#------------------------------------------------------------------------------
#$Date: 2022-10-21 02:51:57 +0100 (Fri, 21 Oct 2022) $
#$Revision: 278679 $
#$URL: svn://www.crystallography.net/cod/cif/2/24/41/2244199.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2244199
loop_
_publ_author_name
'Priyanka, Prabhakar'
'Jayanna, Bidarur K.'
Vinaya
'Shankara Prasad, Holehundi J.'
'Divakara, Thayamma R.'
'Yathirajan, Hemmige S.'
'Parkin, Sean'
_publ_section_title
;
 Synthesis and crystal structure of 2-chloro-1-(3-hydroxyphenyl)ethanone
;
_journal_coeditor_code           VM2272
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2056989022009835
_journal_volume                  78
_journal_year                    2022
_chemical_formula_iupac          'C8 H7 Cl O2'
_chemical_formula_moiety         'C8 H7 Cl O2'
_chemical_formula_sum            'C8 H7 Cl O2'
_chemical_formula_weight         170.59
_chemical_name_systematic
;
2-Chloro-1-(3-hydroxyphenyl)ethanone
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           'SHELXL-2019/2 and CIFFIX'
_cell_angle_alpha                90
_cell_angle_beta                 96.2940(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   4.9172(2)
_cell_length_b                   12.7016(4)
_cell_length_c                   11.8573(3)
_cell_measurement_reflns_used    9994
_cell_measurement_temperature    90.0(2)
_cell_measurement_theta_max      27.49
_cell_measurement_theta_min      2.36
_cell_volume                     736.10(4)
_computing_cell_refinement
;
<i>APEX3</i> (Bruker, 2016)
;
_computing_data_collection
;
<i>APEX3</i> (Bruker, 2016)
;
_computing_data_reduction
;
<i>APEX3</i> (Bruker, 2016)
;
_computing_molecular_graphics
;
<i>XP</i> in <i>SHELXTL</i> (Sheldrick, 2008)
;
_computing_publication_material
;
<i>SHELX</i> (Sheldrick, 2008) and <i>publCIF</i> (Westrip,
2010)
;
_computing_structure_refinement
;
<i>SHELXL2019/2</i> (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT</i> (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      90.0(2)
_diffrn_detector_area_resol_mean 7.41
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker D8 Venture dual source'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0283
_diffrn_reflns_av_unetI/netI     0.0183
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            12264
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.532
_diffrn_reflns_theta_min         2.357
_diffrn_source                   microsource
_exptl_absorpt_coefficient_mu    0.456
_exptl_absorpt_correction_T_max  0.971
_exptl_absorpt_correction_T_min  0.855
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(<i>SADABS</i>; Krause <i>et al.</i>,  2015)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.539
_exptl_crystal_description       'cut block'
_exptl_crystal_F_000             352
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.220
_exptl_crystal_size_min          0.190
_refine_diff_density_max         0.349
_refine_diff_density_min         -0.181
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.044
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     106
_refine_ls_number_reflns         1685
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.044
_refine_ls_R_factor_all          0.0267
_refine_ls_R_factor_gt           0.0243
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0323P)^2^+0.3660P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0651
_refine_ls_wR_factor_ref         0.0671
_reflns_number_gt                1569
_reflns_number_total             1685
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            vm2272sup1.cif
_cod_data_source_block           I
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2244199
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.895
_shelx_estimated_absorpt_t_max   0.918
_shelx_hkl_file
;
   1   0   0 0.60824 0.62384   3
   1   0   0 1.58002 1.04297   4
   1   0   0 1.55436 0.96419   5
  -1   0   0 -1.0400 0.63312   3
  -1   0   0 0.43364 0.90642   5
   2   0   0 539.896 18.7582   4
   2   0   0 514.199 18.1760   5
   2   0   0 529.232 18.2850   3
  -2   0   0 518.498 18.4295   3
   3   0   0 0.25649 1.31241   4
   3   0   0 2.85120 2.16231   5
   3   0   0 0.32106 1.20900   3
  -3   0   0 0.77069 1.40314   3
  -3   0   0 5.02249 2.44289   5
  -4   0   0 2619.87 81.5092   3
  -4   0   0 2540.99 81.5198   5
   4   0   0 2763.03 81.9810   4
   4   0   0 2783.45 80.8066   5
   4   0   0 2662.09 80.4556   3
   5   0   0 0.63649 3.46929   5
   5   0   0 0.86685 3.66769   4
   5   0   0 -3.1727 2.93998   3
   6   0   0 1.39582 4.05680   5
   6   0   0 1.41419 4.54299   4
   2  -1   0 174.245 8.55978   3
   2  -1   0 178.658 8.70918   4
   2  -1   0 186.397 8.47083   5
  -2  -1   0 195.643 8.89266   3
  -2  -1   0 180.387 9.96953   5
   2   1   0 182.823 8.79358   5
   2   1   0 181.621 8.47013   3
  -2   1   0 187.820 9.96435   3
  -3  -1   0 561.851 22.0978   3
   3  -1   0 588.644 21.6754   5
   3  -1   0 585.447 22.0684   3
  -3  -1   0 593.167 22.5960   5
   3  -1   0 644.479 23.1089   4
  -3   1   0 586.625 22.4927   3
  -3   1   0 551.660 22.0002   5
   3   1   0 598.773 22.8855   4
   3   1   0 603.161 22.2819   5
   3   1   0 588.213 21.8419   3
   4  -1   0 781.244 28.9919   3
  -4  -1   0 768.872 29.7680   3
  -4  -1   0 693.142 29.3025   5
   4  -1   0 743.308 29.4170   4
   4  -1   0 790.824 28.7196   5
  -4   1   0 716.008 31.3430   5
   4   1   0 807.684 29.0206   3
   4   1   0 785.329 29.2590   5
   4   1   0 797.977 30.2191   4
  -4   1   0 725.005 29.3736   3
   5  -1   0 119.032 11.2157   4
   5  -1   0 117.840 10.4561   5
   5   1   0 104.231 11.4041   3
   5   1   0 102.539 10.0622   4
   5   1   0 101.364 9.65906   5
   6  -1   0 176.527 17.6141   4
   6  -1   0 236.968 15.9940   5
   6   1   0 186.975 17.4155   4
   6   1   0 243.925 16.4936   5
  -6   1   0 216.705 16.2013   2
   0  -2   0 472.093 15.2181   4
   0  -2   0 519.779 14.7716   2
   0   2   0 490.862 14.2790   5
   0   2   0 499.402 14.7961   2
   0   2   0 462.764 15.1146   4
  -1  -2   0 4745.78 146.646   1
   1   2   0 4929.15 146.398   1
  -2  -2   0 1259.52 40.8451   5
   2  -2   0 1348.49 40.9521   4
   2  -2   0 1324.39 39.8703   5
  -2  -2   0 1320.94 40.3940   3
  -2   2   0 1385.92 41.2454   3
   2   2   0 1379.49 40.2709   3
   2   2   0 1352.95 41.0407   5
  -2   2   0 1376.26 41.0642   4
  -3  -2   0 2231.34 66.1132   3
   3  -2   0 2216.36 65.1325   5
  -3  -2   0 2157.75 66.5533   5
   3  -2   0 2281.11 66.6951   4
  -3   2   0 2195.06 66.0281   5
   3   2   0 2318.90 66.7209   5
  -3   2   0 2121.92 66.3948   4
   3   2   0 2167.75 65.3076   3
  -3   2   0 2159.77 66.6541   3
  -4  -2   0 88.0140 8.62896   5
   4  -2   0 96.1846 8.94791   4
   4  -2   0 116.785 8.80380   5
   4   2   0 84.2311 8.18872   4
   4   2   0 108.726 8.44314   3
  -4   2   0 106.373 8.94196   3
   4   2   0 97.1049 8.92342   5
   5  -2   0 1629.07 56.6492   4
   5  -2   0 1743.20 58.3416   5
   5   2   0 1562.07 55.1929   5
   5   2   0 1604.57 56.5124   4
   6  -2   0 2.51903 4.62179   5
   6   2   0 20.4898 5.65558   5
  -6   2   0 2.94563 3.73042   2
   0  -3   0 0.64502 0.82882   2
   0  -3   0 -0.2291 0.69578   4
   0   3   0 0.57164 0.67497   5
   0   3   0 1.16735 0.63261   5
   0   3   0 0.54247 0.77174   4
   0   3   0 0.24239 0.83159   2
  -1  -3   0 85.9988 4.59870   5
  -1  -3   0 89.5183 4.56928   3
   1  -3   0 95.8570 5.33339   4
   1  -3   0 86.1569 4.33520   5
  -1  -3   0 83.2507 4.83771   2
   1  -3   0 94.5294 4.96643   2
   1   3   0 85.4102 4.91453   5
   1   3   0 89.3720 4.55932   3
   1   3   0 86.3567 4.85816   2
  -1   3   0 85.0791 4.89098   4
  -1   3   0 97.7223 4.68325   5
  -1   3   0 93.2501 5.06390   2
   2  -3   0 52.4062 4.22958   5
  -2  -3   0 54.7080 4.79237   2
  -2  -3   0 59.2651 5.04140   5
  -2  -3   0 53.6966 4.47355   3
   2  -3   0 61.3448 5.12613   4
  -2   3   0 59.0719 4.70647   2
  -2   3   0 61.8678 5.16399   5
   2   3   0 57.7006 4.32470   3
   2   3   0 65.0980 5.27431   5
  -2   3   0 53.8420 4.94040   3
  -2   3   0 54.7791 4.80527   4
   3  -3   0 202.471 10.3798   5
  -3  -3   0 184.014 11.0028   5
  -3  -3   0 209.612 11.0112   3
   3  -3   0 209.452 11.3726   4
   3   3   0 212.264 11.5814   5
  -3   3   0 208.831 11.5992   3
  -3   3   0 200.783 11.1596   4
  -3   3   0 193.469 10.7136   5
  -3   3   0 201.573 11.1359   2
   3   3   0 195.862 10.2987   3
   4  -3   0 1109.27 36.3759   5
   4  -3   0 1037.86 37.9150   4
  -4  -3   0 1073.54 40.8607   5
  -4  -3   0 994.131 39.4392   3
   4   3   0 1010.44 37.2501   5
  -4   3   0 1026.60 37.3142   2
   4   3   0 1026.78 38.3165   4
   4   3   0 1077.94 36.5425   3
   5  -3   0 2.49870 2.77970   4
   5  -3   0 6.07597 4.31534   5
   5   3   0 3.74842 4.15240   4
   5   3   0 3.69749 3.99762   5
  -5   3   0 0.52782 2.55156   2
   5   3   0 -3.4048 2.76132   3
   6  -3   0 253.114 16.8184   5
  -6   3   0 298.552 19.5664   2
   6   3   0 262.770 20.0672   5
   6   3   0 231.990 16.0952   3
   6   3   0 245.533 18.2905   4
  -1  -4   0 2256.02 63.3588   3
  -2  -4   0 4459.68 155.913   1
   2  -4   0 4506.55 145.588   1
   2   4   0 4434.50 152.777   1
  -2   4   0 4684.83 148.419   1
  -3  -4   0 86.2109 6.94339   5
   3  -4   0 80.4893 6.95629   4
  -3  -4   0 91.9811 6.93132   3
  -3  -4   0 85.1267 7.29508   2
   3   4   0 88.6115 7.54475   5
   3   4   0 78.1669 6.36633   3
  -3   4   0 84.6067 7.24523   2
  -3   4   0 83.4573 6.60623   5
  -3   4   0 90.8558 7.38531   4
  -3   4   0 90.6668 7.45906   3
   4  -4   0 259.746 13.6849   5
  -4  -4   0 275.164 15.3365   2
   4  -4   0 259.819 15.1255   4
  -4  -4   0 275.393 15.0080   3
  -4   4   0 268.329 15.0049   2
   4   4   0 262.802 13.7480   3
   4   4   0 262.630 15.2333   5
   5  -4   0 65.1430 8.28092   5
   5  -4   0 81.1992 9.85472   4
   5   4   0 57.3572 8.75766   4
   5   4   0 82.3079 9.82825   5
  -5   4   0 76.9083 9.71017   2
   5   4   0 74.7399 8.18458   3
   6  -4   0 178.477 14.2656   5
   6  -4   0 134.945 13.2442   4
   6   4   0 157.516 14.3576   5
   6   4   0 156.833 12.8564   3
   6   4   0 174.683 14.4862   4
  -6   4   0 164.321 14.2504   2
   0  -5   0 2.48561 1.56593   4
   0  -5   0 1.37117 1.18695   2
   0   5   0 1.02432 1.06106   5
   0   5   0 2.47947 1.01443   5
   0   5   0 3.28442 1.74704   4
   0   5   0 0.98059 1.37663   2
  -1  -5   0 186.887 8.64749   2
   1  -5   0 168.389 9.05180   4
   1  -5   0 172.617 8.44043   2
   1  -5   0 167.297 6.57107   5
  -1  -5   0 171.430 7.26289   5
   1   5   0 182.083 7.99888   3
  -1   5   0 188.695 8.89606   2
  -1   5   0 162.889 8.65596   4
  -1   5   0 169.575 7.86906   5
   1   5   0 187.612 8.75452   2
   1   5   0 173.465 8.35808   5
  -2  -5   0 7.60171 2.35115   2
   2  -5   0 3.51968 1.61352   5
  -2  -5   0 2.05034 1.79590   5
   2  -5   0 2.15107 2.14546   4
  -2  -5   0 4.35644 1.66171   3
  -2   5   0 3.90097 1.65847   3
  -2   5   0 4.70891 1.62428   5
  -2   5   0 6.09863 2.31946   4
  -2   5   0 5.03459 2.04914   2
   2   5   0 3.94993 2.19151   5
   2   5   0 4.74922 1.57223   3
   3  -5   0 102.322 8.35632   4
  -3  -5   0 86.3467 7.00573   3
   3  -5   0 105.237 7.04381   5
  -3  -5   0 97.9470 7.93449   2
  -3  -5   0 105.677 8.09128   5
  -3   5   0 97.0531 7.64137   4
  -3   5   0 91.5266 7.78193   2
   3   5   0 95.3846 7.12536   3
   3   5   0 98.8049 7.92118   5
  -3   5   0 85.0004 9.17191   3
  -3   5   0 100.036 7.25731   5
  -4  -5   0 106.513 9.54587   2
   4  -5   0 118.364 8.74401   5
   4  -5   0 106.505 9.52274   4
  -4  -5   0 102.563 8.79914   3
  -4   5   0 108.624 9.38714   2
   4   5   0 95.6202 9.40872   5
   4   5   0 120.387 8.78448   3
   5  -5   0 1191.38 42.2188   5
   5  -5   0 1216.01 46.0816   4
   5   5   0 1160.77 45.8052   4
  -5   5   0 1285.23 46.2756   2
   5   5   0 1195.61 45.2746   5
   5   5   0 1234.51 43.2025   3
   6  -5   0 48.7692 8.22783   5
   6  -5   0 81.0784 10.0784   4
   6   5   0 67.3650 10.5096   5
   6   5   0 60.3067 10.0545   4
  -6   5   0 80.9817 11.1253   2
   6   5   0 68.8182 8.92333   3
   0  -6   0 28.0901 4.32613   4
   0  -6   0 30.4095 3.85859   2
   0   6   0 27.9770 3.48782   5
   0   6   0 26.3202 2.79347   5
   0   6   0 24.4046 3.19099   2
   0   6   0 28.1423 4.23896   4
   1  -6   0 2224.75 64.8994   2
  -1  -6   0 2337.95 65.2861   2
  -1  -6   0 2254.46 62.2380   5
   1  -6   0 2070.79 66.3500   4
  -1   6   0 2204.77 65.2840   2
  -1   6   0 2220.94 65.6355   4
  -1   6   0 2249.66 64.0953   5
   1   6   0 2193.84 64.4718   5
   1   6   0 2265.49 67.3116   4
   1   6   0 2231.62 65.2833   2
   1   6   0 2257.37 64.1404   3
  -2  -6   0 644.807 23.5222   2
   2  -6   0 644.468 24.5233   4
   2  -6   0 648.664 20.9766   5
  -2  -6   0 638.913 22.3123   5
  -2  -6   0 667.832 24.1706   3
  -2   6   0 597.164 23.4236   2
   2   6   0 624.355 23.5846   5
  -2   6   0 610.229 22.1494   5
  -2   6   0 655.299 23.8219   4
   2   6   0 666.381 22.5121   3
  -2   6   0 657.742 23.9690   3
   2   6   0 631.621 23.2344   2
   3  -6   0 1125.60 39.0134   4
  -3  -6   0 1136.32 36.8366   3
  -3  -6   0 1065.59 37.8347   2
  -3  -6   0 1131.39 37.4521   5
   3  -6   0 1091.20 35.2357   5
  -3   6   0 1084.34 38.6841   3
   3   6   0 1110.61 38.4756   5
  -3   6   0 1094.71 38.1302   2
   3   6   0 1086.42 36.1585   3
  -3   6   0 1102.57 36.7365   5
  -3   6   0 1044.07 37.5905   4
   4  -6   0 233.669 12.7334   5
  -4  -6   0 233.479 14.5535   2
  -4  -6   0 234.467 15.6166   3
   4   6   0 235.937 13.0302   3
  -4   6   0 256.870 15.0811   2
   4   6   0 252.772 15.2977   5
   5  -6   0 51.8913 7.36420   5
   5  -6   0 58.9495 8.28913   4
