7 1 82.85 2.64 -10 7 1 89.10 2.78 10 -7 -1 87.20 2.82 10 -7 -1 84.67 2.58 -10 7 0 18.66 1.12 -10 7 0 17.76 0.99 10 -7 0 19.24 0.98 10 -7 0 19.12 1.23 -10 6 7 8.53 1.15 -10 6 7 9.27 1.20 10 -6 -7 6.35 1.33 10 -6 -7 7.83 0.89 -10 6 6 76.84 2.55 -10 6 6 72.46 2.40 10 -6 -6 75.31 2.53 10 -6 -6 67.81 2.11 -10 6 5 33.95 1.45 -10 6 5 30.57 1.38 10 -6 -5 33.17 1.20 10 -6 -5 33.03 1.51 -10 6 4 132.80 3.98 -10 6 4 140.40 4.27 10 -6 -4 136.10 4.18 10 -6 -4 136.00 4.02 -10 6 3 112.50 3.49 -10 6 3 116.60 3.53 10 -6 -3 112.50 3.35 10 -6 -3 111.40 3.50 -10 6 2 188.70 5.54 -10 6 2 187.50 5.58 10 -6 -2 186.70 5.57 10 -6 -2 190.80 5.55 -10 6 1 140.80 4.28 -10 6 1 143.40 4.27 10 -6 -1 139.70 4.11 10 -6 -1 141.60 4.28 -10 6 0 241.30 7.04 -10 6 0 239.50 7.06 10 -6 0 235.10 6.93 10 -6 0 224.40 6.52 -10 6 -1 44.35 1.75 -10 6 -1 43.04 1.59 10 -6 1 45.26 1.53 10 -6 1 44.37 1.71 -10 6 -2 295.80 8.57 -10 6 -2 276.60 8.12 10 -6 2 286.40 8.41 10 -6 2 291.10 8.42 -10 5 7 21.09 1.44 -10 5 7 21.27 1.39 10 -5 -7 20.56 1.02 10 -5 -7 18.85 1.44 -10 5 6 26.73 1.43 -10 5 6 26.53 1.39 10 -5 -6 26.80 1.52 10 -5 -6 28.58 1.16 -10 5 5 94.60 3.01 -10 5 5 88.30 2.74 10 -5 -5 90.70 2.73 10 -5 -5 91.99 2.91 -10 5 4 23.11 1.11 -10 5 4 24.72 1.26 10 -5 -4 26.21 1.37 10 -5 -4 22.57 0.95 -10 5 3 333.50 9.72 -10 5 3 320.50 9.28 10 -5 -3 330.10 9.63 10 -5 -3 327.20 9.45 -10 5 2 105.40 3.29 -10 5 2 96.90 2.98 10 -5 -2 95.40 2.87 10 -5 -2 98.99 3.13 -10 5 1 223.10 6.51 -10 5 1 223.20 6.58 10 -5 -1 227.80 6.62 10 -5 -1 220.90 6.53 -10 5 0 192.30 5.65 -10 5 0 192.30 5.71 10 -5 0 194.40 5.77 10 -5 0 196.10 5.70 -10 5 -1 71.20 2.25 -10 5 -1 65.59 2.22 10 -5 1 70.88 2.20 10 -5 1 68.85 2.34 -10 5 -2 274.10 7.96 -10 5 -2 267.60 7.87 10 -5 2 279.80 8.09 10 -5 2 263.90 7.75 -10 5 -3 31.67 1.26 -10 5 -3 28.27 1.29 10 -5 3 32.84 1.49 10 -5 3 31.01 1.15 -10 5 -4 157.30 4.74 -10 5 -4 166.50 4.91 10 -5 4 164.50 4.82 10 -5 4 165.30 5.00 -10 4 7 19.67 1.33 -10 4 7 19.36 1.40 10 -4 -7 20.73 1.48 10 -4 -7 19.26 1.03 -10 4 6 4.52 1.07 -10 4 6 4.73 0.96 10 -4 -6 3.91 0.74 10 -4 -6 4.41 1.19 -10 4 5 1.86 0.95 -10 4 5 2.47 1.12 10 -4 -5 1.82 0.68 10 -4 -5 1.26 1.01 -10 4 4 26.32 1.37 -10 4 4 24.20 1.19 10 -4 -4 23.09 1.29 10 -4 -4 24.40 1.03 -10 4 3 56.30 1.87 -10 4 3 58.73 2.07 10 -4 -3 56.93 1.80 10 -4 -3 56.91 2.05 -10 4 2 58.33 1.93 -10 4 2 65.02 2.14 10 -4 -2 61.04 2.12 10 -4 -2 59.09 1.86 -10 4 1 63.15 2.14 -10 4 1 63.16 2.00 10 -4 -1 61.83 2.12 10 -4 -1 65.59 2.02 -10 4 0 217.90 6.35 -10 4 0 228.30 6.72 10 -4 0 233.70 6.78 10 -4 0 227.60 6.71 -10 4 -1 21.72 1.15 -10 4 -1 20.92 0.95 10 -4 1 20.34 1.20 10 -4 1 20.93 0.92 -10 4 -2 308.90 9.02 -10 4 -2 310.80 9.00 10 -4 2 335.60 9.68 10 -4 2 312.40 9.12 -10 4 -3 3.79 0.86 -10 4 -3 3.45 0.77 10 -4 3 3.96 0.99 10 -4 3 3.97 0.64 -10 4 -4 315.00 9.10 -10 4 -4 322.70 9.40 10 -4 4 344.40 9.93 10 -4 4 331.80 9.68 -10 4 -5 -0.60 0.94 -10 4 -5 0.97 0.75 10 -4 5 0.75 0.63 10 -4 5 0.91 1.04 -10 3 7 68.66 2.34 -10 3 7 65.61 2.40 10 -3 -7 60.96 2.00 10 -3 -7 59.57 2.29 -10 3 6 63.71 2.30 -10 3 6 64.09 2.14 10 -3 -6 58.32 1.88 10 -3 -6 56.10 2.11 -10 3 5 31.54 1.34 -10 3 5 32.00 1.47 10 -3 -5 29.71 1.45 10 -3 -5 26.88 1.04 -10 3 4 44.52 1.63 -10 3 4 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3 -4 91.45 2.90 10 3 -4 82.73 2.73 -10 -3 3 310.20 8.99 -10 -3 3 293.60 8.59 10 3 -3 288.00 8.34 10 3 -3 300.20 8.76 -10 -3 2 213.90 6.35 -10 -3 2 213.10 6.24 10 3 -2 209.60 6.11 10 3 -2 206.60 6.12 -10 -3 1 159.60 4.82 -10 -3 1 167.80 4.95 10 3 -1 179.00 5.25 10 3 -1 161.10 4.87 -10 -3 0 135.40 4.01 -10 -3 0 127.90 3.92 -10 -3 -1 54.82 1.92 -10 -3 -1 58.71 1.90 10 3 1 56.68 1.80 10 3 1 58.82 2.05 -10 -3 -2 33.33 1.24 -10 -3 -2 34.34 1.37 10 3 3 48.92 1.58 10 3 3 49.78 1.81 -10 -3 -4 21.32 1.03 -10 -3 -4 21.01 1.02 10 3 4 21.24 0.85 10 3 4 21.36 1.20 -10 -3 -5 77.71 2.42 -10 -3 -5 77.48 2.47 10 3 5 76.57 2.47 10 3 5 75.03 2.28 -10 -3 -6 5.93 0.79 -10 -3 -6 6.23 0.81 10 3 6 7.54 0.94 10 3 6 6.57 0.63 -10 -3 -7 146.60 4.39 -10 -3 -7 147.10 4.34 10 3 7 147.30 4.30 10 3 7 148.60 4.46 -10 -3 -8 12.25 0.98 -10 -3 -8 11.55 0.80 10 3 8 11.15 0.71 10 3 8 10.53 0.99 -10 -3 -9 76.15 2.37 -10 -3 -9 77.42 2.51 10 3 9 72.96 2.40 10 3 9 79.98 2.40 -10 -3 -10 84.84 2.70 -10 -3 -10 78.72 2.45 10 3 10 76.68 2.51 10 3 10 81.15 2.44 -10 -4 5 49.25 2.01 -10 -4 4 25.47 1.49 -10 -4 4 30.78 1.51 10 4 -4 21.60 1.48 10 4 -4 22.04 1.28 -10 -4 3 78.04 2.48 -10 -4 3 76.58 2.63 -10 -4 2 195.70 5.80 -10 -4 2 204.00 5.99 10 4 -2 202.00 5.90 10 4 -2 199.00 5.89 -10 -4 1 106.10 3.21 -10 -4 1 108.80 3.39 10 4 -1 99.56 3.13 10 4 -1 102.70 3.11 -10 -4 0 253.90 7.38 -10 -4 0 249.40 7.30 10 4 0 245.30 7.20 10 4 0 248.90 7.22 -10 -4 -1 36.02 1.42 -10 -4 -1 35.67 1.33 10 4 1 33.54 1.36 10 4 1 36.64 1.34 -10 -4 -2 155.10 4.57 -10 -4 -2 152.30 4.54 10 4 2 147.40 4.42 10 4 2 160.40 4.69 -10 -4 -3 26.30 1.17 -10 -4 -3 26.49 1.11 10 4 3 23.56 1.10 10 4 3 25.25 1.02 -10 -4 -4 117.40 3.58 10 4 4 121.10 3.72 10 4 4 112.40 3.35 -10 -4 -5 93.12 2.83 -10 -4 -5 88.95 2.76 10 4 5 86.47 2.73 10 4 5 90.46 2.71 -10 -4 -6 121.70 3.63 -10 -4 -6 121.00 3.66 10 4 6 117.30 3.45 10 4 6 118.30 3.61 -10 -4 -7 269.70 7.82 -10 -4 -7 258.50 7.53 10 4 7 258.40 7.46 10 4 7 255.50 7.48 -10 -4 -8 116.10 3.51 -10 -4 -8 114.90 3.44 10 4 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2.32 0.94 -10 -6 -5 151.40 4.56 -10 -6 -5 144.40 4.37 10 6 5 165.90 4.89 10 6 5 161.60 4.88 -10 -6 -6 19.59 1.00 -10 -6 -6 19.20 1.07 -10 -6 -6 18.89 1.07 10 6 6 16.59 1.08 10 6 6 19.51 0.94 -10 -6 -7 15.09 0.90 -10 -6 -7 15.37 0.88 -10 -6 -7 13.67 0.99 10 6 7 15.01 0.84 10 6 7 14.57 1.08 -10 -6 -8 13.97 0.88 -10 -6 -8 14.73 0.91 -10 -6 -8 14.53 0.89 10 6 8 13.49 0.78 10 6 8 14.36 1.09 -10 -6 -9 0.86 0.73 -10 -6 -9 0.55 0.73 10 6 9 1.05 0.83 10 6 9 0.68 0.65 -10 -6 -10 0.17 0.70 10 6 10 1.96 0.60 -10 -7 2 10.31 1.19 -10 -7 2 11.09 1.53 -10 -7 2 10.09 1.15 10 7 -2 9.53 1.28 10 7 -2 12.90 1.23 -10 -7 1 76.38 2.50 -10 -7 1 81.79 2.64 -10 -7 1 73.24 2.50 10 7 -1 76.00 2.50 10 7 -1 73.77 2.42 -10 -7 0 3.08 1.00 -10 -7 0 3.09 0.87 -10 -7 0 3.94 1.07 10 7 0 3.46 0.98 10 7 0 3.59 0.85 -10 -7 -1 135.90 4.10 -10 -7 -1 133.50 4.00 10 7 1 139.10 4.21 10 7 1 137.50 4.13 10 7 2 32.99 1.39 10 7 2 35.75 1.41 -10 -7 -3 194.30 5.71 -10 -7 -3 197.80 5.80 10 7 3 200.40 5.92 10 7 3 183.50 5.38 -10 -7 -4 116.40 3.54 -10 -7 -4 111.60 3.37 10 7 4 111.50 3.35 10 7 4 117.40 3.60 -10 -7 -5 212.10 6.22 -10 -7 -5 204.40 5.99 10 7 5 214.40 6.32 10 7 5 197.90 5.77 -10 -7 -6 116.10 3.56 -10 -7 -6 111.80 3.35 10 7 6 114.20 3.52 10 7 6 105.90 3.17 -10 -7 -7 143.00 4.23 -10 -7 -7 134.30 4.03 10 7 7 136.00 4.00 10 7 7 141.20 4.26 -10 -7 -8 151.00 4.49 -10 -7 -8 150.40 4.44 -10 -7 -8 153.70 4.57 10 7 8 154.80 4.55 10 7 8 148.00 4.43 -10 -7 -9 68.22 2.17 -10 -7 -9 62.94 2.11 10 7 9 59.02 2.00 10 7 9 63.87 2.01 -10 -8 2 6.72 1.28 -10 -8 2 5.42 1.49 -10 -8 2 6.63 1.42 10 8 -2 4.41 1.29 10 8 -2 4.18 1.09 -10 -8 1 45.64 2.07 -10 -8 1 47.57 1.82 10 8 -1 52.83 1.94 10 8 -1 46.79 1.83 -10 -8 0 0.68 1.31 -10 -8 0 0.46 1.03 10 8 0 -0.32 1.08 10 8 0 0.78 0.99 -10 -8 -1 70.10 2.38 -10 -8 -1 73.50 2.41 10 8 1 69.01 2.25 10 8 1 63.07 2.09 -10 -8 -2 6.71 0.97 -10 -8 -2 7.66 1.01 10 8 2 6.03 0.93 10 8 2 5.62 1.10 -10 -8 -3 115.60 3.49 -10 -8 -3 118.10 3.62 10 8 3 117.00 3.56 10 8 3 114.70 3.49 -10 -8 -4 23.27 1.13 -10 -8 -4 25.17 1.25 10 8 4 23.80 1.17 10 8 4 24.61 1.10 -10 -8 -5 83.40 2.60 -10 -8 -5 77.64 2.50 10 8 5 74.71 2.33 10 8 5 78.02 2.50 -10 -8 -6 63.60 2.14 -10 -8 -6 63.95 2.10 10 8 6 59.65 2.06 10 8 6 55.22 1.84 -10 -8 -7 50.16 1.83 -10 -8 -7 51.09 1.71 10 8 7 48.50 1.63 10 8 7 49.07 1.78 -10 -8 -8 74.35 2.32 -10 -8 -8 81.72 2.60 10 8 8 79.37 2.58 10 8 8 77.90 2.38 -10 -9 1 1.87 1.49 -10 -9 1 1.95 1.24 10 9 -1 1.55 1.26 10 9 -1 0.63 1.33 -10 -9 0 10.68 1.38 -10 -9 0 6.92 1.19 10 9 0 7.51 1.15 10 9 0 8.56 1.19 -10 -9 -1 3.03 1.09 -10 -9 -1 1.73 1.24 10 9 1 -0.25 1.01 10 9 1 1.13 1.03 -10 -9 -2 9.96 1.09 -10 -9 -2 10.24 1.07 -10 -9 -3 14.67 1.15 -10 -9 -3 14.06 1.01 10 9 3 12.14 0.98 10 9 3 14.25 1.17 -10 -9 -4 14.08 1.13 -10 -9 -4 13.64 0.98 10 9 4 15.48 1.16 10 9 4 14.83 1.14 -10 -9 -5 53.70 1.80 -10 -9 -5 54.42 1.87 10 9 5 53.10 1.92 10 9 5 55.61 1.92 -10 -9 -6 24.12 1.17 10 9 6 23.64 1.21 -11 6 5 1.66 1.28 -11 6 5 2.66 1.51 11 -6 -5 1.44 1.31 11 -6 -5 3.16 0.96 -11 6 4 54.36 2.07 -11 6 4 55.56 2.12 11 -6 -4 52.74 2.08 11 -6 -4 55.86 1.85 -11 6 3 -1.73 1.15 11 -6 -3 1.16 0.98 11 -6 -3 -1.06 0.75 -11 