#------------------------------------------------------------------------------ #$Date: 2022-07-23 05:07:00 +0100 (Sat, 23 Jul 2022) $ #$Revision: 276895 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/41/2244125.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244125 loop_ _publ_author_name 'Velazquez-Garcia, Jose de Jesus' 'Techert, Simone' _publ_section_title ; Synthesis and structure of hexaaquacobalt bis(2-methyl-1H-imidazol-3-ium) tetraaquabis(benzene-1,3,5-tricarboxylato-\kO)cobalt ; _journal_coeditor_code JQ2016 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989022007046 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac '(C4 H7 N2)2 [Co (H2 O)6] [Co (C9 H3 O6)2 (H2 O)4]' _chemical_formula_moiety 'C18 H14 Co O16, Co H12 O6, 2(C4 H7 N2)' _chemical_formula_sum 'C26 H40 Co2 N4 O22' _chemical_formula_weight 878.48 _chemical_name_systematic ; Hexaaquacobalt bis(2-methyl-1H-imidazol-3-ium) tetraaquabis(benzene-1,3,5-tricarboxylato-\kO)cobalt ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary difmap _atom_sites_solution_secondary dual _audit_creation_method SHELXL-2019/2 _cell_angle_alpha 86.551(2) _cell_angle_beta 79.378(2) _cell_angle_gamma 72.369(2) _cell_formula_units_Z 1 _cell_length_a 9.2008(4) _cell_length_b 9.3137(4) _cell_length_c 10.6470(4) _cell_measurement_reflns_used 9913 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 30.636 _cell_measurement_theta_min 2.295 _cell_volume 854.61(6) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX2 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2019/2 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2018) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device_type 'Bruker CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0260 _diffrn_reflns_av_unetI/netI 0.0221 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 26203 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.721 _diffrn_reflns_theta_min 1.946 _exptl_absorpt_coefficient_mu 1.069 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6994 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour 'clear light pink' _exptl_crystal_density_diffrn 1.707 _exptl_crystal_description prism _exptl_crystal_F_000 454 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.595 _refine_diff_density_min -0.421 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.036 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 285 _refine_ls_number_reflns 5250 _refine_ls_number_restraints 47 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.0315 _refine_ls_R_factor_gt 0.0263 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0331P)^2^+0.4935P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0662 _refine_ls_wR_factor_ref 0.0693 _reflns_number_gt 4605 _reflns_number_total 5250 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jq2016sup1.cif _cod_data_source_block I _cod_database_code 2244125 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.815 _shelx_estimated_absorpt_t_max 0.901 _shelx_hkl_file ; -1 0 0 216.28 5.00 -1 0 0 224.58 5.30 -1 0 0 221.88 5.00 -1 0 0 217.88 5.20 -1 0 0 217.58 4.80 -1 0 0 213.98 5.40 1 0 0 215.58 5.10 1 0 0 212.28 5.40 -2 0 0 893.01 18.70 -2 0 0 892.91 20.30 -2 0 0 896.81 19.10 -2 0 0 883.21 19.70 -2 0 0 876.91 18.40 -2 0 0 881.41 18.70 -2 0 0 896.11 20.10 2 0 0 896.91 19.10 2 0 0 904.01 20.40 -3 0 0 31.80 2.10 -3 0 0 31.70 2.00 -3 0 0 28.70 1.90 -3 0 0 34.70 1.80 -3 0 0 32.60 2.20 -3 0 0 32.80 1.90 3 0 0 32.70 2.30 -4 0 0 425.06 12.30 -4 0 0 438.46 12.00 -4 0 0 463.25 12.60 -4 0 0 462.65 11.60 -4 0 0 438.36 11.50 -4 0 0 457.95 11.10 4 0 0 471.75 12.90 4 0 0 430.86 11.80 -5 0 0 516.35 12.80 -5 0 0 525.75 14.60 -5 0 0 496.95 13.40 -5 0 0 505.95 13.20 -5 0 0 502.55 14.40 -5 0 0 502.65 13.30 -5 0 0 489.15 13.90 5 0 0 522.85 14.90 5 0 0 506.75 13.80 -6 0 0 47.40 3.40 -6 0 0 50.19 3.90 -6 0 0 55.89 3.80 -6 0 0 47.10 3.60 -6 0 0 48.20 3.30 -6 0 0 51.09 3.20 6 0 0 52.99 3.90 -7 0 0 40.60 3.40 -7 0 0 49.60 4.60 -7 0 0 49.70 4.00 -7 0 0 47.70 4.50 -7 0 0 34.70 3.90 -7 0 0 50.19 3.40 7 0 0 43.60 4.50 -8 0 0 453.45 15.60 -8 0 0 483.55 14.20 -8 0 0 445.76 13.30 -8 0 0 453.45 15.10 -8 0 0 472.85 14.90 -8 0 0 452.45 14.50 8 0 0 463.65 15.20 -9 0 0 372.96 14.20 -9 0 0 387.36 13.90 -9 0 0 342.67 12.90 -9 0 0 350.86 11.90 -9 0 0 380.66 13.80 -9 0 0 359.06 12.50 9 0 0 337.67 13.50 -10 0 0 532.45 16.30 -10 0 0 540.25 17.70 -10 0 0 540.35 18.30 -10 0 0 550.44 18.60 -10 0 0 513.95 18.90 10 0 0 533.85 18.50 -11 0 0 1.10 2.50 -11 0 0 1.40 2.00 -11 0 0 0.70 2.50 -11 0 0 1.40 2.60 -11 0 0 3.20 2.80 11 0 0 0.90 2.30 -12 0 0 285.37 14.50 -12 0 0 276.17 13.30 -12 0 0 283.17 13.90 12 0 0 284.07 14.20 12 0 0 264.37 12.60 12 -1 0 0.60 3.80 12 -1 0 5.00 3.30 -12 1 0 5.10 3.70 -12 1 0 1.40 2.90 -12 1 0 0.50 3.10 11 -1 0 7.30 3.30 11 -1 0 3.30 3.10 -11 1 0 6.60 3.50 -11 1 0 -0.10 2.50 -11 1 0 2.60 3.00 -11 1 0 9.00 3.10 -11 1 0 1.30 2.50 10 -1 0 29.20 4.90 10 -1 0 23.50 3.90 -10 1 0 27.40 4.60 -10 1 0 21.90 4.10 -10 1 0 24.60 3.80 -10 1 0 24.60 4.50 -10 1 0 31.30 4.60 9 -1 0 34.20 4.90 -9 1 0 35.50 4.80 -9 1 0 35.20 4.10 -9 1 0 49.20 5.70 -9 1 0 31.90 4.50 -9 1 0 38.90 5.00 8 -1 0 6.60 2.50 -8 1 0 5.70 2.40 -8 1 0 5.70 1.80 -8 1 0 7.00 2.00 -8 1 0 5.00 2.30 -8 1 0 4.40 1.90 -8 1 0 13.00 2.90 7 -1 0 109.59 6.10 -7 1 0 90.39 5.40 -7 1 0 100.99 5.10 -7 1 0 105.59 6.10 -7 1 0 112.89 6.30 -7 1 0 105.89 6.00 6 -1 0 30.00 3.40 -6 1 0 46.60 4.50 -6 1 0 48.30 3.20 -6 1 0 40.50 4.10 -6 1 0 48.20 3.50 -6 1 0 40.40 4.00 5 -1 0 137.19 5.90 5 -1 0 152.18 6.80 -5 1 0 138.59 6.40 -5 1 0 133.49 5.90 -5 1 0 141.49 5.60 -5 1 0 128.09 5.90 -5 1 0 128.59 5.10 -5 1 0 132.39 5.80 4 -1 0 0.80 0.90 4 -1 0 2.30 1.30 -4 1 0 -0.50 0.30 -4 1 0 2.00 0.90 -4 1 0 0.50 0.80 -4 1 0 0.50 0.80 -4 1 0 0.10 0.80 -4 1 0 1.40 0.90 -4 1 0 1.90 1.00 3 -1 0 95.49 4.20 3 -1 0 89.39 3.80 3 -1 0 94.99 3.40 -3 1 0 90.39 3.30 -3 1 0 92.59 3.90 -3 1 0 87.19 3.70 -3 1 0 93.39 3.60 -3 1 0 87.29 3.40 -3 1 0 93.09 4.20 2 -1 0 8.60 1.20 2 -1 0 12.40 1.20 2 -1 0 8.80 1.30 2 -1 0 9.90 1.30 -2 1 0 10.20 1.20 -2 1 0 11.90 1.30 -2 1 0 9.30 1.10 -2 1 0 12.30 1.10 -2 1 0 5.00 0.90 -2 1 0 11.10 1.40 1 -1 0 173.28 4.30 1 -1 0 171.48 4.20 1 -1 0 167.88 4.50 1 -1 0 170.08 4.90 1 -1 0 160.38 4.70 -1 1 0 172.28 4.90 -1 1 0 176.48 4.50 -1 1 0 170.28 4.30 -1 1 0 167.58 4.20 -1 1 0 174.38 4.60 -1 1 0 175.68 5.00 -1 1 0 173.08 4.10 0 -1 0 350.46 7.70 0 -1 0 356.76 7.40 0 -1 0 352.96 8.20 0 -1 0 348.57 7.90 0 -1 0 340.97 7.50 0 -1 0 339.87 8.10 0 -1 0 346.47 7.40 0 1 0 339.77 8.20 0 1 0 350.86 7.40 0 1 0 347.77 7.90 0 1 0 349.57 7.80 0 1 0 360.46 8.20 -1 -1 0 98.19 3.00 -1 -1 0 100.69 3.00 -1 -1 0 103.99 2.70 -1 -1 0 102.49 3.10 -1 -1 0 103.09 2.80 -1 -1 0 81.99 2.80 1 1 0 101.49 2.60 1 1 0 99.29 3.00 1 1 0 99.59 3.10 -2 -1 0 66.89 2.50 -2 -1 0 61.39 2.40 -2 -1 0 66.49 2.20 -2 -1 0 69.99 2.20 -2 -1 0 68.59 2.60 -2 -1 0 66.89 2.60 -2 -1 0 69.79 2.70 2 1 0 62.09 2.40 2 1 0 62.89 2.60 -3 -1 0 34.20 2.10 -3 -1 0 36.40 2.10 -3 -1 0 39.70 2.20 -3 -1 0 37.10 1.80 -3 -1 0 38.20 2.30 -3 -1 0 37.30 1.90 3 1 0 40.80 2.40 -4 -1 0 20.80 2.10 -4 -1 0 23.80 1.90 -4 -1 0 22.60 2.30 -4 -1 0 24.40 1.70 -4 -1 0 24.90 2.60 -4 -1 0 24.30 2.00 -4 -1 0 25.10 2.60 4 1 0 26.40 2.30 -5 -1 0 116.29 4.40 -5 -1 0 121.79 5.40 -5 -1 0 122.49 5.10 -5 -1 0 117.59 4.80 -5 -1 0 108.79 5.00 -5 -1 0 119.19 5.00 -5 -1 0 122.99 5.50 5 1 0 124.49 5.70 5 1 0 123.69 5.30 -6 -1 0 47.10 3.40 -6 -1 0 52.79 3.80 -6 -1 0 48.90 3.70 -6 -1 0 47.70 3.40 -6 -1 0 47.00 3.00 -6 -1 0 49.99 3.40 -6 -1 0 47.80 3.40 6 1 0 52.59 4.50 6 1 0 44.50 3.50 -7 -1 0 65.19 3.80 -7 -1 0 54.39 4.10 -7 -1 0 58.59 4.40 -7 -1 0 64.59 4.30 -7 -1 0 59.59 4.10 -7 -1 0 60.19 4.20 7 1 0 62.59 4.60 -8 -1 0 57.59 4.80 -8 -1 0 54.39 4.20 -8 -1 0 65.49 4.20 -8 -1 0 65.29 4.80 -8 -1 0 71.59 5.00 -8 -1 0 59.29 4.60 8 1 0 58.99 4.80 -9 -1 0 10.80 2.90 -9 -1 0 10.80 2.50 -9 -1 0 4.90 1.90 -9 -1 0 10.70 2.70 -9 -1 0 11.10 3.00 -9 -1 0 7.90 2.40 9 1 0 11.50 3.10 -10 -1 0 16.10 3.60 -10 -1 0 18.40 3.60 -10 -1 0 17.40 3.60 -10 -1 0 11.30 3.10 -10 -1 0 12.00 2.80 -10 -1 0 16.20 3.10 10 1 0 16.40 3.90 -11 -1 0 4.20 2.70 -11 -1 0 5.10 2.40 -11 -1 0 1.30 2.30 -11 -1 0 0.50 2.50 -11 -1 0 4.60 2.90 11 1 0 4.70 3.10 -12 -1 0 38.20 6.30 -12 -1 0 27.50 4.80 -12 -1 0 34.20 5.70 -12 -1 0 29.00 5.40 12 1 0 26.70 5.40 11 -2 0 95.49 7.50 11 -2 0 88.79 9.30 -11 2 0 86.19 7.60 -11 2 0 98.59 8.10 -11 2 0 83.59 7.90 -11 2 0 111.99 9.00 10 -2 0 170.08 9.10 10 -2 0 174.58 10.20 -10 2 0 183.58 10.40 -10 2 0 164.08 9.90 -10 2 0 166.88 8.60 -10 2 0 173.98 9.40 -10 2 0 174.38 10.20 9 -2 0 285.17 12.60 9 -2 0 292.17 11.50 -9 2 0 286.97 12.70 -9 2 0 309.87 13.00 -9 2 0 335.77 12.40 -9 2 0 301.97 12.90 -9 2 0 309.07 11.40 8 -2 0 233.78 10.40 8 -2 0 234.28 9.50 -8 2 0 262.47 11.10 -8 2 0 246.78 9.90 -8 2 0 237.78 10.70 -8 2 0 238.78 10.60 7 -2 0 203.98 8.30 7 -2 0 209.38 9.10 -7 2 0 217.28 7.80 -7 2 0 209.78 9.30 -7 2 0 215.58 9.40 -7 2 0 210.48 9.30 -7 2 0 216.28 8.60 6 -2 0 64.79 4.10 6 -2 0 62.99 4.60 -6 2 0 63.89 4.60 -6 2 0 64.59 4.20 -6 2 0 69.19 3.80 -6 2 0 70.09 4.80 -6 2 0 68.99 4.70 5 -2 0 627.14 15.30 5 -2 0 621.94 16.70 5 -2 0 589.84 15.50 -5 2 0 640.04 18.10 -5 2 0 593.94 16.40 -5 2 0 614.34 17.10 -5 2 0 612.74 15.90 -5 2 0 631.54 15.30 4 -2 0 51.69 3.40 4 -2 0 56.59 3.10 4 -2 0 48.50 3.30 4 -2 0 55.49 3.10 -4 2 0 54.09 2.70 -4 2 0 49.20 3.00 -4 2 0 56.29 3.80 -4 2 0 50.59 3.30 -4 2 0 55.49 3.60 -4 2 0 54.19 3.40 3 -2 0 4292.47 89.39 3 -2 0 3931.41 81.19 3 -2 0 4106.89 83.29 3 -2 0 3948.71 88.29 3 -2 0 4123.69 81.69 -3 2 0 4162.38 81.89 -3 2 0 4136.49 83.09 -3 2 0 4035.70 82.19 -3 2 0 3992.90 87.19 -3 2 0 4185.68 89.19 2 -2 0 63.89 3.10 2 -2 0 61.09 2.90 2 -2 0 70.49 2.80 2 -2 0 67.49 2.80 2 -2 0 71.29 3.50 -2 2 0 62.49 3.00 -2 2 0 65.09 2.80 -2 2 0 65.29 3.40 -2 2 0 62.79 3.00 -2 2 0 70.69 2.90 -2 2 0 67.09 2.40 1 -2 0 127.09 3.80 1 -2 0 123.19 4.30 1 -2 0 128.49 3.80 1 -2 0 122.39 4.00 1 -2 0 124.59 3.30 1 -2 0 132.19 4.50 -1 2 0 130.19 4.00 -1 2 0 121.89 4.30 -1 2 0 117.49 3.70 -1 2 0 123.79 3.40 -1 2 0 124.79 4.50 -1 2 0 122.49 3.90 0 -2 0 1999.80 42.10 0 -2 0 1982.20 40.40 0 -2 0 2013.90 39.90 0 -2 0 2004.20 40.70 0 -2 0 1986.10 43.30 0 2 0 2001.30 43.40 0 2 0 2049.59 40.20 0 2 0 1996.10 43.50 0 2 0 2006.70 42.30 0 2 0 2009.90 39.60 0 2 0 1947.31 42.10 -1 -2 0 1259.87 26.00 -1 -2 0 1320.07 27.80 -1 -2 0 1302.77 26.30 -1 -2 0 1284.77 28.60 -1 -2 0 1284.27 27.00 -1 -2 0 1268.17 26.50 1 2 0 1284.07 27.60 1 2 0 1291.47 28.50 1 2 0 1315.57 28.60 -2 -2 0 4239.48 86.89 -2 -2 0 4269.07 89.89 -2 -2 0 4267.67 84.49 -2 -2 0 4452.35 91.19 -2 -2 0 4116.39 83.69 2 2 0 4278.87 91.19 2 2 0 4337.07 92.49 -3 -2 0 6.00 0.90 -3 -2 0 3.20 0.90 -3 -2 0 7.20 1.00 -3 -2 0 6.20 1.20 -3 -2 0 6.20 1.20 -3 -2 0 3.50 1.00 3 2 0 2.50 0.90 3 2 0 2.50 0.80 -4 -2 0 151.78 5.90 -4 -2 0 163.58 5.60 -4 -2 0 162.48 5.80 -4 -2 0 184.08 6.10 -4 -2 0 174.08 5.10 -4 -2 0 163.38 5.60 -4 -2 0 170.18 5.10 4 2 0 173.78 5.80 4 2 0 159.58 6.10 -5 -2 0 475.95 12.80 -5 -2 0 474.05 11.80 -5 -2 0 464.95 12.60 -5 -2 0 460.55 11.50 -5 -2 0 459.95 13.10 5 2 0 435.26 12.60 5 2 0 467.65 13.50 -6 -2 0 269.77 8.00 -6 -2 0 264.67 8.90 -6 -2 0 247.98 8.80 -6 -2 0 284.57 9.50 -6 -2 0 263.17 8.80 -6 -2 0 267.37 8.40 6 2 0 264.57 9.80 6 2 0 254.37 8.90 -7 -2 0 1080.49 26.80 -7 -2 0 1101.19 26.50 -7 -2 0 1086.59 25.70 -7 -2 0 1089.29 27.10 -7 -2 0 1081.19 24.90 7 2 0 1100.19 27.00 7 2 0 1099.99 27.60 -8 -2 0 82.09 5.30 -8 -2 0 77.19 5.00 -8 -2 0 81.59 5.70 -8 -2 0 87.89 5.50 -8 -2 0 89.39 4.80 -8 -2 0 87.39 5.40 8 2 0 83.59 5.30 -9 -2 0 900.91 25.70 -9 -2 0 849.22 24.00 -9 -2 0 856.31 23.80 -9 -2 0 826.42 22.90 -9 -2 0 881.81 22.10 -9 -2 0 887.91 23.80 9 2 0 871.31 24.40 9 2 0 873.51 24.20 -10 -2 0 583.24 18.60 -10 -2 0 581.14 18.60 -10 -2 0 603.14 17.20 -10 -2 0 572.04 20.00 -10 -2 0 576.74 18.30 -10 -2 0 587.24 19.00 10 2 0 589.64 19.10 10 2 0 606.94 19.40 -11 -2 0 380.86 15.10 -11 -2 0 360.36 13.00 -11 -2 0 381.06 16.00 -11 -2 0 374.86 14.40 -11 -2 0 363.36 14.60 -11 -2 0 375.96 14.60 11 2 0 398.26 15.50 11 2 0 356.06 14.60 -12 -2 0 44.50 5.30 -12 -2 0 51.69 6.90 -12 -2 0 51.59 7.00 -12 -2 0 59.89 6.90 12 2 0 45.80 6.10 12 2 0 51.99 6.80 11 -3 0 14.60 4.30 -11 3 0 20.30 5.20 -11 3 0 14.10 3.90 -11 3 0 26.80 5.70 10 -3 0 32.60 4.90 10 -3 0 45.50 6.40 -10 3 0 27.90 5.00 -10 3 0 46.80 6.60 -10 3 0 35.10 5.20 -10 3 0 26.30 5.40 -10 3 0 34.00 4.80 9 -3 0 1.30 2.10 9 -3 0 0.70 2.00 -9 3 0 4.80 2.50 -9 3 0 -1.40 1.90 -9 3 0 0.70 2.30 -9 3 0 4.40 2.30 8 -3 0 10.50 2.70 8 -3 0 6.50 2.60 -8 3 0 12.80 3.30 -8 3 0 12.40 2.80 -8 3 0 5.90 2.40 -8 3 0 12.10 3.40 7 -3 0 24.10 3.90 7 -3 0 21.90 3.10 -7 3 0 33.40 4.20 -7 3 0 26.80 3.80 -7 3 0 30.70 3.70 -7 3 0 23.90 3.70 6 -3 0 8.60 2.20 6 -3 0 9.80 2.60 -6 3 0 10.30 2.70 -6 3 0 7.70 2.00 -6 3 0 9.80 1.70 -6 3 0 9.30 2.30 -6 3 0 9.40 2.20 5 -3 0 88.89 4.60 5 -3 0 81.59 5.00 5 -3 0 85.19 5.00 -5 3 0 79.79 4.50 -5 3 0 90.59 5.20 -5 3 0 88.89 3.90 -5 3 0 90.49 5.10 4 -3 0 47.80 3.10 4 -3 0 49.30 3.20 4 -3 0 49.30 3.50 4 -3 0 48.20 3.60 -4 3 0 53.39 2.70 -4 3 0 46.10 3.10 -4 3 0 54.29 3.80 -4 3 0 48.80 3.40 -4 3 0 49.40 4.00 3 -3 0 105.79 4.90 3 -3 0 109.59 4.40 3 -3 0 110.39 4.80 3 -3 0 100.49 4.20 -3 3 0 105.79 4.60 -3 3 0 106.89 4.30 -3 3 0 108.49 3.70 -3 3 0 98.69 4.90 -3 3 0 93.39 5.00 -3 3 0 96.69 4.60 2 -3 0 23.10 2.20 2 -3 0 23.80 2.10 2 -3 0 25.90 1.90 -2 3 0 19.10 2.30 -2 3 0 23.20 1.50 -2 3 0 22.60 2.30 -2 3 0 23.20 2.70 1 -3 0 244.28 6.00 1 -3 0 245.28 6.60 1 -3 0 248.88 6.90 1 -3 0 237.88 6.60 1 -3 0 245.68 7.50 -1 3 0 244.18 7.50 -1 3 0 247.78 6.80 -1 3 0 248.78 7.00 -1 3 0 230.68 7.70 -1 3 0 245.78 6.20 0 -3 0 251.47 6.80 0 -3 0 257.87 7.70 0 -3 0 263.67 6.50 0 -3 0 265.57 6.80 0 -3 0 271.27 6.80 0 3 0 244.38 7.30 0 3 0 243.88 7.80 0 3 0 265.47 6.60 0 3 0 257.87 7.00 -1 -3 0 775.92 17.30 -1 -3 0 794.02 17.80 -1 -3 0 786.72 17.50 -1 -3 0 756.12 18.70 -1 -3 0 764.82 16.90 -1 -3 0 822.32 17.20 1 3 0 814.72 16.20 1 3 0 789.12 18.00 1 3 0 836.12 19.00 1 3 0 755.92 18.70 -2 -3 0 1.80 0.80 -2 -3 0 0.80 0.70 -2 -3 0 0.60 0.60 -2 -3 0 0.40 0.60 -2 -3 0 0.40 0.70 2 3 0 -0.90 0.70 2 3 0 1.00 0.70 -3 -3 0 14.80 1.80 -3 -3 0 16.70 1.10 -3 -3 0 18.50 1.50 -3 -3 0 19.60 2.00 -3 -3 0 15.50 1.80 -3 -3 0 19.60 2.00 3 3 0 14.40 1.90 -4 -3 0 356.56 9.90 -4 -3 0 368.56 8.80 -4 -3 0 382.16 10.70 -4 -3 0 366.56 10.60 -4 -3 0 345.47 9.10 4 3 0 351.56 10.20 4 3 0 359.46 10.80 -5 -3 0 323.67 9.60 -5 -3 0 317.47 9.60 -5 -3 0 323.17 8.50 -5 -3 0 314.07 10.20 -5 -3 0 304.57 9.90 -5 -3 0 340.17 10.30 -5 -3 0 331.97 8.80 5 3 0 317.87 10.40 5 3 0 317.37 9.80 -6 -3 0 131.09 5.10 -6 -3 0 129.89 6.20 -6 -3 0 129.29 5.80 -6 -3 0 134.49 5.20 -6 -3 0 134.59 5.80 -6 -3 0 139.39 6.20 -6 -3 0 126.69 6.20 6 3 0 132.09 5.80 -7 -3 0 79.29 4.90 -7 -3 0 76.09 4.30 -7 -3 0 70.09 4.60 -7 -3 0 68.79 3.90 -7 -3 0 80.69 4.70 7 3 0 78.79 4.70 -8 -3 0 22.20 3.50 -8 -3 0 19.30 2.70 -8 -3 0 25.60 3.50 -8 -3 0 25.70 3.60 -8 -3 0 25.90 3.60 -8 -3 0 28.50 3.40 8 3 0 23.70 3.30 8 3 0 25.80 3.70 -9 -3 0 26.90 3.60 -9 -3 0 26.00 4.10 -9 -3 0 33.20 4.40 -9 -3 0 23.30 3.10 -9 -3 0 26.10 3.90 -9 -3 0 24.50 3.70 9 3 0 26.50 3.80 9 3 0 21.80 3.60 -10 -3 0 1.80 1.90 -10 -3 0 0.10 1.60 -10 -3 0 1.30 2.00 -10 -3 0 3.30 1.90 -10 -3 0 1.80 2.00 -10 -3 0 -0.90 1.90 10 3 0 1.00 2.10 10 3 0 0.80 1.70 -11 -3 0 1.20 2.10 -11 -3 0 -0.80 2.20 -11 -3 0 0.00 1.60 -11 -3 0 -0.90 1.70 -11 -3 0 -0.70 1.90 -11 -3 0 0.10 2.10 11 3 0 -0.60 1.80 11 3 0 -0.60 2.20 -12 -3 0 5.90 3.30 -12 -3 0 6.60 3.40 -12 -3 0 3.30 2.60 -12 -3 0 1.90 2.70 -12 -3 0 3.90 2.30 -12 -3 0 6.80 3.20 12 3 0 5.90 2.80 12 3 0 1.40 2.40 10 -4 0 311.07 14.70 -10 4 0 303.77 14.50 -10 4 0 344.17 15.70 -10 4 0 329.07 14.80 9 -4 0 268.27 11.40 9 -4 0 288.87 13.00 -9 4 0 287.07 11.90 -9 4 0 293.27 13.60 -9 4 0 263.47 13.10 -9 4 0 258.97 12.50 8 -4 0 155.88 8.00 8 -4 0 160.58 9.00 -8 4 0 171.88 8.40 -8 4 0 163.48 8.90 -8 4 0 151.68 9.20 -8 4 0 175.98 9.60 7 -4 0 633.24 19.50 7 -4 0 638.94 18.20 -7 4 0 651.53 19.90 -7 4 0 637.04 19.80 -7 4 0 642.24 18.40 -7 4 0 673.33 21.00 6 -4 0 25.70 3.20 6 -4 0 25.70 3.80 -6 4 0 24.40 3.50 -6 4 0 29.60 3.50 -6 4 0 29.90 4.20 -6 4 0 19.30 3.10 5 -4 0 89.09 5.60 5 -4 0 85.89 4.80 5 -4 0 90.69 5.50 -5 4 0 85.69 4.80 -5 4 0 97.19 5.40 -5 4 0 92.19 5.50 -5 4 0 95.89 5.90 4 -4 0 113.99 5.20 4 -4 0 117.29 6.00 4 -4 0 118.09 5.80 -4 4 0 121.99 4.40 -4 4 0 120.79 5.70 -4 4 0 121.59 5.90 -4 4 0 116.99 5.20 -4 4 0 113.09 7.20 3 -4 0 415.76 13.00 3 -4 0 422.26 11.60 3 -4 0 422.46 11.70 3 -4 0 435.56 12.40 -3 4 0 454.05 14.00 -3 4 0 443.66 10.70 -3 4 0 437.66 12.60 -3 4 0 435.66 12.30 -3 4 0 446.56 13.30 2 -4 0 420.36 10.80 2 -4 0 404.06 10.80 2 -4 0 409.56 12.20 2 -4 0 396.46 11.30 -2 4 0 415.46 11.50 -2 4 0 401.16 12.70 -2 4 0 434.26 10.20 -2 4 0 416.36 12.20 -2 4 0 403.96 11.20 1 -4 0 1302.27 27.70 1 -4 0 1289.57 27.70 1 -4 0 1280.27 27.30 1 -4 0 1298.97 28.30 -1 4 0 1304.47 31.00 -1 4 0 1279.17 30.00 -1 4 0 1309.27 27.70 -1 4 0 1294.87 27.90 0 -4 0 690.03 15.80 0 -4 0 654.13 17.50 0 -4 0 703.33 15.90 0 -4 0 698.93 16.10 0 -4 0 703.83 15.60 0 4 0 713.63 16.60 0 4 0 673.73 17.90 0 4 0 705.33 15.60 0 4 0 699.83 17.10 -1 -4 0 1770.62 36.20 -1 -4 0 1760.12 36.90 -1 -4 0 1717.13 37.80 -1 -4 0 1757.92 36.60 -1 -4 0 1730.63 39.50 -1 -4 0 1714.23 35.90 1 4 0 1739.83 38.20 1 4 0 1743.23 38.20 1 4 0 1752.12 39.70 1 4 0 1734.83 35.10 -2 -4 0 1527.05 31.80 -2 -4 0 1486.35 29.80 -2 -4 0 1492.45 34.60 -2 -4 0 1512.45 33.40 -2 -4 0 1512.85 32.70 -2 -4 0 1501.35 31.40 2 4 0 1515.65 30.00 2 4 0 1494.55 33.30 -3 -4 0 2279.57 50.99 -3 -4 0 2337.07 52.19 -3 -4 0 2348.27 