   5   6   0 71.0204 7.82465   3
  -5   6   0 60.7259 8.19790   2
   5   6   0 43.4643 8.22397   5
   5   6   0 63.6129 9.54600   4
   0  -7   0 0.56461 1.33217   2
   0  -7   0 1.77408 2.24625   4
   0   7   0 1.94798 1.51916   5
   0   7   0 0.19385 1.27146   2
   0   7   0 0.34863 1.03987   5
   0   7   0 0.07166 1.83580   4
  -1  -7   0 40.1517 2.77132   5
  -1  -7   0 42.1940 4.46016   2
   1  -7   0 34.0162 4.96203   4
   1  -7   0 32.9808 3.82861   2
   1   7   0 35.5838 3.91036   3
   1   7   0 37.6910 4.24616   5
   1   7   0 36.6726 4.38696   2
  -1   7   0 35.9372 4.03074   5
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   0  -2  -1 2309.74 72.5116   1
   0   2   1 2093.73 71.7316   1
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   1   2   1 2048.28 73.6068   1
   3  -2   1 174.719 9.31515   5
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   3   2   1 171.771 10.0419   3
   3   2   1 174.685 10.3235   5
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   4  -2   1 823.826 29.7682   5
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   4   2   1 821.503 31.9995   4
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   5   2   1 142.851 12.4240   4
   5   2   1 130.639 11.6890   5
   5   2   1 152.925 11.3615   3
   6  -2   1 434.500 22.0383   5
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   6   2   1 452.471 23.0923   5
   6   2   1 394.328 22.1258   3
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   6   3  -1 347.687 23.1359   5
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   5  -3  -1 183.436 14.0737   4
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   5   3  -1 184.485 11.8551   3
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   1   3   1 171.860 7.66040   3
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   2  -3   1 5.32572 1.56352   5
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   4  -3   1 465.278 21.4241   4
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   4   3   1 480.012 22.1202   4
   4   3   1 473.181 20.9929   3
   4   3   1 479.669 21.6794   5
   5  -3   1 1101.58 41.6285   4
   5  -3   1 1063.63 38.2678   5
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   5   3   1 1098.61 40.7778   5
   5   3   1 1047.42 39.7495   3
   5   3   1 1075.81 41.6433   4
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   6  -3   1 4.38085 4.37814   4
   6   3   1 5.16947 4.42698   3
   6   3   1 5.55382 3.80491   4
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   6  -4  -1 444.451 24.7983   4
   6   4  -1 403.577 23.3322   5
   6   4  -1 374.813 23.1883   4
   5  -4  -1 576.145 25.1043   5
   5  -4  -1 564.314 27.1325   4
   5   4  -1 525.377 26.2836   4
   5   4  -1 555.015 23.9964   3
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   4  -4  -1 43.1372 6.45157   5
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   4   4  -1 40.5245 6.56743   5
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   4   4   1 150.089 10.5491   3
   5  -4   1 389.825 18.3481   5
   5  -4   1 365.935 20.2609   4
   5   4   1 309.495 19.3344   5
   5   4   1 362.302 19.1046   3
   5   4   1 366.500 20.5900   4
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   6  -4   1 100.770 11.5756   4
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   6   4   1 127.756 12.2253   5
   6   4   1 107.300 10.9179   3
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   4   5  -1 353.360 18.0262   5
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   1   5  -1 3480.16 113.493   1
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   4   5   1 986.832 36.2893   3
   5  -5   1 70.6365 8.12940   5
   5  -5   1 72.2487 9.75098   4
   5   5   1 78.3676 10.0854   4
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   5   5   1 66.8403 9.43506   5
   5   5   1 62.3224 8.04955   3
   6  -5   1 30.1643 7.21111   4
   6   5   1 29.4743 7.12691   4
   5  -6  -1 188.943 12.7600   5
   5  -6  -1 155.615 13.3141   4
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   5   6  -1 182.405 11.9176   3
   5   6  -1 167.038 13.7162   4
   5   6  -1 168.025 13.6558   5
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   4  -6  -1 245.595 13.5231   5
   4  -6  -1 224.025 17.0887   4
   4   6  -1 236.338 12.5943   3
   4   6  -1 267.364 17.3810   5
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   3  -6  -1 366.001 16.1795   5
   3   6  -1 373.313 17.6411   5
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   3   6  -1 370.003 15.3284   3
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   2   6  -1 19.2496 2.68869   3
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   1  -6  -1 1830.75 56.2891   2
   1  -6  -1 1927.20 54.8741   5
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   1   6  -1 1941.08 54.5098   3
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   1   6  -1 1846.12 54.8594   5
   1   6  -1 1893.87 58.1058   4
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   0  -6   1 4173.45 125.660   1
   0   6   1 3914.00 136.281   1
   0   6  -1 4120.47 127.843   1
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   3   6   1 124.143 8.50865   3
  -3   6  -1 120.843 9.43402   3
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   2   0  -2 1749.65 50.5244   5
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   3   0   2 -0.0314 1.76335   5
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   5   0   2 -0.7004 3.48905   5
   5   0   2 0.77335 3.52827   4
   5   0   2 -1.6546 2.07452   3
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   6   0   2 219.483 15.3825   5
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   6   1  -2 592.127 28.5881   5
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   6   1  -2 573.348 29.5661   4
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   5  -1  -2 118.689 10.8346   5
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   5   1  -2 126.908 11.5237   4
   5   1  -2 148.181 12.0638   5
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   4  -1  -2 38.0923 5.43376   5
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   4   1  -2 60.0912 6.62141   4
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   4   1  -2 47.3729 6.60526   5
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   3  -1  -2 2212.70 63.8620   4
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   3   1  -2 2175.91 63.7699   4
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   3   1  -2 1998.76 62.6822   5
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   2  -1  -2 193.315 9.39428   5
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   2   1  -2 195.438 9.56382   4
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   2   1  -2 196.565 9.39521   5
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   0  -1  -2 2414.55 78.5986   1
   0   1  -2 2615.43 71.1538   1
   0   1   2 2286.79 78.2013   1
   1  -1   2 1605.95 45.3880   5
   1   1   2 1634.36 47.2279   5
   2  -1   2 29.4464 3.77045   3
   2  -1   2 25.5390 3.01330   5
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   2  -1   2 30.8584 3.30433   4
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   2   1   2 37.2113 3.69377   5
   2   1   2 36.4704 4.11683   3
   3  -1   2 123.691 8.17090   4
   3  -1   2 109.974 7.37668   5
   3  -1   2 112.627 8.11985   3
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   3   1   2 121.277 8.38260   3
   3   1   2 119.829 8.27728   4
   3   1   2 116.750 8.08016   5
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   4  -1   2 533.098 21.8147   5
   4  -1   2 533.670 23.1724   4
   4  -1   2 578.432 23.9809   3
   4   1   2 590.107 24.3774   4
   4   1   2 523.041 22.5433   5
   4   1   2 562.868 23.6632   3
   5  -1   2 1220.34 41.9482   5
   5  -1   2 1210.25 44.1495   3
   5  -1   2 1176.14 43.9073   4
   5   1   2 1128.30 43.2437   3
   5   1   2 1188.55 42.7353   5
   5   1   2 1173.18 44.1055   4
   6  -1   2 996.325 38.2053   5
   6   1   2 960.393 38.8708   5
   6   1   2 993.438 40.1966   3
   6  -2  -2 4.15038 4.65610   5
   6   2  -2 -3.6411 4.09975   5
   6   2  -2 -1.5831 3.31161   4
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   5  -2  -2 935.558 38.1954   4
   5  -2  -2 979.638 37.2442   5
   5   2  -2 1026.37 38.1768   5
   5   2  -2 977.069 38.6118   4
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   4  -2  -2 101.644 8.68869   4
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   4  -2  -2 119.979 9.38953   5
   4   2  -2 101.271 9.14904   4
  -4   2   2 98.8138 8.73747   3
   4   2  -2 91.0703 8.52828   5
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   3  -2  -2 7381.31 224.941   1
  -3  -2   2 6449.57 226.067   1
   3   2  -2 6814.27 223.499   1
  -3   2   2 7220.06 228.776   1
  -2  -2   2 652.171 20.2978   3
   2  -2  -2 658.109 22.2981   4
   2  -2  -2 634.299 21.6979   5
  -2  -2   2 616.970 21.2273   5
  -2   2   2 633.325 21.9393   4
   2   2  -2 620.572 19.8078   3
  -2   2   2 631.775 21.6571   5
   2   2  -2 638.041 21.6739   5
  -2   2   2 597.996 21.1821   2
  -2   2   2 681.274 21.9439   3
   0  -2  -2 815.671 25.9059   5
   0  -2  -2 897.879 26.7072   5
   0  -2  -2 909.224 26.6073   2
   0  -2  -2 829.355 26.1673   4
   0  -2   2 882.599 24.8247   4
   0   2   2 925.760 26.6719   5
   0   2   2 918.717 26.3734   4
   0   2  -2 879.476 24.7506   4
   0   2   2 840.762 26.2908   3
   0   2   2 853.718 26.1563   5
   0   2   2 865.452 26.5711   2
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   1   2   2 6746.07 208.904   1
   2  -2   2 936.363 27.8715   5
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   2  -2   2 941.651 28.9393   5
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   2  -2   2 941.620 29.4232   4
   2  -2   2 888.305 30.2166   3
   2   2   2 908.785 30.2779   3
  -2   2  -2 896.783 30.4321   3
  -2   2  -2 937.958 31.2823   4
  -2   2  -2 989.471 30.7251   5
   2   2   2 865.591 29.7490   5
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   3  -2   2 2489.58 74.4682   4
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   3  -2   2 2454.73 75.1322   3
  -3   2  -2 2648.70 76.5302   3
  -3   2  -2 2494.09 74.4448   5
   3   2   2 2472.15 75.0723   3
   3   2   2 2694.66 75.3544   5
   4  -2   2 48.0941 6.11700   5
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   4  -2   2 62.7643 7.59073   3
   4  -2   2 67.2987 7.65247   4
   4   2   2 58.4426 7.27028   3
   4   2   2 61.5837 7.07321   4
   4   2   2 66.8915 7.76498   5
   5  -2   2 47.0302 6.97600   3
   5  -2   2 64.3378 7.76266   4
   5  -2   2 50.5380 7.20998   5
   5   2   2 51.7429 8.16253   4
   5   2   2 54.2286 8.22075   5
   5   2   2 54.4628 8.09370   3
   6  -2   2 45.4249 8.50392   5
   6   2   2 21.5600 6.62162   4
   6   2   2 34.6372 6.84606   3
   6   2   2 26.8537 6.85700   5
   6  -3  -2 23.1373 6.65658   5
   6  -3  -2 11.4509 5.33759   4
  -6   3   2 8.30881 4.73089   2
   5  -3  -2 21.5548 5.64503   5
   5  -3  -2 27.7412 5.89862   4
   5   3  -2 26.2275 5.96872   5
  -5   3   2 18.8703 5.43409   2
   5   3  -2 23.8656 6.19247   4
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   4  -3  -2 98.6214 8.90179   4
   4  -3  -2 106.067 9.15830   5
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  -4   3   2 108.647 9.04458   2
   4   3  -2 117.933 7.84083   3
   4   3  -2 119.746 9.98806   4
  -4   3   2 107.556 9.06190   3
   4   3  -2 110.585 9.03835   5
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   3  -3  -2 1205.92 40.8677   4
   3  -3  -2 1320.98 40.4565   5
  -3   3   2 1251.87 40.1615   2
   3   3  -2 1200.99 40.2284   5
  -3   3   2 1256.88 40.6143   3
   3   3  -2 1181.36 37.6860   3
  -3   3   2 1176.74 40.4662   4
  -3   3   2 1239.10 40.1782   5
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   2  -3  -2 1406.87 42.5130   4
  -2  -3   2 1433.51 40.3852   2
   2  -3  -2 1324.22 41.5973   5
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  -2   3   2 1295.40 41.7667   4
   2   3  -2 1364.52 41.4859   5
  -2   3   2 1361.88 41.5480   5
   2   3  -2 1386.73 39.2537   3
  -2   3   2 1373.72 41.7582   2
  -1  -3   2 2686.58 82.3407   1
   1  -3  -2 2303.40 84.4457   1
   1   3  -2 2585.55 80.4240   1
  -1   3   2 2359.29 85.9231   1
   0   3   2 1904.01 54.4768   5
   0   3   2 1877.14 54.3924   4
   1  -3   2 406.385 13.4026   4
  -1  -3  -2 377.465 14.7811   2
  -1  -3  -2 372.021 14.2906   3
   1  -3   2 381.803 13.6926   3
  -1  -3  -2 346.867 14.0644   5
   1   3   2 401.044 14.9540   2
   1   3   2 411.472 15.2567   5
  -1   3  -2 385.453 11.7345   5
  -1   3  -2 378.993 13.0460   4
  -1   3  -2 381.686 13.8400   3
   1   3   2 388.246 14.4426   5
   1   3   2 337.018 13.9133   3
  -2  -3  -2 721.006 26.6761   2
   2  -3   2 765.241 26.1601   3
   2  -3   2 760.462 25.3053   4
   2  -3   2 772.189 23.8117   5
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   2  -3   2 757.287 23.0510   5
  -2   3  -2 775.538 25.3710   4
   2   3   2 767.341 26.5264   5
   2   3   2 747.570 27.0900   5
   2   3   2 766.121 26.2724   3
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  -2   3  -2 728.542 24.3267   5
   3  -3   2 1216.29 40.5716   3
   3  -3   2 1218.93 37.5284   5
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   3  -3   2 1221.84 40.0330   4
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   3   3   2 1284.68 40.9920   5
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   4  -3   2 687.385 28.6488   3
   4  -3   2 734.364 28.7818   4
   4  -3   2 720.118 26.0292   5
   4   3   2 724.130 28.7152   3
   4   3   2 735.007 29.5488   4
