#------------------------------------------------------------------------------ #$Date: 2023-03-14 03:11:18 +0000 (Tue, 14 Mar 2023) $ #$Revision: 281861 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/42/2244223.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244223 loop_ _publ_author_name 'Herbig, Marcus' 'B\"ohme, Uwe' _publ_section_title ; Two polymorphs of N,N'-diphenyl-2-[1-(propylamino)ethylidene]propanediamide ; _journal_coeditor_code PK2679 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1 _journal_page_last 0 _journal_paper_doi 10.1107/S2056989023002141 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C20 H23 N3 O2' _chemical_formula_moiety 'C20 H23 N3 O2' _chemical_formula_sum 'C20 H23 N3 O2' _chemical_formula_weight 337.41 _chemical_name_systematic ; N,N'-Diphenyl-2-[1-(propylamino)ethylidene]propanediamide ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 107.724(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.3881(4) _cell_length_b 24.3653(9) _cell_length_c 9.2614(5) _cell_measurement_reflns_used 18377 _cell_measurement_temperature 193(2) _cell_measurement_theta_max 27.42 _cell_measurement_theta_min 2.31 _cell_volume 1802.99(15) _computing_cell_refinement ; X-AREA (Stoe, 2009) ; _computing_data_collection ; X-AREA (Stoe, 2009) ; _computing_data_reduction ; X-RED (Stoe, 2009) ; _computing_molecular_graphics ; ORTEP3 for Windows (Farrugia, 2012) ; _computing_publication_material ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 193(2) _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'Stoe IPDS 2' _diffrn_measurement_method 'rotation method' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0537 _diffrn_reflns_av_unetI/netI 0.0296 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 31 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 18377 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.996 _diffrn_reflns_theta_min 2.455 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _exptl_absorpt_coefficient_mu 0.082 _exptl_absorpt_correction_T_max 0.9801 _exptl_absorpt_correction_T_min 0.8204 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; (X-RED; Stoe, 2009) ; _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.243 _exptl_crystal_description Prism _exptl_crystal_F_000 720 _exptl_crystal_size_max 0.480 _exptl_crystal_size_mid 0.210 _exptl_crystal_size_min 0.180 _refine_diff_density_max 0.141 _refine_diff_density_min -0.227 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.153 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 240 _refine_ls_number_reflns 3882 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.153 _refine_ls_R_factor_all 0.0742 _refine_ls_R_factor_gt 0.0514 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0475P)^2^+0.6249P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1119 _refine_ls_wR_factor_ref 0.1291 _reflns_number_gt 2967 _reflns_number_total 3882 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file pk2679sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2244223 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.962 _shelx_estimated_absorpt_t_max 0.985 _shelx_hkl_file ; 2 0 0 3682.56 14.36 0 -2 0 0 3718.11 14.69 0 4 0 0 405.64 6.53 0 -4 0 0 386.05 5.72 0 4 0 0 410.51 5.79 0 6 0 0 46.87 4.14 0 -6 0 0 48.88 4.20 0 6 0 0 45.87 5.25 0 -8 0 0 407.07 4.54 0 8 0 0 447.77 4.94 0 8 0 0 389.56 6.46 0 10 0 0 193.33 4.36 0 -10 0 0 179.34 4.19 0 10 0 0 175.37 6.25 0 10 0 0 177.04 6.93 0 -1 1 0 1836.88 15.31 0 -1 -1 0 1826.37 15.14 0 1 -1 0 1919.29 15.53 0 -1 -1 0 1964.51 20.55 0 1 1 0 1839.92 15.08 0 1 1 0 1890.75 20.25 0 3 1 0 38.16 6.63 0 3 -1 0 41.69 5.60 0 3 1 0 45.20 5.34 0 -3 -1 0 28.18 5.70 0 -3 1 0 36.68 5.68 0 -4 1 0 489.35 5.96 0 4 1 0 477.86 7.44 0 4 1 0 511.59 6.10 0 -4 -1 0 480.69 5.94 0 4 -1 0 504.90 6.01 0 5 -1 0 228.58 5.97 0 5 -1 0 254.74 4.93 0 -5 1 0 220.15 4.75 0 -5 -1 0 233.63 4.94 0 5 1 0 243.80 4.97 0 5 1 0 228.29 6.31 0 -6 1 0 163.60 4.44 0 6 1 0 179.77 4.26 0 6 1 0 165.14 5.73 0 6 -1 0 162.94 5.45 0 -6 -1 0 156.13 4.32 0 6 -1 0 178.20 4.43 0 7 1 0 371.67 4.96 0 -7 1 0 314.19 4.63 0 7 -1 0 332.95 4.77 0 -7 -1 0 332.58 4.57 0 7 -1 0 326.28 6.25 0 7 1 0 304.45 6.53 0 8 1 0 -0.09 5.09 0 8 -1 0 7.11 4.82 0 8 1 0 6.92 3.73 0 8 -1 0 3.56 4.64 0 -8 -1 0 10.61 3.65 0 8 -1 0 11.36 3.62 0 -8 1 0 14.68 3.67 0 9 -1 0 -2.68 5.17 0 9 1 0 5.75 5.13 0 9 -1 0 2.95 3.61 0 9 -1 0 6.53 4.68 0 9 1 0 -4.57 5.15 0 9 1 0 -3.99 3.62 0 -9 1 0 5.55 3.63 0 -9 -1 0 1.70 3.47 0 10 -1 0 -2.13 4.97 0 10 -1 0 10.48 3.63 0 10 1 0 -1.26 5.43 0 10 1 0 0.37 5.64 0 10 -1 0 -1.02 5.37 0 -10 1 0 -17.44 3.73 0 10 1 0 1.62 3.62 0 -10 -1 0 -1.89 3.64 0 1 -2 0 21.74 8.08 0 -1 -2 0 23.74 8.82 0 1 -2 0 20.89 8.54 0 -1 -2 0 24.74 9.75 0 1 2 0 24.25 8.54 0 1 2 0 19.12 9.42 0 -1 2 0 19.96 9.46 0 -2 -2 0 1586.40 10.74 0 2 2 0 1681.41 14.75 0 -2 2 0 1722.35 11.29 0 2 2 0 1761.70 10.89 0 2 -2 0 1805.39 11.26 0 -2 -2 0 1783.33 14.82 0 3 2 0 194.08 7.43 0 3 2 0 213.06 6.01 0 3 -2 0 212.04 5.92 0 -3 -2 0 195.11 6.04 0 -3 2 0 196.50 6.14 0 4 2 0 10.58 4.90 0 -4 -2 0 3.29 4.82 0 -4 2 0 5.99 4.80 0 4 2 0 15.53 5.53 0 4 -2 0 -7.11 4.78 0 5 -2 0 20.60 4.55 0 5 2 0 27.99 5.65 0 5 2 0 31.86 4.46 0 -5 -2 0 32.40 4.46 0 -5 2 0 31.64 4.59 0 6 -2 0 0.97 4.78 0 6 -2 0 -4.79 4.29 0 6 2 0 4.08 3.82 0 6 2 0 9.05 5.02 0 -6 -2 0 -4.00 3.85 0 -6 2 0 0.11 4.19 0 7 -2 0 1.99 3.87 0 7 -2 0 2.18 4.84 0 7 2 0 2.47 5.33 0 -7 -2 0 3.73 3.74 0 7 2 0 1.69 3.70 0 -7 2 0 -1.96 4.12 0 8 2 0 87.25 3.89 0 8 -2 0 87.70 3.86 0 8 -2 0 80.86 5.16 0 -8 2 0 80.66 4.15 0 -8 -2 0 75.70 3.73 0 8 2 0 76.58 5.31 0 8 -2 0 74.76 4.93 0 9 2 0 2.09 5.19 0 9 -2 0 9.11 4.68 0 -9 2 0 -7.88 3.77 0 9 2 0 -0.39 3.55 0 9 -2 0 -16.49 3.79 0 9 -2 0 5.73 4.63 0 9 2 0 4.38 5.54 0 -9 -2 0 -0.37 3.60 0 10 -2 0 6.37 5.30 0 -10 2 0 27.29 3.57 0 10 2 0 5.65 5.60 0 -10 -2 0 -6.51 3.46 0 10 2 0 7.52 5.87 0 10 -2 0 3.40 3.53 0 10 2 0 -0.85 3.80 0 10 -2 0 6.02 4.84 0 1 3 0 16.78 7.81 0 1 -3 0 10.42 8.94 0 -1 -3 0 21.78 8.00 0 -1 3 0 19.58 8.80 0 1 3 0 17.54 8.75 0 -1 -3 0 18.34 8.97 0 1 -3 0 16.99 8.96 0 2 -3 0 6131.58 18.15 0 -2 -3 0 6034.22 22.68 0 2 3 0 5803.47 16.64 0 -2 -3 0 5465.06 16.26 0 -2 3 0 6012.10 18.25 0 2 3 0 5741.20 22.34 0 3 3 0 1184.38 10.77 0 -3 -3 0 1185.05 10.74 0 3 3 0 1221.41 8.04 0 -3 3 0 1140.97 8.18 0 3 -3 0 1239.87 8.16 0 -3 -3 0 1140.30 7.88 0 4 3 0 154.96 6.23 0 4 -3 0 162.15 5.12 0 -4 -3 0 143.83 5.17 0 -4 3 0 157.11 5.26 0 4 3 0 162.51 5.23 0 5 -3 0 29.11 4.52 0 5 3 0 38.19 4.45 0 -5 -3 0 32.31 4.17 0 -5 3 0 24.91 4.58 0 5 3 0 29.44 5.29 0 6 -3 0 125.62 4.49 0 -6 -3 0 112.02 3.87 0 6 3 0 120.46 4.08 0 6 3 0 113.87 5.53 0 -6 3 0 110.03 4.54 0 7 -3 0 -3.29 5.30 0 7 3 0 12.96 5.49 0 7 -3 0 6.75 4.85 0 7 -3 0 17.87 3.80 0 -7 -3 0 10.31 3.53 0 -7 3 0 18.85 3.85 0 7 3 0 8.74 3.69 0 -8 -3 0 5.42 3.55 0 -8 3 0 -2.62 3.82 0 8 -3 0 -7.39 4.55 0 8 -3 0 4.11 4.52 0 8 3 0 -1.02 3.97 0 8 -3 0 -2.42 3.70 0 9 -3 0 33.33 4.67 0 9 -3 0 48.85 5.08 0 -9 3 0 62.95 3.67 0 9 3 0 47.42 3.91 0 9 -3 0 32.19 3.76 0 -9 -3 0 38.23 3.97 0 9 3 0 39.65 5.61 0 10 3 0 5.87 5.84 0 -10 -3 0 -4.05 3.49 0 -10 3 0 -0.19 3.40 0 10 -3 0 3.56 5.29 0 10 3 0 8.20 5.72 0 10 -3 0 4.54 4.58 0 10 -3 0 7.55 3.45 0 10 3 0 10.74 3.45 0 0 -4 0 6606.53 23.22 0 1 4 0 5192.05 20.51 0 1 -4 0 6091.98 24.30 0 -1 4 0 5606.68 23.67 0 -1 -4 0 5390.13 20.72 0 -1 4 0 4763.13 17.78 0 -1 -4 0 5077.60 20.04 0 1 -4 0 5135.44 18.42 0 1 4 0 5205.85 21.05 0 2 4 0 923.17 8.54 0 -2 -4 0 870.52 9.20 0 2 4 0 863.33 10.90 0 2 -4 0 984.22 9.00 0 2 -4 0 836.69 9.18 0 -2 4 0 909.29 8.98 0 -2 -4 0 922.19 11.10 0 3 4 0 101.95 7.10 0 -3 -4 0 107.97 7.02 0 -3 4 0 103.61 5.60 0 3 4 0 107.33 5.54 0 -3 -4 0 105.36 5.53 0 3 -4 0 105.71 5.63 0 4 4 0 91.08 5.01 0 4 4 0 90.77 6.51 0 4 -4 0 100.65 4.94 0 -4 4 0 88.96 4.98 0 -4 -4 0 84.65 5.07 0 -5 -4 0 -7.35 4.33 0 5 4 0 -0.71 5.13 0 -5 4 0 10.49 4.54 0 5 4 0 1.25 4.28 0 5 -4 0 -4.11 4.42 0 -6 4 0 2.49 4.68 0 6 -4 0 9.13 4.30 0 6 4 0 9.54 3.82 0 -6 -4 0 0.15 3.75 0 6 -4 0 8.04 4.79 0 6 4 0 1.67 5.12 0 7 -4 0 19.18 4.56 0 7 -4 0 19.30 3.83 0 -7 -4 0 7.08 3.63 0 -7 4 0 10.69 3.73 0 7 4 0 14.92 3.07 0 7 4 0 17.85 5.27 0 8 -4 0 6.36 4.38 0 -8 4 0 -13.86 3.62 0 8 -4 0 16.49 3.97 0 -8 -4 0 -4.43 3.55 0 8 -4 0 -11.30 4.59 0 8 4 0 15.33 3.66 0 9 -4 0 14.66 4.40 0 -9 4 0 14.70 3.50 0 -9 -4 0 0.16 3.61 0 9 -4 0 18.27 4.98 0 9 4 0 1.15 5.61 0 9 4 0 -13.49 3.74 0 9 -4 0 18.13 3.62 0 10 -4 0 14.76 3.32 0 -10 -4 0 17.12 3.23 0 -10 4 0 2.94 3.30 0 10 4 0 -0.04 5.91 0 10 4 0 -1.20 3.62 0 10 -4 0 7.36 4.53 0 10 -4 0 9.73 5.31 0 10 4 0 3.87 5.84 0 -1 -5 0 938.68 11.17 0 -1 5 0 912.91 12.58 0 1 -5 0 871.28 9.71 0 1 5 0 860.55 10.91 0 1 5 0 840.77 10.13 0 -1 5 0 833.09 9.62 0 -1 -5 0 834.73 10.97 0 2 5 0 508.41 7.18 0 2 -5 0 519.88 8.05 0 -2 5 0 502.37 8.17 0 2 5 0 482.92 8.36 0 -2 -5 0 479.17 7.34 0 -2 -5 0 506.96 9.03 0 2 -5 0 467.51 7.18 0 -3 5 0 397.31 6.55 0 3 5 0 406.92 6.19 0 -3 -5 0 388.90 6.23 0 3 -5 0 468.52 6.61 0 3 -5 0 376.50 6.10 0 3 5 0 392.10 7.97 0 -3 -5 0 418.88 7.81 0 4 5 0 172.51 6.34 0 4 -5 0 178.15 5.93 0 -4 -5 0 181.20 5.16 0 4 -5 0 168.80 5.07 0 4 5 0 188.14 5.21 0 -4 -5 0 194.43 6.63 0 -4 5 0 183.50 5.73 0 5 -5 0 2.15 4.86 0 5 -5 0 -7.37 5.15 0 5 5 0 4.11 5.69 0 -5 -5 0 4.96 4.32 0 -5 5 0 13.45 4.50 0 5 5 0 10.92 4.35 0 -6 -5 0 9.74 3.86 0 6 5 0 12.88 5.74 0 -6 5 0 -0.55 4.24 0 6 5 0 4.18 3.93 0 6 -5 0 1.33 4.95 0 6 -5 0 6.22 4.64 0 7 -5 0 24.09 3.75 0 7 5 0 17.90 5.67 0 -7 5 0 19.08 3.84 0 7 -5 0 22.96 4.64 0 -7 -5 0 26.37 3.64 0 7 5 0 42.83 3.65 0 8 -5 0 25.29 4.65 0 8 -5 0 26.60 3.95 0 8 -5 0 34.12 3.70 0 8 5 0 16.83 3.79 0 -8 -5 0 28.55 3.69 0 -8 5 0 22.70 3.65 0 9 5 0 20.12 5.88 0 -9 5 0 24.92 3.46 0 -9 -5 0 37.82 3.66 0 9 5 0 18.92 3.74 0 9 -5 0 21.84 4.92 0 9 -5 0 16.46 4.23 0 9 -5 0 17.21 3.60 0 -10 5 0 9.72 3.36 0 10 -5 0 1.11 4.42 0 -10 -5 0 8.40 3.56 0 10 5 0 2.20 6.15 0 10 -5 0 9.45 4.88 0 10 5 0 -0.30 6.24 0 1 6 0 771.05 9.23 0 -1 6 0 896.52 11.98 0 -1 6 0 775.04 8.78 0 1 -6 0 842.79 9.19 0 -1 -6 0 837.67 10.12 0 1 6 0 817.07 10.11 0 -1 -6 0 784.90 10.18 0 2 6 0 146.94 6.74 0 2 -6 0 159.56 6.72 0 -2 -6 0 152.26 6.77 0 -2 6 0 158.39 6.76 0 -2 -6 0 157.88 6.12 0 2 6 0 158.02 5.87 0 -3 6 0 1.04 5.22 0 3 -6 0 -0.81 5.05 0 -3 -6 0 6.24 5.55 0 3 6 0 3.52 4.98 0 3 6 0 -1.69 5.66 0 -4 -6 0 136.68 6.17 0 4 6 0 140.62 6.44 0 4 6 0 131.47 5.51 0 -4 -6 0 124.24 4.79 0 -4 6 0 136.87 4.93 0 5 -6 0 29.56 4.87 0 5 -6 0 29.68 4.36 0 -5 -6 0 12.96 4.33 0 5 6 0 26.07 5.92 0 -5 6 0 23.24 4.53 0 5 6 0 32.74 4.21 0 6 6 0 299.76 6.94 0 6 -6 0 273.47 5.42 0 6 6 0 301.90 4.53 0 -6 -6 0 291.18 4.53 0 -6 6 0 275.59 4.89 0 6 -6 0 303.59 5.27 0 -7 -6 0 -2.34 3.68 0 7 6 0 -0.57 5.37 0 7 -6 0 2.56 3.80 0 -7 6 0 -0.44 4.28 0 7 6 0 3.29 3.79 0 7 -6 0 8.84 4.95 0 8 -6 0 10.41 4.02 0 8 6 0 11.33 3.75 0 8 6 0 15.33 5.66 0 -8 -6 0 -8.76 3.61 0 -8 6 0 15.39 3.71 0 8 -6 0 10.65 4.64 0 9 -6 0 38.63 4.72 0 9 6 0 43.18 6.03 0 9 -6 0 39.84 4.49 0 -9 6 0 37.28 3.99 0 -9 -6 0 32.42 3.81 0 9 -6 0 41.89 3.68 0 9 6 0 41.34 4.01 0 -10 -6 0 -2.59 3.20 0 -1 -7 0 214.83 7.52 0 1 7 0 212.34 7.45 0 1 -7 0 226.27 5.95 0 -1 -7 0 214.33 6.68 0 -1 7 0 213.13 6.76 0 -1 7 0 246.46 9.04 0 2 -7 0 34.49 6.07 0 -2 -7 0 32.65 6.01 0 -2 -7 0 25.54 6.11 0 -2 7 0 31.87 6.90 0 2 7 0 36.52 5.28 0 2 7 0 29.75 6.05 0 3 7 0 61.14 5.96 0 3 -7 0 75.01 5.17 0 3 7 0 73.99 5.11 0 -3 7 0 72.36 6.04 0 -3 -7 0 64.10 5.86 0 -4 7 0 84.37 5.01 0 -4 -7 0 81.16 4.76 0 4 7 0 89.47 5.32 0 -4 -7 0 89.64 5.89 0 4 7 0 92.87 6.00 0 5 7 0 45.99 4.34 0 5 -7 0 43.38 5.01 0 -5 -7 0 34.18 5.36 0 5 -7 0 38.33 5.03 0 5 7 0 40.98 5.46 0 -5 -7 0 38.96 4.37 0 -5 7 0 28.46 4.46 0 6 7 0 209.53 4.46 0 6 -7 0 221.47 4.71 0 -6 -7 0 185.92 4.23 0 -6 7 0 195.86 4.81 0 6 -7 0 187.09 5.25 0 -7 -7 0 44.24 3.72 0 -7 7 0 39.60 4.11 0 7 -7 0 40.90 4.81 0 7 -7 0 48.30 3.96 0 7 7 0 49.64 4.08 0 -8 7 0 56.67 3.96 0 8 7 0 71.89 3.90 0 -8 -7 0 48.05 3.73 0 8 -7 0 63.55 3.94 0 8 -7 0 60.80 4.98 0 8 7 0 56.92 5.86 0 9 -7 0 4.62 3.51 0 9 7 0 0.65 5.81 0 9 -7 0 -1.23 4.38 0 9 7 0 -1.21 3.78 0 -9 7 0 14.23 3.46 0 9 -7 0 1.15 3.93 0 -9 -7 0 1.26 3.61 0 -1 -8 0 70.32 6.72 0 1 8 0 66.49 6.94 0 -1 8 0 63.87 7.42 0 -1 -8 0 67.64 6.39 0 -1 8 0 68.26 6.27 0 -1 8 0 84.13 8.17 0 -2 -8 0 1683.09 10.15 0 2 8 0 1601.35 9.65 0 -2 8 0 1741.04 11.47 0 3 -8 0 12.69 5.79 0 3 8 0 23.97 