Crystallography Open Database

Information card for entry 2239112

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Structure parameters

Chemical name	(1,4,7,10,13,16-Hexaoxacyclooctadecane-κ^6^<i>O</i>)bis(tetrahydrofuran-κ<i>O</i>)potassium bis[(1,2,3,4-η)-anthracene]cobalt(-I) tetrahydrofuran monosolvate
Formula	C52 H68 Co K O9
Calculated formula	C52 H68 Co K O9
Title of publication	(1,4,7,10,13,16-Hexaoxacyclooctadecane-κ^6^<i>O</i>)bis(tetrahydrofuran-κ<i>O</i>)potassium bis[(1,2,3,4-η)-anthracene]cobalt({-}I) tetrahydrofuran monosolvate
Authors of publication	He, Haiyan; Klein, Wilhelm; Fässler, Thomas F.
Journal of publication	Acta Crystallographica Section E
Year of publication	2014
Journal volume	70
Journal issue	1
Pages of publication	m9 - m10
a	13.0428 ± 0.001 Å
b	13.3557 ± 0.001 Å
c	27.4939 ± 0.0017 Å
α	90°
β	90°
γ	90°
Cell volume	4789.3 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.1157
Residual factor for significantly intense reflections	0.0454
Weighted residual factors for significantly intense reflections	0.0668
Weighted residual factors for all reflections included in the refinement	0.0758
Goodness-of-fit parameter for all reflections included in the refinement	0.765
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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