5 5 55.75 2.16 -11 5 5 61.88 2.40 11 -5 -5 53.94 1.82 11 -5 -5 55.08 2.16 -11 5 4 98.61 3.17 -11 5 4 105.20 3.34 11 -5 -4 100.70 3.26 11 -5 -4 98.31 2.99 -11 5 3 63.47 2.26 -11 5 3 70.86 2.42 11 -5 -3 68.63 2.34 11 -5 -3 68.57 2.14 -11 5 2 160.30 4.78 -11 5 2 165.10 4.96 11 -5 -2 158.40 4.74 11 -5 -2 156.00 4.55 -11 5 1 47.69 1.78 -11 5 1 52.26 1.99 11 -5 -1 47.54 1.60 11 -5 -1 49.95 2.01 -11 4 5 18.11 1.54 -11 4 5 17.24 1.40 11 -4 -5 17.69 1.43 11 -4 -5 16.82 1.03 -11 4 4 107.60 3.43 -11 4 4 112.40 3.56 11 -4 -4 109.10 3.26 11 -4 -4 108.50 3.42 -11 4 3 9.59 1.30 -11 4 3 8.78 1.14 11 -4 -3 9.73 1.11 11 -4 -3 8.55 0.77 -11 4 2 112.00 3.50 -11 4 2 102.40 3.22 11 -4 -2 104.50 3.11 11 -4 -2 108.90 3.37 -11 4 1 14.62 0.99 -11 4 1 14.80 1.19 11 -4 -1 13.04 0.78 11 -4 -1 15.27 1.27 -11 4 0 85.73 2.66 -11 4 0 91.53 2.95 11 -4 0 93.20 3.02 11 -4 0 90.56 2.73 -11 4 -1 29.93 1.24 11 -4 1 34.48 1.24 -11 3 5 17.88 1.39 -11 3 5 15.83 1.46 11 -3 -5 14.78 1.39 11 -3 -5 15.10 1.06 -11 3 4 9.80 1.44 -11 3 4 12.87 1.24 11 -3 -4 10.59 0.89 11 -3 -4 9.30 1.19 -11 3 3 27.81 1.40 -11 3 3 23.30 1.42 11 -3 -3 26.61 1.45 11 -3 -3 25.01 1.09 -11 3 2 16.83 1.18 -11 3 2 18.32 1.29 11 -3 -2 16.54 0.85 11 -3 -2 17.47 1.13 -11 3 1 30.31 1.43 -11 3 1 31.70 1.33 11 -3 -1 30.17 1.15 11 -3 -1 31.13 1.54 -11 3 0 7.11 1.04 -11 3 0 7.32 0.94 11 -3 0 6.87 0.65 11 -3 0 6.62 1.19 -11 3 -1 48.33 1.71 -11 3 -1 45.74 1.76 11 -3 1 48.64 1.82 11 -3 1 47.31 1.57 -11 3 -2 34.44 1.50 -11 3 -2 34.81 1.45 11 -3 2 35.02 1.65 11 -3 2 35.84 1.25 -11 2 5 15.41 1.51 -11 2 5 12.19 1.44 11 -2 -5 13.91 1.47 11 -2 -5 12.84 1.05 -11 2 4 43.57 1.82 -11 2 4 42.50 1.86 11 -2 -4 38.97 1.42 11 -2 -4 37.82 1.63 -11 2 3 0.79 1.04 -11 2 3 -0.55 1.13 11 -2 -3 0.29 1.00 11 -2 -3 0.23 0.67 -11 2 2 7.69 1.05 -11 2 2 8.94 1.12 11 -2 -2 6.75 1.04 11 -2 -2 8.11 0.76 -11 2 1 -1.17 0.99 -11 2 1 1.53 0.84 11 -2 -1 1.72 1.13 11 -2 -1 0.09 0.66 11 -2 0 22.31 0.95 11 -2 0 21.17 1.34 -11 2 -1 17.43 1.13 -11 2 -1 16.17 1.10 11 -2 1 16.62 0.84 11 -2 1 17.67 1.27 11 -2 2 38.15 1.29 11 -2 2 37.51 1.62 -11 2 -3 20.09 1.26 -11 2 -3 19.67 1.06 11 -2 3 21.07 0.95 11 -2 3 21.11 1.29 -11 1 5 2.72 1.22 -11 1 5 1.12 1.13 -11 1 4 70.85 2.49 -11 1 4 73.84 2.52 11 -1 -4 66.89 2.39 11 -1 -4 68.47 2.20 -11 1 3 5.92 1.07 -11 1 3 6.82 1.20 11 -1 -3 6.00 1.07 11 -1 -3 6.54 0.79 -11 1 2 111.20 3.45 -11 1 2 116.00 3.54 11 -1 -2 123.10 3.76 11 -1 -2 117.80 3.48 -11 1 1 2.59 0.97 -11 1 1 2.32 0.89 11 -1 -1 3.51 0.71 11 -1 -1 2.03 0.97 -11 1 0 132.10 3.97 -11 1 0 140.20 4.27 11 -1 0 132.40 3.89 11 -1 0 130.40 4.03 11 -1 1 12.73 0.78 11 -1 1 11.73 1.12 -11 1 -2 169.10 4.99 -11 1 -2 175.60 5.26 11 -1 2 171.40 5.00 11 -1 2 170.30 5.10 -11 1 -3 31.36 1.35 -11 1 -3 32.19 1.39 11 -1 3 31.02 1.14 11 -1 3 29.79 1.45 -11 1 -4 77.93 2.52 -11 1 -4 73.35 2.48 11 -1 4 75.29 2.31 11 -1 4 73.62 2.51 -11 0 4 31.93 1.69 -11 0 4 30.27 1.53 11 0 -4 28.63 1.37 11 0 -4 26.82 1.59 -11 0 3 0.69 1.09 -11 0 3 -0.43 1.17 11 0 -3 -0.39 0.78 11 0 -3 0.18 1.00 -11 0 2 102.00 3.16 -11 0 2 104.10 3.29 11 0 -2 101.50 3.04 11 0 -2 99.58 3.12 -11 0 1 11.26 1.11 -11 0 1 11.16 1.07 11 0 -1 8.64 0.72 11 0 -1 9.25 1.16 -11 0 0 292.10 8.47 -11 0 0 290.10 8.47 11 0 0 285.20 8.24 11 0 0 286.50 8.40 -11 0 -1 74.82 2.47 -11 0 -1 68.94 2.20 11 0 1 69.97 2.16 11 0 1 74.30 2.44 -11 0 -2 323.50 9.36 -11 0 -2 309.70 9.02 11 0 2 314.10 9.06 11 0 2 308.70 9.02 -11 0 -3 87.49 2.70 -11 0 -3 92.03 2.90 11 0 3 85.34 2.59 11 0 3 95.46 3.06 -11 0 -4 235.40 6.87 -11 0 -4 223.60 6.58 11 0 4 227.30 6.72 11 0 4 227.60 6.60 -11 0 -5 122.20 3.69 -11 0 -5 120.60 3.72 11 0 5 130.50 3.85 11 0 5 118.20 3.71 -11 -1 4 -0.11 1.44 -11 -1 4 1.22 1.18 11 1 -4 0.19 1.04 11 1 -4 -1.09 1.26 -11 -1 3 10.75 1.36 -11 -1 3 9.74 1.17 11 1 -3 10.31 1.00 11 1 -3 9.52 1.13 -11 -1 2 3.89 1.02 -11 -1 2 3.53 1.14 11 1 -2 4.19 0.78 11 1 -2 3.36 1.03 -11 -1 1 17.40 1.16 -11 -1 1 16.95 1.21 11 1 -1 17.27 0.91 11 1 -1 16.24 1.12 -11 -1 0 70.38 2.28 -11 -1 0 74.57 2.46 11 1 0 68.81 2.15 11 1 0 71.80 2.43 -11 -1 -1 4.67 0.96 -11 -1 -1 2.34 0.93 11 1 1 4.21 0.62 11 1 1 5.51 1.04 -11 -1 -2 169.20 4.99 -11 -1 -2 166.80 4.95 11 1 2 161.50 4.86 11 1 2 171.20 4.99 -11 -1 -3 7.49 0.83 -11 -1 -3 8.76 0.98 11 1 3 6.98 0.70 11 