#------------------------------------------------------------------------------ #$Date: 2023-05-06 11:48:33 +0100 (Sat, 06 May 2023) $ #$Revision: 283594 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/42/2244235.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244235 loop_ _publ_author_name 'Laban, Uroš' 'Naeem, Marilyn' 'Chadeayne, Andrew R.' 'Golen, James A.' 'Manke, David R.' _publ_section_title ; Synthesis and structure of 4-hy-droxy-N-iso-propyl-tryptamine (4-HO-NiPT) and its precursors. ; _journal_coeditor_code HB8057 _journal_issue 'Pt 4' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 280 _journal_page_last 286 _journal_paper_doi 10.1107/S2056989023002098 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C15 H13 N O' _chemical_formula_moiety 'C15 H13 N O' _chemical_formula_sum 'C15 H13 N O' _chemical_formula_weight 223.26 _chemical_name_common ; 4-Benzyloxyindole ; _chemical_name_systematic ; 4-Phenoxy-1H-indole ; _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.8201(9) _cell_length_b 9.0067(7) _cell_length_c 26.995(2) _cell_measurement_reflns_used 9827 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 26.34 _cell_measurement_theta_min 2.57 _cell_volume 2387.6(3) _computing_cell_refinement ; SAINT (Bruker, 2021) ; _computing_data_collection ; APEX4 (Bruker, 2021) ; _computing_data_reduction ; SAINT (Bruker, 2021) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 300.15 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 Venture CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0394 _diffrn_reflns_av_unetI/netI 0.0122 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 56335 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.396 _diffrn_reflns_theta_min 3.018 _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.078 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6965 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2021) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.242 _exptl_crystal_description block _exptl_crystal_F_000 944 _exptl_crystal_size_max 0.40 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.156 _refine_diff_density_min -0.121 _refine_ls_extinction_coef 0.0078(11) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2018/3 (Sheldrick 2015b) ; _refine_ls_goodness_of_fit_ref 1.110 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 159 _refine_ls_number_reflns 2451 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.110 _refine_ls_R_factor_all 0.0543 _refine_ls_R_factor_gt 0.0453 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0359P)^2^+0.7870P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1041 _refine_ls_wR_factor_ref 0.1102 _reflns_number_gt 2098 _reflns_number_total 2451 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8057sup1.cif _cod_data_source_block 1 _cod_depositor_comments 'Adding full bibliography for 2244235--2244238.cif.' _cod_original_cell_volume 2387.6(4) _cod_database_code 2244235 _cod_database_fobs_code 2244235 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.969 _shelx_estimated_absorpt_t_max 0.991 _shelx_hkl_file ; 0 -2 0 498.65 9.60 0 -2 0 507.25 9.60 0 2 0 518.25 9.60 0 2 0 513.75 9.60 0 2 0 510.15 10.50 0 -2 0 499.15 10.50 0 -2 0 505.75 10.20 0 3 0 0.40 0.40 0 -3 0 0.10 0.50 0 3 0 0.30 0.40 0 -3 0 0.00 0.40 0 -3 0 0.60 1.00 0 -3 0 0.40 0.90 0 -4 0 343.47 8.70 0 -4 0 352.46 9.00 0 -4 0 350.16 8.10 0 4 0 348.17 6.80 0 -4 0 345.67 6.80 0 -4 0 345.37 6.80 0 4 0 353.56 6.80 0 -5 0 -1.60 1.20 0 -5 0 0.30 2.00 0 -6 0 1.90 2.10 0 -6 0 4.00 2.10 0 -6 0 6.50 1.70 0 -7 0 0.30 2.40 0 -7 0 -2.30 2.10 0 -7 0 1.40 2.20 0 -7 0 0.00 1.80 0 -8 0 307.07 10.90 0 -8 0 331.87 10.50 0 -8 0 326.37 11.10 0 -9 0 -2.70 2.30 0 -9 0 1.10 3.00 0 -9 0 2.80 3.30 0 -9 0 0.00 3.60 0 -10 0 123.29 8.00 0 -10 0 130.59 7.30 0 -10 0 125.99 5.60 0 -10 0 116.19 7.40 0 -11 0 -3.10 2.10 0 -11 0 3.00 2.70 0 -11 0 0.30 2.60 -1 -1 0 1.40 0.60 -1 -1 0 2.40 0.70 1 -1 0 2.90 0.80 1 -1 0 2.80 0.80 1 1 0 2.10 0.60 -1 1 0 2.00 0.60 1 -1 0 1.60 0.70 1 -1 0 3.00 0.70 -1 -1 0 5.10 0.90 -1 1 0 2.70 0.90 1 -1 0 4.20 0.80 -1 1 0 3.10 0.70 -1 1 0 2.10 0.70 1 -2 0 0.60 0.80 1 -2 0 -1.00 0.80 -1 2 0 -0.10 1.20 1 -2 0 0.90 1.20 -1 2 0 0.00 0.80 -1 2 0 0.50 1.00 1 -2 0 -1.60 1.30 -1 2 0 0.20 0.80 1 -3 0 -0.80 1.30 -1 3 0 -0.40 0.70 -1 3 0 0.00 0.70 1 -3 0 0.10 1.00 -1 -3 0 0.20 0.60 1 3 0 1.70 0.60 -1 3 0 0.10 1.20 -1 -3 0 0.80 1.10 -1 -3 0 1.70 0.60 1 -3 0 -1.20 0.70 1 3 0 1.00 0.60 1 -3 0 -0.90 0.70 1 3 0 0.80 1.10 -1 -3 0 2.00 1.00 1 4 0 1.70 1.40 -1 -4 0 1.00 0.60 1 -4 0 1.00 1.40 1 4 0 0.40 0.60 1 -4 0 -1.10 0.80 -1 4 0 -0.50 0.80 1 -4 0 3.00 1.80 1 4 0 2.00 0.60 -1 -4 0 0.10 1.30 -1 4 0 1.80 1.50 -1 4 0 0.20 0.80 -1 -5 0 -0.30 1.50 -1 5 0 -0.60 0.80 1 -5 0 -0.90 1.40 1 5 0 0.90 0.40 1 -5 0 -0.40 0.80 1 -5 0 -0.10 0.70 -1 -5 0 -0.60 1.40 1 5 0 0.40 0.70 -1 -5 0 -0.30 1.50 -1 5 0 -0.70 0.70 -1 -6 0 -0.50 1.60 1 -6 0 -1.20 0.60 1 -6 0 2.50 1.50 1 -6 0 1.30 1.70 -1 -6 0 0.50 1.90 -1 -6 0 0.70 1.80 -1 -6 0 0.90 1.90 -1 6 0 -0.20 0.70 1 -6 0 0.50 2.00 1 -6 0 1.70 0.70 -1 6 0 3.50 1.90 1 -7 0 1.30 2.00 -1 -7 0 3.50 2.30 1 -7 0 3.60 2.60 1 -7 0 1.30 1.70 -1 -7 0 4.50 2.30 -1 -7 0 2.60 2.00 1 -8 0 1.10 2.30 -1 -8 0 -0.70 2.40 -1 -8 0 -1.70 2.50 1 -8 0 -3.80 2.30 -1 -8 0 -3.30 2.30 1 -8 0 -4.30 3.10 -1 -8 0 -0.80 2.20 -1 -9 0 6.10 3.20 1 -9 0 7.80 2.50 1 -9 0 8.00 3.30 -1 -9 0 6.60 2.70 1 -9 0 3.10 3.70 1 -10 0 3.00 2.00 1 -10 0 2.20 2.30 1 -10 0 0.60 3.20 1 -10 0 2.70 3.80 -1 -10 0 -3.00 2.60 -1 -10 0 2.10 2.90 -1 -10 0 4.40 2.60 -1 -10 0 4.30 3.30 1 -10 0 1.40 3.20 1 -11 0 6.70 1.90 -1 -11 0 -1.50 2.20 -1 -11 0 -2.60 3.10 -1 -11 0 2.50 2.90 1 -11 0 1.90 3.50 1 -11 0 -0.30 3.10 -1 -11 0 -0.50 2.60 1 -11 0 2.20 3.20 1 -11 0 1.00 2.40 -2 0 0 7557.34 150.78 2 0 0 7197.28 149.79 2 1 0 53.49 2.60 2 1 0 59.59 2.30 -2 -1 0 50.09 2.50 -2 1 0 50.69 3.00 -2 -1 0 68.59 3.00 2 -1 0 72.29 2.80 2 1 0 54.29 2.70 2 -1 0 72.19 3.00 -2 -1 0 53.29 2.70 2 1 0 70.49 2.90 2 -2 0 5375.46 115.59 2 2 0 5592.04 114.19 -2 2 0 5245.08 115.39 -2 -2 0 5533.15 113.89 2 -3 0 614.64 12.90 -2 3 0 623.44 13.30 -2 -3 0 612.04 12.60 -2 3 0 604.04 12.80 2 3 0 630.74 13.40 2 -3 0 611.04 13.30 2 -3 0 613.54 12.90 2 3 0 607.74 12.60 -2 3 0 616.94 12.90 -2 -3 0 610.64 12.30 2 -3 0 655.83 14.30 -2 3 0 604.44 14.00 -2 -3 0 611.34 13.30 -2 -3 0 608.54 12.50 2 3 0 628.24 12.60 2 -3 0 582.94 12.70 2 -4 0 117.49 4.00 2 4 0 119.69 3.40 2 -4 0 120.29 4.40 2 4 0 112.99 4.50 2 -4 0 121.89 3.80 -2 -4 0 119.69 3.40 -2 -4 0 126.89 4.80 -2 4 0 128.39 4.60 -2 -4 0 121.19 3.70 2 -4 0 126.99 6.20 -2 -4 0 115.69 4.50 2 4 0 120.59 4.30 2 -4 0 122.19 4.50 -2 4 0 116.19 3.80 -2 4 0 123.59 3.90 -2 -5 0 348.07 8.40 2 5 0 331.57 7.30 -2 -5 0 330.27 7.20 2 -5 0 335.77 7.90 2 5 0 338.27 7.30 -2 5 0 325.77 7.80 2 -5 0 338.67 10.00 2 -5 0 338.57 7.90 -2 -5 0 351.56 8.90 2 -5 0 331.87 8.20 -2 5 0 336.57 7.80 2 5 0 343.57 8.90 -2 -5 0 340.07 7.30 2 -5 0 349.57 10.20 -2 5 0 335.17 9.00 -2 -6 0 96.09 2.50 2 -6 0 102.89 4.70 2 -6 0 96.59 3.90 -2 6 0 92.39 3.30 2 -6 0 101.69 5.60 -2 -6 0 99.99 5.00 -2 6 0 95.09 3.30 2 -6 0 94.89 3.30 -2 -6 0 82.19 2.60 -2 6 0 97.89 4.60 -2 -6 0 96.59 4.20 2 6 0 94.19 2.60 2 6 0 87.89 2.60 2 -6 0 89.99 3.30 -2 -7 0 1.00 2.30 -2 -7 0 1.10 2.10 2 -7 0 -0.30 1.70 -2 7 0 -2.80 2.00 2 -7 0 -0.50 1.10 -2 7 0 -0.50 0.90 2 -7 0 0.30 1.90 -2 7 0 -0.40 1.70 2 -7 0 -0.50 2.50 -2 -7 0 0.60 1.90 2 -7 0 -3.30 1.60 -2 -7 0 -1.90 1.80 -2 8 0 37.30 1.80 -2 -8 0 37.10 4.30 2 -8 0 36.20 4.00 2 -8 0 35.80 1.40 2 -8 0 43.90 5.20 -2 -8 0 38.40 4.10 -2 -8 0 32.40 5.60 2 -8 0 43.10 3.30 2 -8 0 36.30 1.50 2 -9 0 115.09 5.20 -2 -9 0 110.59 5.80 -2 -9 0 104.59 6.50 -2 -9 0 103.49 5.60 2 -9 0 112.99 4.80 2 -9 0 112.79 7.50 2 -9 0 100.49 6.10 2 -9 0 117.99 8.20 -2 -10 0 6.50 3.10 -2 -10 0 11.10 4.00 -2 -10 0 8.30 2.90 2 -10 0 8.30 2.50 -2 -10 0 11.90 3.20 2 -10 0 1.60 4.10 2 -10 0 12.40 3.30 2 -10 0 3.10 3.90 2 -10 0 12.40 2.30 -2 -11 0 6.40 2.70 2 -11 0 10.00 2.90 -2 -11 0 6.10 2.80 2 -11 0 7.20 3.60 -2 -11 0 9.10 3.20 2 -11 0 1.60 3.50 2 -11 0 10.80 2.60 -2 -11 0 7.20 3.50 -3 0 0 3.90 1.70 -3 0 0 1.50 1.60 3 0 0 9.20 1.90 3 0 0 8.70 1.90 -3 0 0 4.30 1.70 -3 1 0 2.10 1.70 -3 1 0 -1.00 1.50 3 -1 0 -1.30 1.50 3 -1 0 0.80 1.50 3 1 0 -2.00 1.40 3 1 0 0.70 1.50 -3 -1 0 -1.00 1.40 -3 1 0 0.00 1.40 3 -1 0 0.50 1.60 -3 -1 0 -0.10 1.10 3 -1 0 0.00 1.30 -3 -1 0 -2.80 1.40 -3 1 0 3.80 1.40 -3 -1 0 0.00 1.50 3 1 0 0.70 1.20 3 1 0 -0.80 1.40 3 -1 0 0.40 1.40 -3 -1 0 1.90 1.70 3 2 0 2.50 1.60 3 2 0 0.10 1.30 -3 2 0 1.20 1.60 -3 2 0 2.20 1.40 -3 2 0 2.70 1.50 3 -2 0 1.20 1.50 -3 2 0 1.90 1.50 3 2 0 2.10 1.40 3 -2 0 2.60 1.40 3 -2 0 0.00 1.30 -3 -2 0 1.50 1.30 3 -2 0 1.90 1.50 -3 -2 0 0.90 1.80 3 -2 0 -1.60 1.10 -3 2 0 0.10 1.40 -3 -2 0 1.30 1.40 -3 3 0 15.50 2.30 -3 3 0 13.80 2.00 3 -3 0 14.20 3.60 3 -3 0 8.40 1.80 3 -3 0 5.00 2.60 3 -3 0 13.00 2.00 -3 -4 0 -0.60 1.90 3 4 0 -1.90 1.10 -3 -4 0 1.60 1.20 3 4 0 4.10 1.90 3 -4 0 3.70 1.60 -3 -4 0 -0.30 0.90 3 4 0 0.10 1.20 -3 -4 0 -0.20 1.20 -3 -5 0 -2.20 1.00 3 -5 0 -2.50 1.50 -3 -5 0 0.90 1.80 -3 5 0 -1.00 1.30 3 5 0 -2.30 1.00 3 5 0 -0.40 1.10 3 -5 0 0.20 1.40 -3 5 0 0.50 1.40 3 5 0 0.80 1.70 3 -5 0 0.50 2.10 -3 -5 0 -0.30 1.10 3 -5 0 3.00 1.70 -3 -5 0 -0.10 1.10 3 -5 0 0.30 1.40 -3 5 0 1.00 1.60 3 6 0 1.20 2.10 3 -6 0 -1.70 1.40 -3 6 0 -1.70 1.30 -3 -6 0 -0.70 1.00 -3 -6 0 1.10 2.20 -3 6 0 -3.00 1.20 3 -6 0 1.50 1.70 3 6 0 1.80 1.10 -3 -6 0 -0.70 1.10 3 -6 0 -2.30 2.40 3 -6 0 -0.20 2.10 3 -6 0 0.10 1.50 -3 -6 0 0.40 1.40 3 6 0 2.30 1.10 -3 6 0 -0.70 1.80 -3 -7 0 5.40 2.80 -3 7 0 -0.40 1.50 -3 -7 0 -0.30 0.90 -3 7 0 1.90 2.10 3 7 0 0.20 0.90 3 -7 0 -2.30 1.40 3 -7 0 1.90 2.10 3 -7 0 1.30 2.50 -3 7 0 1.20 1.40 3 7 0 4.70 2.20 -3 -7 0 -0.30 1.60 -3 -7 0 7.20 2.70 -3 -7 0 1.50 1.00 3 -7 0 -0.60 2.90 3 7 0 1.20 1.00 3 -7 0 0.00 1.50 -3 -8 0 2.30 1.90 -3 8 0 -0.30 2.30 3 -8 0 -1.10 1.40 3 -8 0 -3.00 3.70 -3 -8 0 2.90 3.00 3 -8 0 -2.20 2.50 -3 8 0 0.20 1.20 -3 8 0 -0.70 1.30 -3 -8 0 -1.00 2.90 -3 -8 0 2.90 2.80 3 -8 0 4.30 2.00 -3 -9 0 -1.60 3.00 -3 -9 0 -3.70 2.40 -3 9 0 -5.90 2.10 3 -9 0 -1.80 2.10 3 -9 0 -0.20 0.80 -3 -9 0 -1.90 1.80 3 -9 0 6.90 4.30 3 -9 0 -3.30 2.40 -3 -9 0 -1.20 2.40 3 -9 0 1.60 1.90 3 -9 0 1.00 1.40 -3 9 0 1.70 1.20 3 -10 0 7.40 2.20 3 -10 0 -0.10 3.90 3 -10 0 0.60 3.30 -3 -10 0 2.50 2.80 -3 -10 0 2.00 3.00 3 -10 0 2.30 2.10 -3 -10 0 -2.40 2.70 3 -10 0 0.80 2.60 4 0 0 366.26 9.50 -4 0 0 365.96 9.00 -4 0 0 369.66 9.40 4 0 0 357.66 8.90 -4 0 0 361.76 9.20 4 0 0 387.36 9.40 -4 0 0 370.66 9.50 -4 0 0 376.56 9.50 4 0 0 377.36 9.50 4 0 0 377.06 9.50 -4 1 0 248.78 7.10 -4 -1 0 237.68 6.40 4 1 0 241.38 7.10 -4 1 0 245.28 6.80 -4 -1 0 226.08 6.80 4 -1 0 239.88 7.10 4 1 0 240.18 6.90 -4 -1 0 244.28 7.00 -4 -1 0 253.27 6.90 4 -1 0 248.88 7.10 4 -1 0 251.57 6.90 4 1 0 243.58 6.70 -4 1 0 241.28 7.10 4 -1 0 248.88 7.00 4 1 0 231.18 7.10 -4 -1 0 246.18 7.20 -4 1 0 238.68 6.90 4 -1 0 240.78 7.00 -4 1 0 243.78 7.00 4 -2 0 1586.74 31.10 -4 2 0 1516.55 31.50 4 -2 0 1549.45 33.10 -4 -2 0 1510.65 30.90 4 2 0 1503.85 35.40 4 -2 0 1529.05 31.10 -4 2 0 1531.35 31.00 4 -2 0 1557.54 31.30 -4 -2 0 1564.74 31.50 4 -2 0 1551.64 31.10 -4 2 0 1562.94 31.10 -4 2 0 1567.64 31.20 4 2 0 1547.35 30.10 -4 -2 0 1512.95 30.20 -4 -2 0 1500.95 33.70 4 2 0 1495.45 30.90 -4 -2 0 1505.05 31.60 4 2 0 1642.14 32.40 -4 3 0 31.70 3.30 4 3 0 30.70 2.00 4 3 0 19.90 3.00 -4 3 0 23.20 3.20 4 3 0 32.30 3.30 4 -3 0 36.10 3.30 -4 -3 0 32.20 3.10 -4 -3 0 25.60 4.40 4 -3 0 39.50 3.80 -4 -3 0 37.40 3.50 -4 -4 0 326.57 6.90 -4 4 0 321.87 8.90 -4 -4 0 312.87 9.20 -4 -4 0 323.67 8.40 -4 -4 0 329.67 8.40 4 -4 0 315.47 8.80 4 4 0 317.67 9.10 4 4 0 334.17 8.40 -4 4 0 326.87 9.50 4 -4 0 309.27 9.80 -4 4 0 318.67 8.70 4 4 0 322.57 6.90 4 -4 0 326.37 9.00 4 4 0 330.27 8.40 4 -4 0 309.27 8.60 -4 4 0 322.57 9.90 4 5 0 105.19 4.20 -4 5 0 113.89 4.90 -4 -5 0 107.39 2.90 4 -5 0 111.49 6.00 -4 -5 0 106.79 4.20 4 -5 0 106.09 5.30 4 5 0 108.09 4.20 -4 5 0 102.59 5.60 4 5 0 110.39 5.00 -4 5 0 110.79 4.60 -4 -5 0 119.99 5.60 -4 -5 0 103.69 4.20 4 -5 0 109.79 4.70 4 -5 0 104.39 4.50 4 -5 0 107.59 5.00 -4 5 0 102.49 4.50 4 6 0 500.75 11.60 -4 -6 0 501.25 10.40 4 -6 0 512.95 14.70 4 -6 0 494.35 12.20 -4 -6 0 496.95 13.20 -4 -6 0 505.15 11.60 4 -6 0 498.55 12.30 4 -6 0 518.05 13.30 -4 6 0 481.85 15.00 4 6 0 498.65 11.60 -4 6 0 513.55 12.40 -4 6 0 514.45 13.30 4 6 0 506.05 13.30 -4 -6 0 511.25 11.60 4 -6 0 533.85 12.50 4 -7 0 24.30 3.60 4 -7 0 29.10 3.00 -4 -7 0 27.20 2.60 -4 -7 0 25.30 3.70 -4 7 0 24.30 2.80 -4 7 0 20.30 3.10 4 -7 0 22.60 3.00 -4 -7 0 18.80 1.90 4 -7 0 24.20 4.40 -4 7 0 22.50 2.80 4 7 0 22.80 3.50 4 -7 0 25.10 2.90 4 7 0 26.50 2.30 -4 -7 0 25.30 2.40 4 7 0 27.20 2.40 4 -8 0 39.40 3.10 4 8 0 35.40 2.10 -4 -8 0 33.90 2.00 -4 8 0 44.40 3.20 -4 -8 0 40.70 4.50 4 -8 0 36.90 3.20 4 -8 0 36.00 3.50 4 8 0 35.40 2.10 -4 -8 0 