5.84 0 3 8 0 22.78 4.94 0 -3 8 0 19.92 5.76 0 -3 -8 0 20.14 5.78 0 4 8 0 792.73 6.37 0 -4 8 0 814.27 6.80 0 -4 -8 0 774.27 6.31 0 -4 -8 0 825.38 7.83 0 4 8 0 815.47 8.18 0 4 -8 0 836.67 6.69 0 -5 -8 0 299.05 5.33 0 -5 8 0 343.02 5.72 0 -5 -8 0 334.35 6.51 0 5 -8 0 345.13 5.13 0 5 8 0 327.58 5.22 0 5 -8 0 305.65 5.17 0 6 -8 0 671.01 6.56 0 -6 8 0 706.65 5.90 0 -6 -8 0 696.28 5.42 0 6 -8 0 747.09 5.91 0 6 8 0 751.62 5.61 0 -7 -8 0 1.64 3.68 0 7 8 0 -7.40 3.78 0 7 -8 0 1.13 3.89 0 7 -8 0 -7.17 4.57 0 -7 8 0 0.90 4.08 0 8 8 0 23.89 3.78 0 -8 8 0 33.13 3.97 0 8 8 0 40.65 5.46 0 -8 -8 0 38.22 3.44 0 8 -8 0 23.22 4.75 0 8 -8 0 17.38 3.90 0 9 -8 0 7.85 3.98 0 9 -8 0 8.24 4.04 0 -9 8 0 1.94 3.67 0 9 8 0 16.79 3.64 0 9 8 0 0.20 5.99 0 9 -8 0 11.93 5.08 0 -9 -8 0 -4.41 3.51 0 1 9 0 457.89 7.58 0 -1 9 0 495.35 6.89 0 -1 9 0 495.67 9.18 0 -1 -9 0 477.87 6.73 0 2 9 0 40.65 4.99 0 -2 9 0 40.15 6.58 0 -2 -9 0 31.81 5.92 0 -2 9 0 39.68 5.27 0 -3 9 0 475.54 7.04 0 3 9 0 477.29 6.50 0 3 9 0 444.83 7.05 0 3 -9 0 520.49 7.05 0 -3 -9 0 448.07 5.88 0 -3 -9 0 492.05 7.11 0 4 -9 0 339.49 6.14 0 -4 -9 0 283.89 5.39 0 4 9 0 329.64 5.40 0 -4 9 0 341.47 6.18 0 -4 -9 0 324.79 6.18 0 5 9 0 143.53 4.72 0 -5 9 0 127.41 5.17 0 5 -9 0 137.50 4.63 0 -5 -9 0 123.85 4.79 0 -5 -9 0 137.64 5.64 0 5 -9 0 134.95 4.69 0 6 9 0 367.09 4.94 0 -6 9 0 384.20 5.84 0 -6 -9 0 360.23 4.82 0 6 -9 0 375.59 5.62 0 6 -9 0 356.60 5.72 0 7 9 0 160.11 4.16 0 7 -9 0 144.80 5.14 0 -7 -9 0 124.72 3.83 0 -7 9 0 136.41 4.40 0 7 9 0 143.82 5.93 0 7 -9 0 158.11 4.63 0 -8 -9 0 12.01 3.55 0 8 -9 0 -3.90 3.65 0 8 9 0 2.15 5.60 0 8 9 0 -3.93 3.73 0 -8 9 0 5.25 3.83 0 8 -9 0 -2.16 4.90 0 9 -9 0 3.02 4.52 0 9 9 0 -0.53 5.73 0 9 -9 0 10.29 3.60 0 9 9 0 6.73 3.82 0 -9 9 0 3.22 4.13 0 -9 -9 0 -6.77 3.42 0 1 10 0 1123.21 9.94 0 -1 10 0 1197.95 11.03 0 -1 10 0 1117.77 7.83 0 -1 -10 0 1141.59 8.07 0 -2 -10 0 792.92 7.78 0 2 10 0 784.30 7.89 0 -2 10 0 732.70 6.70 0 -2 10 0 828.03 8.82 0 3 10 0 1029.61 7.14 0 -3 -10 0 1062.22 8.22 0 -3 10 0 1080.47 8.54 0 -3 -10 0 971.77 7.10 0 4 -10 0 880.69 6.74 0 -4 10 0 853.79 7.32 0 4 10 0 823.17 6.77 0 -4 -10 0 780.74 6.28 0 -4 -10 0 830.12 7.40 0 5 -10 0 26.17 4.20 0 5 10 0 11.85 4.39 0 -5 -10 0 23.33 4.85 0 -5 10 0 15.91 4.85 0 5 -10 0 6.41 4.40 0 -5 -10 0 15.70 5.03 0 -6 -10 0 97.24 4.21 0 6 -10 0 104.94 4.32 0 6 10 0 106.54 4.22 0 6 -10 0 87.70 5.09 0 -6 10 0 93.15 4.55 0 -6 -10 0 98.93 5.53 0 -7 -10 0 88.91 3.83 0 7 -10 0 81.20 4.62 0 7 10 0 67.38 5.56 0 -7 10 0 82.75 4.26 0 7 10 0 86.66 3.97 0 7 -10 0 95.72 4.12 0 8 10 0 4.03 3.66 0 8 10 0 -0.78 5.30 0 -8 -10 0 -2.96 3.73 0 8 -10 0 6.41 4.46 0 -8 10 0 3.92 3.83 0 8 -10 0 12.60 4.11 0 9 10 0 10.89 3.79 0 -9 -10 0 -3.35 3.33 0 9 -10 0 -7.84 3.55 0 9 10 0 4.69 5.80 0 -9 10 0 20.10 4.02 0 9 -10 0 0.12 4.62 0 -1 11 0 9.72 5.28 0 -1 -11 0 23.82 5.34 0 1 11 0 21.69 6.22 0 -1 11 0 30.83 6.24 0 2 11 0 27.06 5.02 0 -2 11 0 30.92 4.97 0 -2 11 0 31.81 5.98 0 -2 -11 0 23.80 6.08 0 -3 11 0 545.47 7.39 0 -3 -11 0 541.17 6.79 0 3 11 0 530.92 6.67 0 4 11 0 224.60 5.01 0 -4 -11 0 233.51 6.11 0 4 -11 0 270.19 5.78 0 -4 11 0 246.77 5.70 0 5 -11 0 3.19 4.28 0 5 11 0 2.93 4.22 0 -5 -11 0 10.43 4.56 0 -5 -11 0 4.66 4.62 0 -5 11 0 4.56 4.91 0 5 -11 0 -1.50 4.25 0 6 -11 0 6.44 4.95 0 -6 -11 0 5.98 3.89 0 -6 11 0 -0.41 4.91 0 -6 -11 0 5.31 5.35 0 6 -11 0 -2.34 4.80 0 6 11 0 -4.14 3.90 0 -7 -11 0 18.54 3.90 0 7 -11 0 11.43 4.62 0 -7 11 0 22.58 4.08 0 7 11 0 28.18 3.86 0 7 11 0 18.17 5.31 0 7 -11 0 12.72 3.94 0 8 11 0 11.81 3.59 0 -8 -11 0 17.25 3.63 0 8 -11 0 23.26 4.34 0 -8 11 0 23.17 4.18 0 8 11 0 9.13 5.20 0 8 -11 0 15.40 3.97 0 9 11 0 2.30 5.61 0 9 -11 0 -5.48 4.58 0 -9 11 0 5.52 3.86 0 -9 -11 0 -5.89 3.64 0 9 -11 0 -1.80 3.46 0 9 11 0 3.59 3.81 0 0 -12 0 264.67 5.72 0 -1 12 0 11.94 5.04 0 -1 -12 0 13.88 5.20 0 1 12 0 8.65 5.74 0 -2 -12 0 181.41 6.36 0 2 12 0 168.42 5.76 0 -2 12 0 182.57 5.13 0 -2 12 0 187.35 6.91 0 3 12 0 547.39 6.62 0 -3 12 0 589.09 7.13 0 -3 -12 0 569.85 6.12 0 -4 12 0 223.38 5.59 0 4 12 0 204.05 4.74 0 -4 -12 0 220.27 5.47 0 -5 -12 0 14.72 5.38 0 -5 12 0 27.11 4.94 0 5 12 0 12.47 4.54 0 -5 -12 0 15.78 4.58 0 5 -12 0 5.09 4.51 0 -6 12 0 1268.28 7.60 0 6 -12 0 1362.80 7.09 0 6 12 0 1162.78 8.79 0 -6 -12 0 1251.63 8.86 0 -6 -12 0 1262.77 6.31 0 6 12 0 1257.12 6.58 0 6 -12 0 1196.09 7.22 0 7 12 0 24.80 4.96 0 7 12 0 29.89 3.70 0 -7 -12 0 30.07 3.70 0 7 -12 0 31.28 4.42 0 -7 12 0 18.28 4.38 0 7 -12 0 27.56 5.07 0 8 -12 0 2.00 4.59 0 8 12 0 -1.82 3.49 0 8 12 0 5.15 5.27 0 -8 12 0 -8.50 4.14 0 8 -12 0 -5.51 3.91 0 -8 -12 0 9.05 3.40 0 -9 -12 0 7.69 3.59 0 -9 12 0 -1.11 3.83 0 9 12 0 1.72 5.71 0 9 -12 0 -2.65 4.60 0 9 12 0 -2.76 3.68 0 9 -12 0 -8.80 3.74 0 1 13 0 71.07 5.85 0 -1 -13 0 72.68 5.07 0 -1 13 0 67.01 4.01 0 -2 13 0 360.06 5.57 0 -2 13 0 377.07 6.69 0 -2 -13 0 403.30 5.98 0 2 13 0 373.78 6.62 0 -2 13 0 403.64 7.67 0 -3 -13 0 382.06 6.16 0 -3 13 0 385.15 6.99 0 3 13 0 365.21 5.42 0 -4 -13 0 20.81 5.41 0 4 13 0 20.87 4.71 0 -4 13 0 19.41 4.87 0 4 -13 0 14.85 4.95 0 5 13 0 147.47 4.59 0 -5 13 0 166.06 5.25 0 -5 -13 0 134.59 5.50 0 5 -13 0 154.59 5.59 0 -5 -13 0 126.85 4.92 0 6 -13 0 159.89 4.92 0 6 13 0 148.13 4.28 0 -6 -13 0 144.04 5.76 0 6 -13 0 171.56 4.53 0 -6 -13 0 160.37 4.24 0 -6 13 0 157.11 5.23 0 6 13 0 144.41 5.84 0 7 -13 0 277.30 4.58 0 7 13 0 227.95 5.90 0 -7 -13 0 236.46 4.13 0 7 -13 0 260.87 5.40 0 7 13 0 264.03 4.32 0 -7 -13 0 232.93 6.06 0 -7 13 0 229.48 4.92 0 -8 -13 0 19.29 3.50 0 -8 13 0 -4.03 3.95 0 8 13 0 4.46 3.47 0 8 -13 0 -2.67 3.48 0 8 -13 0 -12.59 4.65 0 8 13 0 0.98 5.18 0 -9 -13 0 16.26 3.48 0 9 -13 0 0.87 3.73 0 9 -13 0 23.81 4.36 0 -9 13 0 13.49 3.95 0 9 13 0 46.65 3.60 0 9 13 0 7.14 5.89 0 0 14 0 571.08 8.13 0 0 -14 0 597.98 8.46 0 0 14 0 610.00 6.12 0 1 14 0 15.93 5.53 0 -1 -14 0 24.34 4.64 0 -1 14 0 10.65 4.57 0 -2 14 0 94.87 4.77 0 -2 -14 0 103.92 5.95 0 2 14 0 101.10 5.22 0 -2 14 0 102.54 5.88 0 -2 14 0 112.66 6.44 0 3 14 0 101.39 5.13 0 -3 -14 0 125.88 5.35 0 -3 14 0 113.82 5.87 0 -4 14 0 32.89 5.22 0 4 14 0 32.34 4.76 0 -4 -14 0 29.72 4.89 0 4 -14 0 24.69 4.95 0 5 -14 0 29.13 4.62 0 -5 -14 0 26.55 4.65 0 5 14 0 32.22 4.09 0 -5 -14 0 45.22 3.99 0 -5 14 0 21.87 4.71 0 -6 14 0 101.61 4.97 0 6 14 0 87.95 5.41 0 6 -14 0 90.42 4.96 0 -6 -14 0 90.75 4.57 0 -6 -14 0 91.65 5.24 0 6 14 0 89.47 4.13 0 -7 14 0 -8.81 4.09 0 7 14 0 1.68 3.58 0 7 -14 0 7.13 4.57 0 7 14 0 4.20 4.57 0 -7 -14 0 -13.42 3.57 0 -7 -14 0 2.69 4.60 0 8 -14 0 2.97 3.99 0 -8 14 0 2.87 4.04 0 8 14 0 15.67 3.45 0 -8 -14 0 1.81 3.26 0 8 14 0 5.56 5.21 0 -9 -14 0 6.26 3.22 0 -9 14 0 14.64 3.89 0 9 -14 0 -8.36 4.45 0 -1 15 0 -2.47 4.50 0 1 15 0 8.55 5.42 0 1 -15 0 15.72 4.65 0 -1 -15 0 6.34 5.48 0 -2 15 0 34.54 5.94 0 -2 -15 0 55.19 5.37 0 -2 15 0 36.34 4.68 0 2 15 0 30.28 4.70 0 -3 15 0 23.39 5.23 0 3 15 0 19.93 4.84 0 -3 -15 0 12.85 5.23 0 -4 15 0 41.97 5.22 0 4 -15 0 53.37 5.38 0 4 15 0 44.64 4.95 0 -4 -15 0 38.57 5.00 0 4 15 0 35.84 4.70 0 5 -15 0 6.96 4.40 0 -5 -15 0 -2.37 4.52 0 5 15 0 -10.30 4.65 0 -5 -15 0 -0.60 3.80 0 -5 15 0 -1.53 4.52 0 5 15 0 -0.11 3.84 0 6 15 0 0.95 4.36 0 6 15 0 2.13 3.93 0 -6 15 0 6.09 4.76 0 -6 -15 0 3.55 4.73 0 6 -15 0 5.22 4.30 0 -6 -15 0 10.00 4.34 0 7 -15 0 0.25 4.45 0 -7 -15 0 12.73 4.76 0 7 15 0 -4.37 4.77 0 7 15 0 3.79 3.75 0 -7 -15 0 -3.00 3.62 0 -7 15 0 6.22 3.75 0 8 15 0 6.35 3.74 0 8 15 0 4.96 5.21 0 -8 15 0 6.95 3.67 0 8 -15 0 5.41 4.53 0 -8 -15 0 4.30 3.61 0 0 16 0 29.60 5.74 0 0 16 0 38.11 4.40 0 0 -16 0 29.40 5.98 0 1 -16 0 5.52 4.61 0 -1 16 0 -3.46 4.47 0 -1 -16 0 -1.22 4.68 0 1 16 0 3.40 5.17 0 1 16 0 7.20 4.55 0 -2 16 0 -6.26 4.25 0 2 -16 0 -2.36 4.37 0 -2 -16 0 -3.51 4.75 0 2 16 0 3.76 5.00 0 -2 16 0 4.14 5.71 0 3 -16 0 132.90 4.77 0 -3 -16 0 159.78 5.48 0 3 16 0 154.65 5.20 0 -3 16 0 147.46 5.75 0 4 16 0 59.52 4.96 0 4 16 0 42.08 4.14 0 -4 16 0 61.40 4.92 0 4 -16 0 44.51 4.56 0 -4 -16 0 48.51 4.78 0 5 16 0 360.26 6.37 0 -5 16 0 374.02 5.81 0 -5 -16 0 334.08 4.85 0 5 16 0 378.28 5.52 0 -5 -16 0 361.86 5.74 0 5 -16 0 379.54 5.23 0 6 -16 0 206.47 4.88 0 6 16 0 210.24 5.63 0 6 16 0 210.84 4.90 0 -6 16 0 211.06 5.38 0 -6 -16 0 211.14 5.30 0 -6 -16 0 173.32 4.76 0 -7 -16 0 105.51 3.93 0 -7 -16 0 92.41 4.91 0 7 -16 0 108.33 4.35 0 7 16 0 107.58 3.96 0 7 16 0 85.18 5.22 0 -7 16 0 88.56 4.61 0 8 16 0 4.32 3.47 0 8 16 0 8.77 5.46 0 -8 -16 0 3.09 3.36 0 8 -16 0 9.82 4.47 0 -8 16 0 -2.24 4.32 0 1 -17 0 24.00 4.29 0 -1 -17 0 12.03 5.23 0 1 17 0 4.90 5.06 0 -1 17 0 20.61 4.21 0 -2 -17 0 126.97 5.45 0 2 17 0 150.83 5.41 0 2 17 0 145.10 5.30 0 -2 17 0 143.00 4.32 0 -2 17 0 153.68 6.89 0 -3 17 0 26.12 5.55 0 3 -17 0 12.44 4.27 0 -3 -17 0 25.73 4.59 0 3 17 0 28.79 4.53 0 3 17 0 12.70 5.29 0 4 17 0 7.66 5.16 0 4 -17 0 21.97 4.52 0 -4 17 0 18.53 5.13 0 4 17 0 7.06 4.48 0 -4 -17 0 8.30 4.69 0 -5 -17 0 7.68 4.25 0 -5 17 0 10.27 4.91 0 5 17 0 11.63 4.96 0 -5 -17 0 11.89 5.06 0 5 17 0 11.47 4.31 0 5 -17 0 1.94 4.33 0 6 17 0 29.64 4.91 0 6 17 0 27.58 4.34 0 -6 -17 0 33.50 4.34 0 -6 17 0 44.39 4.62 0 6 -17 0 35.88 4.33 0 -6 -17 0 42.08 4.67 0 -7 -17 0 -0.01 4.70 0 7 17 0 13.71 3.77 0 -7 17 0 6.93 4.14 0 7 17 0 8.07 5.06 0 -7 -17 0 4.24 3.97 0 7 -17 0 -8.66 4.36 0 -8 17 0 17.25 4.28 0 -8 -17 0 19.90 3.75 0 8 17 0 14.33 5.44 0 8 -17 0 8.17 4.09 0 8 17 0 15.26 3.74 0 0 18 0 276.68 6.87 0 0 -18 0 279.95 5.20 0 -1 -18 0 103.29 4.97 0 -1 18 0 109.55 4.25 0 1 18 0 95.65 5.80 0 1 -18 0 107.59 4.31 0 2 18 0 19.60 4.78 0 -2 18 0 9.36 3.92 0 -2 18 0 15.91 6.12 0 2 18 0 16.67 4.37 0 -2 -18 0 15.78 5.29 0 -3 -18 0 11.41 4.51 0 3 18 0 12.44 4.51 0 -3 18 0 7.00 5.47 0 3 -18 0 3.45 4.18 0 -4 -18 0 -2.74 4.67 0 4 18 0 3.22 4.84 0 4 18 0 -8.60 4.69 0 4 -18 0 7.83 4.00 0 -4 -18 0 -0.90 4.42 0 -4 18 0 8.02 5.45 0 -5 -18 0 64.91 4.91 0 5 18 0 58.02 5.27 0 -5 18 0 60.48 4.82 0 5 -18 0 46.53 4.21 0 -5 -18 0 42.91 4.12 0 5 18 0 66.67 3.90 0 6 -18 0 25.90 4.17 0 6 18 0 22.14 3.68 0 -6 18 0 30.41 4.56 0 6 18 0 17.58 4.72 0 -6 -18 0 17.82 4.74 0 -6 -18 0 33.01 4.19 0 7 -18 0 31.05 4.28 0 -7 18 0 50.27 4.05 0 7 18 0 34.33 3.81 0 -7 -18 0 37.89 4.02 0 7 18 0 41.38 4.99 0 -7 -18 0 42.30 4.68 0 -8 -18 0 5.18 3.54 0 -8 -18 0 -4.63 4.61 0 -8 18 0 4.70 3.83 0 8 -18 0 6.73 3.72 0 8 18 0 23.83 3.64 0 8 18 0 -3.52 5.22 0 -1 19 0 297.89 4.64 0 -1 -19 0 331.85 5.34 0 1 19 0 296.98 6.29 0 2 -19 0 26.92 4.16 0 -2 -19 0 29.46 5.08 0 2 19 0 16.42 4.41 0 2 19 0 18.40 5.20 0 -2 19 0 29.80 6.21 0 -2 19 0 39.66 3.90 0 -3 -19 0 377.82 5.86 0 -3 19 0 393.64 7.15 0 3 19 0 374.35 5.63 0 3 -19 0 367.15 5.01 0 -4 19 0 10.56 4.94 0 -4 -19 0 0.04 4.20 0 4 19 0 11.05 4.23 0 -4 -19 0 7.44 4.45 0 4 19 0 0.53 4.04 0 4 -19 0 3.33 3.99 0 5 19 0 14.07 4.20 0 -5 19 0 18.83 4.54 0 -5 -19 0 23.89 3.58 0 5 19 0 0.42 4.82 0 -5 -19 0 -5.83 4.67 0 5 -19 0 4.87 4.05 0 -6 -19 0 14.41 3.96 0 6 -19 0 8.05 4.27 0 6 19 0 26.71 3.67 0 -6 -19 0 19.89 4.34 0 -6 19 0 20.49 4.35 0 6 19 0 29.54 4.91 0 -7 19 0 199.22 5.00 0 7 19 0 197.86 5.86 0 7 19 0 230.20 4.16 0 -7 -19 0 177.79 5.44 0 -7 -19 0 173.03 4.32 0 7 -19 0 202.36 4.34 0 -8 19 0 9.45 3.95 0 0 20 0 2814.56 8.76 0 1 20 0 73.81 5.91 0 -1 20 0 75.67 7.28 0 -1 -20 0 82.91 4.66 0 1 20 0 72.35 4.44 0 -1 20 0 59.63 4.32 0 -2 -20 0 204.52 4.84 0 2 20 0 168.91 5.78 0 2 -20 0 184.24 4.42 0 -2 20 0 183.61 4.37 0 -2 20 0 194.20 7.44 0 2 20 0 205.49 5.01 0 3 20 0 16.84 4.52 0 -3 20 0 30.49 5.69 0 3 -20 0 15.99 4.17 0 3 20 0 15.94 4.57 0 -3 -20 0 12.36 4.89 0 4 20 0 26.42 4.37 0 4 -20 0 4.53 3.85 0 -4 -20 0 23.69 4.29 0 -4 -20 0 8.02 4.36 0 -4 20 0 8.40 4.81 0 4 20 0 28.06 4.66 0 -5 -20 0 1.49 4.14 0 5 20 0 4.15 3.85 0 -5 20 0 8.63 4.48 0 5 20 0 -14.08 4.76 0 5 -20 0 -8.21 3.77 0 -5 -20 0 -5.78 4.47 0 6 -20 0 26.31 3.82 0 6 20 0 38.27 4.97 0 -6 20 0 21.98 4.68 0 -6 -20 0 27.39 4.47 0 6 20 0 27.74 4.20 0 -6 -20 0 35.08 3.93 0 7 -20 0 3.50 3.59 0 -7 20 0 6.78 4.12 0 7 20 0 -9.74 3.47 0 7 20 0 -6.13 4.67 0 -7 -20 0 3.61 4.43 0 -7 -20 0 6.67 3.53 0 1 21 0 401.31 4.91 0 -1 -21 0 426.75 5.20 0 -1 21 0 416.31 4.96 0 -1 21 0 469.90 9.08 0 1 21 0 422.18 6.96 0 -2 21 0 138.42 4.02 0 -2 21 0 137.33 7.34 0 2 21 0 120.38 4.42 0 -2 -21 0 149.85 5.02 0 2 -21 0 131.52 4.14 0 2 21 0 135.15 5.57 0 3 -21 0 94.41 4.15 0 3 21 0 110.30 5.16 0 -3 21 0 116.47 6.10 0 -3 -21 0 129.59 5.01 0 3 21 0 105.62 4.73 0 4 -21 0 -11.20 3.78 0 -4 -21 0 2.44 3.83 0 -4 21 0 -1.80 5.02 0 4 21 0 1.21 