#------------------------------------------------------------------------------ #$Date: 2022-11-11 03:03:07 +0000 (Fri, 11 Nov 2022) $ #$Revision: 279229 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/42/2244215.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244215 loop_ _publ_author_name 'Madhan, S.' 'NizamMohideen, M.' 'Pavunkumar, Vinayagam' 'Arasambattu MohanaKrishnan, K.' _publ_section_title ; Crystal structures of two new carbazole derivatives: ethyl 9-(benzenesulfonyl)-2-(4-fluoro-2-nitrophenyl)-6-methoxy-9H-carbazole-3-carboxylate and 12-(benzenesulfonyl)-12H-quinolino[4,3-b]carbazole ; _journal_coeditor_code PK2671 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989022010684 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac 'C25 H16 N2 O2 S' _chemical_formula_moiety 'C25 H16 N2 O2 S' _chemical_formula_sum 'C25 H16 N2 O2 S' _chemical_formula_weight 408.46 _chemical_name_systematic ; 12-(Benzenesulfonyl)-12H-quinolino[4,3-b]carbazole ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 104.846(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.1420(10) _cell_length_b 12.0970(10) _cell_length_c 16.2218(15) _cell_measurement_reflns_used 9986 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 29.51 _cell_measurement_theta_min 2.73 _cell_volume 1923.8(3) _computing_cell_refinement ; APEX3/SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT/XPREP (Bruker, 2016) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) and Mercury (Macrae et al., 2020) ; _computing_publication_material ; WinGX (Farrugia, 2012), publCIF (Westrip, 2010) and PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2008) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker D8 Venture diffractometer with Photon II detector' _diffrn_measurement_method '\w and \f scan' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0511 _diffrn_reflns_av_unetI/netI 0.0236 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 60289 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.994 _diffrn_reflns_theta_min 3.338 _exptl_absorpt_coefficient_mu 0.194 _exptl_absorpt_correction_T_max 0.9572 _exptl_absorpt_correction_T_min 0.8674 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.410 _exptl_crystal_description Solid _exptl_crystal_F_000 848 _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.350 _exptl_crystal_size_min 0.250 _refine_diff_density_max 0.324 _refine_diff_density_min -0.442 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.127 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 271 _refine_ls_number_reflns 4185 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.127 _refine_ls_R_factor_all 0.0680 _refine_ls_R_factor_gt 0.0537 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0465P)^2^+2.5552P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1413 _refine_ls_wR_factor_ref 0.1612 _reflns_number_gt 3488 _reflns_number_total 4185 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file pk2671sup1.cif _cod_data_source_block II _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2244215 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.926 _shelx_estimated_absorpt_t_max 0.953 _shelx_hkl_file ; -2 0 0 1450.55 75.89 2 0 0 1412.66 75.89 2 0 0 1512.25 82.79 3 0 0 0.00 0.60 3 0 0 -0.50 0.40 3 0 0 0.10 0.40 3 0 0 0.10 0.40 3 0 0 1.00 0.40 -3 0 0 1.30 0.40 -3 0 0 0.80 0.40 -3 0 0 -0.20 0.50 -3 0 0 0.90 0.40 -3 0 0 -0.30 0.50 -4 0 0 169.78 9.30 -4 0 0 176.28 9.30 4 0 0 176.28 9.30 4 0 0 177.28 9.30 4 0 0 173.68 9.40 4 0 0 174.68 9.40 -4 0 0 175.58 9.40 -4 0 0 180.28 9.40 -4 0 0 175.28 9.20 4 0 0 175.38 9.30 4 0 0 174.98 9.30 5 0 0 0.30 0.60 5 0 0 3.20 0.80 5 0 0 3.00 0.80 5 0 0 0.00 0.80 5 0 0 1.00 0.70 -5 0 0 -0.40 0.60 -5 0 0 1.30 0.60 -5 0 0 0.90 0.60 -5 0 0 0.20 0.60 -5 0 0 1.60 0.80 -5 0 0 -0.50 0.80 -6 0 0 775.12 40.00 6 0 0 751.82 40.10 -6 0 0 774.12 40.10 -6 0 0 775.32 40.20 6 0 0 763.82 40.10 6 0 0 798.22 40.20 -6 0 0 787.52 40.00 6 0 0 756.22 40.10 6 0 0 739.73 40.20 6 0 0 783.62 40.30 -8 0 0 61.99 3.70 8 0 0 58.99 4.00 -8 0 0 60.29 3.90 -8 0 0 61.89 4.00 -8 0 0 66.69 3.80 8 0 0 63.29 4.00 8 0 0 61.79 4.30 8 0 0 58.59 4.30 8 0 0 64.99 4.00 8 0 0 61.19 3.90 -8 0 0 62.09 4.30 10 0 0 93.99 5.90 10 0 0 93.99 6.20 -10 0 0 94.99 5.40 -10 0 0 101.99 6.30 10 0 0 96.69 5.80 10 0 0 92.19 6.20 10 0 0 97.09 5.90 -10 0 0 95.59 5.50 11 0 0 -1.90 1.50 11 0 0 0.20 1.40 -11 0 0 -0.50 1.10 -11 0 0 -1.90 1.20 -11 0 0 -0.80 1.00 11 0 0 -0.70 1.30 11 0 0 0.30 1.60 11 0 0 -0.60 1.30 12 0 0 7.80 2.00 12 0 0 7.60 2.10 -12 0 0 7.60 2.20 12 0 0 13.80 2.10 -12 0 0 10.00 1.80 -12 0 0 9.20 1.30 12 0 0 8.60 1.70 12 0 0 10.20 1.80 -13 0 0 2.10 1.40 13 0 0 2.60 1.70 13 0 0 -0.80 1.50 -13 0 0 1.30 0.80 13 0 0 -1.30 2.90 13 0 0 -1.80 1.40 13 0 0 -0.10 1.40 1 -1 0 -0.20 0.20 1 -1 0 -0.10 0.20 -1 -1 0 0.00 0.10 1 -1 0 0.00 0.20 -1 1 0 -0.10 0.10 -1 1 0 -0.10 0.20 -2 -1 0 85.89 4.60 -2 -1 0 80.69 4.50 -2 -1 0 85.29 4.50 2 -1 0 83.19 4.60 2 -1 0 83.59 4.60 2 -1 0 89.09 4.60 2 -1 0 85.89 4.60 -2 -1 0 88.59 4.50 2 -1 0 78.49 4.60 2 -1 0 85.79 4.60 -2 -1 0 77.99 4.50 2 1 0 95.99 4.60 2 1 0 86.59 4.60 2 1 0 83.39 4.50 2 1 0 92.09 4.50 -2 1 0 93.79 4.60 -2 1 0 84.69 4.60 -2 1 0 83.99 4.60 2 1 0 91.39 4.50 -2 1 0 79.99 4.60 2 1 0 85.19 4.50 -2 1 0 81.69 4.60 3 -1 0 8.90 1.10 -3 -1 0 8.20 0.80 -3 -1 0 8.20 0.80 3 -1 0 8.30 1.00 -3 -1 0 8.00 0.70 3 -1 0 7.90 0.90 3 -1 0 7.60 0.80 -3 -1 0 7.50 1.00 -3 -1 0 7.80 0.70 3 -1 0 6.20 0.80 -3 -1 0 8.90 0.80 3 -1 0 7.50 0.90 3 1 0 7.70 0.80 -3 1 0 7.60 0.80 3 1 0 7.80 0.80 -3 1 0 7.20 0.90 3 1 0 8.00 1.00 3 1 0 8.70 0.80 -3 1 0 8.00 0.90 3 1 0 8.20 0.80 3 1 0 7.80 0.80 -3 1 0 8.00 0.80 4 -1 0 -0.30 0.70 4 -1 0 0.50 0.60 4 -1 0 0.30 0.50 -4 -1 0 0.90 0.40 4 -1 0 0.10 0.60 -4 -1 0 0.50 0.60 -4 -1 0 0.20 0.60 4 -1 0 0.00 0.50 4 -1 0 1.20 0.60 -4 -1 0 0.70 0.40 -4 -1 0 0.40 0.40 -4 -1 0 0.50 0.40 4 1 0 0.80 0.70 -4 1 0 1.00 0.50 4 1 0 0.40 0.60 -4 1 0 1.20 0.60 4 1 0 0.60 0.50 4 1 0 0.70 0.50 -4 1 0 0.00 0.50 4 1 0 1.10 0.50 -4 1 0 0.80 0.50 -5 -1 0 55.59 3.20 -5 -1 0 52.79 3.10 5 -1 0 51.59 3.20 5 -1 0 53.49 3.30 5 -1 0 50.79 3.20 5 -1 0 56.39 3.40 -5 -1 0 52.99 3.30 -5 -1 0 56.89 3.10 -5 -1 0 58.39 3.40 5 -1 0 52.89 3.60 5 -1 0 58.49 3.30 -5 -1 0 52.09 3.10 -5 1 0 52.09 3.20 5 1 0 60.99 3.50 -5 1 0 50.29 3.20 5 1 0 52.79 3.20 5 1 0 52.59 3.20 -5 1 0 50.59 3.20 -5 1 0 55.59 3.20 -5 1 0 58.09 3.50 5 1 0 49.30 3.30 -6 -1 0 78.19 4.70 6 -1 0 82.79 4.50 -6 -1 0 69.09 4.30 6 -1 0 75.79 4.70 6 -1 0 72.79 4.50 -6 -1 0 76.59 4.40 -6 -1 0 72.79 4.60 -6 -1 0 73.09 4.30 -6 -1 0 71.99 4.40 6 -1 0 86.69 4.80 6 -1 0 82.69 4.50 6 -1 0 74.79 4.50 -6 1 0 70.19 4.50 -6 1 0 73.99 4.70 -6 1 0 75.29 4.50 6 1 0 73.49 4.40 6 1 0 86.79 4.50 -6 1 0 78.09 4.40 6 1 0 78.19 4.80 -6 1 0 79.39 4.60 6 1 0 83.69 4.50 6 1 0 84.09 4.50 -7 -1 0 0.70 0.80 7 -1 0 -0.10 1.00 7 -1 0 2.00 1.20 -7 -1 0 2.00 1.10 7 -1 0 0.90 1.10 7 -1 0 1.10 0.90 -7 -1 0 0.80 0.70 -7 -1 0 0.30 0.70 7 -1 0 1.10 1.00 -7 -1 0 1.40 1.00 7 -1 0 1.60 1.20 7 1 0 1.70 0.90 -7 1 0 0.70 0.90 7 1 0 1.70 1.00 -7 1 0 -0.40 0.90 7 1 0 -0.40 0.80 7 1 0 1.70 0.90 7 1 0 0.90 0.80 -7 1 0 -0.20 0.90 -7 1 0 0.60 0.90 -7 1 0 0.80 1.30 7 1 0 3.20 1.20 8 -1 0 8.10 1.40 8 -1 0 6.50 1.60 -8 -1 0 10.90 1.30 -8 -1 0 9.50 1.00 8 -1 0 10.10 1.40 -8 -1 0 9.10 1.10 8 -1 0 8.80 1.30 8 -1 0 8.80 1.70 8 -1 0 9.30 1.40 -8 1 0 9.10 1.30 8 1 0 9.10 1.30 8 1 0 10.60 1.40 8 1 0 11.00 1.80 -8 1 0 7.80 1.50 -8 1 0 9.50 1.30 -8 1 0 8.90 1.30 8 1 0 9.00 1.40 8 1 0 9.00 1.30 -8 1 0 8.30 1.20 8 1 0 11.10 1.40 9 -1 0 28.50 2.70 9 -1 0 30.80 3.10 9 -1 0 28.40 3.10 -9 -1 0 29.20 2.90 9 -1 0 28.10 2.70 -9 -1 0 33.40 2.20 9 -1 0 27.30 2.70 -9 -1 0 30.50 2.50 9 -1 0 26.60 2.80 -9 1 0 27.80 2.50 -9 1 0 29.40 2.60 -9 1 0 30.10 2.50 9 1 0 33.40 3.00 9 1 0 29.60 2.60 9 1 0 30.60 2.60 9 1 0 30.50 2.50 9 1 0 31.40 2.60 9 1 0 28.90 2.90 -9 1 0 26.30 3.20 -9 1 0 25.60 2.60 10 -1 0 7.20 1.60 10 -1 0 5.00 1.40 10 -1 0 6.90 1.70 -10 -1 0 5.70 1.60 10 -1 0 5.50 1.50 10 -1 0 8.10 1.90 -10 -1 0 9.80 1.40 10 -1 0 8.40 1.70 -10 -1 0 7.10 1.00 10 1 0 6.50 2.20 -10 1 0 6.60 1.40 10 1 0 8.10 1.60 10 1 0 8.60 1.70 -10 1 0 6.90 1.40 -10 1 0 6.70 1.80 -10 1 0 7.80 1.30 10 1 0 8.50 1.80 10 1 0 8.30 1.50 10 1 0 9.40 1.50 11 -1 0 31.30 3.30 -11 -1 0 36.90 3.10 11 -1 0 33.50 3.20 11 -1 0 36.00 3.80 -11 -1 0 34.80 3.10 11 -1 0 36.60 3.30 11 -1 0 36.90 3.40 11 -1 0 35.90 3.70 -11 -1 0 34.30 2.40 -11 -1 0 36.50 2.50 11 1 0 29.50 3.20 11 1 0 40.30 3.20 -11 1 0 35.10 2.80 -11 1 0 38.70 4.00 -11 1 0 31.00 3.10 11 1 0 38.60 3.80 11 1 0 36.70 3.50 11 1 0 32.20 3.20 11 1 0 34.20 3.60 12 -1 0 -0.20 1.60 12 -1 0 1.30 1.50 -12 -1 0 -0.30 1.70 12 -1 0 0.60 1.50 12 -1 0 -0.70 1.80 12 -1 0 2.90 1.80 -12 -1 0 1.30 1.40 12 1 0 -0.30 1.50 12 1 0 -0.70 1.20 12 1 0 0.00 1.70 12 1 0 1.00 1.60 -12 1 0 0.80 1.40 -12 1 0 1.70 1.00 12 1 0 -0.20 1.50 13 -1 0 1.60 1.60 -13 -1 0 2.20 1.30 13 -1 0 0.00 1.70 13 -1 0 1.90 1.80 13 -1 0 -1.50 1.80 13 1 0 4.10 3.00 13 1 0 -0.10 1.30 13 1 0 0.70 1.50 13 1 0 2.10 1.40 13 1 0 -1.50 1.50 -13 1 0 2.10 1.20 -13 1 0 -0.30 1.40 0 2 0 850.91 49.99 -1 -2 0 284.77 16.10 -1 -2 0 332.77 16.00 2 -2 0 299.57 16.00 -2 -2 0 298.57 15.90 -2 -2 0 310.17 15.90 2 -2 0 322.27 16.10 -2 -2 0 302.07 16.00 -2 -2 0 301.57 15.90 2 -2 0 323.67 16.00 2 -2 0 299.07 16.00 -2 -2 0 295.97 15.90 2 2 0 297.97 15.90 2 2 0 305.97 16.00 2 2 0 301.57 15.90 -2 2 0 331.97 16.00 -2 2 0 309.37 16.00 -2 2 0 336.87 16.10 -2 2 0 298.77 16.00 2 2 0 283.57 15.90 2 2 0 314.97 15.90 -2 2 0 302.07 16.00 -3 -2 0 32.60 1.70 3 -2 0 30.10 2.00 3 -2 0 28.90 1.90 3 -2 0 29.10 2.00 3 -2 0 25.30 1.90 -3 -2 0 31.00 2.00 -3 -2 0 34.10 1.70 -3 -2 0 32.80 1.80 3 -2 0 27.50 2.00 -3 -2 0 29.60 1.80 -3 2 0 28.00 1.90 -3 2 0 26.80 1.90 -3 2 0 29.30 1.90 3 2 0 32.20 1.80 3 2 0 30.00 1.80 3 2 0 31.20 2.00 -3 2 0 30.30 1.90 3 2 0 32.60 1.80 3 2 0 30.90 1.80 4 -2 0 58.99 3.50 4 -2 0 55.49 3.50 -4 -2 0 66.19 3.30 -4 -2 0 63.29 3.30 -4 -2 0 60.09 3.40 4 -2 0 58.19 3.50 4 -2 0 58.69 3.50 4 -2 0 59.09 3.70 4 -2 0 60.49 3.60 -4 -2 0 63.89 3.40 -4 -2 0 64.29 3.60 -4 2 0 58.39 3.70 -4 2 0 59.59 3.50 4 2 0 56.89 3.40 4 2 0 65.19 3.40 -4 2 0 58.69 3.50 4 2 0 64.49 3.40 4 2 0 64.49 3.60 4 2 0 60.29 3.40 -4 2 0 56.39 3.50 -4 2 0 60.49 3.50 5 -2 0 817.42 42.70 -5 -2 0 806.72 42.70 5 -2 0 850.61 42.80 -5 -2 0 841.92 42.80 -5 -2 0 850.91 42.60 -5 -2 0 792.82 42.60 5 -2 0 811.22 42.70 -5 -2 0 832.12 42.50 -5 -2 0 850.01 42.50 5 -2 0 776.22 42.80 5 -2 0 810.62 42.70 5 -2 0 875.31 42.90 5 2 0 834.72 42.60 -5 2 0 860.01 42.70 5 2 0 791.92 42.70 5 2 0 828.62 42.70 5 2 0 805.62 43.00 -5 2 0 842.72 42.70 -5 2 0 807.82 42.90 5 2 0 