46.00 -3 -4 0 2370.36 47.60 -3 -4 0 2323.27 48.30 -3 -4 0 2401.26 49.90 3 4 0 2300.17 52.09 3 4 0 2344.77 52.49 -4 -4 0 1389.16 30.90 -4 -4 0 1438.16 33.30 -4 -4 0 1422.06 30.00 -4 -4 0 1423.26 28.90 -4 -4 0 1385.06 32.60 4 4 0 1400.76 33.10 4 4 0 1471.05 33.80 -5 -4 0 89.59 4.50 -5 -4 0 93.99 3.50 -5 -4 0 96.69 4.10 -5 -4 0 91.29 4.80 -5 -4 0 95.39 4.90 5 4 0 94.49 4.70 5 4 0 104.19 5.40 -6 -4 0 225.58 8.60 -6 -4 0 220.78 7.20 -6 -4 0 213.78 8.00 -6 -4 0 210.08 8.30 -6 -4 0 222.88 6.80 6 4 0 225.78 8.30 -7 -4 0 470.45 14.80 -7 -4 0 479.35 14.30 -7 -4 0 488.55 13.00 -7 -4 0 495.75 15.40 -7 -4 0 470.05 12.70 7 4 0 470.15 14.60 -8 -4 0 9.10 2.20 -8 -4 0 8.60 1.90 -8 -4 0 10.60 2.50 -8 -4 0 14.30 2.90 -8 -4 0 12.50 2.80 -8 -4 0 11.20 2.10 8 4 0 9.80 2.40 -9 -4 0 259.97 11.30 -9 -4 0 236.08 10.40 -9 -4 0 242.68 9.00 -9 -4 0 255.27 10.50 -9 -4 0 250.17 9.30 -9 -4 0 229.68 9.80 9 4 0 240.68 10.30 9 4 0 242.08 10.40 -10 -4 0 10.40 3.00 -10 -4 0 9.70 3.20 -10 -4 0 12.50 2.70 -10 -4 0 9.00 2.80 -10 -4 0 11.40 2.70 -10 -4 0 10.90 2.80 10 4 0 8.50 2.70 10 4 0 7.90 2.80 -11 -4 0 182.68 10.60 -11 -4 0 195.38 10.40 -11 -4 0 183.88 9.60 -11 -4 0 202.98 10.40 -11 -4 0 183.98 8.70 11 4 0 187.28 10.00 11 4 0 187.68 10.30 -12 -4 0 194.78 11.00 -12 -4 0 228.98 10.30 -12 -4 0 201.98 11.30 -12 -4 0 195.98 11.50 -12 -4 0 217.58 11.00 12 4 0 219.58 11.40 12 4 0 213.08 11.70 -13 -4 0 145.19 10.40 10 -5 0 1.50 3.40 -10 5 0 4.00 3.50 9 -5 0 1.50 2.70 -9 5 0 2.20 3.20 8 -5 0 -0.70 2.00 8 -5 0 -2.50 1.70 -8 5 0 1.40 2.60 -8 5 0 -0.70 2.10 -8 5 0 1.60 2.00 7 -5 0 -0.20 1.90 7 -5 0 2.70 1.90 -7 5 0 0.30 1.90 -7 5 0 -0.60 1.90 -7 5 0 4.60 2.10 6 -5 0 10.30 2.70 6 -5 0 12.20 3.10 6 -5 0 13.10 2.60 -6 5 0 21.80 3.50 -6 5 0 13.70 3.20 -6 5 0 14.60 3.30 5 -5 0 126.19 6.70 5 -5 0 120.09 5.90 5 -5 0 116.49 6.90 -5 5 0 122.49 6.40 -5 5 0 111.39 6.80 -5 5 0 114.89 6.60 4 -5 0 154.88 7.10 4 -5 0 157.48 6.50 4 -5 0 165.18 7.70 -4 5 0 159.88 7.30 -4 5 0 159.78 7.80 -4 5 0 157.98 7.00 3 -5 0 -0.30 0.90 3 -5 0 1.70 1.10 3 -5 0 2.30 1.30 3 -5 0 0.20 1.00 -3 5 0 1.50 1.10 -3 5 0 0.90 1.00 -3 5 0 1.10 0.70 -3 5 0 0.20 1.10 -3 5 0 0.00 1.20 2 -5 0 4.50 1.30 2 -5 0 5.30 1.50 2 -5 0 2.30 1.40 2 -5 0 4.80 1.50 -2 5 0 7.30 1.70 -2 5 0 5.80 1.90 -2 5 0 5.70 1.00 -2 5 0 7.10 1.90 -2 5 0 8.10 1.60 1 -5 0 5.40 1.60 1 -5 0 7.80 1.60 1 -5 0 5.90 1.40 1 -5 0 8.00 1.60 1 -5 0 7.90 1.20 -1 5 0 5.20 1.30 -1 5 0 8.90 1.50 -1 5 0 4.40 1.40 -1 5 0 8.80 2.20 -1 5 0 6.60 1.10 0 -5 0 4.10 1.20 0 -5 0 5.60 1.50 0 -5 0 4.90 1.20 0 -5 0 3.40 0.90 0 -5 0 6.00 1.30 0 5 0 2.00 1.10 0 5 0 6.70 1.30 0 5 0 3.20 1.20 0 5 0 5.70 1.20 -1 -5 0 5.60 1.30 -1 -5 0 5.10 1.10 -1 -5 0 2.30 1.10 -1 -5 0 4.40 1.40 -1 -5 0 4.40 1.00 -1 -5 0 3.20 1.10 1 5 0 1.60 0.90 1 5 0 3.20 1.10 1 5 0 3.30 0.80 1 5 0 4.00 1.10 -2 -5 0 -0.40 0.60 -2 -5 0 0.50 0.80 -2 -5 0 -0.30 0.70 -2 -5 0 -0.40 0.60 -2 -5 0 0.10 0.40 -2 -5 0 0.40 0.90 -2 -5 0 0.80 1.00 2 5 0 0.50 0.80 2 5 0 0.50 1.00 2 5 0 0.00 0.50 -3 -5 0 28.00 2.90 -3 -5 0 27.60 2.20 -3 -5 0 30.90 2.50 -3 -5 0 31.60 2.40 -3 -5 0 29.60 1.30 -3 -5 0 30.60 2.90 3 5 0 29.00 2.40 3 5 0 25.70 2.90 -4 -5 0 12.90 2.00 -4 -5 0 15.10 1.90 -4 -5 0 18.40 2.50 -4 -5 0 13.40 2.00 -4 -5 0 13.50 2.30 -4 -5 0 15.50 1.10 4 5 0 12.60 2.00 -5 -5 0 26.50 3.20 -5 -5 0 23.70 1.60 -5 -5 0 19.20 2.60 -5 -5 0 22.90 2.30 -5 -5 0 22.30 2.70 -5 -5 0 23.40 2.70 5 5 0 30.40 3.30 -6 -5 0 -0.30 0.70 -6 -5 0 4.50 1.60 -6 -5 0 3.60 1.30 -6 -5 0 3.80 1.00 -6 -5 0 2.60 1.30 6 5 0 6.50 1.80 -7 -5 0 15.90 2.10 -7 -5 0 9.40 2.20 -7 -5 0 17.30 3.00 -7 -5 0 16.70 2.90 -7 -5 0 14.10 2.20 7 5 0 11.20 2.30 -8 -5 0 39.30 3.70 -8 -5 0 45.30 4.80 -8 -5 0 34.20 4.10 -8 -5 0 40.40 4.50 8 5 0 34.30 4.00 -9 -5 0 1.80 1.40 -9 -5 0 0.00 1.50 -9 -5 0 -1.20 1.50 -9 -5 0 1.20 1.70 9 5 0 0.90 1.60 -10 -5 0 88.19 6.70 -10 -5 0 96.69 7.00 -10 -5 0 86.89 6.70 -10 -5 0 93.49 5.80 10 5 0 104.09 7.20 10 5 0 97.59 6.70 -11 -5 0 8.20 3.30 -11 -5 0 8.50 2.50 -11 -5 0 7.60 3.20 -11 -5 0 9.30 3.10 11 5 0 13.20 3.80 11 5 0 10.10 3.20 -12 -5 0 3.60 3.10 -12 -5 0 2.50 2.70 -12 -5 0 1.80 2.10 -12 -5 0 -0.30 2.50 12 5 0 2.80 2.60 12 5 0 -1.70 2.60 9 -6 0 48.70 6.60 -9 6 0 53.79 7.40 8 -6 0 302.17 13.60 -8 6 0 290.07 13.80 7 -6 0 96.49 6.50 7 -6 0 98.39 7.20 -7 6 0 98.59 7.70 -7 6 0 107.19 7.80 6 -6 0 116.39 7.60 6 -6 0 92.49 5.90 6 -6 0 98.99 6.80 -6 6 0 99.99 6.50 -6 6 0 89.99 6.90 -6 6 0 92.09 6.90 5 -6 0 299.27 12.30 5 -6 0 288.37 10.40 5 -6 0 287.47 11.30 -5 6 0 284.27 11.70 -5 6 0 297.57 12.50 -5 6 0 299.57 11.30 4 -6 0 129.39 6.20 4 -6 0 129.49 7.30 4 -6 0 128.69 6.80 -4 6 0 132.49 7.00 -4 6 0 131.99 7.50 -4 6 0 134.79 6.60 3 -6 0 96.29 6.00 3 -6 0 96.39 5.50 3 -6 0 99.69 5.10 -3 6 0 110.09 5.50 -3 6 0 95.19 6.10 -3 6 0 102.89 5.70 2 -6 0 562.94 14.90 2 -6 0 531.55 14.50 2 -6 0 559.34 15.20 2 -6 0 557.24 16.80 -2 6 0 547.45 15.30 -2 6 0 543.25 16.50 -2 6 0 526.15 14.90 1 -6 0 528.65 13.80 1 -6 0 530.65 14.30 1 -6 0 530.35 15.80 1 -6 0 525.85 12.70 1 -6 0 511.35 13.90 -1 6 0 505.05 16.20 -1 6 0 526.75 13.90 -1 6 0 516.75 15.50 -1 6 0 527.95 14.30 0 -6 0 2218.38 50.69 0 -6 0 2204.88 46.10 0 -6 0 2119.29 46.60 0 -6 0 2189.98 46.10 0 -6 0 2178.78 46.00 0 6 0 2175.78 49.20 0 6 0 2161.18 45.40 0 6 0 2184.38 51.19 0 6 0 2198.58 48.50 -1 -6 0 99.29 4.60 -1 -6 0 98.39 4.20 -1 -6 0 95.79 4.10 -1 -6 0 91.59 4.40 -1 -6 0 99.99 5.20 -1 -6 0 95.39 4.50 1 6 0 92.89 4.30 1 6 0 89.49 3.70 1 6 0 94.99 4.90 1 6 0 97.89 5.50 -2 -6 0 647.34 15.80 -2 -6 0 644.84 16.10 -2 -6 0 641.44 16.10 -2 -6 0 619.54 16.00 -2 -6 0 647.74 15.90 -2 -6 0 622.14 17.60 2 6 0 646.64 14.00 2 6 0 607.44 16.70 2 6 0 628.74 17.90 2 6 0 635.74 16.60 -3 -6 0 112.29 5.10 -3 -6 0 109.39 3.20 -3 -6 0 118.89 5.10 -3 -6 0 123.19 6.00 -3 -6 0 116.59 4.90 -3 -6 0 113.49 5.20 3 6 0 118.99 5.30 3 6 0 120.39 5.90 -4 -6 0 658.33 16.50 -4 -6 0 671.73 17.70 -4 -6 0 680.83 17.80 -4 -6 0 671.03 18.70 -4 -6 0 669.73 17.20 4 6 0 676.53 17.80 4 6 0 658.53 18.70 -5 -6 0 0.70 1.10 -5 -6 0 0.50 0.80 -5 -6 0 2.60 1.30 -5 -6 0 1.40 1.20 5 6 0 -0.40 0.90 -6 -6 0 189.68 7.90 -6 -6 0 203.58 7.30 -6 -6 0 195.68 8.20 -6 -6 0 193.48 8.30 6 6 0 199.28 8.40 -7 -6 0 21.10 2.80 -7 -6 0 20.50 3.20 -7 -6 0 15.60 2.90 -7 -6 0 18.00 3.20 7 6 0 23.90 3.60 -8 -6 0 469.15 15.00 -8 -6 0 438.06 13.30 -8 -6 0 428.46 15.10 -8 -6 0 463.55 15.50 8 6 0 452.55 15.20 -9 -6 0 286.07 12.00 -9 -6 0 285.97 11.70 -9 -6 0 295.67 10.50 -9 -6 0 284.67 12.20 9 6 0 296.57 11.90 -10 -6 0 89.69 5.80 -10 -6 0 101.09 7.10 -10 -6 0 91.89 6.90 -10 -6 0 83.29 6.60 10 6 0 81.39 6.50 -11 -6 0 73.99 7.50 -11 -6 0 78.99 7.80 -11 -6 0 74.99 7.40 -11 -6 0 79.19 5.90 11 6 0 68.19 7.10 11 6 0 77.59 7.80 -12 -6 0 117.29 8.90 -12 -6 0 116.79 9.00 -12 -6 0 123.39 7.90 -12 -6 0 120.19 8.80 12 6 0 109.59 8.60 8 -7 0 22.50 4.90 -8 7 0 14.30 4.50 7 -7 0 0.80 2.50 -7 7 0 -2.10 2.50 -7 7 0 -2.50 2.10 6 -7 0 0.50 2.20 6 -7 0 4.90 2.30 -6 7 0 1.40 2.40 -6 7 0 6.10 3.20 5 -7 0 100.69 6.70 5 -7 0 93.39 5.90 5 -7 0 96.49 7.30 -5 7 0 94.49 6.80 -5 7 0 94.69 7.30 4 -7 0 13.10 2.60 4 -7 0 13.10 3.00 4 -7 0 14.80 3.00 -4 7 0 13.70 3.20 -4 7 0 9.10 2.70 -4 7 0 16.60 3.20 3 -7 0 0.80 1.40 3 -7 0 1.70 1.40 3 -7 0 2.60 1.80 -3 7 0 0.70 1.20 -3 7 0 -0.80 1.20 -3 7 0 -0.20 1.30 2 -7 0 88.89 6.00 2 -7 0 82.89 4.80 2 -7 0 90.89 5.30 -2 7 0 81.59 5.00 -2 7 0 83.89 4.90 -2 7 0 75.19 5.60 1 -7 0 130.29 6.20 1 -7 0 142.29 7.40 1 -7 0 139.59 6.30 1 -7 0 132.19 6.00 1 -7 0 143.69 5.60 -1 7 0 141.19 6.10 -1 7 0 152.38 7.40 -1 7 0 147.59 6.30 -1 7 0 148.99 8.00 0 -7 0 65.19 4.80 0 -7 0 49.99 3.60 0 -7 0 53.99 3.10 0 -7 0 57.89 3.90 0 -7 0 50.59 3.70 0 7 0 48.50 4.10 0 7 0 49.40 3.40 0 7 0 58.79 3.50 0 7 0 45.10 4.80 -1 -7 0 8.60 2.10 -1 -7 0 9.30 1.70 -1 -7 0 6.00 1.70 -1 -7 0 7.90 1.70 -1 -7 0 5.20 1.50 1 7 0 8.30 2.10 1 7 0 7.30 1.60 1 7 0 7.30 1.80 1 7 0 10.70 1.70 -2 -7 0 1.10 1.10 -2 -7 0 0.90 1.00 -2 -7 0 0.30 1.00 -2 -7 0 0.00 0.80 -2 -7 0 0.20 0.90 -2 -7 0 -1.00 1.00 2 7 0 -0.70 1.00 2 7 0 0.20 0.70 2 7 0 0.20 0.80 2 7 0 -0.40 0.90 -3 -7 0 1.70 1.20 -3 -7 0 3.20 1.30 -3 -7 0 0.40 1.00 -3 -7 0 2.40 1.10 3 7 0 0.50 1.30 3 7 0 2.00 1.20 3 7 0 1.00 1.10 -4 -7 0 128.19 6.00 -4 -7 0 126.19 6.10 -4 -7 0 115.79 5.60 -4 -7 0 127.69 5.60 4 7 0 125.49 6.10 4 7 0 140.69 7.00 -5 -7 0 6.50 1.90 -5 -7 0 8.60 2.20 -5 -7 0 6.70 1.70 -5 -7 0 6.50 1.90 5 7 0 5.50 1.90 5 7 0 7.60 2.00 -6 -7 0 15.30 2.40 -6 -7 0 22.60 3.20 -6 -7 0 19.70 2.90 -6 -7 0 18.80 3.20 6 7 0 14.90 2.70 -7 -7 0 142.09 7.30 -7 -7 0 131.29 7.20 -7 -7 0 144.79 6.40 -7 -7 0 139.59 7.20 7 7 0 123.49 7.20 -8 -7 0 24.70 3.80 -8 -7 0 27.70 4.00 -8 -7 0 26.40 4.00 -8 -7 0 21.70 3.20 8 7 0 23.80 3.80 -9 -7 0 51.59 5.50 -9 -7 0 44.50 5.30 -9 -7 0 47.60 4.70 -9 -7 0 52.69 5.90 9 7 0 37.70 4.90 -10 -7 0 12.00 3.40 -10 -7 0 12.40 3.50 -10 -7 0 16.40 3.90 -10 -7 0 14.70 3.10 10 7 0 