40.40 2.10 -4 8 0 39.60 4.00 4 -8 0 39.60 4.50 -4 -8 0 28.20 3.20 4 -8 0 42.10 5.40 4 8 0 39.90 4.00 -4 -9 0 -2.30 2.10 -4 -9 0 0.10 2.60 4 -9 0 0.00 1.80 4 -9 0 -5.30 3.10 4 -9 0 -0.30 1.50 -4 -9 0 -1.20 3.00 -4 9 0 1.30 1.50 -4 -10 0 15.90 3.60 -4 -10 0 21.60 4.40 -4 10 0 26.80 3.20 4 -10 0 23.40 2.90 4 -10 0 16.20 3.50 4 -10 0 19.70 5.00 4 -10 0 14.50 4.90 4 -10 0 17.90 1.60 4 -10 0 18.30 2.90 -4 -10 0 25.20 1.70 -4 -10 0 14.50 3.80 -5 0 0 -1.20 1.90 -5 0 0 -1.50 2.00 5 0 0 -3.10 1.80 5 0 0 -1.30 1.50 5 0 0 -3.40 1.60 -5 0 0 0.00 2.00 -5 0 0 -1.30 1.60 5 0 0 -0.20 2.00 5 0 0 2.30 2.00 5 0 0 -1.80 1.90 -5 0 0 -2.00 1.60 5 -1 0 -2.10 1.80 5 1 0 -0.30 2.00 -5 -1 0 -0.90 1.90 5 -1 0 -0.30 1.90 5 1 0 -3.00 1.60 5 1 0 0.80 2.00 5 -1 0 0.10 2.00 -5 1 0 -2.80 1.90 -5 -1 0 2.40 1.60 5 -1 0 -2.60 1.90 -5 1 0 -1.10 2.00 -5 1 0 0.60 1.60 -5 -1 0 0.10 2.20 5 1 0 1.80 2.10 -5 1 0 -3.00 1.70 -5 -1 0 1.90 2.70 -5 -1 0 0.70 1.80 -5 1 0 1.60 2.10 5 2 0 1.80 2.00 -5 -2 0 2.10 1.60 5 2 0 7.20 2.50 -5 -2 0 5.90 2.40 5 2 0 7.70 2.50 -5 -2 0 4.80 2.50 -5 -2 0 1.00 2.10 -5 -3 0 2.10 2.40 5 3 0 2.80 1.90 -5 -3 0 0.60 2.00 -5 -3 0 2.70 2.00 -5 -3 0 5.00 2.10 5 3 0 2.90 2.00 5 3 0 3.50 1.40 5 3 0 3.50 2.20 -5 3 0 5.70 2.20 5 -4 0 -0.40 1.90 -5 4 0 4.40 2.20 5 -4 0 1.70 2.50 5 4 0 2.00 2.40 -5 -4 0 -1.70 1.70 5 -4 0 5.60 2.30 5 4 0 0.00 0.90 -5 4 0 2.20 2.00 -5 -4 0 -1.90 1.80 -5 4 0 1.30 1.90 -5 -4 0 -4.30 2.30 -5 4 0 -2.20 2.10 -5 4 0 1.10 1.90 5 4 0 -1.40 1.80 -5 5 0 -2.10 2.30 -5 -5 0 -1.70 1.60 -5 5 0 -3.20 2.00 5 -5 0 -3.70 1.80 5 5 0 -5.20 1.50 -5 5 0 -4.60 1.60 -5 5 0 -2.80 1.70 5 -5 0 -2.50 1.90 -5 -5 0 -1.90 1.70 5 5 0 -0.30 1.60 5 5 0 -1.70 2.30 5 -5 0 -2.20 2.60 -5 -5 0 -0.50 2.50 5 -5 0 -1.60 1.90 -5 -6 0 -0.40 1.70 5 6 0 1.00 2.40 -5 6 0 -0.90 2.00 -5 6 0 -2.50 1.80 -5 -6 0 2.30 1.90 5 -6 0 -1.30 2.10 5 -6 0 -0.20 3.00 -5 6 0 -2.90 2.10 5 -6 0 -5.40 1.90 -5 -6 0 0.40 2.60 5 6 0 4.40 1.70 5 -6 0 1.70 2.30 5 6 0 -2.20 1.60 5 -6 0 1.20 2.50 5 -7 0 -2.20 3.10 5 -7 0 0.40 2.30 5 7 0 2.40 2.70 -5 7 0 1.20 2.20 5 -7 0 -2.40 2.70 5 7 0 1.20 1.70 -5 -7 0 -1.30 3.00 5 -7 0 -3.40 2.00 -5 -7 0 -3.10 1.50 5 -8 0 0.20 2.30 5 8 0 0.00 2.30 5 -8 0 -2.10 2.10 -5 8 0 1.40 2.00 -5 -8 0 -0.20 1.50 5 8 0 -0.70 1.30 5 -8 0 -0.80 2.00 5 -8 0 -1.80 2.30 -5 8 0 -0.60 2.40 -5 -8 0 -0.80 1.40 5 -8 0 -6.30 3.00 -5 -8 0 1.40 3.00 5 -9 0 4.80 3.20 -5 -9 0 2.10 2.50 -5 -9 0 5.20 3.50 -5 -9 0 1.00 1.00 5 -9 0 1.00 2.30 -5 -9 0 -0.10 0.90 -5 9 0 -0.40 1.70 5 -9 0 -0.90 3.60 5 -9 0 -2.60 1.70 5 -9 0 1.90 2.10 5 9 0 0.90 1.60 -5 -9 0 3.80 3.20 5 -10 0 -1.10 1.50 5 -10 0 -0.20 1.70 -5 -10 0 -0.70 2.90 5 -10 0 2.30 2.50 -5 -10 0 -4.10 3.10 5 -10 0 -1.80 2.70 -5 -10 0 3.40 2.80 -5 10 0 2.00 2.00 6 0 0 1576.64 32.90 6 0 0 1552.14 32.70 6 0 0 1598.04 33.10 6 0 0 1567.64 32.30 -6 0 0 1548.45 32.30 6 0 0 1550.14 33.10 -6 0 0 1574.44 33.10 -6 0 0 1574.84 32.70 -6 0 0 1545.55 32.80 6 0 0 1554.84 33.00 -6 0 0 1589.84 33.00 -6 1 0 10.40 2.60 -6 -1 0 6.00 2.20 -6 -1 0 5.70 2.70 -6 -1 0 7.00 2.60 -6 1 0 6.20 2.10 6 -1 0 6.90 2.30 6 1 0 5.40 2.30 -6 1 0 4.90 2.50 6 -1 0 8.10 2.50 -6 1 0 5.80 2.20 -6 1 0 5.40 2.50 6 1 0 3.40 2.30 6 1 0 5.70 2.40 6 -1 0 5.10 2.40 -6 -1 0 5.10 2.50 6 -1 0 10.40 2.70 6 -1 0 3.30 2.20 6 1 0 5.50 2.60 -6 2 0 5.70 2.50 -6 -2 0 3.40 2.70 -6 -2 0 3.80 2.50 6 -2 0 3.90 2.10 -6 2 0 8.20 2.60 6 2 0 4.20 2.00 6 2 0 3.50 2.40 -6 2 0 5.30 2.40 -6 2 0 5.00 2.50 6 -2 0 2.50 2.30 6 -2 0 7.40 2.70 -6 -2 0 3.10 2.20 -6 2 0 2.80 2.00 6 -2 0 4.60 2.50 6 2 0 4.90 2.50 6 -2 0 4.90 2.70 -6 -2 0 3.20 2.40 -6 -2 0 3.60 1.80 6 2 0 4.20 2.50 -6 -3 0 32.50 3.80 6 -3 0 35.30 4.10 6 -3 0 46.60 4.30 -6 -3 0 29.20 3.90 6 -3 0 46.40 4.30 -6 3 0 35.50 3.80 6 -3 0 33.70 3.70 -6 3 0 38.80 3.80 -6 3 0 41.10 3.90 6 3 0 35.10 4.00 6 3 0 33.60 3.70 -6 -3 0 29.70 2.80 6 -3 0 44.10 3.90 6 3 0 37.00 3.80 -6 3 0 43.10 3.70 -6 -3 0 31.40 3.60 -6 -3 0 34.50 3.80 -6 3 0 31.20 3.90 6 3 0 35.40 3.10 -6 4 0 31.10 3.60 -6 4 0 33.10 3.80 -6 4 0 30.50 4.50 6 4 0 25.70 3.20 -6 -4 0 26.70 3.40 6 4 0 28.90 2.20 -6 -4 0 21.40 2.60 6 4 0 26.30 3.40 -6 -4 0 29.30 3.60 -6 -4 0 31.80 3.70 6 -4 0 28.30 3.50 -6 -4 0 21.90 3.70 6 -4 0 27.80 3.50 -6 4 0 38.50 4.00 6 4 0 28.20 3.80 6 -4 0 25.60 4.00 -6 4 0 31.50 4.20 6 -4 0 28.80 3.70 6 -4 0 25.40 3.70 -6 5 0 48.60 4.90 -6 -5 0 48.80 5.20 6 5 0 39.30 4.20 -6 -5 0 36.40 3.80 6 -5 0 47.60 5.20 -6 -5 0 40.50 3.80 6 5 0 39.40 4.20 -6 5 0 42.70 4.20 6 -5 0 41.30 4.10 6 -5 0 40.80 4.30 6 5 0 40.70 3.70 6 -5 0 42.30 4.20 -6 5 0 41.60 4.20 -6 5 0 34.80 4.00 6 -5 0 35.00 3.90 6 -6 0 51.89 4.70 6 -6 0 56.79 4.90 6 6 0 60.59 4.10 -6 -6 0 50.79 4.10 6 -6 0 48.60 4.50 6 6 0 54.19 5.00 -6 -6 0 56.69 5.60 6 -6 0 63.69 6.00 6 -6 0 60.59 4.80 -6 -6 0 51.89 4.60 6 -7 0 19.10 3.40 -6 7 0 24.20 3.50 -6 -7 0 28.00 3.20 6 -7 0 22.00 3.40 6 -7 0 23.30 4.00 6 -7 0 26.10 3.70 -6 -7 0 23.40 4.30 -6 -7 0 24.90 3.10 6 7 0 22.00 2.80 -6 7 0 25.70 4.00 6 -7 0 26.10 4.80 6 7 0 20.60 3.70 6 -8 0 14.90 2.70 6 -8 0 8.20 2.90 -6 8 0 9.40 2.70 -6 -8 0 8.40 2.30 6 8 0 8.10 3.00 6 -8 0 7.20 2.80 6 -8 0 6.30 2.70 -6 -8 0 5.50 4.00 6 -8 0 6.30 4.00 -6 -8 0 11.10 2.30 -6 -9 0 8.00 1.90 -6 9 0 2.60 2.30 6 9 0 8.10 1.90 6 -9 0 6.60 2.70 6 -9 0 7.90 4.00 -6 -9 0 7.10 1.80 -6 -9 0 8.80 4.20 6 -9 0 4.00 2.60 6 -9 0 3.00 3.10 6 -9 0 6.70 3.00 -6 -9 0 2.70 3.40 -7 0 0 -2.00 2.00 7 0 0 0.00 2.60 -7 0 0 1.20 1.80 -7 0 0 -0.80 2.50 7 0 0 1.50 2.50 7 0 0 0.50 2.30 7 0 0 -1.60 2.10 -7 0 0 -0.40 2.30 7 0 0 3.20 2.50 7 0 0 -3.20 2.10 -7 0 0 -0.90 2.40 -7 1 0 2.30 2.20 7 1 0 3.30 2.60 -7 -1 0 1.30 2.40 7 1 0 -1.00 2.40 7 -1 0 0.50 2.50 -7 1 0 -0.50 2.00 7 -1 0 -0.60 2.20 -7 -1 0 0.70 2.00 -7 -1 0 -1.10 1.90 7 1 0 -1.50 2.40 7 -1 0 0.60 2.40 7 -1 0 -2.90 2.50 7 -1 0 -0.10 2.80 7 1 0 -1.20 2.20 -7 -1 0 -0.30 2.60 7 -1 0 1.80 2.40 -7 1 0 -2.70 2.40 -7 1 0 2.90 2.70 -7 -1 0 3.60 2.90 -7 1 0 0.00 2.40 7 2 0 1.20 2.20 -7 2 0 6.00 3.00 7 2 0 -0.90 2.40 -7 -2 0 -2.30 2.40 7 2 0 -1.60 2.50 -7 2 0 4.90 2.80 7 -2 0 1.40 2.70 -7 -2 0 -3.20 2.90 7 -2 0 3.40 2.70 -7 -2 0 0.00 2.60 7 2 0 -1.90 2.60 -7 -2 0 1.40 2.20 7 -2 0 6.50 2.70 -7 2 0 2.20 2.80 -7 2 0 4.50 2.70 7 -2 0 1.20 2.80 -7 2 0 10.20 2.60 7 -2 0 4.20 2.80 -7 -2 0 1.70 1.80 7 -3 0 2.30 3.00 -7 -3 0 -1.50 2.50 -7 3 0 2.70 2.20 -7 3 0 2.90 2.80 7 -3 0 5.90 3.00 7 -3 0 0.70 2.70 7 -3 0 2.80 2.70 -7 -3 0 -4.10 2.40 7 3 0 -2.70 2.50 -7 3 0 1.80 2.60 -7 3 0 2.30 2.90 -7 3 0 0.90 2.50 -7 -3 0 -0.60 2.20 -7 -3 