794.92 42.60 -5 2 0 798.52 42.70 5 2 0 826.52 42.80 -5 2 0 798.72 42.70 6 -2 0 151.88 8.00 -6 -2 0 135.89 7.80 -6 -2 0 150.18 7.70 -6 -2 0 143.89 7.50 -6 -2 0 148.09 7.50 -6 -2 0 154.98 8.00 6 -2 0 144.29 7.80 6 -2 0 127.09 8.00 -6 -2 0 131.59 7.60 6 -2 0 142.39 7.80 6 -2 0 149.79 7.80 6 -2 0 136.69 7.80 -6 2 0 130.79 7.70 6 2 0 158.28 7.70 -6 2 0 131.09 7.80 -6 2 0 126.79 7.70 -6 2 0 136.09 8.00 6 2 0 154.68 7.70 -6 2 0 142.39 7.80 7 -2 0 88.69 5.10 7 -2 0 92.79 5.20 -7 -2 0 78.69 5.10 -7 -2 0 84.99 5.20 -7 -2 0 85.29 4.70 7 -2 0 92.69 5.40 -7 -2 0 84.39 5.20 -7 -2 0 89.49 4.70 7 -2 0 87.29 5.40 7 -2 0 85.69 5.20 7 -2 0 96.69 5.20 -7 -2 0 85.39 5.00 -7 2 0 76.59 5.00 7 2 0 88.29 5.00 7 2 0 91.99 5.00 -7 2 0 83.89 5.40 7 2 0 89.69 5.10 -7 2 0 75.99 5.00 7 2 0 91.59 5.00 7 2 0 97.49 5.40 7 2 0 87.89 5.00 -7 2 0 73.29 5.00 8 -2 0 4.70 1.20 -8 -2 0 6.80 1.30 8 -2 0 5.90 1.40 -8 -2 0 4.70 0.80 -8 -2 0 5.00 1.10 8 -2 0 5.40 1.50 8 -2 0 4.60 1.30 8 -2 0 4.30 1.30 8 -2 0 3.50 1.10 8 2 0 7.70 1.20 -8 2 0 2.90 1.20 8 2 0 7.10 1.30 -8 2 0 3.90 1.10 -8 2 0 1.60 1.00 -8 2 0 5.50 1.40 8 2 0 6.00 1.10 8 2 0 4.50 1.00 9 -2 0 5.10 1.40 9 -2 0 4.30 1.30 -9 -2 0 4.40 1.10 -9 -2 0 4.40 1.40 9 -2 0 3.30 1.30 -9 -2 0 5.00 0.70 9 -2 0 5.40 1.60 9 -2 0 4.50 1.50 9 -2 0 6.30 1.50 9 2 0 6.10 1.20 9 2 0 6.30 1.10 -9 2 0 5.10 1.60 9 2 0 5.00 1.50 -9 2 0 5.10 1.40 -9 2 0 2.40 1.20 -9 2 0 5.00 1.30 9 2 0 6.40 1.20 9 2 0 6.20 1.30 9 2 0 6.10 1.30 -10 -2 0 3.30 1.20 10 -2 0 1.40 1.50 10 -2 0 2.60 1.70 10 -2 0 2.00 1.50 -10 -2 0 3.30 0.60 -10 -2 0 4.50 1.50 10 -2 0 2.30 1.30 10 -2 0 3.10 1.50 10 -2 0 4.80 1.60 -10 2 0 0.10 1.20 -10 2 0 1.30 1.20 10 2 0 3.90 1.70 10 2 0 2.80 1.20 10 2 0 4.80 1.50 10 2 0 4.50 1.30 10 2 0 4.10 1.20 -10 2 0 1.80 1.20 10 2 0 4.30 1.50 -10 2 0 1.20 1.30 -11 -2 0 3.80 1.20 -11 -2 0 0.50 1.40 -11 -2 0 1.60 1.20 11 -2 0 0.60 1.40 11 -2 0 3.30 1.60 11 -2 0 1.90 1.30 11 -2 0 2.30 1.40 11 -2 0 6.50 1.80 11 2 0 1.60 1.20 11 2 0 3.10 1.30 -11 2 0 4.20 1.80 -11 2 0 3.90 1.30 -11 2 0 1.60 1.20 -11 2 0 0.50 1.20 11 2 0 4.00 1.50 11 2 0 2.10 1.30 11 2 0 4.60 1.70 12 -2 0 7.20 2.00 12 -2 0 2.30 1.60 12 -2 0 5.80 1.70 -12 -2 0 3.10 1.30 12 -2 0 5.60 1.90 12 -2 0 1.60 1.90 -12 2 0 3.70 1.30 12 2 0 6.50 3.20 -12 2 0 6.30 1.40 -12 2 0 4.80 1.50 12 2 0 1.40 1.50 12 2 0 2.60 1.30 12 2 0 3.00 1.90 12 2 0 3.10 1.40 13 -2 0 0.10 1.80 13 -2 0 -0.10 1.90 -13 -2 0 -0.50 1.20 13 -2 0 -2.90 3.10 13 -2 0 -2.50 1.50 -13 2 0 0.60 1.00 -13 2 0 -3.60 1.30 13 2 0 0.80 1.20 -13 2 0 -2.70 1.30 13 2 0 3.00 2.70 13 2 0 -0.70 1.50 13 2 0 1.00 2.20 13 2 0 1.20 1.50 0 -3 0 0.00 0.30 0 -3 0 0.50 0.40 0 -3 0 0.30 0.30 0 -3 0 -0.20 0.30 0 -3 0 -0.30 0.30 0 3 0 -0.30 0.40 0 3 0 0.20 0.40 0 3 0 0.60 0.40 0 3 0 0.00 0.40 -1 -3 0 8.10 0.70 -1 -3 0 7.30 0.70 -1 -3 0 8.00 0.70 1 -3 0 9.50 0.80 1 -3 0 9.00 0.90 -1 -3 0 6.40 0.70 1 -3 0 8.70 0.90 1 -3 0 7.70 0.90 1 -3 0 8.80 1.00 1 3 0 6.60 0.70 -1 3 0 8.80 0.90 -1 3 0 8.00 0.80 -1 3 0 9.60 0.90 1 3 0 6.80 0.70 -1 3 0 6.90 1.00 -1 3 0 9.00 0.90 1 3 0 6.30 0.70 1 3 0 6.70 0.70 1 3 0 6.30 0.70 -2 -3 0 51.69 3.10 -2 -3 0 51.89 3.00 2 -3 0 58.69 3.30 2 -3 0 59.89 3.10 -2 -3 0 50.39 2.90 2 -3 0 57.99 3.20 2 -3 0 54.69 3.10 -2 -3 0 50.99 2.90 -2 -3 0 61.69 3.00 -2 3 0 61.19 3.10 2 3 0 54.39 3.00 2 3 0 53.19 3.00 -2 3 0 53.69 3.10 -2 3 0 60.19 3.10 -2 3 0 50.69 3.20 2 3 0 53.49 3.00 2 3 0 53.49 3.00 -2 3 0 60.19 3.10 2 3 0 50.79 3.10 -3 -3 0 697.23 36.30 3 -3 0 731.83 36.60 3 -3 0 686.43 36.50 -3 -3 0 716.53 36.50 3 -3 0 699.43 36.50 -3 -3 0 705.33 36.40 3 -3 0 692.23 36.50 -3 -3 0 680.53 36.30 -3 -3 0 702.43 36.30 3 -3 0 675.63 36.50 -3 -3 0 718.53 36.40 3 3 0 700.23 36.40 3 3 0 706.63 36.50 3 3 0 716.03 36.40 -3 3 0 685.03 36.50 -3 3 0 722.33 36.50 3 3 0 682.83 36.40 -3 3 0 749.92 36.50 3 3 0 656.73 36.30 -3 3 0 709.43 36.60 3 3 0 709.43 36.40 4 -3 0 383.56 19.60 -4 -3 0 369.56 19.40 4 -3 0 386.96 19.60 4 -3 0 370.56 19.60 -4 -3 0 376.46 19.60 -4 -3 0 382.66 19.30 -4 -3 0 388.86 19.40 4 -3 0 366.86 19.60 -4 -3 0 381.46 19.40 -4 -3 0 379.36 19.30 4 -3 0 371.66 19.60 4 -3 0 361.96 19.90 -4 3 0 372.06 19.60 4 3 0 367.76 19.40 4 3 0 372.16 19.40 4 3 0 356.26 19.40 -4 3 0 361.36 19.60 -4 3 0 366.16 19.70 4 3 0 381.46 19.40 4 3 0 375.66 19.60 4 3 0 371.96 19.40 -4 3 0 360.76 19.60 5 -3 0 43.00 2.70 -5 -3 0 41.40 2.40 -5 -3 0 39.80 2.40 5 -3 0 40.60 2.70 -5 -3 0 40.50 2.80 -5 -3 0 43.10 2.40 5 -3 0 36.80 2.70 -5 -3 0 41.90 2.50 5 -3 0 38.70 2.70 5 -3 0 40.40 2.70 5 -3 0 34.50 2.90 5 3 0 39.00 2.50 -5 3 0 38.40 2.90 -5 3 0 43.40 2.70 -5 3 0 39.90 2.60 -5 3 0 37.50 2.60 -5 3 0 37.30 2.60 5 3 0 39.10 2.70 6 -3 0 8.90 1.30 6 -3 0 11.20 1.40 -6 -3 0 9.60 1.10 -6 -3 0 8.50 1.30 -6 -3 0 8.90 1.00 6 -3 0 9.60 1.50 -6 -3 0 9.30 0.90 6 -3 0 10.60 1.20 -6 -3 0 8.70 1.00 6 -3 0 10.00 1.40 6 -3 0 9.10 1.20 -6 3 0 8.20 1.10 -6 3 0 8.90 1.20 6 3 0 9.00 1.10 6 3 0 9.10 1.00 6 3 0 9.50 1.00 6 3 0 8.10 1.00 6 3 0 10.20 1.30 6 3 0 10.30 1.10 -6 3 0 11.00 1.70 7 -3 0 93.69 5.50 7 -3 0 94.89 5.50 -7 -3 0 92.19 5.40 7 -3 0 90.59 5.60 -7 -3 0 93.19 5.60 7 -3 0 92.39 5.80 -7 -3 0 95.99 5.40 7 -3 0 89.79 5.40 7 -3 0 96.79 5.50 -7 -3 0 92.09 5.20 -7 -3 0 95.39 4.90 -7 3 0 89.59 5.40 7 3 0 96.59 5.30 7 3 0 96.89 5.30 -7 3 0 82.29 5.40 -7 3 0 89.99 5.40 -7 3 0 88.99 5.40 7 3 0 89.79 5.60 7 3 0 90.29 5.20 -7 3 0 93.89 5.80 7 3 0 94.29 5.30 7 3 0 99.09 5.70 8 -3 0 4.30 1.20 8 -3 0 2.90 1.30 -8 3 0 1.40 1.10 -8 3 0 3.90 1.40 -8 3 0 2.00 1.10 -8 3 0 3.50 1.10 9 -3 0 16.60 2.00 9 -3 0 24.00 2.70 9 -3 0 16.90 2.00 -9 -3 0 20.00 2.00 9 -3 0 22.80 3.00 9 -3 0 17.90 2.10 9 -3 0 18.20 2.10 9 3 0 17.80 2.20 -9 3 0 22.50 3.00 -9 3 0 15.20 2.00 9 3 0 20.40 2.10 9 3 0 19.50 2.30 -9 3 0 17.20 1.90 9 3 0 24.90 2.10 -9 3 0 16.60 1.90 9 3 0 21.40 2.70 9 3 0 21.70 2.20 10 -3 0 3.50 2.10 -10 -3 0 0.60 0.90 10 -3 0 -2.90 1.20 10 -3 0 -1.70 1.30 -10 -3 0 -0.50 1.10 10 -3 0 -1.00 1.20 10 -3 0 -0.90 1.50 -10 3 0 -1.40 0.90 10 3 0 0.10 1.10 -10 3 0 -1.70 1.10 -10 3 0 -0.70 1.10 10 3 0 -0.60 1.00 -10 3 0 -1.30 1.30 10 3 0 -1.10 1.10 10 3 0 -0.30 1.00 10 3 0 -0.50 1.50 -10 3 0 0.30 2.20 11 -3 0 18.90 2.40 11 -3 0 18.80 2.30 11 -3 0 21.70 2.60 11 -3 0 17.80 2.60 -11 -3 0 24.50 2.40 -11 -3 0 26.10 2.40 11 -3 0 29.20 3.50 -11 -3 0 27.20 3.00 11 3 0 26.20 2.50 11 3 0 16.30 2.50 11 3 0 22.20 2.80 11 3 0 18.70 2.90 -11 3 0 22.30 2.50 11 3 0 22.20 2.70 -11 3 0 17.90 2.30 11 3 0 24.80 2.60 -11 3 0 22.80 2.70 12 -3 0 11.00 2.20 12 -3 0 17.20 2.50 12 -3 0 12.50 2.20 12 -3 0 11.80 2.00 12 -3 0 13.70 2.40 12 3 0 12.00 1.60 12 3 0 13.90 2.50 -12 3 0 13.30 1.90 12 3 0 11.40 1.70 12 3 0 13.60 1.90 -12 3 0 13.10 1.70 -12 3 0 8.90 1.80 -13 -3 0 6.60 1.90 13 -3 0 4.30 1.80 -13 -3 0 7.90 1.40 13 -3 0 4.70 3.10 13 -3 0 5.60 2.00 13 -3 0 6.30 2.40 13 3 0 5.90 2.20 -13 3 0 4.40 1.60 -13 3 0 6.90 1.50 13 3 0 5.80 1.60 13 3 0 11.10 2.00 -13 3 0 4.60 1.70 13 3 0 6.90 1.50 13 3 0 7.90 1.80 0 -4 0 3.00 0.50 0 -4 0 2.40 0.50 0 -4 0 1.60 0.50 0 -4 0 2.30 0.50 0 -4 0 2.10 0.60 0 -4 0 1.90 0.40 0 4 0 3.50 0.50 0 4 0 3.30 0.50 0 4 0 1.80 0.50 0 4 0 2.90 0.50 -1 -4 0 11.80 1.00 -1 -4 0 15.40 1.00 1 -4 0 17.10 1.10 1 -4 0 16.40 1.20 -1 -4 0 13.40 1.10 -1 -4 0 13.90 1.00 -1 -4 0 11.70 1.00 1 -4 0 17.00 1.20 1 4 0 13.50 1.00 -1 4 0 16.00 1.10 -1 4 0 15.70 1.20 -1 4 0 16.20 1.20 1 4 0 12.00 1.00 1 4 0 11.40 1.00 1 4 0 12.10 1.00 -1 4 0 15.80 1.20 1 4 0 12.50 1.10 -2 -4 0 176.38 10.60 2 -4 0 215.38 10.80 2 -4 0 213.08 10.70 2 -4 0 212.88 10.80 2 -4 0 222.28 10.80 2 -4 0 218.98 10.80 -2 -4 0 180.98 10.70 2 4 0 182.78 10.60 2 4 0 179.48 10.70 -2 4 0 213.78 10.80 2 4 0 177.98 10.60 -2 4 0 219.28 10.80 -2 4 0 221.88 10.80 -2 4 0 219.18 10.80 2 4 0 184.48 10.60 -2 4 0 215.98 10.80 -3 -4 0 3.70 0.40 -3 -4 0 4.20 0.70 3 -4 0 4.90 0.80 3 -4 0 4.50 0.80 -3 -4 0 4.60 0.50 -3 -4 0 3.10 0.40 3 -4 0 3.90 0.80 -3 -4 0 5.00 0.60 3 -4 0 1.60 0.80 3 4 0 4.80 0.60 3 4 0 5.10 0.80 -3 4 0 3.50 0.80 -3 4 0 3.60 0.70 -3 4 0 4.40 0.80 3 4 0 4.50 0.60 3 4 0 4.40 0.60 -3 4 0 4.50 0.70 3 4 0 3.50 0.40 3 4 0 3.80 0.50 -3 4 0 2.50 0.90 4 -4 0 156.98 8.10 -4 -4 0 148.29 8.10 4 -4 0 144.39 8.10 4 -4 0 151.18 8.10 4 -4 0 157.08 8.10 -4 -4 0 148.79 7.90 4 -4 0 144.99 8.10 4 -4 0 134.49 8.20 -4 -4 0 150.88 7.90 -4 -4 0 153.08 7.90 -4 4 0 138.99 8.20 -4 4 0 150.78 8.00 -4 4 0 144.69 8.00 4 4 0 149.39 7.90 -4 4 0 141.89 8.00 4 4 0 147.09 7.90 -4 4 0 159.78 8.10 4 4 0 138.39 7.80 4 4 0 149.59 7.90 4 4 0 151.88 8.10 4 4 0 155.38 7.90 -5 -4 0 180.48 9.90 -5 -4 0 182.18 9.70 5 -4 0 175.38 9.90 5 -4 0 182.18 9.90 5 -4 0 170.88 9.90 5 -4 0 169.58 10.10 5 -4 0 187.98 9.90 5 -4 0 182.18 9.90 -5 -4 0 188.78 9.70 -5 -4 0 180.78 9.70 5 4 0 185.28 9.70 -5 4 0 171.48 9.90 5 4 0 208.18 10.00 5 4 0 180.48 9.70 5 4 0 190.28 9.70 -5 4 0 175.98 9.80 5 4 0 200.38 9.70 -5 4 0 179.78 9.90 -5 4 0 183.38 10.10 -5 4 0 180.68 9.90 6 -4 0 9.40 1.30 6 -4 0 10.30 1.60 6 -4 0 9.90 1.30 6 -4 0 8.10 1.30 6 -4 0 10.60 1.40 -6 4 0 7.20 1.20 -6 4 0 8.60 1.30 -6 4 0 8.30 1.50 -6 4 0 7.40 1.20 -6 4 0 9.40 1.30 7 -4 0 39.70 3.20 -7 -4 0 43.10 2.80 7 -4 0 44.90 3.40 7 -4 0 41.90 3.60 -7 -4 0 46.10 2.90 -7 -4 0 50.19 3.40 -7 -4 0 41.50 2.80 7 -4 0 40.50 3.20 7 -4 0 42.00 3.30 7 -4 0 44.30 3.20 7 4 0 46.80 2.90 7 4 0 44.70 2.90 -7 4 0 38.20 3.60 7 4 0 46.50 2.90 -7 4 0 38.30 3.10 -7 4 0 42.10 3.10 7 4 0 48.40 2.90 7 4 0 44.80 2.90 -7 4 0 38.20 3.10 -7 4 0 37.10 3.00 7 4 0 51.69 3.50 -8 -4 0 21.20 2.10 8 -4 0 23.10 2.60 8 -4 0 24.50 2.70 -8 -4 0 22.50 2.60 -8 -4 0 23.40 2.00 -8 -4 0 25.20 2.00 -8 4 0 22.90 3.10 8 4 0 20.30 2.60 8 4 0 23.80 2.00 8 4 0 20.00 2.10 8 4 0 27.40 2.20 -9 -4 0 0.60 0.90 9 -4 0 0.00 1.30 9 -4 0 -0.80 1.30 -9 -4 0 -0.70 0.80 9 -4 0 -2.00 1.20 9 -4 0 -0.80 1.40 9 -4 0 -1.90 1.30 9 -4 0 -0.20 1.30 -9 4 0 -2.30 1.10 9 4 0 -0.20 1.00 9 4 0 -0.40 0.90 9 4 0 -1.30 0.90 9 4 0 -0.60 1.00 9 4 0 -0.40 1.30 -9 4 0 -0.30 1.20 9 4 0 -0.10 0.90 -9 4 0 -2.10 1.00 10 -4 0 8.70 1.70 10 -4 0 10.00 1.70 -10 -4 0 7.80 1.20 -10 -4 0 8.00 1.40 10 -4 0 14.20 2.00 10 -4 0 10.10 1.80 10 -4 0 10.40 1.80 10 -4 0 11.60 2.00 10 4 0 7.10 1.30 10 4 0 9.50 1.90 -10 4 0 10.00 1.70 -10 4 0 10.40 2.10 -10 4 0 8.90 1.50 10 4 0 8.20 1.90 -10 4 0 8.70 1.60 -10 4 0 7.60 1.50 10 4 0 6.70 1.40 10 4 0 7.00 1.40 10 4 0 8.60 1.40 -11 -4 0 66.79 4.10 11 -4 0 62.89 4.70 11 -4 0 63.49 5.20 11 -4 0 62.39 4.60 11 -4 0 63.39 4.80 -11 -4 0 61.79 4.50 11 -4 0 62.29 4.80 -11 -4 0 64.99 4.10 11 4 0 49.30 5.10 11 4 0 63.29 4.40 11 4 0 68.19 4.90 11 4 0 60.49 4.30 11 4 0 60.89 4.20 -11 4 0 61.49 4.60 11 4 0 68.49 4.30 -11 4 0 60.89 4.40 -11 4 0 62.59 4.40 12 -4 0 6.40 2.20 12 -4 0 4.20 1.80 12 -4 0 11.10 2.20 12 -4 0 3.80 1.80 -12 -4 0 5.20 1.50 -12 -4 0 7.10 1.30 