#------------------------------------------------------------------------------ #$Date: 2023-03-14 03:17:25 +0000 (Tue, 14 Mar 2023) $ #$Revision: 281866 $ #$URL: svn://www.crystallography.net/cod/cif/2/24/42/2244237.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244237 loop_ _publ_author_name 'Laban, Uro\N-isopropyltryptamine (4-HO-NiPT) and its precursors ; _journal_coeditor_code HB8057 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989023002098 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C20 H25 N2 O +, Cl -' _chemical_formula_moiety 'C20 H25 N2 O +, Cl -' _chemical_formula_sum 'C20 H25 Cl N2 O' _chemical_formula_weight 344.87 _chemical_name_common ; 4-Benzyloxy-N-isopropyltryptammonium chloride ; _chemical_name_systematic ; {2-[4-(Benzyloxy)-1H-indol-3-yl]ethyl}(propan-2-yl)azanium chloride ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _cell_angle_alpha 86.798(3) _cell_angle_beta 79.340(3) _cell_angle_gamma 87.587(3) _cell_formula_units_Z 4 _cell_length_a 10.1895(9) _cell_length_b 10.9117(7) _cell_length_c 17.6887(14) _cell_measurement_reflns_used 9870 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 25.56 _cell_measurement_theta_min 2.81 _cell_volume 1928.7(3) _computing_cell_refinement ; SAINT (Bruker, 2021) ; _computing_data_collection ; APEX4 (Bruker, 2021) ; _computing_data_reduction ; SAINT (Bruker, 2021) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXS2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 300.15 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker D8 Venture CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0332 _diffrn_reflns_av_unetI/netI 0.0234 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 42151 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.785 _diffrn_reflns_theta_min 2.719 _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.206 _exptl_absorpt_correction_T_max 0.7453 _exptl_absorpt_correction_T_min 0.6579 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2021) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.188 _exptl_crystal_description blcok _exptl_crystal_F_000 736 _exptl_crystal_size_max 0.30 _exptl_crystal_size_mid 0.27 _exptl_crystal_size_min 0.20 _refine_diff_density_max 0.263 _refine_diff_density_min -0.289 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.015 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 461 _refine_ls_number_reflns 7362 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.015 _refine_ls_R_factor_all 0.0584 _refine_ls_R_factor_gt 0.0406 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0453P)^2^+0.7204P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1000 _refine_ls_wR_factor_ref 0.1133 _reflns_number_gt 5589 _reflns_number_total 7362 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8057sup1.cif _cod_data_source_block 3a _cod_database_code 2244237 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.941 _shelx_estimated_absorpt_t_max 0.960 _shelx_hkl_file ; -2 0 0 5176.58 106.89 2 0 0 5181.28 106.79 -3 0 0 1664.73 46.70 3 0 0 1661.93 46.60 -4 0 0 31.80 1.80 4 0 0 29.60 2.00 4 0 0 31.50 1.20 4 0 0 31.60 1.80 4 0 0 30.40 1.70 -5 0 0 18.80 1.90 -5 0 0 18.50 1.80 5 0 0 16.30 1.60 5 0 0 22.50 1.10 5 0 0 23.50 1.80 5 0 0 21.20 1.90 -6 0 0 8.70 1.40 6 0 0 2.80 1.20 6 0 0 5.60 1.30 6 0 0 4.60 1.30 6 0 0 6.00 0.80 -7 0 0 3.10 1.40 -7 0 0 6.00 1.40 7 0 0 6.80 1.50 7 0 0 4.80 1.40 7 0 0 4.70 0.80 -8 0 0 10.10 2.90 -8 0 0 6.90 1.70 8 0 0 7.90 1.70 8 0 0 7.40 1.00 8 0 0 10.00 1.80 -9 0 0 0.50 1.70 -9 0 0 -2.40 1.80 9 0 0 -2.90 1.50 9 0 0 0.60 1.80 9 0 0 0.50 0.80 9 0 0 -1.80 1.70 -10 0 0 -1.30 1.90 -10 0 0 -2.50 1.60 10 0 0 -0.40 2.00 10 0 0 0.60 0.90 10 0 0 0.20 1.70 -11 0 0 7.50 2.30 -11 0 0 3.50 2.00 11 0 0 3.80 1.90 11 0 0 -2.00 2.10 11 0 0 -0.70 2.00 -12 0 0 14.10 2.60 -12 0 0 13.30 2.70 12 0 0 6.40 3.00 12 0 0 8.00 2.50 12 0 0 10.30 2.70 12 -1 0 -2.90 2.50 12 -1 0 3.50 4.10 12 -1 0 1.80 2.00 -12 1 0 0.20 1.90 -12 1 0 -1.50 2.30 11 -1 0 1.40 1.90 11 -1 0 1.60 1.00 11 -1 0 0.40 2.40 11 -1 0 2.70 2.20 -11 1 0 -0.10 1.80 -11 1 0 2.20 2.30 10 -1 0 5.20 1.20 10 -1 0 7.70 2.20 10 -1 0 5.30 3.20 10 -1 0 6.40 1.90 -10 1 0 2.60 1.80 -10 1 0 8.30 2.20 9 -1 0 22.70 2.30 9 -1 0 23.40 1.80 9 -1 0 28.50 2.60 9 -1 0 23.80 2.50 -9 1 0 25.50 2.30 -9 1 0 26.40 2.40 8 -1 0 -1.90 1.30 8 -1 0 0.00 1.80 8 -1 0 -0.60 1.50 8 -1 0 0.70 0.90 -8 1 0 0.00 1.50 -8 1 0 0.80 1.50 7 -1 0 14.40 1.70 7 -1 0 18.50 1.50 7 -1 0 15.40 1.70 7 -1 0 12.60 1.80 -7 1 0 19.30 1.90 -7 1 0 15.50 1.70 6 -1 0 43.50 1.80 6 -1 0 46.10 2.40 6 -1 0 53.09 2.50 -6 1 0 43.00 2.40 -6 1 0 47.90 2.40 5 -1 0 189.18 4.70 5 -1 0 200.78 4.70 5 -1 0 180.18 4.30 -5 1 0 196.98 4.70 4 -1 0 51.39 2.10 4 -1 0 50.39 1.70 4 -1 0 53.59 2.10 -4 1 0 58.19 2.90 3 -1 0 3126.99 74.79 -3 1 0 3195.18 75.19 2 -1 0 2322.67 53.79 -2 1 0 2294.67 53.69 1 -1 0 89.59 2.20 1 -1 0 89.09 1.90 -1 1 0 90.29 2.00 -1 -1 0 121.79 2.50 1 1 0 110.99 2.60 -2 -1 0 77.99 2.30 -2 -1 0 75.19 2.10 2 1 0 77.89 2.10 2 1 0 76.49 2.10 2 1 0 76.29 2.20 -3 -1 0 98.99 2.60 3 1 0 98.79 2.60 3 1 0 95.39 2.60 3 1 0 99.29 1.90 -4 -1 0 658.13 12.70 4 1 0 650.93 12.70 4 1 0 651.13 12.90 4 1 0 626.54 12.00 4 1 0 657.63 12.70 -5 -1 0 31.10 2.00 -5 -1 0 27.90 2.00 5 1 0 25.70 2.40 5 1 0 29.70 1.90 5 1 0 28.30 1.00 5 1 0 28.90 2.00 -6 -1 0 35.20 2.20 -6 -1 0 38.40 2.30 6 1 0 41.30 2.30 6 1 0 41.40 1.30 6 1 0 43.50 2.70 6 1 0 40.40 2.30 -7 -1 0 83.89 3.30 -7 -1 0 87.29 3.30 7 1 0 84.99 3.30 7 1 0 79.79 2.10 7 1 0 87.09 3.30 7 1 0 86.59 3.80 -8 -1 0 43.80 3.00 -8 -1 0 44.30 3.00 8 1 0 44.00 2.90 8 1 0 48.30 