#------------------------------------------------------------------------------ #$Date: 2022-07-30 02:57:23 +0100 (Sat, 30 Jul 2022) $ #$Revision: 277012 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/41/2244139.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244139 loop_ _publ_author_name 'Mohamed, Shaaban K.' 'Mague, Joel T.' 'Akkurt, Mehmet' 'Abdel-Rahman, Laila H.' 'Abdel-Hameed, Mohamed' 'Albayati, Mustafa R.' 'Al-Taif, Elham A.' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of (+-)-N'-(2-hydroxy-3-methoxybenzylidene)-2-(4-isobutylphenyl)propionohydrazide ; _journal_coeditor_code TX2052 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 860 _journal_page_last 863 _journal_paper_doi 10.1107/S2056989022007605 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac 'C21 H26 N2 O3' _chemical_formula_moiety 'C21 H26 N2 O3' _chemical_formula_sum 'C21 H26 N2 O3' _chemical_formula_weight 354.44 _chemical_name_systematic (+-)-N'-(2-Hydroxy-3-methoxybenzylidene)-2-(4-isobutylphenyl)propionohydrazide _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 97.042(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.5241(7) _cell_length_b 10.0718(5) _cell_length_c 13.2710(7) _cell_measurement_reflns_used 9778 _cell_measurement_temperature 125(2) _cell_measurement_theta_max 72.4317 _cell_measurement_theta_min 5.5295 _cell_volume 1926.69(17) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 125(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device 'Bruker D8 VENTURE PHOTON 3 CPAD' _diffrn_measurement_device_type 'Bruker D8 VENTURE PHOTON 3 CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0354 _diffrn_reflns_av_unetI/netI 0.0167 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 38584 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 72.425 _diffrn_reflns_theta_min 5.529 _diffrn_source 'INCOATEC I\mS micro----focus source' _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.657 _exptl_absorpt_correction_T_max 0.98 _exptl_absorpt_correction_T_min 0.90 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.222 _exptl_crystal_description plate _exptl_crystal_F_000 760 _exptl_crystal_size_max 0.204 _exptl_crystal_size_mid 0.201 _exptl_crystal_size_min 0.031 _refine_diff_density_max 0.400 _refine_diff_density_min -0.214 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 259 _refine_ls_number_reflns 3758 _refine_ls_number_restraints 8 _refine_ls_restrained_S_all 1.069 _refine_ls_R_factor_all 0.0443 _refine_ls_R_factor_gt 0.0405 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0517P)^2^+0.6940P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1056 _refine_ls_wR_factor_ref 0.1091 _reflns_number_gt 3400 _reflns_number_total 3758 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file tx2052sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2244139 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.878 _shelx_estimated_absorpt_t_max 0.980 _shelx_hkl_file ; 0 0 1 -0.10 0.40 0 0 2 201.18 7.20 0 0 3 0.10 1.30 0 0 3 0.40 1.10 0 0 4 3127.29 89.69 0 0 4 3076.99 89.59 0 0 5 -0.30 1.50 0 0 6 6314.87 180.68 0 0 -6 6304.37 180.58 0 0 -7 -2.70 1.70 0 0 7 1.60 2.20 0 0 -7 1.10 1.00 0 0 7 -0.30 1.10 0 0 8 1.90 2.50 0 0 -8 0.20 2.40 0 0 -8 0.70 1.30 0 0 8 2.10 1.50 0 0 -9 3.20 3.50 0 0 9 -0.70 1.30 0 0 9 2.30 3.00 0 0 9 0.40 2.60 0 0 -9 0.70 1.60 0 0 9 3.50 3.10 0 0 10 21.60 4.70 0 0 10 23.30 4.80 0 0 10 17.50 4.20 0 0 10 23.40 4.60 0 0 -10 16.20 7.30 0 0 10 20.20 5.00 0 0 10 27.60 4.70 0 0 10 32.70 6.80 0 0 11 5.20 3.20 0 0 11 -0.80 2.40 0 0 11 -0.30 2.50 0 0 11 0.30 2.70 0 0 11 0.10 3.40 0 0 11 1.60 3.20 0 0 11 -1.70 3.20 0 0 -11 -1.60 2.10 0 0 12 764.92 27.50 0 0 12 783.32 28.10 0 0 12 772.52 28.20 0 0 12 777.02 28.70 0 0 12 771.52 27.90 0 0 12 745.03 32.80 0 0 13 -3.20 4.80 0 0 13 4.30 3.30 0 0 13 -2.00 2.70 0 0 13 -0.90 2.30 0 0 14 1294.07 41.20 0 0 14 1258.17 40.60 0 0 14 1263.97 40.70 0 0 14 1278.87 41.00 0 0 15 2.40 2.00 0 0 15 -2.50 2.10 0 0 15 1.00 1.80 0 0 16 311.77 12.70 0 1 0 1.40 0.60 0 1 0 0.60 0.60 0 -1 0 0.00 0.50 0 1 -1 1264.77 36.20 0 1 -1 1257.37 36.30 0 1 -1 1232.08 36.40 0 1 1 1280.47 37.10 0 -1 1 1305.97 36.40 0 1 -2 146.59 5.10 0 1 -2 166.48 6.30 0 -1 2 127.09 6.40 0 -1 2 146.39 4.70 0 -1 2 151.88 5.40 0 1 -3 790.02 23.70 0 1 -3 819.42 23.70 0 1 3 801.02 26.20 0 -1 3 853.11 24.10 0 -1 3 841.12 24.20 0 -1 3 792.42 25.70 0 1 -4 5069.69 139.79 0 1 4 4848.11 141.79 0 -1 4 4923.11 142.69 0 -1 4 5132.19 140.39 0 1 -5 16.50 1.80 0 1 5 14.60 1.50 0 1 -5 12.60 1.60 0 1 5 16.70 3.00 0 1 -5 14.80 2.50 0 -1 5 12.70 1.80 0 -1 5 15.00 3.30 0 1 -6 3101.59 90.89 0 1 6 3180.48 95.39 0 1 -6 3209.08 92.79 0 1 6 3301.97 90.89 0 -1 6 3110.59 94.69 0 -1 6 3205.28 91.49 0 -1 -6 3260.57 90.29 0 -1 -6 3209.98 95.59 0 1 7 269.97 12.70 0 1 -7 263.57 10.10 0 1 7 280.27 10.10 0 1 -7 264.47 11.60 0 -1 -7 264.87 13.60 0 -1 7 271.67 10.60 0 -1 7 269.87 13.30 0 -1 -7 274.27 9.60 0 1 8 564.24 21.30 0 1 -8 584.54 21.90 0 1 8 623.54 20.40 0 1 -8 597.54 20.50 0 1 8 638.84 24.00 0 -1 -8 624.64 25.20 0 -1 8 632.24 21.10 0 -1 8 653.33 32.70 0 -1 -8 630.14 19.90 0 1 9 89.89 7.80 0 1 9 85.79 6.90 0 1 9 92.79 6.80 0 1 9 88.49 5.70 0 1 9 88.39 7.10 0 1 9 80.49 7.00 0 1 -9 84.69 5.70 0 -1 -9 82.59 5.30 0 -1 9 74.79 6.70 0 -1 -9 85.59 8.70 0 -1 9 83.39 8.30 0 -1 9 88.59 8.30 0 -1 9 83.99 7.10 0 -1 9 89.09 7.00 0 -1 9 88.39 6.00 0 1 10 999.00 33.90 0 1 10 950.20 33.90 0 1 10 977.50 34.30 0 1 10 1001.70 32.80 0 1 -10 1049.20 33.20 0 1 10 926.01 33.40 0 1 10 1130.49 34.80 0 1 10 956.00 33.90 0 1 10 1017.60 34.70 0 1 10 951.90 36.60 0 -1 10 993.20 34.40 0 -1 10 982.40 34.10 0 -1 10 1051.59 33.60 0 -1 10 983.40 34.70 0 -1 10 976.30 33.90 0 -1 -10 1029.10 38.80 0 -1 -10 1012.50 32.60 0 -1 10 956.60 34.00 0 -1 10 1038.30 38.10 0 1 11 1069.39 36.30 0 1 11 1133.19 38.40 0 1 -11 1231.68 37.80 0 1 11 1144.99 41.40 0 1 11 1115.59 39.00 0 1 11 1085.49 44.30 0 1 11 1067.59 36.90 0 1 11 1093.79 36.90 0 1 11 1142.79 39.60 0 -1 11 1096.19 38.00 0 -1 -11 1129.39 36.90 0 -1 11 1149.58 39.30 0 -1 11 1148.09 42.80 0 -1 -11 1195.98 45.10 0 -1 11 1076.09 45.10 0 -1 11 1172.98 37.70 0 -1 11 1149.58 38.30 0 1 12 1165.38 38.90 0 1 12 1112.59 38.60 0 1 12 1173.68 39.30 0 1 12 1125.49 39.00 0 -1 12 1146.79 38.70 0 -1 12 1210.28 39.90 0 -1 12 1120.99 39.50 0 -1 12 1187.98 39.00 0 -1 12 1161.78 39.10 0 -1 12 1145.09 38.70 0 1 13 157.18 9.70 0 1 13 150.48 9.50 0 1 13 154.18 9.30 0 1 13 144.09 9.70 0 1 13 153.38 12.80 0 -1 13 158.28 12.70 0 -1 13 146.99 9.30 0 -1 13 154.68 9.40 0 -1 13 161.98 10.20 0 -1 13 174.88 11.50 0 -1 13 150.08 9.30 0 1 14 5.20 2.50 0 1 14 4.20 2.50 0 1 14 4.10 2.40 0 1 14 9.60 3.30 0 -1 14 5.60 2.60 0 -1 14 6.10 2.70 0 -1 14 7.80 2.70 0 -1 14 8.30 3.00 0 -1 14 8.60 2.90 0 1 15 5.10 2.10 0 1 15 3.80 2.30 0 1 15 -0.60 1.90 0 1 15 5.50 2.80 0 -1 15 3.90 2.70 0 -1 15 5.40 2.00 0 -1 15 2.90 2.10 0 -1 15 0.80 1.90 0 -1 15 3.30 2.30 0 -1 16 68.99 4.30 0 -1 16 60.69 6.20 0 2 0 1684.83 49.50 0 -2 0 1705.43 49.10 0 -2 0 1690.53 49.10 0 2 3 18.70 2.10 0 2 3 18.60 3.40 0 2 -3 19.10 2.20 0 2 -3 19.80 2.50 0 -2 3 21.40 3.00 0 -2 -3 17.10 1.90 0 -2 3 19.80 2.30 0 -2 4 5123.69 146.79 0 2 5 209.78 8.60 0 2 -5 221.28 8.70 0 2 5 214.08 9.40 0 -2 5 220.78 9.10 0 -2 -5 209.68 8.20 0 -2 5 238.08 10.90 0 2 6 974.40 31.70 0 2 -6 908.61 28.10 0 2 6 1007.60 30.50 0 2 -6 983.00 30.40 0 -2 6 1022.00 31.10 0 -2 6 935.71 33.20 0 -2 -6 963.60 29.60 0 -2 -6 982.00 34.50 0 2 -7 531.45 18.10 0 2 7 476.25 18.40 0 2 7 499.25 19.50 0 2 7 524.95 18.00 0 -2 -7 501.65 22.00 0 -2 -7 515.45 17.30 0 -2 7 526.85 18.60 0 -2 7 497.55 20.90 0 2 -8 43.80 4.20 0 2 8 34.80 4.60 0 2 8 36.90 3.80 0 2 8 47.40 5.50 0 -2 8 37.50 4.20 0 -2 8 34.00 4.70 0 -2 8 36.80 6.40 0 -2 -8 42.50 6.30 0 -2 -8 36.40 3.80 0 2 9 1941.21 59.59 0 2 9 1972.40 59.29 0 2 -9 2057.39 59.39 0 2 9 1886.51 59.89 0 2 9 1913.41 61.59 0 2 9 1950.90 61.59 0 2 9 1821.02 58.29 0 2 9 1844.62 59.89 0 -2 -9 2088.69 65.89 0 -2 9 1863.61 59.49 0 -2 9 1955.10 59.69 0 -2 9 1951.20 63.69 0 -2 9 1851.01 57.89 0 -2 9 1891.11 64.09 0 -2 -9 2013.90 58.29 0 -2 9 1855.71 60.79 0 2 10 1215.98 42.80 0 2 10 1178.18 40.50 0 2 10 1210.18 40.70 0 2 -10 1270.57 40.30 0 2 10 1311.27 40.30 0 2 10 1225.48 40.40 0 2 10 1169.28 40.40 0 2 10 1239.98 39.70 0 2 10 1180.08 40.90 0 -2 10 1197.28 40.80 0 -2 10 1225.88 40.60 0 -2 10 1239.48 45.20 0 -2 -10 1213.58 39.40 0 -2 10 1261.27 41.80 0 -2 10 1254.47 41.30 0 -2 10 1238.68 40.90 0 -2 10 1232.08 40.60 0 2 11 598.94 23.20 0 2 11 564.34 21.50 0 2 11 567.64 22.20 0 2 11 580.44 22.10 0 2 11 541.35 24.40 0 2 -11 587.74 22.40 0 2 11 586.24 22.70 0 -2 11 597.14 23.00 0 -2 11 577.24 22.40 0 -2 11 596.04 23.10 0 -2 -11 553.54 21.60 0 -2 11 589.14 22.80 0 -2 11 617.34 27.20 0 -2 11 604.34 23.70 0 -2 11 501.05 28.10 0 -2 -11 551.24 28.10 0 2 12 22.60 4.70 0 2 12 26.70 5.40 0 2 12 28.40 5.10 0 2 12 20.10 4.70 0 2 -12 19.80 4.50 0 2 12 22.70 4.60 0 2 12 23.50 4.50 0 2 12 19.20 4.50 0 -2 12 27.50 5.30 0 -2 12 27.20 5.00 0 -2 12 30.00 5.10 0 -2 12 24.40 4.70 0 -2 12 20.60 5.10 0 -2 12 19.40 4.30 0 -2 -12 22.30 5.00 0 -2 12 39.30 7.90 0 2 13 373.16 15.50 0 2 13 347.07 15.50 0 2 13 349.37 15.20 0 2 13 337.87 14.90 0 -2 13 351.16 15.10 0 -2 13 312.97 18.70 0 -2 13 349.77 15.30 0 -2 13 335.87 15.70 0 -2 13 353.06 15.50 0 -2 13 333.07 14.50 0 2 14 167.98 8.80 0 2 14 130.79 8.30 0 2 14 176.08 9.20 0 2 14 157.88 8.60 0 -2 14 163.68 9.40 0 -2 14 145.09 8.20 0 -2 14 153.78 8.60 0 -2 14 152.28 8.70 0 -2 14 143.29 8.50 0 2 15 19.60 3.10 0 2 15 29.50 3.50 0 2 15 21.80 3.70 0 -2 15 26.40 3.70 0 -2 15 23.20 3.70 0 -2 15 18.00 2.90 0 -2 16 66.69 4.40 0 3 0 3.70 1.50 0 -3 0 -0.50 1.10 0 -3 0 0.30 1.40 0 -3 0 0.10 1.20 0 3 -1 105.39 5.90 0 3 1 101.99 5.80 0 -3 -1 108.09 5.50 0 -3 1 97.19 5.20 0 -3 1 104.09 5.40 0 -3 -1 95.09 5.80 0 -3 1 101.99 4.70 0 3 2 175.38 8.20 0 3 -2 189.18 8.70 0 3 -2 175.68 7.60 0 -3 2 176.48 6.00 0 -3 -2 180.58 7.80 0 -3 2 174.68 7.60 0 -3 2 175.88 8.10 0 -3 2 177.88 8.30 0 3 3 833.92 27.30 0 3 -3 856.11 26.80 0 -3 3 839.72 27.50 0 -3 3 844.12 27.80 0 -3 -3 845.62 26.70 0 3 4 217.08 9.60 0 3 4 216.08 8.80 0 3 -4 224.28 9.30 0 -3 -4 214.28 9.00 0 -3 4 222.78 10.40 0 -3 4 201.08 9.70 0 3 5 76.39 5.00 0 3 -5 71.29 4.80 0 3 5 65.49 4.90 0 -3 -5 59.39 4.40 0 -3 5 77.59 5.50 0 -3 5 75.39 6.10 0 -3 -5 72.89 6.70 0 3 6 304.27 13.00 0 3 6 324.77 13.30 0 3 -6 313.57 12.90 0 3 6 309.67 12.90 0 -3 6 326.17 13.70 0 -3 -6 317.67 12.60 0 -3 -6 329.07 16.30 0 -3 6 326.47 15.00 0 3 7 49.10 5.30 0 3 7 52.69 4.80 0 3 -7 53.29 4.70 0 3 7 51.79 4.80 0 -3 -7 50.19 4.30 0 -3 7 57.69 5.80 0 -3 -7 39.50 6.30 0 -3 7 54.39 5.10 0 -3 7 48.90 5.70 0 3 8 1232.88 38.90 0 3 -8 1271.37 39.30 0 3 8 1208.58 39.10 0 3 8 1170.78 39.20 0 3 8 1204.78 39.50 0 3 8 1136.49 39.30 0 -3 8 1209.78 40.10 0 -3 8 1196.28 39.90 0 -3 8 1127.69 42.00 0 -3 -8 1172.48 44.20 0 -3 8 1161.88 39.30 0 -3 8 1152.28 39.00 0 -3 -8 1180.88 38.20 0 -3 8 1236.68 38.00 0 3 9 1489.35 53.19 0 3 9 1711.93 53.89 0 3 9 1704.13 53.39 0 3 9 1693.53 53.89 0 3 9 1756.42 53.09 0 3 9 1603.54 53.09 0 3 9 1616.34 53.99 0 3 9 1765.52 53.19 0 -3 -9 1814.82 56.99 0 -3 -9 1705.43 59.79 0 -3 9 1690.23 52.19 0 -3 9 1608.94 57.19 0 -3 9 1715.13 53.49 0 -3 9 1596.94 52.69 0 -3 9 1650.33 51.79 0 -3 9 1693.53 54.29 0 -3 9 1747.23 53.29 0 -3 9 1738.33 53.99 0 3 10 2.30 7.90 0 3 10 8.00 3.50 0 3 10 2.30 3.50 0 3 10 0.10 3.10 0 3 10 2.40 2.90 0 3 10 -0.70 4.50 0 3 10 -0.60 4.10 0 3 -10 1.80 2.50 0 3 10 0.20 2.30 0 3 10 5.40 3.10 0 -3 10 2.00 3.10 0 -3 -10 2.30 2.60 0 -3 10 0.20 2.50 0 -3 10 1.40 3.60 0 -3 10 11.30 3.70 0 -3 10 3.50 3.50 0 -3 10 4.90 4.20 0 -3 10 2.40 2.80 0 -3 10 7.30 3.50 0 -3 10 0.60 3.20 0 3 11 532.85 20.90 0 3 -11 540.95 21.70 0 3 11 547.25 21.50 0 3 11 550.44 24.90 0 3 11 553.24 21.90 0 3 11 521.95 21.20 0 3 11 557.04 21.20 0 -3 -11 507.45 27.50 0 -3 11 547.35 22.30 0 -3 11 540.45 21.70 0 -3 11 514.55 22.30 0 -3 11 498.35 20.60 0 -3 -11 537.55 21.10 0 -3 11 538.75 21.60 0 -3 11 498.95 25.20 0 -3 11 533.55 21.20 0 -3 11 523.15 19.90 0 3 12 309.07 14.00 0 3 12 299.87 14.50 0 3 12 322.27 14.60 0 3 12 293.57 13.90 0 3 12 286.67 13.50 0 -3 12 337.47 24.90 0 -3 12 307.27 15.10 0 -3 12 293.87 14.50 0 -3 12 288.97 13.80 0 -3 12 301.37 14.40 0 -3 12 291.77 13.80 0 3 13 8.40 3.00 0 3 13 7.10 3.00 0 3 13 13.10 3.70 0 3 13 3.80 3.00 0 3 13 10.50 3.20 0 -3 13 -0.40 4.30 0 -3 13 6.30 2.90 0 -3 13 3.80 3.00 0 -3 13 8.50 2.90 0 -3 13 15.30 3.80 0 -3 13 5.20 2.80 0 3 14 87.79 6.50 0 3 14 86.99 6.20 0 3 14 90.49 6.20 0 -3 14 85.99 6.50 0 -3 14 87.09 6.20 0 -3 14 89.69 6.90 0 3 15 3.70 2.30 0 3 15 4.10 1.70 0 3 15 4.20 2.80 0 -3 15 4.10 2.00 0 -3 15 4.70 2.50 0 -3 15 4.30 2.10 0 -3 15 1.00 1.70 0 4 0 1084.19 35.60 0 4 0 1086.49 33.40 0 -4 0 1075.89 34.30 0 -4 0 1123.49 34.70 0 4 1 240.78 11.00 0 4 -1 229.68 11.30 0 4 1 224.28 9.10 0 -4 -1 236.28 10.30 0 -4 1 230.48 9.30 0 -4 1 224.88 9.70 0 -4 1 228.58 10.10 0 -4 -1 230.58 10.70 0 4 -2 129.49 7.70 0 4 2 135.89 6.10 0 4 2 134.29 7.80 0 -4 -2 129.69 7.10 0 -4 2 134.69 7.30 0 -4 2 130.79 5.50 0 -4 2 127.39 7.00 0 4 -3 2262.67 67.39 0 4 3 2110.79 65.19 0 4 3 2290.67 68.59 0 -4 -3 2208.48 67.39 0 -4 -3 2375.36 70.09 0 -4 3 2332.87 68.39 0 4 -4 586.04 20.10 0 4 4 571.74 21.00 0 4 4 500.85 18.00 0 -4 4 572.64 21.30 0 -4 -4 534.25 19.80 0 -4 -4 549.95 22.50 0 -4 4 560.34 21.20 0 4 5 3753.82 107.89 0 4 -5 3834.62 108.69 0 4 5 3742.43 109.59 0 4 5 3636.64 106.49 0 -4 5 3785.62 109.99 0 -4 -5 3634.34 108.29 0 -4 -5 3668.33 112.49 0 -4 5 3729.63 110.39 0 -4 5 3606.74 107.19 0 4 6 17.90 3.70 0 4 6 17.80 3.90 0 4 6 17.90 3.70 0 4 -6 14.50 3.30 0 -4 6 22.00 5.50 0 -4 -6 18.50 5.30 0 -4 6 22.80 4.10 0 -4 -6 16.60 3.40 0 -4 6 24.70 4.70 0 4 -7 10.20 3.10 0 4 7 8.30 3.00 0 4 7 7.90 3.00 0 -4 7 7.40 2.90 0 -4 7 9.40 3.00 0 -4 -7 4.20 2.20 0 -4 7 2.00 2.40 0 -4 -7 8.00 4.40 0 4 8 237.98 12.20 0 4 8 243.28 12.70 0 4 -8 259.27 13.00 0 4 8 236.58 13.00 0 4 8 232.28 12.30 0 4 8 242.98 12.10 0 4 8 249.88 12.90 0 4 8 239.88 12.80 0 -4 8 247.98 12.60 0 -4 8 248.08 17.90 0 -4 8 255.47 12.20 0 -4 -8 265.37 12.70 0 -4 8 238.98 12.50 0 -4 8 250.77 13.00 0 -4 8 251.97 11.60 0 -4 8 243.88 13.50 0 -4 -8 221.78 15.80 0 -4 8 239.78 14.60 0 4 9 821.52 30.60 0 4 9 828.92 29.80 0 4 9 861.31 29.70 0 4 9 813.62 29.90 0 4 9 813.42 29.10 0 4 9 804.42 29.80 0 4 9 760.62 29.20 0 4 -9 938.31 31.80 0 -4 9 833.32 33.80 0 -4 9 853.91 28.50 0 -4 9 861.81 32.10 0 -4 9 785.52 28.40 0 -4 -9 838.62 36.20 0 -4 -9 809.82 29.90 0 -4 9 828.72 30.30 0 -4 9 826.82 29.70 0 -4 9 834.92 29.40 0 -4 9 821.82 30.00 0 -4 9 749.92 28.60 0 4 10 64.69 7.00 0 4 10 63.39 6.80 0 4 10 63.69 7.00 0 4 10 65.79 6.40 0 4 10 62.89 7.00 0 4 -10 63.29 6.90 0 4 10 59.89 6.40 0 -4 10 63.59 6.90 0 -4 10 58.19 6.40 0 -4 10 65.29 6.30 0 -4 -10 67.99 6.80 0 -4 10 62.49 7.10 0 -4 10 66.59 8.20 0 -4 10 57.19 8.00 0 -4 -10 42.50 8.40 0 -4 10 66.69 6.90 0 4 -11 36.70 6.20 0 4 11 41.10 5.50 0 4 11 32.50 6.20 0 4 11 32.70 5.40 0 4 11 34.70 5.50 0 4 11 35.00 5.20 0 4 11 32.80 5.50 0 4 11 30.70 5.30 0 -4 11 30.30 5.10 0 -4 11 39.50 5.50 0 -4 