   4   3   2 705.523 28.3731   5
   5  -3   2 59.3914 8.33157   4
   5  -3   2 66.9643 7.89893   5
   5   3   2 44.3397 7.75187   5
   5   3   2 48.2373 8.19938   4
   5   3   2 49.8249 6.96366   3
   6  -3   2 238.254 15.5646   5
   6  -3   2 202.842 18.8404   4
   6   3   2 238.375 16.2050   3
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   6   3   2 250.244 17.4821   5
   6   3   2 241.854 17.4829   4
   6  -4  -2 175.527 15.0262   5
   6  -4  -2 181.560 15.3770   4
   6   4  -2 183.337 15.2445   4
   6   4  -2 207.844 16.1604   5
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   5   4  -2 134.536 11.6274   4
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   4  -4  -2 1739.04 56.5090   4
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   4   4  -2 1660.32 55.9764   4
   4   4  -2 1749.85 52.1861   3
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   4   4  -2 1692.75 55.3456   5
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   3  -4  -2 899.911 31.3266   4
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   2   4  -2 1129.31 32.7441   3
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   2   4  -2 1168.23 35.4565   5
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   1  -4   2 4963.27 143.048   1
   1   4   2 5152.01 164.393   1
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   2  -4   2 1257.27 41.3070   3
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   2   4   2 1326.10 43.1456   5
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   2   4   2 1237.05 43.5071   3
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   2   4   2 1406.91 42.6543   5
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   3  -4   2 17.6850 3.88578   4
   3  -4   2 16.2265 3.77061   5
   3  -4   2 17.4717 3.95483   3
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   3   4   2 14.0496 3.21697   3
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   4  -4   2 200.078 10.8006   5
   4  -4   2 182.832 11.1844   5
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   4  -4   2 213.930 13.3022   4
   4   4   2 207.461 12.8226   3
   4   4   2 201.507 13.3583   5
   5  -4   2 31.1819 6.53774   5
   5  -4   2 28.7136 5.30305   5
   5  -4   2 25.5417 5.72074   4
   5   4   2 32.5140 6.73073   3
   5   4   2 36.1379 7.13018   4
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   5   4   2 27.0793 6.56263   5
   6  -4   2 7.97771 4.77476   4
   6   4   2 11.2036 5.67021   5
   6   4   2 0.18508 4.88231   4
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   6   4   2 6.52575 3.96998   3
   6  -5  -2 191.385 15.6336   5
   6  -5  -2 198.636 16.4550   4
   6   5  -2 195.436 16.4864   4
   6   5  -2 200.668 16.4804   5
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   5  -5  -2 94.1813 10.7847   4
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   5   5  -2 59.4648 8.87365   4
   5   5  -2 62.5644 6.83287   3
   5   5  -2 63.4260 8.87136   5
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   4  -5  -2 771.561 28.8109   5
   4  -5  -2 758.009 30.2871   4
   4   5  -2 724.786 29.2260   5
   4   5  -2 701.679 25.5378   3
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   3  -5  -2 606.016 23.8526   5
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   3  -5  -2 656.996 25.7686   4
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   3   5  -2 638.859 21.6694   3
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   3   5  -2 638.626 24.7011   5
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   2  -5  -2 351.262 15.2211   2
   2  -5  -2 373.340 16.3620   4
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   2   5  -2 382.622 12.7225   3
   2   5  -2 356.642 14.8030   5
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   0  -5   2 208.140 8.36269   2
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   0   5   2 204.128 9.63076   5
   0   5  -2 221.580 9.74922   4
   0   5   2 223.446 10.5854   5
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   1   5   2 251.843 12.3426   2
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   1   5   2 269.245 11.9592   3
   1   5   2 281.040 12.9423   5
   1   5   2 259.085 12.0582   5
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   2   5   2 289.828 14.3903   5
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   2   5   2 278.736 13.6625   5
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   3  -5   2 193.917 8.73114   5
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   3   5   2 203.957 12.1983   5
   3   5   2 202.013 11.8667   3
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   4  -5   2 132.431 8.78777   5
   4  -5   2 130.692 10.8865   4
   4   5   2 154.009 13.6701   5
   4   5   2 151.604 11.1246   3
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   5  -5   2 1338.74 50.1380   4
   5  -5   2 1379.76 44.8178   5
   5   5   2 1369.79 49.1620   3
   5   5   2 1346.88 50.8746   4
   5   5   2 1441.63 50.7425   5
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   5  -6  -2 123.090 12.4575   4
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   5   6  -2 121.489 11.4030   4
   5   6  -2 116.922 9.11326   3
   5   6  -2 130.821 11.4597   5
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   4  -6  -2 476.091 23.4527   4
   4  -6  -2 474.802 21.3269   5
   4   6  -2 469.830 18.7489   3
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   3  -6  -2 744.481 27.1607   5
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   3   6  -2 756.103 27.8939   5
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   2   6  -2 1185.38 38.7194   5
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   2   6  -2 1117.88 33.4704   3
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   1  -6  -2 86.6924 6.23265   5
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   1   6  -2 88.2917 6.80122   4
   1   6  -2 86.6302 4.93850   5
   1   6  -2 85.1345 5.31303   2
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   0   6  -2 3.45414 1.53683   2
   0   6   2 -0.8254 1.49331   2
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   1   6   2 1561.27 49.5314   5
   1   6   2 1615.43 53.3723   2
   1   6   2 1645.20 50.7145   5
   1   6   2 1607.99 49.5201   3
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   1   6   2 1581.48 51.1617   4
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   2   6   2 1315.65 42.4093   2
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   3   6   2 669.820 26.3290   3
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  -3   6  -2 669.782 27.4035   3
   3   6   2 684.604 27.4546   5
   3   6   2 603.070 27.4169   5
   4  -6   2 162.020 12.0451   4
   4  -6   2 187.473 9.27817   5
   4   6   2 183.424 13.2212   5
   4   6   2 175.563 12.3068   3
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   5  -6   2 135.425 9.90415   5
   5  -6   2 142.044 13.0286   4
   5   6   2 129.246 11.4151   3
   5   6   2 138.926 12.8608   5
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   5  -7  -2 88.5319 10.0832   5
   5  -7  -2 75.7472 9.81568   4
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   5   7  -2 82.0963 10.0353   5
   5   7  -2 78.3270 7.34755   3
   5   7  -2 81.1255 10.5937   4
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   4  -7  -2 0.00660 3.67972   5
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   4   7  -2 0.49049 1.72623   3
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   4   7  -2 3.48436 2.96427   5
   3  -7  -2 324.553 17.7739   4
   3  -7  -2 314.987 15.3339   5
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   3   7  -2 307.864 15.8685   5
  -3   7   2 291.106 17.7467   4
   3   7  -2 311.260 12.7672   3
  -3   7   2 332.229 16.9648   2
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   2  -7  -2 2240.43 67.8607   2
   2  -7  -2 2193.83 69.7117   4
   2  -7  -2 2248.23 66.7896   5
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   2   7  -2 2273.29 63.5828   3
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  -2   7   2 2279.78 66.9484   5
   2   7  -2 2263.17 66.6706   5
  -2   7   2 2127.40 68.2651   2
  -2   7   2 2293.88 68.5548   4
   1  -7  -2 586.694 21.1637   5
   1  -7  -2 584.079 22.1365   2
   1  -7  -2 590.964 23.8083   4
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   1   7  -2 573.763 19.5360   5
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  -1   7   2 576.089 22.8913   2
   1   7  -2 590.606 20.4504   2
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   1   7  -2 598.019 23.0843   4
   1   7  -2 575.609 19.0694   3
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   0  -7  -2 2575.71 80.2425   4
   0   7   2 2740.63 80.1390   4
   0   7   2 2533.11 78.5291   5
   0   7   2 2894.04 80.1416   2
   0   7  -2 2776.15 78.6834   4
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   1   7   2 32.2179 4.45742   5
   1   7   2 24.4716 3.90811   2
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   1   7   2 31.5937 4.52656   5
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   2   7   2 2683.92 82.3004   5
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   2   7   2 2802.93 81.5927   5
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   2   7   2 2879.89 80.8533   3
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   2   7   2 2567.54 81.0730   2
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   3  -7   2 93.6012 8.37637   4
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   3   7   2 75.0819 7.20333   3
  -3   7  -2 73.7677 7.16023   4
   3   7   2 88.7384 8.40731   5
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   4  -7   2 1417.91 50.9133   4
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   4   7   2 1419.14 49.5355   3
   4   7   2 1524.92 52.0418   5
   5  -7   2 2.56961 2.50330   5
   5  -7   2 3.40414 4.77120   5
   5  -7   2 4.78605 3.54054   4
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   5   7   2 9.27980 4.77949   5
   5   7   2 2.70968 4.02049   3
   5  -8  -2 44.3323 8.03217   4
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   5   8  -2 53.8703 9.16215   5
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   4   8  -2 134.455 8.53542   3
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   4   8  -2 141.994 11.8752   5
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   3  -8  -2 1075.22 40.6448   4
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   3   8  -2 1078.94 38.2478   5
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   2  -8  -2 1522.57 49.7135   2
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   2   8  -2 1633.99 47.7842   2
   2   8  -2 1537.73 45.4463   3
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   0   8   2 840.905 28.7094   5
   0   8   2 781.401 29.7145   2
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   4   8   2 412.365 21.9675   5
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   5   8   2 267.194 16.7473   3
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   5   9  -2 502.557 28.9656   5
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   4   9  -2 80.1537 9.50634   5
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   4   9  -2 88.2923 6.80548   3
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   3   9  -2 1255.16 42.5012   5
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   3   9  -2 1182.71 37.1128   3
   2  -9  -2 82.0256 9.42049   4
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   2  -9  -2 78.7245 7.30519   2
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   2   9  -2 76.0104 7.07192   5
   2   9  -2 81.6331 5.66982   3
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   1   9   2 2632.03 78.6191   3
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   1   9   2 2580.84 79.8468   5
   1   9   2 2601.02 80.1195   2
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   2   9   2 349.258 18.9594   5
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   2   9   2 392.114 17.8583   3
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  -1  14   2 85.9381 10.9274   2
   1  14  -2 66.5701 10.4333   5
   1  14  -2 81.6203 9.00512   2
   1  14  -2 87.7578 7.71431   3
   1  14  -2 83.4976 8.54415   5
   0  14   2 1148.83 44.0251   2
   0  14   2 1029.03 40.7888   3
   0  14  -2 989.840 38.3275   5
   0  14   2 1060.66 40.8631   5
   0  14  -2 1091.04 40.8967   2
   0  14  -2 1068.66 37.4923   5
  -1  14  -2 256.508 14.9499   5
   1  14   2 219.790 16.9030   2
   1  14   2 251.055 16.9809   5
   1  14   2 231.749 15.9500   3
  -1  14  -2 258.479 16.7970   2
  -1  14  -2 267.754 13.9013   5
   2 -14   2 620.492 31.7906   4
   2  14   2 694.305 29.2561   3
   2  14   2 642.705 30.6233   5
   2  14   2 615.333 30.4727   2
  -2  14  -2 688.782 31.1930   2
   3 -14   2 98.4718 11.9025   4
  -3  14  -2 99.8719 9.66077   5
   3  14   2 87.5196 10.0939   3
   3  14   2 98.8948 11.3170   5
  -3  14  -2 115.091 12.5404   2
   2 -15  -2 72.4049 14.4569   4
  -2  15   2 50.6789 10.0146   2
   2  15  -2 71.7084 9.16735   5
  -2  15   2 57.6835 8.76344   5
   2  15  -2 46.7827 8.25042   2
   1  15  -2 87.6326 11.3912   2
  -1  15   2 111.313 12.8657   2
   1  15  -2 107.706 10.1357   5
  -1  15   2 97.9807 11.1469   5
   0  15   2 135.876 12.2587   3
   0  15   2 138.816 13.1407   2
   0  15  -2 147.545 12.3631   5
   0  15  -2 159.573 13.1146   2
   0  15   2 135.510 12.9237   5
   0  15  -2 165.655 12.0002   3
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   1  15   2 141.866 12.8783   3
   1  15   2 173.547 15.2993   2
   1  15   2 149.181 13.6180   5