0 -0.50 1.70 7 3 0 -1.10 2.20 7 -3 0 7.50 2.80 -7 -3 0 1.60 3.20 -7 4 0 -3.90 2.60 7 4 0 0.50 1.50 -7 4 0 5.80 2.40 -7 4 0 -0.50 2.60 7 4 0 -2.90 2.10 -7 4 0 -4.60 2.40 -7 -4 0 -0.60 2.50 -7 4 0 0.50 2.50 -7 -4 0 -1.90 2.70 -7 -4 0 0.30 1.90 -7 -4 0 -0.90 2.40 7 4 0 -3.00 2.50 7 -4 0 -0.20 2.90 7 -4 0 -5.30 2.50 7 4 0 -4.60 2.00 -7 -4 0 -3.30 2.80 7 -4 0 4.10 3.20 7 -4 0 0.90 2.60 7 -4 0 -2.10 2.70 -7 -5 0 -2.40 2.50 -7 -5 0 -1.00 1.90 7 -5 0 1.80 2.80 -7 -5 0 0.80 2.70 7 -5 0 4.70 2.70 -7 5 0 1.60 2.70 7 5 0 -0.60 2.30 -7 5 0 6.90 5.60 7 5 0 -1.30 2.90 7 -5 0 -3.50 2.90 -7 -5 0 -6.70 3.30 7 -5 0 0.10 2.80 7 -5 0 -1.90 2.60 7 6 0 2.60 2.40 7 -6 0 -3.00 2.70 -7 6 0 -2.20 2.80 -7 6 0 0.40 2.60 7 -6 0 0.20 2.80 7 -6 0 -3.10 2.80 7 -6 0 -2.20 3.40 -7 -6 0 -1.90 2.20 -7 -6 0 -1.00 2.40 7 -6 0 -2.80 2.50 -7 -7 0 -2.20 2.10 7 -7 0 2.70 3.60 7 -7 0 -2.90 2.60 -7 -7 0 2.50 3.40 7 -7 0 3.10 2.70 -7 -7 0 1.70 2.30 7 -7 0 -0.60 2.50 7 7 0 -0.80 1.90 -7 -8 0 -2.30 3.00 -7 8 0 -1.20 2.70 7 8 0 -0.50 2.10 7 -8 0 2.70 2.90 7 -8 0 -8.10 2.80 7 -8 0 -4.70 3.30 -7 -8 0 -1.80 2.10 7 -8 0 3.70 2.90 7 -8 0 2.60 2.90 -7 -8 0 1.30 2.20 -7 -9 0 -1.90 3.40 7 -9 0 -5.60 3.00 -7 9 0 -1.30 2.90 7 9 0 -1.60 2.10 7 -9 0 2.10 3.90 7 -9 0 2.00 2.70 7 -9 0 3.40 2.40 -7 -9 0 1.20 2.00 7 -9 0 -4.80 2.80 -7 -9 0 0.20 1.80 8 0 0 117.69 6.50 8 0 0 116.69 6.90 -8 0 0 127.09 6.70 8 0 0 117.69 6.70 -8 0 0 117.59 6.60 -8 0 0 119.39 6.20 -8 0 0 115.59 6.80 -8 0 0 119.99 6.30 8 0 0 122.29 6.70 8 -1 0 15.80 3.60 -8 -1 0 9.10 2.70 8 1 0 0.50 2.80 8 1 0 2.00 2.80 8 -1 0 17.20 3.80 8 1 0 7.60 3.20 -8 -1 0 8.90 3.50 -8 1 0 14.90 3.60 -8 1 0 12.70 3.50 8 -1 0 18.30 4.00 8 -1 0 14.90 3.90 8 -1 0 21.40 4.00 -8 1 0 9.50 3.20 -8 1 0 7.30 2.60 -8 1 0 20.70 4.20 -8 -1 0 3.00 3.30 -8 -1 0 5.60 3.20 -8 -1 0 3.10 2.60 8 1 0 4.60 2.90 8 -1 0 15.30 3.60 -8 -2 0 62.69 4.50 -8 -2 0 54.39 4.70 -8 2 0 72.09 5.70 8 -2 0 64.49 5.50 -8 2 0 76.69 5.70 -8 2 0 66.59 5.80 8 2 0 60.59 5.40 8 -2 0 72.69 5.40 -8 -2 0 72.99 5.90 8 2 0 68.29 5.60 8 -2 0 72.69 6.00 8 -2 0 58.09 5.20 -8 -2 0 67.09 5.60 -8 -2 0 57.89 5.80 8 2 0 62.79 5.60 -8 2 0 62.69 4.90 8 2 0 63.49 5.20 8 -2 0 63.29 7.20 8 -2 0 68.39 5.50 8 -3 0 0.90 3.20 8 3 0 2.20 3.20 -8 3 0 -1.30 2.90 -8 3 0 3.70 2.90 -8 -3 0 1.00 2.10 8 -3 0 2.40 5.10 -8 3 0 2.20 3.10 8 3 0 2.10 2.40 8 -3 0 3.60 3.00 8 -3 0 0.60 3.30 -8 3 0 0.70 2.40 -8 -3 0 -3.00 3.10 -8 -3 0 2.90 3.10 8 3 0 1.10 3.50 -8 3 0 -3.20 5.70 -8 -3 0 0.80 2.90 8 -3 0 2.90 2.80 8 -3 0 0.90 3.20 8 3 0 1.80 3.10 8 -4 0 9.60 3.80 8 -4 0 3.60 3.80 8 -4 0 10.90 4.00 -8 4 0 6.80 3.20 8 -4 0 10.40 3.40 -8 -4 0 5.90 3.00 8 -4 0 8.60 3.60 -8 4 0 5.40 3.60 -8 -4 0 10.90 4.40 -8 -4 0 4.90 3.40 -8 -4 0 9.40 2.50 8 4 0 15.00 2.50 -8 4 0 9.30 2.60 8 4 0 9.90 3.40 8 -5 0 -3.50 2.70 -8 5 0 -1.00 3.30 8 -5 0 -1.40 3.30 -8 -5 0 0.60 2.80 -8 -5 0 -2.20 1.90 8 -5 0 2.70 3.40 -8 -5 0 -5.60 2.30 8 -5 0 1.10 3.10 8 5 0 0.70 0.90 -8 -5 0 -0.30 3.50 8 5 0 -0.40 2.70 -8 5 0 2.40 2.80 8 -6 0 9.80 3.40 8 -6 0 9.50 4.30 8 -6 0 3.90 3.40 -8 6 0 10.40 5.30 -8 -6 0 12.30 4.50 8 -6 0 9.80 3.70 -8 -6 0 13.50 3.10 8 -6 0 6.40 3.10 -8 -6 0 8.70 2.20 -8 -6 0 11.00 3.20 8 -7 0 58.29 6.80 -8 -7 0 49.00 5.20 8 -7 0 41.90 5.10 8 -7 0 37.20 5.00 8 -7 0 48.00 5.00 -8 -7 0 35.90 5.50 -8 -7 0 35.10 4.30 -8 7 0 45.50 5.00 8 -7 0 43.90 5.90 8 7 0 39.00 4.30 -8 -7 0 38.40 3.70 8 -8 0 111.39 7.40 -8 -8 0 99.29 5.80 8 -8 0 83.79 6.20 -8 -8 0 96.89 5.30 8 8 0 103.89 5.90 8 -8 0 110.69 6.50 -8 -8 0 103.09 7.70 8 -8 0 118.29 9.00 -8 8 0 102.39 6.60 -9 0 0 -2.80 3.60 -9 0 0 5.50 3.60 9 0 0 10.30 3.70 9 0 0 -0.10 3.40 -9 0 0 -6.90 3.10 -9 0 0 -5.90 2.60 9 0 0 0.90 3.40 -9 -1 0 2.20 3.70 9 1 0 5.60 3.40 -9 -1 0 2.60 3.80 9 -1 0 3.90 3.70 9 -1 0 3.90 3.40 -9 1 0 2.60 3.70 9 1 0 4.80 3.60 9 -1 0 0.40 3.40 9 -1 0 1.60 3.40 -9 -1 0 5.10 2.90 -9 1 0 -1.50 2.70 -9 1 0 5.30 3.80 9 -1 0 2.70 3.00 -9 -1 0 1.60 3.60 -9 2 0 -2.50 2.80 -9 -2 0 7.10 4.00 -9 -2 0 1.20 3.10 9 -2 0 -4.40 2.80 -9 2 0 -3.50 3.40 9 -2 0 -1.30 2.90 9 -2 0 2.80 3.20 -9 2 0 -2.80 3.20 -9 2 0 3.60 3.50 9 -2 0 -0.70 3.40 9 2 0 -5.00 3.00 9 2 0 -4.10 2.60 -9 -2 0 -2.30 2.60 -9 -2 0 4.70 6.40 9 -2 0 2.60 3.70 9 -3 0 -0.90 3.20 9 -3 0 1.40 3.30 9 3 0 -3.40 2.80 -9 -3 0 0.40 3.40 -9 -3 0 2.10 3.30 -9 3 0 -4.10 2.70 9 -3 0 -3.50 2.90 -9 3 0 -0.80 3.40 9 -3 0 -0.10 3.60 -9 -3 0 -0.30 2.40 9 3 0 4.10 3.10 -9 -3 0 -4.20 3.20 -9 -4 0 2.10 2.30 -9 -4 0 -6.20 3.10 -9 -4 0 4.60 3.50 9 -4 0 -1.60 3.00 9 -4 0 2.30 3.60 -9 4 0 -1.60 2.80 -9 -4 0 -0.90 3.00 9 4 0 0.70 3.40 9 -4 0 -2.80 3.30 9 -4 0 -2.70 3.10 9 4 0 -0.70 2.00 -9 4 0 -9.20 3.00 -9 5 0 -2.20 3.30 9 5 0 0.20 3.30 9 -5 0 4.40 3.60 -9 5 0 -1.80 3.00 -9 -5 0 1.70 2.00 9 -5 0 -4.10 2.80 -9 -5 0 1.70 2.90 9 -5 0 0.10 3.50 -9 -5 0 0.10 3.00 9 -5 0 -0.60 3.50 9 5 0 0.30 1.10 -9 -5 0 2.70 3.70 9 -6 0 0.40 3.90 -9 6 0 5.40 3.40 9 6 0 -0.90 2.60 9 -6 0 -2.40 2.60 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2.50 -2 -11 -3 3.10 2.80 2 -11 3 -1.40 3.60 2 -11 3 0.10 2.80 2 -11 3 4.90 3.50 -2 -11 -3 4.70 2.60 -3 0 -3 1.20 1.60 -3 0 3 -0.20 1.50 3 0 -3 1.30 1.60 -3 0 3 -0.40 1.50 3 0 3 -2.10 1.50 -3 0 3 -1.00 1.20 -3 0 3 -2.60 1.50 -3 0 3 -0.50 1.50 -3 0 -3 -1.10 1.50 3 0 3 -2.40 1.50 -3 0 -3 1.80 1.30 3 0 -3 -1.50 2.50 -3 0 -3 -0.50 1.60 -3 0 -3 -0.30 1.30 3 0 -3 1.30 1.40 3 0 -3 -0.70 1.50 3 0 -3 -1.50 1.30 3 0 -3 -3.10 1.50 -3 0 3 0.90 1.10 3 0 3 1.10 1.50 -3 -1 3 2074.09 39.80 3 -1 -3 2075.79 40.00 3 1 3 2062.89 39.80 3 1 3 2036.70 39.90 -3 -1 3 2080.89 39.80 -3 -1 3 2062.99 39.80 3 -1 -3 2055.19 39.60 -3 1 -3 2077.39 40.00 -3 -1 3 2010.50 38.70 3 1 3 2017.10 39.80 -3 1 -3 2057.39 39.90 3 -1 -3 2068.39 39.90 3 -1 -3 2065.19 39.90 -3 1 -3 2075.49 40.20 -3 -1 3 2113.29 40.10 -3 1 -3 2023.00 39.80 3 -1 -3 1982.30 39.80 -3 -1 3 2065.29 40.00 3 -1 -3 2042.70 40.70 -3 1 -3 2049.49 39.40 3 1 -3 2064.69 39.80 3 -1 3 2040.20 40.00 3 -1 3 2071.69 40.10 3 -1 3 2067.39 39.50 -3 -1 -3 2082.69 39.90 -3 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12.30 4.60 -11 4 3 4.00 3.70 11 4 -3 3.10 4.00 11 -4 3 8.60 4.60 -11 4 3 11.90 4.50 11 -4 3 4.70 4.60 -11 -4 -3 10.60 5.50 11 -4 3 4.30 3.70 -12 0 3 0.90 4.10 -12 0 -3 3.40 4.30 12 0 -3 0.30 4.40 -12 0 -3 5.80 4.60 12 0 3 2.10 4.60 -12 0 3 -0.20 4.00 12 1 3 16.10 5.40 -12 -1 3 17.50 6.30 -12 -1 3 1.00 4.40 12 -1 -3 4.20 4.50 -12 1 -3 11.00 4.60 -12 -1 3 3.40 4.40 -12 1 -3 11.80 4.80 12 -1 3 8.10 4.60 12 1 -3 14.60 5.70 -12 1 3 