1 3 7.32 0.97 -11 -1 -4 106.30 3.29 -11 -1 -4 111.10 3.35 11 1 4 114.70 3.56 11 1 4 115.70 3.43 -11 -1 -5 25.67 1.18 -11 -1 -5 26.74 1.39 11 1 5 31.30 1.52 11 1 5 31.50 1.18 -11 -2 3 15.61 1.27 -11 -2 3 13.56 1.30 11 2 -3 12.92 1.32 11 2 -3 16.28 1.11 -11 -2 2 26.59 1.41 -11 -2 2 26.43 1.35 11 2 -2 25.91 1.21 11 2 -2 25.41 1.31 -11 -2 1 -0.36 0.95 -11 -2 1 -0.45 1.07 11 2 -1 -1.29 1.00 11 2 -1 0.12 0.77 -11 -2 0 4.08 0.89 -11 -2 0 4.56 0.93 11 2 0 5.40 0.77 11 2 0 4.66 1.04 -11 -2 -1 4.08 0.85 -11 -2 -1 4.86 0.85 11 2 1 3.42 1.17 11 2 1 4.27 0.68 -11 -2 -2 50.16 1.84 -11 -2 -2 50.67 1.74 11 2 2 50.31 1.82 11 2 2 47.44 1.57 -11 -2 -3 5.18 0.89 -11 -2 -3 7.28 0.87 11 2 3 5.89 0.68 11 2 3 6.66 1.11 -11 -2 -4 90.78 2.84 -11 -2 -4 96.42 2.95 11 2 4 92.26 2.99 11 2 4 88.41 2.68 -11 -2 -5 47.38 1.67 -11 -2 -5 50.16 1.83 11 2 5 52.18 1.69 11 2 5 53.24 2.05 -11 -2 -6 29.32 1.26 11 2 6 27.81 1.12 -11 -3 3 18.67 1.44 -11 -3 3 18.20 1.35 11 3 -3 18.09 1.30 11 3 -3 17.61 1.40 -11 -3 2 167.90 5.01 -11 -3 2 164.70 4.95 11 3 -2 160.40 4.82 11 3 -2 155.50 4.59 -11 -3 1 67.34 2.34 -11 -3 1 69.22 2.35 11 3 -1 65.49 2.09 11 3 -1 64.56 2.21 -11 -3 0 142.40 4.27 -11 -3 0 136.50 4.12 -11 -3 -1 58.30 1.95 -11 -3 -1 60.52 2.10 11 3 1 58.13 1.90 11 3 1 59.47 2.18 -11 -3 -2 50.05 1.72 -11 -3 -2 51.45 1.82 11 3 2 47.94 1.61 11 3 2 52.10 1.95 -11 -3 -3 29.14 1.36 -11 -3 -3 29.25 1.25 11 3 3 25.77 1.07 11 3 3 28.24 1.43 -11 -3 -4 6.28 1.03 -11 -3 -4 7.63 0.82 11 3 4 5.88 0.71 11 3 4 5.78 0.98 -11 -3 -5 7.28 1.07 -11 -3 -5 7.67 0.91 11 3 5 6.73 0.66 11 3 5 4.65 1.07 -11 -3 -6 25.35 1.33 -11 -3 -6 26.54 1.22 11 3 6 27.45 1.04 11 3 6 23.60 1.31 -11 -4 2 167.30 5.03 -11 -4 2 172.70 5.20 -11 -4 1 27.28 1.42 -11 -4 1 26.63 1.43 11 4 -1 24.11 1.23 11 4 -1 28.45 1.52 -11 -4 0 153.40 4.60 -11 -4 0 149.60 4.52 11 4 0 137.60 4.07 11 4 0 137.80 4.17 -11 -4 -1 12.99 1.05 -11 -4 -1 14.62 1.13 11 4 1 13.92 0.94 11 4 1 15.84 1.29 -11 -4 -2 101.20 3.11 -11 -4 -2 102.80 3.21 11 4 2 104.30 3.15 11 4 2 101.80 3.25 -11 -4 -3 0.56 0.76 -11 -4 -3 1.66 0.98 11 4 3 0.72 0.73 11 4 3 1.64 0.95 -11 -4 -4 97.98 3.01 -11 -4 -4 100.50 3.11 11 4 4 93.95 2.84 11 4 4 99.52 3.18 -11 -4 -5 0.35 0.83 -11 -4 -5 0.61 0.86 11 4 5 0.00 0.70 11 4 5 1.84 1.08 -11 -4 -6 100.20 3.14 11 4 6 95.02 2.89 -11 -5 2 50.66 2.07 -11 -5 2 48.84 2.04 11 5 -2 42.84 1.97 11 5 -2 43.48 1.86 -11 -5 1 21.50 1.37 -11 -5 1 23.11 1.36 11 5 -1 19.97 1.23 11 5 -1 18.16 1.49 -11 -5 0 99.03 3.10 -11 -5 0 103.30 3.27 11 5 0 99.45 3.06 11 5 0 101.10 3.17 -11 -5 -1 24.92 1.29 -11 -5 -1 24.98 1.24 -11 -5 -2 115.40 3.54 -11 -5 -2 122.00 3.67 11 5 2 108.60 3.28 11 5 2 114.70 3.57 -11 -5 -3 27.60 1.21 -11 -5 -3 28.30 1.23 11 5 3 27.98 1.18 11 5 3 28.78 1.46 -11 -5 -4 162.00 4.81 -11 -5 -4 167.80 4.95 11 5 4 173.10 5.09 11 5 4 167.40 5.01 -11 -5 -5 8.32 0.92 -11 -5 -5 6.43 0.81 11 5 5 8.95 0.82 11 5 5 9.03 1.11 -11 -6 1 3.02 1.41 -11 -6 1 1.72 1.39 11 6 -1 1.01 1.21 11 6 -1 -0.03 1.19 -11 -6 0 1.74 1.22 -11 -6 0 0.18 1.06 11 6 0 1.25 1.10 11 6 0 2.74 1.12 -11 -6 -1 2.26 1.13 -11 -6 -1 2.79 0.98 11 6 1 1.99 0.99 11 6 1 1.68 0.95 -11 -6 -2 2.75 1.03 -11 -6 -2 2.03 0.98 11 6 2 -0.79 0.91 11 6 2 -0.22 1.06 -11 -6 -3 -1.06 0.98 -11 -6 -3 0.33 0.90 11 6 3 -0.51 0.91 11 6 3 1.07 0.80 -11 -6 -4 1.74 0.94 -11 -6 -4 0.29 0.84 11 6 4 2.47 0.73 11 6 4 2.16 0.88 -11 -7 0 75.13 2.59 -11 -7 0 79.14 2.87 11 7 0 66.78 2.30 11 7 0 70.00 2.42 -11 -7 -1 -0.51 1.23 -11 -7 -1 -1.38 0.99 11 7 1 -0.27 1.08 11 7 1 0.90 0.94 -11 -7 -2 22.02 1.28 11 7 2 24.90 1.30 12 1 -1 75.32 2.44 0 0 0 0.00 0.00 ; _shelx_res_checksum 99262 _shelx_res_file ; TITL P1bar in P-1 CELL 0.71073 8.097 12.604 14.441 64.276 82.421 86.696 ZERR 2 0.0016 0.0025 0.0029 0.03 0.03 0.03 LATT 1 SFAC C H F P Rh Cl UNIT 40 60 12 2 4 6 OMIT -3 50 L.S. 15 ACTA BOND $H FMAP 2 PLAN 20 SIZE 0.015 0.015 0.010 WGHT 0.018000 3.038100 FVAR 0.36831 MOLE 1 RH1A 5 0.100041 0.614633 0.242835 11.00000 0.01543 0.01295 = 0.01698 -0.00688 -0.00149 0.00227 C1A 1 0.128790 0.799517 0.185787 11.00000 0.02129 0.01288 = 0.02482 -0.00841 -0.00639 0.00337 C2A 1 0.085550 0.750067 0.295388 11.00000 0.02167 0.01678 = 0.02659 -0.01290 -0.00522 0.00557 C3A 1 -0.072183 0.691951 0.320291 11.00000 0.02274 0.01758 = 