11 33.80 5.30 0 -4 11 31.40 5.50 0 -4 11 28.40 5.00 0 -4 -11 30.20 8.30 0 -4 11 40.60 5.80 0 -4 11 35.90 7.80 0 -4 11 31.50 5.60 0 -4 -11 22.30 5.00 0 4 12 23.00 4.30 0 4 12 20.90 4.40 0 4 12 25.60 4.40 0 4 12 25.10 4.90 0 -4 12 16.70 4.00 0 -4 12 20.10 4.10 0 -4 12 22.20 6.10 0 4 13 226.28 10.80 0 4 13 230.58 10.80 0 4 13 224.68 10.80 0 4 13 243.78 11.50 0 4 13 243.08 11.80 0 -4 13 238.68 11.50 0 -4 13 233.18 11.60 0 -4 13 217.18 11.80 0 -4 13 218.38 11.00 0 -4 13 195.38 14.40 0 4 14 14.70 2.90 0 4 14 13.10 3.80 0 4 14 15.40 2.80 0 -4 14 18.90 5.00 0 -4 14 10.00 2.80 0 -4 14 17.10 3.20 0 -4 14 13.10 3.10 0 4 15 72.49 4.40 0 4 15 60.69 5.80 0 -4 15 71.99 4.90 0 -4 15 64.89 5.20 0 -4 15 66.79 5.10 0 5 0 -1.40 1.70 0 5 0 -0.90 1.70 0 -5 0 0.50 2.10 0 -5 0 1.40 1.80 0 5 -1 2.50 2.40 0 5 1 2.30 2.10 0 5 1 -0.70 1.70 0 -5 -1 1.70 2.20 0 -5 1 -2.30 2.00 0 -5 -1 4.60 2.70 0 -5 1 -2.80 1.70 0 5 -2 640.84 24.70 0 5 2 682.93 25.30 0 5 2 655.13 21.70 0 -5 -2 663.53 25.10 0 -5 -2 676.13 24.00 0 -5 2 660.43 23.50 0 -5 2 660.63 23.50 0 -5 2 625.74 23.40 0 5 3 1530.35 50.99 0 5 3 1573.84 48.10 0 -5 -3 1625.94 52.19 0 -5 3 1593.34 49.90 0 -5 3 1509.25 47.80 0 -5 -3 1596.04 49.90 0 5 4 1238.88 42.90 0 5 4 1273.07 40.30 0 -5 4 1307.77 42.70 0 -5 -4 1289.87 41.90 0 -5 -4 1240.98 44.40 0 -5 4 1278.27 40.00 0 5 5 28.20 4.70 0 5 5 24.90 4.10 0 -5 5 40.10 9.90 0 -5 -5 28.30 7.20 0 -5 5 31.80 4.60 0 -5 -5 28.50 5.40 0 5 6 281.97 13.80 0 5 6 283.17 13.80 0 5 6 282.87 13.50 0 5 6 303.67 13.30 0 5 6 289.37 14.90 0 -5 6 287.17 13.50 0 -5 -6 292.37 17.30 0 -5 6 291.47 12.90 0 -5 6 259.57 13.20 0 -5 6 309.07 15.70 0 -5 -6 295.17 14.30 0 5 7 424.26 17.10 0 5 7 395.96 18.60 0 5 7 389.66 17.40 0 5 7 415.26 17.40 0 5 7 371.36 17.00 0 5 7 381.86 16.80 0 5 7 374.06 20.90 0 -5 -7 397.96 17.90 0 -5 7 412.26 17.30 0 -5 7 414.16 20.00 0 -5 7 405.56 16.30 0 -5 7 376.16 16.30 0 -5 7 391.76 17.00 0 -5 7 386.36 17.20 0 -5 7 431.36 18.50 0 -5 -7 372.16 21.20 0 5 8 59.09 7.00 0 5 8 53.99 7.00 0 5 8 72.69 7.20 0 5 8 77.99 7.60 0 5 8 71.69 6.40 0 5 8 65.99 6.90 0 5 8 72.79 7.40 0 -5 -8 68.19 7.10 0 -5 8 74.29 7.20 0 -5 -8 63.09 9.20 0 -5 8 65.39 7.00 0 -5 8 61.59 6.00 0 -5 8 62.59 6.80 0 -5 8 60.09 7.50 0 -5 8 69.99 6.70 0 -5 8 76.99 6.60 0 5 9 34.60 6.80 0 5 9 32.50 9.10 0 5 9 30.70 5.10 0 5 9 27.60 5.60 0 5 9 35.30 5.70 0 5 9 23.50 5.60 0 5 9 25.90 5.70 0 -5 9 31.20 7.80 0 -5 -9 31.00 5.50 0 -5 9 25.90 6.50 0 -5 -9 30.60 8.30 0 -5 9 23.20 5.50 0 -5 9 32.20 5.30 0 5 10 741.73 27.40 0 5 10 773.22 27.80 0 5 10 764.12 30.70 0 5 10 741.03 27.80 0 5 10 753.72 28.00 0 5 10 743.43 26.80 0 5 10 709.23 27.20 0 -5 -10 715.13 35.10 0 -5 10 654.03 31.20 0 -5 -10 735.03 30.40 0 -5 10 740.73 26.30 0 -5 10 734.33 27.10 0 -5 10 731.83 28.10 0 -5 10 749.92 27.80 0 -5 10 763.12 28.00 0 -5 10 716.53 26.20 0 5 11 41.10 5.60 0 5 11 40.00 5.50 0 5 11 43.50 5.50 0 5 11 49.50 6.00 0 5 11 46.20 6.00 0 -5 11 47.10 5.90 0 -5 11 44.70 6.00 0 -5 11 39.60 5.40 0 -5 11 39.60 5.90 0 -5 11 41.70 5.50 0 -5 11 42.50 8.50 0 -5 11 42.70 7.30 0 5 12 27.70 4.50 0 5 12 29.30 4.50 0 5 12 34.30 4.80 0 5 12 31.70 4.80 0 5 12 27.30 4.70 0 5 12 29.80 4.70 0 -5 12 27.60 4.30 0 -5 12 32.50 5.00 0 -5 12 31.10 4.80 0 -5 12 20.70 4.70 0 -5 12 24.90 4.10 0 -5 12 19.80 6.00 0 5 13 -0.30 1.70 0 5 13 2.60 2.00 0 5 13 5.10 2.20 0 5 13 -1.90 1.80 0 -5 13 -0.70 2.10 0 -5 13 -0.30 2.10 0 -5 13 5.00 4.10 0 -5 13 2.10 2.00 0 5 14 40.70 4.00 0 5 14 43.30 3.90 0 5 14 31.50 3.70 0 -5 14 40.10 3.80 0 -5 -14 29.80 4.60 0 -5 14 52.19 4.50 0 -5 14 36.20 4.20 0 6 0 522.35 23.20 0 6 0 556.94 20.20 0 -6 0 546.65 19.80 0 -6 0 568.94 21.30 0 -6 0 581.74 22.50 0 6 1 31.60 4.70 0 6 1 27.10 5.40 0 6 -1 24.70 5.30 0 6 -1 24.20 4.10 0 -6 -1 27.40 4.20 0 -6 1 36.00 4.10 0 -6 1 27.80 5.40 0 -6 -1 32.10 5.60 0 -6 -1 29.80 5.20 0 6 2 42.90 6.10 0 6 2 44.10 4.80 0 -6 2 41.40 4.30 0 -6 -2 44.10 6.20 0 -6 -2 49.30 5.00 0 -6 -2 44.30 5.60 0 6 3 1021.00 36.90 0 6 3 999.80 32.60 0 -6 -3 1013.00 35.50 0 -6 3 980.10 34.40 0 -6 -3 917.91 31.60 0 -6 -3 991.50 36.90 0 -6 3 1013.90 32.70 0 6 4 1921.51 56.79 0 6 4 1692.83 57.19 0 6 4 1680.03 52.99 0 6 4 1688.43 54.69 0 -6 4 1689.33 52.99 0 -6 -4 1773.22 56.29 0 -6 -4 1659.63 58.29 0 -6 -4 1503.95 51.39 0 -6 4 1681.13 55.69 0 -6 4 1833.02 55.49 0 6 5 311.97 15.30 0 6 5 266.27 13.30 0 6 5 282.27 13.80 0 6 5 286.07 14.10 0 6 5 297.07 16.20 0 6 5 298.97 14.20 0 6 5 296.27 14.10 0 6 5 279.67 15.20 0 -6 5 300.07 14.00 0 -6 5 282.47 14.30 0 -6 5 287.37 14.40 0 -6 5 287.67 15.30 0 -6 5 272.07 13.60 0 -6 5 284.47 13.80 0 -6 -5 298.37 17.60 0 -6 5 263.57 15.60 0 -6 -5 284.97 15.10 0 6 6 7.70 4.00 0 6 6 6.50 4.30 0 6 6 5.90 3.50 0 6 6 3.80 3.00 0 6 6 7.60 3.30 0 6 6 3.00 3.10 0 6 6 11.60 4.00 0 -6 -6 6.50 3.60 0 -6 6 10.20 3.50 0 -6 6 4.60 4.00 0 -6 6 0.60 2.70 0 -6 6 7.60 3.80 0 -6 6 8.90 3.50 0 -6 -6 9.70 7.70 0 -6 6 7.10 2.90 0 -6 6 6.90 4.00 0 6 7 112.59 9.00 0 6 7 114.09 8.20 0 6 7 126.59 8.90 0 6 7 125.99 11.60 0 6 7 108.29 8.60 0 6 7 122.59 9.30 0 6 7 107.39 8.60 0 -6 7 112.89 8.00 0 -6 7 116.49 8.40 0 -6 7 117.39 10.00 0 -6 7 114.39 8.90 0 -6 7 123.99 10.30 0 -6 7 117.49 8.90 0 -6 7 120.29 8.10 0 -6 7 107.19 9.00 0 6 8 2.80 2.90 0 6 8 -0.10 2.90 0 6 8 3.30 3.30 0 6 8 6.10 3.50 0 6 8 0.30 2.60 0 6 8 1.70 3.00 0 -6 8 5.80 3.30 0 -6 8 -1.90 2.60 0 -6 8 3.00 2.70 0 -6 8 -0.60 2.90 0 -6 -8 6.70 3.70 0 -6 8 3.60 3.30 0 -6 8 1.30 3.60 0 -6 8 -1.00 3.30 0 -6 8 -4.90 5.10 0 -6 -8 -3.60 4.50 0 6 9 4.90 3.10 0 6 9 4.80 3.10 0 6 9 8.40 4.30 0 6 9 3.60 3.20 0 6 9 4.50 3.50 0 6 9 6.40 3.50 0 6 9 9.00 3.30 0 -6 9 3.70 3.30 0 -6 9 7.40 3.30 0 -6 9 5.00 3.20 0 -6 9 5.80 3.00 0 -6 -9 16.40 7.10 0 -6 9 1.90 3.30 0 -6 9 7.60 3.20 0 -6 -9 5.90 4.60 0 -6 9 4.20 3.50 0 6 10 102.49 8.10 0 6 10 89.99 7.80 0 6 10 92.89 7.50 0 6 10 96.99 7.50 0 6 10 117.89 8.40 0 6 10 103.19 8.20 0 -6 10 86.79 7.20 0 -6 10 107.09 8.00 0 -6 10 99.59 8.20 0 -6 10 107.19 13.50 0 -6 10 92.39 7.20 0 -6 10 96.29 8.00 0 -6 10 89.09 7.90 0 6 11 93.79 7.50 0 6 11 97.19 7.40 0 6 11 82.39 7.20 0 6 11 86.29 7.10 0 6 11 89.19 7.00 0 6 11 89.09 6.70 0 -6 11 94.69 7.40 0 -6 11 85.89 7.60 0 -6 11 94.89 6.80 0 -6 11 91.49 6.90 0 -6 11 90.79 7.20 0 -6 11 98.89 7.70 0 -6 11 84.59 9.70 0 6 12 14.60 3.30 0 6 12 19.50 3.80 0 6 12 19.10 3.80 0 6 12 22.20 3.90 0 6 12 31.50 4.30 0 -6 12 15.30 3.40 0 -6 12 21.10 4.10 0 -6 12 25.80 4.50 0 -6 12 17.60 3.40 0 -6 12 16.80 3.30 0 -6 12 17.90 3.90 0 6 13 5.80 2.10 0 6 13 7.10 2.50 0 6 13 9.20 2.40 0 6 13 6.40 2.20 0 -6 13 11.10 2.70 0 -6 13 11.40 2.70 0 -6 13 8.50 2.30 0 6 14 60.19 3.90 0 6 -14 49.60 5.50 0 6 14 59.39 3.80 0 -6 14 53.19 4.30 0 -6 14 56.79 5.00 0 7 0 2.70 4.20 0 7 0 0.30 4.50 0 7 0 0.60 3.30 0 -7 0 -2.30 2.70 0 -7 0 -0.40 2.30 0 -7 0 -3.50 3.20 0 7 1 7.80 3.20 0 7 1 10.20 5.10 0 7 -1 2.40 3.90 0 7 1 1.40 3.60 0 7 1 6.10 4.60 0 7 1 -4.40 3.30 0 7 -1 -5.30 3.70 0 -7 -1 3.10 3.40 0 -7 1 -0.80 2.10 0 -7 1 -4.90 3.00 0 -7 -1 10.50 4.60 0 -7 -1 3.40 3.10 0 -7 1 -2.00 2.90 0 -7 -1 -2.60 2.40 0 7 -2 142.89 10.60 0 7 2 130.99 10.00 0 7 2 136.59 9.50 0 7 2 131.89 11.40 0 7 -2 137.09 9.40 0 7 2 143.39 10.20 0 7 2 138.19 8.30 0 -7 2 137.09 9.60 0 -7 2 140.19 8.70 0 -7 -2 147.49 8.40 0 -7 -2 151.88 11.40 0 -7 -2 147.09 11.30 0 7 3 200.48 10.50 0 7 3 216.18 12.00 0 7 3 183.18 16.40 0 7 3 200.88 11.40 0 7 3 201.28 11.90 0 7 3 211.68 14.50 0 7 -3 218.98 12.00 0 7 -3 222.18 12.20 0 -7 3 223.88 11.00 0 -7 -3 229.78 14.60 0 -7 -3 204.78 10.30 0 -7 3 217.18 11.80 0 -7 3 229.98 11.80 0 -7 3 205.48 10.90 0 -7 -3 202.08 13.50 0 -7 3 198.28 12.70 0 7 4 1.30 3.10 0 7 4 6.50 4.30 0 7 4 7.80 3.70 0 7 4 1.60 3.50 0 7 4 3.30 3.10 0 7 4 7.80 3.90 0 7 4 2.20 2.70 0 -7 4 5.70 5.30 0 -7 4 -2.40 3.40 0 -7 4 2.20 3.00 0 -7 4 0.50 4.30 0 -7 -4 1.30 3.60 0 -7 4 6.90 3.40 0 -7 -4 10.50 3.90 0 -7 -4 8.00 4.90 0 -7 4 8.40 2.90 0 7 5 320.47 15.30 0 7 5 316.27 15.20 0 7 5 307.17 18.40 0 7 5 320.47 15.20 0 7 5 323.67 15.90 0 7 5 318.97 14.50 0 7 5 321.57 15.00 0 -7 5 281.47 15.00 0 -7 5 315.57 17.00 0 -7 -5 306.97 17.60 0 -7 5 316.17 15.00 0 -7 5 334.97 14.50 0 -7 5 322.57 14.60 0 -7 5 347.47 15.60 0 -7 -5 344.67 20.00 0 -7 5 305.07 14.70 0 7 6 119.59 8.30 0 7 6 119.39 11.20 0 7 6 130.49 9.40 0 7 6 110.79 9.20 0 7 6 113.69 9.10 0 7 6 118.19 9.10 0 7 6 127.49 9.40 0 -7 6 118.39 8.30 0 -7 -6 114.79 12.20 0 -7 6 130.09 8.30 0 -7 6 112.49 9.00 0 -7 6 115.29 9.30 0 -7 6 113.89 8.70 0 -7 6 120.89 11.90 0 -7 -6 116.99 11.10 0 -7 6 130.49 9.60 0 7 7 172.08 11.00 0 7 7 191.68 14.10 0 7 7 188.88 11.30 0 7 7 182.38 11.50 0 7 7 195.38 11.60 0 7 7 179.88 11.20 0 7 7 171.88 12.70 0 -7 7 173.78 10.90 0 -7 7 204.28 14.00 0 -7 7 194.88 13.50 0 -7 7 206.98 11.00 0 -7 7 188.18 11.40 0 -7 7 158.78 11.00 0 -7 -7 187.88 16.20 0 -7 7 181.98 11.00 0 -7 7 190.88 11.50 0 -7 -7 189.48 13.80 0 7 8 203.78 11.90 0 7 8 187.28 14.60 0 7 8 211.58 12.00 0 7 8 196.68 11.00 0 7 8 201.08 11.40 0 7 8 208.48 11.90 0 7 8 209.48 11.70 0 -7 8 208.08 11.90 0 -7 8 200.98 11.20 0 -7 8 186.18 11.30 0 -7 8 220.38 19.80 0 -7 8 208.78 11.20 0 -7 8 195.78 11.90 0 -7 -8 199.38 14.60 0 -7 -8 178.18 11.40 0 -7 8 198.58 10.90 0 -7 8 211.28 12.10 0 -7 -8 191.88 17.00 0 7 9 108.69 8.10 0 7 9 113.99 8.50 0 7 9 105.39 8.20 0 7 9 113.29 8.60 0 7 9 96.89 8.10 0 -7 9 101.19 7.60 0 -7 9 95.19 10.40 0 -7 9 108.49 8.10 0 -7 9 95.09 8.00 0 -7 9 108.09 8.50 0 -7 9 114.39 8.70 0 -7 9 105.89 7.60 0 7 10 3.30 2.70 0 7 10 0.00 2.30 0 7 10 1.30 2.50 0 7 10 0.30 2.00 0 7 10 1.90 2.50 0 7 10 0.10 2.70 0 -7 10 1.50 2.40 0 -7 10 -0.30 2.10 0 -7 10 -1.00 2.30 0 -7 10 -2.20 2.40 0 -7 10 2.90 4.20 0 -7 10 -0.60 2.40 0 7 11 22.90 3.60 0 7 11 15.80 3.40 0 7 11 17.80 3.90 0 7 11 18.90 3.70 0 7 11 13.50 3.10 0 7 11 16.90 3.50 0 -7 11 17.20 3.50 0 -7 11 16.50 3.50 0 -7 11 18.10 3.40 0 -7 11 21.70 4.60 0 -7 11 14.70 3.90 0 7 12 31.30 4.00 0 7 12 30.70 3.80 0 7 12 38.70 5.90 0 7 12 21.70 4.50 0 7 12 32.20 4.00 0 -7 12 28.00 4.30 0 -7 12 32.90 3.70 0 -7 12 24.30 3.90 0 -7 12 25.90 5.00 0 7 13 0.40 1.20 0 7 -13 -0.80 2.00 0 7 13 1.00 2.10 0 -7 13 0.90 1.30 0 -7 13 0.50 1.50 0 -7 13 -0.20 1.50 0 8 0 105.19 9.10 0 8 0 102.49 9.20 0 8 0 112.69 8.80 0 -8 0 124.89 8.90 0 -8 0 110.89 8.10 0 -8 0 113.79 7.80 0 8 1 102.39 8.90 0 8 1 95.49 8.50 0 8 1 103.39 9.10 0 8 -1 105.39 10.00 0 8 -1 112.69 8.80 0 8 -1 105.89 8.70 0 8 1 101.69 8.70 0 8 1 91.19 8.20 0 -8 -1 97.59 7.90 0 -8 -1 109.39 7.60 0 -8 1 104.69 7.50 0 -8 1 95.99 7.80 0 -8 1 100.59 8.60 0 -8 1 117.99 9.10 0 -8 -1 108.19 11.10 0 -8 -1 92.69 8.10 0 8 2 245.18 12.80 0 8 2 216.28 17.70 0 8 2 195.78 12.10 0 8 2 254.57 13.30 0 8 2 242.88 12.90 0 8 2 244.28 11.70 0 8 2 236.08 12.90 0 8 -2 229.78 12.60 0 -8 2 252.87 12.80 0 -8 -2 233.38 11.50 0 -8 2 222.58 12.80 0 -8 -2 230.88 12.00 0 -8 -2 237.68 12.70 0 -8 2 225.88 14.20 0 -8 2 245.48 12.20 0 -8 -2 227.68 15.50 0 -8 2 219.08 11.60 0 8 -3 32.30 6.70 0 8 3 35.40 5.90 0 8 3 29.40 8.00 0 8 3 28.40 5.80 0 8 3 21.00 4.90 0 8 -3 32.30 6.30 0 8 3 31.70 5.80 0 8 3 31.40 5.80 0 8 3 29.20 5.20 0 8 -3 32.70 5.70 0 -8 -3 31.20 7.70 0 -8 3 28.90 5.40 0 -8 -3 22.10 4.60 0 -8 3 31.40 5.50 0 -8 3 25.00 4.70 0 -8 3 15.60 6.10 0 -8 -3 27.10 5.10 0 -8 3 32.40 5.20 0 -8 -3 34.40 11.40 0 8 4 134.69 9.50 0 8 4 104.49 12.50 0 8 4 111.49 9.10 0 8 -4 117.99 10.40 0 8 -4 133.59 9.80 0 8 4 113.19 8.20 0 8 4 140.69 10.00 0 -8 4 122.89 9.10 0 -8 -4 111.09 8.10 0 -8 4 131.99 10.20 0 -8 4 115.79 9.50 0 -8 4 122.49 8.50 0 -8 -4 120.39 12.50 0 -8 -4 126.59 13.30 0 -8 4 128.99 8.50 0 8 5 42.50 5.90 0 8 -5 33.70 7.40 0 8 5 54.19 6.40 0 8 -5 52.29 6.70 0 8 5 35.80 6.20 0 8 5 51.69 10.30 0 8 5 45.70 6.50 0 8 5 55.39 6.70 0 8 5 49.70 9.70 0 -8 5 46.50 6.50 0 -8 5 42.00 5.50 0 -8 5 51.89 8.60 0 -8 -5 35.90 8.90 0 -8 -5 42.40 6.70 0 -8 -5 48.20 9.20 0 -8 5 46.90 6.80 0 -8 5 33.70 5.30 0 -8 5 51.09 7.00 0 8 6 226.38 12.30 0 8 6 209.88 21.20 0 8 6 255.77 12.70 0 8 -6 263.97 13.50 0 8 6 248.58 13.20 0 8 6 232.28 12.80 0 8 6 244.48 13.50 0 8 6 234.98 12.80 0 -8 -6 234.88 18.80 0 -8 6 261.47 13.50 0 -8 6 218.98 11.90 0 -8 6 247.78 12.40 0 -8 -6 245.98 12.80 0 -8 6 256.77 13.50 0 -8 6 235.58 12.30 0 -8 6 235.48 12.90 0 -8 -6 226.88 19.80 0 8 7 32.00 5.40 0 8 7 27.40 5.00 0 8 7 33.30 5.30 0 8 7 35.20 6.10 0 8 -7 40.00 6.00 0 8 7 35.50 5.60 0 8 7 27.60 4.80 0 -8 7 31.40 4.70 0 -8 7 33.40 5.00 0 -8 7 32.70 5.70 0 -8 -7 43.30 5.90 0 -8 7 34.20 5.30 0 -8 7 30.10 5.20 0 -8 7 21.60 4.70 0 8 8 6.60 3.40 0 8 -8 5.70 3.60 0 8 8 3.50 2.70 0 8 8 3.30 2.70 0 8 8 6.80 3.80 0 8 8 3.80 2.70 0 8 8 3.10 2.90 0 -8 -8 1.20 3.40 0 -8 8 7.20 3.60 0 -8 8 2.40 3.10 0 -8 8 7.60 2.70 0 -8 8 1.20 2.40 0 -8 8 3.30 2.70 0 -8 8 3.70 3.70 0 8 9 122.39 7.70 0 8 9 130.59 8.40 0 8 9 118.99 8.40 0 8 9 134.99 8.70 0 8 9 123.59 8.30 0 8 9 133.29 8.70 0 8 -9 125.09 8.70 0 -8 9 119.29 8.40 0 -8 9 124.69 8.60 0 -8 9 110.39 7.60 0 -8 9 128.69 8.10 0 -8 9 123.89 7.80 0 8 10 7.30 2.60 0 8 -10 7.50 2.90 0 8 10 9.80 2.80 0 8 10 12.60 3.00 0 8 10 12.90 3.30 0 8 10 12.30 3.10 0 -8 10 8.40 3.60 0 -8 10 10.10 3.00 0 -8 10 10.70 3.20 0 -8 10 11.00 2.90 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3.70 -7 7 3 7.00 4.30 -7 7 3 5.70 4.50 -7 7 3 0.90 4.50 7 7 -3 2.80 3.50 -7 7 3 5.90 3.50 -7 7 3 14.00 6.80 -7 -7 3 1.10 4.20 -7 -7 3 7.90 3.80 7 -7 -3 -2.50 5.80 -7 -7 3 3.00 3.40 -7 -7 3 3.00 2.60 7 -7 -3 11.10 3.50 -7 -7 3 3.00 4.00 -7 7 2 6.30 6.40 -7 7 2 9.20 3.90 -7 7 2 11.30 5.30 -7 7 2 2.10 3.50 -7 7 2 8.70 4.10 -7 7 2 8.40 4.10 -7 7 2 12.40 5.00 7 7 -2 9.30 4.10 7 7 -2 7.60 4.50 -7 -7 2 3.60 5.10 -7 -7 2 2.70 3.70 -7 -7 2 13.30 3.60 -7 -7 2 0.60 8.70 7 -7 -2 4.50 3.50 -7 -7 2 6.50 3.90 -7 -7 2 5.90 3.60 -7 -7 2 10.30 4.60 7 -7 -2 12.10 7.50 -7 -7 2 10.40 4.10 7 -7 -2 7.60 3.70 -7 -7 2 5.20 3.40 7 7 -1 5.40 3.90 -7 7 1 -1.30 4.00 -7 7 1 10.50 4.40 -7 7 1 7.30 4.60 -7 7 1 6.10 5.40 -7 -7 1 7.70 3.50 -7 -7 1 5.50 4.60 -7 -7 1 2.90 5.20 -7 -7 1 -3.50 6.20 7 -7 -1 13.70 3.70 -7 -7 1 4.20 4.00 -7 -7 1 5.50 3.50 7 -7 -1 8.70 4.00 -7 -7 1 2.50 3.50 -7 7 0 127.99 10.60 -7 7 0 117.09 13.20 7 7 0 128.69 12.00 7 7 0 126.29 10.30 -7 7 0 126.19 10.10 7 7 0 138.09 11.20 -7 -7 0 145.19 10.60 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6.70 -7 -7 -4 41.80 5.60 7 -7 4 34.00 5.60 -7 -7 -4 31.60 9.00 -7 -7 -4 34.00 5.90 7 -7 4 34.90 5.30 7 -7 4 49.00 5.40 7 7 5 13.80 3.90 -7 7 -5 17.40 5.10 7 7 5 5.20 5.80 7 7 5 10.20 3.50 7 7 5 14.30 3.90 -7 -7 -5 8.20 3.50 7 -7 5 12.90 4.10 7 -7 5 13.00 3.70 7 -7 5 10.00 3.50 -7 -7 -5 13.30 4.50 7 7 6 49.60 5.90 7 7 6 55.99 6.60 -7 7 -6 59.09 11.20 7 7 6 31.20 5.10 7 7 6 50.39 5.80 7 -7 6 49.30 5.80 -7 -7 -6 57.19 7.90 -7 -7 -6 63.89 6.40 7 -7 6 47.60 5.60 7 -7 6 59.19 7.40 7 -7 6 55.79 5.90 7 7 7 172.88 9.90 7 7 7 161.88 9.40 -7 7 -7 168.58 10.70 7 7 7 156.48 9.20 7 7 7 160.98 9.20 7 -7 7 155.58 9.30 7 -7 7 179.18 9.80 7 -7 7 150.88 8.90 7 -7 7 149.49 8.70 -7 -7 -7 154.78 9.50 -7 -7 -7 175.28 9.90 7 7 8 7.30 3.10 7 7 8 5.90 3.10 7 7 8 7.80 2.70 7 7 8 4.80 2.40 -7 7 -8 3.20 3.10 7 -7 8 21.60 6.30 7 -7 8 5.80 2.40 -7 -7 -8 2.60 2.60 7 -7 8 8.20 3.20 -7 -7 -8 3.50 3.30 7 7 9 0.60 1.70 7 7 9 0.60 3.20 7 7 9 5.30 2.20 7 7 9 -2.90 3.60 -7 7 -9 -2.50 2.40 7 -7 9 5.00 3.20 -7 -7 -9 0.10 2.10 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24.40 3.40 -7 9 9 119.39 6.40 -7 9 9 107.69 6.90 -7 9 9 115.79 6.80 -7 -9 9 120.09 6.30 -7 -9 9 118.09 6.00 7 -9 -9 130.19 6.70 -7 -9 9 119.69 6.50 -7 -9 9 111.59 6.80 7 9 -8 165.68 8.30 -7 9 8 174.18 8.60 -7 9 8 162.38 8.80 -7 9 8 173.68 9.00 -7 9 8 159.28 8.20 -7 -9 8 175.38 9.10 -7 -9 8 170.78 8.70 -7 -9 8 172.58 9.00 -7 -9 8 170.48 8.00 -7 9 7 7.60 3.00 -7 9 7 5.30 3.80 -7 9 7 10.50 3.30 -7 9 7 7.60 2.70 7 9 -7 2.30 3.60 -7 -9 7 10.30 3.10 7 -9 -7 12.80 3.20 -7 -9 7 9.70 2.80 -7 -9 7 7.20 2.70 -7 -9 7 9.60 2.80 7 9 -6 201.78 10.40 -7 9 6 206.58 10.90 -7 9 6 206.28 9.80 -7 9 6 204.98 11.10 -7 9 6 193.18 9.90 -7 -9 6 191.58 9.40 -7 -9 6 199.98 9.90 -7 -9 6 205.68 10.00 7 -9 -6 208.18 9.80 -7 -9 6 208.68 11.10 -7 -9 6 197.68 10.00 -7 9 5 84.99 7.00 -7 9 5 83.69 7.40 -7 9 5 86.29 7.30 7 9 -5 81.69 6.80 -7 9 5 84.79 6.70 -7 -9 5 96.39 9.50 -7 -9 5 79.79 7.10 -7 -9 5 85.19 6.30 7 -9 -5 90.89 6.70 -7 -9 5 89.79 7.40 -7 -9 5 86.39 6.10 7 -9 -5 80.19 6.50 -7 9 4 -2.30 5.30 -7 9 4 3.80 3.00 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663.73 26.70 8 6 3 707.33 29.80 8 -6 3 700.63 25.80 -8 -6 -3 658.13 32.30 8 -6 3 673.03 25.20 -8 -6 -3 699.93 25.20 8 -6 3 688.13 25.30 -8 -6 -3 698.23 26.10 -8 -6 -3 653.33 25.40 -8 6 -4 72.49 8.00 8 6 4 61.59 6.70 8 6 4 54.59 7.20 8 6 4 67.59 8.60 8 6 4 57.89 6.70 -8 -6 -4 80.69 11.70 8 -6 4 61.39 6.80 -8 -6 -4 68.19 6.80 8 -6 4 65.69 6.40 -8 -6 -4 62.99 7.10 8 -6 4 62.69 6.50 8 6 5 12.90 4.00 8 6 5 8.60 5.00 8 6 5 8.90 3.70 8 6 5 10.10 3.70 -8 6 -5 2.80 3.40 -8 -6 -5 7.50 3.40 8 -6 5 1.60 3.00 8 -6 5 8.10 3.40 8 -6 5 12.40 3.80 -8 -6 -5 7.30 7.10 -8 -6 -5 6.80 3.80 8 -6 5 9.10 3.50 8 6 6 4.50 5.10 8 6 6 -1.30 2.40 -8 6 -6 -2.40 3.20 8 6 6 -2.60 2.50 8 6 6 0.50 2.90 8 -6 6 5.10 3.10 8 -6 6 -3.70 2.50 -8 -6 -6 -2.60 3.10 8 -6 6 -2.50 2.60 -8 -6 -6 0.90 2.70 8 -6 6 -1.40 2.70 8 6 7 110.49 8.00 8 6 7 99.09 7.40 -8 6 -7 99.39 8.50 8 6 7 94.49 7.20 8 6 7 94.09 11.10 8 6 7 83.49 7.10 8 -6 7 97.89 8.20 -8 -6 -7 97.99 8.10 8 -6 7 94.29 7.50 -8 -6 -7 100.89 7.70 8 -6 7 97.59 7.60 8 -6 7 72.99 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143.39 8.80 -8 7 10 159.38 8.90 -8 -7 10 147.99 8.50 -8 -7 10 143.19 8.90 -8 -7 10 159.58 8.10 -8 -7 10 164.18 9.00 8 7 -9 10.20 5.40 -8 7 9 15.90 3.60 8 7 -9 16.90 3.90 -8 7 9 12.50 3.40 -8 7 9 19.70 3.90 -8 7 9 16.40 4.00 -8 7 9 9.20 3.20 -8 -7 9 13.70 3.40 8 -7 -9 15.60 3.80 -8 -7 9 19.10 3.40 8 -7 -9 25.00 4.20 -8 -7 9 20.80 3.90 -8 -7 9 13.70 3.80 -8 -7 9 12.20 3.30 -8 7 8 3.00 2.80 -8 7 8 2.70 2.70 8 7 -8 -1.30 3.70 -8 7 8 -2.30 2.40 -8 7 8 -0.10 2.10 8 7 -8 3.60 3.00 -8 -7 8 3.40 3.90 8 -7 -8 3.00 2.80 -8 -7 8 0.10 2.80 -8 -7 8 -0.60 3.20 -8 -7 8 -1.50 2.20 -8 -7 8 1.00 2.80 -8 -7 8 -0.90 2.00 8 -7 -8 -1.60 2.90 -8 7 7 223.58 11.90 -8 7 7 210.48 12.10 -8 7 7 213.78 12.40 -8 7 7 219.48 12.30 -8 7 7 199.08 12.20 8 7 -7 213.48 15.20 8 7 -7 213.58 11.30 -8 -7 7 228.08 12.40 -8 -7 7 210.58 12.30 8 -7 -7 201.78 11.20 -8 -7 7 225.58 12.00 -8 -7 7 226.68 11.30 -8 -7 7 201.68 10.60 -8 -7 7 208.88 11.60 -8 7 6 18.50 4.60 8 7 -6 15.80 4.20 -8 7 6 12.90 4.80 8 7 -6 17.70 6.10 -8 7 6 12.10 3.80 -8 7 6 15.90 4.60 -8 7 6 18.90 4.40 8 -7 -6 17.50 4.20 -8 -7 6 12.90 3.70 -8 -7 6 14.90 4.40 -8 -7 6 14.80 3.50 -8 -7 6 14.00 4.00 -8 -7 6 20.70 5.00 -8 -7 6 14.40 3.90 -8 7 5 -1.70 3.20 -8 7 5 -1.30 2.60 8 7 -5 -5.20 2.90 -8 7 5 2.40 3.00 -8 7 5 -5.90 6.10 -8 7 5 -1.70 3.00 -8 7 5 2.40 3.20 8 7 -5 -5.50 3.10 -8 -7 5 -4.50 2.90 -8 -7 5 -3.00 2.80 -8 -7 5 1.50 2.50 8 -7 -5 1.20 2.60 -8 -7 5 -1.40 3.20 -8 -7 5 0.20 2.70 -8 -7 5 0.70 2.70 -8 7 4 412.66 18.40 -8 7 4 381.86 17.20 -8 7 4 401.46 18.70 -8 7 4 418.16 17.90 -8 7 4 397.86 27.60 -8 7 4 408.66 18.80 8 7 -4 410.96 17.60 -8 7 4 433.46 19.30 -8 -7 4 418.96 18.10 -8 -7 4 413.96 16.60 8 -7 -4 381.86 23.30 -8 -7 4 403.76 17.00 -8 -7 4 447.76 19.40 -8 -7 4 402.76 17.60 -8 -7 4 425.66 18.30 8 -7 -4 416.06 18.10 8 7 -3 37.00 5.70 -8 7 3 13.40 7.60 -8 7 3 29.80 6.10 8 7 -3 28.30 6.70 -8 7 3 39.20 5.90 -8 7 3 27.80 5.50 -8 7 3 32.30 5.90 -8 7 3 33.20 5.90 -8 7 3 45.90 6.80 -8 -7 3 33.20 4.80 -8 -7 3 45.40 6.80 8 -7 -3 30.10 8.90 -8 -7 3 37.30 5.90 -8 -7 3 43.30 5.70 -8 -7 3 47.00 6.30 -8 -7 3 41.80 6.40 8 -7 -3 36.50 5.10 8 7 -2 575.04 26.80 -8 7 2 582.84 23.60 -8 7 2 617.64 24.40 -8 7 2 608.94 24.40 8 7 -2 594.54 22.50 -8 7 2 551.54 22.80 -8 7 2 591.04 22.20 -8 7 2 588.94 22.80 -8 -7 2 557.94 22.50 -8 -7 2 607.54 26.60 -8 -7 2 571.74 22.80 -8 -7 2 490.75 26.30 8 -7 -2 582.34 22.80 -8 -7 2 581.74 22.20 -8 -7 2 575.34 21.20 8 -7 -2 569.74 22.90 -8 -7 2 554.24 22.00 8 7 -1 366.86 16.80 -8 7 1 396.26 18.10 -8 7 1 352.96 16.10 8 7 -1 338.77 19.30 8 7 -1 353.76 16.30 -8 7 1 356.06 16.90 -8 -7 1 375.76 17.10 -8 -7 1 352.96 22.20 8 -7 -1 364.06 16.70 -8 -7 1 365.16 15.10 -8 -7 1 354.96 16.10 8 -7 -1 376.36 16.70 -8 -7 1 355.46 15.80 -8 -7 1 368.06 16.50 -8 7 0 77.99 8.30 8 7 0 74.09 7.40 8 7 0 83.09 7.60 -8 7 0 96.49 9.10 8 7 0 72.59 8.80 -8 7 0 89.29 8.40 -8 -7 0 89.69 8.30 -8 -7 0 94.59 12.70 8 -7 0 78.99 7.20 -8 -7 0 72.49 6.90 8 -7 0 82.29 7.30 -8 -7 0 84.49 8.20 -8 -7 0 90.09 8.00 -8 7 -1 128.79 10.00 -8 7 -1 104.79 8.90 8 7 1 107.39 8.50 8 7 1 90.69 8.00 8 7 1 94.29 9.90 8 -7 1 109.49 8.20 -8 -7 -1 96.09 13.00 8 -7 1 113.09 8.20 -8 -7 -1 86.59 8.20 -8 -7 -1 99.69 8.50 -8 -7 -1 102.39 8.70 -8 -7 -1 101.59 7.80 -8 7 -2 883.01 31.70 8 7 2 837.62 29.70 8 7 2 838.12 30.30 -8 7 -2 826.02 29.70 -8 -7 -2 823.62 30.20 -8 -7 -2 837.02 30.00 8 -7 2 808.52 29.70 -8 -7 -2 920.61 50.99 -8 -7 -2 808.82 29.10 8 -7 2 863.01 30.20 -8 -7 -2 826.32 29.00 8 -7 2 763.72 28.60 8 7 3 688.73 26.30 8 7 3 664.13 25.00 8 7 3 673.03 29.70 -8 7 -3 688.63 26.00 -8 7 -3 695.83 27.40 8 7 3 707.53 26.00 -8 -7 -3 730.03 26.60 -8 -7 -3 706.03 26.50 -8 -7 -3 679.43 33.80 8 -7 3 718.83 26.10 8 -7 3 718.63 26.10 -8 -7 -3 723.03 25.80 8 7 4 7.80 5.40 -8 7 -4 3.40 3.60 8 7 4 6.80 3.30 8 7 4 2.20 3.70 8 7 4 8.50 3.10 -8 7 -4 4.60 3.50 8 -7 4 14.90 6.00 -8 -7 -4 10.90 3.90 8 -7 4 8.70 3.60 -8 -7 -4 11.10 3.70 8 -7 4 7.50 3.10 -8 -7 -4 8.60 3.90 8 7 5 194.08 14.40 8 7 5 208.78 11.50 8 7 5 210.88 10.90 -8 7 -5 205.38 11.70 8 -7 5 208.38 10.90 -8 -7 -5 218.18 12.30 8 -7 5 197.98 10.80 -8 -7 -5 226.18 11.50 8 -7 5 190.78 10.90 8 7 6 -3.10 2.10 8 7 6 -2.30 2.90 -8 7 -6 -1.20 2.90 8 7 6 2.30 2.70 -8 -7 -6 1.90 2.80 -8 -7 -6 -1.00 2.30 8 -7 6 0.90 2.10 8 -7 6 5.30 2.90 -8 -7 -6 -0.10 2.80 8 -7 6 1.90 2.70 -8 7 -7 43.60 5.90 8 7 7 38.90 5.00 8 7 7 32.00 4.90 8 7 7 33.30 4.30 8 -7 7 39.70 4.60 -8 -7 -7 32.30 5.20 -8 -7 -7 32.60 4.90 8 -7 7 37.80 4.50 8 -7 7 36.20 7.30 -8 -7 -7 38.10 4.90 8 7 8 135.39 7.90 8 7 8 142.09 7.60 8 7 8 150.08 8.30 -8 7 -8 160.48 9.30 8 -7 8 143.79 7.90 -8 -7 -8 143.79 8.40 -8 -7 -8 159.18 8.90 8 7 9 1.90 1.70 -8 7 -9 -1.00 2.10 8 7 9 1.70 1.60 -8 7 -9 -0.70 2.20 -8 -7 -9 1.10 1.90 -8 -7 -9 2.90 2.20 -8 7 -10 72.49 4.90 -8 7 -10 76.49 5.00 8 7 10 69.79 4.40 8 -7 10 74.19 4.40 -8 -7 -10 66.19 4.90 -8 -7 -10 54.19 5.90 -8 8 11 5.10 1.70 -8 8 11 6.00 1.70 -8 8 11 8.10 2.00 -8 -8 11 7.80 1.90 8 -8 -11 7.60 2.20 -8 -8 11 8.70 1.70 -8 8 10 53.79 4.60 8 8 -10 41.10 4.90 -8 8 10 53.59 4.60 -8 8 10 47.10 4.50 -8 8 10 50.69 4.20 -8 -8 10 47.90 4.00 -8 -8 10 52.29 4.80 -8 -8 10 59.09 4.50 -8 -8 10 48.80 4.20 -8 8 9 0.20 1.60 -8 8 9 1.60 2.00 -8 8 9 0.00 1.60 -8 8 9 1.50 1.90 -8 -8 9 3.30 2.00 -8 -8 9 2.10 2.10 -8 -8 9 4.30 2.30 -8 -8 9 1.00 1.70 -8 -8 9 -0.70 2.20 -8 8 8 47.90 5.00 -8 8 8 44.40 5.30 8 8 -8 46.10 5.00 -8 8 8 48.20 5.30 -8 8 8 44.50 6.50 -8 8 8 41.80 5.40 -8 -8 8 51.39 5.70 -8 -8 8 51.19 5.30 -8 -8 8 42.50 4.50 8 -8 -8 28.30 6.30 -8 -8 8 48.40 4.80 8 -8 -8 38.60 5.40 -8 -8 8 41.80 5.00 -8 8 7 9.40 3.40 8 8 -7 -1.20 4.20 -8 8 7 8.10 3.00 -8 8 7 11.10 3.50 -8 8 7 5.80 2.60 -8 8 7 4.00 2.80 8 8 -7 3.00 2.70 -8 -8 7 6.10 2.90 -8 -8 7 7.00 2.80 -8 -8 7 3.50 2.70 8 -8 -7 4.70 2.70 8 -8 -7 7.00 2.80 -8 -8 7 8.10 2.60 -8 -8 7 9.20 3.40 -8 8 6 500.15 19.60 8 8 -6 473.95 23.80 -8 8 6 480.55 20.40 8 8 -6 505.05 19.30 -8 8 6 517.85 20.80 -8 8 6 503.45 20.00 -8 -8 6 499.75 19.40 -8 -8 6 502.85 20.10 8 -8 -6 498.65 18.90 -8 -8 6 506.15 18.70 8 -8 -6 505.55 19.80 -8 -8 6 484.25 19.30 -8 -8 6 500.15 20.50 -8 -8 6 500.35 19.10 -8 8 5 117.79 8.50 -8 8 5 129.99 8.70 -8 8 5 119.99 9.20 8 8 -5 118.69 11.10 -8 8 5 120.19 9.10 -8 8 5 121.89 9.10 8 8 -5 120.59 8.40 -8 -8 5 114.59 8.00 -8 -8 5 119.29 8.70 8 -8 -5 128.89 8.20 8 -8 -5 111.89 8.10 -8 -8 5 120.59 7.50 -8 -8 5 114.29 8.40 -8 -8 5 110.19 7.60 -8 -8 5 126.39 9.30 8 8 -4 433.16 22.40 -8 8 4 435.36 18.40 -8 8 4 436.96 17.70 8 8 -4 462.15 19.10 -8 8 4 454.05 19.10 -8 8 4 460.95 18.50 -8 -8 4 416.46 17.40 8 -8 -4 453.05 18.80 8 -8 -4 463.75 19.00 -8 -8 4 437.16 18.50 -8 -8 4 452.95 17.90 -8 -8 4 449.06 17.20 -8 8 3 53.09 7.00 8 8 -3 56.39 8.30 -8 8 3 49.99 6.70 -8 8 3 51.79 7.00 8 8 -3 46.50 6.00 -8 8 3 53.89 7.10 -8 8 3 32.70 5.60 8 -8 -3 53.39 6.00 -8 -8 3 47.20 6.60 -8 -8 3 58.29 6.80 8 -8 -3 49.50 5.90 -8 -8 3 60.59 5.90 -8 -8 3 47.50 5.50 -8 -8 3 52.29 6.50 8 8 -2 475.15 19.30 -8 8 2 483.15 20.20 8 8 -2 459.15 19.40 -8 8 2 474.25 20.30 8 8 -2 402.46 22.10 8 -8 -2 467.75 19.70 -8 -8 2 462.45 19.30 -8 -8 2 465.15 19.30 -8 -8 2 457.45 18.00 8 -8 -2 474.25 19.20 -8 8 1 -1.20 3.60 8 8 -1 3.40 4.40 -8 8 1 -1.10 2.80 8 8 -1 -1.60 2.60 8 8 -1 0.10 2.90 8 -8 -1 2.60 2.40 -8 -8 1 1.30 3.20 8 -8 -1 2.80 2.50 -8 -8 1 12.40 3.90 -8 -8 1 -2.70 2.60 -8 8 0 188.28 11.90 8 8 0 209.38 11.60 8 8 0 200.98 11.20 8 8 0 191.28 13.90 -8 8 0 184.18 11.00 8 -8 0 198.48 11.30 8 -8 0 202.48 11.40 -8 -8 0 180.18 10.80 -8 -8 0 203.38 11.60 8 -8 0 206.58 11.30 -8 -8 0 193.68 10.40 -8 8 -1 8.00 3.70 8 8 1 13.50 3.60 8 8 1 6.10 3.20 8 8 1 5.40 5.00 -8 -8 -1 7.50 3.50 8 -8 1 8.60 3.10 8 -8 1 11.70 6.00 -8 -8 -1 8.20 3.60 8 -8 1 9.80 3.40 -8 8 -2 221.68 12.10 8 8 2 198.48 15.00 -8 8 -2 247.58 14.50 8 8 2 258.27 16.00 8 -8 2 223.88 11.70 -8 -8 -2 248.48 12.00 -8 -8 -2 244.48 12.40 8 -8 2 261.47 12.80 -8 -8 -2 291.87 17.40 8 -8 2 256.87 15.90 -8 -8 -2 252.37 12.50 8 8 3 259.47 12.90 8 8 3 267.27 12.60 8 8 3 271.97 13.00 -8 8 -3 258.47 12.90 8 8 3 251.97 22.00 -8 8 -3 271.37 14.20 -8 -8 -3 265.17 13.00 -8 -8 -3 257.47 12.60 8 -8 3 265.87 13.00 8 -8 3 278.97 12.90 -8 -8 -3 275.97 13.60 8 8 4 10.50 3.10 -8 8 -4 3.40 3.60 -8 8 -4 13.70 3.80 8 8 4 14.60 4.00 8 8 4 15.00 3.60 8 -8 4 12.80 3.50 -8 -8 -4 9.70 3.20 8 -8 4 7.90 3.00 -8 -8 -4 16.30 5.30 -8 -8 -4 17.00 3.90 -8 8 -5 44.30 5.60 -8 8 -5 40.80 6.00 8 8 5 44.40 5.60 8 8 5 40.40 5.00 8 8 5 47.50 7.80 8 -8 5 40.00 4.70 -8 -8 -5 38.50 5.00 8 -8 5 34.20 4.80 -8 -8 -5 39.40 5.40 -8 -8 -5 34.80 5.30 8 8 6 51.39 5.00 8 8 6 54.39 5.20 -8 8 -6 40.70 5.30 8 8 6 56.09 5.60 -8 8 -6 48.60 5.80 -8 -8 -6 47.50 5.30 -8 -8 -6 48.90 5.50 -8 -8 -6 52.09 5.30 8 -8 6 39.60 4.70 8 -8 6 45.50 4.70 8 8 7 3.70 2.20 8 8 7 0.50 3.00 -8 8 -7 2.80 2.30 -8 8 -7 4.10 2.50 8 -8 7 3.40 5.20 -8 -8 -7 4.20 2.50 8 -8 7 0.90 1.90 -8 -8 -7 5.00 2.50 -8 -8 -7 5.90 2.50 8 8 8 1.20 1.80 -8 8 -8 2.20 2.60 8 8 8 -1.50 1.20 -8 -8 -8 -0.90 1.60 -8 -8 -8 -0.40 1.80 -8 -8 -8 -3.30 2.50 8 -8 8 2.00 1.80 -8 8 -9 0.70 1.90 8 8 9 3.30 2.10 -8 8 -9 0.60 1.70 -8 -8 -9 -0.60 1.80 -8 -8 -9 1.80 1.60 8 9 -9 61.69 4.70 -8 9 9 77.79 4.70 -8 9 9 71.89 4.50 8 -9 -9 79.79 4.80 -8 -9 9 71.79 4.20 -8 -9 9 76.49 4.70 -8 -9 9 75.79 4.80 -8 -9 9 67.89 4.30 -8 9 8 13.00 2.60 -8 9 8 16.30 2.80 -8 9 8 12.10 2.60 -8 -9 8 11.80 2.90 -8 -9 8 10.90 2.50 -8 -9 8 9.70 2.50 8 9 -7 -2.80 1.90 -8 9 7 -1.10 1.90 -8 9 7 -0.90 2.10 -8 9 7 3.00 2.20 -8 9 7 2.40 2.50 -8 -9 7 0.10 1.80 8 -9 -7 1.50 2.50 -8 -9 7 -0.30 2.00 -8 -9 7 0.50 1.50 8 -9 -7 0.40 2.70 -8 9 6 57.29 5.60 -8 9 6 57.39 5.20 8 9 -6 57.99 5.10 -8 9 6 49.00 5.50 -8 9 6 64.29 5.90 8 -9 -6 60.39 5.00 -8 -9 6 44.70 4.80 -8 -9 6 60.39 5.50 8 -9 -6 46.80 5.00 -8 -9 6 52.89 5.70 -8 -9 6 57.89 5.20 -8 -9 6 52.09 4.50 -8 9 5 63.19 6.50 -8 9 5 72.29 6.50 8 9 -5 88.09 6.40 -8 9 5 76.79 6.50 -8 9 5 79.39 6.90 8 -9 -5 70.79 5.80 -8 -9 5 73.49 6.40 8 -9 -5 79.69 6.20 -8 -9 5 82.19 5.70 -8 -9 5 88.99 6.60 -8 -9 5 71.79 7.60 8 9 -4 4.90 2.70 8 9 -4 -3.90 2.10 -8 9 4 -0.10 2.80 -8 9 4 0.90 2.60 -8 9 4 4.20 2.90 8 -9 -4 2.20 2.30 -8 -9 4 -1.90 2.80 -8 -9 4 2.20 3.60 -8 -9 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31.70 -10 0 -4 731.53 25.50 10 0 4 729.73 26.20 10 0 5 1.40 4.20 10 0 5 -0.60 2.70 -10 0 -5 -1.80 3.20 10 0 5 1.40 3.20 10 0 5 0.20 3.50 -10 0 -5 7.40 6.20 10 0 5 -0.10 3.10 -10 0 -5 9.00 4.50 10 0 6 2.20 13.20 10 0 6 8.10 4.50 -10 0 -6 -12.40 6.70 10 0 6 8.90 4.10 -10 0 -6 5.80 3.80 10 0 6 5.50 4.00 10 0 6 12.40 4.00 10 0 6 4.70 5.30 10 0 6 17.60 4.20 -10 0 -6 5.60 4.80 10 0 7 1.90 4.00 10 0 7 0.80 2.90 10 0 7 0.10 2.40 10 0 7 -5.80 3.20 10 0 7 3.00 2.90 -10 0 -7 -2.40 3.60 -10 0 -7 -1.10 5.10 10 0 7 0.10 2.90 10 0 8 455.75 23.60 10 0 8 455.25 22.20 10 0 8 462.95 19.00 10 0 8 442.16 19.40 10 0 8 443.56 19.30 10 0 9 -1.00 2.30 10 0 9 -0.30 2.20 10 0 9 -0.70 2.20 10 0 9 -0.40 4.00 10 0 9 2.90 2.50 10 0 9 1.50 2.70 10 0 10 309.97 16.10 10 0 10 279.57 13.50 10 0 10 298.17 12.60 10 0 10 308.97 13.50 10 0 10 298.97 13.50 10 0 11 1.30 1.90 10 0 11 0.50 1.70 10 0 11 -1.40 1.60 10 0 11 3.30 1.90 10 0 12 63.39 4.10 10 0 12 70.29 5.50 10 0 12 64.89 4.60 10 0 12 67.69 4.20 -10 1 14 2.70 2.30 -10 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15.40 6.80 10 -2 8 25.80 4.90 10 -2 8 22.70 4.30 10 2 9 20.50 3.70 10 2 9 20.80 6.40 10 2 9 22.70 4.10 10 2 9 20.50 4.30 10 2 9 20.00 3.70 10 2 9 15.40 3.60 10 -2 9 20.40 3.90 10 -2 9 16.20 3.50 10 -2 9 15.90 3.70 10 -2 9 17.00 7.10 10 -2 9 15.60 3.50 -10 -2 -9 16.50 4.20 10 -2 9 21.30 4.20 -10 -2 -9 30.10 5.00 10 2 10 4.80 2.30 10 2 10 4.50 2.30 10 2 10 4.10 2.40 10 2 10 3.00 2.20 10 2 10 3.20 2.40 10 -2 10 4.50 2.50 10 -2 10 4.20 2.30 10 -2 10 5.80 2.70 10 -2 10 -0.90 2.20 10 -2 10 4.00 2.10 10 2 11 10.50 2.60 10 2 11 12.80 2.60 10 2 11 8.90 2.70 10 2 11 8.70 2.20 10 2 11 12.40 2.50 10 -2 11 10.10 2.60 10 -2 11 5.80 2.40 10 -2 11 8.50 2.30 10 -2 11 5.30 2.10 10 2 12 18.20 2.60 10 2 12 21.30 2.60 10 2 12 18.20 2.70 -10 2 -12 23.80 3.50 10 -2 12 20.90 2.60 10 -2 12 16.00 2.80 10 -2 12 21.20 2.70 -10 3 13 11.10 3.40 -10 3 13 8.90 2.50 -10 3 13 9.70 2.30 -10 -3 13 9.20 3.30 -10 -3 13 11.00 2.70 -10 -3 13 9.00 2.00 -10 -3 13 11.30 2.50 -10 3 12 75.99 6.10 -10 3 12 80.39 7.40 -10 3 12 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-10 3 8 134.89 9.10 -10 3 8 143.29 10.60 -10 3 8 131.09 9.60 -10 3 8 142.19 9.00 10 3 -8 162.58 13.50 -10 3 8 131.69 9.90 -10 -3 8 122.29 8.60 -10 -3 8 154.28 9.80 -10 -3 8 139.49 9.80 -10 -3 8 138.59 10.20 -10 -3 8 133.79 8.80 -10 -3 8 134.69 9.50 -10 -3 8 143.59 10.10 -10 -3 8 129.79 10.40 -10 3 7 837.72 40.20 -10 3 7 855.91 33.60 -10 3 7 877.01 33.10 -10 3 7 882.21 32.30 -10 3 7 917.81 31.10 -10 3 7 901.61 32.60 10 3 -7 902.41 36.20 -10 3 7 870.31 32.80 -10 -3 7 840.72 38.50 -10 -3 7 874.91 31.20 -10 -3 7 898.21 31.80 -10 -3 7 911.11 32.00 -10 -3 7 892.41 32.20 -10 -3 7 860.21 30.70 -10 -3 7 855.91 31.50 -10 -3 7 891.51 30.90 -10 -3 7 867.41 31.70 -10 3 6 49.20 5.60 10 3 -6 46.50 7.20 -10 3 6 48.60 6.10 -10 3 6 35.60 8.70 -10 3 6 52.39 7.40 -10 3 6 44.20 8.60 -10 3 6 50.99 6.70 -10 3 6 42.20 6.70 -10 -3 6 43.30 5.50 -10 -3 6 42.90 7.40 -10 -3 6 42.50 9.40 -10 -3 6 42.20 5.20 -10 -3 6 42.30 6.80 -10 -3 6 46.30 6.70 -10 -3 6 51.39 8.90 -10 -3 6 42.80 6.30 -10 -3 6 38.10 6.80 -10 3 5 2.50 3.50 -10 3 5 0.60 3.30 -10 3 5 -2.30 5.50 -10 3 5 3.90 3.40 -10 3 5 4.80 3.00 -10 3 5 5.90 3.30 10 3 -5 6.20 4.30 -10 3 5 6.80 5.00 -10 3 5 3.10 3.20 -10 -3 5 1.80 2.50 -10 -3 5 4.90 4.70 -10 -3 5 3.70 3.60 -10 -3 5 -2.80 3.00 -10 -3 5 8.10 4.70 -10 -3 5 -2.80 4.60 -10 -3 5 6.50 3.60 -10 -3 5 3.40 3.10 -10 -3 5 5.60 3.50 -10 3 4 335.27 15.00 -10 3 4 304.57 16.30 -10 3 4 319.07 20.90 -10 3 4 346.87 15.70 -10 3 4 318.57 15.70 10 3 -4 326.37 18.10 -10 3 4 334.87 15.10 -10 3 4 335.17 16.30 -10 3 4 334.77 16.40 -10 -3 4 309.67 19.70 -10 -3 4 319.87 15.20 -10 -3 4 343.97 15.90 -10 -3 4 309.07 14.50 -10 -3 4 324.97 14.40 -10 -3 4 342.17 15.70 -10 -3 4 352.76 16.10 -10 -3 4 338.07 14.90 -10 3 3 134.29 9.70 -10 3 3 114.49 8.50 -10 3 3 141.89 8.70 10 3 -3 140.99 11.20 -10 3 3 136.39 9.00 -10 3 3 121.39 12.50 -10 3 3 123.99 9.90 -10 3 3 125.59 9.70 -10 -3 3 125.39 9.60 -10 -3 3 103.89 8.90 -10 -3 3 120.89 8.80 -10 -3 3 139.69 9.70 -10 -3 3 127.09 9.10 -10 -3 3 133.89 12.40 -10 -3 3 125.59 8.50 -10 -3 3 136.19 8.20 -10 3 2 375.16 17.20 -10 3 2 359.66 15.50 -10 3 2 379.96 16.10 -10 3 2 370.36 17.30 10 3 -2 366.66 19.00 10 3 -2 345.57 16.10 -10 3 2 385.56 19.10 -10 3 2 363.46 15.60 -10 3 2 352.26 21.00 -10 -3 2 353.26 17.60 -10 -3 2 359.36 15.50 -10 -3 2 358.96 14.80 -10 -3 2 364.46 16.30 10 -3 -2 323.67 15.70 -10 -3 2 345.07 16.00 -10 -3 2 350.66 16.20 10 3 -1 4.00 3.30 -10 3 1 4.50 4.50 -10 3 1 -0.50 2.50 10 3 -1 1.40 3.50 -10 3 1 3.50 4.10 -10 3 1 2.90 4.50 -10 3 1 3.60 5.10 -10 3 1 3.20 3.30 -10 3 1 2.40 3.10 -10 -3 1 -7.90 3.10 -10 -3 1 3.40 3.50 -10 -3 1 3.20 3.00 -10 -3 1 13.00 3.90 10 -3 -1 4.00 3.90 -10 -3 1 0.60 5.30 -10 -3 1 8.70 3.70 -10 -3 1 2.30 4.70 -10 3 0 -2.60 3.20 -10 3 0 -1.60 2.50 -10 3 0 4.80 3.60 10 3 0 1.50 3.00 -10 3 0 -3.00 5.60 -10 3 0 5.30 4.80 10 3 0 2.80 2.80 -10 3 0 0.10 3.90 -10 3 0 -11.10 4.60 -10 -3 0 1.60 3.20 -10 -3 0 -3.60 3.20 -10 -3 0 -2.10 2.60 -10 -3 0 3.40 3.80 -10 -3 0 -3.20 3.20 10 3 1 44.20 5.80 -10 3 -1 36.30 7.60 10 3 1 28.50 6.40 -10 3 -1 40.00 8.40 -10 3 -1 45.40 7.00 -10 3 -1 40.10 6.10 -10 3 -1 38.50 5.90 10 -3 1 31.40 5.40 10 -3 1 40.00 5.20 10 -3 1 34.40 6.50 -10 -3 -1 35.80 6.10 -10 -3 -1 49.50 7.30 -10 -3 -1 35.40 5.00 -10 -3 -1 24.60 6.60 -10 3 -2 -1.90 3.80 -10 3 -2 -0.20 4.90 10 3 2 1.10 3.00 -10 3 -2 6.50 5.90 -10 3 -2 4.00 4.10 10 3 2 3.00 2.90 10 3 2 1.20 4.60 10 3 2 1.70 3.30 10 -3 2 1.50 3.40 -10 -3 -2 0.20 3.30 10 -3 2 5.90 3.30 -10 -3 -2 2.40 4.40 10 -3 2 1.50 4.00 -10 -3 -2 3.40 4.90 -10 -3 -2 1.90 2.90 10 3 3 72.69 7.20 10 3 3 74.19 7.20 -10 3 -3 80.89 11.10 10 3 3 83.49 7.80 10 3 3 99.99 10.10 -10 3 -3 74.19 8.40 -10 -3 -3 79.29 7.00 -10 -3 -3 81.89 8.60 10 -3 3 63.79 7.60 10 -3 3 72.09 8.30 10 -3 3 73.89 6.70 10 -3 3 87.09 7.70 -10 -3 -3 66.29 7.40 -10 -3 -3 60.59 9.60 10 3 4 -0.70 3.20 10 3 4 -2.80 3.10 10 -3 4 -1.90 4.30 -10 -3 -4 -6.80 5.00 10 -3 4 1.20 5.50 -10 -3 -4 6.90 3.20 -10 -3 -4 6.50 5.70 10 -3 4 3.20 3.90 10 -3 4 1.00 4.90 10 3 5 163.18 10.50 10 3 5 171.58 13.30 10 3 5 167.98 10.60 10 3 5 162.38 10.30 10 3 5 166.98 10.20 10 -3 5 168.48 10.30 -10 -3 -5 174.48 10.80 10 -3 5 152.08 10.50 10 -3 5 169.18 10.70 -10 -3 -5 184.18 16.00 10 -3 5 165.78 12.80 10 3 6 69.39 6.90 10 3 6 44.30 6.30 10 3 6 59.09 6.20 10 3 6 65.19 8.70 10 3 6 65.29 7.10 10 -3 6 67.19 7.60 10 -3 6 65.59 6.90 10 -3 6 50.39 9.60 -10 -3 -6 54.89 6.40 -10 -3 -6 57.29 7.00 10 -3 6 62.09 6.90 10 -3 6 63.29 7.10 -10 -3 -6 53.29 11.10 10 3 7 235.88 11.90 10 3 7 225.38 12.50 10 3 7 223.38 11.70 10 3 7 240.18 12.90 10 3 7 214.68 15.50 10 -3 7 228.88 12.70 -10 -3 -7 209.28 12.20 10 -3 7 224.38 12.10 -10 -3 -7 241.38 12.10 10 -3 7 249.08 12.90 10 -3 7 231.98 11.90 10 -3 7 216.38 15.30 10 3 8 258.47 12.20 10 3 8 257.47 12.50 10 3 8 270.87 13.60 10 3 8 261.27 12.20 10 3 8 270.97 12.80 -10 -3 -8 257.97 12.90 10 -3 8 266.17 13.30 10 -3 8 270.17 12.40 10 -3 8 268.27 16.80 10 -3 8 276.17 13.50 10 -3 8 268.97 12.80 10 -3 8 263.27 12.30 -10 -3 -8 257.97 12.70 10 3 9 14.60 3.50 10 3 9 14.00 5.80 10 3 9 7.80 3.10 10 3 9 4.00 4.00 10 3 9 11.10 2.70 -10 -3 -9 14.50 3.70 10 -3 9 9.40 3.10 -10 -3 -9 7.20 3.40 10 -3 9 11.70 3.10 10 -3 9 8.30 3.00 10 -3 9 12.10 3.60 10 3 10 6.70 2.20 10 3 10 5.90 2.40 10 3 10 7.90 2.30 10 -3 10 8.80 2.40 -10 -3 -10 9.30 3.80 10 -3 10 7.70 2.50 10 -3 10 4.50 2.20 10 -3 10 5.50 3.10 10 3 11 6.10 1.90 10 3 11 8.30 2.20 10 3 11 13.70 3.40 -10 3 -11 8.20 2.50 10 3 11 12.90 2.50 10 -3 11 8.40 2.30 10 -3 11 13.80 2.90 10 -3 11 11.60 2.40 -10 4 13 58.59 4.60 -10 4 13 58.09 4.40 -10 4 13 57.29 4.20 -10 4 13 57.29 6.80 -10 -4 13 60.39 4.40 -10 -4 13 56.79 7.00 -10 4 12 1.70 2.00 -10 4 12 0.60 2.50 -10 4 12 -1.90 1.60 -10 4 12 -0.80 1.80 -10 4 12 4.20 2.50 -10 -4 12 0.60 1.80 -10 -4 12 0.00 1.70 -10 -4 12 1.30 1.70 -10 -4 12 1.90 2.70 -10 4 11 515.85 21.00 -10 4 11 525.15 19.00 -10 4 11 553.34 21.10 -10 4 11 556.74 20.90 -10 4 11 535.05 19.70 -10 4 11 558.34 21.20 -10 -4 11 525.85 19.60 -10 -4 11 542.15 20.30 -10 -4 11 574.14 20.90 -10 -4 11 553.84 20.00 -10 -4 11 544.65 20.20 -10 -4 11 533.75 19.70 -10 4 10 -1.60 2.20 -10 4 10 1.20 2.30 -10 4 10 -2.90 2.20 -10 4 10 -2.40 2.20 10 4 -10 7.30 7.90 -10 4 10 -1.50 2.00 -10 -4 10 0.80 2.30 -10 -4 10 1.00 2.20 -10 -4 10 -3.10 1.70 -10 -4 10 -4.80 3.10 -10 -4 10 2.60 3.20 -10 4 9 23.10 4.40 -10 4 9 21.10 4.60 -10 4 9 23.40 4.50 10 4 -9 14.10 5.30 -10 -4 9 15.90 4.40 -10 -4 9 23.10 4.50 -10 -4 9 18.80 4.30 -10 4 8 0.00 2.50 10 4 -8 -2.10 3.90 -10 4 8 -2.00 2.50 -10 4 8 -6.10 4.20 -10 4 8 3.00 3.00 -10 4 8 1.10 2.90 -10 4 8 -2.60 2.20 -10 4 8 0.80 3.00 -10 -4 8 2.30 2.90 -10 -4 8 1.70 2.90 -10 -4 8 1.30 2.40 -10 -4 8 -0.50 3.50 -10 -4 8 4.20 2.70 -10 -4 8 1.90 2.70 -10 4 7 4.10 3.40 -10 4 7 6.40 3.50 -10 4 7 5.70 3.50 10 4 -7 9.60 4.60 -10 4 7 6.40 3.50 -10 4 7 1.70 3.50 -10 4 7 2.30 4.30 -10 4 7 8.30 3.20 -10 -4 7 2.80 3.90 -10 -4 7 4.20 2.80 -10 -4 7 9.80 4.60 -10 -4 7 6.70 3.40 -10 -4 7 2.50 5.30 -10 -4 7 9.80 4.10 -10 -4 7 3.40 3.20 -10 -4 7 5.20 3.70 10 4 -6 31.20 7.20 -10 4 6 33.90 6.40 -10 4 6 30.20 8.70 -10 4 6 20.90 4.50 -10 4 6 33.70 6.10 -10 4 6 19.30 5.20 -10 4 6 20.00 4.80 -10 -4 6 16.20 5.80 -10 -4 6 23.50 5.20 -10 -4 6 29.30 9.40 -10 -4 6 28.30 4.70 -10 -4 6 30.40 5.30 -10 -4 6 27.80 5.40 -10 -4 6 30.40 5.70 -10 -4 6 17.00 4.50 -10 -4 6 20.50 5.70 -10 4 5 0.80 4.50 -10 4 5 12.90 5.10 -10 4 5 10.40 3.50 -10 4 5 28.30 7.90 -10 4 5 2.50 3.20 -10 4 5 8.60 4.10 10 4 -5 9.80 4.30 -10 4 5 8.80 4.20 -10 -4 5 8.60 7.50 -10 -4 5 7.60 6.30 -10 -4 5 6.80 4.20 -10 -4 5 9.60 3.90 -10 -4 5 12.10 4.10 -10 -4 5 9.60 3.90 -10 -4 5 12.60 5.80 -10 -4 5 11.40 5.10 -10 -4 5 11.90 3.70 10 4 -4 14.30 5.20 -10 4 4 16.60 4.40 -10 4 4 17.20 5.30 -10 4 4 21.80 7.70 -10 4 4 22.00 4.50 -10 4 4 11.80 4.70 -10 4 4 16.30 4.10 -10 4 4 23.40 5.00 -10 4 4 19.30 4.70 -10 -4 4 23.60 5.40 -10 -4 4 15.80 4.30 -10 -4 4 16.10 4.70 -10 -4 4 18.70 5.30 -10 -4 4 17.60 6.90 -10 -4 4 17.80 4.00 -10 -4 4 15.90 4.40 -10 -4 4 14.20 4.50 -10 -4 4 13.40 3.90 -10 4 3 -2.80 3.20 -10 4 3 -1.00 3.30 -10 4 3 10.10 4.10 -10 4 3 9.20 3.60 -10 4 3 -2.20 3.70 -10 4 3 2.50 4.60 -10 4 3 3.90 2.70 -10 -4 3 2.00 6.00 -10 -4 3 7.50 3.20 -10 -4 3 -0.40 3.10 -10 -4 3 4.00 3.40 -10 -4 3 2.70 3.60 -10 -4 3 3.50 3.10 -10 -4 3 1.90 4.10 -10 -4 3 -2.30 3.10 -10 4 2 11.80 5.20 -10 4 2 2.70 3.10 -10 4 2 3.20 4.60 -10 4 2 10.20 4.40 10 4 -2 3.30 3.30 -10 4 2 2.40 4.40 -10 4 2 3.50 3.60 10 4 -2 6.80 3.80 -10 4 2 4.50 4.20 -10 4 2 5.60 3.40 -10 -4 2 8.60 5.00 -10 -4 2 4.90 3.80 -10 -4 2 9.80 4.30 -10 -4 2 6.80 4.30 -10 -4 2 7.60 3.60 -10 -4 2 3.60 3.40 -10 -4 2 4.20 3.00 -10 -4 2 7.30 3.70 10 4 -1 25.60 5.20 -10 4 1 26.80 7.40 -10 4 1 35.60 6.50 -10 4 1 28.60 6.40 -10 4 1 37.10 6.70 -10 4 1 22.70 4.80 10 4 -1 55.19 9.20 -10 4 1 37.40 5.70 -10 4 1 21.50 5.20 -10 -4 1 39.00 6.20 -10 -4 1 33.40 5.60 -10 -4 1 32.10 5.80 -10 -4 1 31.30 5.30 -10 -4 1 32.60 5.30 -10 -4 1 34.00 8.10 -10 -4 1 16.60 5.80 -10 4 0 50.39 7.50 10 4 0 51.69 7.00 10 4 0 53.39 7.70 -10 4 0 59.89 7.90 -10 4 0 59.89 9.70 10 4 0 43.60 6.60 -10 4 0 32.70 6.30 -10 4 0 43.30 6.00 -10 4 0 54.69 6.20 -10 -4 0 40.90 6.50 10 -4 0 49.50 5.50 -10 -4 0 42.20 5.50 -10 -4 0 69.09 9.00 -10 -4 0 44.30 6.40 -10 -4 0 44.50 6.40 10 -4 0 50.99 6.70 -10 4 -1 -1.60 5.90 -10 4 -1 3.30 3.90 -10 4 -1 -4.40 5.50 10 4 1 -2.10 2.70 10 4 1 -2.20 2.80 -10 4 -1 7.00 4.60 10 4 1 3.70 4.20 -10 -4 -1 0.70 2.70 -10 -4 -1 1.30 4.60 -10 -4 -1 -0.60 3.60 10 -4 1 4.70 4.00 -10 -4 -1 -1.30 3.20 10 -4 1 -0.50 2.70 -10 4 -2 1343.77 44.60 10 4 2 1327.57 44.10 10 4 2 1324.47 42.70 10 4 2 1288.27 43.20 10 4 2 1310.97 48.40 -10 -4 -2 1371.86 43.40 -10 -4 -2 1240.58 43.00 10 -4 2 1314.77 43.50 -10 -4 -2 1351.36 44.30 10 -4 2 1295.07 42.60 10 -4 2 1315.97 42.80 -10 -4 -2 1336.17 51.29 10 4 3 1291.07 43.90 10 4 3 1281.37 43.10 -10 4 -3 1262.37 44.20 10 4 3 1330.07 43.90 10 4 3 1319.87 48.30 10 -4 3 1299.37 42.00 -10 -4 -3 1329.57 51.69 -10 -4 -3 1299.57 45.60 -10 -4 -3 1301.57 43.60 -10 -4 -3 1321.27 43.00 10 4 4 692.63 26.10 10 4 4 743.33 27.40 -10 4 -4 711.13 27.70 10 4 4 704.53 31.10 10 4 4 706.03 25.80 -10 -4 -4 733.43 26.60 -10 -4 -4 724.83 26.10 10 -4 4 686.43 25.40 -10 -4 -4 702.43 26.80 10 -4 4 696.83 26.70 10 -4 4 709.63 25.20 -10 -4 -4 726.63 34.40 10 -4 4 707.33 25.50 10 -4 4 737.93 30.30 10 4 5 26.40 5.30 10 4 5 34.40 5.50 10 4 5 22.40 4.70 -10 4 -5 22.30 5.20 10 4 5 15.80 8.10 -10 -4 -5 10.80 7.10 -10 -4 -5 27.00 5.00 -10 -4 -5 28.30 5.40 10 -4 5 28.00 5.20 10 -4 5 28.60 5.00 10 -4 5 23.60 4.60 -10 -4 -5 22.20 5.30 10 4 6 44.90 6.60 10 4 6 29.30 4.70 10 4 6 28.50 5.30 10 4 6 36.80 5.70 -10 4 -6 28.00 5.30 10 -4 6 24.60 4.60 10 -4 6 22.00 5.10 -10 -4 -6 27.80 5.10 -10 -4 -6 22.40 4.60 10 -4 6 24.20 6.80 10 -4 6 33.50 5.20 10 4 7 21.80 6.20 10 4 7 9.90 3.50 10 4 7 15.50 3.50 10 4 7 14.90 3.90 10 4 7 15.40 4.10 10 4 7 16.60 4.20 10 -4 7 11.00 3.90 10 -4 7 16.50 6.30 -10 -4 -7 15.20 4.20 10 -4 7 16.00 3.60 10 -4 7 18.60 4.00 -10 -4 -7 13.00 3.60 10 4 8 129.89 7.50 10 4 8 102.79 11.00 10 4 8 129.89 8.60 10 4 8 112.79 7.40 10 4 8 104.89 7.60 -10 4 -8 109.59 8.50 10 -4 8 118.09 12.10 10 -4 8 111.99 8.00 10 -4 8 115.89 8.00 -10 -4 -8 112.29 8.10 -10 -4 -8 120.29 7.80 10 -4 8 114.49 7.70 -10 4 -9 45.20 5.60 10 4 9 49.00 5.00 10 4 9 53.99 5.10 10 4 9 43.50 4.90 10 4 9 35.20 4.10 10 -4 9 45.50 5.00 -10 -4 -9 49.60 6.20 10 -4 9 41.40 4.90 10 -4 9 37.00 4.70 -10 -4 -9 45.70 5.30 10 4 10 44.50 4.00 10 4 10 39.20 4.10 -10 4 -10 40.20 5.10 -10 -4 -10 39.40 4.30 10 -4 10 47.40 4.90 10 -4 10 34.90 4.00 -10 -4 -10 42.90 5.10 -10 4 -11 -0.10 1.70 10 4 11 4.80 2.00 10 4 11 -0.30 1.20 10 -4 11 0.00 1.10 -10 5 12 -0.50 1.40 -10 5 12 -0.30 1.60 -10 5 12 0.10 1.70 -10 5 12 -0.90 1.70 -10 -5 12 3.70 1.70 -10 -5 12 1.30 1.80 -10 -5 12 1.00 1.50 -10 -5 12 -2.30 1.40 -10 5 11 9.70 3.10 -10 5 11 12.60 2.90 -10 -5 11 13.00 3.00 -10 -5 11 8.10 2.90 10 -5 -11 10.70 3.10 -10 -5 11 10.50 3.80 -10 -5 11 14.10 3.20 -10 5 10 92.19 7.20 -10 5 10 90.59 6.60 -10 5 10 93.39 7.20 -10 5 10 80.69 7.00 -10 5 10 96.19 7.40 -10 -5 10 85.69 6.70 -10 -5 10 87.09 7.10 -10 -5 10 91.29 6.60 -10 -5 10 89.59 6.30 -10 -5 10 80.99 6.80 -10 -5 10 86.99 7.80 -10 5 9 32.80 5.30 -10 5 9 36.90 5.50 -10 5 9 29.40 6.40 -10 5 9 31.10 4.70 -10 5 9 25.60 4.90 -10 5 9 33.90 5.40 10 5 -9 28.30 6.60 -10 -5 9 30.40 5.10 -10 -5 9 34.90 5.80 -10 -5 9 30.60 4.90 -10 -5 9 31.60 4.40 -10 -5 9 37.30 5.30 -10 -5 9 22.50 5.00 -10 5 8 104.49 13.00 -10 5 8 84.89 7.40 -10 5 8 85.99 12.50 -10 5 8 80.39 10.80 -10 5 8 91.99 7.10 -10 5 8 80.99 6.90 10 5 -8 78.59 9.60 -10 5 8 90.19 7.90 -10 -5 8 72.39 7.70 -10 -5 8 82.79 7.50 -10 -5 8 87.59 6.80 10 5 -7 0.30 4.90 -10 5 7 1.70 2.70 -10 5 7 -0.60 2.60 -10 5 7 3.50 3.30 -10 5 7 8.70 4.10 -10 5 7 -0.50 2.60 -10 5 7 6.80 3.40 -10 5 7 3.30 2.90 -10 -5 7 -7.20 3.10 -10 -5 7 0.40 3.00 -10 -5 7 -3.10 2.20 -10 -5 7 14.20 4.30 -10 -5 7 -3.00 2.10 -10 -5 7 1.00 2.40 -10 5 6 112.99 9.50 -10 5 6 120.19 9.50 -10 5 6 116.29 9.30 -10 5 6 132.79 9.30 -10 5 6 122.39 8.70 -10 5 6 94.19 8.80 -10 5 6 103.29 8.20 10 5 -6 117.29 11.30 -10 5 6 108.39 14.40 -10 -5 6 105.89 8.80 -10 -5 6 106.69 8.60 -10 -5 6 119.79 8.10 -10 -5 6 121.89 9.20 -10 -5 6 112.69 8.90 -10 -5 6 114.79 9.30 -10 -5 6 104.89 7.70 -10 5 5 32.40 9.30 -10 5 5 60.69 6.80 -10 5 5 50.79 6.00 -10 5 5 36.00 6.30 -10 5 5 43.90 6.60 10 5 -5 38.20 7.70 -10 5 5 48.20 6.40 -10 5 5 41.60 6.50 -10 5 5 41.50 6.70 -10 -5 5 47.60 5.40 -10 -5 5 53.69 6.80 -10 -5 5 39.20 6.20 -10 -5 5 49.80 6.60 -10 -5 5 24.50 12.20 -10 -5 5 49.40 5.70 -10 -5 5 41.50 6.60 -10 -5 5 39.10 6.40 -10 -5 5 42.50 6.80 -10 5 4 23.10 5.00 -10 5 4 26.70 5.70 -10 5 4 26.30 5.40 -10 5 4 17.00 4.70 -10 5 4 30.70 5.90 -10 5 4 38.00 5.50 10 5 -4 33.40 7.50 -10 5 4 21.80 7.20 -10 -5 4 34.10 5.00 -10 -5 4 25.80 4.60 -10 -5 4 29.10 5.10 -10 -5 4 30.60 5.70 -10 -5 4 30.70 5.40 -10 -5 4 30.70 9.00 -10 -5 4 34.40 5.80 -10 -5 4 26.80 5.90 10 5 -3 260.67 16.70 -10 5 3 272.87 13.40 -10 5 3 248.28 14.10 -10 5 3 276.27 14.20 -10 5 3 278.87 14.60 -10 5 3 280.87 13.80 -10 5 3 256.07 19.20 10 5 -3 250.87 13.40 -10 -5 3 271.77 13.10 -10 -5 3 261.67 13.40 -10 -5 3 261.97 13.70 -10 -5 3 255.27 16.30 -10 -5 3 266.57 12.60 -10 -5 3 252.77 13.30 -10 -5 3 250.57 18.50 -10 -5 3 254.07 13.60 -10 5 2 109.59 9.80 -10 5 2 94.29 12.60 -10 5 2 115.89 8.30 10 5 -2 131.19 11.20 -10 5 2 102.89 11.40 -10 5 2 116.49 10.10 10 5 -2 112.89 9.10 10 5 -2 134.59 9.80 -10 5 2 129.99 8.90 -10 -5 2 102.99 8.60 -10 -5 2 140.99 9.60 -10 -5 2 114.19 12.80 -10 -5 2 102.29 12.30 -10 -5 2 129.09 8.50 -10 -5 2 121.19 8.00 -10 -5 2 132.49 9.90 10 5 -1 14.00 4.50 -10 5 1 12.30 3.70 -10 5 1 20.40 7.10 10 5 -1 2.40 4.20 10 5 -1 10.80 4.40 -10 5 1 7.30 4.10 -10 5 1 9.10 4.10 -10 5 1 14.40 5.10 -10 -5 1 15.80 4.40 -10 -5 1 11.40 3.70 -10 -5 1 1.60 6.90 -10 -5 1 8.20 3.60 10 -5 -1 11.30 3.60 -10 -5 1 6.00 5.90 10 5 0 136.09 9.50 -10 5 0 118.49 10.70 10 5 0 125.69 11.30 -10 5 0 145.09 14.50 -10 5 0 118.79 10.20 10 5 0 136.29 9.60 -10 5 0 135.39 9.70 -10 5 0 142.59 10.50 -10 -5 0 130.09 9.60 -10 -5 0 141.29 9.20 -10 -5 0 137.99 9.60 -10 -5 0 138.49 9.90 -10 -5 0 155.18 14.40 10 -5 0 140.09 8.90 10 5 1 130.39 11.30 -10 5 -1 121.19 9.60 10 5 1 73.69 12.10 10 5 1 98.29 8.20 10 5 1 107.59 8.60 10 -5 1 106.19 9.30 -10 -5 -1 123.79 9.30 -10 -5 -1 104.09 7.80 -10 -5 -1 115.19 12.70 -10 -5 -1 118.99 8.70 10 -5 1 109.79 8.20 10 -5 1 107.29 7.90 10 5 2 136.59 9.20 -10 5 -2 148.29 10.90 10 5 2 141.69 9.50 10 5 2 131.39 11.60 10 5 2 150.38 9.90 -10 -5 -2 133.79 11.30 -10 -5 -2 149.99 14.40 -10 -5 -2 130.59 9.50 10 -5 2 136.29 9.30 10 -5 2 123.79 9.50 -10 -5 -2 151.18 10.00 10 5 3 