11.20 4.90 -12 -1 -3 0.90 4.20 -12 1 3 12.00 4.90 -12 -1 -3 3.80 4.80 -12 2 -3 2.10 4.30 -12 -2 3 11.40 5.40 12 -2 -3 -9.20 3.60 -12 2 -3 2.40 4.70 12 -2 -3 -2.90 3.80 12 2 3 11.00 4.80 -12 -2 3 -1.30 3.90 12 2 3 -2.50 3.80 -12 -2 3 0.70 3.30 12 -2 -3 1.90 4.30 -12 -2 3 4.90 5.50 -12 -2 -3 1.90 4.40 12 -2 3 2.60 4.40 -12 2 3 -3.20 4.30 12 2 -3 3.10 4.50 -12 -2 -3 7.50 4.20 -12 2 3 14.80 5.70 -12 -2 -3 5.40 4.70 0 0 4 2138.79 49.50 0 1 4 -0.90 1.00 0 -1 4 1.30 1.20 0 1 4 1.30 1.10 0 -1 -4 0.50 1.00 0 1 4 -0.40 0.90 0 -1 -4 0.60 1.10 0 1 -4 1.40 0.80 0 -1 4 -0.40 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1.40 0 -5 4 -0.10 1.70 0 -6 -4 46.80 2.40 0 -6 4 48.30 3.50 0 -6 4 42.00 4.20 0 -6 4 48.20 3.50 0 -6 -4 48.60 2.40 0 -6 -4 48.10 3.90 0 -6 4 41.80 3.60 0 6 4 47.60 2.30 0 6 4 43.20 2.30 0 -7 4 -1.80 2.10 0 -7 4 -3.60 1.60 0 7 4 1.10 1.00 0 7 4 0.00 1.00 0 -7 -4 -3.10 2.00 0 -7 4 -1.50 1.90 0 -7 4 -2.10 1.70 0 -7 -4 -0.90 1.00 0 -7 -4 -4.50 2.00 0 -7 -4 1.50 2.50 0 -7 -4 0.00 1.10 0 -7 -4 0.70 1.30 0 -8 4 34.40 4.30 0 -8 4 33.40 3.80 0 -8 -4 29.80 1.70 0 -8 -4 29.40 4.40 0 8 4 29.20 1.80 0 -8 4 29.20 4.30 0 -8 -4 28.70 2.60 0 -8 4 24.10 3.30 0 -8 -4 29.20 4.20 0 -8 -4 31.80 4.00 0 -8 -4 29.00 1.70 0 -9 4 -1.20 2.30 0 -9 -4 -1.40 1.50 0 -9 4 -4.90 3.30 0 -9 -4 -1.90 3.20 0 -9 4 -1.10 3.10 0 -9 -4 0.10 3.40 0 -9 4 -0.20 2.40 0 -10 4 4.30 2.90 0 -10 4 -3.10 3.20 0 -10 -4 -0.30 3.50 0 -10 -4 5.20 3.30 0 -10 4 1.30 2.80 0 -10 -4 -1.70 3.00 0 -10 -4 1.40 1.60 0 -10 4 4.10 3.10 0 -11 4 -4.50 2.60 0 -11 -4 -1.10 3.30 0 -11 4 1.60 2.80 0 -11 4 -4.20 2.60 0 -11 -4 8.80 3.50 0 -11 -4 5.40 3.90 0 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8.60 -1 -3 -4 384.96 9.50 -1 -3 -4 382.26 8.60 -1 4 -4 65.69 3.50 -1 4 -4 69.99 2.20 1 -4 -4 64.79 1.90 -1 -4 4 63.59 3.60 1 4 4 69.79 2.60 -1 4 -4 67.49 2.10 1 -4 -4 65.29 1.90 -1 -4 4 68.59 3.10 -1 -4 4 66.19 1.50 1 4 4 64.69 2.80 -1 -4 4 66.39 1.50 1 -4 -4 69.49 3.40 -1 4 -4 68.79 2.90 -1 -4 4 63.59 3.70 1 4 4 65.59 2.70 1 -4 -4 70.19 4.40 1 -4 -4 65.99 2.80 1 4 -4 67.29 1.70 1 -4 4 68.89 3.60 1 -4 4 63.49 2.80 -1 4 4 67.19 2.80 -1 -4 -4 62.59 2.70 1 -4 4 63.89 2.10 -1 -4 -4 59.59 2.90 -1 -4 -4 65.69 2.60 -1 4 4 72.59 2.90 1 4 -4 66.69 1.60 1 -4 4 60.69 4.20 1 -4 4 68.49 2.20 1 -5 -4 316.97 7.50 -1 5 -4 309.77 6.40 -1 5 -4 306.47 6.40 1 -5 -4 302.17 8.90 -1 -5 4 314.97 9.70 1 -5 -4 309.97 7.50 1 -5 -4 310.37 6.60 1 5 4 311.47 7.30 -1 -5 4 306.07 8.20 -1 -5 4 299.17 8.10 1 -5 -4 300.07 6.60 -1 -5 4 311.17 9.00 1 5 4 317.37 7.30 1 -5 4 309.77 9.20 -1 -5 -4 320.77 7.40 1 -5 4 328.67 10.10 1 -5 4 314.17 6.50 -1 -5 -4 308.27 7.30 -1 -5 -4 299.17 8.10 -1 5 4 312.77 7.50 1 -5 4 306.57 7.90 1 -5 4 302.87 6.30 -1 5 4 308.07 9.00 -1 -5 -4 316.97 7.40 -1 -5 -4 322.67 9.10 -1 5 4 315.37 7.50 1 -6 -4 4.70 1.40 1 6 4 2.00 1.10 1 -6 -4 -0.40 2.20 1 -6 -4 2.60 1.00 -1 -6 4 2.50 1.90 -1 -6 4 1.70 1.40 -1 -6 4 -1.40 1.70 1 -6 -4 4.00 2.10 1 -6 -4 1.60 1.30 1 -6 -4 0.80 1.00 -1 -6 4 -0.10 2.20 1 6 4 5.50 1.20 -1 6 4 1.60 1.20 -1 6 4 3.80 2.00 -1 6 4 2.60 1.30 1 -6 4 4.20 1.70 1 -6 4 1.90 2.00 1 -6 4 0.00 2.30 -1 -6 -4 0.90 1.40 -1 -6 -4 1.70 1.20 -1 -6 -4 0.10 1.70 -1 -6 -4 1.10 1.10 -1 -6 -4 3.60 2.20 -1 -7 4 0.70 2.20 1 7 4 0.10 1.20 -1 -7 4 -0.70 2.20 -1 -7 4 2.10 2.00 1 -7 -4 0.60 1.30 1 -7 -4 2.00 1.20 1 -7 -4 -1.80 2.40 -1 -7 4 1.70 2.50 1 -7 -4 1.30 2.40 1 -7 -4 2.80 1.20 1 7 4 1.30 1.10 -1 -7 -4 1.20 2.50 -1 -7 -4 1.40 1.60 -1 7 4 1.30 1.10 -1 -7 -4 1.00 1.40 1 -7 4 -1.50 2.90 1 -7 4 -0.90 2.50 1 -7 4 1.40 2.20 -1 -7 -4 -0.40 1.10 1 -7 4 -1.70 1.80 -1 7 4 1.50 1.20 -1 -7 -4 -0.20 2.00 1 -8 -4 172.58 4.70 1 -8 -4 163.78 4.60 1 -8 -4 172.38 4.70 -1 -8 4 171.48 7.10 1 8 4 160.68 4.20 1 -8 -4 177.28 7.80 -1 -8 4 179.98 7.10 1 -8 -4 181.18 8.40 -1 -8 4 174.08 7.30 1 -8 -4 186.98 9.00 -1 -8 4 178.68 8.10 -1 8 4 174.48 4.80 -1 -8 -4 168.98 5.50 -1 -8 -4 165.08 4.00 -1 -8 -4 166.58 4.00 1 -8 4 178.58 6.90 -1 8 4 171.68 4.80 1 -8 4 177.08 7.10 -1 -8 -4 170.98 8.10 -1 -8 -4 177.78 7.20 -1 -8 -4 177.08 7.10 -1 -8 -4 185.18 8.10 1 -8 4 166.88 8.50 1 -8 4 175.68 8.10 -1 -9 4 85.09 5.60 -1 -9 4 61.89 6.10 1 -9 -4 69.99 5.70 1 -9 -4 79.79 6.60 -1 -9 4 71.89 5.40 -1 -9 4 73.89 5.20 1 -9 -4 72.09 2.80 1 -9 4 69.59 6.80 1 -9 4 67.49 5.80 -1 9 4 69.09 2.20 -1 -9 -4 61.79 5.30 -1 -9 -4 68.29 5.70 1 -9 4 72.19 5.00 1 -9 4 77.49 5.00 -1 -9 -4 62.69 3.70 -1 9 4 70.89 2.20 -1 -10 4 2.00 3.00 1 -10 -4 0.20 3.20 1 -10 -4 4.10 3.70 1 -10 -4 2.50 3.60 -1 -10 4 3.10 3.10 -1 -10 4 1.50 2.80 1 -10 -4 1.50 1.00 -1 -10 4 7.80 3.20 1 -10 4 0.60 3.40 1 -10 4 -0.60 2.80 -1 -10 -4 1.60 3.60 -1 -10 -4 -0.80 1.80 1 -10 4 3.80 2.80 -1 -10 -4 2.70 2.70 -1 -10 -4 1.40 3.60 1 -10 4 3.30 3.70 1 -11 -4 4.50 3.30 1 -11 -4 2.50 3.40 -1 -11 4 9.90 3.20 -1 -11 4 4.60 3.40 -1 -11 4 4.30 3.30 1 -11 -4 11.00 3.70 -1 -11 4 2.40 2.70 -1 -11 -4 8.20 3.60 1 -11 4 8.30 3.00 -1 -11 -4 8.30 1.80 -1 -11 -4 2.90 3.00 1 -11 4 11.00 3.60 1 -11 4 4.70 3.20 1 -11 4 1.10 3.10 -1 -11 -4 6.80 3.80 2 0 -4 34.20 2.30 -2 0 4 30.80 2.70 -2 0 -4 36.30 2.50 2 0 4 33.40 2.30 2 0 4 28.80 2.40 2 0 4 28.60 2.30 -2 0 4 39.80 4.00 -2 0 -4 37.40 2.40 2 0 -4 34.20 2.20 2 0 4 34.00 2.30 2 0 -4 33.30 2.30 2 0 -4 32.00 1.90 2 0 -4 33.30 2.30 -2 0 4 31.50 2.30 -2 0 4 32.00 2.00 -2 0 -4 27.90 2.40 2 0 -4 35.00 2.80 -2 0 4 33.80 2.30 -2 -1 4 189.68 5.10 2 -1 -4 200.08 5.50 -2 1 -4 201.28 5.30 2 -1 -4 198.48 6.10 2 -1 -4 186.08 5.30 -2 -1 4 207.18 6.50 -2 -1 4 195.08 5.10 2 -1 -4 196.08 5.50 -2 1 -4 202.38 5.30 2 1 4 193.48 5.20 -2 -1 4 202.08 5.60 2 -1 -4 194.28 4.90 2 1 4 192.38 4.80 2 1 4 195.88 5.30 -2 -1 4 201.38 5.10 -2 1 -4 195.28 5.50 2 -1 -4 197.68 5.40 -2 1 -4 193.78 4.70 2 1 4 193.98 5.30 2 -1 4 204.48 5.60 2 -1 4 193.68 6.00 2 -1 4 193.68 5.20 2 -1 4 184.98 5.40 -2 1 4 197.68 5.40 2 -1 4 194.18 4.70 2 1 -4 203.18 5.30 -2 1 4 196.28 6.10 -2 -1 -4 192.78 5.30 2 1 -4 196.08 5.60 -2 -1 -4 193.68 5.30 -2 1 4 191.78 5.40 2 -1 4 189.48 5.20 -2 -1 -4 196.98 5.40 2 1 -4 197.68 5.10 -2 1 4 191.28 5.30 -2 1 4 197.38 5.00 2 1 -4 194.28 5.20 2 1 -4 193.88 4.00 2 1 -4 194.48 5.50 -2 -2 4 1973.00 37.50 -2 -2 4 1974.90 38.20 2 2 4 1973.30 37.70 2 -2 -4 1969.80 38.60 -2 -2 4 2019.70 37.80 2 2 4 1977.30 36.60 -2 -2 4 1939.01 38.40 2 -2 -4 1940.21 38.00 2 -2 -4 1983.30 38.10 2 2 4 1941.41 37.90 -2 -2 4 1996.20 37.60 2 -2 -4 2008.20 37.30 2 2 4 1938.01 37.80 2 -2 -4 2087.09 38.50 -2 2 -4 1949.20 38.50 -2 2 -4 1988.50 