4.40 8 1 0 46.60 1.60 -9 -1 0 14.70 2.10 -9 -1 0 15.80 2.20 9 1 0 13.80 2.10 9 1 0 13.20 2.20 9 1 0 11.10 2.00 -10 -1 0 0.90 1.90 -10 -1 0 2.10 1.80 10 1 0 2.90 1.90 10 1 0 2.30 1.90 -11 -1 0 52.19 3.70 -11 -1 0 50.79 4.10 11 1 0 47.40 5.00 11 1 0 47.90 3.70 11 1 0 52.19 4.10 -12 -1 0 0.20 3.80 -12 -1 0 -1.90 2.40 12 1 0 -0.40 2.20 12 1 0 -3.20 2.50 12 1 0 2.80 3.20 12 -2 0 1.60 1.30 12 -2 0 4.70 2.10 12 -2 0 -1.30 2.60 -12 2 0 0.70 2.00 11 -2 0 0.30 1.20 11 -2 0 0.10 2.00 11 -2 0 1.50 3.90 11 -2 0 0.60 1.80 -11 2 0 -2.10 2.20 -11 2 0 -0.20 1.80 10 -2 0 18.90 2.70 10 -2 0 17.00 2.20 10 -2 0 15.80 2.40 10 -2 0 21.10 2.80 -10 2 0 17.00 2.30 -10 2 0 15.50 2.20 9 -2 0 11.70 1.90 9 -2 0 15.80 1.50 -9 2 0 12.60 2.00 8 -2 0 2.20 1.60 8 -2 0 0.10 1.70 8 -2 0 0.70 1.10 -8 2 0 1.40 1.60 -8 2 0 0.00 1.50 7 -2 0 20.10 1.90 7 -2 0 18.00 1.70 7 -2 0 16.00 1.70 -7 2 0 15.60 1.70 -7 2 0 16.10 1.70 6 -2 0 26.70 2.10 6 -2 0 20.70 1.60 6 -2 0 22.40 2.00 -6 2 0 22.80 1.90 -6 2 0 22.90 2.10 5 -2 0 180.18 4.40 5 -2 0 173.98 4.40 5 -2 0 168.18 4.20 -5 2 0 177.38 4.40 4 -2 0 1.20 0.90 4 -2 0 3.50 1.00 4 -2 0 0.40 0.80 -4 2 0 1.80 1.00 -4 2 0 2.20 1.00 3 -2 0 1.90 0.70 3 -2 0 1.20 0.70 3 -2 0 3.40 0.80 -3 2 0 2.60 0.80 -3 2 0 1.10 0.80 2 -2 0 223.68 4.70 2 -2 0 221.28 4.50 2 -2 0 220.38 4.50 -2 2 0 224.68 4.50 -2 2 0 224.18 4.80 -2 2 0 221.48 4.50 1 -2 0 179.38 3.50 1 -2 0 182.58 3.80 1 -2 0 183.28 3.90 1 -2 0 178.98 3.50 1 -2 0 179.98 3.90 -1 2 0 182.58 3.50 -1 2 0 176.68 3.80 -1 -2 0 113.39 2.50 -1 -2 0 118.99 2.70 -1 -2 0 114.39 2.40 -1 -2 0 114.49 2.70 -1 -2 0 112.99 2.40 1 2 0 114.29 2.40 1 2 0 120.69 2.70 1 2 0 118.09 2.70 1 2 0 114.19 2.50 1 2 0 107.49 3.00 -2 -2 0 322.37 6.60 -2 -2 0 322.97 6.60 -2 -2 0 333.27 6.50 -2 -2 0 323.97 6.40 -2 -2 0 331.37 6.10 2 2 0 331.57 6.40 2 2 0 330.57 6.10 2 2 0 323.87 6.60 2 2 0 324.77 6.40 -3 -2 0 216.58 4.60 -3 -2 0 212.38 4.80 -3 -2 0 217.68 4.60 3 2 0 219.38 4.70 3 2 0 207.78 5.80 3 2 0 212.38 4.60 -4 -2 0 252.87 5.60 -4 -2 0 260.57 5.60 -4 -2 0 254.37 5.80 4 2 0 256.87 5.60 4 2 0 251.37 5.80 -5 -2 0 16.00 1.40 -5 -2 0 10.90 1.30 5 2 0 15.50 1.40 5 2 0 12.50 1.30 5 2 0 15.00 1.40 -6 -2 0 4.10 1.20 6 2 0 2.80 1.10 6 2 0 2.20 1.20 6 2 0 2.10 1.10 -7 -2 0 1.20 1.30 -7 -2 0 -0.10 1.20 7 2 0 2.70 1.30 7 2 0 0.80 1.30 7 2 0 1.80 1.30 -8 -2 0 23.80 2.20 -8 -2 0 28.20 2.80 8 2 0 27.40 2.70 8 2 0 28.60 3.20 8 2 0 29.00 2.70 -9 -2 0 1.70 1.70 -9 -2 0 2.30 1.70 9 2 0 1.10 1.70 9 2 0 1.50 1.80 9 2 0 -2.70 2.80 -10 -2 0 4.20 1.90 -10 -2 0 2.40 1.90 10 2 0 0.00 1.80 10 2 0 1.90 2.00 -11 -2 0 -2.10 2.10 -11 -2 0 -3.00 1.70 11 2 0 -1.80 2.40 11 2 0 0.10 1.90 11 2 0 0.40 2.00 -12 -2 0 3.60 2.00 -12 -2 0 2.90 2.60 12 2 0 5.50 2.20 12 2 0 8.40 2.60 12 2 0 2.00 2.80 11 -3 0 -1.90 2.00 11 -3 0 -2.10 2.30 11 -3 0 0.90 2.10 -11 3 0 -1.20 1.90 -11 3 0 -1.20 1.90 10 -3 0 3.00 2.00 10 -3 0 2.30 1.40 10 -3 0 2.60 2.20 10 -3 0 3.10 1.80 -10 3 0 2.00 1.90 9 -3 0 1.50 1.60 9 -3 0 -0.30 1.80 9 -3 0 2.80 1.20 -9 3 0 1.00 1.70 8 -3 0 81.89 3.50 8 -3 0 90.99 3.80 -8 3 0 86.49 3.60 7 -3 0 1.10 1.30 7 -3 0 1.90 1.50 7 -3 0 3.20 1.20 -7 3 0 -0.40 1.20 -7 3 0 2.70 1.30 6 -3 0 266.87 6.20 6 -3 0 275.57 6.30 6 -3 0 271.37 6.30 -6 3 0 271.17 6.30 -6 3 0 266.47 6.30 5 -3 0 0.30 0.90 5 -3 0 0.80 0.90 5 -3 0 0.00 1.00 -5 3 0 -0.60 0.90 -5 3 0 -1.90 2.10 -5 3 0 0.50 1.00 4 -3 0 1.10 0.90 4 -3 0 1.90 0.80 -4 3 0 1.10 1.00 3 -3 0 437.36 8.60 3 -3 0 431.96 8.90 3 -3 0 442.96 8.60 -3 3 0 440.96 9.00 -3 3 0 433.16 8.60 2 -3 0 457.75 8.70 2 -3 0 443.76 9.10 2 -3 0 455.85 8.70 -2 3 0 451.75 8.70 -2 3 0 452.15 8.90 -2 3 0 463.65 9.20 -1 3 0 1445.76 32.00 0 -3 0 204.98 4.50 0 -3 0 208.78 4.50 0 -3 0 216.28 4.50 0 -3 0 213.68 4.60 0 3 0 212.28 4.60 0 3 0 217.48 4.50 0 3 0 214.88 4.50 -1 -3 0 2493.95 52.09 -1 -3 0 2474.65 52.29 -2 -3 0 47.50 1.80 -2 -3 0 51.99 1.50 -2 -3 0 50.09 1.90 -2 -3 0 48.70 1.50 -2 -3 0 48.00 1.40 2 3 0 47.30 1.40 2 3 0 47.90 1.70 2 3 0 46.70 1.50 2 3 0 47.10 1.80 2 3 0 47.30 1.50 -3 -3 0 231.98 5.00 -3 -3 0 242.28 5.00 -3 -3 0 236.68 5.20 -3 -3 0 230.28 5.20 3 3 0 233.78 5.20 3 3 0 232.28 5.00 3 3 0 233.08 5.00 3 3 0 232.68 4.50 -4 -3 0 26.40 1.70 -4 -3 0 26.10 1.70 4 3 0 25.20 1.80 4 3 0 23.40 1.60 -5 -3 0 7.70 1.20 -5 -3 0 4.30 1.20 -5 -3 0 5.50 1.10 5 3 0 8.70 1.30 5 3 0 4.90 1.10 -6 -3 0 56.29 2.60 -6 -3 0 58.29 2.60 6 3 0 51.89 2.50 6 3 0 54.69 2.90 6 3 0 53.99 2.60 -7 -3 0 0.10 1.30 -7 -3 0 -0.50 1.20 7 3 0 -1.70 1.20 7 3 0 -0.60 1.30 7 3 0 0.40 1.40 -8 -3 0 13.30 1.90 -8 -3 0 14.00 2.20 8 3 0 13.50 1.90 8 3 0 17.10 2.00 8 3 0 16.40 1.90 -9 -3 0 16.70 2.10 -9 -3 0 15.40 2.10 9 3 0 20.00 2.20 9 3 0 13.90 2.10 -10 -3 0 1.50 1.70 -10 -3 0 -1.00 1.90 10 3 0 -2.30 1.80 10 3 0 -1.10 1.70 10 3 0 -3.00 1.20 -11 -3 0 -0.90 2.10 -11 -3 0 1.40 1.80 11 3 0 -0.30 1.80 11 3 0 2.00 2.40 11 3 0 0.50 2.30 11 -4 0 6.90 2.10 11 -4 0 11.90 2.60 11 -4 0 8.30 2.30 -11 4 0 7.80 2.10 -11 4 0 9.50 2.10 10 -4 0 0.70 2.00 10 -4 0 -1.60 1.60 10 -4 0 -2.80 1.80 -10 4 0 -3.60 2.80 -10 4 0 -4.20 1.70 9 -4 0 19.00 2.10 9 -4 0 22.00 2.40 -9 4 0 21.40 2.20 8 -4 0 0.50 1.50 8 -4 0 2.40 1.30 8 -4 0 1.10 1.40 -8 4 0 1.00 1.40 -8 4 0 -0.10 1.50 7 -4 0 174.28 4.90 7 -4 0 181.48 5.10 7 -4 0 177.68 5.00 -7 4 0 181.18 5.00 -7 4 0 188.78 5.10 6 -4 0 0.50 1.00 6 -4 0 0.80 1.10 6 -4 0 1.50 1.10 -6 4 0 -0.10 1.10 -6 4 0 0.10 1.10 5 -4 0 370.76 7.80 5 -4 0 362.26 7.80 5 -4 0 364.06 8.00 -5 4 0 373.86 8.20 -5 4 0 368.46 7.80 -5 4 0 361.96 7.90 4 -4 0 128.19 3.20 4 -4 0 121.19 3.20 4 -4 0 121.59 3.50 -4 4 0 123.69 3.20 -4 4 0 124.79 3.20 -4 4 0 122.59 3.80 -4 4 0 122.29 3.30 3 -4 0 