4.40 0 4 21 0 1.49 4.36 0 5 21 0 0.47 4.68 0 -5 -21 0 2.77 3.88 0 5 21 0 3.27 4.02 0 -5 -21 0 15.26 4.71 0 -5 21 0 -6.41 4.84 0 5 -21 0 -0.44 3.77 0 6 21 0 10.81 3.43 0 6 21 0 22.66 4.45 0 -6 -21 0 1.60 3.42 0 -6 21 0 16.20 4.46 0 -6 -21 0 4.51 4.21 0 6 -21 0 22.94 3.66 0 -7 21 0 86.12 4.47 0 7 21 0 98.58 4.13 0 7 -21 0 88.23 4.37 0 7 21 0 79.38 4.61 0 -7 -21 0 77.93 3.94 0 -7 -21 0 73.44 4.92 0 0 -22 0 957.44 5.86 0 0 22 0 974.93 9.77 0 0 22 0 943.45 5.78 0 -1 22 0 15.99 6.78 0 -1 -22 0 19.83 4.14 0 -1 22 0 21.03 7.04 0 1 -22 0 28.56 3.85 0 1 22 0 13.88 3.85 0 1 22 0 21.36 5.20 0 -1 22 0 3.34 3.93 0 2 -22 0 194.91 4.12 0 2 22 0 191.54 4.43 0 2 22 0 166.45 5.72 0 -2 22 0 185.95 7.53 0 -2 -22 0 202.33 4.54 0 3 22 0 186.96 5.25 0 3 -22 0 195.26 4.30 0 3 22 0 197.13 4.54 0 -3 -22 0 205.48 4.96 0 -3 22 0 187.95 6.74 0 4 22 0 100.69 4.55 0 4 22 0 104.01 4.31 0 -4 22 0 111.47 5.84 0 -4 -22 0 131.80 4.81 0 4 -22 0 86.56 4.15 0 -5 -22 0 122.94 4.28 0 -5 22 0 125.22 5.55 0 5 22 0 112.24 4.65 0 -5 -22 0 130.80 4.68 0 5 22 0 115.17 4.39 0 5 -22 0 120.14 4.08 0 6 22 0 10.98 4.06 0 -6 22 0 11.18 4.29 0 -6 -22 0 7.87 3.54 0 6 -22 0 16.15 3.90 0 -6 -22 0 7.07 4.11 0 6 22 0 -4.18 4.20 0 -7 22 0 1.58 4.02 0 -7 -22 0 20.16 3.65 0 7 -22 0 0.08 3.69 0 7 22 0 11.88 3.49 0 7 22 0 6.35 4.36 0 -7 -22 0 9.09 4.27 0 1 23 0 -0.97 5.01 0 -1 23 0 2.23 6.47 0 1 23 0 3.94 3.71 0 -1 -23 0 2.03 5.44 0 1 -23 0 3.07 3.63 0 -1 23 0 6.32 3.60 0 -1 23 0 -1.16 6.78 0 -1 -23 0 -8.16 4.21 0 2 -23 0 34.33 3.74 0 -2 23 0 33.25 6.68 0 2 23 0 14.02 4.50 0 2 23 0 29.47 4.70 0 -2 -23 0 36.35 4.26 0 -3 -23 0 3.55 4.07 0 3 -23 0 9.13 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140.15 3.84 0 0 28 0 128.13 8.44 0 0 28 0 122.22 8.65 0 0 -28 0 134.14 4.21 0 1 -28 0 39.19 3.76 0 1 28 0 21.89 5.79 0 1 28 0 21.72 3.42 0 -1 -28 0 23.75 3.89 0 -2 -28 0 -1.28 5.08 0 2 28 0 2.44 4.00 0 2 28 0 4.89 5.02 0 -2 -28 0 -3.54 3.68 0 2 -28 0 -1.02 3.76 0 -3 -28 0 4.67 3.62 0 -3 -28 0 1.79 4.47 0 3 -28 0 12.98 3.69 0 3 28 0 7.12 4.63 0 3 28 0 -0.64 3.52 0 -4 -28 0 -4.82 4.15 0 4 28 0 16.16 4.15 0 4 -28 0 0.54 3.64 0 4 28 0 15.05 3.87 0 -4 -28 0 24.68 4.01 0 1 29 0 -9.23 3.41 0 1 29 0 0.23 5.70 0 1 -29 0 -3.06 3.71 0 -1 -29 0 3.64 3.44 0 2 -29 0 22.33 3.72 0 -2 -29 0 17.88 5.35 0 -2 -29 0 33.95 3.73 0 2 29 0 21.78 3.73 0 2 29 0 21.25 5.38 0 -3 -29 0 22.45 3.90 0 -3 -29 0 6.77 4.82 0 3 29 0 1.20 4.64 0 3 29 0 6.62 3.66 0 3 -29 0 21.07 3.61 0 0 -30 0 3.49 3.57 0 1 -30 0 -10.78 3.69 0 -1 -30 0 -4.42 3.47 0 1 30 0 -4.06 3.45 0 1 30 0 1.92 6.46 0 -2 -30 0 5.02 4.08 0 2 30 0 0.10 3.59 0 2 -30 0 0.12 3.52 0 2 30 0 7.54 5.32 0 -9 0 1 24.92 3.66 0 9 0 -1 21.37 6.90 0 9 0 -1 20.71 5.98 0 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18.93 3.64 0 8 1 1 6.10 4.59 0 -8 1 -1 6.09 3.74 0 8 -1 1 5.41 3.86 0 8 1 1 -1.01 3.65 0 9 -1 1 1.43 4.17 0 -9 1 -1 0.06 3.61 0 9 1 1 3.02 4.47 0 -9 -1 -1 14.58 3.79 0 9 1 1 -6.00 3.54 0 9 -1 1 -2.19 4.09 0 10 -2 -1 18.08 5.81 0 10 2 -1 12.68 3.72 0 10 -2 -1 19.15 3.82 0 -10 -2 1 -3.67 3.56 0 -10 2 1 15.56 3.70 0 10 -2 -1 18.98 6.20 0 -9 -2 1 8.06 3.58 0 -9 2 1 13.71 3.67 0 9 2 -1 8.44 3.80 0 9 -2 -1 1.17 6.15 0 9 -2 -1 3.55 5.21 0 9 2 -1 6.23 7.48 0 9 -2 -1 -1.26 3.76 0 9 2 -1 3.44 6.88 0 8 -2 -1 178.32 6.47 0 8 2 -1 163.81 7.52 0 8 -2 -1 179.90 4.13 0 8 2 -1 159.11 8.02 0 8 -2 -1 162.66 5.88 0 -8 -2 1 163.28 4.00 0 -8 2 1 167.62 4.01 0 8 2 -1 195.02 4.09 0 -7 -2 1 -3.48 3.76 0 7 -2 -1 1.29 3.69 0 7 2 -1 2.07 6.98 0 7 2 -1 -2.54 3.84 0 -7 2 1 -0.80 3.88 0 7 -2 -1 -0.18 5.87 0 7 2 -1 4.24 6.88 0 7 -2 -1 -1.86 5.40 0 6 2 -1 219.51 7.74 0 6 2 -1 246.48 4.49 0 6 -2 -1 240.21 4.87 0 -6 2 1 222.71 4.67 0 6 -2 -1 205.03 6.97 0 -6 -2 1 217.33 4.42 0 5 -2 -1 130.59 6.53 0 5 -2 -1 123.21 4.62 0 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32.10 4.06 0 9 -4 -2 49.45 6.13 0 9 -4 -2 64.79 3.81 0 -9 -4 2 42.57 3.99 0 9 -4 -2 53.11 5.84 0 -8 4 2 280.34 4.58 0 8 -4 -2 301.27 4.46 0 -8 -4 2 284.05 4.12 0 8 4 -2 325.60 4.37 0 8 -4 -2 276.37 6.85 0 7 -4 -2 4.85 6.20 0 7 4 -2 -6.02 4.03 0 7 -4 -2 3.08 3.83 0 -7 4 2 -10.84 3.75 0 -7 -4 2 1.65 3.89 0 6 4 -2 89.61 4.36 0 6 -4 -2 98.18 4.80 0 -6 -4 2 83.08 4.27 0 -6 4 2 83.98 4.53 0 6 -4 -2 98.82 6.68 0 5 4 -2 74.40 4.65 0 -5 -4 2 81.78 5.02 0 5 -4 -2 71.32 6.44 0 5 -4 -2 79.49 4.64 0 -5 4 2 84.20 4.63 0 -4 -4 2 1612.46 8.00 0 4 -4 -2 1858.04 8.23 0 4 -4 -2 1605.51 10.60 0 -4 4 2 1676.17 8.04 0 -4 4 2 1515.58 10.29 0 4 4 -2 1660.37 8.17 0 -3 -4 2 0.29 6.02 0 -3 4 2 -1.17 5.21 0 3 -4 -2 -3.18 6.48 0 -3 4 2 -5.20 6.72 0 -3 -4 2 1.72 11.83 0 3 4 -2 5.85 5.15 0 2 -4 -2 1991.17 11.61 0 2 4 -2 2274.96 11.54 0 -2 -4 2 2128.20 11.61 0 -2 4 2 1939.79 11.23 0 -1 4 2 43.98 7.04 0 1 -4 -2 48.26 7.05 0 -1 -4 2 49.87 7.91 0 1 -4 -2 44.59 6.38 0 -1 4 2 45.54 6.48 0 0 -4 -2 7717.91 18.03 0 0 4 2 7838.83 18.40 0 0 -4 -2 7835.63 18.56 0 0 4 2 8055.23 18.75 0 -1 4 -2 1243.26 10.36 0 1 4 2 1286.87 8.50 0 1 -4 2 1227.82 10.51 0 -1 -4 -2 1280.23 8.53 0 1 4 2 1255.32 8.57 0 -1 -4 -2 1283.76 7.93 0 2 4 2 723.08 7.04 0 2 4 2 735.87 6.90 0 -2 4 -2 683.47 7.20 0 -2 -4 -2 742.86 7.00 0 2 -4 2 743.63 7.42 0 -2 -4 -2 719.97 6.81 0 3 -4 2 48.82 5.61 0 3 4 2 39.40 5.55 0 -3 -4 -2 34.12 4.92 0 -3 4 -2 37.70 4.93 0 -3 -4 -2 45.30 5.38 0 3 4 2 46.18 4.73 0 -4 4 -2 964.45 7.18 0 -4 -4 -2 938.93 6.42 0 4 -4 2 962.02 7.32 0 4 4 2 947.70 7.31 0 4 4 2 926.34 6.38 0 5 4 2 -0.82 4.81 0 -5 -4 -2 4.49 3.96 0 -5 4 -2 15.84 4.39 0 5 -4 2 -16.09 4.71 0 5 4 2 3.09 3.99 0 6 4 2 1505.16 8.03 0 -6 -4 -2 1481.72 6.80 0 6 4 2 1538.42 6.81 0 6 -4 2 1523.07 7.76 0 -6 4 -2 1523.52 7.39 0 6 -4 2 1552.92 7.12 0 -7 4 -2 22.01 4.51 0 7 4 2 11.84 3.77 0 7 -4 2 -0.34 4.37 0 -7 -4 -2 10.95 3.64 0 7 -4 2 7.55 3.78 0 7 4 2 2.64 4.23 0 8 -4 2 70.28 4.19 0 8 4 2 81.83 4.02 0 -8 4 -2 89.86 3.98 0 8 -4 2 89.31 3.87 0 -8 -4 -2 93.77 3.94 0 9 -4 2 11.42 4.02 0 -9 -4 -2 21.32 3.38 0 -9 4 -2 32.78 3.77 0 9 -4 2 9.88 4.14 0 9 -4 2 4.15 3.78 0 9 4 2 32.93 3.69 0 10 -5 -2 -7.78 5.91 0 10 5 -2 1.86 3.90 0 10 -5 -2 -1.47 5.45 0 -10 -5 2 -0.83 3.48 0 -10 5 2 1.05 3.50 0 10 -5 -2 -6.60 3.81 0 9 -5 -2 8.03 5.56 0 9 -5 -2 21.48 3.63 0 9 5 -2 16.59 3.49 0 -9 -5 2 21.02 3.65 0 -9 5 2 4.87 3.65 0 9 -5 -2 17.75 5.26 0 8 5 -2 16.96 3.73 0 -8 -5 2 33.86 3.58 0 8 -5 -2 15.16 5.64 0 -8 5 2 28.47 3.68 0 8 -5 -2 18.40 3.57 0 -7 -5 2 22.38 4.05 0 7 -5 -2 28.22 5.92 0 7 5 -2 12.97 4.13 0 7 -5 -2 35.66 4.24 0 -7 5 2 33.93 3.81 0 6 5 -2 14.35 4.32 0 6 -5 -2 12.49 5.87 0 6 -5 -2 22.83 4.35 0 -6 5 2 19.02 4.30 0 -6 -5 2 29.48 4.16 0 5 5 -2 85.82 4.80 0 -5 -5 2 77.19 4.61 0 -5 5 2 76.24 4.78 0 5 -5 -2 84.97 4.44 0 5 -5 -2 77.42 6.03 0 4 -5 -2 -6.96 6.32 0 -4 5 2 0.07 4.70 0 -4 -5 2 4.26 4.72 0 4 5 -2 -6.13 4.78 0 -4 5 2 0.79 6.19 0 -3 -5 2 375.41 6.35 0 3 5 -2 406.13 6.34 0 -3 5 2 408.16 7.98 0 3 -5 -2 359.82 7.13 0 -3 -5 2 392.37 10.97 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347.46 4.57 0 -7 7 2 283.09 4.55 0 7 -7 -2 335.40 4.68 0 -7 -7 2 295.92 4.67 0 6 7 -2 11.44 4.23 0 -6 7 2 6.53 4.25 0 6 -7 -2 8.21 4.44 0 -6 -7 2 11.08 4.12 0 6 -7 -2 -3.70 5.41 0 -5 7 2 274.94 5.04 0 5 7 -2 301.06 5.25 0 -5 -7 2 285.96 5.13 0 5 -7 -2 298.73 6.15 0 -4 -7 2 16.17 4.39 0 -4 7 2 5.93 5.09 0 -4 7 2 15.62 5.59 0 -4 -7 2 13.32 7.76 0 4 7 -2 1.69 4.69 0 4 -7 -2 9.71 5.86 0 -3 -7 2 7.74 6.97 0 3 -7 -2 5.01 6.07 0 -3 7 2 9.02 6.35 0 3 7 -2 14.31 5.90 0 -3 -7 2 10.11 5.02 0 -3 7 2 4.39 5.01 0 -2 7 2 378.57 6.14 0 2 7 -2 413.43 7.45 0 2 -7 -2 402.90 6.48 0 -2 -7 2 381.43 7.31 0 1 -7 -2 180.43 6.10 0 -1 -7 2 183.60 8.45 0 -1 7 2 162.61 6.27 0 1 -7 -2 184.67 5.91 0 -1 -7 2 171.22 6.62 0 0 7 2 200.55 5.65 0 0 -7 2 209.42 12.60 0 0 7 2 219.55 6.30 0 0 -7 -2 215.78 6.64 0 0 -7 -2 220.31 6.11 0 1 7 2 870.14 7.25 0 1 7 2 856.65 7.36 0 -1 7 -2 852.40 10.79 0 -1 -7 -2 880.42 7.31 0 -1 -7 -2 886.75 7.44 0 1 -7 2 898.62 10.98 0 2 -7 2 142.54 6.75 0 -2 -7 -2 133.82 5.19 0 2 7 2 135.08 5.44 0 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621.87 6.89 0 1 -9 -2 678.95 7.67 0 -1 -9 2 635.95 11.62 0 0 9 2 795.54 7.30 0 0 -9 -2 876.61 7.02 0 0 9 2 807.19 6.98 0 0 -9 -2 850.10 8.13 0 0 -9 2 771.59 6.86 0 -1 -9 -2 477.07 6.16 0 1 -9 2 486.04 10.99 0 1 9 2 449.15 6.10 0 -1 -9 -2 461.65 6.21 0 1 9 2 447.06 6.10 0 2 9 2 270.49 5.43 0 2 9 2 265.19 5.18 0 -2 -9 -2 292.48 5.33 0 2 -9 2 305.35 7.24 0 -2 -9 -2 299.93 5.38 0 -2 9 -2 281.40 7.26 0 3 9 2 -5.75 4.37 0 -3 -9 -2 -1.09 4.55 0 -3 -9 -2 0.02 4.62 0 -3 9 -2 0.56 5.08 0 3 9 2 -4.13 5.47 0 3 -9 2 3.99 5.05 0 4 9 2 -2.02 4.94 0 -4 -9 -2 9.76 4.17 0 4 -9 2 4.22 4.63 0 -4 -9 -2 4.27 4.20 0 4 9 2 4.09 4.30 0 -4 9 -2 4.93 4.84 0 5 9 2 -6.08 3.96 0 5 9 2 7.40 4.75 0 -5 -9 -2 -1.46 4.55 0 5 -9 2 5.67 4.61 0 -5 -9 -2 -8.41 3.94 0 -5 9 -2 9.16 4.85 0 6 -9 2 91.38 4.45 0 6 9 2 86.87 3.91 0 -6 -9 -2 82.54 3.88 0 -6 9 -2 83.09 4.77 0 -7 -9 -2 11.40 3.51 0 7 9 2 -1.69 3.96 0 -7 9 -2 -0.25 3.85 0 7 -9 2 3.70 4.21 0 7 -9 2 14.53 4.30 0 8 -9 2 29.80 3.49 0 -8 -9 -2 31.15 3.70 0 8 -9 2 1.61 3.63 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731.42 5.66 0 5 1 -3 7.54 4.46 0 5 -1 -3 1.98 7.73 0 5 -1 -3 7.38 4.44 0 -5 -1 3 -4.23 4.24 0 -5 1 3 5.56 4.41 0 4 1 -3 3738.92 10.85 0 -4 1 3 3404.19 10.37 0 -4 1 3 3613.66 19.46 0 4 -1 -3 3378.60 17.57 0 -4 -1 3 3411.74 10.43 0 -3 -1 3 17.35 5.32 0 -3 1 3 16.85 7.53 0 3 -1 -3 19.59 6.41 0 -3 -1 3 20.56 7.72 0 -3 1 3 9.23 5.40 0 2 1 -3 8.10 6.47 0 2 -1 -3 10.58 5.84 0 -2 -1 3 10.74 6.19 0 -2 1 3 4.14 6.18 0 -1 1 3 53.83 5.97 0 1 -1 -3 65.27 6.49 0 -1 -1 3 57.31 5.71 0 1 -1 -3 74.52 5.63 0 -1 1 3 61.62 5.54 0 -1 -1 3 63.50 5.83 0 0 -1 3 307.46 6.29 0 0 -1 -3 293.18 5.96 0 0 1 3 300.84 5.29 0 0 1 3 314.30 6.18 0 0 1 -3 307.24 6.45 0 0 -1 -3 323.88 6.20 0 0 -1 3 305.81 6.48 0 -1 -1 -3 27.33 5.31 0 1 1 3 36.09 5.37 0 1 -1 3 39.83 5.91 0 1 -1 3 26.07 5.23 0 -1 -1 -3 32.77 5.10 0 1 1 3 32.00 5.09 0 -1 1 -3 32.64 5.21 0 -2 -1 -3 4.68 4.85 0 2 1 3 1.86 4.71 0 2 1 3 4.88 4.87 0 2 -1 3 3.73 4.62 0 2 -1 3 -1.28 5.09 0 -2 1 -3 -9.80 4.88 0 -3 -1 -3 408.97 5.48 0 -3 1 -3 377.03 5.38 0 3 1 3 401.80 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15.98 8.62 0 6 -2 -3 408.86 9.22 0 -6 -2 3 403.83 4.94 0 6 2 -3 467.15 5.14 0 -6 2 3 409.17 4.97 0 6 -2 -3 441.95 5.07 0 5 2 -3 25.55 4.47 0 5 -2 -3 24.15 4.48 0 -5 2 3 30.03 4.24 0 -5 -2 3 16.32 4.45 0 5 -2 -3 25.94 6.71 0 -4 -2 3 213.39 5.33 0 4 -2 -3 211.27 7.41 0 -4 2 3 202.86 5.33 0 4 2 -3 224.60 5.36 0 -4 2 3 212.55 8.74 0 -3 -2 3 265.55 5.82 0 -3 2 3 243.71 7.72 0 3 -2 -3 248.56 6.68 0 -3 -2 3 251.54 8.73 0 -3 2 3 283.62 5.84 0 -2 2 3 35.39 6.36 0 2 -2 -3 33.67 5.92 0 -2 -2 3 26.91 6.85 0 1 -2 -3 8.15 5.39 0 -1 -2 3 15.19 5.57 0 -1 -2 3 10.08 5.63 0 1 -2 -3 8.07 5.30 0 -1 2 3 22.65 5.23 0 -1 2 3 16.21 5.74 0 0 -2 -3 2402.66 10.09 0 0 -2 3 2337.65 10.14 0 0 -2 3 2464.59 11.82 0 0 2 -3 2377.94 11.52 0 0 -2 -3 2431.37 10.31 0 0 2 3 2296.16 10.21 0 0 2 3 2352.36 10.26 0 -1 -2 -3 100.76 5.48 0 -1 2 -3 99.79 5.48 0 1 2 3 93.29 5.43 0 1 -2 3 88.07 5.44 0 1 2 3 97.79 5.44 0 -1 -2 -3 94.42 5.23 0 1 -2 3 91.87 5.35 0 2 -2 3 485.77 5.85 0 2 2 3 487.06 5.89 0 -2 -2 -3 477.58 5.95 0 -2 -2 -3 510.83 5.85 0 2 -2 3 506.35 6.94 0 2 2 3 488.01 5.97 0 -2 2 -3 482.64 6.69 0 -3 -2 -3 194.76 5.04 0 3 2 3 194.63 4.75 0 -3 2 -3 195.95 5.53 0 3 -2 3 197.95 4.70 0 3 2 3 186.73 5.06 0 3 -2 3 198.82 4.95 0 -4 2 -3 223.47 5.07 0 -4 -2 -3 233.40 4.85 0 4 -2 3 239.68 5.33 0 4 2 3 248.15 5.38 0 4 -2 3 237.61 5.03 0 4 2 3 239.36 4.99 0 5 -2 3 414.98 5.12 0 5 -2 3 408.61 5.70 0 5 2 3 395.23 5.16 0 -5 2 -3 418.26 5.21 0 5 2 3 413.45 5.27 0 -5 -2 -3 407.20 4.86 0 6 -2 3 206.26 4.52 0 -6 -2 -3 202.01 4.36 0 -6 2 -3 206.95 4.55 0 6 -2 3 212.63 4.29 0 6 2 3 206.38 5.02 0 6 2 3 212.17 4.40 0 7 -2 3 4.70 3.53 0 -7 -2 -3 2.86 3.65 0 -7 2 -3 12.04 3.75 0 7 2 3 3.92 3.87 0 7 -2 3 18.26 3.56 0 -8 -2 -3 12.51 3.56 0 -8 2 -3 24.14 4.07 0 8 2 3 4.73 3.85 0 8 -2 3 29.11 3.50 0 8 -2 3 1.96 3.87 0 10 -3 -3 20.16 3.60 0 10 3 -3 27.70 3.60 0 -10 3 3 22.58 3.82 0 -10 -3 3 36.16 3.76 0 9 3 -3 21.23 3.91 0 -9 3 3 19.20 3.65 0 9 -3 -3 26.89 3.74 0 -9 -3 3 32.28 3.54 0 -8 -3 3 24.71 3.82 0 8 -3 -3 17.36 7.42 0 8 3 -3 20.33 3.86 0 -8 3 3 25.45 3.75 0 8 -3 -3 21.75 7.16 0 8 -3 -3 17.06 3.77 0 7 -3 -3 45.64 7.43 0 -7 -3 3 52.17 3.96 0 7 3 -3 51.32 4.12 0 -7 3 3 46.29 4.06 0 7 -3 -3 50.31 4.04 0 -6 -3 3 31.55 4.09 0 6 3 -3 45.45 