37.80 2 -2 -4 1971.60 39.20 -2 2 -4 1983.10 37.30 2 2 -4 2005.10 38.40 -2 2 4 1964.80 38.00 -2 2 4 1933.01 38.00 2 2 -4 1766.52 38.10 -2 -2 -4 1953.00 37.90 2 2 -4 1950.01 38.10 2 -2 4 1957.90 37.20 -2 2 4 1942.01 37.20 2 -2 4 1979.60 37.80 2 -2 4 1980.30 38.50 -2 2 4 1974.70 38.30 -2 -2 -4 1959.70 36.60 2 -2 4 1988.30 38.50 2 -2 4 1926.81 38.10 2 2 -4 1944.21 37.50 -2 -2 -4 1991.00 37.90 -2 -2 -4 1944.71 37.70 -2 3 -4 320.47 8.60 -2 -3 4 319.27 7.20 -2 3 -4 321.87 7.50 -2 -3 4 326.47 8.40 2 -3 -4 311.77 8.70 -2 -3 4 320.87 7.20 -2 3 -4 326.57 7.40 2 -3 -4 314.17 9.20 -2 -3 4 312.87 8.10 2 -3 -4 317.97 7.90 2 -3 -4 318.97 7.00 -2 -3 4 328.67 6.80 2 -3 -4 338.77 8.50 2 -3 -4 329.07 10.00 2 3 4 317.47 7.70 2 3 4 318.87 7.60 -2 3 -4 322.57 7.50 2 -3 4 317.87 7.50 -2 -3 -4 311.57 7.70 -2 -3 -4 315.57 6.30 2 -3 4 319.37 7.50 2 3 -4 322.27 7.20 -2 -3 -4 321.37 7.70 2 3 -4 315.37 8.10 2 3 -4 318.77 8.40 -2 3 4 322.57 7.90 -2 -3 -4 322.97 7.70 2 -3 4 311.47 8.50 2 3 -4 320.57 7.20 -2 3 4 319.07 8.30 2 -3 4 343.37 7.50 -2 3 4 326.37 7.00 -2 -4 4 1994.30 39.50 -2 -4 4 1913.31 38.30 2 -4 -4 1923.71 38.90 -2 -4 4 1950.50 38.70 -2 4 -4 1995.50 39.40 2 4 4 1915.91 37.60 -2 4 -4 1978.30 37.20 2 4 4 1872.51 37.40 2 -4 -4 1925.41 37.80 2 4 4 1922.71 37.50 -2 4 -4 1978.80 37.20 2 -4 -4 1952.00 37.80 -2 -4 4 1900.51 36.70 2 -4 -4 1956.60 39.50 -2 4 -4 1928.51 37.60 2 -4 -4 1915.81 36.70 2 -4 4 1950.80 37.20 -2 4 4 1941.61 37.80 -2 4 4 1930.01 37.80 2 4 -4 1937.21 38.40 2 -4 4 2004.00 37.20 2 4 -4 1953.50 38.90 -2 4 4 1911.61 38.70 -2 -4 -4 1928.01 37.60 2 4 -4 1932.11 36.70 -2 -4 -4 1901.51 37.50 -2 -4 -4 1879.91 36.60 -2 -4 -4 1900.21 37.50 2 4 -4 1984.60 37.30 2 -4 4 1959.10 37.50 2 -5 -4 78.49 3.50 -2 -5 4 81.19 2.30 -2 -5 4 83.69 3.50 2 -5 -4 94.69 5.10 2 5 4 81.29 3.20 -2 5 -4 79.89 3.00 -2 -5 4 77.99 4.20 2 -5 -4 80.99 2.80 -2 5 -4 83.69 4.60 -2 5 -4 83.59 3.70 2 5 4 79.09 3.50 -2 -5 4 86.69 4.10 2 5 4 88.39 3.30 -2 5 -4 81.09 3.00 -2 -5 4 80.49 2.30 2 -5 -4 81.69 4.40 2 -5 -4 86.79 3.60 2 -5 4 83.59 3.60 2 -5 4 93.59 5.60 -2 -5 -4 79.79 4.60 -2 5 4 82.69 3.50 2 -5 4 80.39 3.00 -2 -5 -4 79.79 3.90 2 5 -4 78.89 2.30 -2 -5 -4 87.49 3.60 -2 -5 -4 81.99 3.10 2 -5 4 78.59 2.90 -2 -5 -4 73.29 3.20 -2 -5 -4 79.09 3.10 -2 5 4 86.69 4.40 2 -5 4 83.69 4.60 -2 5 4 85.79 3.50 2 5 -4 80.19 2.40 2 6 4 15.80 1.80 2 -6 -4 14.20 2.80 -2 6 -4 16.50 1.60 2 -6 -4 14.70 2.00 -2 -6 4 14.20 2.20 -2 -6 4 17.40 2.60 2 -6 -4 15.20 1.50 2 -6 -4 14.70 2.00 2 6 4 16.80 1.80 -2 -6 4 18.40 3.10 -2 6 -4 16.50 1.50 -2 -6 4 14.60 2.60 2 6 4 15.90 2.10 2 -6 -4 14.20 3.30 2 -6 4 13.40 1.40 -2 -6 -4 16.20 1.80 -2 -6 -4 17.30 2.10 2 -6 4 15.20 1.60 -2 6 4 20.70 2.20 -2 -6 -4 18.30 3.10 -2 6 4 16.00 2.70 2 -6 4 18.00 3.50 -2 6 4 18.70 2.10 -2 -6 -4 15.70 2.20 -2 -6 -4 15.50 2.00 2 -6 4 14.80 2.90 -2 -6 -4 18.10 1.90 -2 -7 4 105.79 5.50 2 -7 -4 96.59 3.90 2 -7 -4 90.49 3.30 2 -7 -4 102.29 5.70 -2 7 -4 97.19 2.80 -2 -7 4 106.19 5.70 2 -7 -4 102.69 4.10 -2 7 -4 93.79 2.80 -2 -7 4 96.19 5.00 -2 -7 4 96.89 5.00 2 7 4 96.89 3.50 2 -7 -4 103.49 6.40 -2 -7 -4 100.09 5.80 2 -7 4 97.49 2.60 -2 7 4 104.59 5.50 -2 7 4 91.39 5.50 -2 -7 -4 95.49 4.40 -2 -7 -4 98.59 3.50 2 -7 4 90.79 5.70 2 -7 4 97.99 7.30 2 -7 4 105.29 4.90 -2 -7 -4 94.59 4.40 -2 -7 -4 99.19 4.50 -2 7 4 95.09 3.90 -2 -7 -4 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76.79 9.30 0 0 -32 87.79 8.00 0 0 -32 83.29 5.40 0 0 32 82.99 7.60 0 -1 -32 -0.60 4.20 0 1 32 2.60 4.60 0 -1 -32 -1.80 2.80 0 1 32 0.20 3.80 0 -1 32 -0.10 4.00 0 1 -32 2.00 4.10 0 1 -32 4.80 2.30 0 -1 32 -0.80 4.20 0 -1 32 -4.90 5.10 0 -1 32 6.30 4.20 0 -2 -32 22.70 4.10 0 -2 32 19.40 5.10 0 2 -32 22.10 5.20 0 2 -32 15.80 2.10 0 2 32 20.70 6.90 0 -2 32 7.30 7.10 0 2 32 17.20 4.10 0 -2 32 21.60 4.60 0 -2 -32 13.60 4.80 0 2 32 21.20 5.50 0 -2 32 14.00 4.50 0 3 32 5.10 4.60 0 3 -32 5.40 4.10 0 3 32 1.80 4.70 0 -3 32 6.50 5.40 0 -3 32 0.40 3.70 0 -3 32 -6.60 5.20 0 -3 -32 -2.90 3.30 0 -3 32 7.20 3.80 0 -3 -32 4.70 4.40 -1 0 -32 3.80 2.80 -1 0 32 12.80 4.60 1 0 32 4.10 5.60 1 0 -32 5.20 3.10 -1 0 32 1.70 5.40 1 0 32 5.80 4.40 -1 0 32 -2.00 3.90 1 0 -32 2.00 4.50 1 0 32 0.40 4.60 -1 0 32 -1.50 3.90 1 0 32 -1.10 4.10 -1 0 -32 12.20 5.00 1 1 32 41.20 6.40 -1 1 -32 53.29 6.80 1 1 32 38.90 7.30 1 -1 -32 38.10 5.40 1 1 32 36.20 5.50 1 -1 -32 49.50 6.80 -1 -1 32 48.50 6.50 -1 -1 32 46.80 6.40 -1 1 -32 48.10 3.80 -1 -1 32 36.40 6.30 -1 -1 -32 43.10 5.00 -1 1 32 45.90 5.70 1 -1 32 37.10 7.50 -1 1 32 43.00 7.60 1 1 -32 42.90 6.20 1 1 -32 39.00 3.90 -1 1 32 50.29 6.90 1 -1 32 40.90 6.20 1 -1 32 39.40 6.10 1 -1 32 47.50 6.30 -1 -1 -32 43.10 6.50 -1 -2 32 1.50 4.50 1 2 32 -0.40 6.20 1 2 32 3.50 4.20 1 -2 -32 -3.50 2.90 -1 2 -32 -1.30 4.20 -1 -2 32 5.10 3.90 -1 -2 32 3.40 6.60 1 2 32 1.90 3.20 -1 -2 32 6.00 3.90 1 -2 -32 5.50 4.40 -1 2 -32 1.60 1.40 -1 -2 -32 -0.10 3.00 1 -2 32 7.00 3.80 1 2 -32 -0.50 1.90 -1 2 32 1.90 5.10 -1 -2 -32 1.30 4.50 -1 2 32 5.00 4.30 1 -2 32 0.40 3.80 1 -2 32 1.60 3.80 -1 2 32 4.70 3.50 1 2 -32 1.90 4.00 -1 -3 32 -2.70 3.30 1 -3 -32 2.80 3.70 1 -3 -32 3.10 4.10 -1 -3 32 5.00 3.90 1 3 32 7.10 3.40 -1 -3 32 4.30 5.40 1 3 32 5.10 4.50 1 3 32 -2.40 4.30 -1 -3 32 -5.10 5.00 -1 3 32 2.80 4.50 -1 -3 -32 5.00 3.40 -1 3 32 2.60 4.90 -1 3 32 4.50 3.80 1 -3 32 1.30 3.70 1 3 -32 6.00 4.90 -1 -3 -32 3.40 4.00 1 -3 32 0.30 3.20 1 -3 32 4.90 6.10 1 -3 32 6.20 4.20 2 0 -32 11.60 4.90 -2 0 32 11.80 3.20 -2 0 32 22.80 5.10 2 0 32 12.50 5.10 2 0 -32 16.90 3.40 2 0 32 17.50 6.80 -2 0 -32 22.40 5.40 -2 0 -32 12.50 2.90 -2 0 32 11.40 4.40 -2 0 32 13.20 4.60 2 -1 -32 0.50 3.20 -2 -1 32 9.00 4.50 -2 1 -32 2.20 2.20 2 1 32 9.60 5.80 -2 -1 32 -2.40 2.60 2 -1 -32 0.80 4.30 -2 -1 32 -4.10 3.80 -2 -1 32 -2.20 4.10 -2 -1 32 5.20 5.80 -2 1 -32 4.80 4.60 2 -1 32 -4.90 3.50 2 1 -32 8.10 4.60 2 1 -32 0.30 2.70 -2 -1 -32 0.30 2.80 -2 1 32 10.20 4.20 2 -1 32 1.50 6.10 -2 1 32 -1.40 3.30 -2 -1 -32 0.90 4.60 -2 -2 32 23.20 4.60 -2 -2 32 21.20 5.20 -2 2 -32 23.80 5.40 -2 -2 32 24.10 7.90 2 2 32 19.80 6.90 -2 -2 32 11.60 6.50 2 -2 -32 31.30 6.20 2 -2 -32 24.10 4.40 -2 -2 -32 22.60 5.00 -2 2 32 12.20 4.80 -2 2 32 19.50 4.50 -2 -2 -32 19.20 4.10 2 -2 32 11.20 7.00 2 2 -32 19.40 3.00 2 -2 32 22.00 5.10 2 2 -32 20.30 5.40 2 3 32 10.70 5.80 -2 -3 32 1.70 3.90 -2 3 -32 9.20 4.60 -2 -3 32 -1.00 5.50 2 -3 -32 -2.40 3.50 2 -3 -32 -1.00 3.00 -2 -3 32 3.20 4.10 -2 -3 -32 0.00 3.30 -2 -3 -32 1.60 4.00 2 3 -32 4.10 3.30 