0.02526 -0.01133 -0.00020 0.00610 C4A 1 -0.128814 0.709051 0.223823 11.00000 0.01821 0.01622 = 0.02741 -0.01054 -0.00246 0.00591 C5A 1 -0.006892 0.776700 0.141371 11.00000 0.02022 0.01218 = 0.02492 -0.00672 -0.00496 0.00290 C6A 1 0.281640 0.869218 0.126431 11.00000 0.02342 0.02047 = 0.03408 -0.00779 -0.00678 -0.00171 AFIX 137 H6AA 2 0.372602 0.841422 0.167470 11.00000 -1.50000 H6AB 2 0.261641 0.950877 0.110154 11.00000 -1.50000 H6AC 2 0.308937 0.860163 0.063512 11.00000 -1.50000 AFIX 0 C7A 1 0.186684 0.757973 0.371696 11.00000 0.03574 0.02676 = 0.03066 -0.01632 -0.01250 0.00504 AFIX 137 H7AA 2 0.162059 0.691816 0.437635 11.00000 -1.50000 H7AB 2 0.159869 0.829582 0.378606 11.00000 -1.50000 H7AC 2 0.303030 0.757594 0.347820 11.00000 -1.50000 AFIX 0 C8A 1 -0.164082 0.627707 0.424820 11.00000 0.03052 0.02691 = 0.02520 -0.01056 0.00452 0.00566 AFIX 137 H8AA 2 -0.216748 0.559559 0.428266 11.00000 -1.50000 H8AB 2 -0.247301 0.678438 0.438031 11.00000 -1.50000 H8AC 2 -0.087677 0.603543 0.475817 11.00000 -1.50000 AFIX 0 C9A 1 -0.288374 0.664733 0.213802 11.00000 0.01971 0.02360 = 0.04267 -0.01511 -0.00418 0.00063 AFIX 137 H9AA 2 -0.277384 0.654390 0.151212 11.00000 -1.50000 H9AB 2 -0.375422 0.720520 0.211605 11.00000 -1.50000 H9AC 2 -0.315474 0.590636 0.272109 11.00000 -1.50000 AFIX 0 C10A 1 -0.017476 0.817305 0.029181 11.00000 0.02773 0.02447 = 0.02546 -0.00982 -0.00819 0.00225 AFIX 137 H10A 2 0.092732 0.824344 -0.006861 11.00000 -1.50000 H10B 2 -0.072021 0.892513 0.002540 11.00000 -1.50000 H10C 2 -0.079980 0.761305 0.019349 11.00000 -1.50000 AFIX 0 CL1 6 0.345720 0.515336 0.323530 11.00000 0.01402 0.01868 = 0.03675 -0.01534 -0.00638 0.00130 CL2 6 0.216079 0.550112 0.110606 11.00000 0.05347 0.02473 = 0.01809 -0.00772 -0.00131 0.01769 CL3 6 -0.008893 0.409723 0.327080 11.00000 0.01469 0.01725 = 0.03367 -0.01207 -0.00442 0.00028 RH1B 5 0.275831 0.371859 0.263182 11.00000 0.01803 0.01362 = 0.01822 -0.00785 -0.00374 0.00375 C1B 1 0.504292 0.297017 0.230478 11.00000 0.02161 0.01850 = 0.02393 -0.01271 -0.00643 0.00785 C2B 1 0.454141 0.240450 0.339881 11.00000 0.02167 0.01502 = 0.02648 -0.00927 -0.00849 0.00889 C3B 1 0.294355 0.187563 0.356798 11.00000 0.02733 0.01409 = 0.02768 -0.00859 -0.00756 0.00602 C4B 1 0.247866 0.208349 0.256793 11.00000 0.02489 0.01629 = 0.03033 -0.01315 -0.00660 0.00430 C5B 1 0.379494 0.273795 0.179748 11.00000 0.02268 0.01791 = 0.02779 -0.01406 -0.00709 0.00724 C6B 1 0.663743 0.362479 0.179015 11.00000 0.02236 0.02531 = 0.03154 -0.01621 -0.00458 0.00437 AFIX 137 H6BA 2 0.646507 0.423624 0.112223 11.00000 -1.50000 H6BB 2 0.747570 0.309076 0.170978 11.00000 -1.50000 H6BC 2 0.699488 0.396752 0.220815 11.00000 -1.50000 AFIX 0 C7B 1 0.552452 0.237282 0.421377 11.00000 0.02801 0.02583 = 0.02385 -0.01102 -0.00889 0.00534 AFIX 137 H7BA 2 0.611248 0.310292 0.396724 11.00000 -1.50000 H7BB 2 0.630864 0.173493 0.437262 11.00000 -1.50000 H7BC 2 0.478545 0.226020 0.482618 11.00000 -1.50000 AFIX 0 C8B 1 0.195458 0.117970 0.458460 11.00000 0.03349 0.02203 = 0.02925 -0.00541 -0.00167 -0.00020 AFIX 137 H8BA 2 0.227048 0.139952 0.509538 11.00000 -1.50000 H8BB 2 0.216610 0.035552 0.479064 11.00000 -1.50000 H8BC 2 0.078980 0.133557 0.452295 11.00000 -1.50000 AFIX 0 C9B 1 0.095101 0.162848 0.238548 11.00000 0.02772 0.02837 = 0.04330 -0.01981 -0.01001 0.00008 AFIX 137 H9BA 2 0.006961 0.155272 0.292475 11.00000 -1.50000 H9BB 2 0.118303 0.087268 0.238597 11.00000 -1.50000 H9BC 2 0.061769 0.216737 0.172835 11.00000 -1.50000 AFIX 0 C10B 1 0.383628 0.311069 0.066704 11.00000 0.02973 0.03037 = 0.02903 -0.01866 -0.00970 0.00737 AFIX 137 H10D 2 0.275626 0.339406 0.046049 11.00000 -1.50000 H10E 2 0.413679 0.245148 0.051318 11.00000 -1.50000 H10F 2 0.464250 0.372731 0.029719 11.00000 -1.50000 AFIX 0 MOLE 2 P1 4 0.655618 -0.008324 0.236696 11.00000 0.02113 0.01575 = 0.02771 -0.01124 -0.00445 0.00255 F1 3 0.698869 0.124095 0.156632 11.00000 0.05556 0.01690 = 0.07459 -0.01511 0.03071 -0.00485 F2 3 0.629201 0.030440 0.328641 11.00000 0.09986 0.04762 = 0.04881 -0.03718 -0.04337 0.04351 F3 3 0.609493 -0.140700 0.315466 11.00000 0.06336 0.01957 = 0.03747 -0.00584 0.01017 0.00821 F4 3 0.679269 -0.048009 0.144943 11.00000 0.07126 0.03190 = 0.02935 -0.01742 -0.00396 0.01410 F5 3 0.464198 0.019351 0.220944 11.00000 0.02650 0.03835 = 0.07570 -0.03482 -0.01708 0.01030 F6 3 0.845629 -0.036363 0.252774 11.00000 0.02965 0.05503 = 0.16261 -0.07597 -0.04068 0.01943 HKLF 4 REM P1bar in P-1 REM R1 = 0.0250 for 4064 Fo > 4sig(Fo) and 0.0254 for all 4158 data REM 299 parameters refined using 0 restraints END WGHT 0.0180 3.0380 REM Highest difference peak 1.026, deepest hole -0.565, 1-sigma level 0.075 Q1 1 0.3161 0.5759 0.1140 11.00000 0.05 1.03 Q2 1 0.3578 0.4010 0.2689 11.00000 0.05 0.50 Q3 1 0.2137 0.3443 0.3350 11.00000 0.05 0.47 Q4 1 0.2107 0.4413 0.2578 11.00000 0.05 0.44 Q5 1 0.0462 0.4345 -0.0106 11.00000 0.05 0.42 Q6 1 0.0323 0.4263 0.2642 11.00000 0.05 0.41 Q7 1 0.0405 0.5886 0.3146 11.00000 0.05 0.41 Q8 1 0.7766 -0.0312 0.1518 11.00000 0.05 0.40 Q9 1 0.5355 0.0513 0.1586 11.00000 0.05 0.40 Q10 1 0.1597 0.6435 0.1749 11.00000 0.05 0.40 Q11 1 0.1701 0.6390 0.2610 11.00000 0.05 0.37 Q12 1 0.2074 0.5195 0.2043 11.00000 0.05 0.33 Q13 1 0.2160 0.4823 0.1500 11.00000 0.05 0.32 Q14 1 -0.0945 0.6996 0.2693 11.00000 0.05 0.31 Q15 1 0.0522 0.6755 0.2291 11.00000 0.05 0.30 Q16 1 0.0871 0.3640 0.3425 11.00000 0.05 0.30 Q17 1 -0.0895 0.7563 0.1789 11.00000 0.05 0.29 Q18 1 0.0836 0.7623 0.1501 11.00000 0.05 0.29 Q19 1 0.3278 0.3930 0.1878 11.00000 0.05 0.29 Q20 1 0.7391 0.1029 0.2066 11.00000 0.05 0.28 ; _shelxl_version_number 2.013 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy Rh Rh1A 0.10004(3) 0.61463(2) 0.24284(2) 0.01511(8) Uani d 1 C C1A 0.1288(4) 0.7995(2) 0.1858(2) 0.0193(6) Uani d 1 C C2A 0.0856(4) 0.7501(2) 0.2954(2) 0.0204(6) Uani d 1 C C3A -0.0722(4) 0.6920(2) 0.3203(3) 0.0216(6) Uani d 1 C C4A -0.1288(4) 0.7091(2) 0.2238(2) 0.0205(6) Uani d 1 C C5A -0.0069(4) 0.7767(2) 0.1414(2) 0.0195(6) Uani d 1 C C6A 0.2816(4) 0.8692(3) 0.1264(3) 0.0270(7) Uani d 1 H H6AA 0.3726 0.8414 0.1675 0.041 Uiso calc 1 H H6AB 0.2616 0.9509 0.1102 0.041 Uiso calc 1 H H6AC 0.3089 0.8602 0.0635 0.041 Uiso calc 1 C C7A 0.1867(4) 0.7580(3) 0.3717(3) 0.0290(7) Uani d 1 H H7AA 0.1621 0.6918 0.4376 0.044 Uiso calc 1 H H7AB 0.1599 0.8296 0.3786 0.044 Uiso calc 1 H H7AC 0.3030 0.7576 0.3478 0.044 Uiso calc 1 C C8A -0.1641(4) 0.6277(3) 0.4248(3) 0.0288(7) Uani d 1 H H8AA -0.2167 0.5596 0.4283 0.043 Uiso calc 1 H H8AB -0.2473 0.6784 0.4380 0.043 Uiso calc 1 H H8AC -0.0877 0.6035 0.4758 0.043 Uiso calc 1 C C9A -0.2884(4) 0.6647(3) 0.2138(3) 0.0283(7) Uani d 1 H H9AA -0.2774 0.6544 0.1512 0.043 Uiso calc 1 H H9AB -0.3754 0.7205 0.2116 0.043 Uiso calc 1 H H9AC -0.3155 0.5906 0.2721 0.043 Uiso calc 1 C C10A -0.0175(4) 0.8173(3) 0.0292(3) 0.0258(7) Uani d 1 H H10A 0.0927 0.8243 -0.0069 0.039 Uiso calc 1 H H10B -0.0720 0.8925 0.0025 0.039 Uiso calc 1 H H10C -0.0800 0.7613 0.0193 0.039 Uiso calc 1 Cl Cl1 0.34572(8) 0.51534(6) 0.32353(6) 0.02165(16) Uani d 1 Cl Cl2 0.21608(12) 0.55011(7) 0.11061(6) 0.0337(2) Uani d 1 Cl Cl3 -0.00889(8) 0.40972(6) 0.32708(6) 0.02133(16) Uani d 1 Rh Rh1B 0.27583(3) 0.37186(2) 0.26318(2) 0.01627(8) Uani d 1 C C1B 0.5043(4) 0.2970(2) 0.2305(2) 0.0200(6) Uani d 1 C C2B 0.4541(4) 0.2404(2) 0.3399(2) 0.0208(6) Uani d 1 C C3B 0.2944(4) 0.1876(2) 0.3568(3) 0.0230(6) Uani d 1 C C4B 0.2479(4) 0.2083(2) 0.2568(3) 0.0226(6) Uani d 1 C C5B 0.3795(4) 0.2738(2) 0.1797(2) 0.0212(6) Uani d 1 C C6B 0.6637(4) 0.3625(3) 0.1790(3) 0.0250(7) Uani d 1 H H6BA 0.6465 0.4236 0.1122 0.038 Uiso calc 1 H H6BB 0.7476 0.3091 0.1710 0.038 Uiso calc 1 H H6BC 0.6995 0.3968 0.2208 0.038 Uiso calc 1 C C7B 0.5525(4) 0.2373(3) 0.4214(3) 0.0254(7) Uani d 1 H H7BA 0.6112 0.3103 0.3967 0.038 Uiso calc 1 H H7BB 0.6309 0.1735 0.4373 0.038 Uiso calc 1 H H7BC 0.4785 0.2260 0.4826 0.038 Uiso calc 1 C C8B 0.1955(4) 0.1180(3) 0.4585(3) 0.0305(7) Uani d 1 H H8BA 0.2270 0.1400 0.5095 0.046 Uiso calc 1 H H8BB 0.2166 0.0356 0.4791 0.046 Uiso calc 1 H H8BC 0.0790 0.1336 0.4523 0.046 Uiso calc 1 C C9B 0.0951(4) 0.1628(3) 0.2385(3) 0.0310(7) Uani d 1 H H9BA 0.0070 0.1553 0.2925 0.046 Uiso calc 1 H H9BB 0.1183 0.0873 0.2386 0.046 Uiso calc 1 H H9BC 0.0618 0.2167 0.1728 0.046 Uiso calc 1 C C10B 0.3836(4) 0.3111(3) 0.0667(3) 0.0273(7) Uani d 1 H H10D 0.2756 0.3394 0.0460 0.041 Uiso calc 1 H H10E 0.4137 0.2451 0.0513 0.041 Uiso