45.20 1.70 3 -4 0 46.00 1.70 3 -4 0 45.40 2.10 -3 4 0 46.20 2.30 -3 4 0 43.60 1.60 -3 4 0 44.00 1.90 2 -4 0 17.50 1.00 2 -4 0 18.40 1.20 2 -4 0 20.20 1.40 2 -4 0 16.40 1.50 -2 4 0 17.70 1.70 -2 4 0 18.80 1.50 1 -4 0 112.69 3.10 1 -4 0 116.79 2.30 1 -4 0 119.79 3.10 1 -4 0 118.99 2.30 1 -4 0 115.39 3.00 -1 4 0 119.49 3.10 -1 4 0 118.39 2.30 -1 4 0 112.99 3.10 -1 4 0 114.49 3.10 -1 4 0 117.89 2.30 0 -4 0 582.64 11.40 0 -4 0 580.14 11.30 0 -4 0 560.44 11.30 0 -4 0 576.74 11.30 0 4 0 581.04 11.30 0 4 0 580.54 11.40 0 4 0 581.54 11.40 -1 -4 0 8.70 1.00 -1 -4 0 8.90 0.60 -1 -4 0 10.60 1.10 -1 -4 0 9.90 0.60 -1 -4 0 11.30 1.20 -1 -4 0 9.10 1.00 1 4 0 9.00 0.70 1 4 0 8.90 1.10 1 4 0 10.70 1.00 1 4 0 9.00 0.60 1 4 0 8.90 0.90 1 4 0 7.40 1.00 -2 -4 0 48.70 1.90 -2 -4 0 42.90 1.70 -2 -4 0 45.70 1.60 -2 -4 0 44.90 1.50 -2 -4 0 46.70 2.00 2 4 0 44.90 1.50 2 4 0 45.30 2.20 2 4 0 46.80 1.60 2 4 0 45.00 2.00 2 4 0 45.40 1.50 -3 -4 0 654.83 12.80 -3 -4 0 664.43 13.20 -3 -4 0 663.33 12.50 -3 -4 0 670.73 13.20 -3 -4 0 674.33 12.80 3 4 0 667.63 13.10 3 4 0 658.03 12.80 3 4 0 665.83 12.80 3 4 0 652.23 12.50 3 4 0 670.73 13.20 -4 -4 0 17.00 1.60 -4 -4 0 19.20 1.80 -4 -4 0 19.90 1.90 -4 -4 0 16.70 1.60 4 4 0 16.30 1.60 4 4 0 18.30 1.60 4 4 0 22.40 1.90 -5 -4 0 0.30 1.00 -5 -4 0 2.70 1.10 -5 -4 0 0.60 0.90 -5 -4 0 -0.10 0.90 5 4 0 0.80 1.00 5 4 0 -0.60 0.90 5 4 0 0.50 0.90 -6 -4 0 54.69 2.60 -6 -4 0 54.99 2.60 -6 -4 0 55.79 3.00 6 4 0 55.79 2.90 6 4 0 51.29 2.60 6 4 0 57.89 2.60 -7 -4 0 9.70 1.60 -7 -4 0 9.20 1.60 -7 -4 0 10.30 1.60 7 4 0 14.40 2.90 7 4 0 11.30 1.70 7 4 0 13.60 1.80 -8 -4 0 25.40 2.20 -8 -4 0 28.00 2.80 8 4 0 30.60 2.50 8 4 0 28.30 3.30 -9 -4 0 1.40 1.70 9 4 0 -1.90 1.70 9 4 0 2.00 1.90 -10 -4 0 13.30 2.20 -10 -4 0 10.70 2.30 10 4 0 9.50 2.20 10 4 0 9.10 2.10 -11 -4 0 0.50 2.20 -11 -4 0 -0.20 2.10 11 4 0 0.40 2.00 11 4 0 2.50 2.00 11 4 0 -2.70 2.20 11 -5 0 -2.30 2.10 11 -5 0 1.70 1.80 11 -5 0 -0.70 3.50 -11 5 0 -0.30 1.80 -11 5 0 1.50 2.30 10 -5 0 -0.70 1.50 10 -5 0 -1.10 2.00 -10 5 0 1.70 1.70 9 -5 0 11.20 2.20 9 -5 0 13.30 2.00 -9 5 0 10.60 1.90 -9 5 0 9.70 1.80 8 -5 0 41.90 2.80 8 -5 0 43.70 3.10 -8 5 0 30.60 2.60 -8 5 0 37.20 2.80 7 -5 0 -2.10 1.30 -7 5 0 -1.90 1.20 -7 5 0 1.30 1.30 -7 5 0 -0.70 1.20 6 -5 0 0.00 1.20 6 -5 0 -0.70 1.10 6 -5 0 -1.20 1.20 -6 5 0 1.40 1.10 -6 5 0 -1.10 1.10 -6 5 0 -0.70 1.00 5 -5 0 -1.20 1.10 5 -5 0 0.00 1.20 5 -5 0 -1.30 0.90 -5 5 0 -1.10 0.90 -5 5 0 -1.90 0.90 -5 5 0 1.10 1.80 -5 5 0 2.40 1.50 4 -5 0 47.60 1.90 4 -5 0 47.70 2.40 4 -5 0 47.10 2.00 -4 5 0 48.70 2.60 -4 5 0 46.80 2.00 -4 5 0 50.39 1.90 -4 5 0 51.09 2.20 3 -5 0 0.60 1.00 3 -5 0 0.30 1.10 3 -5 0 0.70 0.60 3 -5 0 0.40 0.60 -3 5 0 0.40 0.70 -3 5 0 0.10 0.60 -3 5 0 0.90 1.30 -3 5 0 0.80 0.90 2 -5 0 43.00 1.30 2 -5 0 41.80 1.30 2 -5 0 39.50 2.10 2 -5 0 41.20 2.00 2 -5 0 43.10 2.00 -2 5 0 40.80 1.30 -2 5 0 41.00 2.40 -2 5 0 44.10 2.10 1 -5 0 513.05 10.60 1 -5 0 507.75 10.50 1 -5 0 521.35 10.50 1 -5 0 520.95 10.60 -1 5 0 523.55 10.60 -1 5 0 532.95 10.60 -1 5 0 523.85 9.60 -1 5 0 529.15 10.70 -1 5 0 521.85 9.60 0 -5 0 9.50 1.00 0 -5 0 9.00 1.10 0 -5 0 8.30 1.10 0 5 0 8.60 1.20 0 5 0 8.30 1.20 0 5 0 6.40 1.20 -1 -5 0 870.01 16.20 -1 -5 0 876.71 17.10 -1 -5 0 874.71 16.20 -1 -5 0 874.81 17.20 -1 -5 0 889.21 18.10 -1 -5 0 877.11 16.90 1 5 0 885.91 17.00 1 5 0 882.21 16.30 1 5 0 877.71 16.90 1 5 0 884.61 16.20 1 5 0 876.51 17.10 1 5 0 892.81 17.20 -2 -5 0 186.28 3.90 -2 -5 0 190.18 4.70 -2 -5 0 187.68 3.90 -2 -5 0 187.48 4.30 -2 -5 0 186.98 4.50 2 5 0 187.98 3.90 2 5 0 192.98 4.60 2 5 0 186.78 4.50 2 5 0 186.78 4.30 -3 -5 0 192.28 4.20 -3 -5 0 187.88 4.70 -3 -5 0 188.38 4.20 -3 -5 0 190.28 4.80 -3 -5 0 193.98 4.20 3 5 0 187.38 5.20 3 5 0 188.88 4.20 3 5 0 193.08 4.20 3 5 0 187.38 4.20 3 5 0 182.48 4.60 -4 -5 0 36.50 2.20 -4 -5 0 33.00 1.80 -4 -5 0 35.90 1.80 -4 -5 0 34.70 2.20 4 5 0 32.20 1.80 4 5 0 35.70 2.10 4 5 0 35.40 1.90 4 5 0 37.60 2.20 -5 -5 0 9.90 1.30 -5 -5 0 7.80 1.20 -5 -5 0 9.20 1.30 5 5 0 7.20 1.40 5 5 0 7.80 1.20 5 5 0 9.70 1.30 -6 -5 0 31.00 2.30 -6 -5 0 31.10 2.30 -6 -5 0 32.70 2.60 -6 -5 0 30.40 2.20 6 5 0 33.60 2.30 6 5 0 32.10 2.30 6 5 0 32.10 2.60 -7 -5 0 10.50 1.80 -7 -5 0 9.50 1.90 7 5 0 7.30 1.40 7 5 0 7.10 1.50 7 5 0 6.60 1.50 -8 -5 0 140.09 4.80 -8 -5 0 143.99 4.60 8 5 0 130.79 5.40 8 5 0 146.89 4.70 -9 -5 0 117.99 4.70 -9 -5 0 114.09 4.40 9 5 0 119.39 5.20 9 5 0 118.49 4.60 -10 -5 0 4.20 2.00 -10 -5 0 6.70 1.90 10 5 0 7.10 2.10 10 5 0 5.30 1.80 -11 -5 0 53.99 3.80 -11 -5 0 67.59 4.60 11 5 0 58.19 4.10 11 5 0 58.09 5.20 11 5 0 56.79 4.00 10 -6 0 -0.50 1.60 10 -6 0 2.00 2.10 -10 6 0 1.00 2.60 -10 6 0 1.20 1.70 -10 6 0 3.80 1.80 9 -6 0 1.00 1.60 9 -6 0 1.20 1.70 -9 6 0 -0.40 1.50 -9 6 0 3.50 1.70 -9 6 0 1.80 1.50 8 -6 0 5.40 1.50 8 -6 0 4.10 1.50 -8 6 0 3.10 1.40 -8 6 0 3.70 1.60 7 -6 0 20.00 1.80 7 -6 0 25.30 2.50 -7 6 0 23.20 2.40 -7 6 0 24.10 2.30 -7 6 0 20.40 1.80 6 -6 0 1.00 1.10 6 -6 0 0.10 1.10 -6 6 0 1.20 1.30 -6 6 0 0.20 1.10 5 -6 0 -0.40 1.10 5 -6 0 -1.40 1.10 5 -6 0 -1.30 0.90 5 -6 0 -1.30 0.90 -5 6 0 -0.40 0.90 -5 6 0 1.10 0.90 -5 6 0 -0.30 1.00 4 -6 0 43.00 2.40 4 -6 0 45.50 1.90 4 -6 0 47.10 1.90 4 -6 0 46.80 2.50 -4 6 0 43.40 1.80 -4 6 0 47.60 2.30 -4 6 0 47.30 1.90 -4 6 0 52.59 3.00 3 -6 0 1.10 0.60 3 -6 0 1.20 1.00 3 -6 0 0.70 0.60 3 -6 0 2.80 2.00 -3 6 0 0.80 1.40 -3 6 0 1.70 0.60 -3 6 0 -0.10 0.90 2 -6 0 1.00 1.00 2 -6 0 2.20 1.00 2 -6 0 1.00 1.00 2 -6 0 2.20 0.40 2 -6 0 2.60 0.50 -2 6 0 1.70 1.00 -2 6 0 1.00 1.30 -2 6 0 2.10 0.40 -2 6 0 2.20 0.50 1 -6 0 41.00 2.20 1 -6 0 37.80 2.00 1 -6 0 38.30 1.90 1 -6 0 36.90 