2 -3 32 4.20 5.50 -2 3 32 -0.80 5.40 -2 3 32 2.20 3.90 2 3 -32 1.70 3.90 -2 3 32 2.30 4.70 -3 0 -32 14.10 3.30 -3 0 32 16.00 5.20 3 0 32 15.50 4.90 3 0 -32 11.20 4.70 -3 0 32 17.70 6.40 3 0 32 18.30 6.40 -3 0 32 9.20 4.10 -3 0 -32 30.90 9.30 -3 0 32 10.30 4.50 3 0 32 16.50 7.70 3 0 -32 13.20 3.60 -3 -1 32 5.50 4.60 -3 -1 32 -6.60 4.00 3 -1 -32 -0.10 4.30 -3 1 -32 6.80 4.60 3 1 32 11.00 4.80 3 1 32 4.00 6.20 3 -1 -32 -0.70 3.00 -3 -1 32 -1.50 5.40 -3 -1 32 3.80 2.90 -3 -1 32 6.60 4.20 3 -1 32 0.40 4.70 -3 -1 -32 6.90 5.00 3 1 -32 5.00 3.10 -3 -1 -32 5.30 3.10 -3 1 32 6.90 5.50 3 -1 32 7.50 4.20 -3 1 32 9.70 4.40 -3 1 32 3.80 3.90 3 -1 32 9.30 6.50 3 1 -32 7.90 5.00 -3 -2 32 13.60 7.80 -3 -2 32 14.90 2.90 -3 -2 32 0.40 5.50 3 2 32 9.90 5.70 -3 -2 32 8.30 3.90 -3 -2 32 -1.20 3.60 3 -2 -32 2.10 4.40 -3 2 -32 15.30 4.80 3 2 32 10.80 4.80 3 -2 -32 10.50 3.80 3 -2 32 9.80 6.00 3 2 -32 7.70 4.30 -3 2 32 13.50 6.00 -3 -2 -32 9.20 4.60 3 -2 32 13.80 4.50 -3 -2 -32 8.30 3.50 3 2 -32 3.80 2.80 -3 2 32 12.50 4.00 -3 2 32 9.40 4.90 0 0 33 3.40 4.00 0 0 -33 10.80 5.00 0 0 -33 6.40 3.00 0 0 33 5.80 4.30 0 0 33 5.40 4.50 0 -1 33 -0.30 3.70 0 -1 -33 3.80 3.60 0 1 33 1.10 4.00 0 -1 33 -3.90 4.20 0 1 -33 -2.50 2.20 0 -1 -33 -3.20 4.50 0 -1 33 -1.40 3.70 0 1 33 2.30 3.80 0 1 -33 -4.50 4.20 0 -1 33 12.80 6.50 0 -2 -33 -3.40 3.90 0 -2 33 1.20 3.70 0 2 -33 -2.10 1.50 0 -2 33 -3.60 5.60 0 2 -33 4.60 4.40 0 -2 33 4.40 5.20 0 -2 -33 1.80 3.50 0 2 33 -2.60 6.00 0 2 33 2.00 4.50 0 2 33 2.20 3.70 1 0 33 5.30 4.50 1 0 -33 2.00 4.30 -1 0 33 -0.20 4.10 -1 0 -33 -2.40 4.40 1 0 33 0.00 3.90 -1 0 33 0.40 4.00 -1 0 33 4.50 5.90 -1 0 -33 -2.80 2.60 -1 0 33 6.60 4.30 1 0 33 2.70 4.00 1 0 -33 -3.20 2.70 -1 -1 33 37.80 7.60 -1 1 -33 32.00 6.20 -1 -1 33 41.00 6.10 1 1 33 43.90 5.60 1 1 33 30.00 5.60 1 -1 -33 46.90 5.00 1 1 33 32.90 7.20 -1 -1 33 34.80 6.10 -1 1 -33 38.20 3.60 1 -1 -33 32.80 6.30 -1 -1 33 36.00 6.30 1 -1 33 36.20 7.70 -1 1 33 29.80 5.10 1 -1 33 47.00 6.50 1 -1 33 35.00 5.80 1 -1 33 35.80 8.30 -1 1 33 30.40 9.00 -1 -1 -33 39.80 5.60 1 1 -33 36.40 6.40 1 1 -33 30.50 3.70 -1 1 33 47.30 6.50 -1 -1 -33 46.00 6.80 1 2 33 1.90 5.60 -1 -2 33 2.10 4.10 -1 -2 33 1.10 4.20 -1 -2 33 -5.70 5.40 1 -2 -33 -1.00 4.30 1 2 33 -1.90 3.20 1 2 33 12.10 5.00 1 -2 -33 -0.40 3.10 -1 2 -33 3.20 4.60 1 -2 33 4.70 6.70 -1 2 33 2.10 3.40 1 -2 33 5.20 4.60 1 2 -33 5.30 4.40 -1 2 33 -3.60 6.00 1 2 -33 0.90 2.00 -1 -2 -33 9.70 4.90 1 -2 33 6.90 4.10 -1 -2 -33 -2.70 3.40 -1 2 33 5.70 4.50 -2 0 -33 0.10 7.10 -2 0 -33 4.00 2.90 -2 0 33 6.60 4.50 -2 0 33 -1.70 3.90 -2 0 33 -0.40 3.90 2 0 -33 2.90 4.70 2 0 -33 0.50 3.40 -2 0 33 3.20 6.00 -2 -1 33 12.30 4.70 -2 -1 33 13.90 6.70 -2 -1 33 18.60 4.70 2 -1 -33 19.10 4.20 -2 -1 33 22.30 6.40 2 -1 -33 20.40 5.60 2 1 33 22.90 6.60 -2 1 -33 23.70 5.60 -2 1 -33 17.00 2.70 2 -1 33 18.00 6.70 2 1 -33 22.80 5.20 -2 1 33 18.10 5.40 -2 -1 -33 22.70 4.80 -2 -1 -33 17.70 5.70 2 1 -33 15.00 3.30 -2 1 33 17.80 4.70 -2 1 33 20.40 6.80 2 -1 33 18.10 6.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 28111 _shelx_res_file ; TITL umd2762f_a.res in Pbca umd2762f_a.res created by SHELXL-2018/3 at 15:00:51 on 27-Oct-2022 REM Old TITL umd2762f in Pbca REM SHELXT solution in Pbca: R1 0.168, Rweak 0.011, Alpha 0.024 REM 0.904 for 377 systematic absences, Orientation as input REM Formula found by SHELXT: C15 N O CELL 0.71073 9.8201 9.0067 26.995 90 90 90 ZERR 8 0.0009 0.0007 0.0024 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 120 104 8 8 EQIV $1 1.5-X,-0.5+Y,+Z L.S. 10 PLAN 1 SIZE 0.12 0.22 0.4 TEMP 27 CONF HTAB C1 O1_$1 BOND $H LIST 4 htab 2 MORE -1 fmap 2 acta OMIT 1 0 2 REM REM REM WGHT 0.035900 0.787000 EXTI 0.007795 FVAR 0.70324 O1 4 0.451807 0.354852 0.376035 11.00000 0.05113 0.04445 = 0.05504 -0.00826 -0.00920 0.00900 N1 3 0.641923 -0.068024 0.313097 11.00000 0.07132 0.04137 = 0.06959 -0.00411 0.02532 0.00051 H1 2 0.659396 -0.147964 0.296086 11.00000 0.08123 C1 1 0.717542 -0.014369 0.351459 11.00000 0.06238 0.05128 = 0.06695 0.01111 0.01285 0.01068 AFIX 43 H1A 2 0.796959 -0.057322 0.363578 11.00000 -1.20000 AFIX 0 C2 1 0.533028 0.024248 0.304720 11.00000 0.05478 0.04197 = 0.05143 0.00028 0.01889 -0.00997 C3 1 0.431214 0.018796 0.268758 11.00000 0.06974 0.05736 = 0.05261 -0.01295 0.01178 -0.02231 AFIX 43 H3 2 0.428870 -0.056114 0.245062 11.00000 -1.20000 AFIX 0 C4 1 0.335123 0.128301 0.269874 11.00000 0.06179 0.06694 = 0.05128 -0.00268 -0.00412 -0.02113 AFIX 43 H4 2 0.266037 0.127455 0.246312 11.00000 -1.20000 AFIX 0 C5 1 0.337094 0.242139 0.305395 11.00000 0.04961 0.05090 = 0.05277 0.00304 -0.00347 -0.00622 AFIX 43 H5 2 0.269033 0.313937 0.305279 11.00000 -1.20000 AFIX 0 C6 1 0.438951 0.248421 0.340414 11.00000 0.04752 0.03867 = 0.04289 0.00156 0.00286 -0.00558 C7 1 0.540412 0.138404 0.340203 11.00000 0.04785 0.03805 = 0.04257 0.00367 0.00804 -0.00499 C8 1 0.659160 0.111383 0.369266 11.00000 0.05557 0.04436 = 0.05187 0.00522 0.00353 0.00394 AFIX 43 H8 2 0.690629 0.169017 0.395459 11.00000 -1.20000 AFIX 0 C9 1 0.349245 0.468548 0.377471 11.00000 0.05961 0.06009 = 0.08076 -0.01655 -0.01755 0.01925 AFIX 23 H9A 2 0.260551 0.424643 0.383434 11.00000 -1.20000 H9B 2 0.346282 0.520817 0.346073 11.00000 -1.20000 AFIX 0 C10 1 0.384327 0.573864 0.418302 11.00000 0.04651 0.04664 = 0.06364 -0.00598 -0.00156 0.01188 C11 1 0.336575 0.552691 0.465898 11.00000 0.06426 0.06183 = 0.08056 -0.00118 0.01351 -0.00711 AFIX 43 H11 2 0.278860 0.473301 0.472565 11.00000 -1.20000 AFIX 0 C12 1 0.373205 0.647413 0.503578 11.00000 0.08916 0.09075 = 0.06274 -0.01050 0.01646 0.00347 AFIX 43 H12 2 0.340519 0.631075 0.535449 11.00000 -1.20000 AFIX 0 C13 1 0.456628 0.764496 0.494644 11.00000 0.07410 0.07274 = 0.08092 -0.02637 -0.00082 0.00489 AFIX 43 H13 2 0.481679 0.827876 0.520269 11.00000 -1.20000 AFIX 0 C14 1 0.503160 0.788263 0.447992 11.00000 0.07416 0.05692 = 0.10589 -0.00986 0.01054 -0.01400 AFIX 43 H14 2 0.559340 0.869157 0.441610 11.00000 -1.20000 AFIX 0 C15 1 0.467896 0.693512 0.409924 11.00000 0.07016 0.06334 = 0.06733 0.00014 0.01490 -0.00063 AFIX 43 H15 2 0.501146 0.710903 0.378193 11.00000 -1.20000 AFIX 0 HKLF 4 REM umd2762f_a.res in Pbca REM wR2 = 0.1102, GooF = S = 1.110, Restrained GooF = 1.110 for all data REM R1 = 0.0453 for 2098 Fo > 4sig(Fo) and 0.0543 for all 2451 data REM 159 parameters refined using 0 restraints END WGHT 0.0359 0.7870 REM Instructions for potential hydrogen bonds