4.28 0 6 -3 -3 18.52 4.24 0 -6 3 3 25.79 4.18 0 6 -3 -3 28.15 6.68 0 -5 3 3 81.01 4.67 0 5 3 -3 102.75 5.09 0 5 -3 -3 95.91 6.32 0 -5 -3 3 99.26 4.65 0 4 -3 -3 156.58 6.31 0 4 3 -3 180.10 5.08 0 -4 3 3 169.60 7.34 0 -4 3 3 157.79 5.00 0 -4 -3 3 163.78 4.97 0 3 -3 -3 -1.21 6.23 0 -3 3 3 0.61 5.99 0 -3 3 3 9.31 5.07 0 -3 -3 3 7.15 7.13 0 -3 -3 3 11.37 5.65 0 -2 -3 3 642.76 7.34 0 -2 3 3 537.59 7.14 0 -2 -3 3 546.91 8.64 0 -2 3 3 566.02 6.57 0 2 -3 -3 562.42 7.46 0 1 -3 -3 189.98 5.80 0 1 -3 -3 188.42 5.88 0 -1 -3 3 193.05 6.78 0 -1 3 3 200.03 5.91 0 -1 3 3 186.82 5.97 0 0 -3 3 6.77 6.17 0 0 -3 -3 1.19 5.35 0 0 3 3 2.88 4.61 0 0 3 -3 -1.04 6.12 0 0 -3 -3 1.15 5.48 0 0 3 3 -6.69 5.52 0 -1 3 -3 459.62 7.07 0 1 -3 3 451.34 7.14 0 1 3 3 426.71 6.20 0 -1 -3 -3 461.59 6.10 0 1 3 3 439.82 6.15 0 -1 -3 -3 466.04 6.28 0 -2 -3 -3 5.25 4.84 0 -2 3 -3 9.59 4.95 0 2 -3 3 4.49 5.05 0 2 3 3 -3.61 4.86 0 -2 -3 -3 4.20 4.59 0 2 3 3 6.84 4.70 0 -3 -3 -3 38.99 4.56 0 -3 3 -3 43.86 4.68 0 3 3 3 36.11 4.39 0 3 -3 3 23.24 5.46 0 3 -3 3 46.69 4.43 0 3 3 3 49.33 4.56 0 4 -3 3 11.57 4.47 0 -4 -3 -3 1.79 4.25 0 -4 3 -3 0.06 4.40 0 4 3 3 -1.73 4.34 0 4 -3 3 2.50 4.19 0 4 3 3 -7.87 4.37 0 5 3 3 63.06 3.99 0 -5 -3 -3 71.65 4.13 0 5 3 3 60.52 4.29 0 -5 3 -3 67.80 4.83 0 5 -3 3 62.39 4.29 0 5 -3 3 71.80 4.29 0 -6 -3 -3 172.83 4.34 0 6 3 3 176.99 4.24 0 6 3 3 173.01 4.70 0 6 -3 3 179.73 4.65 0 6 -3 3 158.75 4.23 0 -6 3 -3 177.04 4.61 0 -7 3 -3 21.36 3.94 0 7 -3 3 17.50 3.81 0 7 3 3 31.30 3.76 0 7 -3 3 15.13 3.86 0 -7 -3 -3 23.63 3.73 0 -8 -3 -3 272.91 4.40 0 -8 3 -3 252.87 4.49 0 8 -3 3 277.47 4.92 0 8 3 3 277.14 4.64 0 8 -3 3 298.10 4.26 0 -10 4 3 70.75 3.83 0 10 4 -3 42.84 3.93 0 10 -4 -3 47.84 4.05 0 -10 -4 3 48.49 3.74 0 9 -4 -3 1.85 7.01 0 9 4 -3 22.26 3.65 0 9 -4 -3 5.26 6.73 0 -9 4 3 4.16 3.61 0 9 -4 -3 -8.35 3.74 0 -9 -4 3 8.73 3.02 0 8 -4 -3 3.90 3.70 0 -8 -4 3 0.03 3.57 0 -8 4 3 -5.84 3.64 0 8 -4 -3 9.10 6.43 0 8 4 -3 13.86 3.67 0 -7 -4 3 29.58 3.93 0 -7 4 3 27.63 4.04 0 7 4 -3 27.80 4.18 0 7 -4 -3 36.27 4.17 0 7 -4 -3 27.32 6.75 0 6 -4 -3 138.62 4.42 0 6 4 -3 106.66 4.50 0 6 -4 -3 96.91 6.84 0 -6 -4 3 103.20 4.42 0 -6 4 3 107.20 4.28 0 -5 4 3 279.56 4.93 0 -5 4 3 275.97 6.55 0 5 -4 -3 282.57 6.87 0 5 4 -3 292.25 5.31 0 -5 -4 3 285.23 5.48 0 -4 4 3 540.29 6.03 0 4 4 -3 600.97 6.14 0 -4 4 3 588.76 8.04 0 -4 -4 3 565.78 6.03 0 4 -4 -3 538.08 7.47 0 -3 4 3 358.40 6.02 0 -3 4 3 335.34 7.69 0 3 -4 -3 326.18 6.82 0 -3 -4 3 353.41 6.04 0 -3 -4 3 333.64 8.62 0 -2 4 3 4.55 5.07 0 -2 4 3 -4.26 6.19 0 -2 -4 3 -4.31 6.21 0 2 -4 -3 -2.00 6.00 0 -1 4 3 4.99 5.55 0 1 -4 -3 -0.92 5.21 0 1 -4 -3 -1.35 5.59 0 -1 -4 3 -9.07 5.96 0 -1 4 3 1.84 5.42 0 0 -4 3 2017.33 12.18 0 0 -4 -3 1988.16 9.21 0 0 4 -3 1973.36 11.35 0 0 4 3 1973.98 9.39 0 0 -4 -3 2041.18 9.46 0 0 4 3 1998.06 9.46 0 -1 4 -3 36.16 5.59 0 -1 -4 -3 25.44 4.94 0 1 -4 3 30.61 5.91 0 -1 -4 -3 36.66 5.00 0 1 4 3 39.78 5.09 0 1 4 3 27.86 5.14 0 2 4 3 1696.55 8.09 0 2 4 3 1650.23 8.08 0 -2 -4 -3 1661.96 8.12 0 -2 4 -3 1622.00 9.32 0 -2 -4 -3 1687.37 8.27 0 2 -4 3 1716.84 9.61 0 3 4 3 20.49 4.37 0 -3 4 -3 19.23 5.26 0 -3 -4 -3 22.44 4.76 0 3 4 3 13.71 4.35 0 -3 -4 -3 2.80 4.58 0 3 -4 3 14.00 5.24 0 4 -4 3 35.80 4.48 0 -4 -4 -3 41.55 4.35 0 4 4 3 38.13 4.39 0 -4 4 -3 37.99 4.93 0 4 -4 3 42.82 4.26 0 4 4 3 33.10 4.34 0 5 -4 3 6.21 4.13 0 5 4 3 7.32 4.08 0 -5 -4 -3 3.52 3.77 0 5 4 3 9.00 3.96 0 5 -4 3 10.27 4.03 0 -5 4 -3 0.53 4.19 0 6 4 3 172.42 4.18 0 -6 -4 -3 147.63 4.13 0 -6 4 -3 175.96 4.88 0 6 -4 3 174.59 4.30 0 6 -4 3 162.79 4.26 0 6 4 3 171.83 4.64 0 -7 4 -3 7.08 3.88 0 7 4 3 15.93 3.72 0 -7 -4 -3 7.94 3.52 0 7 -4 3 2.10 3.51 0 7 -4 3 1.09 4.26 0 -8 4 -3 -1.71 3.84 0 8 -4 3 -11.57 3.89 0 8 4 3 8.44 3.75 0 -8 -4 -3 -4.79 3.58 0 8 -4 3 -2.93 3.68 0 10 -5 -3 3.98 7.40 0 10 5 -3 -1.71 3.75 0 10 -5 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62.63 5.36 0 0 5 3 57.59 5.55 0 0 -5 -3 44.19 5.47 0 -1 5 -3 16.82 5.64 0 1 5 3 10.40 4.84 0 1 5 3 12.11 5.09 0 -1 -5 -3 17.71 4.90 0 1 -5 3 13.36 6.57 0 -1 -5 -3 24.83 4.81 0 2 5 3 49.68 4.81 0 -2 -5 -3 36.80 4.94 0 2 5 3 48.29 4.93 0 -2 -5 -3 40.62 4.73 0 -2 5 -3 49.85 5.79 0 2 -5 3 45.04 5.93 0 3 5 3 51.62 5.16 0 3 5 3 44.62 4.52 0 -3 -5 -3 30.46 4.59 0 -3 -5 -3 50.65 4.93 0 -3 5 -3 42.15 4.65 0 3 -5 3 51.01 4.65 0 4 -5 3 71.80 4.50 0 4 5 3 57.03 4.45 0 -4 5 -3 58.64 5.03 0 -4 -5 -3 60.70 4.41 0 -4 -5 -3 58.86 4.43 0 4 5 3 63.59 4.34 0 -5 -5 -3 74.46 4.49 0 5 -5 3 102.57 4.33 0 -5 5 -3 80.76 4.84 0 5 -5 3 85.27 4.19 0 5 5 3 81.09 4.45 0 5 5 3 91.18 4.22 0 -6 -5 -3 29.55 3.75 0 -6 5 -3 28.18 3.98 0 6 5 3 27.53 4.45 0 6 -5 3 22.67 4.11 0 6 -5 3 29.74 3.82 0 6 5 3 24.99 3.94 0 7 -5 3 10.19 3.77 0 -7 5 -3 -6.07 3.89 0 7 -5 3 9.50 4.07 0 -7 -5 -3 -3.14 3.71 0 7 5 3 23.92 3.71 0 -8 -5 -3 124.13 3.86 0 -8 5 -3 123.99 4.18 0 8 5 3 115.43 4.00 0 8 -5 3 110.36 4.23 0 8 -5 3 101.34 4.17 0 10 -6 -3 37.57 6.17 0 10 6 -3 25.24 3.67 0 10 -6 -3 35.97 6.28 0 -10 6 3 33.43 3.82 0 -10 -6 3 40.78 3.76 0 9 -6 -3 2.01 5.58 0 9 6 -3 -4.51 3.81 0 -9 6 3 11.51 3.56 0 -9 -6 3 12.25 3.54 0 8 -6 -3 84.67 5.95 0 -8 6 3 93.21 3.80 0 8 6 -3 80.28 4.04 0 -8 -6 3 84.43 3.89 0 7 6 -3 13.81 4.25 0 -7 6 3 0.66 3.75 0 -7 -6 3 7.77 3.74 0 7 -6 -3 3.93 5.73 0 6 6 -3 1462.16 7.12 0 6 -6 -3 1310.59 9.12 0 -6 6 3 1337.54 6.68 0 -6 -6 3 1286.94 6.66 0 5 6 -3 39.94 4.73 0 -5 6 3 27.46 4.38 0 -5 -6 3 43.33 4.46 0 -5 6 3 36.67 5.18 0 5 -6 -3 38.83 5.58 0 -4 6 3 48.58 4.70 0 4 -6 -3 55.59 5.57 0 -4 -6 3 53.82 4.58 0 -4 -6 3 51.51 9.45 0 4 6 -3 51.11 5.23 0 -4 6 3 51.67 6.18 0 3 6 -3 284.37 6.55 0 -3 6 3 242.56 6.84 0 -3 -6 3 251.87 5.76 0 3 -6 -3 241.95 5.91 0 -2 6 3 1990.81 9.61 0 -2 -6 3 2129.48 11.26 0 2 -6 -3 2054.01 9.56 0 -1 6 3 542.44 6.63 0 1 -6 -3 541.39 6.53 0 -1 -6 3 562.29 8.82 0 -1 6 3 538.31 6.46 0 1 -6 -3 557.38 6.63 0 0 6 3 3866.33 11.81 0 0 -6 -3 3865.85 11.68 0 0 6 3 3744.64 11.53 0 0 -6 -3 3817.41 10.87 0 0 6 -3 3833.35 16.23 0 -1 -6 -3 62.70 4.89 0 1 6 3 50.11 4.97 0 1 -6 3 53.19 6.50 0 1 6 3 42.81 5.17 0 -1 -6 -3 53.04 5.01 0 -1 6 -3 37.75 5.67 0 -2 -6 -3 850.74 6.43 0 -2 6 -3 799.92 7.76 0 -2 -6 -3 830.06 6.41 0 2 6 3 819.42 6.53 0 2 6 3 823.92 6.46 0 2 -6 3 825.23 7.98 0 -3 -6 -3 237.22 4.86 0 -3 6 -3 214.24 5.47 0 -3 -6 -3 208.69 5.10 0 3 -6 3 237.23 5.64 0 3 6 3 229.68 4.90 0 3 6 3 240.42 5.16 0 -4 6 -3 960.46 6.61 0 4 -6 3 984.46 7.03 0 4 6 3 980.22 6.48 0 -4 -6 -3 993.90 6.82 0 4 6 3 980.28 5.99 0 -4 -6 -3 1022.32 6.06 0 -5 -6 -3 14.17 3.70 0 5 6 3 1.39 4.62 0 -5 6 -3 -8.13 4.64 0 5 6 3 -8.33 3.94 0 5 -6 3 6.85 4.01 0 -6 -6 -3 205.84 4.19 0 -6 6 -3 197.19 4.58 0 6 6 3 194.76 4.25 0 6 6 3 224.00 4.28 0 6 -6 3 216.98 4.67 0 6 -6 3 216.06 4.98 0 -7 -6 -3 6.99 3.89 0 7 6 3 9.50 3.75 0 -7 6 -3 12.67 4.19 0 7 -6 3 5.54 3.60 0 7 -6 3 29.70 3.69 0 -8 -6 -3 18.49 3.82 0 -8 6 -3 37.70 4.10 0 8 6 3 6.61 4.14 0 8 -6 3 17.69 3.97 0 8 -6 3 33.62 3.68 0 10 -7 -3 60.05 6.21 0 10 7 -3 58.75 4.04 0 10 -7 -3 70.45 5.95 0 -10 -7 3 75.36 3.71 0 -10 7 3 79.29 3.86 0 9 -7 -3 75.36 5.89 0 9 7 -3 81.56 3.85 0 -9 7 3 61.91 3.83 0 -9 -7 3 65.43 3.80 0 -8 -7 3 27.30 3.71 0 -8 7 3 20.38 3.77 0 8 -7 -3 12.40 5.30 0 8 7 -3 24.91 3.74 0 7 7 -3 74.17 4.06 0 -7 7 3 52.21 3.92 0 -7 -7 3 42.15 3.93 0 7 -7 -3 55.18 5.40 0 6 -7 -3 44.52 5.51 0 6 7 -3 44.51 4.67 0 -6 7 3 53.41 4.24 0 -6 -7 3 48.37 4.49 0 5 -7 -3 116.85 5.27 0 -5 7 3 124.64 4.74 0 -5 7 3 129.18 5.33 0 -5 -7 3 126.24 5.22 0 5 7 -3 139.65 5.01 0 -4 7 3 197.99 5.02 0 -4 -7 3 185.30 5.11 0 -4 7 3 182.19 6.58 0 -4 -7 3 194.12 8.71 0 4 7 -3 197.21 5.80 0 4 -7 -3 193.59 5.87 0 3 7 -3 295.54 5.99 0 3 -7 -3 238.43 6.49 0 -3 7 3 253.36 6.62 0 -3 -7 3 247.32 5.79 0 -2 7 3 52.84 5.33 0 -2 -7 3 55.61 6.64 0 2 -7 -3 50.56 5.09 0 -1 7 3 296.03 6.00 0 1 -7 -3 273.32 5.75 0 -1 7 3 283.28 5.62 0 1 -7 -3 278.90 5.81 0 -1 -7 3 275.83 7.55 0 0 7 3 1180.41 7.64 0 0 7 3 1134.03 7.49 0 0 -7 -3 1194.24 7.49 0 0 7 -3 1143.63 10.87 0 0 -7 -3 1125.11 7.72 0 1 7 3 418.04 5.94 0 -1 -7 -3 405.56 5.76 0 1 7 3 422.06 5.78 0 1 -7 3 408.39 7.56 0 -1 7 -3 414.53 7.25 0 -1 -7 -3 437.99 5.97 0 2 -7 3 188.07 5.99 0 -2 -7 -3 182.11 5.07 0 -2 7 -3 168.79 6.28 0 -2 -7 -3 197.53 5.26 0 2 7 3 192.30 5.52 0 2 7 3 185.62 4.98 0 3 -7 3 104.80 5.34 0 3 7 3 106.06 4.85 0 -3 7 -3 95.12 5.31 0 -3 -7 -3 108.58 5.17 0 3 7 3 99.85 4.58 0 -3 -7 -3 95.91 4.67 0 -4 -7 -3 7.63 3.96 0 -4 7 -3 -5.36 4.81 0 -4 -7 -3 1.57 4.81 0 4 7 3 11.73 4.25 0 4 7 3 9.74 3.94 0 4 -7 3 -1.79 4.97 0 5 7 3 517.72 5.82 0 -5 -7 -3 481.23 4.82 0 -5 7 -3 477.28 5.52 0 5 -7 3 506.07 5.74 0 5 7 3 473.16 4.93 0 6 7 3 98.58 4.59 0 6 7 3 70.04 3.92 0 -6 7 -3 75.63 4.20 0 6 -7 3 79.98 3.92 0 6 -7 3 94.82 4.62 0 -6 -7 -3 83.93 3.90 0 7 7 3 -2.23 3.85 0 -7 -7 -3 24.58 3.82 0 7 -7 3 0.20 4.18 0 -7 7 -3 14.28 4.08 0 7 -7 3 3.93 3.92 0 -8 -7 -3 11.62 3.76 0 -8 7 -3 8.20 4.09 0 8 -7 3 12.93 4.11 0 8 -7 3 18.74 3.62 0 8 7 3 -11.90 3.90 0 10 -8 -3 21.55 5.64 0 10 8 -3 19.11 3.88 0 -10 -8 3 18.57 3.63 0 -10 8 3 20.35 3.59 0 9 8 -3 141.93 4.17 0 9 -8 -3 111.44 5.81 0 -9 8 3 118.86 3.77 0 -9 -8 3 130.45 3.82 0 -8 8 3 115.26 4.32 0 -8 -8 3 107.25 3.97 0 8 -8 -3 121.59 5.46 0 8 8 -3 138.99 4.18 0 7 -8 -3 -1.25 5.31 0 -7 8 3 -7.48 3.68 0 7 8 -3 8.49 3.90 0 -7 -8 3 0.01 3.63 0 6 -8 -3 32.54 5.02 0 -6 8 3 37.46 4.22 0 6 8 -3 52.02 4.38 0 5 -8 -3 8.61 4.93 0 -5 -8 3 1.69 4.25 0 -5 8 3 3.71 4.85 0 5 8 -3 6.83 4.99 0 -5 8 3 7.51 4.34 0 -4 -8 3 183.71 8.15 0 -4 8 3 181.50 5.63 0 4 -8 -3 172.36 5.12 0 4 8 -3 202.75 5.89 0 -4 8 3 172.11 4.95 0 3 -8 -3 339.72 5.79 0 -3 -8 3 347.55 6.61 0 -3 8 3 344.71 6.50 0 3 8 -3 399.96 6.78 0 -2 8 3 -2.96 5.16 0 -2 -8 3 10.60 6.15 0 2 -8 -3 10.14 4.84 0 -2 -8 3 4.47 5.51 0 1 -8 -3 106.68 5.26 0 1 -8 -3 102.55 5.90 0 -1 -8 3 101.15 7.10 0 -1 -8 3 116.97 7.30 0 -1 8 3 103.86 5.07 0 -1 8 3 106.73 5.48 0 0 8 3 1788.59 8.49 0 0 8 3 1738.76 8.41 0 0 -8 -3 1866.85 8.50 0 0 -8 -3 1882.23 9.11 0 -1 -8 -3 1188.47 7.28 0 -1 8 -3 1159.34 10.26 0 1 8 3 1155.55 7.19 0 1 -8 3 1197.26 10.56 0 1 8 3 1156.50 7.18 0 -1 -8 -3 1215.44 7.74 0 2 -8 3 18.51 5.60 0 -2 -8 -3 23.90 4.51 0 2 8 3 18.12 4.59 0 -2 -8 -3 1.64 4.44 0 2 8 3 11.81 4.46 0 -2 8 -3 11.91 5.41 0 -3 -8 -3 25.71 4.16 0 -3 -8 -3 23.79 5.10 0 -3 8 -3 8.05 5.25 0 3 -8 3 21.21 4.84 0 3 8 3 26.44 4.62 0 3 8 3 25.11 4.26 0 -4 -8 -3 16.05 3.79 0 4 8 3 14.52 4.34 0 -4 8 -3 19.48 4.63 0 4 -8 3 11.12 4.86 0 -4 -8 -3 11.22 4.68 0 4 8 3 20.60 3.81 0 -5 -8 -3 -4.29 3.71 0 5 8 3 4.83 4.18 0 -5 8 -3 11.49 4.16 0 -5 -8 -3 22.00 4.35 0 5 -8 3 0.01 4.52 0 5 8 3 6.10 3.66 0 6 8 3 35.00 3.75 0 -6 -8 -3 25.03 3.43 0 -6 8 -3 33.10 4.30 0 6 -8 3 22.94 4.24 0 -7 8 -3 39.23 3.89 0 7 -8 3 20.30 4.05 0 7 8 3 51.24 3.75 0 -7 -8 -3 30.28 3.84 0 7 -8 3 30.46 3.82 0 8 -8 3 113.15 3.83 0 -8 -8 -3 124.67 3.85 0 8 8 3 123.67 3.79 0 -8 8 -3 105.45 4.30 0 8 -8 3 101.51 4.24 0 10 -9 -3 39.79 5.48 0 -10 9 3 44.01 3.60 0 10 9 -3 53.89 3.79 0 -10 -9 3 35.72 3.58 0 9 9 -3 153.14 4.05 0 9 -9 -3 114.03 5.52 0 -9 9 3 139.26 4.11 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43.61 4.92 0 -8 -10 3 52.36 4.11 0 7 -10 -3 126.73 5.52 0 -7 -10 3 115.90 4.63 0 7 10 -3 133.60 4.47 0 -7 10 3 121.31 4.76 0 -6 10 3 690.14 5.68 0 6 -10 -3 687.33 6.65 0 6 10 -3 698.60 5.92 0 -6 -10 3 640.34 6.11 0 -5 -10 3 43.80 7.60 0 5 10 -3 40.13 4.50 0 -5 10 3 43.51 4.38 0 5 -10 -3 30.61 4.57 0 -5 10 3 42.04 5.12 0 4 10 -3 76.28 4.74 0 4 -10 -3 69.94 4.83 0 -4 10 3 79.20 4.73 0 -4 10 3 60.36 5.64 0 -4 -10 3 82.09 6.48 0 -4 -10 3 68.10 4.44 0 3 -10 -3 3.31 4.60 0 3 10 -3 9.35 5.85 0 -3 -10 3 12.36 5.23 0 2 -10 -3 18.35 5.20 0 -2 -10 3 11.03 6.25 0 -2 -10 3 10.94 4.88 0 -1 10 3 1350.98 7.82 0 1 -10 -3 1425.71 7.82 0 -1 -10 3 1462.33 14.02 0 1 -10 -3 1391.50 7.87 0 -1 -10 3 1316.23 7.67 0 -1 10 3 1424.27 8.13 0 0 10 3 411.29 5.62 0 0 -10 -3 423.62 5.71 0 0 -10 3 418.07 12.45 0 0 -10 -3 433.54 5.83 0 0 10 3 447.40 5.81 0 -1 -10 -3 557.70 5.78 0 1 10 3 553.47 5.86 0 1 -10 3 573.18 9.72 0 -1 -10 -3 580.66 5.89 0 1 10 3 555.03 5.79 0 2 10 3 66.29 4.77 0 -2 10 -3 66.76 5.36 0 -2 -10 -3 52.38 4.56 0 2 -10 3 61.90 6.05 0 2 10 3 63.93 4.56 0 -2 -10 -3 73.35 4.58 0 -3 10 -3 40.61 5.06 0 3 10 3 53.01 4.58 0 -3 -10 -3 43.24 4.46 0 -3 -10 -3 39.22 4.33 0 3 -10 3 42.04 5.28 0 3 10 3 49.81 4.44 0 -4 -10 -3 89.92 4.33 0 -4 -10 -3 95.52 4.00 0 -4 10 -3 92.72 4.82 0 4 -10 3 102.78 4.85 0 4 10 3 89.20 