2.10 -1 6 0 39.00 2.40 -1 6 0 37.70 2.20 -1 6 0 37.20 2.20 0 -6 0 75.29 2.60 0 -6 0 77.49 2.80 0 -6 0 81.29 2.80 0 -6 0 73.19 2.70 0 6 0 81.59 3.30 0 6 0 80.59 2.90 -1 -6 0 47.50 2.10 -1 -6 0 52.79 1.10 -1 -6 0 54.49 2.30 -1 -6 0 52.09 2.20 -1 -6 0 51.19 1.10 -1 -6 0 49.50 2.30 1 6 0 52.69 2.30 1 6 0 53.19 1.20 1 6 0 52.79 2.30 1 6 0 51.59 2.60 -2 -6 0 1.70 0.80 -2 -6 0 0.30 0.80 -2 -6 0 -0.80 0.50 -2 -6 0 0.70 1.10 2 6 0 0.00 1.20 2 6 0 0.40 1.00 2 6 0 1.10 0.80 2 6 0 -0.20 0.50 2 6 0 0.20 1.10 -3 -6 0 93.39 2.50 -3 -6 0 95.49 3.10 -3 -6 0 91.79 3.30 -3 -6 0 92.89 2.50 -3 -6 0 94.19 2.70 3 6 0 95.39 2.70 3 6 0 93.89 3.20 3 6 0 95.99 3.00 3 6 0 98.89 2.50 3 6 0 93.79 2.50 -4 -6 0 10.40 1.10 -4 -6 0 10.90 1.10 -4 -6 0 9.00 1.20 -4 -6 0 12.90 1.60 -4 -6 0 12.70 1.30 4 6 0 13.70 1.20 4 6 0 12.00 1.30 4 6 0 13.40 1.20 4 6 0 12.90 1.60 -5 -6 0 125.59 3.70 -5 -6 0 122.69 4.00 -5 -6 0 123.49 4.00 -5 -6 0 125.29 3.60 5 6 0 126.79 4.10 5 6 0 125.49 3.50 5 6 0 121.19 3.50 5 6 0 117.69 3.90 -6 -6 0 -1.80 1.30 -6 -6 0 -0.40 1.30 -6 -6 0 0.90 1.20 6 6 0 1.50 1.20 6 6 0 1.50 1.20 6 6 0 2.20 1.20 -7 -6 0 404.06 9.40 -7 -6 0 398.76 8.90 -7 -6 0 384.66 8.80 7 6 0 380.96 8.80 7 6 0 382.46 9.20 7 6 0 383.16 8.80 -8 -6 0 5.40 1.70 -8 -6 0 5.50 1.60 8 6 0 5.70 1.80 8 6 0 5.60 2.70 -9 -6 0 8.10 2.00 -9 -6 0 5.40 1.80 9 6 0 8.40 1.90 9 6 0 5.00 1.80 9 6 0 4.20 1.90 -10 -6 0 12.40 2.50 -10 -6 0 11.50 2.00 10 6 0 11.40 2.30 10 6 0 14.30 2.20 -11 -6 0 -0.60 2.20 -11 -6 0 1.50 1.80 11 6 0 -2.40 2.30 11 6 0 -0.10 1.90 10 -7 0 0.60 1.50 10 -7 0 1.00 1.70 -10 7 0 1.40 1.60 -10 7 0 2.20 1.70 -10 7 0 3.80 1.80 9 -7 0 3.10 1.60 9 -7 0 0.40 1.70 -9 7 0 1.80 1.40 -9 7 0 1.30 1.40 8 -7 0 1.00 1.40 8 -7 0 0.40 1.30 -8 7 0 2.00 1.40 -8 7 0 1.00 1.40 7 -7 0 32.80 2.40 7 -7 0 33.30 2.60 -7 7 0 41.20 2.80 -7 7 0 32.30 2.40 -7 7 0 34.30 2.40 6 -7 0 47.80 3.00 6 -7 0 48.70 2.40 -6 7 0 44.00 2.40 -6 7 0 50.69 2.80 -6 7 0 52.69 2.50 5 -7 0 7.20 1.10 5 -7 0 6.20 1.00 -5 7 0 8.40 1.60 -5 7 0 5.10 1.10 -5 7 0 7.00 1.10 -5 7 0 6.40 2.10 4 -7 0 8.10 1.00 4 -7 0 6.00 1.40 4 -7 0 8.10 1.00 -4 7 0 7.90 1.50 -4 7 0 7.70 1.00 -4 7 0 8.70 1.90 -4 7 0 6.60 0.90 3 -7 0 121.49 4.00 3 -7 0 129.09 2.90 3 -7 0 126.59 2.90 3 -7 0 128.99 3.90 -3 7 0 127.59 2.90 -3 7 0 125.99 2.90 -3 7 0 137.39 4.40 -3 7 0 128.39 3.90 2 -7 0 11.20 1.50 2 -7 0 13.50 1.70 2 -7 0 11.00 0.60 2 -7 0 13.60 1.50 2 -7 0 11.90 1.40 2 -7 0 9.30 0.60 -2 7 0 9.10 0.60 -2 7 0 15.20 1.70 -2 7 0 14.40 1.80 -2 7 0 9.00 0.60 1 -7 0 94.59 3.20 1 -7 0 92.79 3.60 1 -7 0 92.49 3.20 1 -7 0 90.19 3.30 -1 7 0 95.69 3.50 -1 7 0 92.69 3.30 -1 7 0 88.19 3.30 0 -7 0 33.10 2.10 0 -7 0 31.70 2.10 0 -7 0 29.30 2.10 0 -7 0 30.80 2.00 0 7 0 30.60 2.40 0 7 0 30.00 2.30 0 7 0 30.10 2.30 -1 -7 0 226.68 5.50 -1 -7 0 221.78 5.40 -1 -7 0 220.58 5.50 1 7 0 224.98 5.60 1 7 0 229.48 5.60 1 7 0 233.18 5.80 -2 -7 0 150.28 3.10 -2 -7 0 151.98 3.90 -2 -7 0 152.88 4.10 -2 -7 0 144.29 4.30 -2 -7 0 147.49 3.10 2 7 0 143.39 3.10 2 7 0 143.39 4.30 2 7 0 157.08 4.60 2 7 0 145.99 3.10 2 7 0 146.89 4.10 2 7 0 141.99 4.90 -3 -7 0 20.80 1.60 -3 -7 0 18.30 2.00 -3 -7 0 19.10 1.80 -3 -7 0 19.20 1.30 -3 -7 0 17.80 1.30 3 7 0 16.50 1.30 3 7 0 20.10 1.80 3 7 0 21.40 2.10 3 7 0 18.70 2.00 3 7 0 17.20 1.30 -4 -7 0 153.68 4.50 -4 -7 0 150.78 5.10 -4 -7 0 146.29 3.80 -4 -7 0 151.98 3.80 -4 -7 0 154.08 3.80 4 7 0 153.58 3.80 4 7 0 159.48 4.70 4 7 0 161.38 3.80 4 7 0 154.88 4.40 -5 -7 0 -2.00 1.10 -5 -7 0 -1.40 1.00 -5 -7 0 2.00 1.40 5 7 0 1.30 1.60 5 7 0 1.20 1.10 5 7 0 -0.90 1.00 5 7 0 -1.30 1.10 -6 -7 0 4.60 1.30 -6 -7 0 4.10 1.30 -6 -7 0 7.20 1.50 6 7 0 6.80 1.40 6 7 0 6.90 2.20 6 7 0 4.00 1.30 6 7 0 4.90 1.40 -7 -7 0 2.90 1.30 -7 -7 0 1.90 1.40 -7 -7 0 2.10 1.50 7 7 0 4.70 2.00 7 7 0 1.20 1.40 7 7 0 -0.10 1.30 7 7 0 0.60 1.40 -8 -7 0 20.80 2.20 -8 -7 0 15.70 1.80 8 7 0 19.10 2.00 8 7 0 18.60 2.20 -9 -7 0 14.70 2.00 -9 -7 0 9.30 1.90 9 7 0 9.60 1.90 9 7 0 11.60 2.20 9 7 0 7.10 1.80 -10 -7 0 1.80 1.90 -10 -7 0 3.70 2.40 10 7 0 1.50 1.80 10 7 0 3.10 3.20 9 -8 0 3.50 1.60 9 -8 0 2.30 1.60 -9 8 0 4.50 1.80 -9 8 0 6.30 2.70 -9 8 0 1.20 1.40 8 -8 0 1.90 1.40 8 -8 0 4.70 1.50 -8 8 0 2.60 1.40 -8 8 0 3.70 1.50 -8 8 0 7.50 1.80 7 -8 0 -1.80 1.10 7 -8 0 -1.30 1.10 -7 8 0 1.00 1.50 -7 8 0 2.10 1.50 -7 8 0 -0.10 1.10 6 -8 0 57.69 3.90 6 -8 0 61.59 2.70 -6 8 0 65.99 3.30 -6 8 0 65.89 2.60 -6 8 0 61.79 2.70 5 -8 0 0.50 0.90 5 -8 0 -0.90 0.90 -5 8 0 0.50 0.90 -5 8 0 1.30 1.50 -5 8 0 -0.10 0.90 4 -8 0 1.90 0.80 4 -8 0 3.60 0.80 -4 8 0 5.60 1.90 -4 8 0 2.00 0.80 -4 8 0 3.60 1.50 3 -8 0 31.90 1.20 3 -8 0 33.70 1.20 -3 8 0 30.90 1.20 -3 8 0 30.90 2.60 -3 8 0 33.10 1.20 2 -8 0 73.59 3.10 2 -8 0 72.29 3.30 2 -8 0 66.59 3.00 -2 8 0 69.09 3.20 -2 8 0 69.99 3.60 1 -8 0 5.00 1.30 1 -8 0 4.90 1.30 1 -8 0 3.90 1.20 1 -8 0 5.90 1.30 -1 8 0 7.90 1.50 -1 8 0 6.60 1.80 0 -8 0 1.70 1.10 0 -8 0 4.00 1.20 0 -8 0 1.20 1.20 0 -8 0 4.20 1.30 0 8 0 1.50 1.30 0 8 0 1.50 1.40 0 8 0 3.20 1.50 -1 -8 0 19.60 2.20 -1 -8 0 24.00 2.10 -1 -8 0 23.90 2.30 -1 -8 0 22.60 2.10 1 8 0 26.00 2.50 1 8 0 24.10 2.60 1 8 0 25.30 2.30 -2 -8 0 24.50 2.00 -2 -8 0 24.60 0.90 -2 -8 0 23.20 0.90 -2 -8 0 26.60 2.20 2 8 0 26.20 2.30 2 8 0 23.30 0.90 2 8 0 27.10 2.40 2 8 0 26.50 2.70 2 8 0 24.50 2.20 2 8 0 23.80 0.90 -3 -8 0 66.29 2.00 -3 -8 0 65.89 2.60 -3 -8 0 66.89 3.00 -3 -8 0 62.89 2.00 3 8 0 61.09 1.90 3 8 0 62.19 2.30 3 8 0 68.09 3.00 3 8 0 66.39 2.80 3 8 0 70.59 3.20 -4 -8 0 2.00 1.20 -4 -8 0 2.10 1.00 -4 -8 0 -0.30 0.80 -4 -8 0 1.50 0.90 4 8 0 2.40 1.50 4 8 0 -0.20 0.80 4 8 0 0.50 1.10 4 8 0 1.00 0.90 -5 -8 0 22.10 1.90 -5 -8 0 21.50 