10.20 3.00 -11 -7 0 1.70 2.40 -11 -7 0 2.80 2.30 -11 -7 0 1.50 2.60 -11 -7 0 0.80 2.40 11 7 0 0.10 2.10 -12 -7 0 -1.40 2.20 -12 -7 0 -1.50 2.40 -12 -7 0 2.30 3.00 12 7 0 0.00 2.80 7 -8 0 84.69 8.50 -7 8 0 106.09 9.80 6 -8 0 314.67 13.60 -6 8 0 314.17 14.00 -6 8 0 307.97 14.70 5 -8 0 314.67 11.90 5 -8 0 324.67 13.00 -5 8 0 312.67 13.20 -5 8 0 288.97 13.90 4 -8 0 70.39 6.60 4 -8 0 79.19 5.50 -4 8 0 61.49 6.10 -4 8 0 74.09 7.50 3 -8 0 106.29 6.60 3 -8 0 119.29 6.30 -3 8 0 106.49 6.70 -3 8 0 124.49 7.80 2 -8 0 22.80 3.50 2 -8 0 22.10 3.20 -2 8 0 21.10 3.40 -2 8 0 18.90 3.70 1 -8 0 209.78 8.20 1 -8 0 202.88 8.50 -1 8 0 217.98 8.40 -1 8 0 195.78 8.00 -1 8 0 211.08 9.60 0 -8 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3 31.80 3.40 -4 -6 3 26.90 2.60 3 6 -3 79.09 5.00 3 6 -3 71.49 4.50 -3 -6 3 82.49 4.70 -3 -6 3 75.39 3.80 -3 -6 3 79.29 4.20 -3 -6 3 73.29 4.50 2 6 -3 169.58 7.40 2 6 -3 173.78 7.50 -2 -6 3 165.18 6.10 -2 -6 3 171.08 6.20 -2 -6 3 159.08 7.00 -2 -6 3 175.28 7.00 -2 -6 3 173.48 7.00 1 6 -3 5.80 1.70 1 6 -3 8.00 1.80 -1 -6 3 7.00 1.60 -1 -6 3 6.50 1.50 -1 -6 3 9.60 2.00 -1 -6 3 11.90 2.00 -1 -6 3 10.10 1.60 0 6 -3 130.69 6.70 0 6 -3 122.79 6.00 0 6 -3 121.19 6.10 0 6 -3 130.49 4.60 0 -6 3 118.09 4.70 0 -6 3 126.39 5.40 0 -6 3 122.09 5.60 0 -6 3 128.09 6.10 -1 6 -3 2.30 1.10 -1 6 -3 1.00 1.20 -1 6 -3 0.70 1.00 -1 6 -3 0.90 0.90 -1 6 -3 3.50 1.60 1 -6 3 1.60 1.40 1 -6 3 3.10 1.10 1 -6 3 1.70 1.30 1 -6 3 1.30 1.10 -2 6 -3 414.96 11.90 -2 6 -3 412.26 12.70 -2 6 -3 406.56 13.60 -2 6 -3 431.86 14.10 -2 6 -3 440.76 15.20 2 -6 3 421.26 13.20 2 -6 3 414.46 12.20 2 -6 3 415.76 11.00 2 -6 3 439.76 12.70 -3 6 -3 1181.18 32.00 -3 6 -3 1175.88 27.50 -3 6 -3 1185.38 30.30 -3 6 -3 1112.79 30.00 -3 6 -3 1174.08 28.00 3 -6 3 1112.49 28.70 3 -6 3 1148.59 27.70 3 -6 3 1145.39 25.70 -4 6 -3 20.10 3.10 -4 6 -3 26.00 3.20 -4 6 -3 20.10 3.40 -4 6 -3 16.60 3.20 4 -6 3 18.20 3.30 -5 6 -3 30.00 4.20 -5 6 -3 31.20 4.50 -5 6 -3 24.80 3.90 5 -6 3 25.20 4.00 -6 6 -3 11.90 3.30 -6 6 -3 13.00 3.40 -6 6 -3 11.10 3.00 6 -6 3 5.10 2.60 -7 6 -3 -0.30 2.10 -7 6 -3 1.60 2.10 -7 6 -3 1.90 2.40 7 -6 3 0.20 2.20 -8 6 -3 -1.40 2.10 -8 6 -3 -0.70 2.30 -8 6 -3 -0.70 2.30 8 -6 3 0.10 2.40 -9 6 -3 13.10 4.10 -9 6 -3 8.80 3.80 9 -6 3 11.50 4.00 12 5 -3 15.00 4.50 -12 -5 3 9.20 3.90 -12 -5 3 10.80 3.60 -11 -5 3 182.08 10.70 -11 -5 3 185.08 10.60 -11 -5 3 148.79 9.40 10 5 -3 81.99 6.00 -10 -5 3 73.49 7.40 -10 -5 3 80.19 6.50 -10 -5 3 86.29 7.90 -10 -5 3 81.89 5.20 9 5 -3 225.28 9.60 -9 -5 3 223.38 10.60 -9 -5 3 211.28 8.20 -9 -5 3 217.18 10.30 -9 -5 3 226.98 10.90 8 5 -3 43.00 4.30 -8 -5 3 34.30 4.30 -8 -5 3 48.60 5.30 -8 -5 3 51.39 5.60 -8 -5 3 43.20 3.30 7 5 -3 272.57 9.70 -7 -5 3 260.67 10.40 -7 -5 3 260.47 8.50 -7 -5 3 256.77 10.20 -7 -5 3 256.37 10.70 6 5 -3 572.44 16.10 -6 -5 3 574.34 17.00 -6 -5 3 551.84 16.20 -6 -5 3 556.84 17.20 -6 -5 3 583.74 14.40 5 5 -3 381.46 11.60 -5 -5 3 376.16 11.70 -5 -5 3 375.96 12.50 -5 -5 3 379.96 10.20 4 5 -3 85.59 5.10 4 5 -3 85.69 4.50 -4 -5 3 88.19 3.80 -4 -5 3 89.89 5.00 -4 -5 3 89.49 4.60 3 5 -3 200.68 7.50 3 5 -3 196.18 7.20 -3 -5 3 199.88 6.90 -3 -5 3 199.38 7.60 -3 -5 3 191.48 6.20 -3 -5 3 201.58 7.60 2 5 -3 99.79 5.00 2 5 -3 96.49 4.80 2 5 -3 98.19 5.20 -2 -5 3 89.49 4.70 -2 -5 3 100.29 4.60 -2 -5 3 93.99 4.80 -2 -5 3 109.39 4.20 -2 -5 3 104.89 4.30 1 5 -3 178.68 7.00 1 5 -3 191.18 7.20 1 5 -3 189.88 4.70 1 5 -3 178.98 7.20 1 5 -3 175.78 7.10 -1 -5 3 182.78 6.80 -1 -5 3 165.68 6.60 -1 -5 3 178.98 6.00 -1 -5 3 181.68 7.10 -1 -5 3 181.28 5.80 -1 -5 3 193.68 6.90 0 5 -3 328.37 10.60 0 5 -3 304.77 10.30 0 5 -3 323.87 8.20 0 5 -3 316.97 10.30 0 5 -3 318.87 10.80 0 -5 3 324.47 10.10 0 -5 3 320.97 9.20 0 -5 3 318.07 8.40 0 -5 3 323.87 10.20 0 -5 3 322.27 9.70 -1 5 -3 878.11 23.00 -1 5 -3 921.31 20.30 -1 5 -3 901.21 22.20 -1 5 -3 890.71 24.00 -1 5 -3 886.11 22.80 1 -5 3 894.41 23.10 1 -5 3 891.91 22.10 1 -5 3 885.01 21.50 1 -5 3 891.71 19.70 1 -5 3 931.11 21.10 -2 5 -3 804.42 21.40 -2 5 -3 792.72 19.00 -2 5 -3 800.22 20.20 -2 5 -3 804.92 21.30 -2 5 -3 784.02 22.40 2 -5 3 799.62 19.50 2 -5 3 785.02 20.40 2 -5 3 785.82 21.30 2 -5 3 799.32 17.80 2 -5 3 793.22 19.60 -3 5 -3 1991.30 48.40 -3 5 -3 1944.11 46.10 -3 5 -3 1974.50 44.00 -3 5 -3 1986.30 42.90 -3 5 -3 1994.20 46.70 3 -5 3 1936.91 42.90 3 -5 3 1919.81 44.20 3 -5 3 2060.89 41.20 -4 5 -3 350.96 13.50 -4 5 -3 314.77 10.80 -4 5 -3 331.27 12.10 -4 5 -3 345.57 10.90 -4 5 -3 319.27 12.00 4 -5 3 326.07 12.20 4 -5 3 318.57 11.40 4 -5 3 338.17 9.40 4 -5 3 330.37 11.00 -5 5 -3 261.77 10.10 -5 5 -3 259.97 10.90 -5 5 -3 261.97 11.00 -5 5 -3 280.07 9.80 5 -5 3 268.07 10.60 -6 5 -3 44.80 5.00 -6 5 -3 43.20 5.00 -6 5 -3 46.90 5.50 6 -5 3 38.20 4.90 -7 5 -3 33.30 4.90 -7 5 -3 47.10 5.80 -7 5 -3 40.50 5.10 7 -5 3 39.20 5.30 -8 5 -3 17.80 4.10 -8 5 -3 15.80 3.90 -8 5 -3 14.90 3.80 8 -5 3 11.40 3.40 -9 5 -3 8.10 3.40 -9 5 -3 7.40 3.60 -9 5 -3 8.10 3.70 9 -5 3 6.80 3.30 -10 5 -3 163.68 11.00 -10 5 -3 139.49 10.40 10 -5 3 148.79 10.40 12 4 -3 35.40 5.80 -12 -4 3 25.60 5.00 -12 -4 3 33.20 6.20 -12 -4 3 31.60 5.40 11 4 -3 30.50 4.50 11 4 -3 35.30 5.70 -11 -4 3 41.80 6.10 -11 -4 3 30.70 5.00 -11 -4 3 41.20 6.10 -11 -4 3 29.10 3.90 10 4 -3 2.20 1.90 -10 -4 3 4.60 2.50 -10 -4 3 4.70 2.80 -10 -4 3 9.30 2.20 -10 -4 3 8.20 2.80 9 4 -3 11.00 2.40 -9 -4 3 7.80 2.50 -9 -4 3 5.00 2.30 -9 -4 3 6.70 1.70 -9 -4 3 6.20 2.70 8 4 -3 0.40 1.20 -8 -4 3 1.90 1.60 -8 -4 3 -0.10 1.00 -8 -4 3 -0.50 1.30 -8 -4 3 0.70 1.70 7 4 -3 159.28 6.80 -7 -4 3 145.19 7.40 -7 -4 3 159.18 7.60 -7 -4 3 158.58 5.90 -7 -4 3 161.78 7.90 6 4 -3 2.70 1.20 -6 -4 3 0.10 0.90 -6 -4 3 0.10 0.70 -6 -4 3 0.20 1.20 -6 -4 3 1.40 1.00 -6 -4 3 -0.70 1.10 5 4 -3 5.10 1.50 -5 -4 3 6.00 1.70 -5 -4 3 5.50 1.70 -5 -4 3 7.60 1.30 4 4 -3 178.88 6.50 4 4 -3 178.48 6.30 -4 -4 3 173.78 6.50 -4 -4 3 174.78 6.90 -4 -4 3 167.68 4.60 3 4 -3 16.80 2.20 3 4 -3 19.70 2.30 -3 -4 3 17.60 1.50 -3 -4 3 18.60 2.20 -3 -4 3 21.60 2.60 2 4 -3 6.80 1.60 2 4 -3 7.70 1.50 2 4 -3 7.30 1.40 2 4 -3 7.90 1.50 -2 -4 3 6.00 1.50 -2 -4 3 9.40 1.30 -2 -4 3 7.80 1.40 -2 -4 3 7.90 1.60 1 4 -3 505.15 13.80 1 4 -3 523.75 10.80 1 4 -3 529.25 13.70 1 4 -3 496.05 14.10 1 4 -3 499.95 13.60 -1 -4 3 508.25 13.70 -1 -4 3 488.85 13.50 -1 -4 3 526.75 13.40 -1 -4 3 496.35 12.10 -1 -4 3 511.35 12.00 -1 -4 3 503.05 13.40 0 4 -3 605.54 15.90 0 4 -3 585.54 15.70 0 4 -3 611.24 16.10 0 4 -3 612.84 13.30 0 4 -3 575.64 15.60 0 4 -3 632.14 16.40 0 -4 3 612.74 15.40 0 -4 3 586.14 15.10 0 -4 3 591.44 14.20 0 -4 3 624.44 15.70 0 -4 3 603.24 15.60 0 -4 3 585.44 13.40 -1 4 -3 91.39 4.90 -1 4 -3 89.39 4.50 -1 4 -3 94.99 3.70 -1 4 -3 90.59 4.40 -1 4 -3 99.19 4.80 1 -4 3 91.79 3.30 1 -4 3 93.29 4.40 1 -4 3 90.49 4.20 1 -4 3 97.99 4.60 1 -4 3 88.19 3.90 -2 4 -3 60.89 3.60 -2 4 -3 57.09 3.80 -2 4 -3 58.49 3.20 -2 4 -3 57.79 4.20 -2 4 -3 60.39 3.90 2 -4 3 59.59 2.50 2 -4 3 59.09 3.40 2 -4 3 56.59 3.30 2 -4 3 59.59 3.70 2 -4 3 62.59 3.90 -3 4 -3 5.50 2.00 -3 4 -3 2.50 1.30 -3 4 -3 3.40 1.30 -3 4 -3 3.20 1.20 -3 4 -3 2.60 1.40 3 -4 3 2.40 1.30 3 -4 3 2.60 0.90 3 -4 3 2.00 1.20 3 -4 3 0.30 1.00 -4 4 -3 9.20 2.20 -4 4 -3 6.40 1.60 -4 4 -3 9.70 2.50 -4 4 -3 11.50 2.20 -4 4 -3 14.70 2.60 4 -4 3 10.80 2.00 4 -4 3 11.20 1.60 4 -4 3 10.50 2.20 -5 4 -3 187.88 8.40 -5 4 -3 184.58 8.60 -5 4 -3 185.88 7.90 -5 4 -3 186.48 7.50 -5 4 -3 176.08 9.20 5 -4 3 182.78 6.30 5 -4 3 174.08 8.00 5 -4 3 184.58 7.60 -6 4 -3 4.80 2.00 -6 4 -3 8.00 2.60 -6 4 -3 7.90 2.10 -6 4 -3 6.60 2.30 6 -4 3 4.70 2.00 -7 4 -3 50.09 5.50 -7 4 -3 47.30 5.60 -7 4 -3 55.09 6.00 7 -4 3 42.70 5.00 -8 4 -3 3.90 2.60 -8 4 -3 7.40 3.00 -8 4 -3 4.90 2.50 8 -4 3 4.10 2.50 -9 4 -3 26.90 4.80 -9 4 -3 23.90 4.70 -9 4 -3 25.80 4.70 9 -4 3 26.50 5.10 -10 4 -3 88.99 9.10 -10 4 -3 54.99 7.30 10 -4 3 61.39 7.20 12 3 -3 3.50 3.30 -12 -3 3 7.90 3.80 -12 -3 3 9.30 3.60 11 3 -3 87.69 6.60 11 3 -3 95.49 9.10 -11 -3 3 91.99 8.50 -11 -3 3 90.69 7.00 -11 -3 3 96.19 8.00 -11 -3 3 98.19 7.90 -11 -3 3 90.59 5.90 10 3 -3 50.09 5.30 10 3 -3 38.30 5.60 -10 -3 3 56.49 5.90 -10 -3 3 44.70 4.30 -10 -3 3 46.30 5.90 -10 -3 3 47.10 5.80 -10 -3 3 43.20 5.70 9 3 -3 80.49 5.30 -9 -3 3 83.29 5.90 -9 -3 3 81.19 4.70 -9 -3 3 67.59 6.50 -9 -3 3 85.99 5.80 -9 -3 3 88.39 6.30 -9 -3 3 78.79 6.10 8 3 -3 403.66 12.90 -8 -3 3 417.86 14.20 -8 -3 3 411.26 14.20 -8 -3 3 412.66 11.60 -8 -3 3 409.76 12.80 -8 -3 3 390.36 13.50 -8 -3 3 394.16 14.40 7 3 -3 597.24 16.30 -7 -3 3 562.74 17.00 -7 -3 3 584.14 14.60 -7 -3 3 560.84 16.80 -7 -3 3 599.54 17.50 -7 -3 3 596.94 15.70 -7 -3 3 590.94 17.90 -6 -3 3 1111.99 26.80 -6 -3 3 1078.29 26.80 -6 -3 3 1085.79 24.90 -6 -3 3 1097.09 28.00 5 3 -3 642.64 16.60 -5 -3 3 610.24 17.40 -5 -3 3 608.34 16.50 -5 -3 3 634.94 15.00 -5 -3 3 630.04 16.80 4 3 -3 1120.49 26.00 -4 -3 3 1115.19 23.70 -4 -3 3 1098.99 23.20 -4 -3 