HTAB C1 O1_$1 REM Highest difference peak 0.156, deepest hole -0.121, 1-sigma level 0.027 Q1 1 0.5759 0.1211 0.3627 11.00000 0.05 0.16 ; _shelx_res_checksum 50359 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.45181(11) 0.35485(11) 0.37604(4) 0.0502(3) Uani d 1 . . N N1 0.64192(16) -0.06802(16) 0.31310(6) 0.0608(4) Uani d 1 . . H H1 0.659(2) -0.148(2) 0.2961(8) 0.081(6) Uiso d 1 . . C C1 0.71754(19) -0.01437(19) 0.35146(7) 0.0602(5) Uani d 1 . . H H1A 0.796959 -0.057322 0.363578 0.072 Uiso calc 1 . . C C2 0.53303(16) 0.02425(16) 0.30472(6) 0.0494(4) Uani d 1 . . C C3 0.43121(19) 0.01880(19) 0.26876(6) 0.0599(5) Uani d 1 . . H H3 0.428870 -0.056114 0.245062 0.072 Uiso calc 1 . . C C4 0.33512(18) 0.1283(2) 0.26987(6) 0.0600(5) Uani d 1 . . H H4 0.266037 0.127455 0.246312 0.072 Uiso calc 1 . . C C5 0.33709(16) 0.24214(18) 0.30539(6) 0.0511(4) Uani d 1 . . H H5 0.269033 0.313937 0.305279 0.061 Uiso calc 1 . . C C6 0.43895(15) 0.24842(15) 0.34041(5) 0.0430(3) Uani d 1 . . C C7 0.54041(15) 0.13840(15) 0.34020(5) 0.0428(3) Uani d 1 . . C C8 0.65916(17) 0.11138(17) 0.36927(6) 0.0506(4) Uani d 1 . . H H8 0.690629 0.169017 0.395459 0.061 Uiso calc 1 . . C C9 0.34925(19) 0.4685(2) 0.37747(7) 0.0668(5) Uani d 1 . . H H9A 0.260551 0.424643 0.383434 0.080 Uiso calc 1 . . H H9B 0.346282 0.520817 0.346073 0.080 Uiso calc 1 . . C C10 0.38433(16) 0.57386(17) 0.41830(6) 0.0523(4) Uani d 1 . . C C11 0.3366(2) 0.5527(2) 0.46590(7) 0.0689(5) Uani d 1 . . H H11 0.278860 0.473301 0.472565 0.083 Uiso calc 1 . . C C12 0.3732(2) 0.6474(3) 0.50358(8) 0.0809(6) Uani d 1 . . H H12 0.340519 0.631075 0.535449 0.097 Uiso calc 1 . . C C13 0.4566(2) 0.7645(2) 0.49464(8) 0.0759(6) Uani d 1 . . H H13 0.481679 0.827876 0.520269 0.091 Uiso calc 1 . . C C14 0.5032(2) 0.7883(2) 0.44799(9) 0.0790(6) Uani d 1 . . H H14 0.559340 0.869157 0.441610 0.095 Uiso calc 1 . . C C15 0.4679(2) 0.6935(2) 0.40992(7) 0.0669(5) Uani d 1 . . H H15 0.501146 0.710903 0.378193 0.080 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0511(6) 0.0444(6) 0.0550(6) 0.0090(5) -0.0092(5) -0.0083(5) N1 0.0713(10) 0.0414(7) 0.0696(9) 0.0005(7) 0.0253(8) -0.0041(7) C1 0.0624(11) 0.0513(9) 0.0669(10) 0.0107(8) 0.0129(9) 0.0111(8) C2 0.0548(9) 0.0420(8) 0.0514(8) -0.0100(7) 0.0189(7) 0.0003(7) C3 0.0697(11) 0.0574(10) 0.0526(9) -0.0223(9) 0.0118(8) -0.0129(8) C4 0.0618(10) 0.0669(11) 0.0513(9) -0.0211(9) -0.0041(8) -0.0027(8) C5 0.0496(9) 0.0509(9) 0.0528(9) -0.0062(7) -0.0035(7) 0.0030(7) C6 0.0475(8) 0.0387(7) 0.0429(7) -0.0056(6) 0.0029(6) 0.0016(6) C7 0.0478(8) 0.0381(7) 0.0426(7) -0.0050(6) 0.0080(6) 0.0037(6) C8 0.0556(9) 0.0444(8) 0.0519(9) 0.0039(7) 0.0035(7) 0.0052(7) C9 0.0596(11) 0.0601(10) 0.0808(12) 0.0192(9) -0.0176(9) -0.0165(9) C10 0.0465(8) 0.0466(8) 0.0636(10) 0.0119(7) -0.0016(7) -0.0060(7) C11 0.0643(11) 0.0618(11) 0.0806(12) -0.0071(9) 0.0135(10) -0.0012(10) C12 0.0892(15) 0.0908(15) 0.0627(11) 0.0035(13) 0.0165(11) -0.0105(11) C13 0.0741(13) 0.0727(13) 0.0809(13) 0.0049(11) -0.0008(11) -0.0264(11) C14 0.0742(13) 0.0569(11) 0.1059(16) -0.0140(10) 0.0105(12) -0.0099(11) C15 0.0702(12) 0.0633(11) 0.0673(11) -0.0006(9) 0.0149(9) 0.0001(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 O1 C9 . . 117.07(12) ? C1 N1 H1 . . 125.9(14) ? C1 N1 C2 . . 109.56(14) ? C2 N1 H1 . . 124.5(14) ? N1 C1 H1A . . 125.2 ? C8 C1 N1 . . 109.56(16) ? C8 C1 H1A . . 125.2 ? N1 C2 C3 . . 130.67(15) ? N1 C2 C7 . . 106.86(14) ? C3 C2 C7 . . 122.45(15) ? C2 C3 H3 . . 121.5 ? C4 C3 C2 . . 117.05(15) ? C4 C3 H3 . . 121.5 ? C3 C4 H4 . . 118.9 ? C3 C4 C5 . . 122.22(16) ? C5 C4 H4 . . 118.9 ? C4 C5 H5 . . 119.7 ? C6 C5 C4 . . 120.58(16) ? C6 C5 H5 . . 119.7 ? O1 C6 C5 . . 125.45(14) ? O1 C6 C7 . . 115.65(13) ? C5 C6 C7 . . 118.89(14) ? C2 C7 C8 . . 106.97(14) ? C6 C7 C2 . . 118.78(14) ? C6 C7 C8 . . 134.25(14) ? C1 C8 C7 . . 107.03(15) ? C1 C8 H8 . . 126.5 ? C7 C8 H8 . . 126.5 ? O1 C9 H9A . . 110.1 ? O1 C9 H9B . . 110.1 ? O1 C9 C10 . . 108.10(13) ? H9A C9 H9B . . 108.4 ? C10 C9 H9A . . 110.1 ? C10 C9 H9B . . 110.1 ? C11 C10 C9 . . 121.35(17) ? C15 C10 C9 . . 120.96(16) ? C15 C10 C11 . . 117.68(16) ? C10 C11 H11 . . 119.5 ? C12 C11 C10 . . 120.90(18) ? C12 C11 H11 . . 119.5 ? C11 C12 H12 . . 119.7 ? C13 C12 C11 . . 120.56(19) ? C13 C12 H12 . . 119.7 ? C12 C13 H13 . . 120.3 ? C14 C13 C12 . . 119.40(19) ? C14 C13 H13 . . 120.3 ? C13 C14 H14 . . 119.7 ? C13 C14 C15 . . 120.61(19) ? C15 C14 H14 . . 119.7 ? C10 C15 C14 . . 120.84(17) ? C10 C15 H15 . . 119.6 ? C14 C15 H15 . . 119.6 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C6 . 1.3636(17) ? O1 C9 . 1.4368(19) ? N1 H1 . 0.87(2) ? N1 C1 . 1.363(2) ? N1 C2 . 1.373(2) ? C1 H1A . 0.9300 ? C1 C8 . 1.357(2) ? C2 C3 . 1.394(2) ? C2 C7 . 1.407(2) ? C3 H3 . 0.9300 ? C3 C4 . 1.365(3) ? C4 H4 . 0.9300 ? C4 C5 . 1.404(2) ? C5 H5 . 0.9300 ? C5 C6 . 1.377(2) ? C6 C7 . 1.405(2) ? C7 C8 . 1.426(2) ? C8 H8 . 0.9300 ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C9 C10 . 1.494(2) ? C10 C11 . 1.381(2) ? C10 C15 . 1.373(2) ? C11 H11 . 0.9300 ? C11 C12 . 1.375(3) ? C12 H12 . 0.9300 ? C12 C13 . 1.357(3) ? C13 H13 . 0.9300 ? C13 C14 . 1.357(3) ? C14 H14 . 0.9300 ? C14 C15 . 1.380(3) ? C15 H15 . 0.9300 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C1 H1A O1 8_755 0.93 2.61 3.517(2) 164.4 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C6 C7 C2 . . . . 179.47(12) ? O1 C6 C7 C8 . . . . -0.8(2) ? O1 C9 C10 C11 . . . . -90.2(2) ? O1 C9 C10 C15 . . . . 88.3(2) ? N1 C1 C8 C7 . . . . -0.28(18) ? N1 C2 C3 C4 . . . . -179.92(15) ? N1 C2 C7 C6 . . . . -179.18(12) ? N1 C2 C7 C8 . . . . 1.00(15) ? C1 N1 C2 C3 . . . . 177.39(15) ? C1 N1 C2 C7 . . . . -1.20(17) ? C2 N1 C1 C8 . . . . 0.94(18) ? C2 C3 C4 C5 . . . . 0.0(2) ? C2 C7 C8 C1 . . . . -0.45(16) ? C3 C2 C7 C6 . . . . 2.1(2) ? C3 C2 C7 C8 . . . . -177.73(14) ? C3 C4 C5 C6 . . . . 1.0(2) ? C4 C5 C6 O1 . . . . 179.00(14) ? C4 C5 C6 C7 . . . . -0.4(2) ? C5 C6 C7 C2 . . . . -1.1(2) ? C5 C6 C7 C8 . . . . 178.69(15) ? C6 O1 C9 C10 . . . . -179.00(13) ? C6 C7 C8 C1 . . . . 179.77(16) ? C7 C2 C3 C4 . . . . -1.5(2) ? C9 O1 C6 C5 . . . . 0.9(2) ? C9 O1 C6 C7 . . . . -179.63(14) ? C9 C10 C11 C12 . . . . 177.77(18) ? C9 C10 C15 C14 . . . . -178.20(17) ? C10 C11 C12 C13 . . . . 0.4(3) ? C11 C10 C15 C14 . . . . 0.4(3) ? C11 C12 C13 C14 . . . . 0.5(3) ? C12 C13 C14 C15 . . . . -0.9(3) ? C13 C14 C15 C10 . . . . 0.5(3) ? C15 C10 C11 C12 . . . . -0.8(3) ?