calc 1 H H10F 0.4642 0.3727 0.0297 0.041 Uiso calc 1 P P1 0.65562(9) -0.00832(6) 0.23670(6) 0.02081(17) Uani d 1 F F1 0.6989(3) 0.12409(17) 0.1566(2) 0.0543(7) Uani d 1 F F2 0.6292(4) 0.0304(2) 0.32864(19) 0.0580(8) Uani d 1 F F3 0.6095(3) -0.14070(16) 0.31547(17) 0.0444(6) Uani d 1 F F4 0.6793(3) -0.04801(18) 0.14494(16) 0.0435(5) Uani d 1 F F5 0.4642(2) 0.01935(18) 0.2209(2) 0.0425(5) Uani d 1 F F6 0.8456(3) -0.0364(2) 0.2528(3) 0.0699(9) Uani d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Rh1A 0.01543(12) 0.01295(12) 0.01698(14) 0.00227(8) -0.00149(9) -0.00688(9) C1A 0.0213(14) 0.0129(13) 0.0248(17) 0.0034(11) -0.0064(13) -0.0084(11) C2A 0.0217(14) 0.0168(13) 0.0266(17) 0.0056(11) -0.0052(13) -0.0129(12) C3A 0.0227(14) 0.0176(14) 0.0253(18) 0.0061(11) -0.0002(13) -0.0113(12) C4A 0.0182(14) 0.0162(13) 0.0274(18) 0.0059(11) -0.0025(13) -0.0105(12) C5A 0.0202(14) 0.0122(12) 0.0249(17) 0.0029(10) -0.0050(13) -0.0067(11) C6A 0.0234(15) 0.0205(15) 0.0341(19) -0.0017(12) -0.0068(14) -0.0078(13) C7A 0.0357(17) 0.0268(16) 0.0307(19) 0.0050(13) -0.0125(15) -0.0163(14) C8A 0.0305(16) 0.0269(16) 0.0252(19) 0.0057(13) 0.0045(15) -0.0106(14) C9A 0.0197(15) 0.0236(15) 0.043(2) 0.0006(12) -0.0042(14) -0.0151(14) C10A 0.0277(16) 0.0245(15) 0.0255(18) 0.0022(12) -0.0082(14) -0.0098(13) Cl1 0.0140(3) 0.0187(3) 0.0367(4) 0.0013(2) -0.0064(3) -0.0153(3) Cl2 0.0535(5) 0.0247(4) 0.0181(4) 0.0177(3) -0.0013(4) -0.0077(3) Cl3 0.0147(3) 0.0172(3) 0.0337(4) 0.0003(2) -0.0044(3) -0.0121(3) Rh1B 0.01803(12) 0.01362(12) 0.01822(14) 0.00375(8) -0.00374(9) -0.00785(9) C1B 0.0216(14) 0.0185(13) 0.0239(17) 0.0078(11) -0.0064(13) -0.0127(12) C2B 0.0217(14) 0.0150(13) 0.0265(18) 0.0089(11) -0.0085(13) -0.0093(12) C3B 0.0273(15) 0.0141(13) 0.0277(18) 0.0060(11) -0.0076(14) -0.0086(12) C4B 0.0249(15) 0.0163(13) 0.0303(18) 0.0043(11) -0.0066(14) -0.0131(12) C5B 0.0227(14) 0.0179(14) 0.0278(18) 0.0072(11) -0.0071(13) -0.0141(12) C6B 0.0224(15) 0.0253(15) 0.0315(19) 0.0044(12) -0.0046(14) -0.0162(14) C7B 0.0280(16) 0.0258(15) 0.0238(18) 0.0053(12) -0.0089(14) -0.0110(13) C8B 0.0335(17) 0.0220(15) 0.0293(19) -0.0002(13) -0.0017(15) -0.0054(13) C9B 0.0277(16) 0.0284(16) 0.043(2) 0.0001(13) -0.0100(16) -0.0198(15) C10B 0.0297(16) 0.0304(16) 0.0290(19) 0.0074(13) -0.0097(15) -0.0187(14) P1 0.0211(4) 0.0157(4) 0.0277(5) 0.0025(3) -0.0044(3) -0.0112(3) F1 0.0556(14) 0.0169(10) 0.0746(19) -0.0048(9) 0.0307(13) -0.0151(10) F2 0.100(2) 0.0476(13) 0.0488(15) 0.0435(14) -0.0434(15) -0.0372(12) F3 0.0634(14) 0.0196(9) 0.0375(13) 0.0082(9) 0.0102(11) -0.0058(9) F4 0.0713(15) 0.0319(11) 0.0294(12) 0.0141(10) -0.0040(11) -0.0174(9) F5 0.0265(10) 0.0384(11) 0.0757(17) 0.0103(8) -0.0171(11) -0.0348(11) F6 0.0297(11) 0.0550(14) 0.163(3) 0.0194(10) -0.0407(15) -0.0760(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1A Rh1A C4A 66.16(11) C1A Rh1A C3A 66.24(12) C4A Rh1A C3A 39.78(12) C1A Rh1A C2A 39.13(12) C4A Rh1A C2A 65.91(11) C3A Rh1A C2A 39.26(12) C1A Rh1A C5A 39.53(11) C4A Rh1A C5A 38.91(12) C3A Rh1A C5A 65.94(12) C2A Rh1A C5A 65.55(11) C1A Rh1A Cl1 109.38(8) C4A Rh1A Cl1 158.78(9) C3A Rh1A Cl1 119.00(9) C2A Rh1A Cl1 97.15(8) C5A Rh1A Cl1 146.87(8) C1A Rh1A Cl2 110.16(9) C4A Rh1A Cl2 118.62(9) C3A Rh1A Cl2 158.36(9) C2A Rh1A Cl2 147.40(9) C5A Rh1A Cl2 97.28(9) Cl1 Rh1A Cl2 82.58(3) C1A Rh1A Cl3 164.71(8) C4A Rh1A Cl3 99.66(9) C3A Rh1A Cl3 99.37(9) C2A Rh1A Cl3 131.24(9) C5A Rh1A Cl3 131.26(8) Cl1 Rh1A Cl3 81.65(4) Cl2 Rh1A Cl3 81.16(4) C2A C1A C5A 107.8(3) C2A C1A C6A 126.4(3) C5A C1A C6A 125.7(3) C2A C1A Rh1A 71.08(16) C5A C1A Rh1A 71.05(15) C6A C1A Rh1A 126.3(2) C1A C2A C3A 108.5(3) C1A C2A C7A 126.0(3) C3A C2A C7A 125.5(3) C1A C2A Rh1A 69.79(16) C3A C2A Rh1A 69.86(16) C7A C2A Rh1A 126.5(2) C2A C3A C4A 107.4(3) C2A C3A C8A 127.1(3) C4A C3A C8A 125.5(3) C2A C3A Rh1A 70.88(17) C4A C3A Rh1A 70.09(17) C8A C3A Rh1A 125.2(2) C5A C4A C3A 108.2(3) C5A C4A C9A 126.5(3) C3A C4A C9A 125.3(3) C5A C4A Rh1A 71.25(16) C3A C4A Rh1A 70.13(16) C9A C4A Rh1A 125.1(2) C4A C5A C1A 108.0(3) C4A C5A C10A 126.1(3) C1A C5A C10A 125.9(3) C4A C5A Rh1A 69.83(16) C1A C5A Rh1A 69.42(15) C10A C5A Rh1A 126.6(2) C1A C6A H6AA 109.5 C1A C6A H6AB 109.5 H6AA C6A H6AB 109.5 C1A C6A H6AC 109.5 H6AA