   2 -15   2 172.953 16.5899   4
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   2  15   2 209.103 16.5163   5
   2  15   2 203.333 16.5781   2
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   2  15   2 218.223 15.2534   3
   1  16  -2 492.758 23.9965   5
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   1  16  -2 476.484 24.1963   2
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   0  16   2 41.5650 9.03511   2
   0  16   2 57.5313 9.59563   5
   0  16  -2 46.1188 7.34331   3
   0  16  -2 65.8816 9.57150   2
   0  16   2 36.2442 7.40805   3
   0  16  -2 44.1272 7.50231   5
   1  16   2 544.200 31.5978   5
   1  16   2 592.030 30.3242   2
  -1  16  -2 592.244 25.5544   5
   1  16   2 541.611 27.6555   3
   6   0  -3 3.97800 4.15059   4
   6   0  -3 -3.0960 2.92591   5
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   5   0  -3 188.940 13.9406   4
   5   0  -3 173.497 13.3183   5
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  -4   0   3 1.78456 1.84405   3
  -4   0   3 -0.8327 2.14677   2
   4   0  -3 0.40361 2.73000   5
   4   0  -3 0.53357 2.12525   4
   3   0  -3 177.199 10.1340   4
  -3   0   3 183.335 10.1146   5
   3   0  -3 173.212 10.0524   5
  -3   0   3 175.974 10.2898   2
  -3   0   3 168.068 9.09515   3
  -2   0   3 0.58371 0.93925   3
  -2   0   3 0.66300 1.39578   5
   2   0  -3 1.06806 1.18245   4
  -2   0   3 0.65130 1.26696   4
  -2   0   3 -1.1185 0.81008   2
  -2   0   3 0.46654 1.23329   5
   2   0  -3 2.16934 1.35006   5
   0   0   3 1.20054 0.57038   5
   0   0  -3 -0.6887 0.77315   3
   0   0  -3 -0.1145 0.68617   5
   0   0  -3 0.05312 0.58765   2
   0   0   3 -0.3417 0.66660   2
   0   0  -3 1.30656 0.77407   5
   0   0   3 -0.2190 0.77426   3
   0   0   3 0.28995 0.53331   5
   0   0   3 0.43811 0.40207   4
  -1   0  -3 5.02672 1.85103   3
  -1   0  -3 3.78425 1.36891   5
   1   0   3 5.48599 1.75103   3
  -1   0  -3 7.47897 1.90203   5
   1   0   3 3.22652 1.28236   5
   1   0   3 3.49209 1.16043   5
   2   0   3 0.13912 1.23980   4
  -2   0  -3 1.93037 1.51904   5
  -2   0  -3 -0.5669 1.56044   3
   2   0   3 0.66551 1.52737   5
   2   0   3 -1.2017 0.99177   5
  -3   0  -3 3687.28 105.908   5
   3   0   3 3660.67 106.300   3
  -3   0  -3 3729.19 107.088   3
   3   0   3 3559.61 105.553   5
   3   0   3 3600.50 104.958   4
   4   0   3 -2.4453 1.56524   4
   4   0   3 -1.0419 2.57729   5
   4   0   3 2.50431 2.97282   3
   4   0   3 -4.4264 2.84966   5
   5   0   3 466.911 23.8485   3
   5   0   3 505.336 24.1683   4
   6   0   3 5.17977 4.49908   4
   6   0   3 1.19765 3.43871   3
   6   0   3 -7.1293 4.02288   5
   6  -1  -3 4.31074 4.91260   5
  -6  -1   3 -1.4446 4.10765   2
   6  -1  -3 2.60909 4.31903   4
   6   1  -3 -0.6260 4.46118   5
  -6   1   3 -4.5570 2.59562   2
   6   1  -3 1.66186 4.86868   4
  -5  -1   3 865.536 32.8752   2
   5  -1  -3 842.286 34.3630   5
   5  -1  -3 902.576 35.8851   4
  -5   1   3 893.718 34.2018   2
   5   1  -3 869.226 34.6844   5
   5   1  -3 902.482 35.8586   4
   4  -1  -3 577.958 24.2805   5
   4  -1  -3 577.727 24.7551   4
  -4  -1   3 554.776 22.8464   3
  -4  -1   3 544.006 23.8800   5
  -4  -1   3 612.654 22.8629   2
   4   1  -3 611.843 25.1478   4
  -4   1   3 588.406 23.2733   2
  -4   1   3 661.677 27.5830   5
   4   1  -3 594.744 24.5544   5
   3  -1  -3 40.4553 4.65018   4
   3  -1  -3 34.4287 4.83095   5
  -3  -1   3 31.8306 4.05318   5
  -3  -1   3 30.8749 3.80123   3
  -3   1   3 34.6565 4.82969   4
   3   1  -3 27.1003 4.35259   5
  -3   1   3 37.6749 4.73030   5
  -3   1   3 33.1834 3.99208   2
  -3   1   3 28.7609 3.70273   3
   3   1  -3 25.1407 4.20166   4
   2  -1  -3 6.92233 1.99219   4
  -2  -1   3 5.68591 1.38580   3
   2  -1  -3 1.82778 1.70425   5
  -2   1   3 3.64785 1.76678   4
   2   1  -3 1.98555 1.26049   4
   2   1  -3 2.55002 1.52323   5
  -2   1   3 5.02094 1.65457   5
  -1  -1  -3 1208.41 37.8492   3
   1  -1   3 1242.56 34.6473   5
   1  -1   3 1242.51 37.5347   3
  -1  -1  -3 1294.94 38.3743   2
  -1  -1  -3 1271.14 38.1405   5
   1  -1   3 1254.61 35.5731   4
   1  -1   3 1185.37 34.9622   5
  -1  -1  -3 1233.09 37.2847   5
  -1   1  -3 1212.69 37.5414   3
  -1   1  -3 1291.30 36.0055   5
   1   1   3 1270.03 38.0656   3
  -1   1  -3 1236.68 36.5726   5
   1   1   3 1275.88 37.7197   5
   1   1   3 1220.91 36.8564   5
  -2  -1  -3 1161.24 39.0713   3
   2  -1   3 1233.57 37.6389   5
   2  -1   3 1223.83 39.1666   3
  -2  -1  -3 1263.70 38.8886   5
   2  -1   3 1224.12 36.2836   5
   2  -1   3 1234.17 37.4334   4
  -2   1  -3 1255.75 39.4302   3
   2   1   3 1187.12 37.6839   5
  -2   1  -3 1151.21 37.4856   5
   2   1   3 1279.67 41.9703   3
   2   1   3 1217.82 39.0971   5
  -3  -1  -3 409.370 19.0588   3
   3  -1   3 437.501 17.9295   4
  -3  -1  -3 441.672 19.1102   5
   3  -1   3 404.892 18.4773   3
   3  -1   3 449.698 17.1610   5
   3  -1   3 417.795 17.9094   5
   3   1   3 397.864 18.5926   5
   3   1   3 455.591 18.1166   5
  -3   1  -3 438.971 18.5217   5
   3   1   3 425.275 18.8057   3
   3   1   3 414.515 18.1589   4
  -3   1  -3 423.035 19.2880   3
   4  -1   3 3061.75 87.4319   5
   4  -1   3 2914.53 90.4423   3
   4  -1   3 2985.72 89.8885   5
   4  -1   3 2983.50 89.6902   4
   4   1   3 3070.23 90.3832   4
   4   1   3 2635.71 89.8319   5
   4   1   3 3056.48 88.8677   5
   4   1   3 3048.66 90.8976   3
   5  -1   3 -1.0939 3.57350   4
   5  -1   3 5.40941 3.64566   5
   5  -1   3 4.78820 3.17400   3
   5   1   3 0.28100 3.49323   4
   5   1   3 4.50533 3.93879   5
   5   1   3 0.31856 3.97588   3
   6  -1   3 155.397 16.0497   4
   6  -1   3 127.506 12.2351   3
   6  -1   3 134.048 12.0438   5
   6   1   3 115.772 12.9250   4
   6   1   3 123.563 12.7024   5
   6  -2  -3 57.8452 9.98982   5
  -6  -2   3 67.3710 9.24321   2
   6   2  -3 38.2207 9.22522   5
  -6   2   3 69.7059 9.47769   2
   5  -2  -3 6.17638 4.48936   4
   5  -2  -3 6.46071 3.59750   5
  -5  -2   3 1.38152 4.31372   3
  -5   2   3 4.80803 3.90164   2
   5   2  -3 6.86813 4.48247   5
   5   2  -3 8.57679 4.49240   4
  -4  -2   3 230.632 13.6495   5
   4  -2  -3 255.076 14.5069   4
  -4  -2   3 244.289 12.7735   3
   4  -2  -3 248.433 14.0980   5
  -4   2   3 244.138 13.4281   2
  -4   2   3 235.904 13.7072   3
   4   2  -3 242.335 14.0677   5
   4   2  -3 254.437 14.3225   4
   3  -2  -3 9.25436 3.36720   4
   3  -2  -3 6.75714 2.90598   5
  -3  -2   3 11.5921 2.59881   3
  -3  -2   3 15.0779 3.43428   5
  -3   2   3 9.45607 3.11928   5
  -3   2   3 8.66939 2.89303   2
  -3   2   3 9.76539 2.51436   3
  -3   2   3 11.4586 2.92487   4
   3   2  -3 10.7164 2.82849   4
   3   2  -3 9.17221 3.02364   5
   2  -2  -3 302.052 13.0070   5
  -2  -2   3 320.498 11.1637   3
  -2  -2   3 334.006 11.9456   5
  -2  -2   3 309.629 12.2215   5
   2  -2  -3 329.038 13.4957   4
   2   2  -3 299.303 12.7743   4
   2   2  -3 304.543 12.6379   5
  -2   2   3 324.848 12.7768   2
  -2   2   3 326.116 13.2136   4
  -2   2   3 317.505 13.0507   5
  -2   2   3 311.831 12.9538   5
  -1  -2   3 17.9587 1.10489   5
  -1  -2   3 19.3172 1.04702   2
   1  -2  -3 25.8994 2.70411   4
   1  -2  -3 21.2591 2.83875   5
   1  -2  -3 24.1341 2.65917   2
   1  -2  -3 31.2159 3.39576   5
   1   2  -3 20.0153 1.95698   5
  -1   2   3 19.7521 2.28342   4
  -1   2   3 23.9486 2.57092   5
  -1   2   3 20.5116 2.70672   2
   1   2  -3 25.2017 2.01960   5
  -1   2   3 24.6504 3.02484   5
   0  -2  -3 458.900 16.1860   5
   0  -2  -3 455.793 15.9406   2
   0  -2   3 462.970 14.2754   3
   0  -2  -3 452.055 15.6289   5
   0  -2  -3 442.818 15.3527   4
   0   2   3 454.568 15.2687   4
   0   2  -3 451.873 14.3029   3
   0   2   3 458.390 16.1393   2
   0   2   3 476.485 15.7950   5
   0   2   3 457.600 16.0034   3
   0   2   3 467.444 15.8046   5
   0   2  -3 449.821 13.1379   4
   1  -2   3 503.656 16.9328   3
  -1  -2  -3 471.978 17.1292   5
  -1  -2  -3 471.530 17.7411   5
   1  -2   3 485.476 15.1417   4
  -1  -2  -3 456.918 17.5936   2
  -1  -2  -3 455.198 17.2723   3
  -1   2  -3 475.220 15.2069   5
   1   2   3 458.289 17.4794   2
   1   2   3 484.659 17.5275   3
  -1   2  -3 469.327 14.5996   5
   1   2   3 479.337 17.6226   5
  -1   2  -3 464.672 15.1061   4
   1   2   3 497.442 17.0177   5
  -1   2  -3 483.970 16.8914   3
  -2  -2  -3 2113.37 67.0433   2
  -2  -2  -3 2204.91 66.8242   3
   2  -2   3 2316.50 62.7459   5
  -2  -2  -3 2158.15 66.3203   5
   2  -2   3 2296.71 63.8755   5
   2  -2   3 2294.04 66.5485   3
  -2   2  -3 2236.88 66.7541   3
   2   2   3 2323.80 67.4871   5
   2   2   3 2235.57 66.8279   3
  -3  -2  -3 316.560 15.7685   3
   3  -2   3 305.882 14.2435   4
   3  -2   3 290.441 14.9074   3
  -3  -2  -3 288.059 15.4593   2
   3  -2   3 307.390 12.7326   5
  -3  -2  -3 291.912 15.2896   5
   3  -2   3 296.167 13.7335   5
   3   2   3 301.703 14.6267   5
  -3   2  -3 296.682 14.3143   5
  -3   2  -3 297.168 15.4930   3
   3   2   3 308.399 15.7302   5
   3   2   3 309.344 15.2440   3
   4  -2   3 1300.89 44.3978   4
   4  -2   3 1308.38 45.4068   3
   4  -2   3 1218.36 43.1213   5
   4  -2   3 1298.72 41.7940   5
   4   2   3 1241.09 44.9466   3
   4   2   3 1340.31 44.4524   5
   4   2   3 1336.39 45.4992   4
   5  -2   3 27.6019 6.09560   3
   5  -2   3 20.2828 4.76448   5
   5  -2   3 26.5848 5.49830   4
   5   2   3 18.0766 5.26984   5
   5   2   3 22.8857 5.45904   3
   5   2   3 29.0467 6.19556   4
   6  -2   3 311.999 23.1202   4
   6  -2   3 338.476 18.4328   5
   6   2   3 325.731 20.6325   4
   6   2   3 318.289 19.5594   5
   6  -3  -3 220.166 16.7564   5
  -6  -3   3 203.564 14.5002   2
   6  -3  -3 176.115 18.3954   4
   6   3  -3 184.407 17.3623   5
   6   3  -3 217.594 19.6380   4
  -6   3   3 234.695 16.5123   2
   5  -3  -3 656.358 30.0371   4
   5  -3  -3 703.798 29.6428   5
  -5  -3   3 676.473 27.6692   3
  -5   3   3 694.401 29.2846   2
   5   3  -3 690.482 30.2555   4
   5   3  -3 699.574 29.9278   5
   4  -3  -3 266.657 15.1933   5
  -4  -3   3 316.482 14.4441   3
  -4  -3   3 288.235 15.2494   5
   4  -3  -3 284.647 16.2057   4
   4   3  -3 307.629 16.3329   4
  -4   3   3 275.033 15.1754   3
  -4   3   3 303.776 15.2571   2
   4   3  -3 277.519 15.4264   5
   3  -3  -3 1515.24 50.5468   4
  -3  -3   3 1638.18 47.7692   3
   3  -3  -3 1543.57 50.0407   5
  -3  -3   3 1591.91 49.2341   5
  -3   3   3 1563.68 50.0485   5
   3   3  -3 1644.52 50.8588   4
  -3   3   3 1594.50 49.8199   2
  -3   3   3 1609.78 50.1576   3
  -3   3   3 1568.48 50.5322   4
   3   3  -3 1688.74 50.5202   5
   2  -3  -3 1749.38 50.7936   2
  -2  -3   3 1675.14 48.4738   5
  -2  -3   3 1763.86 49.3088   5
  -2  -3   3 1677.33 47.7878   3
  -2   3   3 1663.99 51.0993   4
  -2   3   3 1687.66 50.9057   5
   2   3  -3 1694.64 50.3257   5
  -2   3   3 1687.34 50.9110   2
  -2   3   3 1706.50 51.0811   5
   1  -3  -3 2449.61 70.3382   2
   1  -3  -3 2419.95 70.8955   4
  -1   3   3 2467.03 70.9017   2
  -1   3   3 2579.84 70.6139   4
   0  -3  -3 0.78003 1.03058   2
   0  -3   3 1.07383 0.64691   3
   0  -3  -3 0.27570 1.24081   5
   0  -3  -3 1.38911 1.37842   4
   0  -3  -3 -0.3111 1.24288   5
   0   3   3 -0.7457 1.22890   5
   0   3   3 2.38191 1.11268   4
   0   3   3 0.17157 0.85355   5
   0   3  -3 0.38971 0.61685   4
   0   3   3 4.98888 1.67442   2
   0   3  -3 0.36498 0.56634   3
   0   3   3 0.67434 1.04729   3
  -1   3  -3 6468.67 175.327   1
   1   3   3 5482.44 189.678   1
  -2  -3  -3 1528.78 49.5667   3
   2  -3   3 1593.06 44.6102   5
  -2  -3  -3 1647.72 50.7432   2
   2  -3   3 1546.29 48.9274   3
   2  -3   3 1680.82 47.8842   4
   2  -3   3 1584.79 44.2083   5
  -2  -3  -3 1630.03 49.7887   5
  -2   3  -3 1573.45 46.8700   5
   2   3   3 1553.45 49.0942   5
   2   3   3 1574.20 49.6296   3
  -2   3  -3 1603.22 49.5923   3
   2   3   3 1610.21 50.5295   5
  -2   3  -3 1585.80 47.6846   4
   3  -3   3 96.1757 7.89509   3
   3  -3   3 80.8836 7.08578   4
  -3  -3  -3 90.3076 8.28263   3
   3  -3   3 94.3242 5.89294   5
  -3  -3  -3 88.4183 8.18960   2
   3  -3   3 84.3044 6.39386   5
   3   3   3 100.754 8.31958   3
  -3   3  -3 98.0303 7.56320   5
  -3   3  -3 79.9701 8.83508   3
   3   3   3 100.130 9.49886   5
   3   3   3 95.0496 7.68942   5
   4  -3   3 884.405 32.3590   4
   4  -3   3 759.904 29.5285   5
   4  -3   3 832.975 32.8806   3
   4  -3   3 830.744 28.7050   5
   4   3   3 820.814 32.4764   3
   4   3   3 853.046 32.9271   4
   4   3   3 854.534 32.2337   5
   5  -3   3 230.953 16.2020   5
   5  -3   3 236.111 13.9623   5
   5  -3   3 239.971 15.8969   4
   5  -3   3 245.788 16.3337   3
   5   3   3 244.539 15.7051   5
   5   3   3 218.701 15.6808   4
   5   3   3 253.869 16.3928   3
   6  -4  -3 651.782 31.9790   4
   6  -4  -3 605.295 29.4757   5
  -6   4   3 651.283 30.5698   2
   6   4  -3 621.263 30.2917   5
   6   4  -3 607.939 30.3705   4
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   3   7   3 295.242 16.5522   5
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   3   7   3 315.534 16.5766   3
   4  -7   3 52.9153 7.25047   4
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   4   7   3 46.2369 8.50796   3
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   5   8  -3 20.6522 5.49925   5
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   2  15   3 31.8023 7.20473   3
   2  15   3 29.3002 8.47346   5
   2  15   3 57.0004 10.7328   2
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   1  16  -3 4.18523 3.10287   3
   1  16  -3 -1.4759 4.10345   2
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   0  16   3 -3.9584 4.16158   5
   0  16  -3 -3.6123 4.43103   2
   0  16   3 1.81290 5.37717   2
   0  16   3 5.80389 4.96788   3