12 4 0 10.30 1.60 -12 4 0 5.50 1.60 -12 4 0 5.20 2.00 12 4 0 8.40 1.70 12 4 0 5.40 1.40 12 4 0 6.10 2.10 12 4 0 6.00 1.60 13 -4 0 -0.80 1.50 -13 -4 0 1.40 1.10 13 -4 0 0.60 2.00 13 -4 0 -2.00 1.60 -13 4 0 1.00 1.50 -13 4 0 -0.10 1.30 13 4 0 -1.30 1.30 13 4 0 -0.90 1.40 13 4 0 1.40 1.20 13 4 0 1.90 2.00 0 -5 0 0.70 0.50 0 -5 0 -0.30 0.40 0 -5 0 0.60 0.50 0 -5 0 0.00 0.30 0 -5 0 0.80 0.40 0 -5 0 0.40 0.50 0 5 0 0.00 0.50 0 5 0 -0.10 0.40 0 5 0 0.60 0.50 0 5 0 0.20 0.50 -1 -5 0 403.36 19.60 -1 -5 0 330.57 19.60 -1 -5 0 379.76 19.70 1 -5 0 396.66 19.70 1 -5 0 385.46 19.70 1 -5 0 404.66 19.80 1 -5 0 395.26 19.70 1 -5 0 389.26 19.70 -1 5 0 394.36 19.70 -1 5 0 384.06 19.70 -1 5 0 381.36 19.80 1 5 0 332.37 19.70 -1 5 0 401.76 19.80 1 5 0 333.67 19.60 -1 5 0 398.46 19.80 1 5 0 330.37 19.70 2 -5 0 2.10 0.60 2 -5 0 1.10 0.60 -2 -5 0 1.50 0.40 2 -5 0 2.30 0.80 2 -5 0 2.90 0.70 -2 -5 0 1.50 0.40 2 -5 0 2.60 0.70 -2 -5 0 1.80 0.50 -2 -5 0 0.70 0.40 -2 -5 0 1.30 0.50 2 5 0 1.40 0.50 -2 5 0 1.40 0.70 2 5 0 1.70 0.20 -2 5 0 0.60 0.60 2 5 0 1.30 0.50 -2 5 0 1.10 0.70 2 5 0 1.30 0.50 -2 5 0 0.80 0.70 2 5 0 1.90 0.50 2 5 0 1.00 0.50 -2 5 0 1.60 0.60 -3 -5 0 22.70 1.40 3 -5 0 28.80 1.80 -3 -5 0 22.90 1.80 3 -5 0 27.40 2.00 -3 -5 0 24.50 1.40 -3 -5 0 24.00 1.60 3 -5 0 30.10 2.00 -3 -5 0 26.00 1.60 3 -5 0 29.10 1.90 3 5 0 25.90 1.70 -3 5 0 23.70 2.20 -3 5 0 31.30 2.00 3 5 0 23.60 1.80 3 5 0 24.20 1.70 3 5 0 25.50 1.70 3 5 0 26.90 1.70 -3 5 0 28.60 1.90 -3 5 0 27.30 1.90 4 -5 0 22.40 1.90 4 -5 0 19.70 1.80 4 -5 0 21.80 1.80 4 -5 0 22.90 1.90 -4 -5 0 22.20 1.50 -4 -5 0 23.00 1.50 -4 -5 0 20.50 1.80 4 5 0 24.20 1.60 4 5 0 21.40 1.30 4 5 0 21.30 1.80 -4 5 0 19.30 1.80 -4 5 0 24.40 1.90 -4 5 0 24.00 1.90 -4 5 0 18.20 2.20 -4 5 0 22.10 1.80 5 -5 0 13.40 1.50 5 -5 0 13.90 1.50 5 -5 0 12.70 1.50 5 -5 0 14.00 1.70 5 -5 0 14.30 1.80 -5 5 0 16.10 1.70 -5 5 0 14.60 1.50 -5 5 0 11.10 1.90 -5 5 0 14.30 1.70 -5 5 0 12.30 1.40 6 -5 0 49.70 3.40 6 -5 0 49.80 3.40 6 -5 0 45.70 3.40 6 -5 0 44.40 3.80 6 -5 0 47.90 3.30 6 -5 0 51.59 3.50 -6 -5 0 50.39 3.00 -6 -5 0 52.39 3.00 -6 -5 0 49.99 3.00 6 5 0 49.10 3.10 -6 5 0 53.19 3.80 6 5 0 55.29 3.50 6 5 0 49.30 2.90 -6 5 0 44.10 3.40 6 5 0 49.99 3.00 -6 5 0 46.20 3.40 6 5 0 50.79 3.10 -6 5 0 51.69 3.50 7 -5 0 7.90 1.60 7 -5 0 8.80 1.70 7 -5 0 6.70 1.40 7 -5 0 9.50 1.50 7 -5 0 9.00 1.50 7 -5 0 7.90 1.50 -7 5 0 6.50 1.60 -7 5 0 7.20 1.30 -7 5 0 7.10 1.40 -7 5 0 7.20 1.30 -7 5 0 7.10 1.40 -8 -5 0 33.60 2.30 -8 -5 0 35.30 2.30 8 -5 0 35.10 3.40 8 -5 0 33.90 3.00 8 -5 0 29.40 2.90 8 -5 0 33.90 2.80 8 -5 0 32.60 2.70 -8 -5 0 30.20 2.90 -8 -5 0 34.30 2.40 8 -5 0 37.00 3.00 8 5 0 31.40 2.40 8 5 0 32.80 3.00 8 5 0 35.10 2.50 -8 5 0 27.50 2.80 8 5 0 33.20 2.40 8 5 0 32.10 2.50 -8 5 0 25.70 2.70 -8 5 0 25.80 2.80 -9 -5 0 32.50 2.50 9 -5 0 37.50 3.20 -9 5 0 22.90 2.70 -9 5 0 25.20 2.90 9 5 0 32.30 2.50 10 -5 0 2.20 1.50 10 -5 0 3.00 1.90 -10 -5 0 2.70 1.00 10 -5 0 3.10 1.60 10 -5 0 1.90 1.50 10 -5 0 2.60 1.60 -10 -5 0 1.90 0.90 10 -5 0 3.70 1.60 10 5 0 1.70 1.60 -10 5 0 -0.70 2.10 -10 5 0 0.90 1.30 -10 5 0 2.10 1.40 10 5 0 1.50 1.10 10 5 0 3.20 1.10 -10 5 0 3.30 1.30 10 5 0 3.60 1.10 10 5 0 2.20 1.20 11 -5 0 12.40 2.10 -11 -5 0 10.30 1.30 -11 -5 0 9.60 1.40 -11 -5 0 9.50 1.50 11 -5 0 11.20 2.20 11 -5 0 9.00 2.10 11 -5 0 7.30 2.20 11 -5 0 11.00 2.00 -11 5 0 7.60 1.60 11 5 0 6.50 1.30 11 5 0 7.50 1.50 11 5 0 9.20 1.60 11 5 0 7.40 2.10 11 5 0 8.00 1.40 -11 5 0 10.00 1.90 12 -5 0 5.50 1.80 12 -5 0 3.50 1.90 -12 -5 0 4.40 1.10 12 -5 0 4.60 2.00 12 -5 0 5.00 1.90 -12 -5 0 6.30 1.40 12 -5 0 3.90 1.90 12 5 0 3.50 1.20 -12 5 0 4.30 1.80 12 5 0 4.90 1.40 -12 5 0 2.90 1.60 -12 5 0 3.20 1.50 12 5 0 3.80 1.50 12 5 0 4.50 2.10 13 5 0 0.00 1.10 0 -6 0 47.50 2.50 0 -6 0 37.80 2.50 0 -6 0 38.50 2.50 0 -6 0 47.00 2.50 0 -6 0 36.40 2.50 0 -6 0 46.10 2.40 0 6 0 39.60 2.50 0 6 0 39.20 2.50 0 6 0 35.80 2.50 0 6 0 44.20 2.60 1 -6 0 228.48 11.30 1 -6 0 219.98 11.30 1 -6 0 225.48 11.30 1 -6 0 230.98 11.40 -1 -6 0 220.88 11.20 -1 -6 0 209.98 11.20 -1 -6 0 186.28 11.20 1 -6 0 222.38 11.30 1 6 0 183.78 11.20 -1 6 0 227.18 11.30 -1 6 0 216.58 11.30 -1 6 0 214.88 11.30 -1 6 0 214.98 11.30 1 6 0 193.38 11.20 1 6 0 187.18 11.20 -1 6 0 227.38 11.40 2 -6 0 31.80 2.10 2 -6 0 32.30 2.10 2 -6 0 32.00 2.30 2 -6 0 33.50 2.20 2 -6 0 34.90 2.30 -2 -6 0 30.60 1.90 -2 -6 0 24.30 1.80 -2 -6 0 24.30 1.80 -2 -6 0 23.80 1.90 -2 6 0 31.70 2.10 2 6 0 31.60 1.90 -2 6 0 32.10 2.10 -2 6 0 34.10 2.20 -2 6 0 33.70 2.30 2 6 0 26.10 1.90 -2 6 0 31.70 2.10 -3 -6 0 0.30 0.50 3 -6 0 1.20 0.90 -3 -6 0 0.40 0.30 -3 -6 0 -0.60 0.50 3 -6 0 -0.60 0.60 -3 -6 0 0.40 0.30 3 -6 0 1.20 1.30 -3 -6 0 0.10 0.60 3 -6 0 1.00 0.70 3 -6 0 0.40 0.80 -3 6 0 0.30 0.70 3 6 0 0.90 0.60 3 6 0 0.90 0.60 3 6 0 0.60 0.60 -3 6 0 0.90 0.90 -3 6 0 0.70 0.70 -3 6 0 1.90 0.80 3 6 0 0.50 0.50 -3 6 0 0.40 0.80 -4 -6 0 76.99 4.60 4 -6 0 90.59 5.00 4 -6 0 84.09 4.90 4 -6 0 83.79 4.80 -4 -6 0 76.69 4.80 -4 -6 0 76.29 4.60 4 -6 0 82.49 5.10 4 -6 0 84.99 4.80 4 6 0 84.69 4.70 -4 6 0 77.69 5.10 -4 6 0 84.29 4.90 -4 6 0 83.29 4.90 -4 6 0 82.49 4.90 4 6 0 90.39 4.70 -4 6 0 85.79 4.90 4 6 0 86.79 4.70 4 6 0 93.59 4.70 -5 -6 0 81.19 4.70 -5 -6 0 75.49 4.40 5 -6 0 85.59 4.90 5 -6 0 72.89 4.80 5 -6 0 82.79 4.80 5 -6 0 68.99 5.00 5 -6 0 75.59 4.70 -5 -6 0 75.99 4.40 -5 6 0 88.29 4.80 5 6 0 80.79 4.80 5 6 0 83.69 4.50 -5 6 0 83.19 5.10 5 6 0 81.99 4.60 -5 6 0 76.59 4.80 -5 6 0 89.29 5.00 5 6 0 77.49 4.50 -5 6 0 70.99 4.70 5 6 0 75.09 4.50 6 -6 0 154.48 9.50 6 -6 0 175.38 9.60 6 -6 0 175.08 9.90 -6 -6 0 189.68 9.60 6 -6 0 158.98 9.50 -6 -6 0 189.98 9.30 6 -6 0 158.78 9.50 6 -6 0 170.28 9.60 6 6 0 198.18 9.30 -6 6 0 167.98 9.90 6 6 0 191.68 9.30 -6 6 0 178.28 9.50 -6 6 0 156.38 9.50 -6 6 0 161.48 9.60 -6 6 0 156.18 9.50 -7 -6 0 65.59 3.60 -7 -6 0 60.19 3.60 7 -6 0 55.89 4.10 7 -6 0 57.99 4.20 7 -6 0 55.09 4.50 7 -6 0 62.29 4.20 7 -6 0 61.69 4.20 7 -6 0 58.99 4.00 -7 -6 0 64.19 4.20 7 6 0 65.49 3.70 -7 6 0 51.19 4.50 -7 6 0 52.69 4.00 7 6 0 62.99 3.70 7 6 0 62.99 3.70 -7 6 0 55.29 4.10 7 6 0 59.79 3.70 7 6 0 66.69 4.20 7 6 0 59.89 3.50 -7 6 0 58.49 4.10 -7 6 0 70.99 4.10 8 -6 0 20.70 2.50 -8 -6 0 23.70 1.90 -8 -6 0 24.70 1.90 8 -6 0 25.50 2.70 8 -6 0 23.00 2.50 8 -6 0 25.60 2.60 8 -6 0 26.60 2.80 -8 -6 0 21.70 2.40 -8 6 0 19.40 2.20 8 6 0 23.90 1.90 8 6 0 24.30 2.00 -8 6 0 23.90 2.60 8 6 0 27.80 2.10 8 6 0 23.30 2.10 8 6 0 24.70 2.20 -8 6 0 23.70 2.50 9 -6 0 0.10 1.60 -9 -6 0 0.70 0.80 9 -6 0 2.10 1.40 9 -6 0 0.00 1.40 9 -6 0 1.80 1.50 9 -6 0 -0.40 1.30 9 -6 0 -1.10 1.30 -9 -6 0 0.90 0.80 9 6 0 0.50 0.90 -9 6 0 1.30 0.90 -9 6 0 -0.20 0.90 9 6 0 1.20 0.90 9 6 0 0.50 0.80 9 6 0 -0.20 1.00 9 6 0 -0.60 1.60 -9 6 0 0.20 1.30 -9 6 0 0.00 1.20 -9 6 0 -0.50 1.20 10 -6 0 35.20 3.50 10 -6 0 38.00 3.60 -10 -6 0 34.60 2.60 10 -6 0 31.90 4.00 10 -6 0 32.90 3.40 10 -6 0 37.30 3.60 10 6 0 32.00 2.70 10 6 0 35.00 2.90 10 6 0 31.00 2.60 -10 6 0 33.20 3.20 10 6 0 33.70 3.50 10 6 0 36.80 2.90 -10 6 0 38.90 3.30 -10 6 0 38.20 4.70 11 -6 0 0.70 1.90 11 -6 0 -0.70 1.60 11 -6 0 -1.70 1.60 11 -6 0 0.50 1.70 11 -6 0 -1.30 1.50 -11 -6 0 0.30 1.00 -11 -6 0 0.80 1.50 11 6 0 0.10 1.00 11 6 0 0.60 1.00 11 6 0 -0.20 1.30 -11 6 0 0.20 1.30 -11 6 0 -1.30 1.50 11 6 0 -1.00 1.70 -11 6 0 0.30 1.60 12 -6 0 2.60 1.90 12 -6 0 3.90 1.90 12 -6 0 2.00 2.20 -12 6 0 1.70 1.40 12 6 0 1.00 1.40 -12 6 0 -0.90 1.50 12 6 0 1.90 2.00 12 6 0 3.40 1.10 12 6 0 4.00 1.30 0 -7 0 -0.10 0.40 0 -7 0 -1.50 0.70 0 -7 0 0.10 0.60 0 -7 0 0.00 0.60 0 -7 0 -0.90 0.60 0 -7 0 -0.40 0.60 0 7 0 -1.50 0.60 0 7 0 -0.30 0.70 0 7 0 -0.70 0.70 0 7 0 -1.20 0.70 -1 -7 0 2.40 0.70 -1 -7 0 1.70 0.70 -1 -7 0 2.50 0.60 1 -7 0 4.40 0.80 1 -7 0 2.70 0.90 1 -7 0 2.10 1.30 1 -7 0 4.60 0.80 1 -7 0 3.20 0.50 1 -7 0 2.40 0.90 1 7 0 3.40 0.80 1 7 0 2.80 0.70 -1 7 0 3.80 0.90 -1 7 0 3.70 0.90 1 7 0 2.30 0.80 -1 7 0 3.40 0.90 1 7 0 2.40 0.60 -1 7 0 1.80 0.80 -1 7 0 3.20 0.80 -2 -7 0 204.58 11.80 -2 -7 0 218.98 11.90 -2 -7 0 207.88 11.90 2 -7 0 256.27 12.10 2 -7 0 247.58 12.10 2 -7 0 253.37 12.10 2 7 0 203.78 11.90 2 7 0 207.78 11.90 2 7 0 208.58 12.00 2 7 0 203.98 12.00 -2 7 0 254.47 12.10 -2 7 0 250.87 12.10 3 -7 0 173.58 9.50 3 -7 0 175.38 9.40 3 -7 0 185.98 9.60 3 -7 0 182.58 9.50 -3 -7 0 146.79 9.20 3 -7 0 175.78 9.50 3 7 0 187.58 9.30 -3 7 0 181.78 9.60 -3 7 0 182.88 9.50 -3 7 0 167.88 9.40 3 7 0 147.59 9.30 3 7 0 160.48 9.20 3 7 0 174.28 9.30 -3 7 0 172.68 9.40 -3 7 0 181.78 9.60 3 7 0 182.18 9.30 4 -7 0 60.99 3.70 -4 -7 0 47.50 3.30 4 -7 0 59.49 3.50 4 -7 0 62.99 3.70 4 -7 0 58.99 3.60 4 -7 0 61.69 4.00 -4 -7 0 50.49 3.50 -4 7 0 64.09 5.30 4 7 0 52.09 3.40 -4 7 0 60.19 3.70 4 7 0 54.49 3.50 4 7 0 51.89 3.30 -4 7 0 56.19 3.60 -4 7 0 57.79 3.70 -4 7 0 62.39 3.60 4 7 0 54.79 3.50 4 7 0 53.49 3.40 5 -7 0 14.60 1.50 5 -7 0 15.00 1.70 5 -7 0 12.60 1.80 5 -7 0 13.50 1.70 5 -7 0 12.10 1.50 5 -7 0 12.50 1.60 -5 7 0 14.20 1.70 -5 7 0 11.90 1.60 -5 7 0 15.00 1.90 -5 7 0 12.90 1.60 -5 7 0 15.60 1.70 6 -7 0 57.99 4.00 6 -7 0 58.09 4.10 -6 -7 0 55.19 3.50 -6 -7 0 53.89 3.50 6 -7 0 63.39 3.90 6 -7 0 56.39 4.40 6 -7 0 58.99 3.90 -6 -7 0 56.59 3.90 6 -7 0 68.59 4.20 6 7 0 57.39 3.60 6 7 0 58.49 4.00 -6 7 0 58.79 4.40 -6 7 0 58.79 4.00 -6 7 0 59.49 3.90 6 7 0 54.29 3.60 -6 7 0 69.59 4.10 -6 7 0 58.59 4.00 7 -7 0 1.60 1.50 7 -7 0 6.40 1.50 7 -7 0 3.90 1.40 7 -7 0 4.00 1.30 7 -7 0 6.50 1.50 -7 7 0 5.30 1.30 -7 7 0 3.80 1.70 -7 7 0 5.20 1.40 7 7 0 7.90 1.20 -7 7 0 3.80 1.40 -7 7 0 3.50 1.30 -8 -7 0 11.70 1.20 8 -7 0 12.40 1.80 8 -7 0 10.10 1.90 8 -7 0 12.50 1.80 -8 -7 0 12.40 1.80 -8 7 0 10.90 1.70 8 7 0 13.20 1.40 8 7 0 10.10 1.90 -8 7 0 11.40 1.80 8 7 0 12.00 1.30 8 7 0 16.70 1.60 8 7 0 12.10 1.40 -8 7 0 10.80 2.50 9 -7 0 2.50 1.70 9 -7 0 2.40 1.40 -9 -7 0 -1.80 1.40 -9 -7 0 1.30 0.80 9 -7 0 0.90 1.50 9 -7 0 2.00 1.50 9 -7 0 -0.80 1.60 9 -7 0 1.30 1.50 9 7 0 -0.70 2.40 -9 7 0 0.30 2.00 -9 7 0 1.20 1.60 9 7 0 0.60 1.00 9 7 0 1.40 0.90 9 7 0 2.00 0.90 9 7 0 1.30 1.00 -9 7 0 1.10 1.40 -9 7 0 0.90 1.30 -9 7 0 0.90 1.40 10 -7 0 4.30 1.70 10 -7 0 7.70 1.90 10 -7 0 4.50 1.80 10 -7 0 4.70 1.60 10 -7 0 1.10 2.10 10 7 0 2.00 1.80 10 7 0 6.00 1.10 10 7 0 3.70 1.00 -10 7 0 4.90 1.50 -10 7 0 3.20 1.70 -10 7 0 5.70 1.70 10 7 0 5.20 1.20 10 7 0 3.50 1.30 -11 -7 0 1.50 0.90 11 -7 0 -1.60 1.70 11 -7 0 1.90 1.70 -11 -7 0 1.50 1.10 11 -7 0 -0.50 1.50 11 -7 0 1.00 1.70 11 7 0 2.20 1.50 11 7 0 -1.30 1.70 11 7 0 2.40 1.00 -11 7 0 2.10 1.60 11 7 0 -0.60 1.10 11 7 0 1.20 1.10 -11 7 0 0.70 1.40 12 -7 0 5.20 2.30 12 -7 0 1.70 1.80 12 -7 0 2.40 2.00 12 -7 0 0.10 1.70 -12 7 0 3.60 1.70 12 7 0 4.00 1.10 12 7 0 2.60 1.40 12 7 0 2.80 1.20 -12 7 0 4.70 1.50 12 7 0 1.30 2.20 0 -8 0 201.58 10.20 