917.11 32.70 10 5 3 953.20 38.30 -10 5 -3 1021.60 35.00 10 5 3 944.91 34.00 10 5 3 953.40 32.80 -10 5 -3 910.21 32.40 10 -5 3 964.70 33.40 -10 -5 -3 966.80 42.10 -10 -5 -3 922.11 33.00 10 -5 3 985.80 32.80 -10 -5 -3 957.80 33.30 -10 -5 -3 989.10 34.10 10 -5 3 979.40 32.90 -10 5 -4 156.08 11.20 10 5 4 181.78 10.10 10 5 4 153.78 10.30 10 5 4 163.48 12.80 10 5 4 156.78 9.70 10 -5 4 149.88 9.20 10 -5 4 177.28 10.40 10 -5 4 155.38 9.70 -10 -5 -4 148.09 10.10 -10 -5 -4 170.08 10.40 -10 -5 -4 157.28 9.80 -10 -5 -4 155.08 15.70 10 5 5 151.08 12.50 10 5 5 155.48 9.30 10 5 5 143.39 9.70 -10 5 -5 156.48 10.70 10 -5 5 156.88 9.80 -10 -5 -5 141.39 9.70 -10 -5 -5 157.28 9.80 -10 -5 -5 150.68 9.60 10 -5 5 117.89 10.50 10 5 6 157.28 9.10 -10 5 -6 148.59 10.50 10 5 6 141.69 9.40 10 5 6 167.38 13.00 10 5 6 149.69 9.60 -10 -5 -6 128.49 9.60 -10 -5 -6 156.88 9.40 -10 -5 -6 168.48 10.00 10 -5 6 150.78 9.50 10 -5 6 134.29 8.50 10 -5 6 155.68 9.20 10 5 7 0.30 5.10 10 5 7 5.00 2.30 10 5 7 -0.90 2.30 -10 5 -7 1.00 3.00 -10 -5 -7 2.00 2.60 10 -5 7 1.60 2.70 10 -5 7 -1.90 2.10 -10 -5 -7 -5.80 2.20 10 5 8 6.30 2.90 10 5 8 3.90 2.50 10 5 8 4.70 2.30 -10 5 -8 6.80 3.30 -10 -5 -8 5.80 3.00 10 -5 8 7.10 2.50 -10 -5 -8 1.00 2.10 10 5 9 19.60 3.50 -10 5 -9 29.00 4.60 10 5 9 20.20 3.20 10 5 9 17.20 3.90 10 -5 9 25.50 3.60 -10 -5 -9 17.40 3.30 -10 -5 -9 15.10 3.10 -10 5 -10 16.40 4.20 10 5 10 10.10 2.10 10 5 10 21.50 3.00 10 -5 10 18.40 2.90 -10 -5 -10 34.50 4.70 -10 -5 -10 19.80 3.10 -10 6 12 16.80 2.60 -10 6 12 10.10 2.20 -10 6 12 20.30 2.80 10 6 -12 16.70 3.60 -10 -6 12 19.00 2.80 -10 -6 12 17.90 2.30 -10 -6 12 13.50 3.00 -10 6 11 -0.10 1.50 -10 6 11 0.00 1.60 -10 6 11 1.60 1.60 -10 6 11 -0.40 2.10 -10 -6 11 -1.30 1.30 -10 -6 11 1.10 1.70 -10 -6 11 0.10 1.70 -10 -6 11 2.00 1.80 -10 6 10 38.00 6.50 -10 6 10 36.60 4.80 -10 6 10 27.40 6.80 -10 -6 10 33.10 4.40 -10 -6 10 54.19 7.50 10 -6 -10 33.10 4.40 -10 -6 10 21.00 3.70 -10 -6 10 31.20 3.90 -10 6 9 73.89 6.70 -10 6 9 73.39 6.50 -10 6 9 79.09 6.50 -10 6 9 83.49 6.90 -10 6 9 72.89 6.00 -10 -6 9 71.89 6.50 -10 -6 9 65.89 5.40 10 -6 -9 63.59 5.70 -10 -6 9 73.69 5.80 -10 -6 9 75.89 6.40 -10 -6 9 63.09 7.20 -10 -6 9 71.29 6.30 -10 6 8 12.70 3.60 -10 6 8 10.30 3.40 10 6 -8 7.00 5.20 -10 6 8 7.80 2.90 -10 6 8 10.50 3.30 -10 6 8 8.20 3.30 -10 6 8 10.60 3.20 -10 -6 8 12.10 3.80 -10 -6 8 8.70 3.20 -10 -6 8 9.00 2.80 10 -6 -8 9.60 3.30 -10 -6 8 6.30 2.60 -10 -6 8 9.10 3.00 -10 -6 8 11.30 3.20 -10 6 7 57.69 6.80 -10 6 7 65.29 6.70 -10 6 7 59.59 6.00 -10 6 7 56.89 6.30 -10 6 7 65.79 6.80 -10 6 7 73.59 7.20 10 6 -7 61.09 8.80 -10 -6 7 72.89 7.10 10 -6 -7 54.89 6.00 -10 -6 7 70.69 6.70 -10 -6 7 71.59 6.10 -10 -6 7 63.59 6.60 -10 -6 7 58.19 6.90 -10 -6 7 62.89 6.10 -10 6 6 6.60 3.40 10 6 -6 6.30 4.20 -10 6 6 5.30 3.10 -10 6 6 3.60 3.00 -10 6 6 -0.10 2.70 10 6 -6 4.50 3.70 -10 6 6 2.10 2.90 -10 6 6 3.60 5.50 10 -6 -6 6.20 2.90 -10 -6 6 4.00 2.70 -10 -6 6 -0.50 2.50 -10 -6 6 4.50 3.30 -10 -6 6 5.20 3.10 -10 -6 6 3.20 3.10 -10 -6 6 2.10 2.90 -10 6 5 11.60 3.80 10 6 -5 14.80 5.70 -10 6 5 14.80 4.10 -10 6 5 17.70 4.00 -10 6 5 13.70 4.20 -10 6 5 9.30 3.70 -10 6 5 12.30 4.30 10 6 -5 6.20 4.10 -10 -6 5 13.10 3.90 -10 -6 5 14.00 3.80 -10 -6 5 6.40 3.00 -10 -6 5 11.70 4.00 10 -6 -5 8.10 3.30 -10 -6 5 14.20 3.60 -10 6 4 189.38 11.90 10 6 -4 179.68 14.10 10 6 -4 194.08 11.30 -10 6 4 217.68 11.90 -10 6 4 200.78 12.10 -10 6 4 212.68 12.20 -10 6 4 190.78 18.40 -10 6 4 219.38 11.70 -10 6 4 206.68 12.30 -10 -6 4 220.48 11.80 -10 -6 4 196.08 10.60 -10 -6 4 203.68 11.90 -10 -6 4 203.48 10.70 -10 -6 4 205.48 11.70 -10 -6 4 197.08 11.00 -10 -6 4 211.38 12.10 10 -6 -4 214.18 11.80 -10 6 3 117.39 8.50 -10 6 3 112.39 8.60 10 6 -3 119.59 8.70 -10 6 3 107.29 15.30 10 6 -3 99.09 12.20 -10 6 3 100.19 9.00 -10 6 3 115.09 9.50 -10 6 3 100.69 8.90 -10 6 3 103.09 8.90 -10 -6 3 115.39 8.10 -10 -6 3 103.39 7.90 -10 -6 3 115.49 7.80 -10 -6 3 116.49 8.60 10 -6 -3 126.59 8.70 -10 -6 3 86.19 15.10 -10 -6 3 111.49 8.60 -10 -6 3 111.79 8.80 -10 -6 3 106.59 9.10 -10 6 2 85.79 8.60 -10 6 2 72.09 7.60 -10 6 2 98.79 8.60 -10 6 2 90.89 22.70 10 6 -2 82.49 7.90 -10 6 2 84.49 9.00 10 6 -2 87.09 10.10 10 6 -2 94.89 8.20 -10 6 2 95.79 8.80 -10 -6 2 81.89 7.70 -10 -6 2 93.89 8.00 -10 -6 2 92.49 8.40 -10 -6 2 77.59 7.10 10 -6 -2 97.09 7.70 -10 -6 2 92.49 7.60 -10 -6 2 93.89 18.80 -10 -6 2 95.49 8.00 -10 6 1 26.00 5.20 -10 6 1 5.00 5.10 -10 6 1 18.80 5.20 -10 6 1 12.30 4.60 10 6 -1 23.50 5.00 10 6 -1 20.70 4.90 10 6 -1 14.70 5.40 -10 -6 1 18.90 4.20 10 -6 -1 22.00 4.60 -10 -6 1 21.20 4.50 -10 -6 1 23.40 4.90 -10 -6 1 22.50 4.70 -10 -6 1 17.80 4.20 10 6 0 0.30 3.40 10 6 0 -2.50 4.10 -10 6 0 4.30 3.90 -10 6 0 1.60 3.60 10 6 0 2.10 3.00 -10 -6 0 1.70 2.90 -10 -6 0 -2.10 2.80 -10 -6 0 -2.40 3.60 10 -6 0 0.90 2.60 -10 -6 0 -4.40 9.70 10 -6 0 4.30 3.10 -10 -6 0 10.10 4.00 10 6 1 63.39 8.50 10 6 1 79.89 7.20 -10 6 -1 65.49 7.50 10 6 1 65.39 7.00 10 6 1 65.99 6.70 -10 -6 -1 52.89 10.50 -10 -6 -1 72.79 11.90 10 -6 1 74.89 7.00 -10 -6 -1 72.49 6.80 -10 -6 -1 66.29 7.10 10 -6 1 67.49 6.50 -10 -6 -1 69.59 7.10 10 6 2 227.88 12.50 10 6 2 214.28 11.50 -10 6 -2 204.18 12.10 10 6 2 219.18 11.50 -10 6 -2 225.48 13.10 10 6 2 218.18 15.20 10 -6 2 251.27 12.20 -10 -6 -2 237.38 12.10 -10 -6 -2 211.48 12.20 10 -6 2 229.88 11.90 -10 -6 -2 214.68 19.10 -10 -6 -2 233.98 12.40 10 6 3 122.09 8.30 -10 6 -3 121.39 9.60 10 6 3 111.09 8.60 10 6 3 107.69 11.10 -10 -6 -3 122.99 8.60 -10 -6 -3 118.89 8.70 -10 -6 -3 115.09 9.00 10 -6 3 114.39 8.00 10 -6 3 112.69 8.80 10 -6 3 110.19 8.00 -10 6 -4 116.59 8.80 10 6 4 107.19 10.80 10 6 4 123.39 11.30 10 6 4 90.99 9.60 -10 6 -4 115.89 10.70 10 -6 4 124.39 8.30 -10 -6 -4 126.89 10.50 -10 -6 -4 129.39 10.70 10 -6 4 124.09 8.50 10 -6 4 113.99 8.00 -10 -6 -4 131.69 8.70 -10 6 -5 68.29 7.40 10 6 5 58.09 6.10 10 6 5 61.79 5.90 10 6 5 64.19 8.90 -10 6 -5 61.29 6.90 -10 -6 -5 63.59 6.60 10 -6 5 69.09 6.40 10 -6 5 64.09 5.80 10 -6 5 58.99 6.10 -10 -6 -5 75.29 6.50 -10 -6 -5 65.19 6.60 10 6 6 54.19 5.40 10 6 6 44.50 5.40 10 6 6 32.50 8.60 -10 6 -6 49.60 6.40 -10 6 -6 50.99 6.20 10 -6 6 52.69 5.40 -10 -6 -6 51.49 5.90 10 -6 6 57.69 5.50 -10 -6 -6 48.20 6.40 -10 -6 -6 53.29 5.70 -10 6 -7 176.68 9.40 10 6 7 165.68 9.50 10 6 7 169.68 9.10 -10 6 -7 184.38 10.50 10 -6 7 192.68 11.60 -10 -6 -7 185.88 9.90 -10 -6 -7 184.68 9.60 10 6 8 16.30 3.00 10 6 8 10.60 2.80 -10 6 -8 17.50 3.70 10 -6 8 22.20 3.50 -10 -6 -8 30.10 4.30 -10 -6 -8 29.70 4.10 -10 6 -9 -1.60 1.60 -10 6 -9 -0.40 2.20 10 6 9 0.80 1.40 10 6 9 0.80 1.70 -10 -6 -9 2.30 2.20 10 -6 9 1.30 1.40 10 7 -11 6.00 1.80 -10 7 11 8.50 1.90 -10 7 11 9.80 2.00 -10 7 11 8.20 1.90 -10 -7 11 10.30 1.90 -10 -7 11 4.00 1.50 -10 -7 11 4.90 1.30 -10 7 10 0.80 1.70 -10 7 10 -1.50 1.60 -10 7 10 -0.50 1.40 -10 7 10 -1.00 1.30 -10 -7 10 0.40 1.60 -10 -7 10 0.00 1.20 -10 -7 10 -0.80 1.50 -10 -7 10 0.40 1.60 -10 7 9 15.70 3.10 -10 7 9 14.70 4.80 -10 7 9 12.80 3.00 -10 7 9 12.30 4.30 -10 7 9 11.10 2.70 -10 -7 9 15.90 3.70 -10 -7 9 12.10 2.80 10 -7 -9 12.70 2.70 -10 -7 9 15.70 2.90 -10 -7 9 16.20 2.80 10 -7 -9 12.80 3.20 -10 -7 9 11.30 3.40 -10 7 8 27.90 4.40 -10 7 8 17.60 3.90 -10 7 8 15.00 3.30 -10 7 8 23.80 4.30 -10 7 8 11.60 3.20 10 -7 -8 15.20 3.60 -10 -7 8 14.50 3.10 -10 -7 8 23.80 3.60 -10 -7 8 18.70 3.40 -10 -7 8 13.10 3.30 -10 -7 8 21.70 3.40 10 -7 -8 18.20 3.10 -10 7 7 14.00 3.40 -10 7 7 16.20 4.00 -10 7 7 12.20 3.30 -10 7 7 6.70 3.10 10 7 -7 5.40 4.60 10 7 -7 17.30 4.20 -10 7 7 13.70 3.50 -10 -7 7 8.50 2.80 -10 -7 7 14.80 3.80 -10 -7 7 10.50 2.70 -10 -7 7 8.40 2.90 -10 -7 7 6.90 2.80 10 -7 -7 14.10 3.60 -10 7 6 452.25 19.00 10 7 -6 426.36 22.70 -10 7 6 495.55 19.90 -10 7 6 443.16 18.60 -10 7 6 462.45 19.40 10 7 -6 467.95 17.80 -10 7 6 479.15 19.10 10 -7 -6 458.95 18.80 -10 -7 6 454.35 17.50 -10 -7 6 475.55 18.20 -10 -7 6 460.65 18.60 -10 -7 6 483.85 18.90 -10 -7 6 467.45 18.90 -10 7 5 119.29 8.80 -10 7 5 105.99 8.30 10 7 -5 102.39 7.70 10 7 -5 85.89 10.00 -10 7 5 101.99 8.20 -10 7 5 114.99 8.30 -10 -7 5 111.29 8.20 -10 -7 5 129.39 9.00 -10 -7 5 105.79 7.90 10 -7 -5 114.79 8.20 -10 -7 5 104.39 7.10 10 7 -4 344.77 15.10 -10 7 4 374.46 16.70 10 7 -4 343.97 19.70 -10 7 4 353.96 16.00 -10 7 4 362.06 16.10 10 7 -4 333.57 16.00 -10 7 4 334.67 16.30 -10 7 4 344.07 15.60 10 -7 -4 362.36 16.20 -10 -7 4 361.86 14.40 -10 -7 4 374.06 16.10 -10 -7 4 329.57 14.70 -10 -7 4 373.96 15.80 -10 -7 4 365.76 16.20 10 7 -3 336.27 14.90 -10 7 3 345.87 15.50 -10 7 3 332.27 15.60 10 7 -3 340.37 16.20 10 7 -3 327.07 19.20 -10 7 3 344.17 15.60 -10 -7 3 348.67 16.70 10 -7 -3 360.06 15.80 -10 -7 3 312.97 15.00 -10 -7 3 342.87 14.00 10 -7 -3 365.16 16.00 -10 -7 3 364.16 14.80 -10 -7 3 323.67 17.40 -10 -7 3 321.17 18.10 -10 7 2 18.10 5.00 10 7 -2 13.10 4.10 -10 7 2 5.60 3.70 -10 7 2 16.20 4.90 -10 7 2 2.60 5.40 -10 7 2 10.20 3.80 10 7 -2 11.60 5.10 -10 -7 2 13.00 4.10 -10 -7 2 7.00 3.90 -10 -7 2 12.10 4.40 -10 -7 2 10.40 3.80 10 -7 -2 9.80 3.40 10 -7 -2 14.70 3.60 10 7 -1 47.30 8.70 10 7 -1 50.69 6.20 10 7 -1 62.39 7.70 -10 7 1 46.20 6.60 -10 7 1 45.50 9.10 -10 -7 1 67.89 9.00 -10 -7 1 55.09 6.30 10 -7 -1 49.00 5.80 -10 -7 1 43.30 6.10 10 -7 -1 58.59 6.10 10 7 0 38.40 5.50 10 7 0 43.40 8.10 10 7 0 29.70 4.50 -10 7 0 49.80 6.60 10 -7 0 34.30 5.00 10 -7 0 40.70 5.40 -10 -7 0 30.80 5.20 -10 -7 0 44.10 5.90 -10 -7 0 32.00 5.00 10 7 1 27.50 7.70 10 7 1 22.20 6.10 -10 7 -1 22.40 5.40 10 7 1 23.00 4.40 10 7 1 21.60 4.50 -10 -7 -1 22.60 4.90 -10 -7 -1 26.50 7.60 10 -7 1 24.90 4.70 -10 -7 -1 34.10 5.30 10 -7 1 15.90 4.00 -10 -7 -1 23.90 4.80 -10 7 -2 279.97 13.60 10 7 2 297.87 17.80 10 7 2 313.17 14.70 10 7 2 319.67 14.10 -10 7 -2 315.47 15.80 -10 -7 -2 318.47 14.60 10 -7 2 328.97 14.50 -10 -7 -2 303.57 14.00 10 -7 2 322.57 14.30 -10 -7 -2 318.37 14.70 10 7 3 36.10 5.00 10 7 3 23.40 4.20 10 7 3 22.20 6.60 -10 7 -3 17.40 4.20 -10 7 -3 26.40 5.00 10 -7 3 32.20 4.70 -10 -7 -3 25.50 4.50 -10 -7 -3 21.70 4.40 -10 -7 -3 28.30 4.80 10 -7 3 25.60 5.00 10 7 4 0.50 2.00 10 7 4 1.00 2.40 10 7 4 -3.40 5.00 -10 7 -4 2.90 2.90 -10 7 -4 3.40 3.40 -10 -7 -4 3.20 2.40 10 -7 4 0.80 2.30 -10 -7 -4 2.20 2.60 10 -7 4 1.20 2.70 -10 -7 -4 -2.90 2.40 -10 7 -5 18.50 3.90 10 7 5 27.60 4.50 10 7 5 25.40 4.00 -10 7 -5 30.50 5.10 -10 -7 -5 17.10 3.70 10 -7 5 28.00 4.10 10 -7 5 22.70 4.80 -10 -7 -5 34.60 4.70 10 -7 5 22.00 4.00 -10 -7 -5 30.30 5.00 -10 7 -6 96.89 6.70 10 7 6 92.59 8.30 10 7 6 98.99 6.90 -10 7 -6 105.89 7.60 -10 -7 -6 104.49 7.10 -10 -7 -6 99.39 7.10 -10 -7 -6 101.19 6.70 10 -7 6 96.89 5.80 -10 7 -7 16.70 3.20 -10 7 -7 16.20 3.20 10 7 7 22.40 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6.60 -11 -4 10 82.79 6.50 -11 -4 10 89.69 7.00 -11 -4 10 102.19 7.60 -11 -4 10 82.39 6.10 -11 4 9 199.68 14.30 -11 4 9 150.38 9.90 -11 4 9 155.58 9.00 11 4 -9 152.08 12.90 -11 4 9 168.38 10.30 -11 4 9 167.38 10.50 -11 4 9 149.88 10.10 -11 -4 9 159.98 10.00 -11 -4 9 168.28 11.90 -11 -4 9 155.78 8.80 -11 -4 9 167.58 9.90 -11 -4 9 157.08 9.50 -11 4 8 14.30 4.30 -11 4 8 16.30 6.10 -11 4 8 15.10 3.70 -11 4 8 14.70 6.80 11 4 -8 19.30 6.20 -11 4 8 14.10 6.50 -11 4 8 16.40 4.00 -11 -4 8 11.40 3.30 -11 -4 8 13.00 3.60 -11 -4 8 12.60 4.90 -11 -4 8 17.90 4.40 -11 -4 8 13.30 3.60 -11 -4 8 10.60 4.90 -11 4 7 76.49 6.80 -11 4 7 58.39 7.00 -11 4 7 75.09 7.50 -11 4 7 70.79 7.30 -11 4 7 75.79 6.90 -11 4 7 69.99 7.60 11 4 -7 65.39 16.10 -11 -4 7 56.59 5.90 -11 -4 7 59.69 7.20 -11 -4 7 93.89 10.60 -11 -4 7 62.59 6.20 -11 -4 7 83.19 7.40 -11 -4 7 73.99 7.60 -11 -4 7 72.39 7.70 -11 -4 7 72.29 7.00 -11 4 6 20.00 4.60 -11 4 6 24.00 4.70 -11 4 6 14.80 4.50 -11 4 6 16.90 4.40 -11 4 6 22.60 4.60 -11 4 6 18.90 5.00 11 4 -6 25.80 6.50 -11 4 6 29.90 6.00 -11 4 6 19.30 7.60 -11 -4 6 13.20 4.20 -11 -4 6 15.90 4.40 -11 -4 6 19.90 4.00 -11 -4 6 15.00 3.90 -11 -4 6 20.30 10.60 -11 -4 6 25.20 5.20 -11 -4 6 24.90 5.50 -11 -4 6 21.70 5.50 -11 4 5 108.69 8.20 -11 4 5 122.59 9.10 -11 4 5 105.39 13.30 -11 4 5 108.89 8.30 -11 4 5 112.29 9.00 -11 4 5 114.59 9.60 -11 4 5 116.49 9.50 11 4 -5 124.79 11.30 -11 4 5 137.69 10.10 -11 -4 5 103.99 14.00 -11 -4 5 103.89 8.40 -11 -4 5 110.69 7.80 -11 -4 5 107.09 8.80 -11 -4 5 88.99 9.00 -11 -4 5 111.39 9.10 -11 -4 5 116.79 8.10 -11 -4 5 110.89 8.60 -11 4 4 633.64 24.90 -11 4 4 600.54 23.90 -11 4 4 643.64 23.90 11 4 -4 611.34 28.50 -11 4 4 560.84 31.40 -11 4 4 611.64 24.80 -11 4 4 625.64 25.20 -11 -4 4 632.14 24.10 -11 -4 4 570.74 30.60 -11 -4 4 619.74 24.30 -11 -4 4 607.54 22.70 -11 -4 4 643.54 23.50 -11 -4 4 630.24 24.50 -11 -4 4 641.44 24.50 -11 4 3 35.00 6.10 11 4 -3 31.30 5.80 -11 4 3 42.20 6.60 -11 4 3 38.80 5.70 -11 4 3 31.50 5.10 -11 4 3 41.40 5.90 -11 4 3 48.50 7.70 -11 4 3 34.20 5.80 -11 4 3 34.50 8.40 11 4 -3 38.20 7.70 -11 -4 3 34.70 5.40 -11 -4 3 31.00 5.30 -11 -4 3 37.70 6.30 -11 -4 3 30.20 6.10 -11 -4 3 33.30 7.90 -11 -4 3 40.90 9.80 -11 -4 3 38.70 5.90 -11 -4 3 31.70 5.10 -11 4 2 124.59 13.50 -11 4 2 134.89 9.40 11 4 -2 116.49 10.80 -11 4 2 131.69 8.70 -11 4 2 119.89 10.20 11 4 -2 107.69 8.80 -11 4 2 111.89 10.50 -11 4 2 125.79 8.70 -11 -4 2 119.29 8.80 -11 -4 2 119.79 9.30 -11 -4 2 120.89 9.20 -11 -4 2 109.89 12.90 -11 -4 2 115.99 9.00 -11 -4 2 116.59 8.00 -11 -4 2 132.19 8.80 -11 4 1 414.26 25.90 -11 4 1 293.87 21.10 11 4 -1 411.06 21.40 11 4 -1 412.36 17.70 -11 4 1 381.36 17.20 -11 4 1 365.36 23.00 -11 4 1 384.86 16.70 -11 4 1 385.16 16.90 -11 -4 1 369.56 16.70 -11 -4 1 398.06 16.90 -11 -4 1 420.56 18.00 -11 -4 1 370.96 17.20 -11 -4 1 411.76 23.60 11 -4 -1 375.16 16.70 -11 -4 1 394.06 17.30 11 4 0 181.28 13.80 -11 4 0 206.78 17.10 -11 4 0 187.18 12.00 -11 4 0 202.28 11.20 -11 4 0 238.18 18.20 11 4 0 201.88 11.70 -11 4 0 194.18 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6.70 -11 -5 7 49.80 6.20 -11 -5 7 56.59 5.50 -11 -5 7 55.09 6.60 -11 -5 7 55.89 5.70 -11 -5 7 48.90 6.10 -11 5 6 23.80 4.70 -11 5 6 24.80 4.90 -11 5 6 27.80 5.30 -11 5 6 19.50 4.80 11 5 -6 29.20 7.50 -11 5 6 17.20 4.90 -11 5 6 25.70 5.10 -11 -5 6 23.50 4.40 -11 -5 6 21.50 3.90 -11 -5 6 19.90 5.30 -11 -5 6 23.90 4.70 -11 -5 6 22.10 4.40 -11 -5 6 14.50 5.20 -11 -5 6 30.50 4.70 -11 5 5 10.30 3.80 11 5 -5 9.60 5.50 -11 5 5 11.60 4.00 -11 5 5 16.60 4.30 -11 5 5 7.40 3.60 -11 5 5 11.10 4.50 -11 5 5 14.60 4.20 -11 -5 5 17.10 4.40 -11 -5 5 11.20 3.90 -11 -5 5 15.70 4.30 -11 -5 5 8.70 3.10 -11 -5 5 10.20 3.50 -11 -5 5 11.30 3.70 -11 -5 5 9.00 5.10 11 5 -4 832.52 36.40 11 5 -4 917.01 32.20 -11 5 4 910.41 32.40 -11 5 4 926.11 33.20 -11 5 4 790.62 40.00 -11 5 4 895.31 31.70 -11 5 4 878.21 31.80 -11 5 4 911.71 32.50 -11 5 4 922.91 31.60 -11 -5 4 891.41 30.60 -11 -5 4 775.72 38.90 -11 -5 4 885.91 32.10 -11 -5 4 871.91 30.10 -11 -5 4 894.71 30.90 -11 -5 4 927.11 32.00 -11 -5 4 919.21 31.80 -11 -5 4 911.61 32.00 -11 5 3 530.65 21.80 -11 5 3 546.15 21.60 -11 5 3 543.55 21.30 -11 5 3 502.65 21.50 11 5 -3 536.25 33.10 -11 5 3 565.74 22.70 11 5 -3 559.74 22.00 -11 5 3 537.65 21.70 -11 -5 3 488.65 19.80 -11 -5 3 519.55 21.20 -11 -5 3 508.35 19.60 -11 -5 3 535.15 21.50 -11 -5 3 561.54 20.80 -11 -5 3 535.15 21.50 -11 -5 3 496.15 21.30 -11 -5 3 479.85 