   0  16  -3 4.84440 3.51477   5
   6   0  -4 166.127 14.4861   5
   6   0  -4 141.764 15.2601   4
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   5   0  -4 -0.3681 3.42594   4
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   5   0  -4 4.60565 4.09733   5
  -4   0   4 343.510 15.4067   2
  -4   0   4 314.344 16.5159   5
   4   0  -4 341.629 16.8569   5
  -4   0   4 321.221 15.4284   3
   4   0  -4 312.320 16.5269   4
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   3   0  -4 4.17058 2.39751   4
   3   0  -4 1.53081 1.54229   5
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  -2   0   4 2373.58 67.6776   2
  -2   0   4 2450.27 68.9965   5
   2   0  -4 2384.68 69.1402   4
   2   0  -4 2491.12 69.7703   5
  -2   0   4 2375.70 69.2474   4
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   1   0  -4 0.19788 1.00614   5
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  -1   0   4 1.26496 0.92491   4
   1   0  -4 1.22704 0.78170   4
   1   0  -4 0.42112 0.86693   5
   0   0   4 6586.73 197.648   1
   0   0  -4 6754.99 197.200   1
  -1   0  -4 0.36646 1.00714   5
  -1   0  -4 0.58660 1.36944   5
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   1   0   4 1.66196 0.99207   5
   1   0   4 -0.7316 0.83128   5
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   1   0   4 0.57297 0.99598   3
   2   0   4 3123.65 88.5431   5
   2   0   4 3040.01 89.6410   3
  -2   0  -4 3136.46 88.6954   5
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   3   0   4 -1.3626 1.72254   5
   3   0   4 3.28429 2.24385   3
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   3   0   4 0.48362 1.51076   4
   3   0   4 -2.3818 2.34225   5
   4   0   4 175.821 12.1930   5
   4   0   4 183.300 11.8655   4
   4   0   4 194.262 11.4711   5
   4   0   4 160.430 12.1631   3
   5   0   4 -3.5249 3.35944   5
   5   0   4 0.29602 3.80991   3
   5   0   4 -1.5598 3.53387   4
   6  -1  -4 268.938 17.6043   5
  -6  -1   4 254.945 15.9228   2
  -6   1   4 270.419 17.1448   2
  -5  -1   4 358.053 17.1850   2
   5  -1  -4 336.372 19.2014   4
   5  -1  -4 319.277 18.5987   5
   5   1  -4 322.875 18.8029   4
   5   1  -4 313.340 18.3612   5
  -5   1   4 310.154 16.9961   2
   4  -1  -4 1413.09 47.6610   4
   4  -1  -4 1461.07 47.4387   5
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  -4  -1   4 1416.32 44.4610   2
  -4  -1   4 1360.88 46.4506   5
  -4   1   4 1386.31 45.3427   2
   4   1  -4 1383.43 47.3220   4
   4   1  -4 1342.41 46.6224   5
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  -3  -1   4 247.971 10.8062   2
  -3  -1   4 247.004 11.1838   3
   3  -1  -4 263.850 12.8800   5
   3  -1  -4 249.042 12.6983   4
  -3  -1   4 240.120 11.7413   5
  -3   1   4 253.867 11.9652   3
   3   1  -4 256.037 12.7987   5
  -3   1   4 251.281 12.6315   5
  -3   1   4 243.870 11.5898   2
  -3   1   4 259.593 12.9084   4
  -3   1   4 254.585 12.4865   5
   3   1  -4 246.737 12.6305   4
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  -2  -1   4 39.2934 2.96143   2
   2  -1  -4 42.2494 4.21543   4
  -2  -1   4 35.5516 3.65128   5
  -2  -1   4 35.6892 3.56376   5
   2  -1  -4 40.9864 3.56804   2
  -2   1   4 40.6176 4.14158   5
  -2   1   4 44.2965 4.06546   4
  -2   1   4 39.0914 3.89651   5
  -2   1   4 41.1296 3.70184   2
   2   1  -4 40.9274 4.04573   4
   2   1  -4 34.7081 3.96049   5
   1  -1  -4 1798.47 50.4576   2
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   1  -1  -4 1771.80 50.5467   4
   1  -1  -4 1850.50 51.2550   5
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   1   1  -4 1707.05 48.5744   2
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   1   1  -4 1770.96 50.0819   5
  -1   1   4 1773.03 50.6531   5
  -1   1   4 1815.55 51.2091   5
  -1   1   4 1759.19 50.9036   2
   0  -1  -4 422.537 14.8830   3
   0  -1  -4 401.506 14.6336   5
   0  -1  -4 426.558 13.4627   4
   0  -1   4 398.086 13.8462   3
   0  -1  -4 397.851 14.3171   5
   0  -1  -4 402.968 14.6638   2
   0   1  -4 410.414 13.6684   2
   0   1  -4 402.591 13.8779   3
   0   1   4 381.235 14.5648   3
   0   1   4 400.965 13.7179   5
   0   1  -4 394.526 12.6692   5
   0   1   4 403.900 13.1060   4
   0   1  -4 395.966 12.5054   5
   0   1   4 407.988 13.9999   5
   0   1   4 412.788 14.7484   2
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   1  -1   4 2287.78 63.4690   5
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  -1   1  -4 2295.69 66.1325   5
   1   1   4 2391.61 67.0071   5
  -1   1  -4 2373.77 67.6346   3
   2  -1   4 1595.31 46.6956   5
  -2  -1  -4 1559.46 50.7308   3
  -2  -1  -4 1649.76 50.0881   5
   2  -1   4 1650.49 48.1090   5
   2  -1   4 1583.90 50.2347   3
  -2  -1  -4 1583.55 51.1083   2
   2  -1   4 1647.12 48.1471   4
   2   1   4 1707.65 50.4977   5
  -2   1  -4 1617.72 48.9090   5
   2   1   4 1534.06 50.3916   3
  -2   1  -4 1640.70 50.8744   3
   2   1   4 1673.18 48.9037   5
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   3  -1   4 1022.83 35.8404   3
   3  -1   4 1027.01 33.9527   4
   3  -1   4 989.523 33.8390   5
   3   1   4 972.993 35.2264   5
  -3   1  -4 1028.64 34.8971   5
   3   1   4 1038.81 34.6483   4
   3   1   4 1027.56 33.7536   5
  -3   1  -4 991.236 36.3475   3
   3   1   4 957.262 35.4188   3
   4  -1   4 743.231 27.5441   5
   4  -1   4 725.091 29.4535   4
   4   1   4 785.881 31.3150   3
   4   1   4 796.253 30.4176   4
   4   1   4 827.354 29.5295   5
   4   1   4 713.200 30.5705   5
   5  -1   4 172.788 12.9940   4
   5  -1   4 165.076 12.2657   5
   5  -1   4 176.198 13.4796   3
   5   1   4 171.720 12.5420   5
   5   1   4 180.799 13.6377   3
   5   1   4 167.548 13.2889   4
   6  -2  -4 567.370 28.8617   5
  -6  -2   4 595.279 26.8038   2
  -6   2   4 614.016 29.3810   5
  -6   2   4 637.742 28.8941   2
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   5  -2  -4 990.083 38.6477   5
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   5  -2  -4 1057.12 40.3169   4
   5   2  -4 1092.40 40.3123   4
   5   2  -4 1025.28 38.9694   5
  -5   2   4 912.782 40.1034   2
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   4  -2  -4 26.0499 5.64750   4
  -4  -2   4 32.2598 4.33255   2
   4  -2  -4 33.1666 6.16110   5
   4   2  -4 35.2691 6.07767   5
  -4   2   4 35.0295 5.56789   2
  -4   2   4 28.7869 5.23323   3
   4   2  -4 26.1172 4.71835   4
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   3  -2  -4 1863.39 57.4651   5
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   3   2  -4 1875.45 57.0562   5
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  -3   2   4 1857.25 57.0049   5
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   3   2  -4 1873.52 57.2560   4
   2  -2  -4 4904.11 161.106   1
   2   2  -4 4818.13 154.507   1
   1  -2  -4 462.968 16.8416   5
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   1  -2  -4 405.843 15.0105   2
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   1  -2  -4 461.603 16.2470   5
   1  -2  -4 438.862 15.4655   4
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   1   2  -4 425.686 13.7944   5
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   1   2  -4 437.533 13.9532   4
   1   2  -4 404.498 13.5946   5
  -1   2   4 427.325 15.6798   5
   0  -2   4 727.602 22.0841   3
   0  -2  -4 695.013 23.3820   5
   0  -2  -4 735.536 23.9769   2
   0  -2  -4 693.454 23.8967   5
   0  -2  -4 714.969 22.8827   4
   0   2   4 717.714 23.3910   5
   0   2  -4 697.701 22.0111   3
   0   2   4 768.291 22.8482   4
   0   2   4 684.876 23.7314   3
   0   2   4 704.130 23.1951   5
   0   2  -4 746.207 21.8408   2
   0   2   4 728.295 24.0545   2
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   2  -2   4 -0.2365 1.00839   5
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   2   2   4 -0.3985 1.44737   5
   2   2   4 -0.3881 1.59075   3
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   3  -2   4 837.668 29.4639   4
   3  -2   4 805.280 31.0302   3
   3  -2   4 841.673 27.0294   5
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   3  -2   4 804.628 28.2823   5
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   3   2   4 845.092 31.7005   5
   3   2   4 899.096 32.1782   3
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   3   2   4 830.305 30.0695   5
   4  -2   4 881.380 31.9674   5
   4  -2   4 864.920 32.8761   4
   4  -2   4 817.079 35.2081   5
   4  -2   4 814.968 37.1710   3
   4   2   4 936.728 33.3822   5
   4   2   4 952.491 35.7039   3
   4   2   4 894.304 33.9336   4
   5  -2   4 27.6458 5.66531   4
   5  -2   4 30.1685 6.73347   3
   5  -2   4 33.5407 6.07621   5
   5   2   4 24.1720 5.86474   5
   5   2   4 19.4244 5.84164   3
   5   2   4 33.5874 7.02088   4
   6  -3  -4 632.556 31.3489   4
  -6  -3   4 625.546 27.0880   2
   6  -3  -4 605.200 29.7893   5
   6   3  -4 597.262 33.8720   4
  -6   3   4 647.499 29.7837   2
   6   3  -4 586.453 29.3732   5
   5  -3  -4 13.2935 5.32462   4
   5  -3  -4 -0.5067 4.20249   5
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   5   3  -4 5.25653 4.20495   4
   5   3  -4 -1.4312 3.39073   5
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   4  -3  -4 338.951 17.1416   4
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   4  -3  -4 280.024 15.9439   5
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  -4   3   4 281.241 15.5438   5
  -4   3   4 278.917 15.1155   2
  -4   3   4 267.130 14.9678   3
   4   3  -4 301.437 15.9058   5
   4   3  -4 288.341 15.7731   4
   3  -3  -4 1.40493 2.36400   4
   3  -3  -4 -2.6894 2.12491   5
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   3   3  -4 -1.8202 1.52473   5
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   3   3  -4 -0.3036 1.33598   4
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  -3   3   4 -0.9655 1.95340   3
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  -3   3   4 1.19496 2.26575   5
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   2  -3  -4 325.031 14.1741   4
  -2  -3   4 312.644 10.0476   2
   2  -3  -4 306.190 13.0467   2
  -2   3   4 321.380 15.2933   2
  -2   3   4 319.910 13.6182   5
  -2   3   4 310.660 13.4256   4
   2   3  -4 305.775 12.6834   5
  -2   3   4 312.829 13.6820   5
   1  -3  -4 35.3659 3.92289   4
   1  -3  -4 45.8079 4.11726   5
   1  -3  -4 34.1029 4.29003   5
  -1   3   4 42.6378 4.11042   5
   1   3  -4 33.3166 2.43371   5
  -1   3   4 33.2217 4.00492   2
   1   3  -4 35.6043 2.42445   5
  -1   3   4 35.3813 3.76610   5
  -1   3   4 35.5925 3.60834   4
   0  -3   4 151.539 6.28105   3
   0  -3  -4 142.094 7.72161   4
   0  -3  -4 148.774 9.18521   2
   0  -3  -4 139.960 8.32591   5
   0   3   4 148.965 7.98183   5
   0   3  -4 144.697 5.32218   4
   0   3   4 139.645 7.45142   4
   0   3  -4 151.660 6.41610   3
   0   3   4 165.689 8.67333   2
   0   3   4 141.883 8.12062   3
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   1  -3   4 1455.31 42.0258   4
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   1  -3   4 1476.53 44.2164   3
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   1   3   4 1485.59 45.9368   5
   1   3   4 1480.35 45.0947   5
  -1   3  -4 1435.95 40.7635   5
   1   3   4 1477.89 46.1283   2
  -1   3  -4 1448.23 41.8895   4
  -1   3  -4 1414.52 41.2369   5
   1   3   4 1492.27 45.8571   3
  -2  -3  -4 3967.23 117.355   2
  -2  -3  -4 3910.68 116.613   3
  -2  -3  -4 4106.70 116.530   5
   2   3   4 4175.24 117.365   5
  -2   3  -4 4166.19 116.449   3
   3  -3   4 531.472 17.5718   5
   3  -3   4 515.806 18.3936   5
  -3  -3  -4 527.342 22.9520   3
  -3  -3  -4 502.186 23.3461   2
  -3  -3  -4 535.587 22.9554   5
   3  -3   4 541.263 20.9283   4
   3  -3   4 531.554 22.5493   3
   3   3   4 502.982 22.9634   5
  -3   3  -4 512.972 22.7564   3
  -3   3  -4 528.013 20.9780   5
   3   3   4 531.542 22.8180   3
   3   3   4 517.309 21.5510   5
   4  -3   4 1178.60 39.7774   5
   4  -3   4 1259.38 42.8525   4
   4  -3   4 1189.91 43.8521   3
   4   3   4 1240.14 47.6487   3
   4   3   4 1252.70 43.1037   5
   4   3   4 1207.77 43.5831   4
   5  -3   4 89.0422 9.66531   3
   5  -3   4 74.8784 9.55364   4
   5  -3   4 87.2769 9.47177   5
   5  -3   4 78.9383 8.26946   5
   5   3   4 65.6142 9.22395   3
   5   3   4 81.5543 9.92042   4
   5   3   4 85.7779 9.71106   5
   6  -4  -4 318.207 21.0491   4
  -6  -4   4 313.986 17.7359   2
   6  -4  -4 279.129 19.8121   5
  -6  -4   4 352.744 19.6450   5
  -6   4   4 330.504 20.8598   5
   6   4  -4 329.613 21.0747   4
   6   4  -4 330.206 21.2336   5
  -6   4   4 327.608 20.5049   2
   5  -4  -4 7.00217 3.84017   4
  -5  -4   4 2.71264 2.94149   2
   5  -4  -4 1.74334 4.01131   5
  -5  -4   4 7.70230 4.01303   2
   5   4  -4 11.4817 4.86448   5
  -5   4   4 4.08126 3.49225   5
   5   4  -4 0.85751 2.73850   4
  -5   4   4 9.99351 4.74597   2
   4  -4  -4 56.9257 7.78858   5
  -4  -4   4 54.4182 5.80964   5
   4  -4  -4 57.4362 7.68009   4
  -4  -4   4 54.0721 6.93028   5
  -4  -4   4 56.3952 5.44361   3
  -4  -4   4 48.4390 5.59398   2
  -4   4   4 50.5252 6.78349   2
  -4   4   4 47.8378 6.81720   5
   4   4  -4 50.3424 6.96019   5
   4   4  -4 58.6550 7.35377   4
   3  -4  -4 26.2364 5.10569   5
  -3  -4   4 22.8471 2.98255   2
  -3  -4   4 32.4628 3.66384   5
  -3  -4   4 22.5943 3.82543   5
  -3  -4   4 24.1702 2.75561   3
   3  -4  -4 29.5884 4.59833   4
  -3   4   4 22.0096 3.80236   5
   3   4  -4 17.7362 3.88124   5
  -3   4   4 26.6875 4.91982   5
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   5  -1  -5 446.329 22.4705   5
   5  -1  -5 466.741 23.1778   4
   5   1  -5 420.073 22.1361   4
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   5   1  -5 416.890 21.9299   5