0 -8 0 193.78 10.20 0 -8 0 192.78 10.00 0 -8 0 206.08 10.20 0 8 0 188.38 10.20 0 8 0 183.08 10.20 0 8 0 183.28 10.20 0 8 0 170.98 10.10 0 8 0 189.38 10.20 1 -8 0 13.50 1.60 -1 -8 0 9.70 1.10 1 -8 0 10.30 1.30 1 -8 0 14.30 1.70 -1 -8 0 8.70 1.10 -1 -8 0 12.90 1.30 -1 -8 0 8.60 1.00 1 8 0 8.70 1.10 -1 8 0 10.50 1.30 1 8 0 9.60 1.10 -1 8 0 8.00 1.10 -1 8 0 8.80 1.20 -1 8 0 9.40 1.20 1 8 0 8.30 1.10 -1 8 0 9.90 1.30 1 8 0 8.60 1.20 1 8 0 13.90 1.50 2 -8 0 186.58 9.20 2 -8 0 188.58 9.20 2 -8 0 185.48 9.20 -2 -8 0 151.98 8.90 2 -8 0 185.08 9.50 -2 -8 0 156.38 9.00 -2 -8 0 150.58 9.00 2 8 0 153.58 9.00 2 8 0 154.28 9.10 2 8 0 146.89 9.10 -2 8 0 184.08 9.30 2 8 0 156.18 9.10 2 8 0 148.59 9.10 -2 8 0 192.08 9.60 -2 8 0 186.58 9.30 -2 8 0 187.58 9.30 3 -8 0 37.20 2.70 -3 -8 0 29.20 2.20 -3 -8 0 27.60 2.20 -3 -8 0 26.20 2.20 3 -8 0 39.70 2.70 -3 -8 0 28.80 1.80 3 -8 0 38.60 2.60 3 8 0 26.80 2.30 3 8 0 31.70 2.30 -3 8 0 39.10 2.70 -3 8 0 36.20 2.60 3 8 0 30.50 3.00 -3 8 0 39.40 2.70 3 8 0 29.30 2.30 3 8 0 29.60 2.30 4 -8 0 461.25 22.50 4 -8 0 461.05 22.70 4 -8 0 440.86 22.50 -4 -8 0 381.66 22.30 4 -8 0 445.66 22.30 4 -8 0 440.36 22.50 4 8 0 379.96 22.20 4 8 0 392.76 22.30 -4 8 0 457.65 22.60 -4 8 0 448.96 22.50 4 8 0 381.66 22.30 -4 8 0 464.55 22.70 4 8 0 390.26 22.30 -4 8 0 448.06 22.60 -4 8 0 432.56 22.50 4 8 0 379.76 22.30 -5 -8 0 51.59 3.30 5 -8 0 44.10 3.70 5 -8 0 43.20 3.10 5 -8 0 41.60 3.50 -5 -8 0 43.40 2.90 5 -8 0 41.00 3.40 5 -8 0 41.90 3.30 -5 -8 0 44.50 2.90 5 -8 0 39.10 3.30 -5 8 0 44.80 3.80 5 8 0 48.50 3.00 5 8 0 46.40 3.00 5 8 0 46.70 3.00 -5 8 0 43.30 3.30 -5 8 0 51.59 3.50 5 8 0 46.80 3.10 -5 8 0 43.40 3.30 -5 8 0 45.60 3.50 -6 -8 0 12.80 1.20 -6 -8 0 11.90 1.20 -6 -8 0 13.00 1.60 6 -8 0 7.90 1.60 6 -8 0 11.00 1.50 6 -8 0 9.50 1.60 6 -8 0 11.40 1.60 6 -8 0 11.20 1.80 6 -8 0 6.10 1.80 6 8 0 12.40 1.30 -6 8 0 8.70 1.60 6 8 0 11.40 1.50 6 8 0 13.00 1.30 -6 8 0 9.50 1.50 -6 8 0 9.30 1.60 -6 8 0 10.10 1.60 -6 8 0 6.60 1.90 6 8 0 12.10 1.60 6 8 0 11.40 1.30 -7 -8 0 3.00 0.80 7 -8 0 3.60 1.30 7 -8 0 -1.20 1.60 7 -8 0 3.10 1.50 7 -8 0 0.40 1.30 -7 -8 0 2.40 1.20 7 -8 0 0.80 1.20 -7 8 0 2.70 1.40 -7 8 0 0.20 1.70 7 8 0 1.70 0.90 -7 8 0 0.90 1.30 7 8 0 2.20 0.90 7 8 0 2.30 0.90 7 8 0 1.70 1.40 7 8 0 1.00 1.20 -7 8 0 -0.60 1.10 8 -8 0 3.90 1.70 8 -8 0 0.80 1.30 8 -8 0 0.10 1.00 8 -8 0 -0.90 1.20 -8 -8 0 -0.30 0.70 8 -8 0 -2.40 1.70 -8 -8 0 -0.40 1.10 8 -8 0 2.90 1.50 8 8 0 -2.40 1.30 -8 8 0 0.40 1.30 8 8 0 0.40 1.00 -8 8 0 -1.40 1.20 8 8 0 0.00 1.00 -8 8 0 0.20 1.30 -8 8 0 0.50 1.60 8 8 0 1.80 0.90 -8 8 0 -3.00 1.60 8 8 0 0.40 0.80 9 -8 0 29.50 3.50 -9 -8 0 33.70 2.40 9 -8 0 39.30 3.70 -9 -8 0 29.70 3.20 -9 -8 0 32.20 2.40 9 -8 0 34.40 3.20 9 -8 0 37.80 3.50 9 -8 0 36.00 3.50 -9 8 0 29.50 4.40 9 8 0 27.90 3.40 9 8 0 33.20 2.80 9 8 0 33.10 2.70 9 8 0 32.00 2.70 -9 8 0 32.50 3.10 10 -8 0 1.70 1.90 10 -8 0 1.40 1.60 10 -8 0 0.70 1.40 10 -8 0 -3.60 1.50 10 -8 0 3.10 2.80 10 8 0 0.00 1.10 10 8 0 0.50 1.10 -10 8 0 0.60 1.40 10 8 0 -0.70 0.90 10 8 0 0.90 1.80 -10 8 0 -0.50 1.40 10 8 0 -0.20 0.90 11 -8 0 -1.60 1.60 11 -8 0 -2.60 1.60 11 -8 0 -0.40 1.90 -11 -8 0 -0.60 0.80 -11 -8 0 0.60 0.90 11 -8 0 0.50 1.60 -11 8 0 -0.10 1.40 11 8 0 2.40 1.20 11 8 0 -1.30 1.70 11 8 0 -0.60 0.90 -11 8 0 1.20 1.60 11 8 0 -0.40 1.00 0 -9 0 0.60 0.60 0 -9 0 0.40 0.80 0 -9 0 0.80 0.80 0 -9 0 0.50 0.90 0 -9 0 -0.20 0.80 0 9 0 0.60 0.90 0 9 0 1.60 0.90 0 9 0 0.20 1.00 0 9 0 0.40 0.70 -1 -9 0 87.99 4.90 1 -9 0 92.99 4.80 1 -9 0 93.89 5.10 -1 -9 0 83.69 4.90 1 -9 0 95.79 5.20 1 -9 0 89.49 5.00 1 -9 0 96.99 5.00 -1 -9 0 74.69 4.80 -1 -9 0 79.79 4.80 1 -9 0 95.59 5.20 1 9 0 80.79 5.00 -1 9 0 89.49 5.20 1 9 0 74.39 5.00 -1 9 0 86.89 5.10 1 9 0 82.79 5.10 1 9 0 79.19 5.00 -1 9 0 88.99 5.10 -1 9 0 90.89 5.20 -1 9 0 82.89 5.10 -2 -9 0 14.80 1.30 -2 -9 0 15.40 1.60 -2 -9 0 13.60 1.40 -2 -9 0 13.00 1.50 -2 -9 0 12.90 1.40 2 -9 0 17.90 2.10 2 -9 0 15.20 1.70 -2 9 0 11.50 1.60 2 9 0 11.30 1.20 2 9 0 14.10 1.70 -2 9 0 19.40 2.10 -2 9 0 17.90 1.90 2 9 0 16.50 1.80 2 9 0 17.10 1.80 -2 9 0 17.90 2.10 3 -9 0 1.20 1.10 3 -9 0 2.80 1.30 3 -9 0 1.70 1.00 3 -9 0 0.90 1.40 -3 -9 0 -2.00 0.90 -3 -9 0 -1.60 0.80 3 -9 0 1.80 1.20 -3 -9 0 2.40 0.80 3 9 0 -0.20 1.00 -3 9 0 1.10 1.20 3 9 0 0.50 0.80 -3 9 0 0.40 1.20 3 9 0 -1.30 1.00 -3 9 0 -0.10 1.40 3 9 0 -1.30 0.90 -3 9 0 2.10 1.30 3 9 0 -0.50 0.90 -3 9 0 0.50 1.10 4 -9 0 55.69 4.10 4 -9 0 49.60 3.60 4 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15.60 1 -10 0 321.17 15.80 1 -10 0 312.37 15.80 -1 -10 0 267.77 15.50 1 -10 0 323.97 15.70 -1 -10 0 265.57 15.70 1 -10 0 329.37 15.50 -1 -10 0 277.97 15.70 1 -10 0 317.97 15.80 -1 10 0 297.67 15.80 1 10 0 276.27 15.80 -1 10 0 297.77 15.80 1 10 0 275.27 15.80 -1 10 0 303.67 15.80 1 10 0 264.37 15.70 -1 10 0 312.87 15.90 1 10 0 279.67 15.80 -1 10 0 315.07 15.90 2 -10 0 58.29 3.60 -2 -10 0 44.70 3.10 2 -10 0 56.89 3.50 -2 -10 0 48.30 3.00 2 -10 0 52.69 3.50 2 -10 0 57.29 3.70 2 -10 0 55.29 3.80 -2 -10 0 49.30 3.30 2 -10 0 51.69 3.10 -2 -10 0 49.20 3.10 -2 -10 0 44.30 3.30 2 10 0 50.39 3.40 2 10 0 50.49 3.50 -2 10 0 56.79 3.70 -2 10 0 51.19 3.80 2 10 0 51.29 3.50 -2 10 0 53.29 3.70 -2 10 0 52.49 3.70 2 10 0 47.60 3.50 -2 10 0 57.39 3.80 3 -10 0 4.20 1.40 3 -10 0 3.20 1.30 3 -10 0 4.40 1.50 -3 -10 0 1.50 1.00 -3 -10 0 2.30 0.90 -3 -10 0 1.10 0.90 3 -10 0 2.30 1.10 3 -10 0 3.90 1.30 3 10 0 3.60 1.10 -3 10 0 1.70 1.30 -3 10 0 3.00 1.20 -3 10 0 2.70 1.40 -3 10 0 2.30 1.30 3 10 0 2.20 1.00 3 10 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6.40 1.70 -8 9 3 4.80 1.60 7 -9 -3 -1.90 1.50 -7 -9 3 1.80 0.80 -7 -9 3 3.00 1.00 -7 -9 3 3.70 1.30 7 -9 -3 0.00 1.40 -7 9 3 -1.80 1.30 7 9 -3 0.30 1.30 7 9 -3 1.20 1.00 7 9 -3 0.90 1.10 -7 9 3 -2.20 1.50 7 9 -3 1.10 1.00 7 9 -3 1.90 1.10 -6 -9 3 55.69 3.40 -6 -9 3 57.39 3.80 6 -9 -3 56.79 4.00 -6 -9 3 59.09 4.10 6 -9 -3 63.19 4.30 6 -9 -3 61.89 3.70 -6 -9 3 57.79 3.40 -6 -9 3 55.29 3.80 6 -9 -3 61.59 4.10 6 -9 -3 64.89 4.60 6 -9 -3 60.09 4.10 -6 9 3 62.19 4.10 -6 9 3 65.19 4.30 6 9 -3 58.39 3.90 -6 9 3 70.89 4.30 6 9 -3 54.49 3.90 6 9 -3 63.09 4.10 6 9 -3 59.79 3.90 -6 9 3 70.59 4.70 -5 -9 3 16.60 2.10 -5 -9 3 15.50 1.60 5 -9 -3 14.10 1.90 -5 -9 3 16.40 1.60 5 -9 -3 17.40 1.90 5 -9 -3 17.30 1.60 5 -9 -3 16.80 1.90 5 -9 -3 17.40 1.80 -5 -9 3 12.30 1.50 -5 -9 3 15.30 1.60 5 9 -3 18.30 2.10 5 9 -3 17.00 2.10 -5 9 3 15.40 1.90 5 9 -3 16.80 1.70 -5 9 3 15.70 1.90 -5 9 3 17.80 2.20 5 9 -3 14.20 1.60 5 9 -3 15.50 1.70 -5 9 3 17.30 1.90 -5 9 3 16.80 1.90 4 -9 -3 1.90 1.20 -4 -9 3 -0.40 0.80 4 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2.50 -3 2 8 37.30 2.50 -3 2 8 36.30 2.50 3 2 -8 40.00 2.60 2 -2 -8 20.10 1.60 2 -2 -8 19.70 1.60 2 -2 -8 21.00 1.50 -2 -2 8 21.90 1.80 -2 -2 8 22.30 1.80 -2 -2 8 20.60 1.80 -2 -2 8 22.60 1.80 2 -2 -8 18.50 1.50 -2 -2 8 22.30 1.80 2 2 -8 22.70 1.80 -2 2 8 22.20 1.70 -2 2 8 18.90 1.60 -2 2 8 21.90 1.70 2 2 -8 24.30 1.90 -2 2 8 20.70 1.60 2 2 -8 23.30 2.50 -2 2 8 21.30 1.60 2 2 -8 23.80 1.80 -1 -2 8 649.24 34.10 -1 -2 8 649.04 34.00 1 -2 -8 659.23 33.80 -1 -2 8 648.04 34.00 1 -2 -8 641.34 33.90 1 -2 -8 664.03 33.80 -1 -2 8 663.03 34.00 1 -2 -8 655.83 33.90 1 2 -8 647.24 34.00 -1 2 8 658.73 33.90 -1 2 8 632.54 33.90 -1 2 8 666.03 34.00 -1 2 8 661.03 33.90 1 2 -8 667.53 34.00 1 2 -8 644.84 34.00 1 2 -8 633.14 33.90 0 -2 8 3.50 1.00 0 -2 8 3.00 0.80 0 -2 8 3.10 0.80 0 -2 8 3.00 0.90 0 -2 -8 3.70 0.50 0 -2 8 2.70 0.70 0 -2 -8 3.30 0.50 0 2 8 3.90 0.60 0 2 8 3.70 0.50 0 2 -8 2.20 0.80 0 2 8 4.50 0.60 0 2 -8 2.00 0.70 0 2 -8 3.50 0.80 0 2 -8 2.10 0.80 0 2 8 3.40 0.60 -1 -2 -8 280.77 14.50 1 -2 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5.70 8 4 -9 96.79 6.00 -8 4 9 92.99 5.80 -8 4 9 91.29 5.70 8 4 -9 92.19 5.80 8 4 -9 95.19 5.80 8 4 -9 89.99 5.80 7 -4 -9 30.20 2.80 7 -4 -9 31.30 2.60 7 -4 -9 31.80 2.80 7 -4 -9 30.50 2.70 -7 -4 9 30.90 2.60 -7 -4 9 32.70 2.80 -7 -4 9 32.90 2.90 -7 -4 9 34.40 2.80 7 -4 -9 35.10 2.90 -7 -4 9 29.20 2.80 -7 4 9 33.30 2.90 7 4 -9 31.40 2.90 -7 4 9 29.00 2.80 7 4 -9 32.00 2.90 -7 4 9 29.60 3.10 7 4 -9 27.10 2.80 -7 4 9 30.50 2.80 -7 4 9 33.60 2.90 7 4 -9 29.60 3.10 7 4 -9 32.70 2.90 6 -4 -9 86.19 5.10 6 -4 -9 84.49 5.20 -6 -4 9 88.39 5.50 -6 -4 9 92.79 5.30 6 -4 -9 83.19 5.20 6 -4 -9 81.69 5.20 6 -4 -9 82.79 5.20 -6 -4 9 97.09 5.30 -6 -4 9 91.69 5.30 -6 -4 9 88.89 5.30 -6 4 9 80.59 5.20 -6 4 9 85.79 5.60 6 4 -9 86.99 5.30 6 4 -9 93.79 5.30 -6 4 9 80.49 5.30 -6 4 9 76.69 5.30 -6 4 9 85.09 5.10 6 4 -9 93.29 5.40 6 4 -9 89.29 5.30 -6 4 9 78.09 5.40 6 4 -9 93.39 5.40 -5 -4 9 72.39 4.60 5 -4 -9 78.49 4.50 5 -4 -9 78.39 4.60 5 -4 -9 75.49 4.50 5 -4 -9 70.99 4.50 5 -4 -9 76.29 4.50 -5 -4 9 77.19 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1.80 -2 -4 9 29.80 2.30 2 -4 -9 26.40 2.00 -2 -4 9 28.70 2.40 2 -4 -9 26.00 2.00 -2 -4 9 32.20 2.40 -2 4 9 24.20 2.20 -2 4 9 31.10 2.00 2 4 -9 29.50 2.30 -2 4 9 27.40 2.00 2 4 -9 33.30 2.20 -2 4 9 26.60 2.10 2 4 -9 29.90 2.30 -2 4 9 27.50 2.00 2 4 -9 34.20 2.40 -1 -4 9 37.00 2.60 1 -4 -9 34.20 2.20 -1 -4 9 37.80 2.60 1 -4 -9 33.80 2.20 -1 -4 9 37.80 2.60 -1 -4 9 34.60 2.70 -1 -4 9 38.30 2.50 -1 -4 9 36.60 2.60 -1 4 9 34.40 2.30 -1 4 9 35.30 2.30 1 4 -9 34.70 2.60 1 4 -9 36.80 2.60 -1 4 9 32.00 2.80 -1 4 9 34.20 2.20 -1 4 9 32.60 2.30 1 4 -9 39.60 2.60 0 -4 -9 4.60 0.60 0 -4 9 3.60 1.00 0 -4 9 2.60 0.90 0 -4 9 3.30 1.00 0 -4 9 2.90 1.00 0 -4 9 2.00 0.90 0 4 9 3.60 0.60 0 4 9 4.30 0.60 0 4 9 4.00 0.60 0 4 9 4.30 0.70 0 4 -9 3.40 1.00 1 -4 9 61.49 3.90 1 -4 9 62.19 4.20 -1 -4 -9 63.99 3.30 1 -4 9 60.99 3.90 -1 -4 -9 61.39 3.30 1 -4 9 57.89 3.80 1 4 9 62.49 3.40 -1 4 -9 58.29 4.10 1 4 9 64.79 3.40 -1 4 -9 64.59 3.80 -1 4 -9 62.89 3.80 -1 4 -9 61.29 3.90 1 4 9 65.59 3.40 2 -4 9 88.99 5.10 2 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71.79 4.10 6 4 9 63.29 3.90 6 4 9 63.49 3.90 6 4 9 69.99 4.80 -6 4 -9 65.29 4.70 -6 4 -9 75.69 4.30 6 4 9 71.69 4.80 7 -4 9 10.30 2.00 7 -4 9 10.10 1.80 7 -4 9 11.00 1.80 7 -4 9 9.50 2.80 -7 4 -9 14.00 1.40 -7 4 -9 11.50 1.30 7 4 9 11.30 1.20 7 4 9 14.40 3.30 7 4 9 12.20 2.00 -7 4 -9 12.50 1.70 -7 4 -9 12.50 2.40 -7 4 -9 8.00 1.50 7 4 9 12.80 1.20 8 -4 9 4.10 1.90 8 -4 9 6.60 2.00 8 -4 9 2.50 1.40 8 -4 9 3.90 1.50 8 -4 9 4.10 1.50 8 4 9 3.60 1.50 8 4 9 2.40 0.70 8 4 9 2.90 1.00 8 4 9 2.00 0.90 8 4 9 2.80 0.50 8 4 9 3.90 1.80 -8 4 -9 3.50 0.90 -8 4 -9 3.00 1.20 9 -4 9 2.70 1.70 9 -4 9 3.10 2.10 9 -4 9 2.40 2.00 9 -4 9 3.80 1.50 9 -4 9 2.80 1.30 9 4 9 -0.40 1.00 9 4 9 1.10 1.50 9 4 9 1.20 0.50 -9 4 -9 2.70 1.10 -9 4 -9 1.10 1.20 9 4 9 1.90 0.90 9 4 9 3.10 1.80 10 -4 9 6.20 3.00 10 -4 9 0.90 1.60 10 -4 9 4.50 1.50 10 -4 9 7.10 3.00 10 -4 9 5.80 1.70 