3 1074.09 26.00 -4 -3 3 1106.29 27.00 -4 -3 3 1149.39 25.50 3 3 -3 688.63 16.10 3 3 -3 579.84 15.60 -3 -3 3 649.64 16.40 -3 -3 3 659.63 14.10 -3 -3 3 671.03 17.00 -3 -3 3 660.83 15.70 -3 -3 3 668.13 14.20 2 3 -3 295.37 8.20 2 3 -3 303.97 6.40 -2 -3 3 269.77 6.90 -2 -3 3 287.27 6.60 -2 -3 3 289.97 7.90 1 3 -3 84.99 2.40 1 3 -3 86.79 3.50 1 3 -3 81.89 3.80 1 3 -3 89.49 3.60 1 3 -3 91.79 4.20 -1 -3 3 82.89 3.30 -1 -3 3 82.99 3.10 -1 -3 3 76.79 2.90 -1 -3 3 81.19 3.70 -1 -3 3 79.89 3.70 -1 -3 3 81.69 3.80 0 3 -3 127.19 4.90 0 3 -3 129.59 4.80 0 3 -3 123.59 4.90 0 3 -3 136.09 5.30 0 3 -3 124.59 3.70 0 3 -3 123.49 5.10 0 -3 3 127.39 4.20 0 -3 3 133.79 4.90 0 -3 3 137.69 3.80 0 -3 3 124.39 4.80 0 -3 3 125.69 4.90 0 -3 3 134.69 4.70 -1 3 -3 12.10 1.40 -1 3 -3 14.90 2.00 -1 3 -3 12.30 1.90 -1 3 -3 10.80 1.60 -1 3 -3 10.50 1.80 -1 3 -3 11.30 1.80 1 -3 3 12.20 1.00 1 -3 3 10.50 1.60 1 -3 3 12.60 1.80 1 -3 3 12.70 1.80 1 -3 3 11.50 1.50 -2 3 -3 28.70 2.50 -2 3 -3 33.80 2.60 -2 3 -3 28.00 2.50 -2 3 -3 33.10 2.20 -2 3 -3 31.60 3.40 2 -3 3 28.90 2.50 2 -3 3 32.40 1.60 2 -3 3 32.60 2.40 2 -3 3 31.40 2.50 -3 3 -3 623.14 15.50 -3 3 -3 617.64 17.90 -3 3 -3 643.34 17.40 -3 3 -3 624.84 16.20 -3 3 -3 622.64 16.70 3 -3 3 629.34 13.90 3 -3 3 614.04 16.20 3 -3 3 654.83 15.70 -4 3 -3 1075.69 25.60 -4 3 -3 1059.59 24.90 -4 3 -3 1067.59 28.20 -4 3 -3 1077.69 23.00 -4 3 -3 1048.50 27.10 -4 3 -3 1097.09 26.60 4 -3 3 1066.19 24.70 4 -3 3 1047.30 25.50 4 -3 3 1054.59 23.00 -5 3 -3 931.01 23.10 -5 3 -3 938.91 21.00 -5 3 -3 926.41 25.90 -5 3 -3 926.11 24.10 -5 3 -3 905.21 22.90 -5 3 -3 895.71 24.70 5 -3 3 909.41 23.40 5 -3 3 949.40 22.70 5 -3 3 925.71 20.90 -6 3 -3 263.77 10.00 -6 3 -3 267.77 8.40 -6 3 -3 258.67 10.30 -6 3 -3 272.17 9.70 -6 3 -3 261.87 10.70 6 -3 3 257.17 8.20 6 -3 3 256.17 10.00 -7 3 -3 264.07 10.00 -7 3 -3 259.17 10.70 -7 3 -3 270.97 11.60 -7 3 -3 275.07 11.10 -7 3 -3 267.27 9.10 7 -3 3 271.47 11.00 7 -3 3 265.97 9.00 -8 3 -3 101.89 7.00 -8 3 -3 95.69 7.00 -8 3 -3 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107.59 8.60 -11 -1 5 116.99 9.30 10 1 -5 603.84 20.80 -10 -1 5 586.34 20.50 -10 -1 5 574.04 20.30 -10 -1 5 583.74 19.90 9 1 -5 239.38 11.30 -9 -1 5 204.58 8.00 -9 -1 5 191.68 10.00 -9 -1 5 210.38 10.40 -9 -1 5 208.68 10.60 -9 -1 5 211.18 10.70 8 1 -5 143.89 8.40 -8 -1 5 158.48 6.20 -8 -1 5 143.09 8.00 -8 -1 5 151.58 8.50 -8 -1 5 155.38 8.20 -8 -1 5 154.68 8.50 -7 -1 5 257.27 10.50 -7 -1 5 254.07 10.20 -7 -1 5 255.67 7.90 -7 -1 5 262.47 9.50 -7 -1 5 259.57 10.70 -7 -1 5 262.07 10.80 -6 -1 5 87.79 5.40 -6 -1 5 83.99 5.20 -6 -1 5 86.79 5.60 -6 -1 5 86.69 5.50 -6 -1 5 99.79 5.10 5 1 -5 22.70 2.30 -5 -1 5 18.00 2.70 -5 -1 5 24.30 2.70 -5 -1 5 12.80 2.30 -5 -1 5 19.90 2.80 -5 -1 5 13.70 2.60 4 1 -5 6.40 1.10 -4 -1 5 4.00 1.40 -4 -1 5 6.60 1.50 -4 -1 5 5.00 1.50 -4 -1 5 7.20 1.60 -4 -1 5 5.50 1.60 3 1 -5 259.07 6.50 -3 -1 5 270.97 8.70 -3 -1 5 260.07 8.40 -3 -1 5 272.07 8.30 -3 -1 5 265.67 8.30 -3 -1 5 253.87 8.40 -2 -1 5 901.31 21.80 -2 -1 5 919.71 20.60 -2 -1 5 872.91 21.00 -2 -1 5 896.61 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20.80 4.10 -3 5 -9 17.30 3.60 -3 5 -9 17.90 3.00 -3 5 -9 19.10 4.00 3 -5 9 16.20 3.50 3 -5 9 18.30 3.00 -4 5 -9 480.45 18.30 -4 5 -9 492.35 15.20 -4 5 -9 492.65 18.30 -4 5 -9 465.05 17.40 -4 5 -9 490.85 16.60 4 -5 9 459.15 15.30 4 -5 9 486.05 16.90 -5 5 -9 153.58 10.10 -5 5 -9 171.58 8.50 -5 5 -9 147.89 9.60 -5 5 -9 153.38 9.30 -5 5 -9 162.98 8.90 5 -5 9 159.78 9.10 5 -5 9 157.18 8.50 -6 5 -9 650.53 23.90 -6 5 -9 609.34 19.60 -6 5 -9 636.54 22.80 -6 5 -9 622.84 21.70 6 -5 9 636.04 20.90 -7 5 -9 51.69 7.10 -7 5 -9 42.60 5.70 -7 5 -9 53.19 6.70 7 -5 9 49.10 6.50 -8 5 -9 5.70 3.30 -8 5 -9 2.10 3.00 -8 5 -9 7.90 3.60 8 -5 9 9.00 3.80 8 4 -9 79.79 4.20 -8 -4 9 77.29 7.50 -8 -4 9 73.49 7.50 -8 -4 9 68.59 7.30 7 4 -9 12.50 1.60 7 4 -9 12.40 3.70 -7 -4 9 8.80 1.60 -7 -4 9 10.80 3.20 -7 -4 9 13.60 3.50 -7 -4 9 6.70 2.90 6 4 -9 1.70 2.00 6 4 -9 0.40 0.80 -6 -4 9 1.10 2.00 -6 -4 9 -0.90 1.50 -6 -4 9 0.00 2.00 -6 -4 9 0.60 0.80 5 4 -9 81.19 3.30 5 4 -9 79.29 6.50 -5 -4 9 81.49 6.10 -5 -4 9 82.59 5.90 -5 -4 9 84.49 6.30 -5 -4 9 76.89 3.30 4 4 -9 34.80 2.40 4 4 -9 37.00 5.10 4 4 -9 29.30 4.60 -4 -4 9 34.10 4.60 -4 -4 9 34.80 2.20 -4 -4 9 42.90 5.10 3 4 -9 100.39 6.90 3 4 -9 89.69 4.20 3 4 -9 96.89 6.70 -3 -4 9 96.69 6.40 -3 -4 9 97.19 6.40 -3 -4 9 98.89 3.80 2 4 -9 61.99 5.30 2 4 -9 57.09 3.60 2 4 -9 48.70 5.50 2 4 -9 58.19 4.60 -2 -4 9 59.19 4.90 -2 -4 9 50.39 2.90 -2 -4 9 55.69 5.60 1 4 -9 54.79 4.40 1 4 -9 49.60 5.40 1 4 -9 54.69 3.80 1 4 -9 52.89 5.60 -1 -4 9 42.20 4.70 -1 -4 9 50.89 3.10 0 4 -9 168.68 8.60 0 4 -9 152.38 8.50 0 4 -9 164.08 7.40 0 4 -9 170.68 6.50 0 4 -9 168.18 7.60 0 -4 9 168.18 8.30 0 -4 9 167.78 6.20 -1 4 -9 7.10 2.50 -1 4 -9 3.30 1.50 -1 4 -9 3.20 1.70 -1 4 -9 -0.20 1.50 -1 4 -9 2.50 1.60 1 -4 9 0.90 1.50 1 -4 9 3.40 2.10 1 -4 9 2.10 1.30 -2 4 -9 178.98 9.30 -2 4 -9 175.78 8.70 -2 4 -9 195.68 8.30 -2 4 -9 184.08 9.40 -2 4 -9 191.08 7.50 2 -4 9 182.78 7.40 2 -4 9 185.28 8.80 -3 4 -9 6.00 2.20 -3 4 -9 6.40 2.60 -3 4 -9 8.80 2.70 -3 4 -9 4.60 1.80 -3 4 -9 7.50 2.40 3 -4 9 7.70 2.60 3 -4 9 8.20 2.30 -4 4 -9 28.40 4.50 -4 4 -9 28.70 4.50 -4 4 -9 27.60 4.00 -4 4 -9 28.50 3.70 -4 4 -9 17.20 3.50 4 -4 9 30.70 4.50 4 -4 9 29.00 3.70 -5 4 -9 0.70 1.70 -5 4 -9 0.60 1.70 -5 4 -9 1.70 1.80 -5 4 -9 2.60 2.40 -5 4 -9 -0.40 1.80 5 -4 9 3.10 2.10 5 -4 9 -0.10 1.90 -6 4 -9 85.79 7.10 -6 4 -9 78.79 7.60 -6 4 -9 76.19 8.20 -6 4 -9 83.29 6.30 6 -4 9 72.29 6.50 6 -4 9 78.59 7.20 -7 4 -9 19.90 4.00 -7 4 -9 14.20 3.90 -7 4 -9 20.80 4.20 7 -4 9 20.20 4.30 -8 4 -9 3.50 2.70 -8 4 -9 3.50 3.00 -8 4 -9 1.40 2.30 8 -4 9 2.20 2.70 -9 4 -9 45.70 6.40 -9 4 -9 40.80 6.30 9 -4 9 56.69 7.00 9 3 -9 72.79 8.20 -9 -3 9 89.09 8.80 -9 -3 9 85.39 8.80 -8 -3 9 300.57 13.60 -8 -3 9 289.27 13.30 -7 -3 9 136.89 8.60 -7 -3 9 129.99 8.30 -7 -3 9 143.49 4.90 -7 -3 9 152.98 8.50 6 3 -9 116.19 8.00 -6 -3 9 102.49 3.60 -6 -3 9 93.39 6.50 -6 -3 9 90.59 6.60 -6 -3 9 103.99 6.90 5 3 -9 243.28 11.40 -5 -3 9 238.48 6.10 -5 -3 9 238.88 10.00 -5 -3 9 235.58 10.60 -5 -3 9 241.88 10.30 4 3 -9 376.06 14.20 4 3 -9 372.76 14.20 -4 -3 9 358.76 12.30 -4 -3 9 383.66 13.50 -4 -3 9 368.66 8.50 -4 -3 9 358.96 13.30 3 3 -9 930.81 20.70 3 3 -9 902.01 25.70 3 3 -9 930.01 20.80 3 3 -9 899.31 25.90 -3 -3 9 898.71 25.10 -3 -3 9 912.21 22.80 -3 -3 9 893.01 19.20 -3 -3 9 941.61 24.90 2 3 -9 141.39 7.70 2 3 -9 151.08 5.40 2 3 -9 146.39 5.10 2 3 -9 150.68 8.00 2 3 -9 157.58 6.10 -2 -3 9 145.59 7.50 -2 -3 9 145.89 4.60 -2 -3 9 155.78 7.70 1 3 -9 67.39 4.50 1 3 -9 69.89 3.80 1 3 -9 63.09 3.80 1 3 -9 66.99 5.10 1 3 -9 66.29 5.30 -1 -3 9 60.99 4.80 -1 -3 9 61.89 3.10 -1 -3 9 65.29 4.70 0 3 -9 103.19 5.20 0 3 -9 104.39 6.60 0 3 -9 93.59 5.30 0 3 -9 97.39 6.20 0 3 -9 102.59 4.90 0 -3 9 104.99 4.40 0 -3 9 103.49 6.10 -1 3 -9 102.79 6.50 -1 3 -9 119.29 5.70 -1 3 -9 111.39 5.20 -1 3 -9 99.39 5.60 -1 3 -9 94.19 6.20 1 -3 9 96.69 5.80 1 -3 9 96.59 4.70 1 -3 9 108.19 6.30 -2 3 -9 589.74 18.80 -2 3 -9 582.34 15.80 -2 3 -9 586.24 18.60 -2 3 -9 618.14 16.80 -2 3 -9 568.84 17.80 2 -3 9 581.74 17.30 2 -3 9 570.24 15.40 -3 3 -9 1.70 1.50 -3 3 -9 1.30 1.40 -3 3 -9 2.50 1.50 -3 3 -9 1.50 1.50 -3 3 -9 0.30 1.40 3 -3 9 2.40 1.50 3 -3 9 2.50 1.80 -4 3 -9 78.79 5.20 -4 3 -9 78.39 5.20 -4 3 -9 91.19 6.60 -4 3 -9 78.49 6.10 -4 3 -9 82.69 6.30 4 -3 9 74.49 5.10 4 -3 9 81.49 5.60 -5 3 -9 208.08 10.60 -5 3 -9 202.48 8.90 -5 3 -9 197.18 10.60 -5 3 -9 213.28 10.40 5 -3 9 225.98 9.30 5 -3 9 202.48 9.30 -6 3 -9 178.88 10.70 -6 3 -9 183.98 9.80 -6 3 -9 188.78 10.40 -6 3 -9 185.48 8.80 6 -3 9 194.18 9.10 6 -3 9 175.28 8.90 -7 3 -9 232.58 10.60 -7 3 -9 236.68 12.20 -7 3 -9 223.48 11.50 -7 3 -9 215.28 12.40 7 -3 9 223.38 10.60 7 -3 9 230.68 11.40 -8 3 -9 125.09 9.20 -8 3 -9 124.49 8.70 -8 3 -9 129.09 8.40 8 -3 9 112.59 7.90 -9 3 -9 166.78 10.20 -9 3 -9 147.19 9.90 -9 3 -9 132.49 10.00 9 -3 9 137.49 9.20 9 2 -9 13.70 4.30 9 2 -9 10.10 4.40 -9 -2 9 11.10 4.00 8 2 -9 1.30 2.80 -8 -2 9 -0.70 2.50 -8 -2 9 1.60 2.30 7 2 -9 15.80 3.70 -7 -2 9 11.30 3.20 -7 -2 9 12.10 3.40 -7 -2 9 13.30 1.70 6 2 -9 35.10 4.60 -6 -2 9 38.30 5.10 -6 -2 9 22.20 3.90 -6 -2 9 27.50 3.90 -6 -2 9 26.40 1.80 5 2 -9 3.10 2.10 5 2 -9 8.10 2.60 5 2 -9 7.50 2.60 -5 -2 9 13.20 2.90 -5 -2 9 6.90 0.80 -5 -2 9 7.40 2.50 -5 -2 9 5.00 2.20 -5 -2 9 6.60 2.60 4 2 -9 15.50 3.30 4 2 -9 14.30 3.00 4 2 -9 13.30 2.70 4 2 -9 14.40 2.50 -4 -2 9 8.20 2.20 -4 -2 9 8.80 2.40 -4 -2 9 11.40 2.50 -4 -2 9 12.60 2.80 3 2 -9 18.60 2.80 3 2 -9 17.10 2.50 3 2 -9 17.50 3.30 3 2 -9 14.30 2.90 -3 -2 9 15.90 2.80 -3 -2 9 13.40 2.60 -3 -2 9 12.20 2.40 -3 -2 9 20.90 3.20 2 2 -9 35.10 4.30 2 2 -9 32.60 3.30 2 2 -9 25.40 1.70 2 2 -9 28.20 3.00 2 2 -9 33.00 4.00 2 2 -9 28.10 1.60 -2 -2 9 30.60 3.20 -2 -2 9 