4.07 0 4 10 3 82.40 5.01 0 -5 10 -3 85.17 4.68 0 -5 -10 -3 66.19 3.97 0 5 10 3 76.30 3.92 0 -5 -10 -3 68.55 4.05 0 5 -10 3 75.60 4.23 0 6 -10 3 86.11 4.50 0 6 10 3 78.18 3.71 0 -6 -10 -3 72.62 3.74 0 -6 10 -3 104.26 3.98 0 7 10 3 4.55 3.86 0 -7 -10 -3 24.79 3.67 0 7 -10 3 9.70 3.58 0 -7 10 -3 21.02 4.05 0 7 -10 3 10.82 3.95 0 8 -10 3 61.66 4.27 0 8 10 3 53.55 3.83 0 -8 10 -3 48.96 4.27 0 8 -10 3 56.42 3.91 0 -8 -10 -3 41.12 3.69 0 8 -10 3 40.81 4.42 0 9 -11 -3 92.88 5.04 0 -9 11 3 94.68 4.00 0 -9 -11 3 98.96 3.67 0 9 11 -3 111.03 3.79 0 8 11 -3 28.50 3.81 0 -8 11 3 12.44 3.95 0 8 -11 -3 19.49 4.32 0 -8 -11 3 22.10 3.70 0 7 -11 -3 128.84 5.16 0 -7 11 3 123.46 4.43 0 7 11 -3 149.12 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4.63 0 -6 -12 3 32.34 3.91 0 -5 -12 3 52.02 7.03 0 -5 -12 3 34.80 4.12 0 -5 12 3 42.19 4.32 0 -5 12 3 42.84 5.08 0 5 -12 -3 44.82 5.28 0 5 12 -3 43.63 5.05 0 -4 -12 3 8.96 5.55 0 4 -12 -3 0.23 4.59 0 4 12 -3 16.24 4.91 0 -4 12 3 7.61 4.27 0 -4 12 3 10.52 4.52 0 3 -12 -3 402.23 5.65 0 3 12 -3 443.77 7.14 0 -3 -12 3 383.27 6.58 0 -3 -12 3 386.68 6.70 0 -3 12 3 391.40 5.87 0 -2 -12 3 78.20 6.31 0 2 -12 -3 70.83 4.80 0 1 -12 -3 7.77 4.64 0 1 -12 -3 6.07 4.55 0 -1 -12 3 11.95 4.36 0 -1 -12 3 8.47 9.65 0 0 12 3 244.40 5.18 0 0 12 3 244.03 4.90 0 0 -12 -3 247.39 5.09 0 0 -12 -3 237.15 4.96 0 0 -12 3 232.80 4.98 0 1 12 3 377.94 5.46 0 1 -12 3 440.88 12.89 0 1 -12 3 350.47 5.06 0 -1 -12 -3 401.51 5.32 0 -1 -12 -3 406.66 5.86 0 1 12 3 375.28 5.28 0 -2 -12 -3 339.88 5.65 0 2 12 3 338.88 5.87 0 -2 12 -3 332.81 7.53 0 2 12 3 350.62 5.67 0 2 -12 3 355.53 7.92 0 -2 -12 -3 345.93 5.22 0 3 -12 3 24.58 5.23 0 -3 -12 -3 22.47 4.23 0 3 12 3 18.22 4.49 0 -3 12 -3 25.81 5.39 0 -3 -12 -3 27.89 4.21 0 3 12 3 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14.35 4.21 0 -3 3 -4 6.57 4.83 0 3 3 4 6.69 4.32 0 3 -3 4 20.33 5.05 0 -4 -3 -4 84.62 4.20 0 -4 3 -4 71.95 4.30 0 4 3 4 83.02 4.82 0 4 -3 4 69.74 4.28 0 4 3 4 70.99 4.20 0 4 -3 4 77.13 4.92 0 5 -3 4 6.62 4.06 0 -5 -3 -4 -3.56 3.78 0 -5 3 -4 -1.50 4.40 0 5 3 4 8.85 3.91 0 5 -3 4 7.37 3.90 0 5 3 4 -4.13 3.83 0 6 -3 4 99.18 4.33 0 6 3 4 104.90 4.07 0 6 -3 4 102.94 4.45 0 -6 -3 -4 104.63 4.01 0 6 3 4 104.29 4.31 0 -6 3 -4 111.07 4.59 0 7 3 4 29.37 3.80 0 -7 -3 -4 21.59 3.80 0 -7 3 -4 54.88 3.73 0 7 -3 4 40.06 3.70 0 -8 3 -4 45.12 3.82 0 -8 -3 -4 40.14 3.82 0 8 3 4 56.56 3.80 0 8 -3 4 34.02 3.92 0 -10 4 4 2.01 3.57 0 10 4 -4 4.74 3.73 0 -10 -4 4 0.07 3.42 0 -9 4 4 43.57 3.85 0 9 4 -4 37.86 3.95 0 -9 -4 4 36.98 3.77 0 -8 -4 4 33.01 3.59 0 8 -4 -4 37.61 7.44 0 8 4 -4 42.79 3.87 0 -8 4 4 38.18 3.64 0 7 -4 -4 1.84 6.72 0 -7 -4 4 3.48 3.79 0 7 4 -4 2.19 3.94 0 -7 4 4 12.28 3.81 0 -6 4 4 21.78 3.86 0 6 -4 -4 17.30 6.04 0 6 4 -4 9.15 4.36 0 -6 -4 4 20.47 4.20 0 5 -4 -4 65.26 5.62 0 -5 4 4 77.59 6.69 0 -5 -4 4 83.85 4.55 0 -5 4 4 62.29 4.54 0 4 -4 -4 3.66 5.09 0 -4 4 4 -4.98 6.13 0 -4 -4 4 1.68 6.98 0 -4 4 4 5.79 4.46 0 -4 -4 4 7.74 4.38 0 -3 4 4 0.67 5.85 0 3 -4 -4 1.12 5.41 0 -3 -4 4 0.46 5.77 0 -3 -4 4 -2.73 4.90 0 -3 4 4 -5.73 4.52 0 -2 4 4 385.22 6.88 0 2 -4 -4 366.96 6.44 0 -2 -4 4 379.28 6.71 0 -2 -4 4 384.34 6.92 0 -2 4 4 388.50 5.68 0 -1 4 4 -3.02 5.06 0 1 -4 -4 -3.12 4.82 0 -1 -4 4 1.91 4.97 0 1 -4 -4 0.32 4.77 0 -1 -4 4 4.87 4.67 0 -1 4 4 0.71 4.84 0 0 4 4 11.81 4.87 0 0 4 4 26.21 4.99 0 0 -4 -4 25.00 4.69 0 0 -4 4 22.78 4.76 0 0 -4 4 24.13 5.12 0 0 4 -4 14.26 5.66 0 0 -4 -4 13.44 4.84 0 1 4 4 549.50 6.08 0 1 -4 4 552.12 6.56 0 -1 4 -4 563.22 7.03 0 1 -4 4 561.81 5.83 0 1 4 4 537.80 5.99 0 -1 -4 -4 564.72 5.98 0 -1 -4 -4 555.12 6.04 0 -2 -4 -4 120.23 4.68 0 -2 4 -4 120.24 4.87 0 2 4 4 120.37 4.78 0 2 4 4 118.73 4.69 0 -2 -4 -4 111.63 4.59 0 2 -4 4 113.77 4.93 0 2 -4 4 116.44 4.56 0 -3 -4 -4 0.21 4.18 0 -3 4 -4 3.25 4.72 0 3 4 4 4.53 4.30 0 3 -4 4 -2.46 4.12 0 3 4 4 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0 6 5 -4 2.33 4.31 0 5 -5 -4 209.66 5.61 0 -5 5 4 238.48 7.07 0 -5 -5 4 200.52 5.37 0 -5 5 4 217.27 4.81 0 -4 5 4 4.70 5.37 0 4 -5 -4 1.95 5.77 0 -4 -5 4 10.19 4.93 0 -4 -5 4 3.64 6.78 0 -4 5 4 -3.25 4.55 0 -3 5 4 267.01 6.63 0 -3 -5 4 276.06 5.64 0 3 -5 -4 260.60 6.35 0 -3 -5 4 258.87 6.58 0 -3 5 4 246.16 5.15 0 -2 -5 4 164.76 6.22 0 -2 5 4 165.80 5.62 0 2 -5 -4 160.31 5.24 0 -2 5 4 147.36 4.93 0 -1 5 4 754.40 6.70 0 1 -5 -4 749.99 6.58 0 1 -5 -4 757.50 6.59 0 -1 -5 4 773.67 8.02 0 -1 5 4 766.29 6.53 0 0 5 4 56.94 4.90 0 0 -5 4 54.71 5.79 0 0 5 4 60.27 4.80 0 0 -5 -4 50.67 4.78 0 0 5 -4 50.30 5.57 0 0 -5 -4 53.51 4.80 0 1 5 4 1148.45 7.11 0 1 -5 4 1162.18 8.40 0 -1 -5 -4 1151.54 6.82 0 1 5 4 1135.59 7.10 0 -1 5 -4 1181.95 8.42 0 -1 -5 -4 1145.43 6.42 0 -2 -5 -4 -0.13 4.40 0 -2 5 -4 -1.79 4.29 0 2 5 4 13.10 4.56 0 2 5 4 5.44 4.47 0 -2 -5 -4 15.10 4.34 0 2 -5 4 7.54 5.06 0 3 5 4 152.85 4.65 0 -3 -5 -4 169.59 4.64 0 3 5 4 171.19 4.80 0 -3 -5 -4 172.48 4.57 0 3 -5 4 161.13 4.63 0 -3 5 -4 165.55 5.24 0 3 -5 4 149.80 5.27 0 4 -5 4 66.42 4.79 0 -4 -5 -4 56.00 3.98 0 -4 5 -4 62.08 4.34 0 4 5 4 61.89 4.35 0 4 -5 4 74.40 4.75 0 4 5 4 66.94 4.03 0 5 -5 4 22.07 4.44 0 5 5 4 21.43 3.84 0 -5 5 -4 9.56 3.94 0 5 5 4 7.20 4.41 0 5 -5 4 15.98 3.76 0 -5 -5 -4 31.53 3.89 0 6 5 4 18.36 3.60 0 -6 -5 -4 12.07 3.70 0 6 5 4 9.38 3.56 0 -6 5 -4 26.84 3.77 0 6 -5 4 17.07 3.66 0 6 -5 4 4.36 3.75 0 7 5 4 11.59 3.51 0 -7 -5 -4 15.47 3.68 0 -7 5 -4 -7.75 3.73 0 7 -5 4 6.68 3.38 0 7 -5 4 0.79 3.83 0 -8 5 -4 57.31 4.09 0 8 5 4 82.30 4.00 0 8 -5 4 58.95 3.86 0 -8 -5 -4 44.67 3.76 0 8 -5 4 56.45 4.03 0 -10 6 4 98.37 3.96 0 10 6 -4 145.65 4.20 0 -10 -6 4 103.78 3.88 0 -9 -6 4 16.48 3.66 0 9 6 -4 25.66 3.83 0 9 -6 -4 18.25 6.50 0 -9 6 4 24.74 3.55 0 8 6 -4 19.62 3.88 0 8 -6 -4 8.07 5.52 0 -8 6 4 -6.92 3.57 0 -8 -6 4 -6.93 3.73 0 -7 -6 4 378.86 4.47 0 7 -6 -4 346.77 6.81 0 7 6 -4 408.66 4.89 0 -7 6 4 337.01 4.77 0 -6 6 4 609.68 5.20 0 -6 6 4 546.97 7.34 0 -6 -6 4 586.14 5.43 0 6 6 -4 660.14 5.76 0 6 -6 -4 572.01 7.13 0 -5 6 4 343.37 5.09 0 5 6 -4 406.61 5.49 0 -5 6 4 372.33 6.68 0 -5 -6 4 330.40 5.14 0 5 -6 -4 342.57 6.21 0 4 -6 -4 728.88 7.06 0 -4 6 4 794.94 6.16 0 -4 -6 4 706.77 9.43 0 -4 -6 4 741.81 6.43 0 -4 6 4 704.55 7.28 0 3 -6 -4 411.06 5.93 0 -3 6 4 421.90 6.21 0 -3 6 4 406.28 5.48 0 -3 -6 4 436.77 6.61 0 -2 6 4 149.55 5.26 0 2 -6 -4 141.68 5.19 0 -2 -6 4 179.78 6.31 0 -2 -6 4 146.04 6.18 0 -2 6 4 136.28 4.90 0 1 -6 -4 1766.86 8.21 0 1 -6 -4 1812.28 8.25 0 -1 -6 4 1804.79 10.48 0 -1 6 4 1779.10 8.22 0 -1 6 4 1773.65 8.43 0 0 6 4 226.35 5.29 0 0 -6 4 230.72 6.24 0 0 6 4 224.35 5.46 0 0 -6 -4 222.56 5.20 0 0 6 -4 218.58 6.04 0 0 -6 -4 235.11 5.23 0 -1 -6 -4 8.07 4.43 0 1 6 4 10.59 4.52 0 1 6 4 6.45 4.53 0 1 -6 4 -0.43 5.41 0 -1 6 -4 4.02 5.63 0 -1 -6 -4 7.87 4.52 0 -2 -6 -4 385.72 5.33 0 -2 6 -4 360.72 6.06 0 2 6 4 367.06 5.43 0 2 6 4 348.55 5.19 0 -2 -6 -4 378.83 5.18 0 2 -6 4 370.71 6.08 0 -3 -6 -4 352.03 4.96 0 3 6 4 370.46 5.30 0 -3 6 -4 358.08 5.81 0 -3 -6 -4 360.01 5.24 0 3 6 4 356.34 5.05 0 3 -6 4 354.33 5.32 0 4 -6 4 -2.23 4.64 0 -4 -6 -4 1.55 4.19 0 -4 6 -4 9.30 4.58 0 4 -6 4 -5.83 3.95 0 -4 -6 -4 -0.95 4.55 0 4 6 4 -2.99 3.87 0 4 6 4 10.43 4.15 0 -5 -6 -4 9.41 3.77 0 -5 6 -4 18.58 3.78 0 5 -6 4 2.18 4.58 0 5 -6 4 -8.51 3.85 0 5 6 4 6.95 3.64 0 5 6 4 5.15 3.84 0 6 6 4 40.73 4.06 0 -6 -6 -4 39.27 3.61 0 -6 6 -4 31.07 3.83 0 6 -6 4 35.72 3.89 0 6 -6 4 35.67 3.87 0 7 6 4 5.73 3.75 0 -7 -6 -4 -5.26 3.76 0 -7 6 -4 -22.43 3.78 0 7 -6 4 20.44 3.47 0 7 -6 4 1.72 4.04 0 -8 -6 -4 0.09 3.58 0 -8 6 -4 0.04 3.75 0 8 6 4 28.09 3.62 0 8 -6 4 4.02 3.32 0 8 -6 4 -2.97 3.59 0 10 7 -4 41.62 3.90 0 -10 7 4 15.58 3.80 0 10 -7 -4 16.56 6.57 0 -10 -7 4 21.45 3.58 0 9 -7 -4 8.36 5.73 0 -9 7 4 -0.36 3.74 0 9 7 -4 -7.81 3.78 0 -9 -7 4 14.20 3.45 0 -8 -7 4 76.78 3.86 0 -8 7 4 74.84 3.81 0 8 -7 -4 70.78 5.42 0 8 7 -4 92.24 4.17 0 7 7 -4 -14.07 4.32 0 -7 -7 4 22.95 3.74 0 7 -7 -4 3.59 5.32 0 -7 7 4 8.35 3.65 0 -6 7 4 2.97 3.96 0 -6 -7 4 10.03 4.01 0 6 -7 -4 5.44 5.40 0 6 7 -4 9.95 4.37 0 -6 7 4 0.51 5.54 0 -5 7 4 406.11 5.00 0 5 -7 -4 373.12 6.26 0 -5 7 4 396.76 7.19 0 -5 -7 4 379.56 5.17 0 5 7 -4 439.80 5.52 0 4 -7 -4 6.97 5.18 0 -4 -7 4 0.36 4.58 0 -4 7 4 6.65 4.52 0 -4 -7 4 7.22 5.88 0 -4 7 4 10.81 5.39 0 -3 7 4 850.44 7.06 0 -3 -7 4 871.27 7.13 0 -3 7 4 833.68 6.24 0 3 -7 -4 860.49 7.22 0 -2 7 4 134.63 5.26 0 2 -7 -4 150.41 5.04 0 -2 -7 4 160.21 6.24 0 -2 -7 4 155.36 6.53 0 -2 7 4 160.52 5.02 0 -1 7 4 831.22 6.73 0 1 -7 -4 861.89 6.63 0 1 -7 -4 844.91 6.62 0 -1 -7 4 922.38 8.74 0 -1 7 4 843.59 6.65 0 0 7 4 202.89 5.16 0 0 7 4 202.07 5.21 0 0 -7 4 204.03 6.46 0 0 -7 -4 204.95 5.06 0 0 7 -4 208.34 6.06 0 0 -7 -4 193.06 5.19 0 -1 -7 -4 382.06 5.44 0 1 7 4 385.48 5.23 0 1 7 4 373.34 5.41 0 -1 -7 -4 382.19 5.31 0 -1 7 -4 384.18 6.39 0 -2 -7 -4 995.74 6.40 0 -2 7 -4 977.63 7.66 0 2 7 4 984.24 6.55 0 2 7 4 995.26 5.83 0 -2 -7 -4 992.59 6.76 0 2 -7 4 972.37 8.09 0 -3 -7 -4 700.08 5.47 0 3 7 4 700.01 5.97 0 -3 -7 -4 731.47 5.98 0 3 7 4 674.59 5.49 0 -3 7 -4 704.45 6.61 0 3 -7 4 694.84 6.75 0 -4 -7 -4 28.62 3.79 0 -4 7 -4 43.93 4.12 0 4 7 4 30.83 4.83 0 -4 -7 -4 24.17 4.12 0 4 7 4 39.10 3.93 0 4 -7 4 28.91 4.65 0 -5 -7 -4 53.20 3.82 0 5 7 4 64.73 4.04 0 -5 7 -4 59.89 4.22 0 5 -7 4 62.30 4.53 0 5 -7 4 63.30 3.94 0 5 7 4 82.17 3.81 0 -6 7 -4 7.37 3.69 0 6 -7 4 7.98 4.14 0 6 -7 4 2.41 3.98 0 -6 -7 -4 3.22 3.67 0 6 7 4 -2.01 3.61 0 7 7 4 -1.72 3.60 0 -7 -7 -4 5.81 3.67 0 -7 7 -4 19.38 3.69 0 7 -7 4 7.31 4.01 0 7 -7 4 0.32 3.63 0 -8 -7 -4 -10.19 3.43 0 -8 7 -4 1.15 3.66 0 8 7 4 5.91 3.50 0 8 -7 4 -8.60 3.35 0 8 -7 4 -0.60 3.46 0 10 -8 -4 40.15 6.12 0 -10 8 4 33.67 3.66 0 10 8 -4 61.90 3.76 0 -10 -8 4 41.79 3.62 0 9 -8 -4 28.06 5.37 0 -9 8 4 31.95 3.43 0 9 8 -4 25.96 3.84 0 -9 -8 4 32.50 3.50 0 -8 -8 4 186.92 4.04 0 8 -8 -4 196.91 5.75 0 -8 8 4 223.18 4.53 0 8 8 -4 231.33 4.72 0 7 -8 -4 36.39 5.27 0 -7 -8 4 39.27 3.85 0 -7 8 4 33.66 3.88 0 7 8 -4 38.67 4.20 0 6 8 -4 286.66 5.15 0 -6 -8 4 236.40 4.77 0 -6 8 4 263.45 4.97 0 -6 8 4 240.39 6.13 0 6 -8 -4 232.70 5.86 0 -5 8 4 187.93 4.75 0 5 8 -4 210.51 5.07 0 -5 -8 4 177.73 9.69 0 -5 -8 4 184.61 4.66 0 -5 8 4 181.09 5.84 0 5 -8 -4 167.49 5.31 0 -5 -8 4 176.21 10.60 0 4 -8 -4 157.78 5.36 0 -4 8 4 165.78 4.74 0 -4 8 4 137.41 5.49 0 3 -8 -4 55.91 4.86 0 -3 -8 4 57.12 5.49 0 -3 8 4 56.88 4.36 0 -2 8 4 2836.81 9.72 0 -2 -8 4 3144.22 12.48 0 2 -8 -4 2939.81 9.73 0 -2 -8 4 3069.66 12.42 0 -2 8 4 2886.74 9.68 0 -1 8 4 14.00 4.92 0 1 -8 -4 2.89 4.81 0 1 -8 -4 16.35 4.69 0 -1 -8 4 8.70 5.84 0 -1 8 4 7.53 4.61 0 0 8 4 13.38 4.76 0 0 8 4 16.26 5.02 0 0 -8 -4 7.06 4.50 0 0 -8 -4 2.75 4.68 0 1 8 4 769.52 6.17 0 -1 -8 -4 725.89 5.94 0 1 8 4 717.04 6.08 0 -1 8 -4 710.65 7.85 0 -1 -8 -4 740.12 6.14 0 -2 -8 -4 37.03 4.53 0 -2 8 -4 43.91 4.96 0 2 8 4 50.17 4.68 0 2 8 4 64.64 4.38 0 -2 -8 -4 55.56 4.46 0 2 -8 4 44.32 4.98 0 3 -8 4 317.84 5.71 0 -3 -8 -4 316.57 4.60 0 -3 8 -4 315.07 5.61 0 3 8 4 327.07 5.17 0 -3 -8 -4 312.88 5.06 0 3 8 4 298.37 4.67 0 -4 -8 -4 308.36 4.54 0 -4 8 -4 284.71 5.32 0 4 -8 4 306.66 5.59 0 -4 -8 -4 317.66 4.87 0 4 8 4 300.83 4.58 0 4 8 4 309.25 4.94 0 -5 -8 -4 12.57 3.63 0 -5 8 -4 3.54 4.20 0 5 -8 4 5.23 3.60 0 5 8 4 16.74 3.53 0 -6 8 -4 41.49 3.71 0 -6 -8 -4 34.82 3.92 0 6 -8 4 33.28 4.10 0 6 -8 4 50.88 4.12 0 6 8 4 23.73 3.99 0 7 8 4 58.28 3.78 0 -7 -8 -4 56.99 3.54 0 -7 8 -4 41.64 3.62 0 7 -8 4 48.44 3.92 0 7 -8 4 54.08 3.73 0 -8 -8 -4 5.25 3.32 0 8 8 4 20.51 3.59 0 -8 8 -4 7.21 3.93 0 8 -8 4 -3.22 3.40 0 8 -8 4 17.91 3.36 0 -10 9 4 117.11 4.03 0 10 -9 -4 102.01 6.10 0 -10 -9 4 111.90 3.71 0 10 9 -4 123.11 3.71 0 9 -9 -4 0.92 4.74 0 -9 9 4 4.75 3.60 0 -9 -9 4 2.73 3.34 0 9 9 -4 8.69 3.67 0 -8 -9 4 454.95 4.97 0 8 -9 -4 465.29 6.36 0 -8 9 4 466.36 4.83 0 8 9 -4 549.00 5.10 0 -7 -9 4 135.94 4.78 0 7 -9 -4 154.46 5.10 0 7 9 -4 161.11 5.00 0 -7 9 4 145.52 4.48 0 -6 -9 4 816.88 6.24 0 -6 9 4 830.36 5.93 0 6 9 -4 942.41 6.48 0 -6 9 4 767.16 6.82 0 6 -9 -4 803.67 7.21 0 -5 9 4 56.75 4.51 0 5 9 -4 69.65 5.18 0 -5 -9 4 58.16 4.89 0 -5 -9 4 51.23 8.40 0 5 -9 -4 48.23 5.00 0 -5 9 4 49.23 5.44 0 -4 9 4 75.91 4.75 0 4 -9 -4 73.07 4.59 0 -4 9 4 82.27 4.36 0 -4 9 4 80.73 5.38 0 -3 -9 4 24.75 5.46 0 -3 -9 4 23.73 5.02 0 3 -9 -4 30.79 4.63 0 -3 9 4 24.22 4.35 0 -2 9 4 6.41 4.76 0 -2 -9 4 7.90 5.51 0 2 -9 -4 4.29 4.55 0 -2 9 4 17.37 4.35 0 -2 -9 4 5.73 5.75 0 -1 9 4 26.00 4.80 0 1 -9 -4 33.98 4.76 0 1 -9 -4 32.55 