10 4 9 4.70 2.10 10 4 9 3.00 0.60 -10 4 -9 5.60 1.40 10 4 9 4.00 1.70 10 4 9 2.10 1.10 10 4 9 6.00 1.10 -13 -5 9 3.20 1.50 13 -5 -9 6.00 1.70 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12.40 1.60 3 -5 -9 131.99 7.30 3 -5 -9 133.19 7.30 -3 -5 9 131.69 7.60 -3 -5 9 134.19 7.50 -3 -5 9 136.49 7.80 3 -5 -9 130.79 7.40 3 -5 -9 126.79 7.40 -3 -5 9 137.89 7.50 -3 -5 9 138.49 7.50 -3 -5 9 139.79 7.60 -3 5 9 130.89 7.40 3 5 -9 143.29 7.60 -3 5 9 135.69 7.40 -3 5 9 130.09 7.40 -3 5 9 132.29 7.40 3 5 -9 133.89 7.50 -3 5 9 134.69 7.30 3 5 -9 139.29 7.60 -2 -5 9 8.40 1.20 -2 -5 9 12.20 1.40 -2 -5 9 9.40 1.30 2 -5 -9 10.60 1.10 2 -5 -9 9.50 1.00 2 -5 -9 8.70 1.00 -2 -5 9 10.00 1.30 -2 -5 9 7.40 1.30 -2 -5 9 10.40 1.30 2 -5 -9 10.10 1.10 -2 5 9 10.10 1.10 2 5 -9 9.90 1.30 -2 5 9 9.40 1.10 -2 5 9 11.10 1.20 2 5 -9 8.30 1.30 -2 5 9 8.70 1.00 -1 -5 9 40.40 3.00 -1 -5 9 40.80 2.90 -1 -5 9 39.40 3.00 -1 -5 9 42.30 3.00 1 -5 -9 43.40 2.50 -1 -5 9 41.10 3.00 -1 -5 9 40.20 2.90 1 -5 -9 42.50 2.50 -1 5 9 41.90 2.70 1 5 -9 40.30 3.00 -1 5 9 43.70 2.60 -1 5 9 41.70 2.60 1 5 -9 39.40 2.90 1 5 -9 36.90 4.10 1 5 -9 41.40 3.00 -1 5 9 45.70 2.60 -1 5 9 43.80 2.60 0 -5 9 107.69 6.10 0 -5 9 106.59 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233.88 12.70 6 -4 -10 243.08 12.70 6 -4 -10 231.58 12.70 -6 -4 10 229.68 12.70 6 -4 -10 234.28 12.70 -6 -4 10 236.78 12.90 -6 -4 10 235.58 12.80 -6 4 10 241.28 12.70 6 4 -10 233.08 12.70 6 4 -10 231.78 12.80 6 4 -10 238.28 12.90 -6 4 10 231.58 12.70 6 4 -10 226.68 12.70 -6 4 10 231.48 12.70 -6 4 10 231.08 13.00 -6 4 10 230.98 12.70 6 4 -10 229.48 12.80 5 -4 -10 15.50 1.60 -5 -4 10 15.60 1.80 -5 -4 10 16.20 1.70 5 -4 -10 15.80 1.80 -5 -4 10 14.40 1.80 -5 -4 10 17.40 1.90 5 -4 -10 14.40 1.60 5 -4 -10 18.20 1.80 5 -4 -10 17.10 1.70 -5 -4 10 18.30 2.20 -5 4 10 13.70 1.60 5 4 -10 12.90 1.70 5 4 -10 17.90 1.90 5 4 -10 13.30 1.80 -5 4 10 16.70 1.70 -5 4 10 14.80 1.60 -5 4 10 14.50 1.80 5 4 -10 14.10 1.80 -5 4 10 13.60 1.60 5 4 -10 13.90 1.70 4 -4 -10 13.00 1.60 4 -4 -10 13.30 1.40 -4 -4 10 10.20 1.50 -4 -4 10 13.60 1.60 4 -4 -10 11.50 1.30 -4 -4 10 15.10 1.70 -4 -4 10 12.10 1.50 4 -4 -10 14.10 1.40 -4 -4 10 11.60 1.50 4 4 -10 11.10 1.60 -4 4 10 13.00 1.40 4 4 -10 11.90 1.60 -4 4 10 13.80 1.40 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2.60 3 -4 10 31.00 2.50 3 -4 10 31.90 2.60 3 -4 10 26.00 3.10 -3 4 -10 29.90 2.40 3 4 10 30.00 1.70 3 4 10 28.80 1.80 3 4 10 30.30 1.80 -3 4 -10 31.40 2.50 -3 4 -10 38.30 4.00 3 4 10 34.20 2.90 3 4 10 29.60 1.70 -3 4 -10 31.60 2.50 4 -4 10 -1.80 1.20 4 -4 10 -1.50 0.90 4 -4 10 0.00 1.10 4 -4 10 -1.60 0.90 4 -4 10 -0.70 0.90 -4 4 -10 1.00 0.90 -4 4 -10 -0.90 0.80 4 4 10 -0.70 0.40 -4 4 -10 -0.90 1.80 4 4 10 0.50 0.50 4 4 10 0.40 1.20 -4 4 -10 -0.60 0.90 5 -4 10 30.80 2.70 5 -4 10 34.90 2.80 5 -4 10 33.30 3.30 5 -4 10 32.30 2.80 5 -4 10 29.40 2.70 5 4 10 30.00 3.00 -5 4 -10 31.30 2.50 -5 4 -10 28.40 2.30 5 4 10 27.60 1.90 5 4 10 28.70 1.90 5 4 10 31.10 3.10 6 -4 10 18.40 2.50 6 -4 10 17.40 1.90 6 -4 10 18.20 2.10 6 -4 10 14.30 1.80 6 -4 10 16.30 1.90 -6 4 -10 20.60 1.90 6 4 10 19.90 2.40 6 4 10 18.50 1.60 -6 4 -10 19.30 2.20 6 4 10 22.60 2.80 6 4 10 17.40 1.60 -6 4 -10 15.20 2.10 7 -4 10 28.10 3.40 7 -4 10 23.80 2.80 7 -4 10 22.40 2.40 -7 4 -10 27.60 2.80 -7 4 -10 26.20 2.10 7 4 10 28.30 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10 12.40 2.20 12 5 -10 18.30 2.30 12 5 -10 12.40 2.20 12 5 -10 14.40 2.10 -12 5 10 15.20 2.30 -11 -5 10 0.70 1.10 -11 -5 10 -0.70 1.30 11 -5 -10 1.00 1.60 11 -5 -10 1.60 1.30 11 -5 -10 -1.20 1.30 -11 -5 10 0.00 1.50 -11 5 10 -1.80 1.10 11 5 -10 -0.30 1.40 -11 5 10 -0.50 1.60 11 5 -10 -0.30 1.60 -11 5 10 0.10 1.40 11 5 -10 -0.80 1.40 11 5 -10 0.80 1.40 -10 -5 10 9.00 1.40 10 -5 -10 7.00 1.80 10 -5 -10 7.70 1.60 10 -5 -10 7.70 1.80 -10 -5 10 9.90 1.90 -10 -5 10 8.50 1.80 10 5 -10 8.90 1.80 -10 5 10 6.80 1.80 -10 5 10 8.00 1.60 10 5 -10 9.60 1.80 10 5 -10 8.00 1.90 -10 5 10 10.10 1.90 -10 5 10 5.80 1.60 10 5 -10 11.30 1.90 9 -5 -10 16.70 2.00 9 -5 -10 14.10 2.10 9 -5 -10 18.20 2.10 -9 -5 10 15.80 2.80 9 -5 -10 20.10 2.30 -9 -5 10 14.70 1.90 -9 -5 10 13.30 2.10 9 -5 -10 16.10 2.10 -9 -5 10 18.40 2.00 -9 -5 10 19.30 2.20 -9 -5 10 16.50 2.00 -9 5 10 16.60 2.10 -9 5 10 18.00 2.30 9 5 -10 20.00 2.20 9 5 -10 17.20 2.30 -9 5 10 15.50 2.00 9 5 -10 16.90 2.00 -9 5 10 15.90 2.00 9 5 -10 19.80 2.20 9 5 -10 17.10 2.10 -9 5 10 16.60 2.30 -9 5 10 12.70 2.00 8 -5 -10 10.40 1.70 8 -5 -10 8.80 1.60 8 -5 -10 9.60 1.60 -8 -5 10 8.90 1.60 -8 -5 10 8.40 1.50 8 -5 -10 6.80 1.30 8 -5 -10 7.90 1.40 -8 -5 10 8.70 1.70 -8 -5 10 8.50 1.30 8 5 -10 5.50 1.50 8 5 -10 6.50 2.20 -8 5 10 8.90 1.80 8 5 -10 9.90 1.70 -8 5 10 10.90 1.80 -8 5 10 8.60 1.60 -8 5 10 9.50 1.40 8 5 -10 11.50 1.80 8 5 -10 9.70 2.00 7 -5 -10 146.69 8.30 -7 -5 10 146.69 8.50 7 -5 -10 147.39 8.40 -7 -5 10 145.69 8.40 7 -5 -10 150.68 8.20 -7 -5 10 147.09 8.40 -7 -5 10 156.78 8.40 7 -5 -10 144.69 8.50 7 -5 -10 145.69 8.40 -7 -5 10 143.59 8.20 -7 5 10 142.19 8.40 -7 5 10 146.29 8.40 7 5 -10 150.48 8.40 7 5 -10 152.08 8.70 7 5 -10 144.59 8.40 -7 5 10 147.09 8.40 -7 5 10 131.39 9.10 7 5 -10 149.19 8.50 -7 5 10 148.99 8.40 6 -5 -10 107.39 6.20 6 -5 -10 102.89 6.10 -6 -5 10 103.89 6.20 6 -5 -10 106.39 6.00 -6 -5 10 102.09 6.30 6 -5 -10 107.89 6.10 -6 -5 10 102.19 6.30 -6 -5 10 102.19 6.20 6 -5 -10 106.49 6.20 -6 5 10 93.09 6.50 6 5 -10 110.09 6.40 6 5 -10 109.59 6.30 -6 5 10 99.89 6.00 -6 5 10 101.89 6.20 6 5 -10 106.99 6.30 6 5 -10 97.09 6.20 -6 5 10 104.89 6.20 -6 5 10 107.29 6.20 6 5 -10 99.79 6.20 -5 -5 10 10.00 1.60 -5 -5 10 9.50 1.50 5 -5 -10 8.70 1.30 5 -5 -10 8.10 1.40 5 -5 -10 9.60 1.40 5 -5 -10 11.90 1.40 -5 -5 10 6.60 1.40 -5 -5 10 10.70 1.60 -5 -5 10 6.80 1.50 5 -5 -10 9.30 1.40 -5 5 10 9.40 1.40 5 5 -10 7.20 1.50 5 5 -10 6.80 1.40 -5 5 10 9.50 1.40 -5 5 10 9.30 1.20 5 5 -10 6.40 1.40 5 5 -10 10.90 1.60 -5 5 10 9.40 1.40 -5 5 10 10.90 1.90 5 5 -10 10.20 1.60 -5 5 10 10.40 1.50 -4 -5 10 3.60 1.20 4 -5 -10 2.70 0.90 -4 -5 10 1.00 1.10 4 -5 -10 3.70 1.00 -4 -5 10 4.80 1.20 4 -5 -10 3.00 1.00 -4 -5 10 2.40 1.20 -4 -5 10 3.70 1.20 4 -5 -10 1.80 0.90 -4 5 10 2.80 1.00 -4 5 10 2.70 1.00 -4 5 10 2.50 1.00 4 5 -10 3.20 1.20 -4 5 10 2.00 0.80 4 5 -10 2.50 1.20 -4 5 10 4.70 1.10 4 5 -10 2.30 1.10 4 5 -10 1.70 1.20 3 -5 -10 5.10 1.00 -3 -5 10 4.10 1.30 3 -5 -10 6.00 0.90 -3 -5 10 3.50 1.20 -3 -5 10 4.70 1.20 -3 -5 10 4.10 1.20 -3 -5 10 3.30 1.30 3 -5 -10 4.50 0.90 3 -5 -10 6.50 0.90 -3 -5 10 4.30 1.20 -3 5 10 5.00 1.00 3 5 -10 3.20 1.10 -3 5 10 4.10 1.00 -3 5 10 6.50 1.10 -3 5 10 3.90 1.00 3 5 -10 5.20 1.30 -3 5 10 2.90 0.80 3 5 -10 2.40 1.10 3 5 -10 6.00 1.30 -2 -5 10 211.68 11.70 2 -5 -10 203.08 11.30 -2 -5 10 209.88 11.60 2 -5 -10 215.68 11.20 2 -5 -10 216.68 11.40 -2 -5 10 212.68 11.70 -2 -5 10 211.28 11.70 -2 -5 10 219.48 11.70 -2 5 10 209.28 11.40 -2 5 10 218.68 11.40 2 5 -10 219.08 11.70 -2 5 10 212.88 11.40 -2 5 10 213.88 11.50 2 5 -10 218.68 11.60 2 5 -10 213.08 11.70 -2 5 10 212.68 11.50 2 5 -10 223.68 11.70 -1 -5 10 31.80 2.60 1 -5 -10 31.00 2.10 -1 -5 10 32.80 2.70 -1 -5 10 35.10 2.70 -1 -5 10 33.40 2.60 -1 -5 10 31.80 2.80 1 -5 -10 32.60 2.10 -1 -5 10 28.80 2.60 1 5 -10 35.30 2.70 1 5 -10 38.70 2.80 -1 5 10 32.80 2.30 -1 5 10 29.80 2.30 1 5 -10 35.00 2.80 -1 5 10 32.30 2.20 -1 5 10 32.40 2.30 -1 5 10 33.60 2.30 0 -5 10 44.00 3.00 0 -5 -10 37.20 2.40 0 -5 10 43.90 3.00 0 -5 -10 39.90 2.40 0 -5 10 43.80 3.00 0 -5 10 44.70 3.30 0 -5 10 42.90 3.10 0 5 -10 43.50 3.00 0 5 -10 45.60 3.10 0 5 10 37.60 2.50 0 5 10 39.30 2.50 0 5 -10 43.40 3.10 0 5 10 40.80 2.50 0 5 10 37.40 2.50 1 -5 10 21.10 2.20 1 -5 10 22.50 2.40 1 -5 10 20.30 2.20 1 -5 10 18.10 2.10 1 -5 10 19.30 2.60 1 5 10 19.80 1.50 -1 5 -10 21.20 2.40 1 5 10 20.90 1.50 -1 5 -10 21.80 2.20 -1 5 -10 21.10 2.10 -1 5 -10 18.20 2.20 1 5 10 20.50 1.40 1 5 10 19.80 1.40 2 -5 10 5.40 1.30 2 -5 10 5.00 1.20 2 -5 10 5.80 1.60 2 -5 10 5.30 1.40 2 -5 10 3.00 1.30 -2 5 -10 2.40 1.20 -2 5 -10 4.30 1.20 2 5 10 6.70 0.80 -2 5 -10 7.50 1.40 -2 5 -10 3.30 1.30 2 5 10 6.40 0.60 3 -5 10 7.90 1.50 3 -5 10 7.90 1.50 3 -5 10 9.80 1.50 3 -5 10 8.20 1.80 3 -5 10 7.80 1.50 3 5 10 12.00 0.80 3 5 10 11.10 1.60 -3 5 -10 10.00 1.70 -3 5 -10 8.70 1.50 -3 5 -10 7.30 1.30 3 5 10 9.40 1.50 -3 5 -10 7.90 1.90 -3 5 -10 8.80 1.40 4 -5 10 17.70 2.00 4 -5 10 22.10 2.10 4 -5 10 17.80 2.20 4 -5 10 17.30 2.00 4 -5 10 19.90 2.00 4 5 10 21.10 2.40 -4 5 -10 21.90 2.10 4 5 10 18.70 1.20 -4 5 -10 16.00 2.00 4 5 10 25.00 2.60 -4 5 -10 24.00 3.00 5 -5 10 0.70 1.20 5 -5 10 1.10 1.20 5 -5 10 1.20 1.40 -5 5 -10 0.90 1.20 5 5 10 2.10 1.30 5 5 10 0.90 0.50 5 5 10 1.00 1.20 -5 5 -10 0.30 1.20 -5 5 -10 2.10 1.10 6 -5 10 23.10 2.90 6 -5 10 26.00 2.90 6 -5 10 31.80 3.00 6 -5 10 27.30 3.10 6 -5 10 34.30 3.60 -6 5 -10 34.30 3.80 6 5 10 29.00 3.10 -6 5 -10 28.30 3.20 -6 5 -10 26.70 2.90 6 5 10 33.50 3.20 6 5 10 26.80 1.90 -6 5 -10 33.10 2.60 -6 5 -10 32.80 2.90 6 5 10 26.90 1.90 7 -5 10 0.50 1.60 7 -5 10 0.90 1.30 7 -5 10 -0.80 1.50 7 -5 10 -0.20 1.30 7 -5 10 1.60 1.40 7 5 10 1.40 1.30 7 5 10 1.20 0.70 7 5 10 0.20 1.60 -7 5 -10 1.50 1.30 -7 5 -10 1.50 1.00 7 5 10 1.40 0.70 8 -5 10 1.40 1.60 8 -5 10 1.90 1.90 8 -5 10 4.50 2.00 8 -5 10 3.90 1.60 8 5 10 5.30 1.90 -8 5 -10 4.30 1.40 8 5 10 3.60 1.00 8 5 10 4.60 0.90 -8 5 -10 3.40 1.00 8 5 10 5.50 1.90 9 -5 10 0.10 1.30 9 -5 10 0.50 2.00 9 -5 10 1.50 2.10 9 -5 10 0.00 1.30 9 -5 10 0.30 1.60 -9 5 -10 0.60 1.20 9 5 10 2.30 1.50 9 5 10 0.50 0.80 -9 5 -10 0.30 1.00 9 5 10 0.20 0.90 -12 -6 10 3.40 1.80 -12 -6 10 0.50 1.00 12 -6 -10 3.40 2.00 -12 -6 10 1.50 1.50 12 -6 -10 0.60 1.30 12 -6 -10 0.00 1.60 -12 -6 10 -0.60 1.60 12 6 -10 1.00 1.50 -12 6 10 2.30 1.80 -12 6 10 1.00 1.70 12 6 -10 0.10 1.60 -11 -6 10 4.40 1.70 11 -6 -10 1.40 1.70 11 -6 -10 3.90 1.40 11 -6 -10 2.20 1.60 -11 -6 10 3.70 1.40 -11 6 10 3.60 1.70 11 6 -10 6.60 1.80 11 6 -10 4.70 1.70 -11 6 10 4.40 1.70 11 6 -10 0.30 1.50 11 6 -10 2.70 1.80 -10 -6 10 -0.70 0.80 10 -6 -10 -1.70 1.40 -10 -6 10 0.20 1.40 10 -6 -10 -1.00 1.10 10 -6 -10 -1.60 1.40 -10 6 10 -0.90 1.50 10 6 -10 -0.90 1.20 -10 6 10 1.20 1.20 10 6 -10 -0.80 1.30 10 6 -10 -1.20 1.30 10 6 -10 -0.60 1.50 -10 6 10 -0.80 1.40 9 -6 -10 7.00 1.70 -9 -6 10 8.70 2.20 9 -6 -10 8.00 1.70 -9 -6 10 8.40 1.60 -9 -6 10 6.90 1.20 -9 -6 10 8.20 1.50 9 -6 -10 9.20 1.80 -9 -6 10 8.80 1.80 9 -6 -10 7.90 1.40 9 -6 -10 8.00 1.70 9 6 -10 10.70 1.90 -9 6 10 8.30 1.70 -9 6 10 7.10 1.70 9 6 -10 8.60 1.80 9 6 -10 7.70 1.70 9 6 -10 8.50 1.70 -9 6 10 9.90 1.50 9 6 -10 9.90 1.80 8 -6 -10 16.00 2.00 -8 -6 10 18.40 2.00 8 -6 -10 17.60 2.10 8 -6 -10 19.50 2.10 -8 -6 10 17.80 2.10 -8 -6 10 16.70 