37.10 4.20 -2 -2 9 28.80 3.40 -2 -2 9 27.20 1.50 -2 -2 9 25.30 3.40 1 2 -9 513.15 16.80 1 2 -9 548.95 13.50 1 2 -9 546.25 16.90 1 2 -9 546.25 14.50 1 2 -9 572.04 15.70 1 2 -9 563.44 14.10 -1 -2 9 530.95 16.30 -1 -2 9 536.65 15.20 -1 -2 9 536.35 12.40 -1 -2 9 531.35 16.20 0 2 -9 246.18 8.50 0 2 -9 241.18 10.00 0 2 -9 232.88 8.10 0 2 -9 236.28 8.10 0 2 -9 221.18 9.50 0 -2 9 232.38 9.50 0 -2 9 237.58 6.90 -1 2 -9 8.90 1.90 -1 2 -9 11.50 2.60 -1 2 -9 11.10 2.50 -1 2 -9 10.90 2.10 -1 2 -9 9.90 2.00 1 -2 9 7.60 2.10 1 -2 9 8.60 1.60 -2 2 -9 61.89 4.60 -2 2 -9 61.69 4.10 -2 2 -9 67.19 5.30 -2 2 -9 68.69 5.20 -2 2 -9 67.29 4.10 2 -2 9 70.69 4.70 2 -2 9 69.19 3.90 -3 2 -9 192.78 7.30 -3 2 -9 177.18 8.90 -3 2 -9 185.88 8.70 -3 2 -9 184.18 8.80 -3 2 -9 188.38 7.60 3 -2 9 174.68 7.70 3 -2 9 190.18 7.40 -4 2 -9 30.10 4.20 -4 2 -9 30.20 3.70 -4 2 -9 24.70 4.00 -4 2 -9 27.10 4.00 4 -2 9 35.60 4.10 4 -2 9 28.70 3.50 -5 2 -9 8.90 2.70 -5 2 -9 6.10 2.30 -5 2 -9 10.60 3.10 -5 2 -9 9.20 2.40 5 -2 9 7.60 2.30 5 -2 9 9.30 2.40 -6 2 -9 34.30 4.20 -6 2 -9 13.00 3.30 -6 2 -9 26.00 4.30 -6 2 -9 19.70 3.80 6 -2 9 25.80 3.80 6 -2 9 19.20 3.40 -7 2 -9 21.70 4.30 -7 2 -9 16.80 3.50 -7 2 -9 19.20 4.00 -7 2 -9 18.30 4.10 7 -2 9 23.30 4.00 -8 2 -9 31.20 5.30 -8 2 -9 29.40 4.60 -8 2 -9 26.20 4.80 8 -2 9 33.60 4.80 -9 2 -9 11.90 3.60 -9 2 -9 21.00 4.40 -9 2 -9 6.50 3.30 9 -2 9 10.50 3.50 -10 2 -9 239.28 12.70 -10 2 -9 240.58 12.80 -10 2 -9 241.18 13.60 10 -2 9 226.48 11.70 8 1 -9 30.10 5.10 8 1 -9 38.80 5.70 -8 -1 9 24.80 4.80 7 1 -9 150.08 9.10 -7 -1 9 137.99 5.10 -7 -1 9 149.39 9.00 -7 -1 9 148.99 9.30 6 1 -9 252.07 11.00 -6 -1 9 245.68 6.70 -6 -1 9 284.67 11.40 -6 -1 9 256.17 11.30 -6 -1 9 242.48 10.80 5 1 -9 394.26 13.50 5 1 -9 373.06 13.70 5 1 -9 405.26 14.60 -5 -1 9 390.76 13.40 -5 -1 9 389.26 13.80 -5 -1 9 373.46 13.30 -5 -1 9 377.66 13.40 4 1 -9 172.48 8.30 4 1 -9 163.38 8.20 4 1 -9 158.78 7.50 -4 -1 9 161.58 7.80 -4 -1 9 173.98 7.90 -4 -1 9 157.28 7.80 -4 -1 9 152.58 7.40 3 1 -9 438.86 14.50 3 1 -9 442.56 13.00 3 1 -9 446.06 14.50 3 1 -9 442.56 13.20 -3 -1 9 424.46 13.60 -3 -1 9 410.86 13.60 -3 -1 9 425.46 13.80 -3 -1 9 431.76 13.30 2 1 -9 1.00 1.10 2 1 -9 2.40 1.60 2 1 -9 1.50 1.20 2 1 -9 0.50 1.20 -2 -1 9 0.80 1.30 -2 -1 9 1.00 1.40 -2 -1 9 2.30 1.30 -2 -1 9 -0.70 1.10 1 1 -9 973.40 22.50 1 1 -9 952.20 23.10 1 1 -9 957.50 25.50 1 1 -9 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-1 -13 44.60 6.00 -4 1 13 50.79 6.70 3 -1 -13 147.39 8.80 -3 1 13 159.08 10.00 2 -1 -13 125.99 7.80 -2 1 13 110.39 8.20 1 -1 -13 175.78 5.50 1 -1 -13 177.08 9.10 -1 1 13 158.28 9.50 0 -1 -13 95.49 4.70 0 -1 -13 83.19 6.30 0 1 13 84.79 7.70 -1 -1 -13 163.08 9.20 -1 -1 -13 156.68 8.30 -1 -1 -13 161.48 7.10 -2 -1 -13 269.77 11.20 -2 -1 -13 269.47 10.60 -2 -1 -13 271.47 12.30 -3 -1 -13 131.89 8.60 -3 -1 -13 115.69 7.10 -3 -1 -13 104.89 7.00 -4 -1 -13 109.79 7.30 -4 -1 -13 94.19 7.50 -4 -1 -13 109.59 7.20 -5 -1 -13 12.50 3.40 -5 -1 -13 11.60 3.60 -5 -1 -13 6.10 2.70 -6 -1 -13 268.17 13.30 -6 -1 -13 280.17 12.20 -6 -1 -13 273.27 13.50 -7 -1 -13 172.28 11.00 -7 -1 -13 195.28 12.40 -7 -1 -13 190.68 10.40 -7 -1 -13 189.28 12.40 -8 -1 -13 77.79 7.70 -8 -1 -13 114.29 10.70 -8 -1 -13 95.49 8.20 3 -2 -13 4.10 2.70 -3 2 13 2.60 2.70 2 -2 -13 14.40 3.60 -2 2 13 15.00 4.00 1 -2 -13 20.20 3.80 1 -2 -13 15.80 2.00 -1 2 13 13.80 3.70 0 -2 -13 22.60 2.80 0 -2 -13 19.60 3.90 0 2 13 25.60 4.70 -1 -2 -13 5.30 1.90 -1 -2 -13 3.30 2.30 -2 -2 -13 20.50 4.00 -2 -2 -13 19.00 3.70 -2 -2 -13 19.00 3.20 -3 -2 -13 138.09 8.70 -3 -2 -13 133.99 7.90 -3 -2 -13 133.89 7.60 -4 -2 -13 37.20 5.00 -4 -2 -13 25.90 4.20 -4 -2 -13 33.10 4.90 -5 -2 -13 0.80 2.20 -5 -2 -13 3.70 2.40 -5 -2 -13 0.80 2.10 -6 -2 -13 37.00 5.90 -6 -2 -13 43.70 5.50 -6 -2 -13 45.30 6.20 -7 -2 -13 2.00 2.40 -7 -2 -13 2.40 2.80 -7 -2 -13 4.80 3.10 -8 -2 -13 1.70 2.90 -8 -2 -13 -0.40 2.40 3 -3 -13 193.88 10.70 3 -3 -13 194.38 10.50 -3 3 13 195.78 11.70 2 -3 -13 167.78 9.40 -2 3 13 148.29 10.10 1 -3 -13 307.97 9.80 1 -3 -13 295.67 12.70 -1 3 13 324.37 14.30 0 -3 -13 18.30 2.80 0 -3 -13 15.60 3.70 0 3 13 18.40 4.10 -1 -3 -13 221.68 10.50 -1 -3 -13 245.38 9.60 1 3 13 234.38 11.70 -2 -3 -13 6.70 2.30 -2 -3 -13 4.80 2.50 -3 -3 -13 210.58 10.60 -3 -3 -13 211.98 9.80 -3 -3 -13 190.68 9.70 -4 -3 -13 29.80 4.70 -4 -3 -13 30.30 4.60 -4 -3 -13 32.60 4.90 -5 -3 -13 0.90 2.20 -5 -3 -13 -0.30 1.90 -5 -3 -13 -1.20 2.00 -6 -3 -13 51.49 6.50 -6 -3 -13 35.50 5.60 -6 -3 -13 34.40 4.80 -7 -3 -13 159.48 10.20 -7 -3 -13 177.98 9.90 -7 -3 -13 147.69 10.60 -8 -3 -13 104.09 8.70 -8 -3 -13 105.49 8.40 2 -4 -13 49.99 6.20 2 -4 -13 52.69 6.30 -2 4 13 52.79 7.00 1 -4 -13 -1.30 2.40 -1 4 13 2.80 2.90 0 -4 -13 56.29 6.30 0 4 13 39.20 5.80 -1 -4 -13 2.00 1.70 -1 -4 -13 -1.50 2.10 1 4 13 -0.90 2.30 -2 -4 -13 5.60 2.80 -2 -4 -13 1.80 1.90 2 4 13 2.60 2.70 -3 -4 -13 7.20 2.50 -3 -4 -13 5.40 2.60 -4 -4 -13 41.30 5.30 -4 -4 -13 52.39 6.00 -5 -4 -13 11.20 3.30 -5 -4 -13 9.80 3.20 -5 -4 -13 8.40 3.00 -6 -4 -13 18.50 4.10 -6 -4 -13 17.30 4.10 -6 -4 -13 11.90 3.40 -7 -4 -13 5.20 3.00 -7 -4 -13 3.40 2.80 -8 -4 -13 -1.30 2.50 -8 -4 -13 -4.40 2.00 1 -5 -13 121.39 8.30 1 -5 -13 110.49 8.10 -1 5 13 106.69 9.80 0 -5 -13 194.78 10.30 0 5 13 175.78 11.00 -1 -5 -13 130.29 8.50 1 5 13 159.38 9.90 -2 -5 -13 1.70 2.60 2 5 13 5.00 2.90 -3 -5 -13 22.80 4.20 -4 -5 -13 311.37 13.10 -5 -5 -13 53.69 6.10 -6 -5 -13 217.98 10.90 -6 -5 -13 209.38 11.30 -7 -5 -13 24.60 4.60 -7 -5 -13 23.50 4.80 -8 -5 -13 121.39 9.30 -8 -5 -13 97.39 8.70 0 -6 -13 31.70 5.10 0 -6 -13 27.90 5.00 0 6 13 23.90 5.00 -1 -6 -13 27.60 4.60 -1 -6 -13 32.60 5.50 1 6 13 38.10 6.10 -2 -6 -13 -0.60 2.30 2 6 13 -2.70 2.60 -3 -6 -13 26.70 4.50 -4 -6 -13 39.80 5.50 -5 -6 -13 59.89 6.70 -6 -6 -13 15.90 3.80 -7 -6 -13 9.20 3.60 -7 -6 -13 9.40 3.70 -2 -7 -13 59.89 6.90 -2 -7 -13 56.39 6.60 2 7 13 65.19 7.90 -3 -7 -13 4.70 3.10 3 7 13 8.20 3.70 -4 -7 -13 22.70 4.40 -5 -7 -13 -0.40 2.30 -6 -7 -13 130.09 8.80 1 4 -14 128.79 9.90 1 4 -14 135.49 10.00 0 4 -14 155.08 10.70 0 4 -14 167.18 11.20 -1 4 -14 6.90 3.60 -1 4 -14 3.10 3.20 -2 4 -14 23.40 5.10 -3 4 -14 122.19 9.80 2 3 -14 2.50 3.10 1 3 -14 34.00 5.70 1 3 -14 38.90 6.00 0 3 -14 8.30 3.40 0 3 -14 5.60 3.00 -1 3 -14 0.70 2.60 -1 3 -14 -0.60 2.30 -2 3 -14 0.00 2.40 -2 3 -14 0.10 2.60 -3 3 -14 32.80 5.70 -3 3 -14 44.50 6.70 -4 3 -14 4.50 3.20 -4 3 -14 1.10 2.80 2 2 -14 157.48 10.50 1 2 -14 13.10 4.10 0 2 -14 41.30 6.20 -1 2 -14 45.20 6.50 -1 2 -14 41.20 6.20 -2 2 -14 36.10 5.00 -2 2 -14 42.90 6.50 -2 2 -14 40.00 5.90 -3 2 -14 28.20 5.10 -3 2 -14 34.60 5.10 -3 2 -14 23.00 5.20 -4 2 -14 17.30 4.20 -4 2 -14 26.00 5.40 -4 2 -14 18.70 4.30 -5 2 -14 77.79 8.70 -5 2 -14 70.29 7.20 -5 2 -14 80.69 9.50 1 1 -14 7.90 3.50 1 1 -14 2.60 2.70 0 1 -14 0.10 2.50 0 1 -14 1.60 2.20 -1 1 -14 28.80 4.50 -1 1 -14 27.60 5.00 -2 1 -14 4.20 2.60 -2 1 -14 3.40 2.50 -3 1 -14 1.30 2.30 -3 1 -14 1.70 2.70 -4 1 -14 8.30 3.30 -4 1 -14 8.20 3.20 -4 1 -14 3.90 2.80 -5 1 -14 3.50 2.80 -5 1 -14 0.70 2.50 -5 1 -14 -0.60 2.50 -6 1 -14 11.40 4.10 -6 1 -14 13.60 4.10 2 0 -14 22.40 4.10 -2 0 14 26.30 5.00 1 0 -14 95.59 7.10 0 0 -14 16.60 2.40 0 0 -14 18.90 3.70 0 0 -14 13.50 3.80 -1 0 -14 0.00 1.90 -1 0 -14 1.80 2.50 -2 0 -14 15.90 3.60 -2 0 -14 18.80 4.30 -3 0 -14 337.57 15.00 -3 0 -14 325.47 13.20 -4 0 -14 155.98 8.90 -4 0 -14 151.68 10.10 -5 0 -14 249.28 11.80 -5 0 -14 241.28 13.00 -6 0 -14 54.69 6.60 -6 0 -14 61.49 7.90 2 -1 -14 49.70 5.90 -2 1 14 54.09 6.60 1 -1 -14 11.50 3.30 -1 1 14 13.50 4.00 0 -1 -14 60.89 6.30 -1 -1 -14 0.00 2.20 -2 -1 -14 2.30 2.40 -2 -1 -14 7.50 3.10 -3 -1 -14 -0.10 2.30 -3 -1 -14 4.30 2.60 -4 -1 -14 48.10 5.80 -4 -1 -14 44.70 6.40 -5 -1 -14 1.20 2.50 -5 -1 -14 0.10 2.10 -6 -1 -14 -1.30 2.20 -6 -1 -14 -0.10 2.60 -7 -1 -14 2.90 3.10 2 -2 -14 163.18 9.60 -2 2 14 172.08 10.60 1 -2 -14 300.67 12.80 -1 2 14 272.07 13.50 0 -2 -14 39.80 5.20 0 2 14 30.10 5.20 -1 -2 -14 46.30 5.60 -2 -2 -14 126.19 8.00 -3 -2 -14 32.90 5.10 -3 -2 -14 30.70 5.20 -4 -2 -14 38.30 5.40 -4 -2 -14 30.20 5.10 -5 -2 -14 100.39 7.50 -5 -2 -14 79.29 8.10 -6 -2 -14 79.09 7.80 -6 -2 -14 81.49 8.50 -7 -2 -14 34.80 5.60 -7 -2 -14 35.10 6.10 1 -3 -14 -1.60 2.30 -1 3 14 -0.40 2.80 0 -3 -14 31.40 5.00 0 3 14 41.70 6.20 -1 -3 -14 43.70 5.50 1 3 14 62.79 7.40 -2 -3 -14 17.10 3.90 -3 -3 -14 1.10 2.30 -4 -3 -14 -1.20 2.20 -4 -3 -14 4.30 2.90 -5 -3 -14 40.10 5.50 -5 -3 -14 45.00 6.10 -6 -3 -14 11.00 4.00 -6 -3 -14 11.30 3.50 -7 -3 -14 52.29 6.60 -7 -3 -14 57.89 7.40 0 -4 -14 100.89 7.90 0 4 14 122.89 9.10 -1 -4 -14 17.40 4.10 1 4 14 16.60 4.60 -2 -4 -14 1.30 2.50 -3 -4 -14 151.58 9.30 -4 -4 -14 31.70 5.00 -5 -4 -14 143.39 9.10 -5 -4 -14 127.19 9.60 -6 -4 -14 43.20 6.30 -6 -4 -14 39.20 5.70 -7 -4 -14 26.90 5.30 -7 -4 -14 36.80 5.60 -1 -5 -14 17.70 4.40 1 5 14 8.60 4.10 -2 -5 -14 2.20 2.80 -3 -5 -14 3.70 2.90 -4 -5 -14 60.99 6.70 -5 -5 -14 50.99 6.40 -6 -5 -14 1.50 2.70 -3 -6 -14 116.29 8.50 -4 -6 -14 0.70 2.60 -1 1 -15 38.70 5.60 -1 1 -15 37.90 6.40 -2 1 -15 194.68 10.40 -2 1 -15 204.58 12.10 -3 1 -15 5.00 3.30 -3 1 -15 8.40 3.90 0 0 -15 1.10 2.60 -1 0 -15 39.80 6.30 -1 0 -15 25.20 4.60 -2 0 -15 5.20 3.30 -2 0 -15 4.70 3.00 -3 0 -15 22.10 5.10 -3 0 -15 23.70 4.70 -4 0 -15 3.70 3.20 -4 0 -15 13.50 4.10 -1 -1 -15 164.68 9.50 -2 -1 -15 187.68 10.30 -3 -1 -15 170.08 9.80 -3 -1 -15 175.38 11.00 -4 -1 -15 21.20 4.90 -4 -1 -15 16.40 4.20 -1 -2 -15 -0.80 2.40 -2 -2 -15 -1.60 2.20 -3 -2 -15 -1.80 2.50 -4 -2 -15 1.30 3.20 -4 -2 -15 1.00 2.90 -2 -3 -15 9.50 3.60 -3 -3 -15 51.49 6.70 -4 -3 -15 25.30 4.