4.62 0 -1 -9 4 21.25 6.18 0 -1 9 4 32.70 4.90 0 0 9 4 1594.81 7.75 0 0 9 4 1642.37 7.15 0 0 -9 -4 1657.15 7.64 0 0 -9 -4 1637.20 7.74 0 1 9 4 770.27 6.08 0 1 9 4 718.63 5.96 0 -1 -9 -4 748.31 6.00 0 -1 9 -4 742.09 8.19 0 -1 -9 -4 762.79 5.98 0 -2 9 -4 200.89 5.78 0 2 9 4 200.46 5.12 0 -2 -9 -4 203.93 4.91 0 2 9 4 198.08 4.66 0 2 -9 4 206.33 5.51 0 -2 -9 -4 209.98 4.47 0 3 -9 4 1.34 4.92 0 -3 9 -4 -2.02 4.79 0 3 9 4 0.56 4.30 0 -3 -9 -4 7.75 4.08 0 3 9 4 5.06 3.77 0 -3 -9 -4 11.93 3.76 0 -4 -9 -4 110.65 3.95 0 -4 9 -4 112.73 4.91 0 4 -9 4 117.01 4.90 0 -4 -9 -4 139.31 4.60 0 4 9 4 110.04 4.14 0 -5 9 -4 28.24 4.27 0 -5 -9 -4 26.16 3.64 0 5 -9 4 28.35 4.31 0 -5 -9 -4 27.92 4.44 0 5 9 4 33.34 3.59 0 -6 -9 -4 14.81 3.97 0 -6 9 -4 9.92 4.00 0 6 -9 4 27.86 4.11 0 6 -9 4 33.72 3.98 0 6 9 4 8.94 3.95 0 7 9 4 28.68 3.80 0 -7 -9 -4 28.49 3.74 0 -7 9 -4 46.43 3.67 0 7 -9 4 51.12 3.78 0 7 -9 4 50.26 3.72 0 10 -10 -4 7.32 4.99 0 -10 10 4 -4.37 3.43 0 -10 -10 4 18.90 3.31 0 10 10 -4 19.64 3.45 0 9 -10 -4 12.32 4.46 0 -9 10 4 0.19 3.50 0 9 10 -4 14.36 3.43 0 -9 -10 4 16.00 3.31 0 8 -10 -4 -2.17 4.65 0 -8 10 4 -7.68 3.63 0 -8 -10 4 3.05 3.72 0 8 10 -4 2.25 3.97 0 -7 -10 4 391.42 5.22 0 -7 10 4 397.01 4.60 0 7 -10 -4 396.62 6.05 0 7 10 -4 445.49 5.25 0 -6 -10 4 -0.65 4.01 0 6 10 -4 -11.43 4.80 0 -6 10 4 -5.23 4.07 0 -6 10 4 2.08 4.77 0 6 -10 -4 0.52 4.83 0 -5 -10 4 623.12 10.08 0 5 -10 -4 608.66 6.58 0 -5 10 4 642.47 5.73 0 -5 -10 4 632.90 6.18 0 5 10 -4 732.53 6.35 0 -5 10 4 640.56 6.36 0 4 -10 -4 233.80 5.50 0 -4 10 4 242.79 5.82 0 -4 10 4 241.44 4.69 0 -4 10 4 250.53 5.60 0 3 -10 -4 18.70 4.73 0 -3 10 4 28.89 4.37 0 -3 -10 4 9.93 4.93 0 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71.38 3.88 0 7 -3 5 70.55 3.95 0 -10 -4 5 -13.25 3.51 0 -10 4 5 11.70 3.58 0 -9 -4 5 1.48 3.78 0 -9 4 5 18.07 3.89 0 -8 -4 5 19.91 3.61 0 8 -4 -5 27.99 7.31 0 -8 4 5 26.35 3.66 0 -7 4 5 101.21 3.94 0 7 -4 -5 100.54 6.56 0 -7 -4 5 110.02 4.10 0 6 -4 -5 5.28 5.53 0 -6 4 5 5.49 3.84 0 -6 4 5 -1.26 6.43 0 -6 -4 5 3.12 4.02 0 -5 -4 5 41.84 8.04 0 -5 -4 5 41.81 4.46 0 5 -4 -5 50.77 5.05 0 -5 4 5 40.72 4.18 0 -5 4 5 36.92 5.49 0 -4 4 5 61.60 5.90 0 -4 -4 5 60.21 5.71 0 4 -4 -5 59.37 4.95 0 -4 -4 5 59.55 4.67 0 -3 -4 5 35.95 4.79 0 -3 4 5 30.98 5.54 0 3 -4 -5 31.96 5.18 0 -3 -4 5 29.87 5.58 0 -3 -4 5 35.96 4.62 0 -3 4 5 35.17 4.34 0 -2 4 5 215.50 5.11 0 2 -4 -5 224.46 4.88 0 -2 -4 5 214.13 5.24 0 -2 -4 5 231.80 5.97 0 -2 4 5 217.73 4.99 0 -1 4 5 1621.09 7.92 0 1 -4 -5 1668.23 8.13 0 -1 -4 5 1679.39 8.29 0 1 -4 -5 1646.49 7.84 0 -1 -4 5 1724.01 9.19 0 -1 4 5 1586.66 7.66 0 0 4 5 1381.92 7.17 0 0 -4 5 1361.54 8.52 0 0 4 5 1341.75 7.14 0 0 -4 -5 1281.23 7.05 0 0 -4 5 1300.01 7.12 0 0 4 -5 1345.29 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6.95 4.01 0 -2 6 -5 5.59 4.62 0 -3 -6 -5 5.68 3.91 0 -3 6 -5 8.99 3.97 0 3 6 5 4.96 4.11 0 3 6 5 3.02 3.77 0 -3 -6 -5 -1.03 3.88 0 3 -6 5 8.18 4.08 0 3 -6 5 -0.45 4.79 0 -4 -6 -5 7.76 3.71 0 -4 6 -5 -2.06 4.17 0 4 6 5 11.97 3.75 0 4 -6 5 4.11 3.64 0 4 6 5 8.60 3.87 0 4 -6 5 -12.26 4.39 0 -5 -6 -5 206.06 4.34 0 5 -6 5 201.44 4.53 0 -5 6 -5 206.44 4.43 0 5 6 5 204.15 4.49 0 5 -6 5 202.32 4.36 0 5 6 5 204.22 4.22 0 -6 -6 -5 4.97 3.74 0 6 -6 5 7.61 3.65 0 6 -6 5 7.94 3.48 0 -6 6 -5 14.33 4.09 0 6 6 5 17.75 3.57 0 7 6 5 26.47 3.70 0 -7 -6 -5 -14.14 3.68 0 -7 6 -5 3.60 3.48 0 7 -6 5 21.95 3.91 0 7 -6 5 9.51 3.63 0 -10 7 5 -2.69 3.61 0 -10 -7 5 -6.31 3.59 0 -9 -7 5 14.45 3.59 0 9 -7 -5 1.83 5.82 0 -9 7 5 14.39 3.57 0 9 7 -5 26.54 3.83 0 8 -7 -5 13.09 5.44 0 -8 -7 5 16.85 3.56 0 -8 7 5 22.90 3.57 0 -7 7 5 167.16 4.25 0 7 -7 -5 173.45 5.87 0 -7 -7 5 169.54 4.20 0 -7 7 5 160.85 5.78 0 6 -7 -5 86.92 5.43 0 -6 -7 5 85.30 4.88 0 -6 7 5 71.62 6.03 0 -6 7 5 80.60 4.15 0 5 -7 -5 31.63 4.62 0 -5 -7 5 29.69 7.01 0 -5 7 5 31.93 4.89 0 -5 7 5 32.70 4.07 0 -5 -7 5 34.97 7.03 0 -5 -7 5 35.84 4.04 0 -4 7 5 22.69 5.28 0 4 -7 -5 27.84 4.95 0 -4 -7 5 26.38 4.34 0 -4 -7 5 35.29 5.67 0 -4 7 5 34.54 4.15 0 -3 7 5 6.28 4.73 0 3 -7 -5 15.52 4.34 0 -3 -7 5 16.25 4.83 0 -3 -7 5 5.44 4.91 0 -3 7 5 0.69 4.12 0 2 -7 -5 700.23 6.05 0 -2 7 5 698.60 6.21 0 -2 -7 5 718.23 7.11 0 -2 7 5 727.10 5.33 0 -1 7 5 117.09 4.89 0 1 -7 -5 124.15 4.69 0 -1 7 5 135.56 4.55 0 1 -7 -5 112.67 4.60 0 -1 -7 5 136.70 5.49 0 0 7 5 46.82 4.43 0 0 7 5 59.63 4.74 0 0 -7 -5 59.98 4.47 0 0 7 -5 49.41 5.35 0 0 -7 -5 51.65 4.40 0 0 -7 5 53.12 5.18 0 1 7 5 136.41 4.78 0 1 -7 5 143.61 5.26 0 -1 -7 -5 156.55 4.55 0 1 7 5 133.21 4.46 0 -1 7 -5 136.00 5.09 0 -1 -7 -5 143.67 4.57 0 2 7 5 13.39 4.23 0 2 7 5 -6.31 3.74 0 -2 -7 -5 3.78 4.15 0 -2 -7 -5 11.04 3.70 0 2 -7 5 11.24 4.72 0 -2 7 -5 -1.25 4.54 0 -3 -7 -5 27.96 3.98 0 -3 7 -5 13.74 4.58 0 3 7 5 25.86 4.23 0 3 7 5 27.00 3.96 0 -3 -7 -5 18.34 4.09 0 3 -7 5 23.60 3.91 0 3 -7 5 17.17 4.74 0 4 -7 5 -2.27 4.40 0 -4 -7 -5 -6.14 3.72 0 -4 7 -5 3.66 4.38 0 4 7 5 13.39 3.85 0 4 -7 5 16.08 3.63 0 -4 -7 -5 3.65 3.81 0 4 7 5 -11.17 3.73 0 -5 -7 -5 212.18 4.58 0 -5 7 -5 234.12 4.88 0 5 -7 5 218.09 4.46 0 5 -7 5 232.90 4.38 0 5 7 5 194.26 4.20 0 -6 -7 -5 -0.61 3.71 0 6 7 5 -1.08 3.73 0 -6 7 -5 -11.58 4.05 0 6 -7 5 3.38 4.07 0 6 -7 5 -5.33 3.57 0 7 7 5 -11.34 3.70 0 -7 -7 -5 -4.94 3.58 0 -7 7 -5 2.68 3.44 0 7 -7 5 13.36 3.46 0 7 -7 5 -3.04 3.89 0 10 -8 -5 5.00 6.02 0 -10 8 5 8.08 3.64 0 10 8 -5 0.89 3.49 0 -10 -8 5 15.58 3.25 0 -9 -8 5 24.73 3.46 0 9 -8 -5 25.51 5.55 0 -9 8 5 37.08 3.86 0 9 8 -5 24.51 3.72 0 -8 -8 5 101.58 4.02 0 8 -8 -5 112.35 5.27 0 -8 8 5 126.74 3.90 0 7 -8 -5 6.41 4.80 0 -7 8 5 5.15 3.72 0 -7 -8 5 15.75 3.78 0 -7 8 5 8.44 5.16 0 -6 -8 5 974.63 6.06 0 -6 8 5 919.56 8.14 0 -6 8 5 1034.78 6.02 0 6 -8 -5 964.69 7.19 0 -5 8 5 43.84 4.10 0 5 -8 -5 47.54 5.11 0 -5 -8 5 43.22 6.95 0 -5 -8 5 34.06 7.47 0 -5 -8 5 39.69 4.87 0 -5 8 5 45.41 5.14 0 -4 8 5 251.87 5.70 0 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10.78 3.58 0 -5 8 -5 18.60 4.30 0 5 -8 5 10.80 4.29 0 5 -8 5 -3.05 3.75 0 5 8 5 18.63 3.58 0 -6 8 -5 25.44 3.53 0 -6 -8 -5 29.37 3.67 0 6 -8 5 27.08 4.13 0 6 -8 5 39.84 3.56 0 6 8 5 21.37 3.83 0 7 8 5 36.73 3.59 0 -7 -8 -5 43.32 3.79 0 -7 8 -5 36.66 3.51 0 7 -8 5 27.52 3.74 0 7 -8 5 38.65 4.10 0 10 -9 -5 9.93 5.53 0 -10 9 5 8.55 3.65 0 10 9 -5 -4.88 3.55 0 -10 -9 5 7.12 3.49 0 -9 -9 5 1.20 3.48 0 9 -9 -5 16.68 5.13 0 -9 9 5 15.82 3.62 0 9 9 -5 12.14 3.58 0 -8 -9 5 0.34 4.16 0 8 -9 -5 8.34 4.55 0 -8 9 5 10.86 3.82 0 8 9 -5 -0.10 4.15 0 7 -9 -5 17.42 4.62 0 -7 9 5 20.77 3.83 0 -7 -9 5 22.21 3.95 0 -7 9 5 11.39 4.86 0 6 -9 -5 22.23 5.19 0 -6 -9 5 33.15 4.17 0 -6 9 5 20.49 5.08 0 -6 9 5 25.87 4.09 0 -5 9 5 836.02 5.75 0 -5 9 5 766.23 7.09 0 5 -9 -5 733.92 6.68 0 -5 -9 5 771.76 9.74 0 -5 9 5 723.00 5.40 0 -5 -9 5 781.06 10.70 0 -5 -9 5 774.29 6.13 0 -4 9 5 149.92 4.87 0 -4 -9 5 165.01 4.69 0 4 -9 -5 163.98 4.61 0 -4 9 5 152.96 4.54 0 3 -9 -5 211.25 5.44 0 -3 9 5 192.89 4.54 0 -2 9 5 181.88 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19.17 3.68 0 -7 -9 -5 31.13 3.31 0 -7 9 -5 21.14 4.03 0 7 -9 5 12.97 3.53 0 7 -9 5 13.74 3.63 0 -9 10 5 5.28 3.56 0 9 10 -5 -0.46 3.62 0 9 -10 -5 5.78 4.63 0 -9 -10 5 1.68 3.41 0 -8 -10 5 289.15 4.50 0 8 -10 -5 290.97 5.82 0 -8 10 5 313.26 4.68 0 8 10 -5 361.99 4.89 0 7 -10 -5 12.88 4.55 0 -7 -10 5 -2.92 3.89 0 -7 10 5 15.50 3.89 0 -7 10 5 -0.69 4.92 0 6 -10 -5 2290.78 9.45 0 -6 -10 5 2295.41 8.55 0 -6 10 5 2214.15 10.01 0 -6 10 5 2378.37 7.97 0 5 -10 -5 97.09 5.20 0 -5 10 5 109.06 4.38 0 -5 -10 5 104.51 6.79 0 -5 -10 5 115.49 4.53 0 -5 10 5 88.16 4.04 0 -5 10 5 104.67 4.97 0 -5 -10 5 114.18 8.22 0 -4 10 5 479.63 5.64 0 4 -10 -5 505.68 5.52 0 -4 10 5 513.65 5.26 0 3 -10 -5 13.42 5.01 0 -3 10 5 -3.25 4.46 0 2 -10 -5 196.85 4.94 0 -2 -10 5 204.08 5.58 0 -2 -10 5 183.64 6.26 0 -2 10 5 179.01 4.63 0 1 -10 -5 131.02 4.67 0 1 -10 -5 149.63 4.60 0 -1 10 5 138.94 4.56 0 -1 -10 5 150.70 6.29 0 0 10 5 133.39 4.42 0 0 10 5 146.47 4.65 0 0 -10 5 133.35 6.04 0 0 -10 -5 138.71 4.49 0 0 -10 -5 138.25 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11 -5 29.03 4.42 0 -7 -11 5 83.72 3.87 0 7 -11 -5 87.08 5.10 0 -7 11 5 95.08 3.94 0 -7 11 5 78.85 4.79 0 -6 11 5 43.89 3.84 0 -6 -11 5 49.68 10.23 0 6 -11 -5 39.86 4.80 0 -6 -11 5 39.59 4.15 0 -6 -11 5 38.86 9.58 0 -6 11 5 39.78 5.08 0 -5 11 5 693.11 6.50 0 5 -11 -5 677.94 6.02 0 -5 11 5 730.27 5.84 0 -5 -11 5 677.74 5.96 0 -5 11 5 666.34 5.46 0 -5 -11 5 699.46 9.33 0 4 -11 -5 260.22 5.58 0 -4 11 5 254.86 4.70 0 -4 11 5 268.14 5.18 0 -3 -11 5 94.54 4.96 0 3 -11 -5 109.63 4.54 0 -3 11 5 86.93 4.52 0 2 -11 -5 14.24 4.57 0 -2 -11 5 14.00 5.68 0 -2 11 5 16.01 4.24 0 -2 -11 5 9.09 5.45 0 -1 -11 5 33.93 6.31 0 1 -11 -5 34.77 4.22 0 1 -11 -5 33.88 4.29 0 -1 11 5 30.60 4.28 0 0 11 5 93.62 4.49 0 0 11 5 94.96 4.44 0 0 -11 -5 100.32 4.28 0 0 -11 5 104.25 6.36 0 0 -11 -5 90.76 4.51 0 1 11 5 414.30 4.96 0 1 11 5 420.76 4.97 0 -1 -11 -5 431.69 4.82 0 1 -11 5 421.19 7.35 0 -1 11 -5 419.02 6.95 0 -1 -11 -5 461.05 4.98 0 2 11 5 48.53 4.20 0 2 11 5 37.02 4.12 0 -2 -11 -5 56.69 4.04 0 2 -11 5 47.59 5.49 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4.07 0 -7 -14 5 -0.08 3.64 0 7 -14 -5 4.36 4.34 0 -7 14 5 -2.65 3.88 0 -7 14 5 9.97 4.53 0 -6 -14 5 89.97 3.99 0 -6 -14 5 78.16 7.24 0 6 -14 -5 79.36 4.34 0 -6 14 5 102.19 4.16 0 -6 14 5 77.13 3.91 0 -6 14 5 73.08 4.74 0 5 -14 -5 106.06 4.88 0 -5 14 5 116.77 4.60 0 -5 14 5 72.72 3.96 0 -5 14 5 96.64 5.18 0 -5 -14 5 79.44 5.95 0 4 -14 -5 4.61 4.13 0 -4 14 5 3.82 3.79 0 -4 -14 5 9.36 5.06 0 -4 14 5 -3.94 4.28 0 3 -14 -5 405.96 5.11 0 -3 -14 5 396.42 6.75 0 -3 14 5 385.33 4.83 0 2 -14 -5 48.51 4.77 0 -2 -14 5 39.82 6.52 0 -2 -14 5 35.34 6.48 0 -2 -14 5 37.54 4.24 0 -2 14 5 45.29 4.18 0 -1 14 5 100.35 4.89 0 -1 -14 5 103.27 8.53 0 1 -14 -5 103.25 4.26 0 1 -14 -5 108.59 4.52 0 0 14 5 17.96 4.06 0 0 14 5 4.84 4.08 0 0 -14 -5 11.45 3.78 0 0 -14 5 15.05 9.25 0 0 -14 -5 20.58 4.04 0 0 -14 5 5.36 9.10 0 1 14 5 7.23 3.96 0 -1 -14 -5 4.61 3.97 0 1 -14 5 13.65 7.75 0 -1 -14 -5 10.91 4.07 0 -2 -14 -5 158.16 4.12 0 2 14 5 159.63 4.17 0 2 -14 5 162.19 6.84 0 -2 14 -5 146.53 6.34 0 -2 -14 -5 158.41 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6.87 0 3 -15 -5 222.57 4.67 0 -3 -15 5 207.28 6.55 0 -3 -15 5 210.70 6.57 0 -3 15 5 184.72 4.36 0 2 -15 -5 156.38 4.32 0 -2 -15 5 142.46 8.00 0 -2 -15 5 139.61 7.95 0 -2 15 5 127.36 4.73 0 -1 15 5 48.63 4.09 0 1 -15 -5 53.99 4.25 0 1 -15 -5 54.11 4.21 0 0 15 5 35.72 4.09 0 0 -15 -5 49.29 4.06 0 0 -15 -5 59.81 4.12 0 1 15 5 -0.48 3.75 0 -1 -15 -5 3.73 3.79 0 -1 -15 -5 -4.32 3.74 0 1 -15 5 -0.07 8.79 0 2 15 5 8.14 3.78 0 -2 -15 -5 5.81 3.74 0 2 15 5 6.50 3.74 0 -2 15 -5 14.28 6.09 0 -2 -15 -5 11.59 3.79 0 2 -15 5 13.01 6.50 0 -3 -15 -5 0.77 3.65 0 3 15 5 2.07 3.64 0 -3 15 -5 4.04 5.18 0 -3 -15 -5 15.77 3.44 0 -4 15 -5 -3.24 4.68 0 -4 -15 -5 5.72 3.60 0 4 15 5 -2.52 3.76 0 -4 -15 -5 4.90 3.74 0 -5 -15 -5 -11.61 3.56 0 -5 15 -5 -8.84 4.29 0 5 -15 5 1.57 4.67 0 -5 -15 -5 5.45 3.40 0 5 15 5 -9.49 3.72 0 -6 -15 -5 4.42 3.55 0 -6 15 -5 6.09 4.39 0 6 -15 5 0.02 4.36 0 -6 -15 -5 11.57 3.77 0 6 15 5 2.04 3.46 0 8 -16 -5 30.84 4.16 0 -8 -16 5 28.68 4.09 0 8 16 -5 33.93 4.10 0 -8 16 5 16.82 4.21 0 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67.72 3.82 0 -5 0 -7 59.32 3.69 0 -10 -1 7 -6.81 3.74 0 -10 1 7 10.25 3.71 0 -9 -1 7 16.70 3.60 0 -9 1 7 21.46 3.63 0 -8 1 7 14.52 3.65 0 -8 -1 7 9.94 3.79 0 -7 -1 7 152.46 4.39 0 -7 1 7 143.41 4.06 0 -7 1 7 147.09 7.72 0 -7 -1 7 143.11 9.71 0 -6 1 7 182.45 6.46 0 -6 -1 7 172.91 6.64 0 -6 1 7 202.16 4.21 0 -6 -1 7 202.57 4.30 0 -5 -1 7 24.63 4.62 0 -5 1 7 33.25 5.00 0 -5 -1 7 32.24 5.87 0 -5 -1 7 29.53 4.02 0 -5 1 7 27.34 3.67 0 -5 1 7 36.87 3.98 0 -4 1 7 19.71 5.03 0 -4 -1 7 9.03 4.89 0 4 -1 -7 17.12 4.52 0 -4 -1 7 10.89 4.26 0 -4 1 7 -0.75 4.19 0 -3 1 7 -8.61 4.83 0 -3 -1 7 -1.63 4.95 0 3 -1 -7 6.96 3.97 0 -3 -1 7 -0.71 4.16 0 -3 1 7 2.15 4.10 0 -2 1 7 417.72 5.36 0 -2 -1 7 405.03 5.16 0 2 -1 -7 424.23 5.15 0 -2 1 7 424.93 5.38 0 -2 -1 7 449.45 5.83 0 -1 1 7 51.85 4.36 0 -1 -1 7 44.77 4.98 0 1 1 -7 36.88 4.01 0 1 -1 -7 38.18 4.16 0 -1 1 7 44.85 4.41 0 -1 -1 7 50.32 4.68 0 0 1 7 38.75 4.17 0 0 -1 7 41.15 4.80 0 0 1 7 38.93 3.96 0 0 -1 7 51.56 3.94 0 0 1 -7 35.16 4.55 0 0 -1 -7 29.81 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-6 -10 10 5.24 4.59 0 -6 -10 10 3.10 3.74 0 6 -10 -10 11.06 3.73 0 -6 10 