2.00 8 -6 -10 17.50 2.10 -8 -6 10 17.20 2.00 -8 -6 10 13.20 2.00 -8 6 10 16.70 2.10 -8 6 10 17.20 2.30 -8 6 10 19.00 2.10 8 6 -10 16.10 2.00 8 6 -10 16.60 2.10 8 6 -10 18.90 2.20 8 6 -10 19.20 2.40 -8 6 10 18.70 2.10 -7 -6 10 3.80 1.40 7 -6 -10 4.90 1.10 -7 -6 10 4.00 1.50 7 -6 -10 3.70 1.30 -7 -6 10 6.20 1.60 7 -6 -10 3.80 1.40 7 -6 -10 5.90 1.40 7 6 -10 4.20 1.40 7 6 -10 4.00 1.50 -7 6 10 4.00 1.10 7 6 -10 3.50 1.50 -7 6 10 5.30 1.50 -7 6 10 3.00 1.50 -7 6 10 3.20 1.30 -7 6 10 5.50 1.50 7 6 -10 4.00 1.50 7 6 -10 5.00 1.50 6 -6 -10 22.00 2.00 6 -6 -10 19.60 2.00 -6 -6 10 18.60 2.30 6 -6 -10 15.90 1.90 6 -6 -10 20.80 2.40 -6 -6 10 19.60 2.50 -6 -6 10 22.90 2.60 -6 -6 10 19.70 2.30 -6 -6 10 20.00 2.10 -6 6 10 20.00 2.80 6 6 -10 19.20 2.10 -6 6 10 20.30 2.10 6 6 -10 23.60 2.70 6 6 -10 24.90 2.30 -6 6 10 17.30 2.00 -6 6 10 16.70 2.00 -6 6 10 19.80 2.30 -6 6 10 16.70 2.00 6 6 -10 21.20 2.20 -5 -6 10 374.06 19.20 5 -6 -10 347.27 19.10 -5 -6 10 355.06 19.30 -5 -6 10 349.67 19.00 5 -6 -10 371.56 19.10 -5 -6 10 369.06 19.20 -5 -6 10 361.76 19.20 -5 -6 10 375.06 19.20 5 -6 -10 360.26 18.90 5 -6 -10 359.56 19.10 5 -6 -10 362.26 19.10 5 6 -10 369.36 19.20 5 6 -10 364.26 19.20 -5 6 10 355.96 19.10 -5 6 10 347.47 19.10 -5 6 10 349.37 18.90 5 6 -10 380.06 19.40 -5 6 10 333.57 19.10 5 6 -10 345.97 19.20 5 6 -10 374.56 19.20 -5 6 10 352.56 19.50 -5 6 10 341.67 19.10 4 -6 -10 3.80 1.00 -4 -6 10 3.80 1.30 4 -6 -10 2.80 1.00 -4 -6 10 2.70 1.30 -4 -6 10 2.50 1.30 -4 -6 10 3.70 1.10 -4 -6 10 3.60 1.30 4 -6 -10 4.20 1.00 4 -6 -10 2.90 0.90 -4 -6 10 2.90 1.30 -4 6 10 3.00 1.10 -4 6 10 3.20 1.20 4 6 -10 3.00 1.30 4 6 -10 4.50 1.40 4 6 -10 3.80 1.30 4 6 -10 4.50 1.30 -4 6 10 1.90 1.10 -4 6 10 1.90 1.10 -4 6 10 1.20 0.80 -3 -6 10 9.10 1.60 -3 -6 10 10.80 1.50 3 -6 -10 8.30 1.00 -3 -6 10 7.20 1.50 3 -6 -10 7.20 0.90 -3 -6 10 9.70 1.50 3 -6 -10 8.10 1.10 -3 -6 10 7.70 1.30 -3 -6 10 7.50 1.40 3 -6 -10 7.40 1.10 3 6 -10 6.30 1.40 3 6 -10 7.60 1.40 -3 6 10 7.50 1.20 3 6 -10 8.80 1.50 -3 6 10 8.60 1.30 3 6 -10 6.60 1.50 -3 6 10 6.70 1.10 -3 6 10 7.50 0.90 -2 -6 10 7.60 1.50 -2 -6 10 9.20 1.40 2 -6 -10 10.00 1.10 -2 -6 10 9.50 1.40 -2 -6 10 8.10 1.30 2 -6 -10 9.60 1.10 -2 -6 10 9.50 1.40 -2 -6 10 5.70 1.40 -2 6 10 8.10 1.10 -2 6 10 8.60 0.90 2 6 -10 5.60 1.40 -2 6 10 8.30 1.10 2 6 -10 9.60 1.50 -2 6 10 6.80 1.10 -2 6 10 8.20 1.10 2 6 -10 7.90 1.50 -1 -6 10 67.39 4.10 -1 -6 10 66.19 4.20 -1 -6 10 61.39 4.20 1 -6 -10 60.49 3.60 -1 -6 10 57.79 4.00 -1 -6 10 60.89 4.10 -1 -6 10 64.49 4.20 -1 6 10 58.79 3.70 -1 6 10 61.99 4.00 -1 6 10 60.49 3.70 1 6 -10 61.19 4.10 1 6 -10 59.39 4.10 -1 6 10 60.89 3.70 1 6 -10 68.69 4.10 -1 6 10 61.99 3.60 1 6 -10 67.89 4.30 0 -6 10 51.49 3.40 0 -6 10 52.09 3.60 0 -6 -10 40.10 2.90 0 -6 10 46.00 3.40 0 -6 10 48.20 3.40 0 -6 10 47.00 3.40 0 -6 -10 45.80 2.70 0 -6 10 48.80 3.60 0 6 -10 48.80 3.50 0 6 10 43.70 2.80 0 6 -10 51.69 3.50 0 6 10 45.20 2.90 0 6 10 46.20 2.90 0 6 -10 47.70 3.30 0 6 -10 49.00 3.50 1 -6 10 23.60 2.70 1 -6 10 24.10 2.50 1 -6 10 22.20 2.40 1 -6 10 24.30 2.40 1 -6 10 21.00 2.60 -1 6 -10 27.20 2.60 -1 6 -10 29.00 2.60 -1 6 -10 24.90 2.50 -1 6 -10 24.50 2.50 1 6 10 24.50 1.70 1 6 10 23.40 1.60 1 6 10 24.00 1.70 2 -6 10 26.40 2.60 2 -6 10 21.50 2.60 2 -6 10 21.00 2.80 2 -6 10 21.10 2.70 2 -6 10 28.80 3.00 -2 6 -10 26.30 2.70 -2 6 -10 23.80 2.60 2 6 10 31.50 2.30 2 6 10 32.60 1.80 -2 6 -10 26.30 2.90 2 6 10 33.50 1.80 -2 6 -10 26.40 2.60 3 -6 10 -2.60 1.10 3 -6 10 -0.70 1.20 3 -6 10 -2.10 1.40 3 -6 10 -3.50 1.10 3 -6 10 -2.30 1.10 -3 6 -10 -2.40 1.10 3 6 10 0.20 1.00 -3 6 -10 -2.40 1.40 3 6 10 1.10 0.40 -3 6 -10 -3.90 1.20 3 6 10 -0.20 1.10 4 -6 10 4.40 1.70 4 -6 10 1.50 1.40 4 -6 10 5.00 1.40 4 -6 10 0.80 1.50 4 -6 10 4.00 1.40 -4 6 -10 2.50 1.20 -4 6 -10 4.00 1.60 4 6 10 4.50 1.30 -4 6 -10 3.50 1.30 -4 6 -10 3.50 1.40 4 6 10 4.70 1.40 5 -6 10 36.80 4.30 5 -6 10 35.50 3.80 5 -6 10 32.70 3.60 5 -6 10 34.90 3.40 5 -6 10 39.10 3.30 5 6 10 38.20 3.40 -5 6 -10 46.60 3.50 5 6 10 37.70 3.30 -5 6 -10 37.30 3.00 -5 6 -10 41.00 3.90 -5 6 -10 42.10 3.30 6 -6 10 34.10 3.20 6 -6 10 34.50 3.20 6 -6 10 36.40 3.90 6 -6 10 39.90 3.50 6 -6 10 35.20 3.30 6 6 10 32.50 2.10 6 6 10 43.70 3.40 -6 6 -10 34.00 3.10 -6 6 -10 39.60 2.80 6 6 10 38.30 3.40 6 6 10 30.30 2.10 -6 6 -10 38.60 3.30 7 -6 10 1.70 1.50 7 -6 10 2.50 1.70 7 -6 10 4.50 1.50 7 -6 10 1.10 1.50 7 6 10 1.20 0.60 -7 6 -10 3.00 1.30 7 6 10 2.10 1.30 7 6 10 2.90 0.70 -7 6 -10 1.50 1.30 -7 6 -10 2.50 1.10 7 6 10 1.50 1.50 8 -6 10 1.50 1.90 8 -6 10 2.80 1.60 8 -6 10 -2.10 1.20 8 -6 10 -0.80 1.70 8 6 10 -0.30 1.50 -8 6 -10 0.80 1.00 8 6 10 0.20 0.70 8 6 10 0.80 2.60 -8 6 -10 -1.10 1.20 8 6 10 -0.90 0.60 -8 6 -10 1.30 1.10 9 -6 10 -2.30 1.40 9 -6 10 0.90 3.00 9 -6 10 0.90 2.20 9 -6 10 2.50 1.80 9 6 10 0.50 0.90 9 6 10 -1.50 1.60 -9 6 -10 2.30 1.30 9 6 10 0.90 1.40 -9 6 -10 -0.60 0.90 -9 6 -10 -0.80 1.30 9 6 10 -0.20 0.80 12 -7 -10 3.30 1.80 -12 -7 10 2.30 1.40 -12 -7 10 1.80 0.90 -12 -7 10 0.30 1.60 12 -7 -10 3.10 1.50 12 -7 -10 1.40 1.80 12 7 -10 4.30 1.60 12 7 -10 1.70 1.80 -12 7 10 1.40 1.80 12 7 -10 1.40 1.50 -12 7 10 3.30 1.80 -11 -7 10 8.10 1.80 -11 -7 10 7.40 1.60 11 -7 -10 8.50 2.00 11 -7 -10 5.40 1.50 -11 -7 10 7.20 1.10 11 -7 -10 8.20 2.00 11 7 -10 4.80 1.60 11 7 -10 7.40 2.00 11 7 -10 9.80 3.40 11 7 -10 8.10 1.90 -11 7 10 7.20 1.90 10 -7 -10 20.20 2.50 10 -7 -10 21.60 2.50 -10 -7 10 17.60 1.90 -10 -7 10 19.40 3.50 10 -7 -10 19.10 2.40 -10 -7 10 17.90 2.20 -10 7 10 21.50 2.60 10 7 -10 15.50 2.20 10 7 -10 18.90 2.20 10 7 -10 17.10 2.50 -10 7 10 17.40 2.30 10 7 -10 26.30 2.90 -9 -7 10 1.50 1.40 9 -7 -10 6.40 1.70 -9 -7 10 5.50 1.00 -9 -7 10 2.10 1.10 9 -7 -10 4.40 1.50 9 -7 -10 4.40 1.50 -9 -7 10 6.80 1.60 9 -7 -10 3.10 1.20 -9 7 10 2.90 1.60 -9 7 10 1.50 1.50 9 7 -10 7.00 1.60 9 7 -10 1.50 1.60 9 7 -10 5.00 1.60 9 7 -10 5.60 1.70 8 -7 -10 1.80 1.00 -8 -7 10 -1.00 1.30 8 -7 -10 2.10 1.30 -8 -7 10 0.50 1.30 -8 -7 10 1.20 1.40 -8 -7 10 -0.40 1.30 8 -7 -10 0.30 1.30 8 -7 -10 -0.50 1.20 -8 -7 10 -1.10 1.30 -8 -7 10 0.80 0.90 8 7 -10 -0.20 1.40 8 7 -10 -0.70 1.30 8 7 -10 -0.30 1.40 -8 7 10 1.70 1.30 -8 7 10 0.60 0.90 8 7 -10 -0.40 1.40 -8 7 10 2.20 1.80 -8 7 10 0.50 1.30 -8 7 10 3.10 1.30 8 7 -10 -0.60 1.30 -7 -7 10 -1.50 1.20 7 -7 -10 -1.30 1.10 7 -7 -10 0.00 1.20 -7 -7 10 -0.60 0.80 7 -7 -10 0.30 1.10 -7 -7 10 -2.40 1.20 7 -7 -10 -0.20 0.80 -7 -7 10 -0.70 1.20 -7 7 10 -0.10 2.00 -7 7 10 0.10 1.50 7 7 -10 -5.00 1.90 -7 7 10 -2.40 2.00 7 7 -10 -2.00 2.00 -7 7 10 0.40 2.10 -7 7 10 -0.80 0.80 7 7 -10 -1.00 1.20 7 7 -10 -2.00 1.40 7 7 -10 -2.30 1.90 6 -7 -10 28.20 2.60 -6 -7 10 30.70 2.90 6 -7 -10 30.80 2.80 6 -7 -10 29.20 2.80 -6 -7 10 25.90 2.90 -6 -7 10 35.70 4.00 -6 -7 10 32.90 3.00 6 7 -10 26.90 2.70 -6 7 10 30.10 2.90 -6 7 10 32.40 3.60 -6 7 10 29.80 2.70 6 7 -10 29.10 2.90 6 7 -10 34.00 3.10 -6 7 10 27.70 2.90 6 7 -10 33.60 3.20 -6 7 10 26.60 2.20 6 7 -10 32.30 3.00 -5 -7 10 135.39 7.90 -5 -7 10 143.69 7.90 -5 -7 10 133.29 7.70 5 -7 -10 134.89 7.80 -5 -7 10 136.59 8.00 5 -7 -10 117.69 7.70 -5 -7 10 144.39 7.90 5 -7 -10 143.59 7.70 -5 -7 10 140.79 7.90 5 7 -10 143.19 7.90 -5 7 10 136.59 8.30 5 7 -10 144.19 8.00 5 7 -10 146.69 8.10 -5 7 10 132.49 7.80 -5 7 10 139.29 7.90 -5 7 10 128.99 7.40 -5 7 10 132.19 7.80 5 7 -10 134.79 7.90 4 -7 -10 148.39 8.50 -4 -7 10 155.18 8.50 -4 -7 10 156.78 8.70 -4 -7 10 156.78 8.60 -4 -7 10 149.79 8.70 -4 -7 10 153.78 8.70 4 -7 -10 150.68 8.30 4 -7 -10 143.79 8.50 -4 -7 10 156.78 8.80 4 -7 -10 149.19 8.30 -4 7 10 159.28 9.00 -4 7 10 150.18 8.50 -4 7 10 144.39 8.50 -4 7 10 149.39 8.10 -4 7 10 141.29 8.50 4 7 -10 157.98 8.70 4 7 -10 160.38 8.80 4 7 -10 161.78 8.70 -3 -7 10 12.80 1.90 -3 -7 10 13.20 1.80 -3 -7 10 14.80 1.60 3 -7 -10 12.70 1.40 3 -7 -10 13.30 1.20 3 -7 -10 10.70 1.30 -3 -7 10 14.10 1.90 -3 -7 10 16.10 1.90 3 -7 -10 12.00 1.40 -3 -7 10 11.80 1.70 -3 7 10 11.60 1.50 3 7 -10 15.30 1.90 3 7 -10 14.00 1.80 3 7 -10 14.20 1.80 -3 7 10 14.50 1.30 -3 7 10 14.70 1.60 -3 7 10 15.60 1.60 -2 -7 10 144.79 8.40 -2 -7 10 143.59 8.50 -2 -7 10 147.29 8.50 -2 -7 10 148.29 8.50 -2 -7 10 152.18 8.50 -2 -7 10 150.18 8.40 2 -7 -10 146.69 8.10 2 -7 -10 148.69 8.20 2 7 -10 152.88 8.60 -2 7 10 151.88 7.90 -2 7 10 142.99 8.20 2 7 -10 166.38 8.60 2 7 -10 147.59 8.40 2 7 -10 151.38 8.50 -2 7 10 150.08 8.30 -2 7 10 155.48 8.20 -1 -7 10 6.90 1.50 -1 -7 10 9.90 1.40 -1 -7 10 8.10 1.50 -1 -7 10 5.30 1.40 -1 -7 10 7.10 1.50 -1 -7 10 8.20 1.50 1 -7 -10 8.40 1.00 -1 7 10 8.30 1.10 -1 7 10 7.20 1.10 -1 7 10 7.10 1.10 -1 7 10 8.30 1.00 1 7 -10 11.80 1.70 1 7 -10 11.20 1.70 1 7 -10 7.30 1.40 1 7 -10 8.60 1.60 0 -7 10 11.70 1.60 0 -7 10 19.60 2.00 0 -7 10 18.90 1.90 0 -7 -10 18.70 1.70 0 -7 -10 13.90 1.20 0 -7 10 14.50 1.90 0 -7 10 19.20 2.00 0 7 10 14.60 1.40 0 7 -10 19.00 1.90 0 7 -10 18.20 2.20 0 7 10 15.10 1.50 0 7 10 12.90 1.50 0 7 10 13.60 1.40 0 7 10 14.90 1.40 1 -7 10 64.09 4.30 1 -7 10 64.49 4.60 1 -7 10 67.29 4.40 1 -7 10 64.29 4.30 1 -7 10 58.19 4.70 -1 7 -10 68.79 4.40 -1 7 -10 74.39 4.50 1 7 10 65.19 3.60 1 7 10 64.09 3.70 -1 7 -10 64.89 4.40 1 7 10 66.79 3.70 1 7 10 63.79 3.60 -1 7 -10 69.49 4.40 1 7 10 65.79 3.90 2 -7 10 3.10 1.30 2 -7 10 2.90 1.50 2 -7 10 1.50 1.20 2 -7 10 3.70 1.40 2 -7 10 1.30 1.30 -2 7 -10 3.60 1.30 2 7 10 2.70 1.00 -2 7 -10 1.00 1.40 -2 7 -10 2.20 1.30 2 7 10 3.80 0.60 2 7 10 3.60 0.60 -2 7 -10 1.60 1.30 3 -7 10 39.20 3.20 3 -7 10 42.00 3.10 3 -7 10 36.90 3.20 3 -7 10 42.40 3.30 3 -7 10 39.30 3.70 -3 7 -10 42.00 3.20 -3 7 -10 41.50 3.20 -3 7 -10 40.30 3.60 3 7 10 38.10 2.20 3 7 10 42.20 2.90 3 7 10 38.00 2.20 3 7 10 36.10 3.30 -3 7 -10 39.20 3.40 4 -7 10 53.39 4.00 4 -7 10 55.09 4.00 4 -7 10 50.59 4.10 -4 7 -10 53.39 4.00 4 7 10 48.90 3.90 4 7 10 50.49 3.60 -4 7 -10 57.89 3.90 -4 7 -10 55.19 3.80 5 -7 10 1.00 1.40 5 -7 10 2.00 1.40 5 -7 10 2.30 1.30 5 -7 10 -0.40 1.50 5 -7 10 2.40 1.40 -5 7 -10 5.00 1.70 -5 7 -10 2.90 1.40 5 7 10 1.50 1.20 5 7 10 3.00 1.30 -5 7 -10 0.40 1.20 -5 7 -10 1.30 1.40 -5 7 -10 0.00 1.20 6 -7 10 8.90 1.80 6 -7 10 7.90 1.70 6 -7 10 6.90 1.70 6 -7 10 6.80 1.90 6 7 10 8.10 1.70 -6 7 -10 7.60 1.80 -6 7 -10 6.80 1.50 6 7 10 6.80 1.50 -6 7 -10 6.00 1.40 7 -7 10 1.20 1.60 7 -7 10 2.30 1.50 7 -7 10 1.60 1.70 7 -7 10 3.60 1.50 -7 7 -10 2.60 1.50 7 7 10 0.50 1.40 7 7 10 2.90 1.30 -7 7 -10 2.90 1.40 -7 7 -10 0.50 1.20 8 -7 10 7.80 1.70 8 -7 10 5.70 2.20 8 -7 10 5.20 1.80 8 -7 10 4.50 2.00 -8 7 -10 8.00 1.50 8 7 10 3.30 0.80 8 7 10 3.80 0.80 -8 7 -10 3.20 1.50 8 7 10 5.90 1.80 -8 7 -10 4.10 1.30 8 7 10 4.00 1.50 9 -7 10 1.50 1.50 9 -7 10 -1.20 1.90 9 -7 10 1.50 1.50 9 -7 10 3.90 2.00 9 7 10 -1.40 1.30 -9 7 -10 -0.10 1.30 -9 7 -10 3.70 1.30 9 7 10 