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 28736 _shelx_res_file ; TITL co_complex_a.res in P-1 I.res created by SHELXL-2019/2 at 21:51:03 on 07-Jul-2022 REM Old TITL Co_complex in P-1 REM SHELXT solution in P-1: R1 0.061, Rweak 0.004, Alpha 0.041 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C15 O11 Co CELL 0.71073 9.2008 9.3137 10.647 86.551 79.378 72.369 ZERR 1 0.0004 0.0004 0.0004 0.002 0.002 0.002 LATT 1 SFAC C H Co N O UNIT 26 40 2 4 22 L.S. 20 PLAN 5 SIZE 0.1 0.2 0.1 TEMP 23 CONF list 4 MORE -1 BOND $H fmap 2 acta EQIV $1 x+1, y-1, z HTAB O1 O7_$1 HTAB O1 O4 EQIV $2 x+1, y, z HTAB O2 O5_$2 EQIV $3 -x+1, -y+1, -z+2 HTAB O2 O6_$3 HTAB O9 O4 EQIV $4 -x+1, -y+1, -z+1 HTAB O9 O7_$4 HTAB O10 O7_$2 HTAB O10 O6_$3 EQIV $5 -x+2, -y+1, -z+1 HTAB O11 O8_$5 EQIV $6 x+1, y, z-1 HTAB O11 O5_$6 HTAB N1 O8_$4 EQIV $7 -x+1, -y, -z+2 HTAB N2 O5_$7 sadi o1 h1a o1 h1b o2 h2a o2 h2b o9 h9a o9 h9b o10 h10a o10 h10b o11 h11a sadi n1 h1 n2 h2 sadi h1a h1b h2a h2b h9a h9b h10a h10b h11a h11b WGHT 0.033100 0.493500 FVAR 0.61976 0.57603 CO1 3 1.000000 0.500000 0.500000 10.50000 0.00602 0.00746 = 0.00589 0.00102 -0.00054 -0.00185 CO2 3 1.000000 0.000000 1.000000 10.50000 0.00718 0.00685 = 0.00737 0.00140 -0.00184 -0.00111 O1 5 1.092257 -0.041855 0.806387 11.00000 0.01441 0.01327 = 0.01087 -0.00022 -0.00310 0.00359 H1A 2 1.127899 -0.115820 0.765353 11.00000 -1.50000 H1B 2 1.031932 0.015004 0.769904 11.00000 -1.50000 O2 5 1.068735 0.196765 0.981826 11.00000 0.01548 0.00923 = 0.01931 0.00361 -0.00967 -0.00367 H2A 2 1.106825 0.214662 1.036075 11.00000 -1.50000 H2B 2 1.015264 0.272576 0.959001 11.00000 -1.50000 O3 5 0.785490 0.122963 0.955542 11.00000 0.00997 0.01145 = 0.00876 0.00348 -0.00206 -0.00045 O4 5 0.857741 0.184066 0.752662 11.00000 0.01113 0.01310 = 0.00893 0.00339 0.00063 0.00059 O5 5 0.232195 0.299497 1.153778 11.00000 0.01229 0.00809 = 0.00849 0.00271 -0.00084 -0.00214 O6 5 0.103543 0.534995 1.107934 11.00000 0.01012 0.01028 = 0.01049 0.00212 0.00128 0.00011 O7 5 0.246984 0.692296 0.653944 11.00000 0.00784 0.01100 = 0.00990 0.00186 -0.00295 -0.00130 O8 5 0.499737 0.655132 0.581674 11.00000 0.00906 0.01509 = 0.01160 0.00660 -0.00116 -0.00297 O9 5 0.919674 0.312817 0.530415 11.00000 0.01225 0.01293 = 0.00771 0.00378 -0.00288 -0.00670 H9A 2 0.898054 0.277607 0.597512 11.00000 -1.50000 H9B 2 0.865547 0.302408 0.486172 11.00000 -1.50000 O10 5 1.092036 0.466187 0.671568 11.00000 0.00889 0.01384 = 0.00768 0.00155 -0.00111 -0.00467 H10A 2 1.134414 0.526489 0.679747 11.00000 -1.50000 H10B 2 1.031338 0.468882 0.735496 11.00000 -1.50000 O11 5 1.206060 0.366558 0.401613 11.00000 0.00772 0.01437 = 0.00919 -0.00086 -0.00064 -0.00282 H11A 2 1.289792 0.368423 0.402825 11.00000 -1.50000 H11B 2 1.204820 0.350208 0.328121 11.00000 -1.50000 N1 4 0.504584 0.140602 0.612488 11.00000 0.01469 0.00960 = 0.01115 0.00296 -0.00360 -0.00289 H1 2 0.509682 0.207750 0.546918 11.00000 -1.20000 N2 4 0.575350 -0.039742 0.744576 11.00000 0.01164 0.00958 = 0.01266 0.00313 -0.00170 -0.00120 H2 2 0.635150 -0.120835 0.778520 11.00000 -1.20000 C1 1 0.760582 0.197969 0.854841 11.00000 0.00808 0.00748 = 0.00857 0.00085 -0.00211 -0.00203 C2 1 0.602717 0.310866 0.859158 11.00000 0.00733 0.00665 = 0.00800 0.00041 -0.00205 -0.00159 C3 1 0.571202 0.414526 0.760321 11.00000 0.00822 0.00832 = 0.00789 0.00108 -0.00136 -0.00262 AFIX 43 H3 2 0.647875 0.413232 0.689599 11.00000 -1.20000 AFIX 0 C4 1 0.425463 0.520148 0.766799 11.00000 0.00890 0.00842 = 0.00683 0.00183 -0.00197 -0.00330 C5 1 0.310781 0.522106 0.873130 11.00000 0.00813 0.00821 = 0.00820 0.00047 -0.00182 -0.00218 AFIX 43 H5 2 0.213899 0.593210 0.878284 11.00000 -1.20000 AFIX 0 C6 1 0.340942 0.417849 0.971647 11.00000 0.00843 0.00790 = 0.00658 0.00070 -0.00098 -0.00279 C7 1 0.486642 0.312483 0.964107 11.00000 0.00953 0.00734 = 0.00738 0.00142 -0.00236 -0.00221 AFIX 43 H7 2 0.506641 0.242605 1.029673 11.00000 -1.20000 AFIX 0 C8 1 0.216976 0.419026 1.085545 11.00000 0.00865 0.00936 = 0.00670 0.00046 -0.00275 -0.00390 C9 1 0.388988 0.630542 0.659337 11.00000 0.00986 0.00724 = 0.00767 0.00025 -0.00259 -0.00247 C10 1 0.375951 0.146976 0.705620 11.00000 0.01212 0.01256 = 0.01709 0.00145 -0.00276 -0.00196 AFIX 43 H10 2 0.277987 0.216042 0.710213 11.00000 -1.20000 AFIX 0 C11 1 0.420652 0.033075 0.788633 11.00000 0.01228 0.01358 = 0.01340 0.00169 -0.00002 -0.00296 AFIX 43 H11 2 0.359239 0.008535 0.861228 11.00000 -1.20000 AFIX 0 C12 1 0.624110 0.027052 0.637229 11.00000 0.01402 0.00820 = 0.01127 0.00049 -0.00221 -0.00420 C13 1 0.780390 -0.018112 0.557198 11.00000 0.01480 0.01368 = 0.01680 -0.00148 0.00233 -0.00460 AFIX 137 H13A 2 0.806962 -0.121788 0.533113 21.00000 -1.50000 H13B 2 0.854729 -0.005633 0.604826 21.00000 -1.50000 H13C 2 0.780728 0.043824 0.481802 21.00000 -1.50000 AFIX 137 part 2 H13D 2 0.804580 0.069870 0.519273 -21.00000 -1.50000 H13E 2 0.782325 -0.084695 0.491083 -21.00000 -1.50000 H13F 2 0.855513 -0.068771 0.609385 -21.00000 -1.50000 AFIX 0 HKLF 4 REM co_complex_a.res in P-1 REM wR2 = 0.0693, GooF = S = 1.036, Restrained GooF = 1.032 for all data REM R1 = 0.0263 for 4605 Fo > 4sig(Fo) and 0.0315 for all 5250 data REM 285 parameters refined using 47 restraints END WGHT 0.0331 0.4935 REM Highest difference peak 0.595, deepest hole -0.421, 1-sigma level 0.068 Q1 1 0.4147 0.3657 0.9642 11.00000 0.05 0.60 Q2 1 0.3747 0.5206 0.8207 11.00000 0.05 0.55 Q3 1 0.3331 0.4676 0.9224 11.00000 0.05 0.54 Q4 1 0.4031 0.5771 0.7191 11.00000 0.05 0.53 Q5 1 0.6764 0.2590 0.8556 11.00000 0.05 0.50 ; _shelx_res_checksum 40353 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co Co1 1.000000 0.500000 0.500000 0.00661(6) Uani d 1 . . Co Co2 1.000000 0.000000 1.000000 0.00734(6) Uani d 1 . . O O1 1.09226(11) -0.04186(11) 0.80639(9) 0.01446(19) Uani d 1 . . H H1A 1.128(2) -0.1158(16) 0.7654(16) 0.022 Uiso d 1 . . H H1B 1.0319(19) 0.0150(17) 0.7699(17) 0.022 Uiso d 1 . . O O2 1.06874(11) 0.19677(11) 0.98183(10) 0.01395(18) Uani d 1 . . H H2A 1.107(2) 0.215(2) 1.0361(15) 0.021 Uiso d 1 . . H H2B 1.0153(19) 0.2726(17) 0.9590(17) 0.021 Uiso d 1 . . O O3 0.78549(10) 0.12296(10) 0.95554(8) 0.01077(17) Uani d 1 . . O O4 0.85774(10) 0.18407(10) 0.75266(8) 0.01246(18) Uani d 1 . . O O5 0.23219(10) 0.29950(10) 1.15378(8) 0.01007(16) Uani d 1 . . O O6 0.10354(10) 0.53500(10) 1.10793(8) 0.01151(17) Uani d 1 . . O O7 0.24698(10) 0.69230(10) 0.65394(8) 0.00982(16) Uani d 1 . . O O8 0.49974(10) 0.65513(10) 0.58167(8) 0.01243(18) Uani d 1 . . O O9 0.91967(10) 0.31282(10) 0.53041(9) 0.01031(17) Uani d 1 . . H H9A 0.898(2) 0.278(2) 0.5975(12) 0.015 Uiso d 1 . . H H9B 0.8655(19) 0.302(2) 0.4862(14) 0.015 Uiso d 1 . . O O10 1.09204(10) 0.46619(10) 0.67157(8) 0.00996(16) Uani d 1 . . H H10A 1.1344(18) 0.5265(17) 0.6797(16) 0.015 Uiso d 1 . . H H10B 1.0313(17) 0.4689(19) 0.7355(13) 0.015 Uiso d 1 . . O O11 1.20606(10) 0.36656(11) 0.40161(9) 0.01061(17) Uani d 1 . . H H11A 1.2898(16) 0.368(2) 0.4028(16) 0.016 Uiso d 1 . . H H11B 1.2048(19) 0.350(2) 0.3281(17) 0.016 Uiso d 1 . . N N1 0.50458(13) 0.14060(12) 0.61249(10) 0.0119(2) Uani d 1 . . H H1 0.510(2) 0.2077(18) 0.5469(15) 0.014 Uiso d 1 . . N N2 0.57535(12) -0.03974(12) 0.74458(10) 0.0119(2) Uani d 1 . . H H2 0.6351(19) -0.1208(18) 0.7785(16) 0.014 Uiso d 1 . . C C1 0.76058(13) 0.19797(13) 0.85484(11) 0.0081(2) Uani d 1 . . C C2 0.60272(13) 0.31087(13) 0.85916(11) 0.0074(2) Uani d 1 . . C C3 0.57120(13) 0.41453(13) 0.76032(11) 0.0082(2) Uani d 1 . . H H3 0.647875 0.413232 0.689599 0.010 Uiso calc 1 . . C C4 0.42546(13) 0.52015(13) 0.76680(11) 0.0079(2) Uani d 1 . . C C5 0.31078(13) 0.52211(13) 0.87313(11) 0.0082(2) Uani d 1 . . H H5 0.213899 0.593210 0.878284 0.010 Uiso calc 1 . . C C6 0.34094(13) 0.41785(13) 0.97165(11) 0.0076(2) Uani d 1 . . C C7 0.48664(13) 0.31248(13) 0.96411(11) 0.0081(2) Uani d 1 . . H H7 0.506641 0.242605 1.029673 0.010 Uiso calc 1 . . C C8 0.21698(13) 0.41903(13) 1.08554(11) 0.0078(2) Uani d 1 . . C C9 0.38899(13) 0.63054(13) 0.65934(11) 0.0081(2) Uani d 1 . . C C10 0.37595(15) 0.14698(15) 0.70562(13) 