1.80 -5 -8 0 25.60 2.60 5 8 0 22.40 1.90 5 8 0 26.50 2.50 5 8 0 28.90 3.00 -6 -8 0 7.60 1.40 -6 -8 0 6.80 1.60 -6 -8 0 7.70 1.30 6 8 0 9.70 2.10 6 8 0 8.80 2.30 6 8 0 8.10 1.50 6 8 0 9.50 1.40 -7 -8 0 31.40 3.00 -7 -8 0 36.70 2.60 -7 -8 0 32.10 2.40 7 8 0 32.30 2.60 7 8 0 33.00 3.40 7 8 0 31.00 3.00 -8 -8 0 5.60 1.50 -8 -8 0 9.30 1.70 -8 -8 0 4.20 1.60 8 8 0 4.80 1.50 8 8 0 5.40 2.20 8 8 0 5.20 1.70 8 8 0 7.00 1.70 -9 -8 0 1.90 1.40 -9 -8 0 1.30 1.70 9 8 0 2.90 1.60 9 8 0 3.60 2.90 9 8 0 1.10 2.30 -10 -8 0 10.10 2.00 -10 -8 0 10.30 2.20 10 8 0 7.60 2.40 10 8 0 11.00 2.80 8 -9 0 19.60 1.80 8 -9 0 15.10 1.70 -8 9 0 22.10 1.90 -8 9 0 20.80 1.90 -8 9 0 20.10 2.20 7 -9 0 1.90 1.20 7 -9 0 2.20 1.20 -7 9 0 2.90 1.70 -7 9 0 0.00 1.10 6 -9 0 1.70 1.00 6 -9 0 3.20 1.10 -6 9 0 5.20 1.80 -6 9 0 1.00 1.00 -6 9 0 3.20 1.10 5 -9 0 55.89 2.50 5 -9 0 54.99 2.10 -5 9 0 54.59 5.50 -5 9 0 52.49 2.10 4 -9 0 -0.80 0.60 4 -9 0 -0.10 0.60 -4 9 0 -0.60 1.50 -4 9 0 -0.60 0.60 -4 9 0 0.40 0.70 3 -9 0 4.60 1.50 -3 9 0 11.10 2.20 -3 9 0 6.20 1.70 2 -9 0 20.40 2.10 -2 9 0 19.90 2.30 -2 9 0 18.80 2.30 1 -9 0 188.68 5.60 -1 9 0 196.78 5.80 -1 9 0 217.48 8.90 -1 9 0 193.38 5.80 0 -9 0 -1.60 1.10 0 -9 0 -2.00 2.00 0 9 0 -1.90 1.80 0 9 0 -1.60 1.70 0 9 0 -0.70 1.50 -1 -9 0 4.30 1.30 -1 -9 0 5.20 1.30 -1 -9 0 4.00 1.70 1 9 0 5.10 2.10 1 9 0 4.30 1.70 1 9 0 3.50 1.60 -2 -9 0 10.90 1.50 -2 -9 0 7.80 1.30 2 9 0 7.10 1.70 2 9 0 11.40 2.10 2 9 0 12.00 1.80 -3 -9 0 5.70 0.70 -3 -9 0 4.40 1.30 -3 -9 0 4.50 0.70 -3 -9 0 5.30 1.30 3 9 0 4.70 0.70 3 9 0 3.40 1.30 3 9 0 4.60 0.70 3 9 0 5.70 1.70 -4 -9 0 184.18 4.90 -4 -9 0 192.38 5.50 -4 -9 0 192.48 4.40 4 9 0 197.58 6.30 4 9 0 191.38 5.50 4 9 0 186.28 4.30 -5 -9 0 3.30 1.30 -5 -9 0 5.30 1.10 -5 -9 0 4.30 1.10 5 9 0 3.70 1.40 5 9 0 5.60 1.90 5 9 0 5.40 1.10 5 9 0 3.80 1.80 -6 -9 0 20.70 2.00 -6 -9 0 18.30 1.90 -6 -9 0 22.40 2.10 6 9 0 26.60 2.90 6 9 0 27.40 3.10 6 9 0 24.00 2.10 6 9 0 20.60 2.10 -7 -9 0 11.40 1.70 -7 -9 0 13.80 1.70 -7 -9 0 11.20 1.50 7 9 0 16.70 1.70 7 9 0 13.00 2.30 7 9 0 15.80 2.00 -8 -9 0 1.10 1.40 -8 -9 0 1.80 1.50 -8 -9 0 2.00 1.60 8 9 0 -0.90 1.40 8 9 0 0.30 2.20 8 9 0 -0.40 1.50 8 9 0 2.40 1.40 -9 -9 0 0.70 2.40 -9 -9 0 4.40 1.80 9 9 0 2.70 1.60 9 9 0 1.20 2.40 9 9 0 3.30 1.60 7 -10 0 -0.30 1.00 7 -10 0 0.20 1.00 -7 10 0 -1.70 1.70 -7 10 0 -1.20 0.90 6 -10 0 6.20 1.10 6 -10 0 8.00 1.40 -6 10 0 10.10 2.10 -6 10 0 9.30 1.20 5 -10 0 1.00 0.70 5 -10 0 0.40 0.70 -5 10 0 2.70 1.80 -5 10 0 0.10 0.70 -5 10 0 0.70 0.70 4 -10 0 218.98 6.80 -4 10 0 221.68 6.40 3 -10 0 6.30 1.80 -3 10 0 6.70 1.90 2 -10 0 7.90 1.70 -2 10 0 6.70 1.90 -2 10 0 9.40 2.20 1 -10 0 1.00 1.30 -1 10 0 -0.20 2.00 -1 10 0 -0.30 1.80 0 -10 0 84.49 3.80 0 10 0 94.69 4.30 0 10 0 88.89 4.20 0 10 0 102.19 4.20 -1 -10 0 82.79 3.60 1 10 0 94.09 4.40 1 10 0 78.79 3.90 -2 -10 0 4.80 1.40 2 10 0 5.10 1.80 -3 -10 0 78.69 3.50 -3 -10 0 77.39 3.20 3 10 0 77.69 1.80 3 10 0 84.69 3.90 -4 -10 0 -0.90 0.60 -4 -10 0 -0.20 1.10 -4 -10 0 -1.40 1.20 -4 -10 0 0.10 0.70 4 10 0 2.00 1.70 4 10 0 0.20 0.70 4 10 0 -0.90 0.70 4 10 0 0.30 1.30 -5 -10 0 6.50 1.00 -5 -10 0 3.80 1.40 -5 -10 0 5.60 1.00 5 10 0 1.80 1.90 5 10 0 4.30 1.10 5 10 0 5.00 1.00 5 10 0 5.30 1.60 -6 -10 0 14.20 1.80 -6 -10 0 17.90 1.60 -6 -10 0 18.40 1.90 6 10 0 16.00 1.50 6 10 0 20.60 3.60 6 10 0 14.40 1.50 6 10 0 15.80 2.30 -7 -10 0 -0.40 1.40 -7 -10 0 0.50 1.20 -7 -10 0 1.60 1.20 7 10 0 3.00 2.10 7 10 0 0.80 1.70 7 10 0 1.60 1.40 7 10 0 0.00 1.20 -8 -10 0 4.40 1.60 -8 -10 0 6.80 1.60 -8 -10 0 4.90 1.50 8 10 0 8.20 2.40 8 10 0 8.10 2.80 8 10 0 5.50 1.50 8 10 0 3.80 1.80 6 -11 0 0.30 1.70 6 -11 0 3.90 0.80 6 -11 0 0.20 0.80 -6 11 0 1.00 1.80 -6 11 0 1.50 0.80 -6 11 0 1.00 0.70 5 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62.39 3.20 -9 5 -5 1.40 1.60 -9 5 -5 1.40 1.70 9 -5 5 1.30 1.70 9 -5 5 1.30 1.50 -10 5 -5 -0.70 1.70 10 -5 5 2.40 2.10 10 -5 5 2.90 1.80 -11 5 -5 19.10 2.70 -11 5 -5 17.00 2.50 11 -5 5 24.00 2.80 11 -5 5 17.60 2.40 10 4 -5 1.80 2.10 10 4 -5 -1.80 1.90 10 4 -5 -2.60 3.50 -10 -4 5 1.80 2.10 -10 -4 5 -0.20 2.10 9 4 -5 1.70 1.90 9 4 -5 5.80 2.10 9 4 -5 5.40 2.20 -9 -4 5 3.80 2.00 -9 -4 5 2.80 1.70 8 4 -5 1.30 1.80 -8 -4 5 4.50 1.60 -8 -4 5 -0.90 1.80 -8 -4 5 -2.40 1.60 -8 -4 5 3.00 2.00 7 4 -5 0.20 1.60 7 4 -5 -1.50 1.70 -7 -4 5 1.20 1.60 -7 -4 5 -0.90 1.50 -7 -4 5 1.90 1.20 -7 -4 5 -0.80 1.60 6 4 -5 124.89 5.10 6 4 -5 127.09 4.10 -6 -4 5 120.59 3.90 -6 -4 5 122.99 4.10 -6 -4 5 126.19 4.10 -6 -4 5 132.89 4.90 5 4 -5 16.70 1.60 5 4 -5 12.50 1.60 5 4 -5 17.40 1.60 -5 -4 5 20.10 1.80 -5 -4 5 11.00 1.60 -5 -4 5 16.00 0.90 -5 -4 5 13.70 1.40 -5 -4 5 13.80 1.50 4 4 -5 157.18 4.70 4 4 -5 156.38 4.10 4 4 -5 160.88 4.20 -4 -4 5 162.08 4.90 -4 -4 5 152.38 4.20 -4 -4 5 158.68 4.20 -4 -4 5 150.38 4.20 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1.70 -8 -3 5 2.70 1.20 -8 -3 5 0.40 1.60 7 3 -5 91.59 3.70 7 3 -5 84.19 3.70 7 3 -5 89.49 4.30 -7 -3 5 86.09 3.70 -7 -3 5 78.49 3.10 -7 -3 5 84.99 3.70 -7 -3 5 82.59 6.10 6 3 -5 2.10 1.30 6 3 -5 2.30 1.50 -6 -3 5 -0.60 1.20 -6 -3 5 1.00 1.00 -6 -3 5 1.70 1.30 -6 -3 5 0.20 1.50 5 3 -5 68.29 3.30 5 3 -5 65.39 2.90 5 3 -5 70.79 2.80 -5 -3 5 66.49 2.50 -5 -3 5 72.49 2.90 -5 -3 5 66.79 2.80 -5 -3 5 68.59 3.40 4 3 -5 2.00 1.00 4 3 -5 2.00 1.30 4 3 -5 1.50 1.00 -4 -3 5 1.90 0.90 -4 -3 5 1.80 1.10 -4 -3 5 2.40 1.00 -4 -3 5 1.90 1.20 3 3 -5 2.40 1.00 3 3 -5 3.20 0.90 3 3 -5 3.30 1.00 3 3 -5 3.30 1.10 -3 -3 5 4.10 1.10 -3 -3 5 3.50 1.10 -3 -3 5 2.90 0.90 -3 -3 5 4.70 1.00 2 3 -5 84.99 3.00 2 3 -5 74.69 2.40 2 3 -5 76.19 2.60 2 3 -5 74.69 2.50 -2 -3 5 