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   4  -1  -5 2446.79 75.9879   5
   4  -1  -5 2501.03 76.3236   4
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   4   1  -5 2326.38 75.3166   4
   4   1  -5 2520.06 75.9628   5
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   3  -1  -5 197.010 11.1746   4
   3  -1  -5 211.647 11.7021   5
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   3   1  -5 199.150 11.2098   5
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  -3   1   5 202.525 11.0436   5
   3   1  -5 198.987 11.1585   4
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   2   1  -5 7676.00 230.171   1
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   1  -1  -5 2684.57 75.6128   2
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   0  -1  -5 1340.07 39.4896   5
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   0   1  -5 1286.68 37.6542   5
   0   1   5 1307.23 37.3570   4
   0   1   5 1280.28 38.0843   5
   0   1   5 1253.06 38.4013   5
   0   1  -5 1290.70 38.9347   3
   0   1   5 1362.63 40.1890   3
   0   1  -5 1257.89 37.3361   5
   0   1   5 1310.68 39.8011   2
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   1   1   5 2424.87 69.8621   5
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   2  -1   5 2673.54 79.1652   3
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   2  -1   5 2612.68 74.1318   5
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   2   1   5 2655.69 76.6002   5
   2   1   5 2702.38 78.1870   5
   2   1   5 2540.77 79.2079   3
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   3  -1   5 1461.54 45.0185   4
   3  -1   5 1385.78 44.3527   5
   3  -1   5 1393.64 47.4610   3
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   3  -1   5 1394.32 42.7156   5
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   3   1   5 1408.13 44.7310   5
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   3   1   5 1409.65 47.8681   3
   3   1   5 1368.02 46.4650   5
   4  -1   5 217.299 13.2283   4
   4  -1   5 221.391 14.9299   3
   4  -1   5 240.636 14.4384   5
   4  -1   5 243.582 12.2075   5
   4   1   5 222.348 13.0931   5
   4   1   5 229.607 14.8993   3
   4   1   5 229.527 14.0124   4
   4   1   5 233.677 16.2667   5
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   5  -1   5 104.916 10.7025   3
   5  -1   5 90.3854 8.86115   5
   5   1   5 98.5606 10.1442   5
   5   1   5 101.282 10.5711   4
   5   1   5 94.6663 10.3108   3
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   4   2  -5 4.39600 3.12472   5
   4   2  -5 2.43448 3.32864   4
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   3   2  -5 4.13142 2.02010   4
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   2  -2  -5 264.898 11.5881   2
   2   2  -5 284.466 11.7177   4
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   2   2  -5 270.584 11.8820   5
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   1   2  -5 13.8921 2.03166   5
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   1   2  -5 13.5050 1.89877   5
   1   2  -5 15.3185 1.71550   4
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   0  -2  -5 2492.07 69.4704   4
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   0   2   5 2456.68 68.9596   4
   0   2   5 2404.69 69.7998   5
   0   2   5 2348.67 70.9470   3
   0   2   5 2384.56 71.0154   2
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   1   2   5 1.94859 1.44408   5
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   2  -2   5 2214.27 60.5982   5
   2  -2   5 2189.56 67.2702   3
   2  -2   5 2244.44 60.4364   5
   2   2   5 2101.73 67.7075   3
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   2   2   5 2270.36 66.1200   5
   2   2   5 2159.78 67.2591   5
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   3  -2   5 184.347 10.4427   4
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   3  -2   5 185.544 8.70093   5
   3  -2   5 200.428 12.6221   3
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   3   2   5 213.375 13.1175   5
  -3   2  -5 207.955 11.8835   5
  -3   2  -5 188.869 12.4552   3
   3   2   5 233.315 13.6998   3
   3   2   5 188.328 11.2808   5
   4  -2   5 195.407 12.4597   4
   4  -2   5 206.950 14.2361   3
   4  -2   5 210.020 10.8220   5
   4   2   5 219.732 13.7689   4
   4   2   5 188.117 13.9117   3
   4   2   5 215.859 13.2135   5
   5  -2   5 -2.3998 3.84554   3
   5  -2   5 2.63655 3.64251   5
   5  -2   5 1.97045 5.38015   5
   5  -2   5 -2.4204 3.49987   4
   5   2   5 2.44183 3.23882   3
   5   2   5 9.42202 4.33350   5
   5   2   5 8.48662 4.64211   4
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   6   3  -5 88.6746 11.6700   5
   6   3  -5 85.3711 10.3712   4
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   5  -3  -5 411.455 22.7158   4
   5  -3  -5 413.084 22.3957   5
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  -5   3   5 452.816 21.7639   2
   5   3  -5 442.927 22.6882   4
  -5   3   5 422.902 22.0854   5
   5   3  -5 436.433 22.0897   5
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   4  -3  -5 844.716 32.1709   5
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   4  -3  -5 796.822 31.7664   4
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  -4   3   5 837.268 30.6909   2
   4   3  -5 773.047 30.8848   4
   4   3  -5 810.219 31.1168   5
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  -4   3   5 819.673 31.0861   5
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   3  -3  -5 2066.78 64.8460   4
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   3  -3  -5 2184.75 65.4793   5
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   3   3  -5 2186.49 64.0221   5
   3   3  -5 2096.62 63.8804   4
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   2  -3  -5 3288.73 95.6304   4
   2  -3  -5 3367.31 96.3100   5
   2  -3  -5 3402.06 94.6164   2
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  -2   3   5 3306.23 95.4779   5
  -2   3   5 3521.21 95.2655   4
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   1  -3  -5 783.627 26.1691   2
   1  -3  -5 797.936 29.4437   5
   1  -3  -5 810.517 26.5231   4
   1  -3  -5 736.561 25.8916   5
   1   3  -5 785.796 23.2713   5
   1   3  -5 771.068 23.2101   5
  -1   3   5 789.936 26.6911   5
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   0  -3  -5 51.8823 5.50441   5
   0  -3  -5 56.1232 4.86364   5
   0  -3   5 53.5056 3.74241   3
   0  -3  -5 51.8085 5.09437   2
   0  -3  -5 48.3109 4.34952   4
   0   3   5 58.5632 5.16925   5
   0   3   5 50.2511 4.25314   4
   0   3   5 55.7320 5.12134   2
   0   3  -5 57.4571 2.15539   4
   0   3   5 51.3691 4.95918   3
   0   3   5 57.3284 5.07629   5
   0   3  -5 51.8227 3.75189   3
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   1  -3   5 6592.83 200.369   1
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   1   3   5 7178.15 227.215   1
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   2  -3   5 166.524 8.40574   4
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   2  -3   5 192.252 10.7227   3
   2   3   5 189.041 11.5222   3
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   2   3   5 188.078 11.5063   5
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   2   3   5 181.030 10.4880   5
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   3  -3   5 219.757 8.26746   5
   3  -3   5 217.647 11.5074   4
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   3  -3   5 238.047 13.5970   3
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   3  -3   5 229.212 8.02992   5
   3   3   5 224.534 14.0353   5
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   3   3   5 212.897 12.5569   5
   3   3   5 261.140 14.5262   3
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   4  -3   5 145.107 8.91128   5
   4  -3   5 156.357 12.4798   3
   4  -3   5 163.103 11.1149   4
   4  -3   5 165.161 8.45386   5
   4   3   5 168.904 12.1813   5
   4   3   5 159.902 12.2126   4
   4   3   5 171.419 12.7275   3
   5  -3   5 98.8460 9.68704   4
   5  -3   5 100.419 8.03300   5
   5  -3   5 109.917 10.9611   3
   5   3   5 99.8947 10.5385   5
   5   3   5 113.508 11.6844   3
   5   3   5 93.6605 10.5292   4
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   6  -4  -5 -0.4879 3.29055   4
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   6   4  -5 3.67710 4.78694   5
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   5  -4  -5 132.073 11.7390   5
   5  -4  -5 105.244 10.7536   4
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   5   4  -5 111.338 10.6294   4
   5   4  -5 110.546 10.4371   5
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   4  -4  -5 83.9524 10.3707   4
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   4  -4  -5 72.6690 8.87064   5
   4   4  -5 68.7084 7.88939   5
   4   4  -5 63.4937 7.81723   4
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   3  -4  -5 50.5075 6.57355   4
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   3   4  -5 49.4267 5.75689   5
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   3   4  -5 54.9499 5.71092   4
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   2  -4  -5 1109.77 38.2354   4
   2  -4  -5 1185.23 37.3704   2
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   2   4  -5 1120.61 35.6029   5
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   1  -4  -5 1070.91 34.5620   2
   1  -4  -5 1014.42 34.7254   4
   1  -4  -5 1081.33 34.2739   5
   1  -4  -5 1106.55 35.9713   5
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  -1   4   5 1070.67 34.0832   4
   1   4  -5 1039.72 30.1388   5
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   1   4  -5 1065.74 30.2906   5
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   0  -4  -5 1774.20 53.0810   4
   0  -4  -5 1674.31 53.8903   5
   0  -4  -5 1734.95 52.7597   5
   0  -4  -5 1728.47 53.5154   2
   0  -4   5 1722.13 49.5204   3
   0   4   5 1868.06 55.9753   5
   0   4   5 1705.12 53.5574   3
   0   4   5 1808.13 54.5794   2
   0   4   5 1704.92 52.3188   4
   0   4   5 1722.18 52.9957   5
   0   4  -5 1749.70 49.9873   3
   0   4  -5 1679.11 48.2520   4
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   1   4   5 7.70376 2.62086   5
   1   4   5 6.17756 2.30076   3
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   1   4   5 6.91600 2.69746   5
   1   4   5 10.6208 3.21503   2
   1   4   5 13.5362 3.27207   4
   2  -4   5 126.073 7.07861   4
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   2  -4   5 111.140 8.18355   3
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   2   4   5 92.0187 8.36181   3
   2   4   5 119.837 8.80633   5
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   2   4   5 103.111 8.72809   5
   3  -4   5 528.832 20.8059   4
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   3  -4   5 546.797 23.0521   3
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   3   4   5 515.073 22.3231   5
   3   4   5 505.433 23.7103   5
   3   4   5 493.020 22.9502   3
  -3   4  -5 509.371 20.7106   5
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   4  -4   5 235.544 14.0283   4
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   3   3   7 190.657 15.8669   3
   3   3   7 213.795 12.6174   5
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   4   3   7 44.2918 7.17659   3
   4   3   7 47.4878 7.43728   4
   4   3   7 64.0804 7.93252   5
   5  -3   7 423.102 24.0713   3
   5  -3   7 418.050 21.6519   4
   5   3   7 400.559 24.5303   3
   5   3   7 427.640 21.6262   5
   5   3   7 446.892 23.2758   4
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   5  -4  -7 372.080 22.1424   5
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   2   6   7 2351.16 74.5116   4
   2   6   7 2363.66 75.5574   3
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   3  -7   7 1459.45 50.4017   3
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   3   7   7 1417.27 52.7284   3
   3   7   7 1475.13 51.7801   5
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   1   8   7 413.508 21.6841   2
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   2   8   7 584.447 27.8823   3
   2   8   7 616.728 28.8628   2
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   3   8   7 639.805 30.4680   5
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   4   8   7 170.248 14.6776   3
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   2   9   7 54.9558 8.92039   2
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   5   2   8 58.7651 9.42487   3
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   4  -3  -8 3.77212 4.42326   5
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   4  -3  -8 24.3981 6.08873   4
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   4   3  -8 10.4286 3.73855   5
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   4   3  -8 14.1357 4.28870   4
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   3  -3  -8 112.458 8.63739   2
   3  -3  -8 116.518 10.0199   4
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   3   3  -8 107.442 8.98793   5
   3   3  -8 113.363 8.02318   4
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   2  -3  -8 67.7820 6.42540   5
   2  -3  -8 75.2948 6.42536   2
   2  -3  -8 63.6539 6.23341   4
   2  -3  -8 65.4366 7.54885   5
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   2   3  -8 68.7185 4.93504   4
   2   3  -8 65.3317 5.68616   5
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   2   3  -8 58.7264 5.32517   5
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   1   3  -8 3.51721 0.82251   4
   1   3  -8 0.36871 1.57404   5