0.0143(2) Uani d 1 . . H H10 0.277987 0.216042 0.710213 0.017 Uiso calc 1 . . C C11 0.42065(15) 0.03308(15) 0.78863(12) 0.0137(2) Uani d 1 . . H H11 0.359239 0.008535 0.861228 0.016 Uiso calc 1 . . C C12 0.62411(14) 0.02705(14) 0.63723(12) 0.0110(2) Uani d 1 . . C C13 0.78039(15) -0.01811(15) 0.55720(13) 0.0156(2) Uani d 1 . . H H13A 0.806962 -0.121788 0.533113 0.023 Uiso calc 0.58(5) . . H H13B 0.854729 -0.005633 0.604826 0.023 Uiso calc 0.58(5) . . H H13C 0.780728 0.043824 0.481802 0.023 Uiso calc 0.58(5) . . H H13D 0.804580 0.069870 0.519273 0.023 Uiso calc 0.42(5) A 2 H H13E 0.782325 -0.084695 0.491083 0.023 Uiso calc 0.42(5) A 2 H H13F 0.855513 -0.068771 0.609385 0.023 Uiso calc 0.42(5) A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.00602(10) 0.00746(11) 0.00589(10) -0.00185(8) -0.00054(7) 0.00102(7) Co2 0.00718(10) 0.00685(11) 0.00737(10) -0.00111(8) -0.00184(7) 0.00140(8) O1 0.0144(4) 0.0133(5) 0.0109(4) 0.0036(4) -0.0031(3) -0.0002(3) O2 0.0155(4) 0.0092(4) 0.0193(5) -0.0037(3) -0.0097(4) 0.0036(3) O3 0.0100(4) 0.0115(4) 0.0088(4) -0.0005(3) -0.0021(3) 0.0035(3) O4 0.0111(4) 0.0131(4) 0.0089(4) 0.0006(3) 0.0006(3) 0.0034(3) O5 0.0123(4) 0.0081(4) 0.0085(4) -0.0021(3) -0.0008(3) 0.0027(3) O6 0.0101(4) 0.0103(4) 0.0105(4) 0.0001(3) 0.0013(3) 0.0021(3) O7 0.0078(4) 0.0110(4) 0.0099(4) -0.0013(3) -0.0029(3) 0.0019(3) O8 0.0091(4) 0.0151(4) 0.0116(4) -0.0030(3) -0.0012(3) 0.0066(3) O9 0.0123(4) 0.0129(4) 0.0077(4) -0.0067(3) -0.0029(3) 0.0038(3) O10 0.0089(4) 0.0138(4) 0.0077(4) -0.0047(3) -0.0011(3) 0.0016(3) O11 0.0077(4) 0.0144(4) 0.0092(4) -0.0028(3) -0.0006(3) -0.0009(3) N1 0.0147(5) 0.0096(5) 0.0111(5) -0.0029(4) -0.0036(4) 0.0030(4) N2 0.0116(5) 0.0096(5) 0.0127(5) -0.0012(4) -0.0017(4) 0.0031(4) C1 0.0081(5) 0.0075(5) 0.0086(5) -0.0020(4) -0.0021(4) 0.0009(4) C2 0.0073(5) 0.0067(5) 0.0080(5) -0.0016(4) -0.0021(4) 0.0004(4) C3 0.0082(5) 0.0083(5) 0.0079(5) -0.0026(4) -0.0014(4) 0.0011(4) C4 0.0089(5) 0.0084(5) 0.0068(5) -0.0033(4) -0.0020(4) 0.0018(4) C5 0.0081(5) 0.0082(5) 0.0082(5) -0.0022(4) -0.0018(4) 0.0005(4) C6 0.0084(5) 0.0079(5) 0.0066(5) -0.0028(4) -0.0010(4) 0.0007(4) C7 0.0095(5) 0.0073(5) 0.0074(5) -0.0022(4) -0.0024(4) 0.0014(4) C8 0.0086(5) 0.0094(5) 0.0067(5) -0.0039(4) -0.0027(4) 0.0005(4) C9 0.0099(5) 0.0072(5) 0.0077(5) -0.0025(4) -0.0026(4) 0.0003(4) C10 0.0121(5) 0.0126(6) 0.0171(6) -0.0020(4) -0.0028(4) 0.0015(5) C11 0.0123(5) 0.0136(6) 0.0134(6) -0.0030(5) 0.0000(4) 0.0017(4) C12 0.0140(5) 0.0082(5) 0.0113(5) -0.0042(4) -0.0022(4) 0.0005(4) C13 0.0148(6) 0.0137(6) 0.0168(6) -0.0046(5) 0.0023(5) -0.0015(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O11 Co1 O11 . 2_766 180.0 ? O11 Co1 O9 . 2_766 90.60(4) ? O11 Co1 O9 2_766 2_766 89.40(4) ? O11 Co1 O9 . . 89.40(4) ? O11 Co1 O9 2_766 . 90.60(4) ? O9 Co1 O9 2_766 . 180.0 ? O11 Co1 O10 . . 90.76(4) ? O11 Co1 O10 2_766 . 89.24(4) ? O9 Co1 O10 2_766 . 86.64(3) ? O9 Co1 O10 . . 93.36(4) ? O11 Co1 O10 . 2_766 89.24(4) ? O11 Co1 O10 2_766 2_766 90.76(4) ? O9 Co1 O10 2_766 2_766 93.36(3) ? O9 Co1 O10 . 2_766 86.64(4) ? O10 Co1 O10 . 2_766 180.0 ? O3 Co2 O3 2_757 . 180.00(5) ? O3 Co2 O1 2_757 2_757 90.97(4) ? O3 Co2 O1 . 2_757 89.03(4) ? O3 Co2 O1 2_757 . 89.03(4) ? O3 Co2 O1 . . 90.97(4) ? O1 Co2 O1 2_757 . 180.0 ? O3 Co2 O2 2_757 2_757 89.79(4) ? O3 Co2 O2 . 2_757 90.21(4) ? O1 Co2 O2 2_757 2_757 88.38(4) ? O1 Co2 O2 . 2_757 91.62(4) ? O3 Co2 O2 2_757 . 90.21(4) ? O3 Co2 O2 . . 89.79(4) ? O1 Co2 O2 2_757 . 91.62(4) ? O1 Co2 O2 . . 88.38(4) ? O2 Co2 O2 2_757 . 180.0 ? Co2 O1 H1A . . 133.6(14) ? Co2 O1 H1B . . 104.8(13) ? H1A O1 H1B . . 107.5(16) ? Co2 O2 H2A . . 117.6(14) ? Co2 O2 H2B . . 121.0(13) ? H2A O2 H2B . . 108.3(16) ? C1 O3 Co2 . . 126.90(8) ? Co1 O9 H9A . . 125.1(13) ? Co1 O9 H9B . . 117.8(13) ? H9A O9 H9B . . 108.5(16) ? Co1 O10 H10A . . 111.8(12) ? Co1 O10 H10B . . 115.7(13) ? H10A O10 H10B . . 106.0(15) ? Co1 O11 H11A . . 128.6(13) ? Co1 O11 H11B . . 114.9(12) ? H11A O11 H11B . . 105.6(16) ? C12 N1 C10 . . 109.77(10) ? C12 N1 H1 . . 124.4(11) ? C10 N1 H1 . . 125.7(11) ? C12 N2 C11 . . 109.55(11) ? C12 N2 H2 . . 123.4(11) ? C11 N2 H2 . . 127.0(11) ? O4 C1 O3 . . 124.51(11) ? O4 C1 C2 . . 118.73(10) ? O3 C1 C2 . . 116.76(10) ? C7 C2 C3 . . 119.40(10) ? C7 C2 C1 . . 119.49(10) ? C3 C2 C1 . . 121.11(10) ? C2 C3 C4 . . 120.45(10) ? C2 C3 H3 . . 119.8 ? C4 C3 H3 . . 119.8 ? C3 C4 C5 . . 119.66(10) ? C3 C4 C9 . . 120.93(10) ? C5 C4 C9 . . 119.40(10) ? C6 C5 C4 . . 120.20(11) ? C6 C5 H5 . . 119.9 ? C4 C5 H5 . . 119.9 ? C7 C6 C5 . . 119.71(10) ? C7 C6 C8 . . 120.09(10) ? C5 C6 C8 . . 120.19(10) ? C6 C7 C2 . . 120.56(10) ? C6 C7 H7 . . 119.7 ? C2 C7 H7 . . 119.7 ? O6 C8 O5 . . 123.36(11) ? O6 C8 C6 . . 118.94(10) ? O5 C8 C6 . . 117.70(10) ? O8 C9 O7 . . 124.60(11) ? O8 C9 C4 . . 118.45(10) ? O7 C9 C4 . . 116.95(10) ? C11 C10 N1 . . 106.62(11) ? C11 C10 H10 . . 126.7 ? N1 C10 H10 . . 126.7 ? C10 C11 N2 . . 106.72(11) ? C10 C11 H11 . . 126.6 ? N2 C11 H11 . . 126.6 ? N1 C12 N2 . . 107.33(11) ? N1 C12 C13 . . 125.58(11) ? N2 C12 C13 . . 127.07(11) ? C12 C13 H13A . . 109.5 ? C12 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C12 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C12 C13 H13D . . 109.5 ? H13A C13 H13D . . 135.3 ? H13B C13 H13D . . 76.7 ? H13C C13 H13D . . 35.5 ? C12 C13 H13E . . 109.5 ? H13A C13 H13E . . 35.5 ? H13B C13 H13E . . 135.3 ? H13C C13 H13E . . 76.7 ? H13D C13 H13E . . 109.5 ? C12 C13 H13F . . 109.5 ? H13A C13 H13F . . 76.7 ? H13B C13 H13F . . 35.5 ? H13C C13 H13F . . 135.3 ? H13D C13 H13F . . 109.5 ? H13E C13 H13F . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 O11 . 2.0576(9) ? Co1 O11 2_766 2.0576(9) ? Co1 O9 2_766 2.0772(9) ? Co1 O9 . 2.0772(9) ? Co1 O10 . 2.1196(9) ? Co1 O10 2_766 2.1196(9) ? Co2 O3 2_757 2.0835(9) ? Co2 O3 . 2.0835(9) ? Co2 O1 2_757 2.0912(9) ? Co2 O1 . 2.0912(9) ? Co2 O2 2_757 2.1000(9) ? Co2 O2 . 2.1000(9) ? O1 H1A . 0.787(12) ? O1 H1B . 0.785(12) ? O2 H2A . 0.778(12) ? O2 H2B . 0.783(12) ? O3 C1 . 1.2624(14) ? O4 C1 . 1.2601(14) ? O5 C8 . 1.2777(14) ? O6 C8 . 1.2526(15) ? O7 C9 . 1.2687(14) ? O8 C9 . 1.2580(14) ? O9 H9A . 0.785(12) ? O9 H9B . 0.775(12) ? O10 H10A . 0.791(12) ? O10 H10B . 0.793(12) ? O11 H11A . 0.778(12) ? O11 H11B . 0.809(17) ? N1 C12 . 1.3289(16) ? N1 C10 . 1.3854(16) ? N1 H1 . 0.913(15) ? N2 C12 . 1.3375(15) ? N2 C11 . 1.3832(16) ? N2 H2 . 0.890(15) ? C1 C2 . 1.5078(16) ? C2 C7 . 1.3934(15) ? C2 C3 . 1.3944(16) ? C3 C4 . 1.3948(16) ? C3 H3 . 0.9300 ? C4 C5 . 1.3949(15) ? C4 C9 . 1.5066(16) ? C5 C6 . 1.3934(15) ? C5 H5 . 0.9300 ? C6 C7 . 1.3926(16) ? C6 C8 . 1.5019(15) ? C7 H7 . 0.9300 ? C10 C11 . 1.3537(17) ? C10 H10 . 0.9300 ? C11 H11 . 0.9300 ? C12 C13 . 1.4818(17) ? C13 H13A . 0.9600 ? C13 H13B . 0.9600 ? C13 H13C . 0.9600 ? C13 H13D . 0.9600 ? C13 H13E . 0.9600 ? C13 H13F . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 H1A O7 1_645 0.787(12) 2.096(12) 2.8789(13) 173.5(19) yes O1 H1B O4 . 0.785(12) 1.904(13) 2.6401(13) 155.8(18) yes O2 H2A O5 1_655 0.778(12) 2.175(13) 2.9371(13) 166.5(19) yes O2 H2B O6 2_667 0.783(12) 1.965(12) 2.7458(13) 175(2) yes O9 H9A O4 . 0.785(12) 1.850(12) 2.6339(12) 176.4(19) yes O9 H9B O7 2_666 0.775(12) 1.957(12) 2.7150(13) 165.9(18) yes O10 H10A O7 1_655 0.791(12) 2.085(12) 2.8592(13) 166.1(17) yes O10 H10B O6 2_667 0.793(12) 1.891(12) 2.6835(12) 176.3(18) yes O11 H11A O8 2_766 0.778(12) 1.919(13) 2.6911(13) 171.6(18) yes O11 H11B O5 1_654 0.809(17) 1.896(18) 2.6989(13) 172.0(17) yes N1 H1 O8 2_666 0.913(15) 1.811(15) 2.7214(13) 174.6(16) yes N2 H2 O5 2_657 0.890(15) 1.931(15) 2.8206(14) 178.0(17) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Co2 O3 C1 O4 . . . . 16.76(18) ? Co2 O3 C1 C2 . . . . -163.49(8) ? O4 C1 C2 C7 . . . . 170.61(11) ? O3 C1 C2 C7 . . . . -9.15(17) ? O4 C1 C2 C3 . . . . -9.89(17) ? O3 C1 C2 C3 . . . . 170.35(11) ? C7 C2 C3 C4 . . . . 0.72(18) ? C1 C2 C3 C4 . . . . -178.78(11) ? C2 C3 C4 C5 . . . . 0.16(18) ? C2 C3 C4 C9 . . . . -178.68(11) ? C3 C4 C5 C6 . . . . -0.83(18) ? C9 C4 C5 C6 . . . . 178.03(11) ? C4 C5 C6 C7 . . . . 0.61(18) ? C4 C5 C6 C8 . . . . -179.42(11) ? C5 C6 C7 C2 . . . . 0.29(18) ? C8 C6 C7 C2 . . . . -179.69(11) ? C3 C2 C7 C6 . . . . -0.95(18) ? C1 C2 C7 C6 . . . . 178.56(11) ? C7 C6 C8 O6 . . . . 161.30(11) ? C5 C6 C8 O6 . . . . -18.68(17) ? C7 C6 C8 O5 . . . . -19.76(17) ? C5 C6 C8 O5 . . . . 160.27(11) ? C3 C4 C9 O8 . . . . -19.45(17) ? C5 C4 C9 O8 . . . . 161.70(11) ? C3 C4 C9 O7 . . . . 160.47(11) ? C5 C4 C9 O7 . . . . -18.38(17) ? C12 N1 C10 C11 . . . . -0.03(15) ? N1 C10 C11 N2 . . . . 0.19(15) ? C12 N2 C11 C10 . . . . -0.29(15) ? C10 N1 C12 N2 . . . . -0.15(15) ? C10 N1 C12 C13 . . . . 178.19(12) ? C11 N2 C12 N1 . . . . 0.27(15) ? C11 N2 C12 C13 . . . . -178.04(13) ? _cod_database_fobs_code 2244125