83.69 3.10 -2 -3 5 76.19 2.50 -2 -3 5 80.59 2.50 -2 -3 5 73.79 2.80 1 3 -5 73.49 2.70 1 3 -5 71.19 2.20 1 3 -5 67.49 2.40 1 3 -5 74.09 1.80 1 3 -5 74.19 2.20 -1 -3 5 72.19 2.20 -1 -3 5 76.59 2.80 -1 -3 5 73.49 2.20 -1 -3 5 75.59 2.40 0 3 -5 20.00 1.60 0 3 -5 21.70 1.80 0 3 -5 22.50 1.30 0 3 -5 25.30 1.40 0 -3 5 23.40 1.40 0 -3 5 24.00 1.60 0 -3 5 24.80 1.80 0 -3 5 25.10 1.30 -1 3 -5 30.50 1.80 -1 3 -5 31.00 1.40 -1 3 -5 32.10 1.40 -1 3 -5 30.90 2.00 1 -3 5 32.70 1.10 1 -3 5 30.90 1.40 1 -3 5 33.80 2.00 1 -3 5 34.80 1.50 -2 3 -5 143.19 3.40 -2 3 -5 147.89 3.40 2 -3 5 145.89 4.00 2 -3 5 140.09 3.40 2 -3 5 148.39 3.50 -3 3 -5 20.50 1.50 -3 3 -5 23.10 1.60 3 -3 5 19.10 1.50 3 -3 5 21.10 1.50 -4 3 -5 276.07 6.10 4 -3 5 277.37 6.10 4 -3 5 279.97 6.10 -5 3 -5 61.09 2.40 -5 3 -5 54.09 2.40 5 -3 5 59.39 2.50 5 -3 5 59.59 2.50 -6 3 -5 -0.50 1.00 -6 3 -5 0.00 1.20 6 -3 5 0.20 1.10 6 -3 5 -0.10 1.10 6 -3 5 -1.20 1.10 -7 3 -5 30.70 3.20 -7 3 -5 31.90 2.40 7 -3 5 30.30 2.30 7 -3 5 30.20 2.40 7 -3 5 32.80 2.60 -8 3 -5 23.00 2.10 8 -3 5 16.70 1.80 8 -3 5 23.60 2.30 8 -3 5 20.80 2.00 -9 3 -5 1.00 1.50 9 -3 5 -0.50 1.50 9 -3 5 -0.10 1.60 -10 3 -5 37.80 3.20 10 -3 5 32.30 3.00 10 -3 5 29.60 2.80 -11 3 -5 2.00 2.00 11 -3 5 2.00 2.20 11 -3 5 1.00 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1.00 2 8 -6 6.30 1.30 2 8 -6 5.10 1.80 2 8 -6 5.60 1.70 -2 -8 6 5.30 1.00 -2 -8 6 3.40 1.00 -2 -8 6 5.90 1.70 1 8 -6 1.60 1.70 1 8 -6 -0.80 1.60 1 8 -6 2.20 1.10 1 8 -6 1.80 0.90 1 8 -6 -0.10 0.80 -1 -8 6 2.00 0.90 -1 -8 6 0.00 0.80 -1 -8 6 1.30 1.40 -1 -8 6 1.40 1.20 0 8 -6 15.70 1.30 0 8 -6 16.00 1.40 0 8 -6 16.30 2.20 0 -8 6 17.10 1.40 0 -8 6 13.20 1.30 0 -8 6 16.90 1.50 0 -8 6 12.80 1.60 0 -8 6 14.30 1.90 -1 8 -6 43.90 1.80 -1 8 -6 44.80 2.20 -1 8 -6 45.80 3.30 1 -8 6 41.30 3.30 1 -8 6 42.00 2.20 1 -8 6 43.80 1.80 1 -8 6 46.50 1.80 -2 8 -6 66.49 2.20 -2 8 -6 69.29 2.30 -2 8 -6 70.79 3.60 2 -8 6 67.09 2.20 2 -8 6 66.29 2.20 2 -8 6 68.09 4.20 2 -8 6 65.59 2.70 -3 8 -6 2.90 1.70 -3 8 -6 2.90 1.00 -3 8 -6 1.70 0.90 3 -8 6 1.50 0.90 3 -8 6 3.80 0.90 3 -8 6 5.20 1.30 3 -8 6 2.30 1.60 -4 8 -6 120.59 4.70 -4 8 -6 112.79 3.30 -4 8 -6 118.49 3.40 4 -8 6 117.39 4.90 4 -8 6 109.69 3.80 4 -8 6 118.49 3.40 4 -8 6 114.19 3.30 -5 8 -6 1.20 1.00 -5 8 -6 3.00 1.80 -5 8 -6 0.00 1.00 5 -8 6 0.90 1.00 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21.30 2.10 4 7 -6 22.10 2.70 4 7 -6 23.90 2.10 -4 -7 6 22.80 2.20 -4 -7 6 27.20 3.20 -4 -7 6 16.30 1.60 -4 -7 6 20.00 1.70 3 7 -6 7.20 1.80 3 7 -6 5.70 1.20 3 7 -6 5.90 1.80 3 7 -6 8.20 1.30 3 7 -6 8.80 1.50 -3 -7 6 3.00 1.50 -3 -7 6 6.20 1.20 -3 -7 6 5.70 1.10 2 7 -6 163.98 4.10 2 7 -6 168.08 5.20 2 7 -6 161.88 5.10 2 7 -6 168.08 4.20 2 7 -6 161.28 4.10 -2 -7 6 161.18 4.10 -2 -7 6 166.08 4.40 -2 -7 6 167.98 5.30 -2 -7 6 161.48 4.10 1 7 -6 22.50 2.10 1 7 -6 26.50 2.70 1 7 -6 23.20 1.60 1 7 -6 24.00 1.60 1 7 -6 24.00 1.70 -1 -7 6 25.00 1.60 -1 -7 6 24.90 2.00 -1 -7 6 23.60 1.60 -1 -7 6 26.00 2.70 0 7 -6 38.60 1.70 0 7 -6 41.40 2.90 0 7 -6 38.70 1.70 0 7 -6 41.60 2.00 0 7 -6 41.80 2.80 0 -7 6 38.90 1.70 0 -7 6 38.30 2.40 0 -7 6 41.20 2.90 0 -7 6 35.50 3.20 0 -7 6 39.90 1.90 0 -7 6 41.30 1.80 -1 7 -6 12.20 1.80 -1 7 -6 9.10 1.00 -1 7 -6 12.10 1.00 1 -7 6 11.80 1.70 1 -7 6 11.00 1.60 1 -7 6 11.80 1.30 1 -7 6 9.80 1.00 1 -7 6 9.50 1.00 -2 7 -6 108.89 2.90 -2 7 -6 107.29 3.00 -2 7 -6 113.49 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1.90 -8 -4 6 -0.30 1.20 -8 -4 6 -0.70 1.50 7 4 -6 79.79 3.60 7 4 -6 86.39 4.60 -7 -4 6 87.49 4.60 -7 -4 6 89.69 3.90 -7 -4 6 74.69 3.20 -7 -4 6 83.39 3.70 6 4 -6 5.00 1.70 6 4 -6 3.20 1.40 -6 -4 6 4.40 0.50 -6 -4 6 5.10 2.30 -6 -4 6 4.40 0.50 -6 -4 6 4.80 1.70 -6 -4 6 5.70 1.60 -6 -4 6 2.10 1.40 5 4 -6 0.20 1.30 5 4 -6 1.60 1.20 5 4 -6 2.50 1.40 -5 -4 6 1.60 1.20 -5 -4 6 0.30 1.10 -5 -4 6 1.20 1.20 -5 -4 6 2.10 1.40 4 4 -6 5.50 1.30 4 4 -6 5.60 1.30 4 4 -6 4.80 1.30 4 4 -6 7.20 1.30 -4 -4 6 8.40 1.30 -4 -4 6 4.40 1.40 -4 -4 6 6.00 1.20 -4 -4 6 5.30 1.30 3 4 -6 291.37 7.20 3 4 -6 299.17 6.50 3 4 -6 291.77 6.50 3 4 -6 292.57 6.70 -3 -4 6 298.47 6.50 -3 -4 6 289.77 6.50 -3 -4 6 287.27 6.60 -3 -4 6 301.67 7.30 2 4 -6 112.79 3.10 2 4 -6 107.19 3.10 2 4 -6 113.19 2.70 2 4 -6 110.69 3.80 2 4 -6 107.29 3.80 -2 -4 6 115.09 3.90 -2 -4 6 112.89 3.20 -2 -4 6 116.89 3.20 -2 -4 6 111.19 3.30 1 4 -6 199.28 4.70 1 4 -6 205.78 4.70 1 4 -6 205.78 5.40 1 4 -6 228.08 6.90 1 4 -6 203.88 4.20 -1 -4 6 201.58 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89.79 2.90 -2 -4 7 92.69 3.10 -2 -4 7 98.39 3.00 -2 -4 7 93.29 3.00 -2 -4 7 97.59 3.60 1 4 -7 15.40 1.60 1 4 -7 15.80 1.80 1 4 -7 16.70 1.60 1 4 -7 14.30 1.50 1 4 -7 17.10 0.80 -1 -4 7 15.60 1.60 -1 -4 7 17.20 1.70 -1 -4 7 17.00 1.80 -1 -4 7 15.00 1.60 0 4 -7 53.99 2.50 0 4 -7 51.99 2.70 0 4 -7 50.19 2.00 0 4 -7 52.89 2.10 0 -4 7 51.69 2.70 0 -4 7 54.19 2.10 -1 4 -7 17.30 1.30 -1 4 -7 12.30 1.40 -1 4 -7 11.60 1.10 -1 4 -7 14.40 1.50 1 -4 7 12.00 1.50 1 -4 7 14.60 1.40 1 -4 7 15.90 1.30 1 -4 7 13.40 0.80 -2 4 -7 30.40 2.20 -2 4 -7 32.70 1.70 -2 4 -7 31.60 1.70 2 -4 7 33.40 2.30 2 -4 7 31.00 1.30 2 -4 7 29.20 1.70 -3 4 -7 552.54 11.80 -3 4 -7 560.44 11.40 -3 4 -7 558.54 11.40 3 -4 7 579.64 11.40 3 -4 7 573.34 11.40 3 -4 7 578.34 12.20 -4 4 -7 111.49 3.40 -4 4 -7 112.59 3.30 4 -4 7 117.39 3.40 4 -4 7 112.59 3.30 4 -4 7 114.29 4.00 -5 4 -7 134.49 3.90 -5 4 -7 130.79 3.90 5 -4 7 138.09 3.90 5 -4 7 135.79 3.90 -6 4 -7 15.20 1.70 -6 4 -7 17.00 1.80 6 -4 7 17.60 1.70 6 -4 7 11.10 1.70 6 -4 7 14.20 1.60 -7 4 -7 38.50 2.70 -7 4 -7 41.00 2.70 7 -4 7 42.90 2.90 7 -4 7 42.80 