10 5.41 3.55 0 -6 -10 10 2.49 3.94 0 -6 10 10 0.16 3.22 0 -5 10 10 15.51 4.02 0 -5 -10 10 8.09 4.07 0 5 -10 -10 23.14 3.70 0 -5 -10 10 14.99 4.06 0 -5 10 10 20.65 3.43 0 -5 -10 10 11.43 4.17 0 -4 -10 10 27.53 4.03 0 4 -10 -10 34.55 3.43 0 -4 -10 10 22.85 3.91 0 -4 -10 10 17.90 3.95 0 -4 10 10 19.69 3.62 0 -3 -10 10 0.26 4.12 0 -3 -10 10 -8.97 4.23 0 -3 -10 10 14.12 3.49 0 -3 10 10 11.15 3.58 0 -2 10 10 -17.22 3.65 0 -2 -10 10 0.77 4.07 0 -2 -10 10 17.99 3.85 0 2 -10 -10 5.47 3.39 0 -1 10 10 -1.51 3.73 0 -1 -10 10 8.50 4.22 0 -1 -10 10 19.42 3.27 0 1 -10 -10 18.97 3.58 0 1 -10 -10 13.36 3.68 0 0 10 10 3.74 3.56 0 0 -10 10 7.58 4.09 0 0 -10 10 3.64 3.43 0 0 -10 -10 20.57 3.43 0 0 -10 -10 6.58 3.53 0 1 10 10 43.34 3.70 0 1 -10 10 69.92 3.63 0 1 -10 10 58.53 4.51 0 -1 -10 -10 59.36 3.40 0 -1 -10 -10 37.34 3.61 0 -6 11 10 126.64 4.56 0 -6 -11 10 114.35 4.16 0 -6 -11 10 141.08 4.90 0 6 -11 -10 118.01 4.50 0 -6 11 10 123.25 4.14 0 -6 -11 10 100.51 4.47 0 -6 11 10 109.46 3.82 0 -5 11 10 18.30 3.57 0 -5 -11 10 30.57 4.10 0 5 -11 -10 16.17 3.81 0 -5 -11 10 15.37 3.74 0 -5 -11 10 15.96 3.82 0 -5 11 10 12.38 3.47 0 -4 -11 10 46.63 4.35 0 -4 -11 10 58.66 4.13 0 4 -11 -10 39.51 3.51 0 -4 -11 10 46.98 4.08 0 -4 11 10 63.99 3.83 0 -3 -11 10 26.93 4.16 0 -3 -11 10 40.64 3.47 0 -3 -11 10 31.90 4.55 0 -3 11 10 26.88 3.58 0 -2 11 10 60.70 4.11 0 -2 -11 10 46.35 4.65 0 -2 -11 10 55.47 3.68 0 2 -11 -10 66.25 3.78 0 -1 11 10 -1.42 3.73 0 -1 -11 10 18.55 4.53 0 -1 -11 10 16.31 3.40 0 1 -11 -10 -4.71 3.54 0 1 -11 -10 13.12 3.60 0 0 11 10 35.58 3.67 0 0 -11 10 26.59 3.50 0 0 -11 10 24.49 4.40 0 0 -11 -10 22.55 3.51 0 0 -11 -10 35.20 3.61 0 1 11 10 4.04 3.15 0 1 -11 10 -3.04 3.63 0 -1 -11 -10 -8.40 3.35 0 1 -11 10 4.83 3.97 0 -1 -11 -10 4.44 3.39 0 -6 12 10 -6.88 4.15 0 -6 -12 10 3.18 3.96 0 -6 12 10 -6.35 3.65 0 -6 -12 10 3.73 4.03 0 6 -12 -10 -11.74 3.94 0 -6 -12 10 6.51 3.75 0 -6 12 10 0.21 3.47 0 -6 -12 10 -2.73 4.40 0 -5 12 10 -1.76 3.51 0 -5 -12 10 10.86 4.00 0 5 -12 -10 0.86 3.37 0 -5 -12 10 12.21 4.12 0 -5 -12 10 4.57 3.93 0 -5 12 10 3.85 3.49 0 -4 12 10 -2.08 3.86 0 -4 -12 10 10.86 4.20 0 -4 -12 10 16.84 4.04 0 4 -12 -10 22.82 3.37 0 -4 12 10 13.99 3.57 0 -4 -12 10 16.43 4.07 0 -3 12 10 -0.37 3.42 0 -3 -12 10 -3.70 4.37 0 -3 12 10 -4.42 3.58 0 -3 -12 10 0.86 4.36 0 -3 -12 10 -7.10 3.86 0 3 -12 -10 3.09 3.24 0 -2 12 10 5.20 3.51 0 -2 -12 10 0.38 4.42 0 -2 -12 10 1.72 3.74 0 2 -12 -10 3.29 3.37 0 -1 12 10 -19.91 3.62 0 -1 -12 10 -9.07 4.52 0 -1 -12 10 6.60 3.49 0 1 -12 -10 5.05 3.43 0 1 -12 -10 -2.73 3.37 0 0 12 10 3.08 3.47 0 0 -12 10 6.63 3.40 0 0 -12 10 12.28 4.27 0 0 -12 -10 0.04 3.47 0 0 -12 -10 8.39 3.43 0 -5 13 10 30.13 3.80 0 -5 -13 10 17.68 4.26 0 -5 -13 10 24.35 4.02 0 5 -13 -10 12.43 3.68 0 -5 -13 10 18.08 4.39 0 -5 13 10 4.22 3.51 0 -4 13 10 15.30 3.88 0 -4 -13 10 6.47 3.92 0 4 -13 -10 22.17 3.37 0 -4 -13 10 13.04 4.32 0 -4 13 10 4.02 3.51 0 -4 -13 10 2.60 4.14 0 -3 13 10 13.04 3.63 0 -3 -13 10 24.22 4.13 0 -3 13 10 43.71 3.57 0 3 -13 -10 37.90 3.37 0 -3 -13 10 40.65 3.81 0 -3 -13 10 23.01 4.54 0 -2 13 10 1.15 3.56 0 -2 -13 10 9.93 4.51 0 -2 -13 10 2.74 3.36 0 2 -13 -10 12.08 3.14 0 -2 -13 10 4.07 4.66 0 -1 13 10 -1.66 3.42 0 -1 -13 10 -4.82 4.32 0 -1 -13 10 2.20 3.49 0 1 -13 -10 10.19 3.26 0 1 -13 -10 13.50 3.33 0 0 13 10 7.78 3.51 0 0 -13 10 -2.16 3.02 0 0 -13 -10 5.31 3.25 0 0 -13 10 9.25 4.23 0 0 -13 -10 -11.04 3.40 0 -5 14 10 16.35 3.94 0 -5 -14 10 9.99 4.35 0 -5 -14 10 10.30 4.05 0 5 -14 -10 18.84 3.29 0 -5 -14 10 0.90 4.41 0 -5 14 10 1.53 3.36 0 -4 14 10 23.49 3.65 0 4 -14 -10 24.51 3.42 0 -4 -14 10 20.55 3.84 0 -4 -14 10 1.40 4.54 0 -4 14 10 9.94 3.46 0 -4 -14 10 2.48 4.74 0 -3 14 10 4.07 3.75 0 -3 14 10 9.92 3.54 0 -3 -14 10 -4.87 4.35 0 -3 -14 10 15.32 4.55 0 3 -14 -10 18.60 3.36 0 -3 -14 10 9.48 3.81 0 -2 14 10 11.24 3.36 0 -2 -14 10 -8.61 4.58 0 2 -14 -10 -23.79 3.39 0 -2 -14 10 4.55 3.74 0 -2 -14 10 2.86 4.85 0 -1 14 10 22.09 3.33 0 -1 -14 10 9.40 4.59 0 1 -14 -10 12.46 3.44 0 -1 -14 10 5.40 3.64 0 1 -14 -10 8.37 3.36 0 0 14 10 8.81 3.35 0 -4 15 10 10.25 3.68 0 -4 -15 10 -8.53 4.21 0 4 -15 -10 1.10 3.74 0 -4 -15 10 -0.72 3.86 0 -4 15 10 -9.90 3.38 0 -4 -15 10 -3.39 4.26 0 -3 15 10 9.51 3.44 0 -3 15 10 -4.31 3.48 0 -3 -15 10 -1.61 4.63 0 3 -15 -10 2.54 3.16 0 -3 -15 10 0.98 3.73 0 -3 -15 10 -4.15 4.74 0 -2 15 10 28.46 3.75 0 -2 -15 10 32.73 4.76 0 2 -15 -10 38.42 3.46 0 -2 -15 10 39.62 3.54 0 -2 -15 10 48.55 4.83 0 -1 15 10 -4.37 3.56 0 1 -15 -10 1.04 3.27 0 -1 -15 10 10.07 4.94 0 -1 -15 10 4.92 3.51 0 1 -15 -10 4.28 3.54 0 -3 16 10 -0.27 3.49 0 -3 16 10 20.75 3.31 0 3 -16 -10 5.32 3.20 0 -3 -16 10 11.76 4.63 0 -3 -16 10 13.23 3.79 0 -2 -16 10 -2.52 4.93 0 2 -16 -10 0.46 3.33 0 -5 0 11 5.51 4.24 0 -5 0 11 5.67 4.05 0 -3 0 11 1.55 3.64 0 -1 0 11 27.23 3.71 0 -6 1 11 46.75 4.30 0 -6 -1 11 46.69 3.89 0 -6 -1 11 39.24 4.36 0 -6 1 11 42.92 3.52 0 -6 -1 11 38.37 4.06 0 -6 1 11 29.46 3.80 0 -5 1 11 -3.95 4.32 0 -5 -1 11 -0.28 4.24 0 -5 -1 11 9.12 3.69 0 -5 1 11 -8.50 3.69 0 -5 -1 11 -2.59 4.10 0 -4 1 11 20.00 3.63 0 -4 -1 11 25.17 3.85 0 -4 1 11 11.21 3.93 0 -4 -1 11 12.19 3.70 0 -3 1 11 -6.38 3.61 0 -3 -1 11 4.20 3.63 0 -3 -1 11 1.79 3.38 0 -2 1 11 14.16 3.56 0 -2 -1 11 9.61 3.62 0 -1 1 11 -3.13 3.74 0 -1 -1 11 25.95 3.71 0 0 1 11 18.91 3.79 0 0 -1 11 18.63 3.67 0 0 1 -11 21.03 3.52 0 0 -1 -11 25.58 3.85 0 -6 2 11 -0.04 4.13 0 -6 2 11 4.83 3.52 0 -6 -2 11 6.28 4.16 0 -6 -2 11 -12.34 3.82 0 -6 2 11 1.94 3.39 0 -6 -2 11 -9.75 3.72 0 -5 2 11 0.70 4.19 0 -5 -2 11 -8.29 3.84 0 -5 -2 11 0.05 3.61 0 -5 2 11 3.35 3.59 0 -5 -2 11 -13.35 4.04 0 -4 2 11 -9.06 3.49 0 -4 -2 11 -2.63 4.04 0 -4 2 11 -5.66 3.53 0 -4 -2 11 -6.14 3.90 0 -3 2 11 5.81 3.44 0 -3 -2 11 28.18 4.00 0 -3 -2 11 20.49 3.49 0 -2 2 11 29.30 3.58 0 -2 -2 11 12.38 3.95 0 -1 2 11 1.16 3.65 0 -1 -2 11 -0.19 3.56 0 0 2 11 -4.05 3.99 0 0 -2 11 5.63 3.84 0 0 2 -11 3.91 3.71 0 0 -2 -11 -4.47 3.50 0 -6 3 11 19.07 4.18 0 -6 3 11 31.88 3.47 0 -6 -3 11 19.12 4.33 0 -6 -3 11 20.76 4.03 0 -6 -3 11 19.53 3.72 0 -6 3 11 20.04 3.40 0 -5 3 11 49.78 4.28 0 -5 -3 11 48.92 3.91 0 -5 -3 11 39.40 3.72 0 -5 3 11 43.68 3.83 0 -5 -3 11 40.25 4.07 0 -4 3 11 9.73 3.45 0 -4 -3 11 3.65 3.90 0 -4 3 11 8.32 3.46 0 -4 -3 11 4.44 3.87 0 -3 3 11 -2.34 3.35 0 -3 -3 11 21.67 3.73 0 -3 -3 11 1.96 3.49 0 -2 3 11 37.41 3.55 0 -2 -3 11 26.30 3.69 0 -1 3 11 -3.99 3.60 0 -1 -3 11 14.63 3.90 0 0 3 11 28.48 3.57 0 0 -3 11 19.19 3.40 0 0 -3 -11 16.10 3.36 0 -6 4 11 -0.18 4.04 0 -6 -4 11 1.37 4.41 0 -6 -4 11 -8.06 3.96 0 -6 4 11 4.16 3.53 0 -6 -4 11 -0.35 3.53 0 -6 4 11 15.68 3.25 0 -5 -4 11 16.25 3.86 0 -5 4 11 17.54 4.16 0 -5 -4 11 14.54 3.82 0 -5 -4 11 25.79 4.04 0 -5 4 11 8.22 3.48 0 -4 4 11 6.95 3.37 0 -4 -4 11 6.82 3.78 0 -4 4 11 -9.22 3.66 0 -4 -4 11 1.65 3.48 0 -3 4 11 10.19 3.61 0 -3 -4 11 9.19 3.42 0 -3 -4 11 6.94 3.36 0 -2 4 11 45.38 3.68 0 -2 -4 11 35.74 4.25 0 -1 4 11 38.84 3.42 0 -1 -4 11 37.85 3.68 0 0 4 11 -1.67 3.34 0 0 -4 11 7.40 3.97 0 0 -4 -11 8.45 3.25 0 -6 5 11 32.84 4.21 0 -6 -5 11 39.87 4.63 0 -6 -5 11 40.84 3.57 0 -6 5 11 42.39 3.91 0 -6 -5 11 27.62 3.62 0 -6 5 11 32.53 3.51 0 -5 5 11 4.25 4.12 0 -5 -5 11 -4.75 3.83 0 -5 -5 11 6.80 3.72 0 -5 -5 11 8.24 3.86 0 -5 5 11 5.26 3.55 0 -4 5 11 87.11 3.83 0 -4 -5 11 90.99 4.31 0 -4 -5 11 82.32 3.79 0 -4 5 11 85.07 4.05 0 -3 5 11 23.33 3.79 0 -3 -5 11 36.87 4.11 0 -3 -5 11 26.29 3.49 0 -2 5 11 11.62 3.69 0 -2 -5 11 12.01 3.63 0 -2 -5 11 18.70 3.98 0 -1 5 11 18.56 3.40 0 -1 -5 11 4.53 3.57 0 0 5 11 -10.40 3.37 0 0 -5 11 -11.09 3.43 0 0 -5 11 19.29 3.96 0 0 -5 -11 5.78 3.24 0 -6 6 11 -16.20 3.62 0 -5 -6 11 -1.83 3.45 0 -5 6 11 1.27 4.03 0 -5 -6 11 5.94 3.76 0 -5 -6 11 1.57 3.38 0 -5 6 11 12.46 3.63 0 -4 6 11 20.54 3.68 0 -4 -6 11 11.79 3.93 0 -4 6 11 30.70 3.86 0 -4 -6 11 22.50 4.14 0 -3 6 11 54.54 4.08 0 -3 -6 11 63.72 3.94 0 -3 -6 11 66.62 3.71 0 -2 6 11 -11.23 3.51 0 -2 -6 11 11.37 3.81 0 -2 -6 11 -7.05 3.89 0 -1 6 11 10.78 3.66 0 -1 -6 11 16.19 4.04 0 -1 -6 11 26.95 3.49 0 0 -6 -11 2.69 3.20 0 6 -7 -11 4.08 3.57 0 -5 7 11 19.38 4.18 0 -5 -7 11 4.31 3.87 0 5 -7 -11 27.50 3.66 0 -5 -7 11 15.16 3.95 0 -5 7 11 1.66 3.62 0 -5 -7 11 29.00 3.88 0 -4 7 11 15.90 3.50 0 -4 -7 11 25.16 4.02 0 -4 -7 11 26.31 3.99 0 4 -7 -11 24.20 3.58 0 -4 7 11 13.63 3.63 0 -4 -7 11 5.64 3.82 0 -3 7 11 75.85 3.87 0 -3 -7 11 76.75 4.23 0 -3 -7 11 75.08 3.73 0 3 -7 -11 82.58 3.81 0 -2 7 11 0.09 3.60 0 -2 -7 11 9.97 3.96 0 -2 -7 11 16.95 3.50 0 -1 7 11 -0.77 3.26 0 -1 -7 11 -10.44 3.90 0 -1 -7 11 5.58 3.28 0 -5 8 11 16.90 3.96 0 -5 -8 11 6.96 4.09 0 -5 -8 11 -4.22 4.07 0 5 -8 -11 5.66 3.64 0 -5 -8 11 26.08 3.83 0 -5 8 11 -10.15 3.35 0 -4 -8 11 85.65 4.00 0 -4 8 11 66.31 3.72 0 -4 -8 11 68.46 3.81 0 4 -8 -11 68.16 4.09 0 -4 8 11 62.78 3.97 0 -4 -8 11 72.46 4.29 0 -3 8 11 8.01 3.71 0 -3 -8 11 -9.01 4.14 0 -3 8 11 3.61 3.67 0 -3 -8 11 2.41 3.90 0 3 -8 -11 -4.92 3.46 0 -2 8 11 14.29 3.34 0 -2 -8 11 -6.29 3.80 0 -2 -8 11 -6.98 3.38 0 2 -8 -11 -8.84 3.20 0 -1 8 11 24.71 3.62 0 -1 -8 11 5.99 3.76 0 -1 -8 11 9.82 3.37 0 -5 9 11 -4.58 4.00 0 -5 -9 11 11.93 3.89 0 -5 -9 11 17.13 4.09 0 -4 9 11 8.29 3.52 0 -4 -9 11 -0.92 3.60 0 4 -9 -11 7.28 3.67 0 -4 -9 11 -10.70 3.95 0 -4 9 11 -1.58 3.55 0 -4 -9 11 0.73 4.10 0 -3 9 11 16.13 3.46 0 -3 -9 11 9.07 4.00 0 -3 9 11 16.76 3.81 0 -3 -9 11 14.00 3.73 0 3 -9 -11 10.67 3.52 0 -2 9 11 6.10 3.79 0 -2 -9 11 45.49 3.87 0 -2 -9 11 37.82 3.81 0 2 -9 -11 33.38 3.32 0 -1 9 11 -8.28 3.58 0 -1 -9 11 -0.73 4.05 0 -4 10 11 61.13 3.72 0 -4 -10 11 56.39 4.08 0 4 -10 -11 50.15 3.62 0 -4 -10 11 56.23 4.27 0 -4 10 11 57.75 3.71 0 -4 -10 11 39.02 4.32 0 -3 10 11 20.94 3.54 0 -3 -10 11 11.54 4.07 0 -3 -10 11 -0.30 4.12 0 -3 10 11 2.41 3.74 0 -3 -10 11 10.11 3.42 0 3 -10 -11 5.65 3.54 0 -2 10 11 6.05 3.50 0 -2 -10 11 5.24 4.18 0 -2 -10 11 12.47 3.40 0 2 -10 -11 18.58 3.48 0 ; _shelx_hkl_checksum 3489 _shelx_res_file ; TITL MH271 KLEINES PRISMA MH271_13.res created by SHELXL-2018/3 at 13:32:57 on 16-Jan-2023 CELL 0.71073 8.38810 24.36530 9.26140 90.00000 107.72400 90.00000 ZERR 4 0.00040 0.00090 0.00050 0.00000 0.00400 0.00000 LATT 1 SYMM -X+ 0.50000, Y+ 0.50000, -Z+ 0.50000 SFAC C H N O UNIT 80 92 12 8 LIST 4 OMIT -3 55 L.S. 30 FMAP 2 PLAN 5 ACTA BOND $H CONF MPLA 4 O2 C14 N3 C5 H3N C15 MPLA 6 C15 > C20 N3 MPLA 3 O2 C14 N3 H3N C15 MPLA 4 N1 C4 C5 C6 C3 C7 C14 MPLA 3 O1 C7 N2 H2N C8 MPLA 6 C8 > C13 N2 MPLA 4 O1 C7 N2 C5 H2N C8 MPLA 3 N1 C4 C5 C6 MPLA 4 O2 C14 N3 C5 H3N C15 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y+2, -z+1 HTAB N1 O2 HTAB N2 O2_$1 HTAB N3 O1 HTAB C6 N2 EQIV $2 x-1, y, z HTAB C10 O1_$2 HTAB C13 O1 HTAB C20 O2 SIZE 0.18 0.21 0.48 TEMP -80 WGHT 0.047500 0.624900 FVAR 0.91992 MOLE 1 C1 1 0.149019 1.228133 0.645018 11.00000 0.06707 0.03581 = 0.06564 0.00151 0.01869 0.00316 AFIX 137 H1A 2 0.059051 1.234402 0.690216 11.00000 -1.50000 H1B 2 0.138400 1.254351 0.562369 11.00000 -1.50000 H1C 2 0.257591 1.233135 0.722392 11.00000 -1.50000 AFIX 0 C2 1 0.136660 1.170115 0.583231 11.00000 0.05140 0.03723 = 0.04762 -0.00140 0.01396 0.00126 AFIX 23 H2A 2 0.034581 1.166745 0.495147 11.00000 -1.20000 H2B 2 0.234587 1.162517 0.547866 11.00000 -1.20000 AFIX 0 C3 1 0.130404 1.128295 0.702050 11.00000 0.03521 0.03130 = 0.04246 -0.00755 0.01215 0.00116 AFIX 23 H3A 2 0.220902 1.135805 0.797292 11.00000 -1.20000 H3B 2 0.021949 1.131048 0.723328 11.00000 -1.20000 AFIX 0 N1 3 0.150260 1.073178 0.648630 11.00000 0.03569 0.03166 = 0.03747 -0.00334 0.01424 0.00059 H1N 2 0.186564 1.069767 0.566899 11.00000 0.05003 C4 1 0.146019 1.026129 0.720478 11.00000 0.02509 0.03520 = 0.03323 -0.00166 0.00936 -0.00098 C5 1 0.186302 0.975881 0.667114 11.00000 0.02666 0.03228 = 0.03102 0.00061 0.01028 0.00089 C6 1 0.104657 1.031629 0.867060 11.00000 0.04332 0.04327 = 0.03746 -0.00475 0.01864 0.00014 AFIX 137 H6A 2 0.175144 1.060165 0.929658 11.00000 -1.50000 H6B 2 0.125317 0.996585 0.921533 11.00000 -1.50000 H6C 2 -0.013406 1.041718 0.845375 11.00000 -1.50000 AFIX 0 C7 1 0.149111 0.923125 0.729059 11.00000 0.02888 0.03574 = 0.02981 0.00111 0.01056 0.00199 O1 4 0.242575 0.882676 0.750267 11.00000 0.03955 0.04222 = 0.04722 0.01175 0.02099 0.01152 N2 3 -0.003880 0.920868 0.751854 11.00000 0.02922 0.03160 = 0.04176 0.00642 0.01367 0.00201 H2N 2 -0.073034 0.946806 0.707765 11.00000 0.04856 C8 1 -0.075794 0.877249 0.810291 11.00000 