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   1   3  -8 2.37699 1.44176   5
  -1   3   8 3.17117 1.88150   4
  -1   3   8 4.42569 2.55065   2
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   0  -3   8 1807.08 54.9928   3
   0  -3  -8 1774.48 57.8195   2
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   0  -3  -8 1887.67 59.5553   5
   0   3   8 1805.88 58.2275   2
   0   3   8 1931.89 59.0835   3
   0   3  -8 1869.64 53.3267   5
   0   3   8 1858.22 54.5985   4
   0   3  -8 1827.41 55.3466   3
   0   3   8 1871.50 55.7489   5
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   0   3   8 1800.13 56.2291   5
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   1   3   8 508.133 20.3360   5
   1   3   8 512.734 22.6140   2
   1   3   8 538.067 20.0747   4
   1   3   8 498.796 22.5337   3
   1   3   8 494.524 20.3049   5
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   2  -3   8 952.208 34.9585   3
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   2   3   8 931.850 33.0635   5
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   2   3   8 911.539 36.2158   3
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   2   3   8 954.894 37.0815   5
   3  -3   8 344.072 15.0936   4
   3  -3   8 311.211 17.9524   3
   3   3   8 347.953 19.6193   3
   3   3   8 347.859 16.8698   5
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   4  -3   8 664.362 30.3483   3
   4  -3   8 666.859 26.7294   4
   4   3   8 636.216 29.2438   5
   4   3   8 698.056 31.8968   3
   4   3   8 623.139 27.5784   4
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   5  -4  -8 6.90974 6.10740   4
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   4   4  -8 660.206 26.6267   4
   4   4  -8 641.844 27.2837   5
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   3  -4  -8 624.964 25.1024   2
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   3  -4  -8 679.764 27.7423   4
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   3   4  -8 661.649 25.3997   5
   3   4  -8 644.184 24.2737   4
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   2  -4  -8 378.189 19.3265   5
   2  -4  -8 375.070 17.6610   4
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   2   4  -8 393.853 14.5803   4
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   2   4  -8 375.944 15.3465   5
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   1   4  -8 3.47160 1.05536   4
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   1   4  -8 2.81642 0.85694   4
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   0  -4   8 2945.19 84.8855   3
   0   4   8 3012.75 90.1074   2
   0   4   8 3095.11 86.4517   4
   0   4  -8 2891.10 81.9645   5
   0   4   8 2818.46 89.3926   3
   0   4  -8 2973.30 85.4838   3
   0   4   8 3035.46 88.2304   5
   0   4  -8 2928.08 82.3881   5
   0   4  -8 3006.70 84.6710   2
   0   4   8 3003.12 87.3891   5
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   1   4   8 563.488 21.9339   5
   1   4   8 504.281 21.4178   5
   1   4   8 483.205 20.5185   4
   1   4   8 513.120 23.0828   3
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   1   4   8 493.037 23.0498   2
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   2  -4   8 268.296 11.3143   4
   2  -4   8 302.157 15.6280   3
   2   4   8 311.336 16.4829   5
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   2   4   8 270.899 15.0192   4
   2   4   8 300.092 15.1851   5
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   2   4   8 278.722 16.6482   3
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   3  -4   8 11.9726 4.34575   3
   3  -4   8 10.1804 2.85264   4
   3   4   8 -0.8468 3.37007   3
   3   4   8 4.69119 3.41831   5
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   4  -4   8 48.5689 6.76697   4
   4  -4   8 58.8735 8.14889   3
   4   4   8 53.9956 9.06988   3
   4   4   8 47.3146 7.81441   5
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   5   5  -8 -0.9966 2.70679   4
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   4   5  -8 -0.1263 2.04177   4
   4   5  -8 3.14761 3.71133   5
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   3  -5  -8 34.4461 7.23519   5
   3  -5  -8 36.1081 6.21621   4
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   3   5  -8 51.6992 5.75961   4
   3   5  -8 45.8334 5.96600   5
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   2  -5  -8 10.6912 3.53844   4
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   2   5  -8 8.02119 2.21512   4
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   1   5  -8 1246.50 36.3722   5
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   1   5  -8 1262.43 35.5314   4
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   1   5  -8 1261.84 36.1886   4
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   0   5  -8 26.5472 2.02650   5
   0   5   8 23.5476 5.00849   3
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   0   5   8 19.9611 4.81157   5
   0   5   8 23.0925 5.05922   5
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   1   5   8 787.429 32.2498   2
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   1   5   8 852.277 31.4254   5
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   2  -5   8 27.3573 3.52762   4
   2   5   8 20.7941 4.92977   5
   2   5   8 20.2391 6.31619   3
   2   5   8 24.2091 4.77130   4
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   3  -5   8 579.970 22.5689   4
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   3   5   8 589.445 28.3124   3
   4  -5   8 85.8185 9.45906   3
   4  -5   8 86.4413 8.59039   4
   4   5   8 70.4851 9.33949   5
   4   5   8 71.7046 10.4414   3
   5  -6  -8 814.158 36.8975   4
   5  -6  -8 750.746 36.2330   5
   5   6  -8 795.255 34.2541   5
   5   6  -8 748.970 33.0796   4
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   4  -6  -8 954.045 40.5302   5
   4  -6  -8 1023.71 41.2526   4
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   4   6  -8 1046.59 37.9101   5
   4   6  -8 1009.71 37.6371   4
   3  -6  -8 433.453 23.0274   5
   3  -6  -8 424.117 21.8563   4
   3   6  -8 419.607 18.5134   4
  -3   6   8 419.026 21.7783   2
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   3   6  -8 430.646 18.8234   5
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   2   6  -8 103.283 7.00915   5
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   2   6  -8 104.355 6.91436   4
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   1  -6  -8 973.514 36.1566   4
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   1   6  -8 980.626 29.0694   5
   1   6  -8 976.516 28.9065   5
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   1   6  -8 989.397 30.1124   4
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   0   6   8 10.2810 3.88686   3
   0   6   8 18.6540 4.60682   5
   0   6  -8 14.6389 2.55861   2
   0   6   8 21.1711 4.61070   4
   0   6  -8 12.7969 1.13956   4
   0   6  -8 10.8007 2.09046   2
   0   6   8 20.3148 4.68787   5
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   1   6   8 401.180 19.8626   5
   1   6   8 409.268 21.2449   3
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   1   6   8 423.356 20.0316   4
   1   6   8 408.630 21.4568   2
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   2  -6   8 6.31065 1.96581   4
   2  -6   8 5.20374 3.29018   3
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   2   6   8 11.2657 4.40942   5
   2   6   8 10.7979 4.83663   3
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   2   6   8 6.01050 3.73727   4
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   3  -6   8 10.1151 3.22307   4
   3  -6   8 15.6787 4.43044   3
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   3   6   8 7.89945 4.13200   5
   3   6   8 2.63389 4.27055   3
   4  -6   8 41.7535 7.09231   4
   4  -6   8 27.2111 6.18361   3
   4   6   8 54.0135 9.21328   3
   4   6   8 39.4430 7.96792   5
   5  -7  -8 155.853 14.5990   4
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   5   7  -8 122.084 11.5181   4
   4  -7  -8 106.074 12.3217   4
   4  -7  -8 93.6120 11.8484   5
   4   7  -8 94.0493 9.57363   5
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   4   7  -8 110.707 10.1045   4
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   3  -7  -8 32.2166 6.87240   4
   3  -7  -8 12.1517 4.98237   5
   3   7  -8 20.0342 4.52539   4
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   3   7  -8 22.0965 4.51683   5
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   2  -7  -8 1.55585 3.65796   4
   2  -7  -8 6.66115 4.96603   5
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   2   7  -8 4.97772 2.28130   5
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   1  -7  -8 399.410 21.1581   5
   1  -7  -8 352.077 18.9843   4
   1   7  -8 377.707 12.3317   5
   1   7  -8 366.769 14.4096   4
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   1   7  -8 366.177 12.2496   5
   0  -7  -8 926.288 37.6328   5
   0   7   8 960.995 37.5322   3
   0   7   8 964.415 36.5563   5
   0   7   8 970.038 35.3702   4
   0   7  -8 952.778 29.6091   2
   0   7  -8 997.881 28.3467   4
   0   7   8 942.667 37.7817   2
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   1   7   8 202.021 16.5501   3
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   1   7   8 197.502 14.7549   2
   1   7   8 201.540 13.3270   4
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   1   7   8 201.824 13.6817   5
   2  -7   8 941.376 30.8030   4
   2  -7   8 895.035 33.6937   3
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   2   7   8 927.943 37.8544   3
   2   7   8 940.274 36.3960   5
   2   7   8 901.161 37.9909   2
   3  -7   8 10.6532 4.91438   3
   3  -7   8 6.00671 3.12341   4
   3   7   8 13.1300 5.29695   3
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   3   7   8 13.0840 5.38607   5
   4  -7   8 438.980 21.5258   4
  -4   7  -8 486.889 25.0063   2
   4   7   8 479.612 29.7156   3
   4   7   8 429.389 23.6226   5
   4  -8  -8 549.816 29.3436   4
   4  -8  -8 563.835 29.2747   5
   4   8  -8 565.355 25.4083   4
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   4   8  -8 563.257 25.5816   5
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   3  -8  -8 694.339 32.6361   5
   3  -8  -8 769.743 33.6787   4
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   3   8  -8 688.873 27.7461   4
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   3   8  -8 725.763 27.6696   5
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   4   1 -11 110.029 11.6050   5
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   2   1  11 453.083 24.1925   3
   2   1  11 467.256 15.1508   5
   2   1  11 477.554 17.7041   4
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   3   1  11 261.655 18.5224   3
   3   1  11 256.579 14.3238   4
   3   1  11 255.992 9.62501   5
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   4   3 -11 514.877 23.0162   4
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   3   3  11 8.28576 5.18449   3
   3   3  11 12.1726 4.65126   5
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   4   4 -11 574.985 24.4085   4
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   4   4 -11 599.092 26.8760   5
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   2   4  11 89.6720 9.60660   4
   2   4  11 97.6823 10.5641   3
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   3   4  11 860.725 38.8467   3
   4  -5 -11 191.501 15.2619   4
   4   5 -11 224.921 15.1779   5
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   4   5 -11 194.670 12.5464   4
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   2   5 -11 148.899 9.37822   5
   2   5 -11 165.424 10.0249   5
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   3  -5  11 0.76058 1.95307   4
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   4   6 -11 29.8381 6.29898   5
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   3   6 -11 0.76586 3.09698   5
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   2  -6 -11 220.211 17.3698   5
   2   6 -11 185.082 8.47610   4
   2   6 -11 198.788 8.15799   4
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  -1   7  13 329.811 21.4690   2
  -1   7  13 308.647 19.2763   5
  -1   7  13 332.250 22.1468   3
   0  -7  13 9.01327 2.75908   3
   0   7  13 2.16610 5.11363   2
   0   7  13 6.34255 4.95481   5
   0   7 -13 11.4810 4.06092   5
   0   7 -13 7.56987 3.67516   5
   0   7 -13 14.1455 4.69478   3
   0   7  13 12.7949 5.20288   3
   0   7 -13 9.40488 2.38120   2
  -1  -7 -13 253.947 20.7318   5
   1   7  13 229.289 18.6267   3
   1   7  13 248.344 16.6614   5
  -1   7 -13 232.879 20.4764   5
   2  -8 -13 794.920 40.3265   5
   2  -8 -13 871.564 37.6057   4
   2   8 -13 868.651 33.5266   5
  -2   8  13 817.097 36.4917   5
  -2   8  13 804.360 38.1188   2
   1  -8 -13 46.0646 9.99128   5
  -1   8  13 71.8271 11.3103   2
   1   8 -13 70.9725 6.81040   5
  -1   8  13 38.3593 8.83587   5
   0  -8 -13 -1.3158 3.76475   5
   0   8 -13 -0.6698 2.92915   5
   0   8 -13 0.90432 1.58000   2
   0   8  13 -6.7662 3.24644   2
   0   8  13 -3.5690 4.26142   5
   0   8  13 -4.8055 4.53458   3
   3   0 -14 -0.3906 2.88583   4
  -3   0  14 0.86482 3.73776   3
   3   0 -14 -8.4628 4.03922   5
  -3   0  14 0.27460 3.04501   2
  -2   0  14 72.3487 8.53140   3
   2   0 -14 59.7471 6.96256   2
   2   0 -14 61.1571 9.80461   5
   1   0 -14 -0.5775 2.55102   5
   1   0 -14 8.73743 3.73871   2
   0   0  14 33.0996 7.42244   3
   0   0 -14 26.5859 7.44199   5
  -1   0 -14 -5.3055 4.44985   5
   1   0  14 -2.1919 2.51945   3
  -2   0 -14 74.1852 11.6652   5