0.40 1.60 9 7 10 -0.60 0.70 -9 7 -10 3.30 1.20 -11 -8 10 1.40 2.00 11 -8 -10 3.30 1.90 -11 -8 10 5.30 1.70 11 -8 -10 -1.00 1.70 11 -8 -10 2.10 1.40 -11 8 10 6.20 2.10 11 8 -10 4.40 1.70 11 8 -10 2.50 1.90 -11 8 10 3.60 2.80 11 8 -10 4.80 2.60 11 8 -10 6.10 2.00 10 -8 -10 10.20 2.00 10 -8 -10 7.70 1.50 10 -8 -10 11.90 2.10 -10 -8 10 11.20 1.30 -10 -8 10 10.20 1.20 -10 -8 10 10.20 1.90 10 8 -10 11.80 1.90 -10 8 10 11.70 2.10 -10 8 10 8.80 1.90 10 8 -10 10.20 2.20 10 8 -10 11.70 1.90 10 8 -10 12.50 2.10 9 -8 -10 4.30 1.80 -9 -8 10 4.50 0.80 9 -8 -10 4.20 1.60 -9 -8 10 4.70 1.50 9 -8 -10 5.30 1.10 -9 -8 10 5.50 0.80 -9 -8 10 6.30 1.70 9 8 -10 4.30 1.70 9 8 -10 2.40 1.50 -9 8 10 5.40 1.70 9 8 -10 3.80 1.70 9 8 -10 4.00 1.60 -9 8 10 4.00 1.60 -9 8 10 0.40 1.70 -8 -8 10 2.90 1.60 -8 -8 10 2.80 1.40 -8 -8 10 3.10 0.80 -8 -8 10 0.50 1.20 8 -8 -10 0.80 1.60 -8 -8 10 3.20 0.80 8 -8 -10 1.60 1.40 -8 -8 10 4.70 1.60 8 -8 -10 2.60 0.90 -8 8 10 1.30 1.30 8 8 -10 2.50 1.30 -8 8 10 2.50 1.60 8 8 -10 3.70 1.50 8 8 -10 2.40 1.60 -8 8 10 2.90 1.50 8 8 -10 2.80 1.50 -7 -8 10 49.60 3.80 7 -8 -10 51.59 3.90 -7 -8 10 55.09 3.90 -7 -8 10 51.49 4.10 7 -8 -10 54.19 3.40 7 -8 -10 53.99 3.70 -7 -8 10 50.19 3.90 -7 -8 10 47.30 3.20 -7 -8 10 49.10 3.20 7 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1.70 -3 6 21 0.40 1.10 6 0 -22 8.60 1.40 6 0 -22 5.90 1.40 -6 0 22 7.00 1.80 -6 0 22 6.40 2.00 -5 0 22 -0.30 1.40 -5 0 22 -2.20 1.30 5 0 -22 1.00 1.00 5 0 -22 0.70 1.40 5 0 -22 -1.70 1.00 -4 0 22 34.00 3.20 4 0 -22 24.70 2.90 4 0 -22 25.70 2.30 4 0 -22 27.30 2.50 -4 0 22 27.20 3.00 -4 0 22 33.80 4.10 -4 0 22 26.50 3.20 -3 0 22 0.90 1.50 -3 0 22 -0.20 1.30 3 0 -22 0.30 0.60 3 0 -22 2.10 1.30 -3 0 22 -2.10 1.20 -3 0 22 -0.20 1.80 -2 0 22 4.10 1.50 -2 0 22 4.10 1.60 -2 0 22 5.50 1.60 2 0 -22 3.90 1.40 -2 0 22 2.10 1.80 -1 0 22 1.30 1.90 1 0 -22 1.80 1.80 -1 0 22 2.90 1.50 -1 0 22 0.40 1.20 -1 0 22 3.40 1.40 -6 -1 22 12.80 2.30 -6 -1 22 10.20 2.10 6 -1 -22 8.50 1.70 -6 1 22 11.10 2.40 6 1 -22 10.10 2.00 6 1 -22 9.10 1.70 -6 1 22 12.80 2.00 -6 1 22 12.50 1.90 5 -1 -22 -0.20 0.90 5 -1 -22 1.20 1.30 -5 -1 22 0.70 1.40 5 -1 -22 -0.20 0.90 -5 -1 22 -0.10 1.50 -5 1 22 0.40 2.00 5 1 -22 2.60 1.60 -5 1 22 -1.50 1.30 5 1 -22 -0.50 1.10 -5 1 22 -2.50 1.50 4 -1 -22 3.60 0.80 4 -1 -22 3.80 1.10 -4 -1 22 0.50 1.90 -4 -1 22 4.60 1.60 -4 -1 22 3.50 1.80 4 -1 -22 0.60 1.30 4 1 -22 4.10 1.20 4 1 -22 3.90 1.00 -4 1 22 3.30 1.60 -4 1 22 3.50 1.40 -4 1 22 2.10 1.40 4 1 -22 4.80 1.60 -3 -1 22 -0.90 1.30 -3 -1 22 2.20 1.80 3 -1 -22 0.90 1.20 -3 -1 22 2.10 1.70 -3 -1 22 0.10 1.40 3 1 -22 0.60 1.30 -3 1 22 -0.20 1.40 -3 1 22 2.90 1.50 3 1 -22 -1.30 0.90 -3 1 22 0.70 1.30 -3 1 22 1.30 1.90 -2 -1 22 4.00 1.60 -2 -1 22 -0.20 1.80 -2 -1 22 5.70 1.50 -2 -1 22 2.10 1.40 -2 1 22 5.20 2.10 -2 1 22 4.80 1.60 -2 1 22 2.30 1.30 2 1 -22 1.50 1.30 -1 -1 22 5.60 1.50 -1 -1 22 5.50 1.70 -1 -1 22 1.70 1.30 1 -1 -22 5.50 1.20 -1 -1 22 4.10 1.90 -1 1 22 6.30 1.60 -1 1 22 3.90 1.40 -1 1 22 4.00 1.90 1 1 -22 5.40 1.40 6 -2 -22 11.60 1.50 6 2 -22 10.60 1.80 -5 -2 22 16.30 2.40 5 -2 -22 14.50 2.00 -5 -2 22 20.10 2.50 5 -2 -22 17.80 1.80 -5 -2 22 12.40 2.90 5 -2 -22 20.70 2.40 -5 2 22 23.80 2.70 5 2 -22 13.70 1.90 5 2 -22 23.30 2.60 5 2 -22 18.70 2.40 4 -2 -22 10.80 1.70 -4 -2 22 13.90 2.80 -4 -2 22 10.40 1.90 -4 -2 22 11.40 2.00 4 2 -22 11.30 1.90 4 2 -22 11.30 2.40 -4 2 22 14.40 1.90 -4 2 22 11.60 1.90 -4 2 22 11.30 2.00 -3 -2 22 0.20 1.40 3 -2 -22 1.10 1.20 -3 -2 22 -1.50 1.60 -3 2 22 0.70 1.30 -3 2 22 2.90 1.90 -3 2 22 1.40 1.40 3 2 -22 -1.90 1.40 3 2 -22 -0.20 1.00 3 2 -22 0.90 0.90 -2 -2 22 1.30 1.40 2 -2 -22 1.10 1.10 -2 -2 22 4.20 1.40 -2 -2 22 0.70 1.80 -2 -2 22 1.70 2.10 -2 2 22 1.30 1.40 2 2 -22 0.30 0.90 -2 2 22 1.60 1.40 2 2 -22 -0.10 1.30 -2 2 22 0.10 1.70 -1 -2 22 4.30 1.40 -5 -3 22 0.70 1.50 5 -3 -22 0.80 1.20 -5 -3 22 2.60 2.10 5 3 -22 3.40 1.70 5 3 -22 2.20 1.40 -5 3 22 5.70 1.50 -5 3 22 5.90 1.40 -4 -3 22 1.80 1.50 4 -3 -22 4.60 1.40 -4 -3 22 0.70 1.90 -4 -3 22 3.00 1.70 -4 3 22 3.30 1.40 4 3 -22 3.10 1.30 -4 3 22 3.50 1.30 4 3 -22 3.50 2.00 4 3 -22 4.30 1.30 -3 -3 22 14.70 2.10 -3 -3 22 12.40 2.00 -3 -3 22 12.80 2.50 -3 -3 22 16.30 2.80 3 -3 -22 12.70 1.60 -3 3 22 11.30 2.00 -3 3 22 11.30 2.70 -3 3 22 11.30 2.00 3 3 -22 13.00 2.10 -2 -3 22 6.10 2.20 -2 -3 22 6.40 1.90 2 -3 -22 5.00 1.20 -2 -3 22 3.20 1.50 2 3 -22 4.20 1.60 2 3 -22 4.40 1.20 2 3 -22 4.50 1.10 -2 3 22 3.50 1.20 -2 3 22 7.10 2.10 -2 3 22 6.80 1.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 14572 _shelx_res_file ; TITL SM9_a.res in P2(1)/n shelx.res created by SHELXL-2018/3 at 11:14:32 on 03-Sep-2022 CELL 0.71073 10.1420 12.0970 16.2218 90.000 104.846 90.000 ZERR 4.00 0.0010 0.0010 0.0015 0.000 0.004 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O S UNIT 100 64 8 8 4 MERG 2 OMIT -3.00 54.00 OMIT -9 1 4 OMIT 0 1 2 OMIT 1 1 1 OMIT 1 0 1 OMIT -1 1 1 OMIT 0 0 2 OMIT 1 1 0 HTAB C2 O2 HTAB C11 O1 EQIV $1 x-1/2, -y+1/2, z+1/2 HTAB C21 N2_$1 FMAP 2 PLAN 20 SIZE 0.250 0.350 0.400 ACTA BOND $H CONF L.S. 4 TEMP 23.00 WGHT 0.046500 2.555200 FVAR 0.45880 C1 1 0.865919 0.195068 0.624732 11.00000 0.04080 0.03777 = 0.04091 0.00036 0.00695 0.00118 C2 1 0.857624 0.128116 0.693022 11.00000 0.05323 0.05335 = 0.05020 0.00836 0.01561 0.00055 AFIX 43 H2 2 0.796204 0.142990 0.725444 11.00000 -1.20000 AFIX 0 C3 1 0.944737 0.038691 0.710362 11.00000 0.06286 0.05174 = 0.05939 0.01737 0.00895 -0.00126 AFIX 43 H3 2 0.941923 -0.007334 0.755800 11.00000 -1.20000 AFIX 0 C4 1 1.036409 0.015077 0.662321 11.00000 0.05585 0.04415 = 0.06713 0.01077 0.00559 0.00847 AFIX 43 H4 2 1.094393 -0.045445 0.676287 11.00000 -1.20000 AFIX 0 C5 1 1.041832 0.080684 0.594285 11.00000 0.04740 0.04650 = 0.05833 0.00226 0.00967 0.01192 AFIX 43 H5 2 1.102062 0.064446 0.561328 11.00000 -1.20000 AFIX 0 C6 1 0.956028 0.171655 0.575422 11.00000 0.03798 0.03766 = 0.03919 -0.00055 0.00555 0.00190 C7 1 0.941495 0.257613 0.511997 11.00000 0.03231 0.03782 = 0.03856 -0.00320 0.00611 0.00258 C8 1 1.008447 0.276946 0.449579 11.00000 0.03751 0.04369 = 0.04923 -0.00181 0.01559 0.01078 AFIX 43 H8 2 1.075496 0.228451 0.441961 11.00000 -1.20000 AFIX 0 C9 1 0.974418 0.370479 0.397692 11.00000 0.03580 0.04515 = 0.03856 -0.00291 0.01306 0.00294 C10 1 0.873637 0.445627 0.409031 11.00000 0.03280 0.03369 = 0.03436 -0.00525 0.00637 -0.00221 C11 1 0.806942 0.426150 0.473728 11.00000 0.03738 0.03386 = 0.03930 -0.00360 0.01289 0.00301 AFIX 43 H11 2 0.741028 0.474851 0.482689 11.00000 -1.20000 AFIX 0 C12 1 0.841816 0.332967 0.523535 11.00000 0.03246 0.03635 = 0.03361 -0.00383 0.00928 0.00109 C13 1 0.845904 0.540028 0.352126 11.00000 0.03602 0.03788 = 0.03610 -0.00410 0.00607 -0.00520 C14 1 0.750496 0.622820 0.356083 11.00000 0.04768 0.04283 = 0.04746 0.00125 0.01379 0.00126 AFIX 43 H14 2 0.701230 0.617974 0.397050 11.00000 -1.20000 AFIX 0 C15 1 0.728529 0.710860 0.300588 11.00000 0.05390 0.04196 = 0.06492 0.00582 0.01138 0.00358 AFIX 43 H15 2 0.664791 0.764658 0.304288 11.00000 -1.20000 AFIX 0 C16 1 0.801293 0.719701 0.238972 11.00000 0.05648 0.04818 = 0.06097 0.01491 0.00958 -0.00617 AFIX 43 H16 2 0.786655 0.779570 0.201767 11.00000 -1.20000 AFIX 0 C17 1 0.894143 0.640492 0.233158 11.00000 0.04981 0.05840 = 0.05364 0.00943 0.01691 -0.00978 AFIX 43 H17 2 0.941880 0.646462 0.191462 11.00000 -1.20000 AFIX 0 C18 1 0.918651 0.550085 0.289232 11.00000 0.04019 0.04642 = 0.04368 0.00088 0.01176 -0.00499 C19 1 1.040844 0.391044 0.331030 11.00000 0.04803 0.06061 = 0.05537 0.00398 0.02634 0.01234 AFIX 43 H19 2 1.107016 0.340809 0.324773 11.00000 -1.20000 AFIX 0 C20 1 0.525751 0.247592 0.549430 11.00000 0.03779 0.06198 = 0.04319 -0.00151 0.01739 0.01351 C21 1 0.489176 0.149391 0.581736 11.00000 0.04415 0.05807 = 0.06843 -0.00367 0.02105 0.00824 AFIX 43 H21 2 0.529794 0.128664 0.637693 11.00000 -1.20000 AFIX 0 C22 1 0.391570 0.082551 0.529812 11.00000 0.05130 0.07047 = 0.11110 -0.02025 0.02434 -0.00214 AFIX 43 H22 2 0.364572 0.017708 0.551609 11.00000 -1.20000 AFIX 0 C23 1 0.334651 0.110959 0.446968 11.00000 0.04147 0.11633 = 0.11173 -0.04836 0.00791 0.00972 AFIX 43 H23 2 0.270298 0.064956 0.412217 11.00000 -1.20000 AFIX 0 C24 1 0.372711 0.208157 0.414739 11.00000 0.04865 0.14789 = 0.05903 -0.02123 -0.00140 0.03156 AFIX 43 H24 2 0.333913 0.226625 0.358053 11.00000 -1.20000 AFIX 0 C25 1 0.467724 0.278796 0.465302 11.00000 0.04702 0.09773 = 0.05268 0.00525 0.01413 0.02024 AFIX 43 H25 2 0.491861 0.344837 0.443700 11.00000 -1.20000 AFIX 0 N1 3 0.795231 0.295822 0.594624 11.00000 0.04203 0.03909 = 0.04147 0.00245 0.01546 0.00613 N2 3 1.015931 0.474141 0.278797 11.00000 0.05440 0.06678 = 0.05517 0.00677 0.02835 0.00318 O1 4 0.623937 0.444277 0.587370 11.00000 0.07721 0.04672 = 0.07263 0.00801 0.04394 0.02027 O2 4 0.660373 0.303627 0.701295 11.00000 0.06958 0.06262 = 0.03961 -0.00387 0.02485 0.00561 S1 5 0.648936 0.332474 0.614902 11.00000 0.05080 0.04552 = 0.04185 0.00024 0.02302 0.00906 HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00 REM SM9_a.res in P2(1)/n REM wR2 = 0.1612, GooF = S = 1.127, Restrained GooF = 1.127 for all data REM R1 = 0.0537 for 3488 Fo > 4sig(Fo) and 0.0680 for all 4185 data REM 271 parameters refined using 0 restraints END WGHT 0.0463 2.5552 REM Highest difference peak 0.324, deepest hole -0.442, 1-sigma level 0.060 Q1 1 1.1603 0.3645 0.3313 11.00000 0.05 0.32 Q2 1 0.5543 0.2839 0.5790 11.00000 0.05 0.27 Q3 1 0.5189 0.1375 0.6567 11.00000 0.05 0.26 Q4 1 0.6291 0.3353 0.5421 11.00000 0.05 0.24 Q5 1 0.8592 0.5326 0.3105 11.00000 0.05 0.24 Q6 1 0.8971 0.5615 0.3342 11.00000 0.05 0.23 Q7 1 1.0023 0.2855 0.5055 11.00000 0.05 0.23 Q8 1 1.0056 0.0249 0.6074 11.00000 0.05 0.22 Q9 1 0.7664 0.2973 0.5382 11.00000 0.05 0.22 Q10 1 0.7364 0.6232 0.1588 11.00000 0.05 0.22 Q11 1 0.6812 0.3382 0.6797 11.00000 0.05 0.22 Q12 1 0.8803 0.5237 0.3976 11.00000 0.05 0.22 Q13 1 0.8910 0.1769 0.5886 11.00000 0.05 0.21 Q14 1 0.8082 0.4220 0.4162 11.00000 0.05 0.21 Q15 1 0.8217 0.6014 0.3598 11.00000 0.05 0.21 Q16 1 0.5138 0.2600 0.5142 11.00000 0.05 0.21 Q17 1 0.9231 0.2470 0.4592 11.00000 0.05 0.20 Q18 1 0.9397 0.4194 0.4132 11.00000 0.05 0.20 Q19 1 0.8212 0.1362 0.6297 11.00000 0.05 0.20 Q20 1 0.5626 0.3203 0.6855 11.00000 0.05 0.20 ; _shelx_res_checksum 36252 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.8659(3) 0.1951(2) 0.62473(17) 0.0405(6) Uani d 1 . . C C2 0.8576(3) 0.1281(3) 0.69302(19) 0.0518(7) Uani d 1 . . H H2 0.796204 0.142990 0.725444 0.062 Uiso calc 1 . . C C3 0.9447(3) 0.0387(3) 0.7104(2) 0.0592(8) Uani d 1 . . H H3 0.941923 -0.007334 0.755800 0.071 Uiso calc 1 . . C C4 1.0364(3) 0.0151(3) 0.6623(2) 