2.60 -8 4 -7 0.70 0.90 -8 4 -7 -3.30 1.40 8 -4 7 0.30 1.70 8 -4 7 1.20 1.60 -9 4 -7 1.20 1.50 9 -4 7 0.60 1.70 9 -4 7 0.80 1.50 -10 4 -7 5.90 1.80 -10 4 -7 6.80 2.10 10 -4 7 5.00 2.10 10 -4 7 3.20 1.70 -11 4 -7 6.20 2.20 -11 4 -7 3.80 2.00 11 -4 7 2.60 1.80 11 -4 7 6.50 2.40 10 3 -7 4.70 2.20 10 3 -7 4.40 2.70 10 3 -7 1.70 2.00 -10 -3 7 3.60 2.20 -10 -3 7 3.10 3.00 9 3 -7 4.60 2.40 9 3 -7 9.20 2.20 9 3 -7 5.60 2.00 -9 -3 7 6.70 1.90 -9 -3 7 8.80 2.20 -9 -3 7 5.50 1.30 8 3 -7 41.00 3.50 8 3 -7 38.90 3.30 -8 -3 7 36.90 2.70 -8 -3 7 36.70 3.20 -8 -3 7 44.30 4.10 -8 -3 7 43.40 3.60 7 3 -7 6.80 2.00 7 3 -7 4.10 1.60 -7 -3 7 5.50 0.70 -7 -3 7 5.70 1.90 -7 -3 7 5.40 1.20 -7 -3 7 3.70 1.90 -7 -3 7 7.90 3.30 6 3 -7 1.90 1.60 6 3 -7 0.40 1.50 6 3 -7 -1.40 1.30 -6 -3 7 -0.50 1.00 -6 -3 7 -1.10 2.40 -6 -3 7 1.60 0.70 -6 -3 7 -1.80 1.40 5 3 -7 286.67 7.40 5 3 -7 286.67 6.80 5 3 -7 280.67 6.80 -5 -3 7 275.57 7.40 -5 -3 7 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5.60 -4 7 -9 162.08 4.50 4 -7 9 143.39 6.00 4 -7 9 162.48 4.40 4 -7 9 170.48 5.90 4 -7 9 167.08 4.50 -5 7 -9 37.10 3.50 -5 7 -9 40.50 2.50 -5 7 -9 40.10 2.60 5 -7 9 40.20 3.70 5 -7 9 36.20 2.50 5 -7 9 36.50 2.40 -6 7 -9 1.10 1.90 -6 7 -9 2.20 1.30 -6 7 -9 0.20 0.80 6 -7 9 -0.20 1.20 6 -7 9 2.10 1.40 6 -7 9 1.80 1.80 6 -7 9 -1.90 1.20 -7 7 -9 25.10 2.70 -7 7 -9 24.30 2.30 -7 7 -9 30.30 2.70 7 -7 9 24.50 2.80 7 -7 9 24.50 2.50 7 -7 9 23.50 2.10 -8 7 -9 9.90 2.50 -8 7 -9 11.10 1.80 -8 7 -9 8.60 1.70 8 -7 9 10.80 1.80 8 -7 9 8.70 2.10 8 -7 9 15.20 2.10 -9 7 -9 0.30 1.50 -9 7 -9 -0.20 2.30 -9 7 -9 1.60 1.70 9 -7 9 3.10 1.90 9 -7 9 -0.10 2.40 8 6 -9 9.50 2.60 8 6 -9 10.60 2.10 8 6 -9 9.80 2.10 -8 -6 9 9.10 2.40 -8 -6 9 5.30 2.70 -8 -6 9 12.90 2.30 7 6 -9 22.20 2.60 7 6 -9 12.30 2.30 -7 -6 9 11.40 2.00 -7 -6 9 16.80 0.80 -7 -6 9 15.30 2.20 -7 -6 9 13.40 2.40 6 6 -9 5.50 1.70 6 6 -9 3.10 2.10 6 6 -9 3.50 1.60 -6 -6 9 4.10 2.00 -6 -6 9 5.00 0.90 -6 -6 9 3.50 1.50 -6 -6 9 3.50 1.80 5 6 -9 21.50 2.20 5 6 -9 15.10 1.60 -5 -6 9 21.70 2.20 -5 -6 9 15.40 2.50 -5 -6 9 12.90 1.80 4 6 -9 90.49 2.90 4 6 -9 88.99 4.40 4 6 -9 92.89 4.00 4 6 -9 92.49 3.60 4 6 -9 89.19 3.60 -4 -6 9 95.39 3.70 -4 -6 9 88.39 4.60 -4 -6 9 88.79 3.60 3 6 -9 0.70 1.70 3 6 -9 0.90 1.50 3 6 -9 0.90 0.80 3 6 -9 1.50 1.20 3 6 -9 1.60 1.30 -3 -6 9 0.90 1.40 -3 -6 9 1.90 1.60 -3 -6 9 2.50 1.70 2 6 -9 217.08 6.80 2 6 -9 186.28 5.00 2 6 -9 189.88 5.60 2 6 -9 184.88 4.20 2 6 -9 181.28 5.90 -2 -6 9 186.08 5.00 -2 -6 9 196.78 5.10 -2 -6 9 197.08 6.40 1 6 -9 15.50 1.50 1 6 -9 11.90 1.90 1 6 -9 11.40 1.40 1 6 -9 13.00 2.10 -1 -6 9 10.60 1.40 -1 -6 9 13.70 1.90 -1 -6 9 13.30 1.50 0 6 -9 53.79 2.40 0 6 -9 55.29 3.20 0 6 -9 53.29 2.90 0 6 -9 43.50 5.00 0 -6 9 59.29 2.50 0 -6 9 55.19 3.50 0 -6 9 54.19 2.50 -1 6 -9 380.96 8.30 -1 6 -9 372.06 9.40 -1 6 -9 412.86 11.40 -1 6 -9 384.66 9.10 1 -6 9 378.76 7.60 1 -6 9 388.66 9.40 1 -6 9 393.26 8.40 1 -6 9 387.96 8.30 -2 6 -9 6.00 1.90 -2 6 -9 5.10 1.10 2 -6 9 7.20 1.00 2 -6 9 3.00 1.40 2 -6 9 5.20 1.20 2 -6 9 7.30 1.30 -3 6 -9 -0.70 1.00 -3 6 -9 -1.00 1.00 3 -6 9 0.00 0.80 3 -6 9 -0.40 1.00 3 -6 9 0.00 1.10 3 -6 9 0.40 1.30 -4 6 -9 1.70 1.40 -4 6 -9 1.20 1.60 -4 6 -9 1.40 1.10 4 -6 9 0.80 1.00 4 -6 9 1.50 1.50 4 -6 9 0.00 1.10 4 -6 9 2.10 1.20 -5 6 -9 198.38 6.10 -5 6 -9 209.98 5.30 -5 6 -9 209.88 5.40 5 -6 9 195.48 5.30 5 -6 9 191.18 5.40 5 -6 9 213.28 6.60 -6 6 -9 37.30 2.60 -6 6 -9 36.40 3.50 -6 6 -9 35.90 2.70 6 -6 9 39.20 2.80 6 -6 9 38.20 2.60 6 -6 9 38.80 3.60 -7 6 -9 43.10 2.90 -7 6 -9 47.90 3.80 7 -6 9 43.40 3.70 7 -6 9 39.10 2.80 7 -6 9 44.00 3.00 -8 6 -9 -1.20 1.50 -8 6 -9 -0.60 1.50 8 -6 9 1.50 1.40 8 -6 9 -0.40 1.70 8 -6 9 0.80 1.60 -9 6 -9 -2.80 1.50 -9 6 -9 -0.70 3.10 9 -6 9 -0.40 1.80 9 -6 9 -0.60 1.60 -10 6 -9 8.60 2.10 -10 6 -9 8.00 2.00 10 -6 9 8.50 1.90 10 -6 9 12.30 2.40 9 5 -9 1.30 2.10 9 5 -9 -1.90 2.20 -9 -5 9 4.40 2.30 -9 -5 9 2.40 1.90 -9 -5 9 4.30 2.30 8 5 -9 2.20 1.90 8 5 -9 6.80 2.00 8 5 -9 1.50 2.30 -8 -5 9 4.10 2.00 -8 -5 9 5.00 2.10 -8 -5 9 6.30 2.10 7 5 -9 3.00 2.20 -7 -5 9 1.40 1.90 -7 -5 9 4.30 1.70 -7 -5 9 5.40 0.70 -7 -5 9 3.50 2.00 6 5 -9 36.50 3.10 -6 -5 9 47.20 3.30 -6 -5 9 38.90 4.10 -6 -5 9 42.90 3.10 5 5 -9 3.60 1.30 5 5 -9 6.40 1.80 5 5 -9 7.40 1.80 -5 -5 9 9.40 1.70 -5 -5 9 5.40 1.40 -5 -5 9 6.50 1.70 -5 -5 9 6.30 2.10 4 5 -9 8.90 1.60 4 5 -9 10.20 1.70 4 5 -9 7.00 1.90 4 5 -9 13.80 1.80 -4 -5 9 11.40 1.70 -4 -5 9 10.90 1.70 -4 -5 9 9.90 1.50 -4 -5 9 6.10 1.80 3 5 -9 36.70 2.50 3 5 -9 35.20 3.00 3 5 -9 34.20 2.50 3 5 -9 40.00 2.70 3 5 -9 35.30 1.60 -3 -5 9 35.10 3.30 -3 -5 9 33.80 2.40 -3 -5 9 35.90 2.40 -3 -5 9 40.20 2.60 2 5 -9 20.70 2.30 2 5 -9 22.70 2.00 2 5 -9 17.10 1.80 2 5 -9 22.20 2.00 -2 -5 9 19.20 2.10 -2 -5 9 21.20 1.90 -2 -5 9 23.50 2.10 -2 -5 9 20.60 2.10 1 5 -9 11.10 1.50 1 5 -9 11.60 1.30 1 5 -9 12.80 1.70 1 5 -9 13.90 1.40 -1 -5 9 12.40 1.40 -1 -5 9 10.90 1.70 -1 -5 9 13.10 1.30 0 5 -9 19.90 1.80 0 5 -9 21.00 2.30 0 5 -9 23.00 2.50 0 5 -9 22.00 1.80 0 -5 9 16.40 1.70 0 -5 9 23.10 1.80 0 -5 9 19.00 1.80 -1 5 -9 13.30 1.70 -1 5 -9 15.90 1.50 -1 5 -9 9.60 1.20 1 -5 9 14.60 1.40 1 -5 9 14.10 1.40 1 -5 9 10.30 1.50 -2 5 -9 496.65 10.20 -2 5 -9 477.55 10.20 -2 5 -9 502.45 10.90 2 -5 9 495.35 10.20 2 -5 9 511.75 11.20 2 -5 9 482.55 9.60 2 -5 9 498.95 10.30 -3 5 -9 11.30 1.40 -3 5 -9 10.70 1.70 -3 5 -9 6.80 1.30 3 -5 9 10.30 1.40 3 -5 9 8.30 1.20 3 -5 9 9.60 1.70 3 -5 9 10.50 1.00 -4 5 -9 181.88 4.70 -4 5 -9 177.78 4.70 -4 5 -9 180.78 5.40 4 -5 9 175.08 5.60 4 -5 9 177.58 4.70 4 -5 9 180.28 4.80 -5 5 -9 -0.60 1.10 -5 5 -9 -0.80 1.20 5 -5 9 -1.70 