   2   0  14 77.5701 12.4487   3
   3  -1 -14 0.55775 3.11926   4
  -3  -1  14 2.55407 3.16140   3
   3   1 -14 -0.8794 2.81436   5
  -3   1  14 -1.5284 3.84153   2
  -3   1  14 6.38832 4.47816   3
   3   1 -14 5.33963 3.16584   4
  -2  -1  14 67.3675 8.06516   3
   2  -1 -14 55.8462 7.74544   2
   2  -1 -14 67.4841 10.6852   5
   2   1 -14 62.7113 9.67519   5
  -2   1  14 80.4838 8.18811   2
   2   1 -14 76.3309 6.37604   2
  -2   1  14 70.7215 9.06767   3
  -1  -1  14 107.072 9.46919   3
   1  -1 -14 106.933 12.6664   5
   1   1 -14 108.961 9.10494   2
  -1   1  14 121.916 11.4667   3
   1   1 -14 106.797 11.7865   5
   0  -1 -14 2079.83 73.1762   5
   0  -1  14 2137.19 69.7420   3
   0   1 -14 2121.41 71.7795   5
   0   1  14 2109.03 71.0657   3
  -1  -1 -14 695.155 33.8188   5
   1  -1  14 700.701 31.2111   3
   1   1  14 703.626 32.4383   3
  -1   1 -14 663.842 32.2907   5
   3  -2 -14 119.164 14.4998   5
   3  -2 -14 137.811 11.0488   4
   3   2 -14 123.697 12.8124   5
  -3   2  14 132.813 11.1514   2
  -3   2  14 150.331 12.8309   3
   2  -2 -14 24.1837 7.26009   5
  -2  -2  14 26.2672 4.99496   3
  -2   2  14 20.6165 5.16434   2
  -2   2  14 31.3376 6.94566   3
   2   2 -14 23.6597 6.31581   5
  -1  -2  14 1.11214 3.45390   3
   1  -2 -14 -2.7059 3.09625   5
   1   2 -14 0.89859 3.86600   5
  -1   2  14 6.95563 4.99505   3
   1   2 -14 1.96149 2.74327   2
   0  -2 -14 283.367 20.3574   5
   0  -2  14 284.331 17.0611   3
   0   2  14 285.589 18.9283   3
   0   2 -14 253.225 15.4646   2
   0   2 -14 282.125 18.4514   5
  -1  -2 -14 23.1387 6.33901   5
   1  -2  14 27.3950 6.79288   3
   1   2  14 22.9202 6.58858   3
  -1   2 -14 31.3391 7.37418   5
   3  -3 -14 7.37934 4.44149   4
   3  -3 -14 4.31508 5.92623   5
   3   3 -14 10.0968 5.15949   5
  -3   3  14 3.06083 4.63321   2
  -3   3  14 3.90903 4.15696   5
  -3   3  14 1.93245 4.79430   3
   2  -3 -14 255.907 20.1195   5
  -2  -3  14 280.157 13.9309   3
   2   3 -14 290.694 17.6369   5
  -2   3  14 279.451 17.7834   3
  -1  -3  14 353.471 17.0181   3
   1  -3 -14 349.473 22.6136   5
   1   3 -14 318.915 18.7882   5
  -1   3  14 303.794 19.2820   3
  -1   3  14 361.294 20.0976   2
   1   3 -14 322.048 13.8108   2
   0  -3  14 198.498 13.8095   3
   0  -3 -14 221.083 18.0812   5
   0   3  14 226.943 10.3817   5
   0   3 -14 184.834 12.5284   2
   0   3 -14 184.480 14.3383   5
   0   3  14 210.359 16.4131   3
  -1  -3 -14 6.46434 5.27069   5
   1  -3  14 1.97530 4.37391   3
  -1   3 -14 6.48920 4.54795   5
   1   3  14 -1.6856 2.49175   5
   1   3  14 2.26224 4.65287   3
   2  -4 -14 0.71501 3.19447   4
   2   4 -14 1.98404 3.87538   5
  -2   4  14 2.80627 3.56340   3
  -2   4  14 2.39934 4.51243   5
  -2   4  14 7.68794 4.75462   2
   1  -4 -14 -4.5043 3.05713   5
  -1  -4  14 0.39459 2.62436   3
   1   4 -14 1.62574 1.84459   2
  -1   4  14 0.52514 6.03093   5
  -1   4  14 -3.1365 4.11137   2
   1   4 -14 10.3123 5.15175   5
  -1   4  14 2.74372 3.64104   5
  -1   4  14 -4.5817 2.94734   4
  -1   4  14 2.22415 3.45606   3
   0  -4  14 86.1888 8.73221   3
   0  -4 -14 98.7946 13.4439   5
   0   4  14 82.1241 10.0666   3
   0   4  14 65.2438 10.5707   5
   0   4 -14 95.8511 11.0804   5
   0   4 -14 82.4789 7.87396   2
  -1  -4 -14 34.7315 10.2417   5
   1  -4  14 33.7484 6.79486   3
  -1   4 -14 25.7573 6.51587   5
   1   4  14 30.1691 6.86535   3
   1   4  14 24.0843 4.87279   5
   2  -5 -14 239.811 15.6529   4
   2  -5 -14 244.834 20.4606   5
  -2   5  14 282.510 18.6932   3
   2   5 -14 223.750 14.9947   5
  -2   5  14 266.546 18.3119   2
  -1   5  14 374.745 22.2497   2
  -1   5  14 346.148 21.4983   3
   0  -5  14 185.894 12.1661   3
   0   5  14 174.060 15.3215   2
   0   5  14 167.015 14.9441   3
  -1  -5 -14 470.040 28.5350   5
   1  -5  14 406.257 21.1077   3
   1   5  14 400.161 24.6325   3
  -1   5 -14 406.125 21.7181   5
   1  -6 -14 1.14179 4.28886   5
  -1   6  14 0.23480 4.00756   5
  -1   6  14 -3.7601 3.23870   3
   1   6 -14 -0.4578 3.97646   5
  -1   6  14 3.61726 3.49975   2
   0  -6  14 19.2579 4.52219   3
   0  -6 -14 12.9238 7.55441   5
   0   6 -14 19.8931 4.79577   5
   0   6  14 21.9957 7.47275   2
   0   6  14 7.92435 4.73971   5
  -2   0  15 -2.6235 3.75502   3
   2   0 -15 9.53111 5.07134   5
  -1   0  15 863.890 35.8820   3
   1   0 -15 902.953 39.5483   5
   0   0  15 5.45724 5.00114   3
   0   0 -15 -0.4237 4.87780   5
  -2  -1  15 -1.8007 3.84287   3
  -2   1  15 4.49351 4.42838   3
   2   1 -15 -4.6562 4.06156   5
  -1  -1  15 7.65409 4.50184   3
   1  -1 -15 -3.8290 4.43708   5
   1   1 -15 -2.0436 4.48372   5
  -1   1  15 -0.2992 3.01900   3
   0  -1 -15 113.499 13.9544   5
   0  -1  15 127.335 12.5941   3
   0   1  15 145.833 13.8002   3
   0   1 -15 129.469 14.0286   5
  -1  -2  15 196.439 13.9406   3
  -1   2  15 260.433 17.6583   3
   1   2 -15 222.534 17.0855   5
   0  -2  15 4.93233 4.44616   3
   0   2  15 4.27089 3.70544   3
   0   2 -15 11.0491 5.58694   5
   1  -3 -15 517.492 30.1400   5
  -1   3  15 535.904 27.7552   3
   1   3 -15 511.172 26.6122   5
   0  -3  15 173.209 13.4514   3
   0  -3 -15 164.542 17.3254   5
   0   3  15 201.152 16.4444   3
   0   3 -15 209.815 16.5449   5
   0   0   0    0.00    0.00   0
;
_shelx_hkl_checksum              80093
_shelx_res_file
;
TITL m22158 : P21/n
    m22158.res
    created by SHELXL-2019/2 at 08:26:30 on 28-Sep-2022
CELL  0.71073   4.9172  12.7016  11.8573   90.000   96.294   90.000
ZERR        4   0.0002   0.0004   0.0003    0.000    0.001    0.000
LATT  1
SYMM 1/2-X, 1/2+Y, 1/2-Z
SFAC C H CL O
UNIT 32 28 4 8
TEMP -183
SIZE 0.25 0.22 0.19
REM COLR colourless
REM FORM cut block
L.S. 10
BOND $H
LIST 4
ACTA
REM Instructions for potential hydrogen bonds:
EQIV $1 -x+1, -y+1, -z+1
HTAB O1 O2_$1
HTAB C2 O2_$1
EQIV $2 -x+3/2, y-1/2, -z+3/2
HTAB C8 O1_$2
REM EQIV $3 x+3/2, -y+1/2, z+1/2
REM HTAB C4 Cl1_$3
HTAB
REM Distance between inversion-related H2, forced into close contact:
RTAB dist H2 H2_$1
REM Planarity of molecule:
MPLA 11 O1 > C8 H1O
RTAB tors C1 C7  C8 Cl1
RTAB tors C2 C3 O1 H1O
RTAB tors C4 C3 O1 H1O
CONF
FMAP 2
PLAN 20
REM EXTI    0.002287 not significant
WGHT    0.032300    0.366000
FVAR       1.48724
O1    4    1.056410    0.598303    0.661674    11.00000    0.02124    0.01165 =
         0.01913    0.00063   -0.00479   -0.00266
H1O   2    0.938208    0.621706    0.616561    11.00000   -1.20000
O2    4    0.387277    0.329079    0.486482    11.00000    0.01848    0.01457 =
         0.01984    0.00254   -0.00425   -0.00068
CL1   3    0.221344    0.109708    0.484486    11.00000    0.01466    0.01477 =
         0.02144   -0.00204   -0.00114   -0.00314
C1    1    0.775739    0.330597    0.623176    11.00000    0.01281    0.01283 =
         0.01372   -0.00096    0.00211   -0.00031
C2    1    0.809292    0.438783    0.608139    11.00000    0.01432    0.01320 =
         0.01410    0.00081   -0.00010    0.00063
REM AFIX  43
H2    2    0.686385    0.475680    0.555336    11.00000   -1.20000
REM AFIX   0
C3    1    1.018985    0.492117    0.671740    11.00000    0.01597    0.01195 =
         0.01411   -0.00115    0.00302   -0.00060
C4    1    1.199722    0.437897    0.749686    11.00000    0.01421    0.01618 =
         0.01461   -0.00323   -0.00041   -0.00040
AFIX  43
H4    2    1.345037    0.474217    0.792591    11.00000   -1.20000
AFIX   0
C5    1    1.166174    0.330231    0.764336    11.00000    0.01588    0.01568 =
         0.01504   -0.00007   -0.00057    0.00331
AFIX  43
H5    2    1.289511    0.293235    0.817524    11.00000   -1.20000
AFIX   0
C6    1    0.954637    0.276072    0.702200    11.00000    0.01607    0.01213 =
         0.01591    0.00001    0.00198    0.00104
AFIX  43
H6    2    0.931888    0.202668    0.713351    11.00000   -1.20000
AFIX   0
C7    1    0.542630    0.279150    0.552863    11.00000    0.01357    0.01287 =
         0.01385   -0.00061    0.00286    0.00005
C8    1    0.510786    0.161484    0.568614    11.00000    0.01252    0.01264 =
         0.01841    0.00049   -0.00200   -0.00110
AFIX  23
H8A   2    0.493730    0.146717    0.649517    11.00000   -1.20000
H8B   2    0.677307    0.125426    0.548476    11.00000   -1.20000
AFIX   0
HKLF 4
REM  m22158 : P21/n
REM wR2 = 0.0671, GooF = S = 1.044, Restrained GooF = 1.044 for all data
REM R1 = 0.0243 for 1569 Fo > 4sig(Fo) and 0.0267 for all 1685 data
REM 106 parameters refined using 0 restraints
END
WGHT      0.0323      0.3660
REM Instructions for potential hydrogen bonds
HTAB O1 O2_$1
HTAB C2 O2_$1
EQIV $3 x+3/2, -y+1/2, z+1/2
HTAB C4 Cl1_$3
HTAB C8 O1_$2
REM Highest difference peak  0.349,  deepest hole -0.181,  1-sigma level  0.045
Q1    1   0.6732  0.3030  0.5875  11.00000  0.05    0.35
Q2    1   0.5177  0.2222  0.5589  11.00000  0.05    0.34
Q3    1   1.1241  0.4592  0.7046  11.00000  0.05    0.32
Q4    1   1.1623  0.3859  0.7537  11.00000  0.05    0.31
Q5    1   0.8665  0.3018  0.6533  11.00000  0.05    0.29
Q6    1   0.7908  0.3836  0.6176  11.00000  0.05    0.29
Q7    1   0.9257  0.4644  0.6412  11.00000  0.05    0.28
Q8    1   1.0468  0.3083  0.7421  11.00000  0.05    0.26
Q9    1   1.4486  0.5031  0.7971  11.00000  0.05    0.26
Q10   1   1.0347  0.5358  0.6630  11.00000  0.05    0.19
Q11   1   0.3443  0.1036  0.4131  11.00000  0.05    0.14
Q12   1   0.4200  0.3031  0.5387  11.00000  0.05    0.14
Q13   1   0.5029  0.2982  0.5000  11.00000  0.05    0.14
Q14   1   0.2799  0.3011  0.4370  11.00000  0.05    0.13
Q15   1   0.3755  0.1358  0.5282  11.00000  0.05    0.13
Q16   1   0.5784  0.1376  0.5995  11.00000  0.05    0.13
Q17   1   0.1797  0.1589  0.4231  11.00000  0.05    0.11
Q18   1   1.1888  0.3168  0.8033  11.00000  0.05    0.10
Q19   1   0.7029  0.4607  0.6025  11.00000  0.05    0.10
Q20   1   1.1312  0.2011  0.8621  11.00000  0.05    0.10
;
_shelx_res_checksum              91247
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O O1 1.05641(18) 0.59830(6) 0.66167(7) 0.01786(19) Uani d 1 . .
H H1O 0.938(3) 0.6217(12) 0.6166(14) 0.021 Uiso d 1 . .
O O2 0.38728(17) 0.32908(6) 0.48648(7) 0.01810(19) Uani d 1 . .
Cl Cl1 0.22134(5) 0.10971(2) 0.48449(2) 0.01719(10) Uani d 1 . .
C C1 0.7757(2) 0.33060(8) 0.62318(9) 0.0131(2) Uani d 1 . .
C C2 0.8093(2) 0.43878(9) 0.60814(9) 0.0140(2) Uani d 1 . .
H H2 0.686(3) 0.4757(12) 0.5553(12) 0.017 Uiso d 1 . .
C C3 1.0190(2) 0.49212(9) 0.67174(9) 0.0139(2) Uani d 1 . .
C C4 1.1997(2) 0.43790(9) 0.74969(9) 0.0151(2) Uani d 1 . .
H H4 1.345037 0.474217 0.792591 0.018 Uiso calc 1 . .
C C5 1.1662(2) 0.33023(9) 0.76434(9) 0.0157(2) Uani d 1 . .
H H5 1.289511 0.293235 0.817524 0.019 Uiso calc 1 . .
C C6 0.9546(2) 0.27607(9) 0.70220(9) 0.0147(2) Uani d 1 . .
H H6 0.931888 0.202668 0.713351 0.018 Uiso calc 1 . .
C C7 0.5426(2) 0.27915(8) 0.55286(9) 0.0133(2) Uani d 1 . .
C C8 0.5108(2) 0.16148(9) 0.56861(10) 0.0148(2) Uani d 1 . .
H H8A 0.493730 0.146717 0.649517 0.018 Uiso calc 1 . .
H H8B 0.677307 0.125426 0.548476 0.018 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O1 0.0212(4) 0.0116(4) 0.0191(4) -0.0027(3) -0.0048(3) 0.0006(3)
O2 0.0185(4) 0.0146(4) 0.0198(4) -0.0007(3) -0.0042(3) 0.0025(3)
Cl1 0.01466(15) 0.01477(15) 0.02144(16) -0.00314(9) -0.00114(11) -0.00204(10)
C1 0.0128(5) 0.0128(5) 0.0137(5) -0.0003(4) 0.0021(4) -0.0010(4)
C2 0.0143(5) 0.0132(5) 0.0141(5) 0.0006(4) -0.0001(4) 0.0008(4)
C3 0.0160(5) 0.0120(5) 0.0141(5) -0.0006(4) 0.0030(4) -0.0012(4)
C4 0.0142(5) 0.0162(5) 0.0146(5) -0.0004(4) -0.0004(4) -0.0032(4)
C5 0.0159(5) 0.0157(5) 0.0150(5) 0.0033(4) -0.0006(4) -0.0001(4)
C6 0.0161(5) 0.0121(5) 0.0159(5) 0.0010(4) 0.0020(4) 0.0000(4)
C7 0.0136(5) 0.0129(5) 0.0138(5) 0.0000(4) 0.0029(4) -0.0006(4)
C8 0.0125(5) 0.0126(5) 0.0184(5) -0.0011(4) -0.0020(4) 0.0005(4)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C3 O1 H1O . . 109.2(11) ?
C6 C1 C2 . . 119.91(10) ?
C6 C1 C7 . . 123.12(10) ?
C2 C1 C7 . . 116.97(10) ?
C3 C2 C1 . . 120.16(10) ?
C3 C2 H2 . . 120.1(9) ?
C1 C2 H2 . . 119.7(9) ?
O1 C3 C2 . . 122.25(10) ?
O1 C3 C4 . . 117.60(10) ?
C2 C3 C4 . . 120.15(10) ?
C5 C4 C3 . . 119.57(10) ?
C5 C4 H4 . . 120.2 ?
C3 C4 H4 . . 120.2 ?
C6 C5 C4 . . 120.86(10) ?
C6 C5 H5 . . 119.6 ?
C4 C5 H5 . . 119.6 ?
C5 C6 C1 . . 119.35(10) ?
C5 C6 H6 . . 120.3 ?
C1 C6 H6 . . 120.3 ?
O2 C7 C1 . . 121.59(10) ?
O2 C7 C8 . . 121.91(10) ?
C1 C7 C8 . . 116.50(9) ?
C7 C8 Cl1 . . 112.57(8) ?
C7 C8 H8A . . 109.1 ?
Cl1 C8 H8A . . 109.1 ?
C7 C8 H8B . . 109.1 ?
Cl1 C8 H8B . . 109.1 ?
H8A C8 H8B . . 107.8 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
O1 C3 . 1.3682(13) ?
O1 H1O . 0.803(17) ?
O2 C7 . 1.2138(14) ?
Cl1 C8 . 1.7725(11) ?
C1 C6 . 1.3967(15) ?
C1 C2 . 1.3978(15) ?
C1 C7 . 1.4921(15) ?
C2 C3 . 1.3857(15) ?
C2 H2 . 0.945(15) ?
C3 C4 . 1.3922(16) ?
C4 C5 . 1.3906(16) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.3892(16) ?
C5 H5 . 0.9500 ?
C6 H6 . 0.9500 ?
C7 C8 . 1.5164(15) ?
C8 H8A . 0.9900 ?
C8 H8B . 0.9900 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O1 H1O O2 3_666 0.803(17) 2.004(18) 2.8029(12) 173.4(16) yes
C2 H2 O2 3_666 0.945(15) 2.547(15) 3.2633(14) 132.7(11) yes
C8 H8A O1 2_646 0.99 2.36 3.3485(14) 175.6 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C6 C1 C2 C3 . . . . -0.24(16) ?
C7 C1 C2 C3 . . . . 179.06(10) ?
C1 C2 C3 O1 . . . . -178.62(10) ?
C1 C2 C3 C4 . . . . 0.97(16) ?
O1 C3 C4 C5 . . . . 178.75(10) ?
C2 C3 C4 C5 . . . . -0.85(16) ?
C3 C4 C5 C6 . . . . 0.00(17) ?
C4 C5 C6 C1 . . . . 0.73(17) ?
C2 C1 C6 C5 . . . . -0.61(16) ?
C7 C1 C6 C5 . . . . -179.86(10) ?
C6 C1 C7 O2 . . . . 178.50(11) ?
C2 C1 C7 O2 . . . . -0.77(15) ?
C6 C1 C7 C8 . . . . -1.61(15) ?
C2 C1 C7 C8 . . . . 179.11(9) ?
O2 C7 C8 Cl1 . . . . -2.07(14) ?
C1 C7 C8 Cl1 . . . . 178.05(7) ?

_cod_database_fobs_code 2244199