28.60 11 5 -2 1.50 3.60 -11 5 2 0.80 3.50 -11 5 2 0.30 3.40 -11 5 2 2.10 3.10 -11 5 2 6.00 4.20 -11 5 2 6.00 7.40 11 5 -2 2.60 3.30 -11 5 2 -0.50 2.60 -11 5 2 2.60 4.00 -11 -5 2 2.40 3.00 -11 -5 2 -2.60 2.90 -11 -5 2 -1.10 3.40 11 -5 -2 1.50 2.20 -11 -5 2 0.70 7.50 -11 -5 2 -5.90 3.50 -11 -5 2 1.20 3.50 -11 -5 2 2.10 2.60 -11 5 1 16.10 8.60 11 5 -1 5.30 4.40 -11 5 1 9.50 4.40 -11 5 1 8.50 4.30 11 5 -1 7.10 3.50 -11 5 1 5.10 3.20 -11 5 1 2.00 3.60 -11 5 1 4.70 4.00 11 5 -1 4.60 4.40 11 -5 -1 6.80 3.40 -11 -5 1 10.10 3.90 -11 -5 1 10.00 4.40 -11 -5 1 12.80 7.70 -11 -5 1 10.20 3.70 -11 -5 1 7.00 3.10 -11 -5 1 2.50 3.20 -11 5 0 25.00 5.50 -11 5 0 18.90 5.60 -11 5 0 16.60 4.70 -11 5 0 20.30 5.30 11 5 0 16.00 4.30 11 5 0 29.90 5.00 11 5 0 17.60 5.70 -11 -5 0 23.40 4.60 -11 -5 0 19.90 5.30 11 -5 0 27.90 4.60 -11 -5 0 36.30 6.10 -11 -5 0 15.70 4.10 11 5 1 611.64 24.00 11 5 1 564.34 22.20 11 5 1 578.34 33.60 -11 5 -1 603.44 24.10 11 5 1 594.24 23.00 11 -5 1 627.74 23.30 -11 -5 -1 593.84 23.60 11 -5 1 609.34 23.00 11 -5 1 633.64 23.20 -11 -5 -1 615.54 23.60 -11 -5 -1 606.44 23.00 11 5 2 204.08 11.10 11 5 2 187.68 14.20 11 5 2 223.68 12.00 11 5 2 204.48 11.20 -11 5 -2 195.68 12.20 -11 -5 -2 199.48 11.60 11 -5 2 191.98 11.20 -11 -5 -2 192.88 11.10 11 -5 2 212.18 11.10 -11 -5 -2 200.58 11.80 11 -5 2 217.58 11.00 -11 -5 -2 176.08 16.80 11 5 3 42.90 6.20 11 5 3 43.40 5.90 -11 5 -3 45.70 6.80 11 5 3 55.19 6.20 -11 -5 -3 60.59 6.90 11 -5 3 62.09 6.20 11 -5 3 52.09 6.20 -11 -5 -3 51.89 6.00 -11 -5 -3 54.29 6.60 11 -5 3 45.30 5.70 11 5 4 85.69 6.90 11 5 4 76.89 6.80 11 5 4 87.89 9.70 -11 5 -4 85.29 10.20 11 5 4 71.49 7.00 -11 -5 -4 77.69 6.90 11 -5 4 91.59 6.90 -11 -5 -4 83.59 7.50 11 -5 4 73.29 7.10 -11 -5 -4 81.99 7.40 11 -5 4 73.79 10.10 11 5 5 21.20 6.20 -11 5 -5 18.20 4.80 11 5 5 8.40 3.00 11 5 5 17.00 3.90 -11 5 -5 12.50 3.90 11 5 5 16.30 4.00 -11 -5 -5 16.90 4.20 -11 -5 -5 12.40 3.20 -11 -5 -5 20.90 4.60 11 -5 5 15.20 3.70 11 -5 5 14.20 3.60 11 5 6 61.09 6.10 -11 5 -6 68.39 8.20 11 5 6 63.79 6.80 -11 5 -6 63.59 6.90 11 5 6 59.89 5.50 -11 -5 -6 62.99 6.30 11 -5 6 52.99 5.70 -11 -5 -6 62.89 5.90 -11 5 -7 13.90 3.80 11 5 7 6.30 2.40 -11 5 -7 10.10 3.40 11 5 7 9.00 2.90 11 -5 7 12.00 2.90 -11 -5 -7 6.50 3.20 -11 -5 -7 10.20 3.00 11 5 8 41.90 4.50 -11 5 -8 33.40 5.00 -11 5 -8 42.30 5.30 11 5 8 42.00 4.00 -11 -5 -8 36.60 4.40 11 -5 8 41.90 4.40 -11 -5 -8 42.10 6.90 -11 5 -9 129.99 7.70 11 -5 9 130.09 6.70 -11 -5 -9 133.39 6.80 -11 6 11 65.19 5.20 11 6 -11 48.60 4.10 -11 6 11 53.79 4.20 -11 -6 11 60.99 4.40 -11 -6 11 50.99 3.70 -11 -6 11 42.40 4.90 -11 6 10 277.67 11.80 -11 6 10 273.97 11.60 -11 6 10 276.57 11.70 -11 -6 10 243.18 10.30 11 -6 -10 267.87 11.00 -11 -6 10 268.97 11.10 11 -6 -10 249.88 10.40 -11 -6 10 250.47 10.40 -11 -6 10 260.17 11.20 -11 6 9 144.69 8.30 -11 6 9 133.99 9.30 -11 6 9 158.18 11.40 -11 6 9 122.19 8.20 -11 6 9 153.08 12.40 -11 -6 9 158.28 9.20 -11 -6 9 146.49 9.20 -11 -6 9 137.39 8.00 -11 -6 9 136.89 7.60 11 -6 -9 125.89 7.90 -11 -6 9 129.99 9.50 -11 6 8 52.39 5.80 -11 6 8 54.59 5.10 -11 6 8 55.69 6.00 -11 6 8 49.70 5.50 -11 6 8 52.69 5.50 -11 6 8 51.99 5.60 11 -6 -8 42.50 4.90 -11 -6 8 54.39 5.70 -11 -6 8 44.50 4.80 -11 -6 8 54.79 5.40 -11 -6 8 51.99 4.90 -11 -6 8 49.10 5.50 -11 6 7 8.80 2.90 11 6 -7 6.40 6.90 -11 6 7 14.20 3.60 -11 6 7 13.30 3.70 -11 6 7 18.70 4.50 -11 6 7 13.80 3.50 -11 6 7 16.60 3.80 -11 -6 7 10.70 3.40 -11 -6 7 13.50 3.20 -11 -6 7 17.20 3.80 11 -6 -7 14.80 3.70 -11 -6 7 13.60 3.30 -11 -6 7 12.00 3.20 -11 6 6 340.97 14.70 -11 6 6 327.07 14.90 -11 6 6 311.07 16.00 11 6 -6 301.17 18.40 -11 6 6 345.37 15.80 -11 6 6 333.87 15.40 -11 6 6 311.07 15.40 -11 -6 6 328.37 13.90 -11 -6 6 330.37 15.00 11 -6 -6 334.07 15.10 -11 -6 6 345.17 15.50 -11 -6 6 330.07 15.00 -11 6 5 284.07 13.80 -11 6 5 284.17 14.00 -11 6 5 290.17 14.30 11 6 -5 286.57 17.90 -11 6 5 298.67 14.60 -11 6 5 297.77 13.80 -11 6 5 288.37 14.50 -11 -6 5 292.07 12.70 -11 -6 5 243.88 14.20 -11 -6 5 268.07 12.80 11 -6 -5 296.17 14.20 -11 -6 5 297.47 14.10 -11 -6 5 297.07 14.10 -11 -6 5 297.37 13.90 11 6 -4 6.30 4.60 -11 6 4 0.40 3.80 11 6 -4 3.20 3.20 -11 6 4 0.90 3.00 -11 6 4 5.70 3.20 -11 6 4 7.50 3.90 -11 6 4 -1.60 3.40 -11 -6 4 -0.70 4.30 -11 -6 4 6.90 3.00 -11 -6 4 2.70 4.10 -11 -6 4 -0.90 3.60 11 -6 -4 2.60 2.70 -11 -6 4 2.10 3.00 -11 -6 4 0.70 2.80 -11 -6 4 1.40 3.00 -11 6 3 521.45 21.70 11 6 -3 555.44 22.00 -11 6 3 553.94 21.90 -11 6 3 540.55 21.40 11 6 -3 497.45 20.50 -11 6 3 563.94 22.20 11 6 -3 497.65 25.40 -11 -6 3 551.84 21.50 -11 -6 3 564.94 21.90 11 -6 -3 547.95 21.80 -11 -6 3 552.24 21.50 -11 -6 3 502.95 19.90 -11 -6 3 518.45 20.40 -11 -6 3 574.44 20.40 -11 6 2 236.88 12.80 11 6 -2 219.38 12.50 -11 6 2 227.28 12.40 11 6 -2 202.48 12.10 11 6 -2 254.37 17.70 -11 6 2 249.08 13.20 -11 6 2 242.48 12.90 -11 -6 2 234.88 12.00 -11 -6 2 233.88 12.40 -11 -6 2 236.48 12.50 -11 -6 2 237.38 12.70 -11 -6 2 233.88 12.20 11 -6 -2 224.68 12.20 -11 6 1 6.10 4.30 11 6 -1 -5.60 3.70 11 6 -1 10.20 3.60 11 6 -1 5.90 3.40 -11 6 1 8.90 7.10 -11 6 1 3.90 3.50 -11 6 1 0.30 3.60 -11 -6 1 6.00 3.70 11 -6 -1 9.50 3.40 -11 -6 1 7.80 3.60 -11 -6 1 1.30 3.50 -11 -6 1 7.20 3.20 11 -6 -1 7.20 3.30 11 6 0 12.50 3.70 -11 6 0 18.70 4.50 11 6 0 20.90 4.50 11 6 0 18.70 5.60 11 6 0 17.60 4.00 11 -6 0 11.10 3.80 -11 -6 0 17.20 4.20 -11 -6 0 13.50 4.10 11 -6 0 13.80 3.70 -11 -6 0 13.40 3.70 11 6 1 2.00 3.50 11 6 1 1.00 4.80 11 6 1 8.10 3.30 -11 6 -1 3.90 3.80 11 -6 1 5.60 2.70 -11 -6 -1 -1.60 2.70 11 -6 1 9.30 3.30 -11 -6 -1 7.00 3.50 -11 -6 -1 0.80 3.20 -11 6 -2 86.99 12.10 11 6 2 91.49 7.20 11 6 2 85.99 6.80 11 6 2 62.39 8.60 11 -6 2 84.79 7.00 -11 -6 -2 86.69 8.40 11 -6 2 83.39 6.90 -11 -6 -2 84.89 7.10 11 6 3 19.30 4.00 11 6 3 16.40 3.80 -11 6 -3 19.90 4.30 11 6 3 22.90 6.40 11 6 3 29.20 4.70 -11 -6 -3 16.50 4.20 11 -6 3 24.80 4.20 11 -6 3 24.80 4.70 11 -6 3 20.70 5.00 -11 -6 -3 22.60 4.40 -11 -6 -3 10.40 3.50 11 6 4 77.19 6.20 -11 6 -4 84.29 7.70 11 6 4 64.49 9.40 11 6 4 81.79 8.10 11 6 4 72.89 6.60 11 -6 4 82.79 7.00 11 -6 4 79.59 6.40 -11 -6 -4 72.29 6.90 -11 -6 -4 91.19 7.40 11 -6 4 72.39 6.10 -11 6 -5 -3.20 2.20 11 6 5 1.60 2.40 11 6 5 0.50 2.00 -11 6 -5 0.70 3.80 -11 -6 -5 0.80 2.40 11 -6 5 -0.10 2.40 -11 -6 -5 8.50 4.30 -11 -6 -5 1.70 2.30 -11 6 -6 27.20 5.00 -11 6 -6 13.70 3.40 11 6 6 15.20 3.30 -11 -6 -6 10.70 3.00 11 -6 6 14.60 3.10 -11 -6 -6 12.20 3.40 11 6 7 37.90 4.50 -11 6 -7 58.89 5.40 11 6 7 47.20 4.30 -11 6 -7 52.39 5.40 11 -6 7 44.80 4.50 -11 -6 -7 43.50 4.80 -11 -6 -7 44.30 4.90 -11 6 -8 1.00 1.70 11 6 8 1.60 1.60 -11 -6 -8 3.60 2.20 11 -6 8 0.90 1.40 11 7 -10 1.40 1.70 -11 7 10 -0.40 1.30 -11 7 10 1.00 1.10 -11 7 10 1.20 1.30 -11 7 10 3.30 1.80 -11 -7 10 2.70 1.30 -11 -7 10 0.60 1.70 -11 -7 10 1.50 1.40 -11 -7 10 -0.30 1.40 -11 7 9 0.00 1.70 -11 7 9 4.20 2.20 -11 7 9 0.50 1.40 -11 7 9 1.30 1.60 11 -7 -9 0.30 3.10 11 -7 -9 0.40 1.60 -11 -7 9 3.90 1.70 -11 -7 9 1.80 2.10 -11 -7 9 0.30 1.40 11 7 -8 45.20 4.70 -11 7 8 51.69 5.10 -11 7 8 47.30 4.70 -11 7 8 45.50 4.80 -11 7 8 38.20 4.40 -11 7 8 38.90 4.50 -11 -7 8 51.39 4.10 11 -7 -8 46.50 4.40 -11 -7 8 48.40 4.70 11 -7 -8 38.40 4.20 -11 -7 8 42.70 4.30 -11 -7 8 49.40 4.70 -11 -7 8 37.30 6.00 11 7 -7 50.39 5.30 -11 7 7 43.50 5.00 -11 7 7 52.29 5.30 -11 7 7 50.79 5.40 11 -7 -7 50.09 7.30 -11 -7 7 53.09 4.90 -11 -7 7 43.30 4.90 -11 -7 7 49.00 5.40 -11 -7 7 56.39 4.50 -11 -7 7 55.19 5.30 11 7 -6 2.10 2.40 -11 7 6 -1.50 2.20 -11 7 6 -0.40 2.30 -11 7 6 2.20 2.70 -11 7 6 2.10 2.50 -11 7 6 2.00 2.40 -11 -7 6 -0.70 3.30 -11 -7 6 2.50 2.30 -11 -7 6 4.10 2.70 11 -7 -6 0.10 2.20 -11 -7 6 2.80 2.50 -11 -7 6 0.90 2.10 11 -7 -6 -0.60 2.10 -11 7 5 18.30 4.20 -11 7 5 21.80 4.30 -11 7 5 20.20 4.00 11 7 -5 23.00 5.40 -11 7 5 27.30 4.50 11 7 -5 23.20 5.90 -11 7 5 30.40 5.00 11 7 -5 27.30 4.60 11 -7 -5 22.60 4.20 -11 -7 5 21.10 3.90 -11 -7 5 17.20 3.70 -11 -7 5 20.20 3.30 -11 -7 5 29.00 4.80 11 -7 -5 28.70 4.40 -11 -7 5 23.30 4.20 -11 7 4 38.60 5.90 -11 7 4 38.50 5.40 -11 7 4 41.10 5.70 -11 7 4 34.30 5.80 11 7 -4 27.80 6.30 -11 7 4 33.90 5.90 11 7 -4 37.70 5.30 11 7 -4 41.50 6.20 11 -7 -4 43.40 5.30 11 -7 -4 29.90 4.60 -11 -7 4 42.40 5.10 -11 -7 4 49.10 5.70 -11 -7 4 39.30 5.40 -11 -7 4 36.20 5.60 -11 -7 4 38.90 5.80 -11 7 3 61.79 7.40 -11 7 3 69.19 7.00 11 7 -3 71.49 7.00 11 7 -3 80.69 7.00 -11 7 3 77.29 7.20 -11 7 3 81.59 8.10 -11 7 3 63.89 6.80 11 7 -3 62.39 8.40 -11 -7 3 72.09 6.90 11 -7 -3 73.39 6.40 -11 -7 3 68.99 7.10 -11 -7 3 80.19 6.60 -11 -7 3 69.99 7.00 -11 -7 3 69.49 7.30 11 -7 -3 70.49 6.50 -11 7 2 1.30 2.90 -11 7 2 -0.70 3.00 -11 7 2 5.80 7.20 11 7 -2 3.20 2.50 11 7 -2 2.10 3.10 11 7 -2 11.70 5.20 11 -7 -2 6.10 2.90 -11 -7 2 0.90 3.30 -11 -7 2 1.40 2.90 -11 -7 2 1.20 2.60 11 -7 -2 6.00 2.80 -11 -7 2 0.40 3.50 11 7 -1 38.80 5.30 11 7 -1 38.80 5.10 11 7 -1 35.40 5.10 -11 7 1 28.10 4.70 -11 7 1 42.60 6.10 11 7 -1 30.60 7.30 -11 -7 1 33.80 5.30 11 -7 -1 40.70 5.10 -11 -7 1 30.60 4.90 -11 -7 1 37.50 5.60 -11 -7 1 34.40 5.50 11 -7 -1 38.20 5.10 11 7 0 26.30 6.60 -11 7 0 48.30 6.20 11 7 0 39.20 5.30 11 7 0 37.80 5.20 11 7 0 39.40 5.30 11 -7 0 36.00 4.80 11 -7 0 38.10 6.00 -11 -7 0 36.50 5.50 11 -7 0 40.40 6.60 -11 -7 0 45.20 5.30 -11 -7 0 33.80 5.40 -11 -7 0 36.90 5.70 11 7 1 11.90 3.40 11 7 1 8.20 3.40 11 7 1 11.60 3.40 11 7 1 16.80 5.80 -11 7 -1 12.50 4.00 11 -7 1 7.40 3.10 11 -7 1 6.30 2.60 -11 -7 -1 6.20 3.20 -11 -7 -1 9.70 3.20 -11 -7 -1 8.10 3.20 -11 7 -2 8.30 3.70 11 7 2 3.70 4.50 11 7 2 10.80 3.10 11 7 2 10.00 3.40 -11 -7 -2 8.70 3.00 11 -7 2 12.20 3.10 -11 -7 -2 15.00 3.70 11 -7 2 9.50 3.10 -11 -7 -2 8.90 3.10 11 7 3 34.60 4.50 11 7 3 36.80 4.80 -11 7 -3 24.60 4.40 11 -7 3 40.60 5.00 11 -7 3 30.60 4.30 -11 -7 -3 28.40 4.60 -11 -7 -3 35.60 4.90 -11 -7 -3 24.70 4.10 11 7 4 1.90 2.20 -11 7 -4 6.00 3.00 11 7 4 2.60 2.10 11 -7 4 3.20 3.30 11 -7 4 2.20 3.00 -11 -7 -4 8.60 2.80 -11 -7 -4 3.10 2.60 11 7 5 115.39 6.80 -11 7 -5 99.49 9.90 11 7 5 116.99 9.10 -11 -7 -5 120.49 7.30 11 -7 5 121.09 7.10 -11 -7 -5 128.09 7.40 11 7 6 57.89 4.80 11 7 6 54.89 4.40 -11 -7 -6 56.19 4.80 -11 -7 -6 53.89 4.90 11 7 7 82.79 6.60 -11 7 -7 63.09 5.80 11 7 7 83.09 4.90 -11 -7 -7 83.49 5.40 -11 8 8 35.40 3.40 -11 8 8 37.90 3.60 11 8 -8 37.00 3.60 -11 8 8 42.40 3.80 -11 -8 8 31.70 3.40 -11 -8 8 32.30 3.10 11 8 -7 54.89 4.80 -11 8 7 53.09 4.80 -11 8 7 66.49 4.90 -11 -8 7 67.09 4.80 -11 -8 7 67.49 5.00 -11 -8 7 59.39 5.50 -11 -8 7 57.99 4.00 -11 -8 7 72.19 5.60 11 -8 -7 67.49 4.50 -11 8 6 110.49 6.50 -11 8 6 97.39 6.70 -11 8 6 112.09 6.40 11 8 -6 118.69 7.00 -11 8 6 112.79 7.00 -11 8 6 132.09 9.80 -11 -8 6 107.49 6.40 -11 -8 6 99.19 6.00 -11 -8 6 106.99 6.60 -11 -8 6 103.99 6.30 11 -8 -6 109.59 6.30 -11 -8 6 107.39 6.60 11 -8 -6 111.99 6.80 -11 8 5 12.10 2.90 -11 8 5 26.70 4.10 -11 8 5 13.60 3.20 -11 8 5 21.70 4.00 11 8 -5 19.40 3.70 -11 -8 5 23.70 3.80 -11 -8 5 15.80 4.00 -11 -8 5 10.20 2.80 -11 -8 5 13.70 3.30 11 -8 -5 11.80 2.60 -11 -8 5 17.30 3.20 11 -8 -5 23.00 3.70 -11 8 4 110.49 9.70 11 8 -4 121.99 7.60 -11 8 4 124.79 8.40 -11 8 4 107.79 7.40 -11 -8 4 131.69 7.70 11 -8 -4 124.69 7.30 11 -8 -4 112.79 7.40 11 8 -3 33.40 4.60 11 8 -3 29.30 4.10 11 8 -3 32.50 4.30 -11 8 3 26.00 4.30 -11 -8 3 35.20 5.00 11 -8 -3 34.70 4.20 11 -8 -3 42.70 4.60 11 8 -2 1.20 2.30 11 8 -2 0.90 1.90 -11 8 2 -0.80 2.40 11 8 -2 2.00 2.50 11 -8 -2 -0.60 1.90 -11 -8 2 -0.20 2.30 11 -8 -2 4.50 2.70 -11 -8 2 -2.20 2.70 -11 8 1 44.90 5.80 11 8 -1 47.20 4.90 11 8 -1 47.00 5.30 -11 -8 1 52.89 5.70 11 -8 -1 47.40 4.90 -11 -8 1 37.90 5.60 -11 -8 1 30.40 4.70 11 -8 -1 54.49 5.10 11 -8 -1 54.49 5.40 -11 -8 1 49.30 5.80 11 8 0 0.10 2.10 11 8 0 8.60 2.70 -11 8 0 4.50 3.00 11 -8 0 2.50 4.00 11 -8 0 0.00 2.20 11 -8 0 5.40 2.20 -11 -8 0 7.70 2.70 -11 -8 0 6.00 3.00 11 8 1 2.90 2.20 11 8 1 3.20 2.50 -11 8 -1 5.60 2.70 -11 -8 -1 1.80 2.20 -11 -8 -1 1.50 2.50 11 -8 1 -1.20 1.70 -11 -8 -1 -2.60 2.50 -11 8 -2 0.90 2.40 11 8 2 0.80 2.00 11 8 2 0.00 1.80 11 -8 2 2.40 2.20 -11 -8 -2 0.50 3.00 -11 -8 -2 -1.90 2.10 -11 -8 -2 0.80 3.70 -11 8 -3 22.60 4.10 11 8 3 23.50 3.50 11 8 3 26.90 3.90 11 -8 3 21.80 3.60 11 -8 3 18.20 3.00 -11 -8 -3 18.70 3.40 -11 -8 -3 25.10 4.20 -11 -8 -3 19.50 3.30 11 8 4 18.10 4.10 11 8 4 14.80 2.90 -11 8 -4 12.00 3.00 -11 -8 -4 8.80 2.60 -11 -8 -4 12.80 2.90 11 8 5 7.80 2.40 -11 8 -5 5.40 2.30 11 8 5 8.50 2.10 11 -8 5 9.40 2.10 -11 -8 -5 8.10 2.30 -11 -8 -5 10.30 2.70 -11 -8 -5 8.30 2.50 -11 8 -6 2.80 1.80 11 8 6 0.70 1.40 11 8 6 3.60 1.50 -11 -8 -6 3.80 2.50 -11 -8 -6 4.20 1.90 11 9 -6 4.30 1.60 -11 9 6 4.10 1.70 11 -9 -6 6.20 1.70 -11 -9 6 8.50 2.10 -11 -9 6 4.70 1.80 11 -9 -6 5.20 1.60 11 9 -5 8.70 2.00 -11 9 5 6.40 2.90 11 -9 -5 5.40 2.10 -11 -9 5 10.10 2.20 11 -9 -5 12.00 3.20 11 -9 -5 8.40 2.30 -11 -9 5 4.30 2.00 -11 9 4 0.40 1.60 11 9 -4 1.00 1.60 11 -9 -4 1.70 1.80 11 -9 -4 1.80 1.80 -11 -9 4 -0.90 1.60 -11 -9 4 0.80 1.60 -11 9 3 1.40 1.90 11 9 -3 0.20 1.70 11 9 -3 -0.60 2.10 11 -9 -3 0.60 1.50 -11 -9 3 -0.30 1.60 11 -9 -3 3.40 1.90 11 -9 -3 1.60 1.80 -11 -9 3 -0.10 1.70 11 9 -2 2.60 1.80 -11 9 2 1.20 1.90 11 9 -2 1.80 1.90 11 -9 -2 -2.40 1.80 11 -9 -2 1.50 1.90 -11 -9 2 -0.60 1.70 11 -9 -2 2.60 1.60 -11 -9 2 1.00 2.00 -11 9 1 4.00 2.30 11 9 -1 1.70 1.70 11 -9 -1 3.10 1.70 -11 -9 1 4.50 2.70 -11 -9 1 4.80 2.20 11 -9 -1 6.20 2.40 11 -9 -1 9.10 2.70 11 9 0 138.79 8.30 -11 9 0 157.98 8.10 11 9 0 150.38 7.80 11 -9 0 160.08 7.60 -11 -9 0 162.78 8.00 -11 9 -1 59.99 5.20 -11 -9 -1 66.79 5.00 11 -9 1 55.79 4.40 11 -9 1 57.59 4.60 11 9 2 6.10 2.00 11 9 2 4.40 1.70 -11 9 -2 2.80 2.70 11 -9 2 1.90 1.40 11 -9 2 1.10 2.30 -11 -9 -2 3.80 1.90 -11 -9 -2 5.20 2.30 11 9 3 7.60 1.90 -11 9 -3 10.50 2.30 11 9 3 7.50 1.90 -11 -9 -3 7.10 2.00 11 -9 3 9.30 1.80 -11 -9 -3 9.80 2.40 -12 0 13 1.00 1.80 -12 0 13 -0.10 1.40 -12 0 13 1.20 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41.00 7.70 -12 5 -3 64.09 7.10 12 -5 3 56.59 6.30 -12 -5 -3 50.29 6.20 12 -5 3 68.29 6.20 -12 -5 -3 64.89 6.50 12 -5 3 66.39 6.00 -12 -5 -3 60.59 6.30 12 5 4 -0.60 2.30 12 5 4 0.30 2.60 -12 5 -4 3.80 3.30 12 5 4 -0.80 2.80 12 5 4 1.20 3.60 -12 -5 -4 2.40 2.60 12 -5 4 1.60 2.60 12 -5 4 -1.10 2.50 -12 -5 -4 1.20 3.40 -12 -5 -4 6.60 3.70 12 5 5 61.09 5.50 12 5 5 45.20 5.20 12 5 5 57.59 10.30 12 5 5 52.29 5.50 -12 5 -5 59.59 6.50 12 -5 5 64.29 5.60 -12 -5 -5 57.09 5.90 -12 -5 -5 53.49 5.60 12 5 6 32.40 4.00 12 5 6 31.30 4.40 -12 5 -6 35.30 5.10 12 5 6 32.00 6.00 -12 -5 -6 32.40 4.50 -12 -5 -6 33.90 4.90 12 -5 6 40.30 4.70 12 5 7 6.40 2.20 -12 5 -7 0.80 2.30 12 5 7 4.60 2.10 -12 -5 -7 3.30 2.30 -12 -5 -7 3.50 2.30 12 -5 7 3.30 1.80 -12 5 -8 11.60 3.80 12 5 8 10.70 2.00 -12 -5 -8 16.20 4.00 12 -5 8 13.50 2.70 -12 -5 -8 11.20 2.40 -12 6 10 71.29 4.80 12 6 -10 78.49 4.50 -12 6 10 82.79 5.10 -12 -6 10 64.99 5.30 12 -6 -10 93.29 5.40 -12 -6 10 74.99 5.60 -12 -6 10 75.29 4.90 12 6 -9 304.67 12.40 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4.20 2.40 12 7 -1 -2.30 5.00 -12 7 1 -0.20 2.70 -12 -7 1 6.50 3.40 -12 -7 1 -2.20 2.80 -12 -7 1 -0.10 2.20 12 -7 -1 -0.30 2.00 -12 -7 1 -4.50 2.60 12 -7 -1 0.60 1.90 12 7 0 -1.60 2.30 -12 7 0 -0.50 2.30 12 7 0 1.40 2.20 12 7 0 0.80 3.00 12 -7 0 1.70 1.90 -12 -7 0 4.50 2.80 -12 -7 0 -2.40 2.10 -12 -7 0 3.00 2.90 12 -7 0 1.50 2.30 12 7 1 15.40 3.20 12 7 1 10.70 3.20 -12 7 -1 10.80 3.40 12 7 1 8.20 2.80 12 -7 1 12.50 3.30 12 -7 1 9.30 2.70 -12 -7 -1 8.90 3.00 -12 -7 -1 8.90 2.90 -12 -7 -1 8.80 3.00 12 7 2 3.40 2.50 12 7 2 6.00 2.50 -12 7 -2 -0.70 2.30 12 -7 2 10.70 3.00 -12 -7 -2 1.80 2.20 -12 -7 -2 5.60 2.70 12 -7 2 2.80 2.70 12 7 3 126.29 6.80 12 7 3 126.79 7.80 -12 -7 -3 131.29 7.60 -12 -7 -3 127.39 7.40 12 -7 3 118.09 6.80 -12 -7 -3 105.19 10.20 12 -7 3 115.29 7.00 12 7 4 0.00 2.10 -12 7 -4 -2.00 1.90 12 7 4 -0.40 1.70 -12 -7 -4 0.50 3.50 -12 -7 -4 -1.90 3.40 12 -7 4 0.40 1.90 -12 -7 -4 -0.20 2.10 12 7 5 2.80 1.80 12 7 5 3.70 1.80 -12 7 -5 0.40 2.00 -12 -7 -5 1.20 1.90 -12 -7 -5 1.30 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-2.40 2.50 13 4 -5 3.40 4.20 -13 4 5 3.50 2.90 -13 4 5 2.60 2.70 -13 4 5 1.80 3.20 -13 4 5 3.30 3.00 -13 -4 5 2.80 2.40 -13 -4 5 6.60 3.50 -13 -4 5 1.40 3.20 -13 -4 5 1.40 2.50 -13 -4 5 3.20 3.40 -13 -4 5 1.50 3.00 -13 -4 5 0.20 2.40 -13 4 4 165.18 12.80 -13 4 4 148.69 10.20 -13 4 4 172.08 10.30 -13 4 4 141.99 9.50 13 4 -4 144.49 9.30 -13 4 4 150.08 9.90 13 4 -4 132.29 11.80 -13 -4 4 138.39 12.00 -13 -4 4 135.59 8.50 -13 -4 4 174.98 13.20 -13 -4 4 135.99 9.70 -13 -4 4 148.69 9.30 -13 -4 4 134.39 8.40 -13 -4 4 148.69 9.40 -13 4 3 0.40 4.80 13 4 -3 -3.90 3.10 -13 4 3 -1.70 2.10 -13 4 3 8.80 4.50 -13 4 3 -4.70 3.20 -13 4 3 0.00 2.50 -13 4 3 5.00 3.50 -13 -4 3 3.30 2.90 -13 -4 3 -3.30 2.60 -13 -4 3 6.30 3.40 -13 -4 3 -4.50 3.50 -13 -4 3 2.50 3.20 -13 4 2 252.47 12.70 -13 4 2 252.67 13.20 -13 4 2 258.17 16.30 -13 4 2 246.78 12.90 -13 4 2 264.27 13.20 13 4 -2 252.97 16.70 13 4 -2 276.87 13.40 -13 4 2 267.37 13.60 -13 -4 2 255.67 12.70 -13 -4 2 268.17 13.70 13 -4 -2 266.67 13.00 -13 -4 2 267.47 13.50 -13 -4 2 245.18 12.70 -13 4 1 163.78 9.50 -13 4 1 153.08 10.20 -13 4 1 128.09 11.40 -13 4 1 158.28 9.70 13 4 -1 142.09 12.40 13 4 -1 156.38 9.90 13 4 -1 158.38 9.70 -13 -4 1 156.18 10.00 -13 -4 1 146.39 9.90 13 -4 -1 157.98 9.30 -13 -4 1 145.69 9.40 13 -4 -1 143.09 9.40 13 4 0 7.90 3.50 13 4 0 7.20 4.90 13 4 0 7.60 3.20 -13 4 0 14.30 4.50 -13 4 0 9.50 4.00 -13 4 0 8.60 4.00 13 -4 0 7.00 3.40 -13 -4 0 8.40 3.80 13 -4 0 8.40 3.80 -13 -4 0 6.70 3.50 -13 4 -1 13.10 4.70 13 4 1 16.80 4.30 -13 4 -1 12.70 4.50 13 4 1 5.20 4.30 13 4 1 10.60 3.30 13 -4 1 19.00 3.90 13 -4 1 6.90 3.40 13 -4 1 13.70 3.70 -13 -4 -1 10.10 3.60 -13 -4 -1 8.00 3.20 13 4 2 3.60 4.60 13 4 2 7.60 2.90 -13 4 -2 11.40 4.00 13 4 2 6.40 2.80 13 -4 2 21.10 4.40 13 -4 2 4.20 2.80 -13 -4 -2 4.50 3.10 -13 -4 -2 2.10 3.00 -13 -4 -2 5.30 3.10 13 -4 2 9.20 3.40 13 4 3 14.30 5.40 13 4 3 11.50 3.40 -13 4 -3 14.20 4.20 13 4 3 8.00 2.80 -13 -4 -3 15.30 3.60 -13 -4 -3 16.60 4.10 13 -4 3 15.20 3.70 13 -4 3 19.00 3.80 -13 -4 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5 8 11.70 2.80 -13 5 8 13.50 2.90 -13 5 8 11.30 2.70 -13 5 8 8.50 2.60 13 -5 -8 15.30 3.30 -13 -5 8 11.00 2.40 -13 -5 8 13.10 2.90 -13 -5 8 10.10 2.90 -13 -5 8 11.50 3.30 -13 5 7 12.00 3.10 13 5 -7 14.40 3.20 -13 5 7 17.80 3.70 -13 5 7 8.50 2.50 -13 5 7 10.20 2.80 -13 5 7 16.90 3.80 -13 -5 7 16.10 3.60 -13 -5 7 25.90 4.30 -13 -5 7 11.80 2.90 13 -5 -7 20.10 4.00 -13 -5 7 14.50 3.00 -13 -5 7 18.50 4.90 13 5 -6 56.59 5.60 -13 5 6 56.79 6.00 -13 5 6 67.59 6.30 -13 5 6 61.79 5.60 -13 5 6 69.19 6.30 -13 5 6 51.69 5.80 -13 -5 6 66.09 5.40 -13 -5 6 63.79 5.90 -13 -5 6 71.49 6.50 -13 -5 6 61.19 6.20 -13 -5 6 61.59 6.00 -13 -5 6 60.59 5.20 13 -5 -6 62.89 5.80 -13 5 5 80.59 6.90 -13 5 5 88.29 7.30 -13 5 5 89.09 7.10 13 5 -5 74.89 6.50 13 5 -5 90.09 10.50 -13 5 5 90.29 6.80 -13 5 5 88.99 7.20 -13 -5 5 71.79 6.90 -13 -5 5 90.39 7.40 -13 -5 5 71.99 7.10 -13 -5 5 83.69 6.10 -13 -5 5 100.29 7.40 -13 -5 5 76.29 6.80 13 -5 -5 87.59 6.90 -13 -5 5 93.39 6.40 -13 5 4 263.77 13.00 -13 5 4 302.67 13.70 -13 5 4 298.27 14.10 -13 5 4 298.87 14.10 13 5 -4 310.47 13.90 -13 5 4 300.37 14.30 13 5 -4 314.37 18.40 -13 5 4 294.67 13.90 -13 -5 4 300.47 13.60 -13 -5 4 310.87 14.10 -13 -5 4 289.77 13.40 13 -5 -4 346.57 18.40 -13 -5 4 284.57 14.10 -13 -5 4 299.07 12.80 -13 -5 4 302.47 12.50 -13 -5 4 292.37 13.90 13 5 -3 243.08 12.20 -13 5 3 232.68 12.40 13 5 -3 221.88 15.30 -13 5 3 236.98 12.10 -13 5 3 237.38 12.20 -13 5 3 235.78 11.70 -13 5 3 240.48 12.30 -13 5 3 235.58 11.90 -13 -5 3 241.88 12.50 -13 -5 3 241.48 12.40 -13 -5 3 239.48 11.80 -13 -5 3 211.68 12.10 13 -5 -3 229.78 11.80 -13 5 2 93.39 7.40 -13 5 2 78.09 7.70 13 5 -2 98.09 7.70 -13 5 2 91.79 8.00 13 5 -2 91.19 9.80 13 5 -2 91.49 7.30 -13 5 2 84.79 7.80 -13 -5 2 97.79 7.80 -13 -5 2 109.09 8.10 -13 -5 2 101.69 7.80 -13 -5 2 94.69 7.90 13 -5 -2 95.59 7.20 -13 5 1 82.49 7.60 -13 5 1 66.19 9.90 13 5 -1 79.79 6.70 13 5 -1 77.89 6.90 13 5 -1 59.49 8.60 -13 5 1 68.29 7.60 -13 5 1 85.09 7.60 -13 -5 1 87.89 7.30 -13 -5 1 75.69 6.70 13 -5 -1 64.09 7.90 -13 -5 1 86.59 7.40 -13 5 0 25.40 4.90 13 5 0 30.40 4.80 13 5 0 24.70 4.60 -13 5 0 30.90 5.60 13 5 0 27.00 6.60 -13 -5 0 20.10 4.10 -13 -5 0 12.80 3.60 13 -5 0 27.40 4.50 -13 -5 0 37.40 5.50 13 -5 0 29.40 4.50 13 5 1 -2.70 3.20 -13 5 -1 2.70 3.10 13 5 1 -3.80 2.10 13 5 1 2.70 2.40 13 -5 1 4.40 3.50 13 -5 1 -1.30 2.10 -13 -5 -1 0.10 3.00 -13 -5 -1 -1.10 2.60 13 -5 1 4.00 3.00 13 5 2 1.90 6.40 13 5 2 2.30 2.30 -13 5 -2 7.50 3.40 13 5 2 5.70 2.80 13 -5 2 11.20 3.60 13 -5 2 5.30 2.80 -13 -5 -2 6.20 3.30 -13 -5 -2 10.20 3.20 -13 -5 -2 3.80 2.70 13 5 3 96.99 10.30 -13 5 -3 123.79 8.40 13 5 3 119.39 8.00 13 5 3 120.89 7.60 13 -5 3 131.79 7.20 -13 -5 -3 122.29 7.80 -13 -5 -3 113.19 8.10 13 5 4 364.46 15.00 -13 5 -4 365.96 15.20 13 5 4 326.77 13.50 -13 -5 -4 343.17 14.90 13 -5 4 340.77 13.90 -13 5 -5 62.29 6.00 13 5 5 51.19 5.20 -13 -5 -5 67.19 5.60 13 -5 5 66.99 5.30 -13 5 -6 109.29 6.80 13 5 6 107.29 6.50 -13 -5 -6 102.09 6.50 -13 -5 -6 106.59 6.60 13 -5 6 104.39 6.10 13 5 7 168.48 7.80 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1.80 16 3 -5 1.20 1.60 16 -3 -5 -0.20 2.10 -16 -3 5 -2.90 2.10 -16 -3 5 4.80 2.60 -16 -3 5 1.40 2.00 -16 -3 5 0.40 2.10 -16 3 4 34.20 4.00 -16 3 4 42.20 5.00 -16 3 4 42.10 4.60 16 3 -4 38.40 4.20 -16 3 4 33.40 4.10 16 -3 -4 37.10 4.50 -16 -3 4 32.80 4.50 -16 -3 4 37.90 4.50 -16 -3 4 34.70 4.40 -16 3 3 16.90 3.30 -16 3 3 15.40 3.10 16 3 -3 26.40 4.00 -16 -3 3 17.40 3.40 16 -3 -3 22.00 3.60 -16 -3 3 24.90 4.00 -16 -3 3 19.80 3.80 -16 3 2 64.99 5.60 -16 3 2 71.49 5.70 16 3 -2 68.59 5.50 16 -3 -2 62.29 6.00 -16 -3 2 70.69 6.00 -16 -3 2 72.79 5.70 16 -3 -2 74.09 7.20 -16 -3 2 69.89 5.80 16 3 -1 41.40 4.40 -16 3 1 41.20 5.00 -16 3 1 40.70 4.80 16 3 -1 39.50 5.60 -16 -3 1 38.20 4.60 16 -3 -1 34.50 4.90 -16 -3 1 46.50 4.80 -16 3 0 0.70 2.70 16 3 0 1.10 1.60 -16 -3 0 -0.70 2.10 -16 -3 0 4.80 2.90 -16 -3 0 6.30 2.50 16 -3 0 -0.20 2.80 16 3 1 12.80 2.50 16 -3 1 12.10 2.60 -16 -3 -1 7.80 2.70 -16 -3 -1 13.40 2.70 16 3 2 56.99 4.60 16 3 2 52.79 4.50 -16 -3 -2 52.89 4.90 -16 -3 -2 54.49 4.90 16 3 3 5.90 2.00 16 3 3 3.50 1.50 16 -3 3 4.80 1.90 -16 -3 -3 1.90 2.00 -16 -3 -3 -0.20 1.80 16 3 4 6.90 1.80 -16 -3 -4 4.00 1.90 16 -3 4 4.90 1.80 -16 4 7 6.00 2.10 -16 -4 7 14.90 3.30 -16 4 6 48.50 4.60 16 4 -6 59.09 4.20 -16 4 6 66.19 4.80 16 -4 -6 59.69 4.50 -16 -4 6 66.99 4.70 -16 -4 6 66.69 4.90 -16 4 5 7.30 2.70 -16 4 5 8.10 2.00 16 4 -5 11.80 3.00 -16 -4 5 10.40 2.50 16 -4 -5 7.60 4.30 -16 4 4 29.40 3.60 16 4 -4 34.80 3.60 -16 4 4 30.20 3.90 -16 -4 4 33.70 3.90 -16 -4 4 32.50 4.00 16 -4 -4 37.90 5.80 -16 -4 4 28.70 4.40 16 4 -3 45.80 4.20 -16 4 3 36.00 4.10 -16 -4 3 39.60 4.20 -16 -4 3 39.10 4.60 -16 -4 3 40.40 4.30 16 -4 -3 44.80 4.70 16 -4 -3 39.10 4.40 16 4 -2 17.30 3.00 -16 4 2 7.60 4.10 16 4 -2 15.00 2.80 -16 4 2 9.10 2.60 -16 -4 2 8.70 2.90 -16 -4 2 13.90 3.00 16 -4 -2 24.10 3.40 -16 4 1 20.80 3.40 16 4 -1 31.30 3.80 16 4 -1 27.90 3.50 -16 -4 1 30.80 4.20 16 -4 -1 32.10 3.50 -16 -4 1 31.30 4.00 -16 -4 1 35.90 5.10 16 4 0 58.59 4.50 16 4 0 56.29 4.50 -16 -4 0 47.20 4.70 -16 -4 0 51.19 5.00 -16 -4 0 56.49 5.10 16 4 1 47.20 5.80 16 4 1 48.20 4.10 -16 -4 -1 47.50 4.40 -16 -4 -1 52.69 4.50 16 4 2 35.20 5.00 16 4 2 50.19 4.00 -16 -4 -2 46.20 4.30 -16 -4 -2 57.19 4.40 16 4 3 9.50 1.90 16 4 3 7.70 1.70 -16 -4 -3 5.20 1.80 -16 -4 -3 7.80 2.30 -16 5 5 219.38 9.10 -16 -5 5 236.48 9.30 -16 5 4 159.38 7.70 -16 -5 4 145.69 7.40 -16 -5 4 116.79 7.40 16 -5 -4 155.28 6.60 16 5 -3 7.50 1.80 16 5 -3 9.00 3.90 -16 -5 3 7.10 2.60 -16 -5 3 6.70 2.20 16 -5 -3 4.60 1.60 16 5 -2 -3.20 2.00 16 5 -2 0.20 1.30 -16 -5 2 -0.30 1.60 -16 -5 2 -4.00 2.10 -16 -5 2 -1.00 1.60 16 -5 -2 -0.70 1.40 16 5 -1 100.19 5.30 -16 -5 1 92.09 5.30 -16 -5 1 88.59 5.90 16 5 0 67.59 4.20 -16 -5 0 69.79 6.00 -16 -5 0 60.99 4.60 16 5 1 2.30 1.50 16 5 1 5.50 1.70 -16 -5 -1 0.70 2.00 -16 -5 -1 2.80 1.70 -17 0 7 0.10 1.40 -17 0 7 0.20 1.40 -17 0 7 0.50 1.50 -17 0 6 3.00 2.50 -17 0 6 0.60 1.60 -17 0 6 3.00 1.70 -17 0 6 3.80 1.70 17 0 -5 0.40 1.70 -17 0 5 -0.40 1.80 -17 0 5 -1.30 1.50 -17 0 5 0.40 1.90 -17 0 5 -1.10 1.70 -17 0 4 65.49 6.60 -17 0 4 68.99 5.50 -17 0 4 63.29 5.00 -17 0 4 66.49 5.20 -17 0 3 -1.00 1.60 17 0 -3 -1.00 2.70 -17 0 3 1.90 2.70 -17 0 3 1.20 1.90 17 0 -2 46.40 4.30 -17 0 2 50.49 4.80 -17 0 2 46.50 4.60 -17 0 1 0.80 2.00 17 0 -1 1.60 1.70 -17 0 1 -1.60 1.90 17 0 0 2.70 1.70 -17 0 0 3.60 2.20 -17 0 0 4.60 2.30 -17 0 -1 -1.10 1.90 -17 0 -2 40.90 4.00 17 0 2 42.60 3.80 17 0 3 0.10 1.30 -17 1 6 1.60 1.60 17 1 -6 -0.30 1.40 -17 1 6 2.40 1.60 -17 1 6 -1.70 1.60 -17 -1 6 2.40 2.40 -17 -1 6 -0.70 1.50 -17 -1 6 -5.70 2.20 -17 -1 6 0.30 1.80 -17 1 5 6.50 2.40 17 1 -5 8.70 2.10 -17 1 5 12.20 2.20 -17 1 5 5.30 2.00 -17 -1 5 7.80 2.50 -17 -1 5 8.60 2.40 -17 -1 5 6.60 2.70 17 1 -4 115.39 6.20 -17 1 4 108.89 6.70 -17 1 4 108.89 7.10 17 -1 -4 107.39 6.00 -17 -1 4 119.79 7.00 -17 -1 4 112.19 7.20 -17 -1 4 121.19 6.80 17 1 -3 -0.50 1.30 -17 1 3 1.60 2.10 -17 1 3 -1.30 1.50 -17 -1 3 0.30 1.80 17 -1 -3 1.50 1.90 -17 -1 3 -0.40 2.00 -17 -1 3 -0.60 2.10 -17 1 2 192.78 9.30 17 1 -2 200.08 9.10 -17 1 2 197.58 9.40 -17 -1 2 180.68 9.20 -17 -1 2 199.98 9.50 17 -1 -2 194.78 8.60 -17 1 1 20.30 4.40 17 1 -1 31.70 3.70 -17 1 1 35.50 4.60 17 -1 -1 29.50 3.70 -17 -1 1 37.70 4.50 -17 -1 1 38.40 4.30 17 1 0 68.09 5.00 -17 1 0 59.29 4.80 -17 1 0 62.49 7.80 -17 -1 0 69.59 5.40 17 -1 0 64.99 4.80 -17 -1 0 70.89 5.40 17 1 1 0.70 1.80 -17 1 -1 1.20 1.90 17 -1 1 -1.80 1.40 -17 -1 -1 -2.80 2.20 -17 -1 -1 -1.00 1.60 17 1 2 -1.40 1.20 -17 -1 -2 -2.00 1.60 17 -1 2 -2.00 2.00 17 1 3 0.30 1.20 17 -1 3 2.10 1.30 -17 -1 -3 0.30 2.00 -17 2 6 -1.00 1.60 17 2 -6 2.10 1.40 -17 2 6 2.70 1.70 -17 -2 6 -2.10 1.30 -17 -2 6 -0.30 1.40 -17 2 5 30.00 3.50 -17 -2 5 40.00 3.80 -17 -2 5 45.00 5.60 -17 2 4 5.00 2.00 -17 2 4 5.70 2.10 17 2 -4 5.80 1.80 -17 -2 4 2.80 1.90 -17 -2 4 4.60 2.30 -17 -2 4 5.10 2.20 17 2 -3 -0.30 1.40 -17 2 3 0.90 1.70 -17 2 3 -3.90 1.90 -17 -2 3 -0.20 1.70 -17 -2 3 0.10 2.00 -17 -2 3 -3.60 1.90 -17 2 2 3.80 2.50 17 2 -2 1.60 1.40 -17 2 2 4.40 2.10 -17 -2 2 1.60 2.10 -17 -2 2 -2.70 2.70 -17 -2 2 0.20 1.70 17 2 -1 -1.10 1.30 -17 2 1 -1.30 2.50 17 -2 -1 -4.20 1.80 -17 -2 1 0.80 1.50 -17 -2 1 0.00 2.10 -17 2 0 172.98 8.00 17 2 0 212.78 11.10 -17 -2 0 178.38 8.60 17 -2 0 186.58 7.90 17 2 1 1.50 1.40 -17 -2 -1 4.00 1.90 17 -2 1 2.00 1.60 -17 -2 -1 7.60 3.10 17 2 2 44.50 5.10 -17 -2 -2 43.10 3.70 17 -2 2 34.00 3.40 17 3 -5 0.60 1.20 -17 3 5 0.10 1.30 -17 -3 5 2.10 1.50 17 -3 -5 -1.50 1.30 -17 -3 5 2.50 1.60 -17 3 4 2.00 1.60 -17 -3 4 -0.70 2.40 -17 -3 4 2.90 1.70 -17 -3 4 2.70 1.70 17 -3 -4 0.10 1.60 -17 3 3 4.30 2.00 17 3 -3 1.90 1.40 -17 -3 3 -2.20 2.30 -17 -3 3 -1.10 1.60 17 -3 -3 2.30 2.00 -17 -3 3 2.50 1.90 -17 3 2 4.60 2.10 17 3 -2 1.70 1.40 -17 -3 2 6.10 2.40 -17 -3 2 0.30 1.70 17 3 -1 0.90 1.30 -17 -3 1 -0.30 1.50 -17 -3 1 1.90 2.00 -17 -3 0 19.80 3.60 -17 -3 0 25.30 3.10 17 3 1 20.60 2.60 -17 -3 -1 19.40 3.10 -17 -3 -1 11.10 2.60 -17 -4 2 0.10 1.60 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 79524 _shelx_res_file ; TITL SKM-352 in P2(1)/c shelx.res created by SHELXL-2018/3 at 11:36:14 on 30-May-2022 CELL 1.54178 14.5241 10.0718 13.2710 90.000 97.042 90.000 ZERR 4.00 0.0007 0.0005 0.0007 0.000 0.002 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 84 104 8 12 MERG 2 SADI C18 C19 C18 C19A SADI C19 C20 C19 C21 SADI C19A C20A C19A C21A DFIX 1.50 0.01 C15 C18 DFIX 1.51 0.01 C18 C19 C18 C19A DFIX 0.91 0.01 N2 HN2 DFIX 0.84 0.01 O1 HO1 EADP C19 C19A EADP C20 C20A EADP C21 C21A HTAB O1 N1 EQIV $1 x, -y+3/2, z-1/2 HTAB N2 O1_$1 HTAB N2 O2_$1 HTAB C10 O1_$1 FMAP 2 PLAN 5 SIZE 0.031 0.201 0.204 ACTA BOND $H CONF LIST 4 L.S. 13 TEMP -148.00 WGHT 0.051700 0.694000 FVAR 1.12500 0.92941 O1 4 0.481170 0.831247 0.629496 11.00000 0.02929 0.04220 = 0.02757 -0.00627 0.00591 -0.01054 HO1 2 0.458570 0.797252 0.573534 11.00000 0.06076 O2 4 0.571581 0.950294 0.781754 11.00000 0.03845 0.04940 = 0.02603 -0.00828 0.00540 -0.01485 O3 4 0.301670 0.644794 0.441003 11.00000 0.03152 0.04951 = 0.02447 -0.00111 0.00170 -0.00243 N1 3 0.469228 0.759556 0.440811 11.00000 0.02872 0.02950 = 0.02376 -0.00233 -0.00047 0.00241 N2 3 0.424482 0.695297 0.357824 11.00000 0.02899 0.03519 = 0.02254 -0.00468 0.00124 0.00107 HN2 2 0.456111 0.679956 0.304596 11.00000 0.04128 C1 1 0.598688 0.880425 0.519477 11.00000 0.02788 0.02649 = 0.02698 0.00291 0.00250 0.00168 C2 1 0.563495 0.886507 0.612960 11.00000 0.02460 0.02520 = 0.02783 0.00266 0.00252 -0.00021 C3 1 0.614080 0.951507 0.695204 11.00000 0.02908 0.02775 = 0.02570 0.00196 0.00241 0.00027 C4 1 0.698299 1.010233 0.684999 11.00000 0.02912 0.03073 = 0.03151 0.00128 -0.00275 -0.00222 AFIX 43 H4 2 0.732144 1.054394 0.741015 11.00000 -1.20000 AFIX 0 C5 1 0.733413 1.004262 0.591697 11.00000 0.02873 0.04124 = 0.03953 0.00168 0.00516 -0.00781 AFIX 43 H5 2 0.791294 1.044688 0.584278 11.00000 -1.20000 AFIX 0 C6 1 0.684654 0.940188 0.510537 11.00000 0.03300 0.03966 = 0.03063 0.00220 0.00795 -0.00431 AFIX 43 H6 2 0.709452 0.936307 0.447606 11.00000 -1.20000 AFIX 0 C7 1 0.615413 1.020158 0.868106 11.00000 0.03495 0.03936 = 0.02748 -0.00653 -0.00083 -0.00253 AFIX 137 H7A 2 0.675774 0.979590 0.890582 11.00000 -1.50000 H7B 2 0.576255 1.015696 0.923125 11.00000 -1.50000 H7C 2 0.624321 1.113185 0.849937 11.00000 -1.50000 AFIX 0 C8 1 0.547866 0.814162 0.432431 11.00000 0.03075 0.03063 = 0.02555 0.00164 0.00388 0.00128 AFIX 43 H8 2 0.572764 0.811269 0.369529 11.00000 -1.20000 AFIX 0 C9 1 0.341881 0.635373 0.366105 11.00000 0.02860 0.03095 = 0.02264 0.00147 -0.00050 0.00496 C10 1 0.304828 0.555291 0.272082 11.00000 0.02897 0.03269 = 0.02551 -0.00236 -0.00004 0.00208 AFIX 13 H10 2 0.352167 0.557419 0.223374 11.00000 -1.20000 AFIX 0 C11 1 0.292245 0.410956 0.304270 11.00000 0.05220 0.03261 = 0.04136 -0.00018 -0.00209 0.00319 AFIX 137 H11A 2 0.250084 0.407883 0.356498 11.00000 -1.50000 H11B 2 0.352538 0.373853 0.331631 11.00000 -1.50000 H11C 2 0.266064 0.358829 0.245264 11.00000 -1.50000 AFIX 0 C12 1 0.216464 0.619201 0.221382 11.00000 0.02772 0.02812 = 0.02346 -0.00436 -0.00086 -0.00086 C13 1 0.217564 0.688114 0.130733 11.00000 0.02874 0.03027 = 0.02701 -0.00340 0.00293 -0.00270 AFIX 43 H13 2 0.273825 0.694597 0.101326 11.00000 -1.20000 AFIX 0 C14 1 0.137977 0.747514 0.082540 11.00000 0.04140 0.03302 = 0.02647 0.00035 -0.00024 0.00323 AFIX 43 H14 2 0.140562 0.794801 0.021011 11.00000 -1.20000 AFIX 0 C15 1 0.054267 0.738655 0.123303 11.00000 0.03591 0.04667 = 0.02893 -0.00949 -0.00251 0.01225 C16 1 0.053597 0.668928 0.213787 11.00000 0.02961 0.06679 = 0.02972 -0.00634 0.00588 0.00475 AFIX 43 H16 2 -0.002864 0.660731 0.242608 11.00000 -1.20000 AFIX 0 C17 1 0.133169 0.611408 0.262590 11.00000 0.03326 0.05309 = 0.02301 0.00087 0.00355 -0.00130 AFIX 43 H17 2 0.130938 0.566028 0.324999 11.00000 -1.20000 AFIX 0 C18 1 -0.034393 0.802308 0.073745 11.00000 0.04388 0.06518 = 0.04093 -0.00958 -0.00321 0.02293 AFIX 23 H18A 2 -0.087137 0.761937 0.103331 11.00000 -1.20000 H18B 2 -0.032812 0.897690 0.091900 11.00000 -1.20000 AFIX 0 PART 1 C19 1 -0.053461 0.791176 -0.040593 21.00000 0.03407 0.03531 = 0.03757 0.00167 -0.00390 0.00529 AFIX 13 H19 2 -0.002595 0.838797 -0.070091 21.00000 -1.20000 AFIX 0 C20 1 -0.144740 0.860673 -0.078535 21.00000 0.04243 0.04411 = 0.05275 0.00183 -0.01122 0.01100 AFIX 137 H20A 2 -0.196295 0.813447 -0.053316 21.00000 -1.50000 H20B 2 -0.153574 0.860749 -0.152939 21.00000 -1.50000 H20C 2 -0.142860 0.952371 -0.053670 21.00000 -1.50000 AFIX 0 C21 1 -0.054944 0.650116 -0.078248 21.00000 0.04144 0.03561 = 0.04309 0.00215 -0.00656 0.00141 AFIX 137 H21A 2 0.004431 0.607334 -0.054798 21.00000 -1.50000 H21B 2 -0.064915 0.649641 -0.152632 21.00000 -1.50000 H21C 2 -0.105315 0.601541 -0.051829 21.00000 -1.50000 AFIX 0 PART 2 C19A 1 -0.101065 0.749963 -0.007040 -21.00000 0.03407 0.03531 = 0.03757 0.00167 -0.00390 0.00529 AFIX 13 H19A 2 -0.140915 0.702544 0.037706 -21.00000 -1.20000 AFIX 0 C20A 1 -0.171836 0.851841 -0.047357 -21.00000 0.04243 0.04411 = 0.05275 0.00183 -0.01122 0.01100 AFIX 137 H20D 2 -0.224290 0.807511 -0.087183 -21.00000 -1.50000 H20E 2 -0.143533 0.914905 -0.090648 -21.00000 -1.50000 H20F 2 -0.193809 0.899507 0.009485 -21.00000 -1.50000 AFIX 0 C21A 1 -0.064200 0.628536 -0.053580 -21.00000 0.04144 0.03561 = 0.04309 0.00215 -0.00656 0.00141 AFIX 137 H21D 2 -0.072593 0.551247 -0.010781 -21.00000 -1.50000 H21E 2 0.001967 0.640502 -0.059041 -21.00000 -1.50000 H21F 2 -0.097861 0.614437 -0.121356 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM SKM-352 in P2(1)/c REM wR2 = 0.1091, GooF = S = 1.064, Restrained GooF = 1.069 for all data REM R1 = 0.0405 for 3400 Fo > 4sig(Fo) and 0.0443 for all 3758 data REM 259 parameters refined using 8 restraints END WGHT 0.0517 0.6940 REM Highest difference peak 0.400, deepest hole -0.214, 1-sigma level 0.035 Q1 1 -0.0806 0.7657 0.0172 11.00000 0.05 0.40 Q2 1 0.8488 1.0446 0.6227 11.00000 0.05 0.37 Q3 1 0.0010 0.8603 0.0378 11.00000 0.05 0.36 Q4 1 0.0651 0.7497 0.1917 11.00000 0.05 0.30 Q5 1 0.0949 0.7870 0.1157 11.00000 0.05 0.22 ; _shelx_res_checksum 63898 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.48117(6) 0.83125(10) 0.62950(7) 0.0328(2) Uani d 1 . . H HO1 0.4586(13) 0.7973(19) 0.5735(10) 0.061(6) Uiso d 1 . . O O2 0.57158(7) 0.95029(10) 0.78175(7) 0.0378(2) Uani d 1 . . O O3 0.30167(6) 0.64479(10) 0.44100(7) 0.0353(2) Uani d 1 . . N N1 0.46923(7) 0.75956(10) 0.44081(8) 0.0276(2) Uani d 1 . . N N2 0.42448(7) 0.69530(11) 0.35782(8) 0.0291(2) Uani d 1 . . H HN2 0.4561(10) 0.6800(17) 0.3046(10) 0.041(4) Uiso d 1 . . C C1 0.59869(9) 0.88043(12) 0.51948(9) 0.0272(3) Uani d 1 . . C C2 0.56349(8) 0.88651(12) 0.61296(9) 0.0259(3) Uani d 1 . . C C3 0.61408(9) 0.95151(12) 0.69520(9) 0.0276(3) Uani d 1 . . C C4 0.69830(9) 1.01023(13) 0.68500(10) 0.0310(3) Uani d 1 . . H H4 0.732144 1.054394 0.741015 0.037 Uiso calc 1 . . C C5 0.73341(9) 1.00426(15) 0.59170(11) 0.0364(3) Uani d 1 . . H H5 0.791294 1.044688 0.584278 0.044 Uiso calc 1 . . C C6 0.68465(9) 0.94019(14) 0.51054(10) 0.0341(3) Uani d 1 . . H H6 0.709452 0.936307 0.447606 0.041 Uiso calc 1 . . C C7 0.61541(9) 1.02016(14) 0.86811(10) 0.0343(3) Uani d 1 . . H H7A 0.675774 0.979590 0.890582 0.051 Uiso calc 1 . . H H7B 0.576255 1.015696 0.923125 0.051 Uiso calc 1 . . H H7C 0.624321 1.113185 0.849937 0.051 Uiso calc 1 . . C C8 0.54787(9) 0.81416(13) 0.43243(9) 0.0289(3) Uani d 1 . . H H8 0.572764 0.811269 0.369529 0.035 Uiso calc 1 . . C C9 0.34188(9) 0.63537(13) 0.36611(9) 0.0277(3) Uani d 1 . . C C10 0.30483(9) 0.55529(13) 0.27208(9) 0.0293(3) Uani d 1 . . H H10 0.352167 0.557419 0.223374 0.035 Uiso calc 1 . . C C11 0.29224(12) 0.41096(14) 0.30427(12) 0.0427(4) Uani d 1 . . H H11A 0.250084 0.407883 0.356498 0.064 Uiso calc 1 . . H H11B 0.352538 0.373853 0.331631 0.064 Uiso calc 1 . . H H11C 0.266064 0.358829 0.245264 0.064 Uiso calc 1 . . C C12 0.21646(8) 0.61920(12) 0.22138(9) 0.0268(3) Uani d 1 . . C C13 0.21756(9) 0.68811(13) 0.13073(9) 0.0287(3) Uani d 1 . . H H13 0.273825 0.694597 0.101326 0.034 Uiso calc 1 . . C C14 0.13798(10) 0.74751(13) 0.08254(10) 0.0340(3) Uani d 1 . . H H14 0.140562 0.794801 0.021011 0.041 Uiso calc 1 . . C C15 0.05427(10) 0.73865(15) 0.12330(10) 0.0377(3) Uani d 1 . . C C16 0.05360(10) 0.66893(17) 0.21379(11) 0.0419(4) Uani d 1 . . H H16 -0.002864 0.660731 0.242608 0.050 Uiso calc 1 . . C C17 0.13317(10) 0.61141(16) 0.26259(10) 0.0364(3) Uani d 1 . . H H17 0.130938 0.566028 0.324999 0.044 Uiso calc 1 . . C C18 -0.03439(12) 0.80231(19) 0.07374(12) 0.0507(4) Uani d 1 . . H H18A -0.087137 0.761937 0.103331 0.061 Uiso calc 1 A 1 H H18B -0.032812 0.897690 0.091900 0.061 Uiso calc 1 A 1 C C19 -0.05346(11) 0.79118(15) -0.04059(12) 0.0363(4) Uani d 0.929(3) B 1 H H19 -0.002595 0.838797 -0.070091 0.044 Uiso calc 0.929(3) B 1 C C20 -0.14474(15) 0.8607(2) -0.07853(17) 0.0478(5) Uani d 0.929(3) B 1 H H20A -0.196295 0.813447 -0.053316 0.072 Uiso calc 0.929(3) B 1 H H20B -0.153574 0.860749 -0.152939 0.072 Uiso calc 0.929(3) B 1 H H20C -0.142860 0.952371 -0.053670 0.072 Uiso calc 0.929(3) B 1 C C21 -0.05494(17) 0.6501(2) -0.07825(16) 0.0410(5) Uani d 0.929(3) B 1 H H21A 0.004431 0.607334 -0.054798 0.062 Uiso calc 0.929(3) B 1 H H21B -0.064915 0.649641 -0.152632 0.062 Uiso calc 0.929(3) B 1 H H21C -0.105315 0.601541 -0.051829 0.062 Uiso calc 0.929(3) B 1 C C19A -0.1011(12) 0.7500(17) -0.0070(13) 0.0363(4) Uani d 0.071(3) B 2 H H19A -0.140915 0.702544 0.037706 0.044 Uiso calc 0.071(3) B 2 C C20A -0.172(2) 0.852(3) -0.047(3) 0.0478(5) Uani d 0.071(3) B 2 H H20D -0.224290 0.807511 -0.087183 0.072 Uiso calc 0.071(3) B 2 H H20E -0.143533 0.914905 -0.090648 0.072 Uiso calc 0.071(3) B 2 H H20F -0.193809 0.899507 0.009485 0.072 Uiso calc 0.071(3) B 2 C C21A -0.064(3) 0.629(3) -0.054(3) 0.0410(5) Uani d 0.071(3) B 2 H H21D -0.072593 0.551247 -0.010781 0.062 Uiso calc 0.071(3) B 2 H H21E 0.001967 0.640502 -0.059041 0.062 Uiso calc 0.071(3) B 2 H H21F -0.097861 0.614437 -0.121356 0.062 Uiso calc 0.071(3) B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0293(5) 0.0422(5) 0.0276(5) -0.0105(4) 0.0059(4) -0.0063(4) O2 0.0384(5) 0.0494(6) 0.0260(5) -0.0148(4) 0.0054(4) -0.0083(4) O3 0.0315(5) 0.0495(6) 0.0245(5) -0.0024(4) 0.0017(4) -0.0011(4) N1 0.0287(5) 0.0295(5) 0.0238(5) 0.0024(4) -0.0005(4) -0.0023(4) N2 0.0290(5) 0.0352(6) 0.0225(5) 0.0011(4) 0.0012(4) -0.0047(4) C1 0.0279(6) 0.0265(6) 0.0270(6) 0.0017(5) 0.0025(5) 0.0029(5) C2 0.0246(6) 0.0252(6) 0.0278(6) -0.0002(5) 0.0025(5) 0.0027(5) C3 0.0291(6) 0.0278(6) 0.0257(6) 0.0003(5) 0.0024(5) 0.0020(5) C4 0.0291(6) 0.0307(6) 0.0315(6) -0.0022(5) -0.0028(5) 0.0013(5) C5 0.0287(6) 0.0412(7) 0.0395(7) -0.0078(6) 0.0052(5) 0.0017(6) C6 0.0330(7) 0.0397(7) 0.0306(7) -0.0043(6) 0.0080(5) 0.0022(5) C7 0.0349(7) 0.0394(7) 0.0275(6) -0.0025(6) -0.0008(5) -0.0065(5) C8 0.0308(6) 0.0306(6) 0.0255(6) 0.0013(5) 0.0039(5) 0.0016(5) C9 0.0286(6) 0.0309(6) 0.0226(6) 0.0050(5) -0.0005(5) 0.0015(5) C10 0.0290(6) 0.0327(7) 0.0255(6) 0.0021(5) 0.0000(5) -0.0024(5) C11 0.0522(9) 0.0326(7) 0.0414(8) 0.0032(6) -0.0021(7) -0.0002(6) C12 0.0277(6) 0.0281(6) 0.0235(6) -0.0009(5) -0.0009(5) -0.0044(5) C13 0.0287(6) 0.0303(6) 0.0270(6) -0.0027(5) 0.0029(5) -0.0034(5) C14 0.0414(7) 0.0330(7) 0.0265(6) 0.0032(6) -0.0002(5) 0.0003(5) C15 0.0359(7) 0.0467(8) 0.0289(7) 0.0122(6) -0.0025(5) -0.0095(6) C16 0.0296(7) 0.0668(10) 0.0297(7) 0.0047(6) 0.0059(5) -0.0063(6) C17 0.0333(7) 0.0531(8) 0.0230(6) -0.0013(6) 0.0036(5) 0.0009(6) C18 0.0439(9) 0.0652(11) 0.0409(8) 0.0229(8) -0.0032(7) -0.0096(7) C19 0.0341(8) 0.0353(8) 0.0376(8) 0.0053(6) -0.0039(6) 0.0017(6) C20 0.0424(11) 0.0441(9) 0.0527(12) 0.0110(8) -0.0112(8) 0.0018(9) C21 0.0414(10) 0.0356(10) 0.0431(13) 0.0014(8) -0.0066(9) 0.0022(8) C19A 0.0341(8) 0.0353(8) 0.0376(8) 0.0053(6) -0.0039(6) 0.0017(6) C20A 0.0424(11) 0.0441(9) 0.0527(12) 0.0110(8) -0.0112(8) 0.0018(9) C21A 0.0414(10) 0.0356(10) 0.0431(13) 0.0014(8) -0.0066(9) 0.0022(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 O1 HO1 . . 106.1(14) ? C3 O2 C7 . . 117.83(10) ? C8 N1 N2 . . 118.14(11) ? C9 N2 N1 . . 118.74(10) ? C9 N2 HN2 . . 121.8(11) ? N1 N2 HN2 . . 118.3(11) ? C2 C1 C6 . . 118.76(12) ? C2 C1 C8 . . 121.27(11) ? C6 C1 C8 . . 119.97(11) ? O1 C2 C1 . . 123.27(11) ? O1 C2 C3 . . 116.91(11) ? C1 C2 C3 . . 119.82(11) ? O2 C3 C4 . . 125.61(11) ? O2 C3 C2 . . 113.71(11) ? C4 C3 C2 . . 120.68(12) ? C3 C4 C5 . . 119.52(12) ? C3 C4 H4 . . 120.2 ? C5 C4 H4 . . 120.2 ? C6 C5 C4 . . 120.36(12) ? C6 C5 H5 . . 119.8 ? C4 C5 H5 . . 119.8 ? C5 C6 C1 . . 120.86(12) ? C5 C6 H6 . . 119.6 ? C1 C6 H6 . . 119.6 ? O2 C7 H7A . . 109.5 ? O2 C7 H7B . . 109.5 ? H7A C7 H7B . . 109.5 ? O2 C7 H7C . . 109.5 ? H7A C7 H7C . . 109.5 ? H7B C7 H7C . . 109.5 ? N1 C8 C1 . . 119.85(11) ? N1 C8 H8 . . 120.1 ? C1 C8 H8 . . 120.1 ? O3 C9 N2 . . 123.24(12) ? O3 C9 C10 . . 123.52(12) ? N2 C9 C10 . . 113.23(11) ? C12 C10 C9 . . 109.42(10) ? C12 C10 C11 . . 113.75(11) ? C9 C10 C11 . . 108.38(11) ? C12 C10 H10 . . 108.4 ? C9 C10 H10 . . 108.4 ? C11 C10 H10 . . 108.4 ? C10 C11 H11A . . 109.5 ? C10 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C10 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C17 C12 C13 . . 118.13(12) ? C17 C12 C10 . . 122.10(11) ? C13 C12 C10 . . 119.77(11) ? C14 C13 C12 . . 121.14(12) ? C14 C13 H13 . . 119.4 ? C12 C13 H13 . . 119.4 ? C13 C14 C15 . . 120.75(13) ? C13 C14 H14 . . 119.6 ? C15 C14 H14 . . 119.6 ? C16 C15 C14 . . 117.78(12) ? C16 C15 C18 . . 119.51(14) ? C14 C15 C18 . . 122.71(14) ? C17 C16 C15 . . 121.48(13) ? C17 C16 H16 . . 119.3 ? C15 C16 H16 . . 119.3 ? C16 C17 C12 . . 120.70(13) ? C16 C17 H17 . . 119.6 ? C12 C17 H17 . . 119.6 ? C19A C18 C15 . . 128.4(7) ? C19 C18 C15 . . 116.46(13) ? C19 C18 H18A . . 108.2 ? C15 C18 H18A . . 108.2 ? C19 C18 H18B . . 108.2 ? C15 C18 H18B . . 108.2 ? H18A C18 H18B . . 107.3 ? C21 C19 C18 . . 113.35(14) ? C21 C19 C20 . . 110.26(15) ? C18 C19 C20 . . 109.95(14) ? C21 C19 H19 . . 107.7 ? C18 C19 H19 . . 107.7 ? C20 C19 H19 . . 107.7 ? C19 C20 H20A . . 109.5 ? C19 C20 H20B . . 109.5 ? H20A C20 H20B . . 109.5 ? C19 C20 H20C . . 109.5 ? H20A C20 H20C . . 109.5 ? H20B C20 H20C . . 109.5 ? C19 C21 H21A . . 109.5 ? C19 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C19 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C18 C19A C21A . . 111.2(18) ? C18 C19A C20A . . 112.3(16) ? C21A C19A C20A . . 132(2) ? C18 C19A H19A . . 96.7 ? C21A C19A H19A . . 96.7 ? C20A C19A H19A . . 96.7 ? C19A C20A H20D . . 109.5 ? C19A C20A H20E . . 109.5 ? H20D C20A H20E . . 109.5 ? C19A C20A H20F . . 109.5 ? H20D C20A H20F . . 109.5 ? H20E C20A H20F . . 109.5 ? C19A C21A H21D . . 109.5 ? C19A C21A H21E . . 109.5 ? H21D C21A H21E . . 109.5 ? C19A C21A H21F . . 109.5 ? H21D C21A H21F . . 109.5 ? H21E C21A H21F . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C2 . 1.3609(15) ? O1 HO1 . 0.847(9) ? O2 C3 . 1.3690(15) ? O2 C7 . 1.4265(15) ? O3 C9 . 1.2167(16) ? N1 C8 . 1.2847(17) ? N1 N2 . 1.3706(14) ? N2 C9 . 1.3594(17) ? N2 HN2 . 0.902(9) ? C1 C2 . 1.3999(17) ? C1 C6 . 1.4042(18) ? C1 C8 . 1.4545(17) ? C2 C3 . 1.4011(17) ? C3 C4 . 1.3802(18) ? C4 C5 . 1.397(2) ? C4 H4 . 0.9500 ? C5 C6 . 1.3751(19) ? C5 H5 . 0.9500 ? C6 H6 . 0.9500 ? C7 H7A . 0.9800 ? C7 H7B . 0.9800 ? C7 H7C . 0.9800 ? C8 H8 . 0.9500 ? C9 C10 . 1.5272(17) ? C10 C12 . 1.5174(17) ? C10 C11 . 1.5324(19) ? C10 H10 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 C17 . 1.3896(18) ? C12 C13 . 1.3907(18) ? C13 C14 . 1.3863(19) ? C13 H13 . 0.9500 ? C14 C15 . 1.393(2) ? C14 H14 . 0.9500 ? C15 C16 . 1.392(2) ? C15 C18 . 1.5146(19) ? C16 C17 . 1.381(2) ? C16 H16 . 0.9500 ? C17 H17 . 0.9500 ? C18 C19A . 1.453(8) ? C18 C19 . 1.513(2) ? C18 H18A . 0.9900 ? C18 H18B . 0.9900 ? C19 C21 . 1.505(3) ? C19 C20 . 1.529(2) ? C19 H19 . 1.0000 ? C20 H20A . 0.9800 ? C20 H20B . 0.9800 ? C20 H20C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C19A C21A . 1.50(3) ? C19A C20A . 1.50(3) ? C19A H19A . 1.0000 ? C20A H20D . 0.9800 ? C20A H20E . 0.9800 ? C20A H20F . 0.9800 ? C21A H21D . 0.9800 ? C21A H21E . 0.9800 ? C21A H21F . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 HO1 N1 . 0.847(9) 1.827(13) 2.5914(13) 149(2) yes N2 HN2 O1 4_575 0.902(9) 2.398(11) 3.2470(14) 156.8(14) yes N2 HN2 O2 4_575 0.902(9) 2.179(14) 2.8745(14) 133.4(14) yes C10 H10 O1 4_575 1.00 2.63 3.5545(16) 154.6 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C8 N1 N2 C9 . . . . 179.02(11) ? C6 C1 C2 O1 . . . . -179.68(12) ? C8 C1 C2 O1 . . . . 0.51(19) ? C6 C1 C2 C3 . . . . 0.03(18) ? C8 C1 C2 C3 . . . . -179.78(11) ? C7 O2 C3 C4 . . . . 2.85(19) ? C7 O2 C3 C2 . . . . -176.72(11) ? O1 C2 C3 O2 . . . . -0.43(16) ? C1 C2 C3 O2 . . . . 179.84(11) ? O1 C2 C3 C4 . . . . 179.97(11) ? C1 C2 C3 C4 . . . . 0.25(18) ? O2 C3 C4 C5 . . . . -179.74(13) ? C2 C3 C4 C5 . . . . -0.20(19) ? C3 C4 C5 C6 . . . . -0.1(2) ? C4 C5 C6 C1 . . . . 0.4(2) ? C2 C1 C6 C5 . . . . -0.4(2) ? C8 C1 C6 C5 . . . . 179.46(13) ? N2 N1 C8 C1 . . . . -178.45(11) ? C2 C1 C8 N1 . . . . -0.19(18) ? C6 C1 C8 N1 . . . . 180.00(12) ? N1 N2 C9 O3 . . . . 6.17(18) ? N1 N2 C9 C10 . . . . -173.84(10) ? O3 C9 C10 C12 . . . . 66.06(16) ? N2 C9 C10 C12 . . . . -113.93(12) ? O3 C9 C10 C11 . . . . -58.49(16) ? N2 C9 C10 C11 . . . . 121.52(12) ? C9 C10 C12 C17 . . . . -73.14(15) ? C11 C10 C12 C17 . . . . 48.22(17) ? C9 C10 C12 C13 . . . . 106.89(13) ? C11 C10 C12 C13 . . . . -131.75(13) ? C17 C12 C13 C14 . . . . -0.01(19) ? C10 C12 C13 C14 . . . . 179.96(11) ? C12 C13 C14 C15 . . . . -0.6(2) ? C13 C14 C15 C16 . . . . 0.3(2) ? C13 C14 C15 C18 . . . . 179.73(13) ? C14 C15 C16 C17 . . . . 0.7(2) ? C18 C15 C16 C17 . . . . -178.79(14) ? C15 C16 C17 C12 . . . . -1.3(2) ? C13 C12 C17 C16 . . . . 1.0(2) ? C10 C12 C17 C16 . . . . -179.00(13) ? C16 C15 C18 C19A . . . . -96.1(12) ? C14 C15 C18 C19A . . . . 84.4(13) ? C16 C15 C18 C19 . . . . -139.06(16) ? C14 C15 C18 C19 . . . . 41.5(2) ? C15 C18 C19 C21 . . . . 56.4(2) ? C15 C18 C19 C20 . . . . -179.71(16) ? C15 C18 C19A C21A . . . . -11(3) ? C15 C18 C19A C20A . . . . -170.6(16) ? _cod_database_fobs_code 2244139