0.0576(8) Uani d 1 . . H H4 1.094393 -0.045445 0.676287 0.069 Uiso calc 1 . . C C5 1.0418(3) 0.0807(2) 0.5943(2) 0.0515(7) Uani d 1 . . H H5 1.102062 0.064446 0.561328 0.062 Uiso calc 1 . . C C6 0.9560(3) 0.1717(2) 0.57542(16) 0.0391(5) Uani d 1 . . C C7 0.9415(2) 0.2576(2) 0.51200(16) 0.0368(5) Uani d 1 . . C C8 1.0084(3) 0.2769(2) 0.44958(17) 0.0427(6) Uani d 1 . . H H8 1.075496 0.228451 0.441961 0.051 Uiso calc 1 . . C C9 0.9744(3) 0.3705(2) 0.39769(16) 0.0392(6) Uani d 1 . . C C10 0.8736(2) 0.4456(2) 0.40903(15) 0.0340(5) Uani d 1 . . C C11 0.8069(3) 0.4262(2) 0.47373(15) 0.0363(5) Uani d 1 . . H H11 0.741028 0.474851 0.482689 0.044 Uiso calc 1 . . C C12 0.8418(2) 0.3330(2) 0.52353(15) 0.0340(5) Uani d 1 . . C C13 0.8459(2) 0.5400(2) 0.35213(15) 0.0372(5) Uani d 1 . . C C14 0.7505(3) 0.6228(2) 0.35608(18) 0.0457(6) Uani d 1 . . H H14 0.701230 0.617974 0.397050 0.055 Uiso calc 1 . . C C15 0.7285(3) 0.7109(3) 0.3006(2) 0.0543(7) Uani d 1 . . H H15 0.664791 0.764658 0.304288 0.065 Uiso calc 1 . . C C16 0.8013(3) 0.7197(3) 0.2390(2) 0.0562(8) Uani d 1 . . H H16 0.786655 0.779570 0.201767 0.067 Uiso calc 1 . . C C17 0.8941(3) 0.6405(3) 0.2332(2) 0.0533(7) Uani d 1 . . H H17 0.941880 0.646462 0.191462 0.064 Uiso calc 1 . . C C18 0.9187(3) 0.5501(2) 0.28923(17) 0.0432(6) Uani d 1 . . C C19 1.0408(3) 0.3910(3) 0.33103(19) 0.0523(7) Uani d 1 . . H H19 1.107016 0.340809 0.324773 0.063 Uiso calc 1 . . C C20 0.5258(3) 0.2476(3) 0.54943(17) 0.0464(6) Uani d 1 . . C C21 0.4892(3) 0.1494(3) 0.5817(2) 0.0557(8) Uani d 1 . . H H21 0.529794 0.128664 0.637693 0.067 Uiso calc 1 . . C C22 0.3916(4) 0.0826(3) 0.5298(3) 0.0770(11) Uani d 1 . . H H22 0.364572 0.017708 0.551609 0.092 Uiso calc 1 . . C C23 0.3347(4) 0.1110(5) 0.4470(3) 0.0920(16) Uani d 1 . . H H23 0.270298 0.064956 0.412217 0.110 Uiso calc 1 . . C C24 0.3727(4) 0.2082(5) 0.4147(3) 0.0880(15) Uani d 1 . . H H24 0.333913 0.226625 0.358053 0.106 Uiso calc 1 . . C C25 0.4677(3) 0.2788(4) 0.4653(2) 0.0656(9) Uani d 1 . . H H25 0.491861 0.344837 0.443700 0.079 Uiso calc 1 . . N N1 0.7952(2) 0.29582(18) 0.59462(14) 0.0400(5) Uani d 1 . . N N2 1.0159(3) 0.4741(2) 0.27880(17) 0.0562(7) Uani d 1 . . O O1 0.6239(2) 0.44428(18) 0.58737(15) 0.0610(6) Uani d 1 . . O O2 0.6604(2) 0.30363(18) 0.70130(12) 0.0553(5) Uani d 1 . . S S1 0.64894(7) 0.33247(6) 0.61490(4) 0.0440(2) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0408(13) 0.0378(13) 0.0409(13) 0.0012(11) 0.0070(11) 0.0004(10) C2 0.0532(17) 0.0534(17) 0.0502(16) 0.0005(14) 0.0156(13) 0.0084(13) C3 0.0629(19) 0.0517(18) 0.0594(18) -0.0013(15) 0.0089(15) 0.0174(15) C4 0.0558(18) 0.0442(16) 0.067(2) 0.0085(14) 0.0056(15) 0.0108(14) C5 0.0474(16) 0.0465(16) 0.0583(17) 0.0119(13) 0.0097(13) 0.0023(13) C6 0.0380(13) 0.0377(13) 0.0392(13) 0.0019(10) 0.0056(10) -0.0006(10) C7 0.0323(12) 0.0378(13) 0.0386(12) 0.0026(10) 0.0061(10) -0.0032(10) C8 0.0375(13) 0.0437(14) 0.0492(15) 0.0108(11) 0.0156(11) -0.0018(11) C9 0.0358(13) 0.0451(14) 0.0386(13) 0.0029(11) 0.0131(10) -0.0029(11) C10 0.0328(11) 0.0337(12) 0.0344(12) -0.0022(9) 0.0064(9) -0.0052(9) C11 0.0374(12) 0.0339(12) 0.0393(13) 0.0030(10) 0.0129(10) -0.0036(10) C12 0.0325(11) 0.0363(12) 0.0336(11) 0.0011(10) 0.0093(9) -0.0038(9) C13 0.0360(12) 0.0379(13) 0.0361(12) -0.0052(10) 0.0061(10) -0.0041(10) C14 0.0477(15) 0.0428(14) 0.0475(15) 0.0013(12) 0.0138(12) 0.0013(12) C15 0.0539(17) 0.0420(15) 0.0649(19) 0.0036(13) 0.0114(14) 0.0058(14) C16 0.0565(18) 0.0482(17) 0.0610(19) -0.0062(14) 0.0096(14) 0.0149(14) C17 0.0498(16) 0.0584(18) 0.0536(17) -0.0098(14) 0.0169(13) 0.0094(14) C18 0.0402(14) 0.0464(15) 0.0437(14) -0.0050(11) 0.0118(11) 0.0009(11) C19 0.0480(16) 0.0606(18) 0.0554(17) 0.0123(14) 0.0263(13) 0.0040(14) C20 0.0378(13) 0.0620(18) 0.0432(14) 0.0135(12) 0.0174(11) -0.0015(13) C21 0.0441(16) 0.0581(18) 0.068(2) 0.0082(14) 0.0211(14) -0.0037(15) C22 0.051(2) 0.070(2) 0.111(3) -0.0021(17) 0.024(2) -0.020(2) C23 0.0415(19) 0.116(4) 0.112(4) 0.010(2) 0.008(2) -0.048(3) C24 0.049(2) 0.148(5) 0.059(2) 0.032(3) -0.0014(16) -0.021(3) C25 0.0470(17) 0.098(3) 0.0527(18) 0.0202(18) 0.0141(14) 0.0052(18) N1 0.0420(12) 0.0391(11) 0.0415(11) 0.0061(9) 0.0155(9) 0.0025(9) N2 0.0544(15) 0.0668(17) 0.0552(15) 0.0032(13) 0.0283(12) 0.0068(13) O1 0.0772(15) 0.0467(12) 0.0726(14) 0.0203(11) 0.0439(12) 0.0080(10) O2 0.0696(14) 0.0626(13) 0.0396(10) 0.0056(11) 0.0249(10) -0.0039(9) S1 0.0508(4) 0.0455(4) 0.0419(4) 0.0091(3) 0.0230(3) 0.0002(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 C1 C2 . . 121.5(3) ? C6 C1 N1 . . 108.8(2) ? C2 C1 N1 . . 129.7(3) ? C3 C2 C1 . . 116.9(3) ? C3 C2 H2 . . 121.6 ? C1 C2 H2 . . 121.6 ? C2 C3 C4 . . 122.2(3) ? C2 C3 H3 . . 118.9 ? C4 C3 H3 . . 118.9 ? C5 C4 C3 . . 120.2(3) ? C5 C4 H4 . . 119.9 ? C3 C4 H4 . . 119.9 ? C4 C5 C6 . . 118.9(3) ? C4 C5 H5 . . 120.5 ? C6 C5 H5 . . 120.5 ? C5 C6 C1 . . 120.2(3) ? C5 C6 C7 . . 132.2(3) ? C1 C6 C7 . . 107.5(2) ? C8 C7 C12 . . 119.6(2) ? C8 C7 C6 . . 131.9(2) ? C12 C7 C6 . . 108.5(2) ? C7 C8 C9 . . 119.2(2) ? C7 C8 H8 . . 120.4 ? C9 C8 H8 . . 120.4 ? C8 C9 C10 . . 121.1(2) ? C8 C9 C19 . . 120.2(2) ? C10 C9 C19 . . 118.8(2) ? C11 C10 C9 . . 119.4(2) ? C11 C10 C13 . . 123.7(2) ? C9 C10 C13 . . 116.9(2) ? C12 C11 C10 . . 118.3(2) ? C12 C11 H11 . . 120.9 ? C10 C11 H11 . . 120.9 ? C11 C12 C7 . . 122.4(2) ? C11 C12 N1 . . 130.0(2) ? C7 C12 N1 . . 107.5(2) ? C14 C13 C18 . . 117.8(2) ? C14 C13 C10 . . 123.8(2) ? C18 C13 C10 . . 118.5(2) ? C15 C14 C13 . . 121.3(3) ? C15 C14 H14 . . 119.3 ? C13 C14 H14 . . 119.3 ? C14 C15 C16 . . 120.2(3) ? C14 C15 H15 . . 119.9 ? C16 C15 H15 . . 119.9 ? C17 C16 C15 . . 119.9(3) ? C17 C16 H16 . . 120.0 ? C15 C16 H16 . . 120.0 ? C16 C17 C18 . . 120.9(3) ? C16 C17 H17 . . 119.5 ? C18 C17 H17 . . 119.5 ? N2 C18 C17 . . 116.7(3) ? N2 C18 C13 . . 123.4(2) ? C17 C18 C13 . . 119.9(3) ? N2 C19 C9 . . 125.2(3) ? N2 C19 H19 . . 117.4 ? C9 C19 H19 . . 117.4 ? C21 C20 C25 . . 121.0(3) ? C21 C20 S1 . . 119.5(2) ? C25 C20 S1 . . 119.5(3) ? C22 C21 C20 . . 119.3(4) ? C22 C21 H21 . . 120.4 ? C20 C21 H21 . . 120.4 ? C23 C22 C21 . . 120.6(4) ? C23 C22 H22 . . 119.7 ? C21 C22 H22 . . 119.7 ? C22 C23 C24 . . 119.9(4) ? C22 C23 H23 . . 120.0 ? C24 C23 H23 . . 120.0 ? C23 C24 C25 . . 121.3(4) ? C23 C24 H24 . . 119.4 ? C25 C24 H24 . . 119.4 ? C24 C25 C20 . . 117.9(4) ? C24 C25 H25 . . 121.1 ? C20 C25 H25 . . 121.1 ? C12 N1 C1 . . 107.6(2) ? C12 N1 S1 . . 125.03(17) ? C1 N1 S1 . . 123.60(18) ? C19 N2 C18 . . 117.3(2) ? O2 S1 O1 . . 120.34(13) ? O2 S1 N1 . . 106.19(12) ? O1 S1 N1 . . 106.70(12) ? O2 S1 C20 . . 108.65(14) ? O1 S1 C20 . . 108.92(15) ? N1 S1 C20 . . 104.97(12) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 C6 . 1.389(4) ? C1 C2 . 1.392(4) ? C1 N1 . 1.435(3) ? C2 C3 . 1.379(4) ? C2 H2 . 0.9300 ? C3 C4 . 1.387(5) ? C3 H3 . 0.9300 ? C4 C5 . 1.372(4) ? C4 H4 . 0.9300 ? C5 C6 . 1.388(4) ? C5 H5 . 0.9300 ? C6 C7 . 1.444(4) ? C7 C8 . 1.376(4) ? C7 C12 . 1.409(3) ? C8 C9 . 1.400(4) ? C8 H8 . 0.9300 ? C9 C10 . 1.415(3) ? C9 C19 . 1.435(4) ? C10 C11 . 1.407(3) ? C10 C13 . 1.450(3) ? C11 C12 . 1.379(3) ? C11 H11 . 0.9300 ? C12 N1 . 1.426(3) ? C13 C14 . 1.405(4) ? C13 C18 . 1.409(4) ? C14 C15 . 1.375(4) ? C14 H14 . 0.9300 ? C15 C16 . 1.390(5) ? C15 H15 . 0.9300 ? C16 C17 . 1.364(5) ? C16 H16 . 0.9300 ? C17 C18 . 1.403(4) ? C17 H17 . 0.9300 ? C18 N2 . 1.390(4) ? C19 N2 . 1.297(4) ? C19 H19 . 0.9300 ? C20 C21 . 1.387(4) ? C20 C25 . 1.393(4) ? C20 S1 . 1.750(3) ? C21 C22 . 1.384(5) ? C21 H21 . 0.9300 ? C22 C23 . 1.364(6) ? C22 H22 . 0.9300 ? C23 C24 . 1.381(7) ? C23 H23 . 0.9300 ? C24 C25 . 1.388(6) ? C24 H24 . 0.9300 ? C25 H25 . 0.9300 ? N1 S1 . 1.660(2) ? O1 S1 . 1.427(2) ? O2 S1 . 1.420(2) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C2 H2 O2 . 0.93 2.36 2.944(4) 120.9 yes C11 H11 O1 . 0.93 2.34 2.940(3) 122.2 yes C21 H21 N2 4_566 0.93 2.64 3.476(4) 149.8 yes C4 H4 Cg1 4_555 0.93 2.80 3.605(4) 145 yes C16 H16 Cg3 2_655 0.93 2.99 3.747(3) 139 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 C1 C2 C3 . . . . 1.1(4) ? N1 C1 C2 C3 . . . . -176.1(3) ? C1 C2 C3 C4 . . . . -0.3(5) ? C2 C3 C4 C5 . . . . -0.8(5) ? C3 C4 C5 C6 . . . . 1.1(5) ? C4 C5 C6 C1 . . . . -0.3(4) ? C4 C5 C6 C7 . . . . 176.9(3) ? C2 C1 C6 C5 . . . . -0.9(4) ? N1 C1 C6 C5 . . . . 176.9(2) ? C2 C1 C6 C7 . . . . -178.7(3) ? N1 C1 C6 C7 . . . . -0.9(3) ? C5 C6 C7 C8 . . . . 0.0(5) ? C1 C6 C7 C8 . . . . 177.4(3) ? C5 C6 C7 C12 . . . . -177.5(3) ? C1 C6 C7 C12 . . . . 0.0(3) ? C12 C7 C8 C9 . . . . -1.1(4) ? C6 C7 C8 C9 . . . . -178.3(3) ? C7 C8 C9 C10 . . . . 0.6(4) ? C7 C8 C9 C19 . . . . -178.7(3) ? C8 C9 C10 C11 . . . . 0.2(4) ? C19 C9 C10 C11 . . . . 179.6(2) ? C8 C9 C10 C13 . . . . 179.9(2) ? C19 C9 C10 C13 . . . . -0.8(4) ? C9 C10 C11 C12 . . . . -0.7(4) ? C13 C10 C11 C12 . . . . 179.7(2) ? C10 C11 C12 C7 . . . . 0.2(4) ? C10 C11 C12 N1 . . . . 177.2(2) ? C8 C7 C12 C11 . . . . 0.6(4) ? C6 C7 C12 C11 . . . . 178.5(2) ? C8 C7 C12 N1 . . . . -176.9(2) ? C6 C7 C12 N1 . . . . 0.9(3) ? C11 C10 C13 C14 . . . . 0.7(4) ? C9 C10 C13 C14 . . . . -179.0(2) ? C11 C10 C13 C18 . . . . -179.5(2) ? C9 C10 C13 C18 . . . . 0.9(3) ? C18 C13 C14 C15 . . . . 0.0(4) ? C10 C13 C14 C15 . . . . 179.8(3) ? C13 C14 C15 C16 . . . . -0.1(5) ? C14 C15 C16 C17 . . . . 0.4(5) ? C15 C16 C17 C18 . . . . -0.6(5) ? C16 C17 C18 N2 . . . . -179.5(3) ? C16 C17 C18 C13 . . . . 0.5(4) ? C14 C13 C18 N2 . . . . 179.8(3) ? C10 C13 C18 N2 . . . . 0.0(4) ? C14 C13 C18 C17 . . . . -0.2(4) ? C10 C13 C18 C17 . . . . 180.0(2) ? C8 C9 C19 N2 . . . . 179.1(3) ? C10 C9 C19 N2 . . . . -0.2(5) ? C25 C20 C21 C22 . . . . -1.2(4) ? S1 C20 C21 C22 . . . . 179.9(2) ? C20 C21 C22 C23 . . . . 2.0(5) ? C21 C22 C23 C24 . . . . -1.1(6) ? C22 C23 C24 C25 . . . . -0.5(6) ? C23 C24 C25 C20 . . . . 1.2(5) ? C21 C20 C25 C24 . . . . -0.4(4) ? S1 C20 C25 C24 . . . . 178.5(2) ? C11 C12 N1 C1 . . . . -178.7(2) ? C7 C12 N1 C1 . . . . -1.4(3) ? C11 C12 N1 S1 . . . . 22.5(4) ? C7 C12 N1 S1 . . . . -160.13(18) ? C6 C1 N1 C12 . . . . 1.4(3) ? C2 C1 N1 C12 . . . . 179.0(3) ? C6 C1 N1 S1 . . . . 160.52(19) ? C2 C1 N1 S1 . . . . -21.9(4) ? C9 C19 N2 C18 . . . . 1.1(5) ? C17 C18 N2 C19 . . . . 179.1(3) ? C13 C18 N2 C19 . . . . -0.9(4) ? C12 N1 S1 O2 . . . . -163.8(2) ? C1 N1 S1 O2 . . . . 40.7(2) ? C12 N1 S1 O1 . . . . -34.3(3) ? C1 N1 S1 O1 . . . . 170.2(2) ? C12 N1 S1 C20 . . . . 81.2(2) ? C1 N1 S1 C20 . . . . -74.3(2) ? C21 C20 S1 O2 . . . . -19.3(3) ? C25 C20 S1 O2 . . . . 161.8(2) ? C21 C20 S1 O1 . . . . -152.1(2) ? C25 C20 S1 O1 . . . . 29.0(3) ? C21 C20 S1 N1 . . . . 94.0(2) ? C25 C20 S1 N1 . . . . -84.9(2) ? _cod_database_fobs_code 2244215