C6A H6AC 109.5 H6AB C6A H6AC 109.5 C2A C7A H7AA 109.5 C2A C7A H7AB 109.5 H7AA C7A H7AB 109.5 C2A C7A H7AC 109.5 H7AA C7A H7AC 109.5 H7AB C7A H7AC 109.5 C3A C8A H8AA 109.5 C3A C8A H8AB 109.5 H8AA C8A H8AB 109.5 C3A C8A H8AC 109.5 H8AA C8A H8AC 109.5 H8AB C8A H8AC 109.5 C4A C9A H9AA 109.5 C4A C9A H9AB 109.5 H9AA C9A H9AB 109.5 C4A C9A H9AC 109.5 H9AA C9A H9AC 109.5 H9AB C9A H9AC 109.5 C5A C10A H10A 109.5 C5A C10A H10B 109.5 H10A C10A H10B 109.5 C5A C10A H10C 109.5 H10A C10A H10C 109.5 H10B C10A H10C 109.5 Rh1A Cl1 Rh1B 82.26(3) Rh1A Cl2 Rh1B 81.99(3) Rh1B Cl3 Rh1A 80.78(4) C1B Rh1B C4B 66.30(12) C1B Rh1B C3B 66.24(12) C4B Rh1B C3B 39.79(12) C1B Rh1B C5B 39.35(11) C4B Rh1B C5B 39.13(12) C3B Rh1B C5B 65.93(12) C1B Rh1B C2B 39.27(12) C4B Rh1B C2B 65.99(11) C3B Rh1B C2B 39.15(12) C5B Rh1B C2B 65.51(11) C1B Rh1B Cl1 106.37(8) C4B Rh1B Cl1 160.83(9) C3B Rh1B Cl1 121.24(9) C5B Rh1B Cl1 142.82(8) C2B Rh1B Cl1 96.84(8) C1B Rh1B Cl2 109.99(9) C4B Rh1B Cl2 116.63(9) C3B Rh1B Cl2 156.37(9) C5B Rh1B Cl2 95.96(9) C2B Rh1B Cl2 147.91(9) Cl1 Rh1B Cl2 82.39(3) C1B Rh1B Cl3 166.37(8) C4B Rh1B Cl3 102.35(9) C3B Rh1B Cl3 100.28(10) C5B Rh1B Cl3 134.81(8) C2B Rh1B Cl3 130.39(9) Cl1 Rh1B Cl3 81.93(3) Cl2 Rh1B Cl3 81.46(5) C2B C1B C5B 108.0(3) C2B C1B C6B 125.8(3) C5B C1B C6B 126.1(3) C2B C1B Rh1B 71.41(16) C5B C1B Rh1B 71.21(16) C6B C1B Rh1B 125.8(2) C3B C2B C1B 108.2(3) C3B C2B C7B 126.3(3) C1B C2B C7B 125.6(3) C3B C2B Rh1B 69.76(16) C1B C2B Rh1B 69.32(15) C7B C2B Rh1B 126.7(2) C2B C3B C4B 107.8(3) C2B C3B C8B 126.9(3) C4B C3B C8B 125.2(3) C2B C3B Rh1B 71.09(16) C4B C3B Rh1B 70.09(16) C8B C3B Rh1B 126.6(2) C5B C4B C3B 107.7(3) C5B C4B C9B 126.3(3) C3B C4B C9B 125.9(3) C5B C4B Rh1B 70.96(16) C3B C4B Rh1B 70.12(16) C9B C4B Rh1B 127.2(2) C4B C5B C1B 108.3(3) C4B C5B C10B 125.2(3) C1B C5B C10B 126.5(3) C4B C5B Rh1B 69.91(17) C1B C5B Rh1B 69.44(16) C10B C5B Rh1B 126.2(2) C1B C6B H6BA 109.5 C1B C6B H6BB 109.5 H6BA C6B H6BB 109.5 C1B C6B H6BC 109.5 H6BA C6B H6BC 109.5 H6BB C6B H6BC 109.5 C2B C7B H7BA 109.5 C2B C7B H7BB 109.5 H7BA C7B H7BB 109.5 C2B C7B H7BC 109.5 H7BA C7B H7BC 109.5 H7BB C7B H7BC 109.5 C3B C8B H8BA 109.5 C3B C8B H8BB 109.5 H8BA C8B H8BB 109.5 C3B C8B H8BC 109.5 H8BA C8B H8BC 109.5 H8BB C8B H8BC 109.5 C4B C9B H9BA 109.5 C4B C9B H9BB 109.5 H9BA C9B H9BB 109.5 C4B C9B H9BC 109.5 H9BA C9B H9BC 109.5 H9BB C9B H9BC 109.5 C5B C10B H10D 109.5 C5B C10B H10E 109.5 H10D C10B H10E 109.5 C5B C10B H10F 109.5 H10D C10B H10F 109.5 H10E C10B H10F 109.5 F6 P1 F2 90.85(15) F6 P1 F3 89.65(15) F2 P1 F3 90.74(14) F6 P1 F1 91.30(15) F2 P1 F1 89.88(15) F3 P1 F1 178.86(16) F6 P1 F5 179.7(2) F2 P1 F5 89.10(14) F3 P1 F5 90.11(13) F1 P1 F5 88.95(13) F6 P1 F4 89.88(15) F2 P1 F4 179.11(16) F3 P1 F4 88.76(12) F1 P1 F4 90.60(13) F5 P1 F4 90.17(13) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Rh1A C1A 2.123(3) Rh1A C4A 2.126(3) Rh1A C3A 2.127(3) Rh1A C2A 2.140(3) Rh1A C5A 2.145(3) Rh1A Cl1 2.4372(11) Rh1A Cl2 2.4448(10) Rh1A Cl3 2.4860(11) C1A C2A 1.428(5) C1A C5A 1.443(4) C1A C6A 1.493(4) C2A C3A 1.434(4) C2A C7A 1.496(4) C3A C4A 1.447(4) C3A C8A 1.483(5) C4A C5A 1.423(4) C4A C9A 1.485(4) C5A C10A 1.485(4) C6A H6AA 0.9600 C6A H6AB 0.9600 C6A H6AC 0.9600 C7A H7AA 0.9600 C7A H7AB 0.9600 C7A H7AC 0.9600 C8A H8AA 0.9600 C8A H8AB 0.9600 C8A H8AC 0.9600 C9A H9AA 0.9600 C9A H9AB 0.9600 C9A H9AC 0.9600 C10A H10A 0.9600 C10A H10B 0.9600 C10A H10C 0.9600 Cl1 Rh1B 2.4426(9) Cl2 Rh1B 2.4485(13) Cl3 Rh1B 2.4675(10) Rh1B C1B 2.119(3) Rh1B C4B 2.129(3) Rh1B C3B 2.129(3) Rh1B C5B 2.142(3) Rh1B C2B 2.147(3) C1B C2B 1.434(5) C1B C5B 1.435(4) C1B C6B 1.496(4) C2B C3B 1.433(4) C2B C7B 1.491(4) C3B C4B 1.449(4) C3B C8B 1.490(5) C4B C5B 1.430(5) C4B C9B 1.492(4) C5B C10B 1.486(5) C6B H6BA 0.9600 C6B H6BB 0.9600 C6B H6BC 0.9600 C7B H7BA 0.9600 C7B H7BB 0.9600 C7B H7BC 0.9600 C8B H8BA 0.9600 C8B H8BB 0.9600 C8B H8BC 0.9600 C9B H9BA 0.9600 C9B H9BB 0.9600 C9B H9BC 0.9600 C10B H10D 0.9600 C10B H10E 0.9600 C10B H10F 0.9600 P1 F6 1.583(2) P1 F2 1.589(2) P1 F3 1.590(2) P1 F1 1.591(2) P1 F5 1.593(2) P1 F4 1.594(2) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA C8A H8AB F3 1_465 0.96 2.53 3.244(5) 131 C10A H10A F1 2_665 0.96 2.43 3.328(4) 156 C6B H6BB F1 . 0.96 2.49 3.152(5) 126