0.03415 0.03131 = 0.03043 -0.00114 0.01365 -0.00122 C9 1 -0.249306 0.876269 0.774746 11.00000 0.03340 0.03848 = 0.03894 0.00166 0.01431 0.00078 AFIX 43 H9 2 -0.314313 0.903796 0.710646 11.00000 -1.20000 AFIX 0 C10 1 -0.327806 0.835620 0.831860 11.00000 0.03532 0.04502 = 0.04848 -0.00057 0.01857 -0.00432 AFIX 43 H10 2 -0.446393 0.835127 0.806474 11.00000 -1.20000 AFIX 0 C11 1 -0.234020 0.795690 0.925851 11.00000 0.04708 0.03959 = 0.05294 0.00534 0.02282 -0.00765 AFIX 43 H11 2 -0.287648 0.767829 0.965915 11.00000 -1.20000 AFIX 0 C12 1 -0.062246 0.796504 0.961161 11.00000 0.04514 0.04032 = 0.05054 0.01173 0.01502 0.00146 AFIX 43 H12 2 0.002335 0.769047 1.025872 11.00000 -1.20000 AFIX 0 C13 1 0.017631 0.836964 0.903320 11.00000 0.03290 0.04024 = 0.04320 0.00696 0.01062 -0.00015 AFIX 43 H13 2 0.136133 0.836958 0.927613 11.00000 -1.20000 AFIX 0 C14 1 0.253986 0.974053 0.539461 11.00000 0.02326 0.03365 = 0.03261 0.00112 0.00803 0.00058 O2 4 0.252693 1.014702 0.456127 11.00000 0.03440 0.03473 = 0.03734 0.00458 0.01650 0.00289 N3 3 0.318516 0.925382 0.511876 11.00000 0.04137 0.03288 = 0.03927 0.00364 0.02100 0.00730 H3N 2 0.312683 0.898578 0.575703 11.00000 0.04052 C15 1 0.359314 0.909103 0.381897 11.00000 0.02547 0.04064 = 0.03524 -0.00160 0.01147 0.00451 C16 1 0.368176 0.852935 0.359798 11.00000 0.04214 0.04246 = 0.04585 -0.00168 0.01797 0.00774 AFIX 43 H16 2 0.347921 0.828183 0.431518 11.00000 -1.20000 AFIX 0 C17 1 0.406117 0.832565 0.234702 11.00000 0.04811 0.05242 = 0.04955 -0.01436 0.01576 0.00827 AFIX 43 H17 2 0.412200 0.794052 0.221270 11.00000 -1.20000 AFIX 0 C18 1 0.435166 0.868140 0.129303 11.00000 0.03588 0.07116 = 0.03905 -0.01381 0.01238 0.00575 AFIX 43 H18 2 0.459997 0.854333 0.042642 11.00000 -1.20000 AFIX 0 C19 1 0.427674 0.924040 0.151430 11.00000 0.03715 0.06680 = 0.03975 0.00064 0.01808 0.00189 AFIX 43 H19 2 0.447291 0.948603 0.078995 11.00000 -1.20000 AFIX 0 C20 1 0.391923 0.945023 0.277868 11.00000 0.03543 0.04500 = 0.04310 -0.00005 0.01930 0.00262 AFIX 43 H20 2 0.389836 0.983552 0.292900 11.00000 -1.20000 AFIX 0 HKLF 4 REM MH271 KLEINES PRISMA REM wR2 = 0.1291, GooF = S = 1.153, Restrained GooF = 1.153 for all data REM R1 = 0.0514 for 2967 Fo > 4sig(Fo) and 0.0742 for all 3882 data REM 240 parameters refined using 0 restraints END WGHT 0.0475 0.6242 REM Highest difference peak 0.141, deepest hole -0.227, 1-sigma level 0.044 Q1 1 -0.5000 0.9107 0.8400 11.00000 0.05 0.14 Q2 1 0.0574 1.1145 0.9391 11.00000 0.05 0.14 Q3 1 0.1159 1.0847 0.9007 11.00000 0.05 0.14 Q4 1 0.1716 0.9545 0.7011 11.00000 0.05 0.14 Q5 1 0.1805 1.0030 0.3079 11.00000 0.05 0.13 ; _shelx_res_checksum 52121 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.1490(3) 1.22813(9) 0.6450(3) 0.0565(6) Uani d 1 . . H H1A 0.059051 1.234402 0.690216 0.085 Uiso calc 1 . . H H1B 0.138400 1.254351 0.562369 0.085 Uiso calc 1 . . H H1C 0.257591 1.233135 0.722392 0.085 Uiso calc 1 . . C C2 0.1367(3) 1.17012(8) 0.5832(2) 0.0457(5) Uani d 1 . . H H2A 0.034581 1.166745 0.495147 0.055 Uiso calc 1 . . H H2B 0.234587 1.162517 0.547866 0.055 Uiso calc 1 . . C C3 0.1304(2) 1.12830(7) 0.7020(2) 0.0363(4) Uani d 1 . . H H3A 0.220902 1.135805 0.797292 0.044 Uiso calc 1 . . H H3B 0.021949 1.131048 0.723328 0.044 Uiso calc 1 . . N N1 0.15026(19) 1.07318(6) 0.64863(18) 0.0342(3) Uani d 1 . . H H1N 0.187(3) 1.0698(10) 0.567(3) 0.050(6) Uiso d 1 . . C C4 0.1460(2) 1.02613(7) 0.72048(19) 0.0311(4) Uani d 1 . . C C5 0.1863(2) 0.97588(7) 0.66711(19) 0.0297(4) Uani d 1 . . C C6 0.1047(2) 1.03163(8) 0.8671(2) 0.0399(4) Uani d 1 . . H H6A 0.175144 1.060165 0.929658 0.060 Uiso calc 1 . . H H6B 0.125317 0.996585 0.921533 0.060 Uiso calc 1 . . H H6C -0.013406 1.041718 0.845375 0.060 Uiso calc 1 . . C C7 0.1491(2) 0.92312(7) 0.72906(19) 0.0311(4) Uani d 1 . . O O1 0.24257(16) 0.88268(6) 0.75027(15) 0.0413(3) Uani d 1 . . N N2 -0.00388(19) 0.92087(6) 0.75185(18) 0.0336(3) Uani d 1 . . H H2N -0.073(3) 0.9468(10) 0.708(3) 0.049(6) Uiso d 1 . . C C8 -0.0758(2) 0.87725(7) 0.81029(19) 0.0311(4) Uani d 1 . . C C9 -0.2493(2) 0.87627(8) 0.7747(2) 0.0362(4) Uani d 1 . . H H9 -0.314313 0.903796 0.710646 0.043 Uiso calc 1 . . C C10 -0.3278(2) 0.83562(8) 0.8319(2) 0.0416(4) Uani d 1 . . H H10 -0.446393 0.835127 0.806474 0.050 Uiso calc 1 . . C C11 -0.2340(3) 0.79569(8) 0.9259(2) 0.0448(5) Uani d 1 . . H H11 -0.287648 0.767829 0.965915 0.054 Uiso calc 1 . . C C12 -0.0622(3) 0.79650(9) 0.9612(2) 0.0452(5) Uani d 1 . . H H12 0.002335 0.769047 1.025872 0.054 Uiso calc 1 . . C C13 0.0176(2) 0.83696(8) 0.9033(2) 0.0390(4) Uani d 1 . . H H13 0.136133 0.836958 0.927613 0.047 Uiso calc 1 . . C C14 0.25399(19) 0.97405(7) 0.53946(19) 0.0299(4) Uani d 1 . . O O2 0.25269(15) 1.01470(5) 0.45613(14) 0.0342(3) Uani d 1 . . N N3 0.3185(2) 0.92538(7) 0.51188(18) 0.0359(4) Uani d 1 . . H H3N 0.313(3) 0.8986(9) 0.576(2) 0.041(6) Uiso d 1 . . C C15 0.3593(2) 0.90910(8) 0.3819(2) 0.0333(4) Uani d 1 . . C C16 0.3682(2) 0.85294(9) 0.3598(2) 0.0425(5) Uani d 1 . . H H16 0.347921 0.828183 0.431518 0.051 Uiso calc 1 . . C C17 0.4061(3) 0.83256(10) 0.2347(2) 0.0498(5) Uani d 1 . . H H17 0.412200 0.794052 0.221270 0.060 Uiso calc 1 . . C C18 0.4352(2) 0.86814(10) 0.1293(2) 0.0485(5) Uani d 1 . . H H18 0.459997 0.854333 0.042642 0.058 Uiso calc 1 . . C C19 0.4277(2) 0.92404(10) 0.1514(2) 0.0465(5) Uani d 1 . . H H19 0.447291 0.948603 0.078995 0.056 Uiso calc 1 . . C C20 0.3919(2) 0.94502(8) 0.2779(2) 0.0395(4) Uani d 1 . . H H20 0.389836 0.983552 0.292900 0.047 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0671(15) 0.0358(11) 0.0656(15) 0.0032(10) 0.0187(12) 0.0015(10) C2 0.0514(12) 0.0372(11) 0.0476(11) 0.0013(9) 0.0140(9) -0.0014(9) C3 0.0352(9) 0.0313(9) 0.0425(10) 0.0012(7) 0.0122(8) -0.0075(8) N1 0.0357(8) 0.0317(8) 0.0375(8) 0.0006(6) 0.0142(7) -0.0033(6) C4 0.0251(8) 0.0352(9) 0.0332(9) -0.0010(7) 0.0094(7) -0.0017(7) C5 0.0267(8) 0.0323(9) 0.0310(8) 0.0009(6) 0.0103(7) 0.0006(7) C6 0.0433(10) 0.0433(11) 0.0375(10) 0.0001(8) 0.0186(8) -0.0047(8) C7 0.0289(8) 0.0357(9) 0.0298(8) 0.0020(7) 0.0106(7) 0.0011(7) O1 0.0395(7) 0.0422(8) 0.0472(8) 0.0115(6) 0.0210(6) 0.0118(6) N2 0.0292(7) 0.0316(8) 0.0418(8) 0.0020(6) 0.0137(6) 0.0064(7) C8 0.0342(9) 0.0313(9) 0.0304(8) -0.0012(7) 0.0137(7) -0.0011(7) C9 0.0334(9) 0.0385(10) 0.0389(10) 0.0008(7) 0.0143(8) 0.0017(8) C10 0.0353(10) 0.0450(11) 0.0485(11) -0.0043(8) 0.0186(8) -0.0006(9) C11 0.0471(11) 0.0396(11) 0.0529(12) -0.0077(9) 0.0228(9) 0.0053(9) C12 0.0451(11) 0.0403(11) 0.0505(12) 0.0015(8) 0.0150(9) 0.0117(9) C13 0.0329(9) 0.0402(10) 0.0432(10) -0.0001(8) 0.0106(8) 0.0070(8) C14 0.0233(7) 0.0337(9) 0.0326(9) 0.0006(6) 0.0080(6) 0.0011(7) O2 0.0344(6) 0.0347(7) 0.0373(7) 0.0029(5) 0.0165(5) 0.0046(5) N3 0.0414(8) 0.0329(8) 0.0393(8) 0.0073(7) 0.0210(7) 0.0036(7) C15 0.0255(8) 0.0406(10) 0.0352(9) 0.0045(7) 0.0115(7) -0.0016(7) C16 0.0421(10) 0.0425(11) 0.0459(11) 0.0077(8) 0.0180(9) -0.0017(9) C17 0.0481(12) 0.0524(13) 0.0495(12) 0.0083(9) 0.0158(9) -0.0144(10) C18 0.0359(10) 0.0712(15) 0.0390(10) 0.0057(10) 0.0124(8) -0.0138(10) C19 0.0372(10) 0.0668(14) 0.0397(11) 0.0019(9) 0.0181(8) 0.0006(10) C20 0.0354(10) 0.0450(11) 0.0431(10) 0.0026(8) 0.0193(8) -0.0001(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 2 30 -2 0.1227 3 -30 -1 0.2541 2 -5 30 1.4494 -30 -1 12 0.6521 -4 -30 2 0.2163 -30 -1 -2 0.7056 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 C1 H1A . . 109.5 ? C2 C1 H1B . . 109.5 ? H1A C1 H1B . . 109.5 ? C2 C1 H1C . . 109.5 ? H1A C1 H1C . . 109.5 ? H1B C1 H1C . . 109.5 ? C3 C2 C1 . . 111.53(18) ? C3 C2 H2A . . 109.3 ? C1 C2 H2A . . 109.3 ? C3 C2 H2B . . 109.3 ? C1 C2 H2B . . 109.3 ? H2A C2 H2B . . 108.0 ? N1 C3 C2 . . 109.93(15) ? N1 C3 H3A . . 109.7 ? C2 C3 H3A . . 109.7 ? N1 C3 H3B . . 109.7 ? C2 C3 H3B . . 109.7 ? H3A C3 H3B . . 108.2 ? C4 N1 C3 . . 126.89(16) ? C4 N1 H1N . . 114.0(15) ? C3 N1 H1N . . 118.2(15) ? N1 C4 C5 . . 122.05(16) ? N1 C4 C6 . . 114.99(16) ? C5 C4 C6 . . 122.87(16) ? C4 C5 C14 . . 120.53(15) ? C4 C5 C7 . . 121.41(15) ? C14 C5 C7 . . 117.88(15) ? C4 C6 H6A . . 109.5 ? C4 C6 H6B . . 109.5 ? H6A C6 H6B . . 109.5 ? C4 C6 H6C . . 109.5 ? H6A C6 H6C . . 109.5 ? H6B C6 H6C . . 109.5 ? O1 C7 N2 . . 121.60(16) ? O1 C7 C5 . . 123.75(15) ? N2 C7 C5 . . 114.50(15) ? C7 N2 C8 . . 128.54(16) ? C7 N2 H2N . . 115.0(15) ? C8 N2 H2N . . 115.2(15) ? C13 C8 C9 . . 119.29(17) ? C13 C8 N2 . . 123.20(16) ? C9 C8 N2 . . 117.48(16) ? C10 C9 C8 . . 120.55(18) ? C10 C9 H9 . . 119.7 ? C8 C9 H9 . . 119.7 ? C11 C10 C9 . . 120.02(18) ? C11 C10 H10 . . 120.0 ? C9 C10 H10 . . 120.0 ? C12 C11 C10 . . 119.58(18) ? C12 C11 H11 . . 120.2 ? C10 C11 H11 . . 120.2 ? C11 C12 C13 . . 120.78(19) ? C11 C12 H12 . . 119.6 ? C13 C12 H12 . . 119.6 ? C8 C13 C12 . . 119.77(18) ? C8 C13 H13 . . 120.1 ? C12 C13 H13 . . 120.1 ? O2 C14 N3 . . 120.18(15) ? O2 C14 C5 . . 122.81(16) ? N3 C14 C5 . . 117.00(15) ? C14 N3 C15 . . 128.45(16) ? C14 N3 H3N . . 114.1(14) ? C15 N3 H3N . . 116.0(14) ? C20 C15 C16 . . 119.20(17) ? C20 C15 N3 . . 124.55(17) ? C16 C15 N3 . . 116.25(17) ? C17 C16 C15 . . 120.9(2) ? C17 C16 H16 . . 119.6 ? C15 C16 H16 . . 119.6 ? C18 C17 C16 . . 120.1(2) ? C18 C17 H17 . . 119.9 ? C16 C17 H17 . . 119.9 ? C17 C18 C19 . . 119.21(19) ? C17 C18 H18 . . 120.4 ? C19 C18 H18 . . 120.4 ? C18 C19 C20 . . 121.2(2) ? C18 C19 H19 . . 119.4 ? C20 C19 H19 . . 119.4 ? C15 C20 C19 . . 119.38(19) ? C15 C20 H20 . . 120.3 ? C19 C20 H20 . . 120.3 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 C2 . 1.517(3) ? C1 H1A . 0.9800 ? C1 H1B . 0.9800 ? C1 H1C . 0.9800 ? C2 C3 . 1.512(3) ? C2 H2A . 0.9900 ? C2 H2B . 0.9900 ? C3 N1 . 1.458(2) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? N1 C4 . 1.331(2) y N1 H1N . 0.90(2) ? C4 C5 . 1.400(2) y C4 C6 . 1.506(2) ? C5 C14 . 1.460(2) ? C5 C7 . 1.479(2) ? C6 H6A . 0.9800 ? C6 H6B . 0.9800 ? C6 H6C . 0.9800 ? C7 O1 . 1.237(2) y C7 N2 . 1.364(2) y N2 C8 . 1.409(2) ? N2 H2N . 0.87(2) ? C8 C13 . 1.382(3) ? C8 C9 . 1.391(2) ? C9 C10 . 1.381(3) ? C9 H9 . 0.9500 ? C10 C11 . 1.381(3) ? C10 H10 . 0.9500 ? C11 C12 . 1.377(3) ? C11 H11 . 0.9500 ? C12 C13 . 1.388(3) ? C12 H12 . 0.9500 ? C13 H13 . 0.9500 ? C14 O2 . 1.254(2) y C14 N3 . 1.360(2) y N3 C15 . 1.405(2) ? N3 H3N . 0.89(2) ? C15 C20 . 1.389(3) ? C15 C16 . 1.389(3) ? C16 C17 . 1.384(3) ? C16 H16 . 0.9500 ? C17 C18 . 1.381(3) ? C17 H17 . 0.9500 ? C18 C19 . 1.382(3) ? C18 H18 . 0.9500 ? C19 C20 . 1.392(3) ? C19 H19 . 0.9500 ? C20 H20 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N O2 . 0.90(2) 1.87(2) 2.623(2) 139(2) yes N3 H3N O1 . 0.89(2) 1.92(2) 2.687(2) 142.9(19) yes C6 H6B N2 . 0.98 2.45 2.943(3) 110.6 yes C13 H13 O1 . 0.95 2.37 2.905(2) 115.0 yes C20 H20 O2 . 0.95 2.29 2.854(2) 117.4 yes N2 H2N O2 3_576 0.87(2) 2.02(2) 2.843(2) 158(2) yes C10 H10 O1 1_455 0.95 2.76 3.635(2) 154.3 yes C13 H13 Cg2 1_556 0.95 3.40 4.011(2) 123.8 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C1 C2 C3 N1 . . . . -169.39(17) y C2 C3 N1 C4 . . . . -177.75(17) ? C3 N1 C4 C5 . . . . -172.23(16) ? C3 N1 C4 C6 . . . . 4.4(3) ? N1 C4 C5 C14 . . . . 7.3(3) ? C6 C4 C5 C14 . . . . -169.03(16) ? N1 C4 C5 C7 . . . . -167.58(16) ? C6 C4 C5 C7 . . . . 16.1(2) ? C4 C5 C7 O1 . . . . -142.19(18) ? C14 C5 C7 O1 . . . . 42.8(2) ? C4 C5 C7 N2 . . . . 42.2(2) ? C14 C5 C7 N2 . . . . -132.82(16) ? O1 C7 N2 C8 . . . . 5.0(3) ? C5 C7 N2 C8 . . . . -179.29(16) ? C7 N2 C8 C13 . . . . 24.0(3) ? C7 N2 C8 C9 . . . . -157.83(18) ? C13 C8 C9 C10 . . . . 0.1(3) ? N2 C8 C9 C10 . . . . -178.08(17) ? C8 C9 C10 C11 . . . . 0.4(3) ? C9 C10 C11 C12 . . . . -0.5(3) ? C10 C11 C12 C13 . . . . 0.0(3) ? C9 C8 C13 C12 . . . . -0.6(3) ? N2 C8 C13 C12 . . . . 177.48(18) ? C11 C12 C13 C8 . . . . 0.6(3) ? C4 C5 C14 O2 . . . . -12.5(3) ? C7 C5 C14 O2 . . . . 162.54(15) ? C4 C5 C14 N3 . . . . 168.22(15) ? C7 C5 C14 N3 . . . . -16.7(2) ? O2 C14 N3 C15 . . . . -13.5(3) ? C5 C14 N3 C15 . . . . 165.78(17) ? C14 N3 C15 C20 . . . . 22.0(3) ? C14 N3 C15 C16 . . . . -158.64(18) ? C20 C15 C16 C17 . . . . -1.1(3) ? N3 C15 C16 C17 . . . . 179.48(18) ? C15 C16 C17 C18 . . . . -0.3(3) ? C16 C17 C18 C19 . . . . 0.7(3) ? C17 C18 C19 C20 . . . . 0.2(3) ? C16 C15 C20 C19 . . . . 2.0(3) ? N3 C15 C20 C19 . . . . -178.67(17) ? C18 C19 C20 C15 . . . . -1.5(3) ? _cod_database_fobs_code 2244223