1.50 5 -5 9 -0.50 1.10 5 -5 9 -0.90 1.20 -6 5 -9 11.70 1.70 -6 5 -9 7.30 1.50 6 -5 9 8.00 1.70 6 -5 9 9.90 1.70 6 -5 9 8.00 1.60 -7 5 -9 52.69 3.10 7 -5 9 49.70 3.80 7 -5 9 45.40 3.10 7 -5 9 50.99 2.90 -8 5 -9 0.20 1.50 -8 5 -9 -1.20 2.20 8 -5 9 0.30 1.60 8 -5 9 -1.60 1.30 -9 5 -9 55.89 3.50 -9 5 -9 51.49 3.60 9 -5 9 44.80 3.30 -10 5 -9 -0.60 1.70 10 -5 9 -1.70 2.00 9 4 -9 5.00 2.50 9 4 -9 5.30 2.20 9 4 -9 10.40 2.40 -9 -4 9 8.90 2.40 -9 -4 9 5.20 2.70 -9 -4 9 7.60 2.50 8 4 -9 7.40 2.40 8 4 -9 13.00 2.20 -8 -4 9 7.50 2.20 -8 -4 9 6.10 2.00 -8 -4 9 10.70 1.90 7 4 -9 -1.80 1.90 7 4 -9 -0.80 1.80 -7 -4 9 0.00 1.60 -7 -4 9 -0.60 1.10 -7 -4 9 -0.40 0.70 -7 -4 9 0.20 1.70 -7 -4 9 -2.20 2.00 6 4 -9 6.30 1.90 -6 -4 9 9.70 2.20 -6 -4 9 6.90 1.40 -6 -4 9 8.10 1.80 -6 -4 9 7.20 1.80 5 4 -9 -1.90 1.40 5 4 -9 2.70 1.50 5 4 -9 0.00 0.70 -5 -4 9 0.90 1.50 -5 -4 9 -0.70 1.60 -5 -4 9 1.10 1.20 -5 -4 9 1.50 1.50 4 4 -9 56.49 2.70 4 4 -9 52.09 2.90 4 4 -9 52.09 2.90 4 4 -9 51.99 3.40 -4 -4 9 51.59 2.60 -4 -4 9 53.49 2.90 -4 -4 9 56.49 2.90 -4 -4 9 54.39 3.80 3 4 -9 81.99 3.10 3 4 -9 75.19 3.00 3 4 -9 77.09 3.60 3 4 -9 78.49 3.10 -3 -4 9 73.99 2.90 -3 -4 9 76.89 3.10 -3 -4 9 77.79 3.10 -3 -4 9 82.79 3.90 2 4 -9 187.58 3.80 2 4 -9 180.18 4.80 2 4 -9 183.88 5.40 2 4 -9 185.98 4.80 2 4 -9 189.68 4.90 -2 -4 9 180.58 4.90 -2 -4 9 190.48 4.90 -2 -4 9 188.68 5.60 -2 -4 9 188.48 4.90 1 4 -9 61.49 2.50 1 4 -9 62.59 2.80 1 4 -9 64.19 2.50 1 4 -9 58.39 2.90 -1 -4 9 61.79 2.60 -1 -4 9 61.09 3.20 -1 -4 9 58.59 2.50 0 4 -9 0.70 1.20 0 4 -9 -0.20 0.90 0 4 -9 -0.50 1.00 0 4 -9 0.10 0.90 0 -4 9 -0.60 1.10 0 -4 9 -0.70 1.00 0 -4 9 -0.40 1.00 -1 4 -9 44.30 2.10 -1 4 -9 51.09 2.60 -1 4 -9 48.50 2.20 -1 4 -9 45.30 2.70 1 -4 9 47.70 2.20 1 -4 9 47.30 2.20 1 -4 9 48.80 2.90 -2 4 -9 19.30 1.80 -2 4 -9 19.40 1.70 -2 4 -9 20.80 2.20 2 -4 9 20.30 0.90 2 -4 9 16.90 1.70 2 -4 9 20.90 2.30 2 -4 9 18.10 1.70 -3 4 -9 34.40 2.10 -3 4 -9 37.20 2.10 -3 4 -9 41.30 2.60 3 -4 9 38.30 2.10 3 -4 9 35.40 2.10 3 -4 9 37.70 2.80 -4 4 -9 5.50 1.20 -4 4 -9 5.80 1.30 4 -4 9 4.70 1.20 4 -4 9 4.30 1.30 4 -4 9 5.60 1.20 -5 4 -9 23.50 2.20 -5 4 -9 26.30 2.20 5 -4 9 32.00 2.90 5 -4 9 28.00 2.20 5 -4 9 23.50 2.20 -6 4 -9 63.69 3.10 -6 4 -9 62.59 3.00 6 -4 9 60.99 3.00 6 -4 9 63.69 3.60 -7 4 -9 1.50 1.20 -7 4 -9 -0.70 1.30 7 -4 9 -2.50 1.30 7 -4 9 -0.50 1.40 -8 4 -9 2.20 1.50 8 -4 9 1.20 1.50 8 -4 9 3.80 1.90 -9 4 -9 0.10 1.60 9 -4 9 0.10 1.50 9 -4 9 -2.40 1.70 -10 4 -9 9.50 2.10 -10 4 -9 4.60 2.00 10 -4 9 12.10 2.30 10 -4 9 7.30 1.90 -11 4 -9 1.80 2.00 -11 4 -9 -1.20 3.30 11 -4 9 2.90 2.40 11 -4 9 2.10 1.80 9 3 -9 -2.30 2.20 9 3 -9 0.60 1.90 9 3 -9 0.80 1.90 -9 -3 9 -0.30 1.10 -9 -3 9 1.10 1.90 -9 -3 9 2.10 2.20 8 3 -9 -2.80 1.80 8 3 -9 -1.10 2.10 -8 -3 9 -1.80 1.80 -8 -3 9 0.80 1.90 -8 -3 9 -0.20 1.90 7 3 -9 0.80 1.60 7 3 -9 0.60 1.70 -7 -3 9 -1.10 1.50 -7 -3 9 0.20 0.80 -7 -3 9 2.60 1.80 -7 -3 9 1.00 1.90 -7 -3 9 0.60 1.10 6 3 -9 26.90 2.70 6 3 -9 29.90 2.50 -6 -3 9 25.20 2.00 -6 -3 9 26.70 3.90 -6 -3 9 30.30 2.90 -6 -3 9 19.90 2.40 -6 -3 9 28.60 1.80 5 3 -9 41.20 3.30 5 3 -9 42.10 2.90 5 3 -9 43.80 2.80 -5 -3 9 39.40 2.20 -5 -3 9 44.80 2.90 -5 -3 9 38.30 3.60 -5 -3 9 46.60 4.30 4 3 -9 32.50 2.10 4 3 -9 33.40 2.70 4 3 -9 32.70 3.40 4 3 -9 32.50 2.50 -4 -3 9 30.30 2.00 -4 -3 9 33.40 3.10 -4 -3 9 35.60 2.50 -4 -3 9 31.10 2.50 3 3 -9 87.99 4.60 3 3 -9 82.79 3.10 3 3 -9 80.79 3.10 3 3 -9 83.79 3.60 -3 -3 9 79.59 3.10 -3 -3 9 79.09 2.80 -3 -3 9 87.49 3.80 -3 -3 9 82.09 3.10 2 3 -9 22.60 2.00 2 3 -9 30.60 2.50 2 3 -9 26.00 2.00 -2 -3 9 23.50 2.00 -2 -3 9 27.40 2.60 -2 -3 9 27.30 2.10 1 3 -9 295.47 7.20 1 3 -9 282.77 6.50 1 3 -9 291.27 6.60 1 3 -9 300.47 7.20 -1 -3 9 285.67 7.20 -1 -3 9 287.77 6.60 -1 -3 9 291.87 6.60 0 3 -9 5.90 1.10 0 3 -9 5.40 1.20 0 3 -9 8.20 1.20 0 3 -9 5.30 1.20 0 -3 9 5.70 1.10 0 -3 9 9.60 1.30 0 -3 9 5.60 1.30 -1 3 -9 42.20 2.40 -1 3 -9 50.69 2.20 -1 3 -9 46.50 2.10 -1 3 -9 43.60 2.60 1 -3 9 47.90 2.70 1 -3 9 48.90 2.20 1 -3 9 47.10 2.20 -2 3 -9 12.90 1.30 -2 3 -9 14.20 1.60 -2 3 -9 15.70 1.70 2 -3 9 16.20 1.70 2 -3 9 18.10 1.70 2 -3 9 18.60 1.70 -3 3 -9 7.50 1.20 -3 3 -9 8.00 1.20 3 -3 9 5.50 1.20 3 -3 9 7.90 1.30 3 -3 9 8.90 1.30 -4 3 -9 122.49 3.60 -4 3 -9 121.69 3.60 4 -3 9 121.29 4.20 4 -3 9 117.49 3.60 4 -3 9 120.09 3.60 -5 3 -9 28.30 2.20 -5 3 -9 22.20 2.10 5 -3 9 28.10 2.10 5 -3 9 20.30 2.10 5 -3 9 24.30 2.60 -6 3 -9 22.80 2.30 -6 3 -9 19.80 2.10 6 -3 9 17.80 1.80 6 -3 9 23.50 2.00 -7 3 -9 35.50 2.70 7 -3 9 34.20 2.60 7 -3 9 36.00 2.80 -8 3 -9 -0.40 1.50 8 -3 9 1.80 1.60 8 -3 9 0.30 1.40 -9 3 -9 15.60 3.20 9 -3 9 21.30 2.30 9 -3 9 20.40 2.20 -10 3 -9 16.80 2.40 -10 3 -9 17.70 2.40 10 -3 9 15.20 2.20 10 -3 9 16.50 2.40 -11 3 -9 1.60 2.00 -11 3 -9 -0.40 1.90 11 -3 9 1.30 1.80 11 -3 9 3.90 2.30 10 2 -9 3.30 3.00 10 2 -9 2.10 2.30 -10 -2 9 3.10 2.40 -10 -2 9 2.30 1.10 -10 -2 9 0.20 2.10 9 2 -9 8.40 4.00 9 2 -9 5.50 2.40 9 2 -9 8.80 2.20 -9 -2 9 5.80 2.10 -9 -2 9 10.00 2.40 -9 -2 9 8.30 1.00 -9 -2 9 8.80 1.30 8 2 -9 15.90 2.30 -8 -2 9 15.70 2.30 -8 -2 9 14.10 2.20 -8 -2 9 12.00 1.30 -8 -2 9 13.60 1.50 7 2 -9 5.80 1.80 7 2 -9 4.80 1.80 -7 -2 9 2.60 2.00 -7 -2 9 4.00 1.70 -7 -2 9 4.40 1.10 -7 -2 9 3.60 1.00 -7 -2 9 5.50 1.80 6 2 -9 36.20 3.00 6 2 -9 34.50 2.90 -6 -2 9 32.20 2.90 -6 -2 9 36.20 2.00 -6 -2 9 37.20 3.80 -6 -2 9 36.10 2.00 -6 -2 9 37.60 3.00 5 2 -9 1.60 1.40 5 2 -9 -0.60 1.40 5 2 -9 3.10 1.50 -5 -2 9 2.60 1.60 -5 -2 9 -0.20 1.40 -5 -2 9 1.30 0.90 -5 -2 9 -0.40 1.40 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22.70 2.50 0 8 -10 24.10 2.10 0 8 -10 23.60 2.20 0 -8 10 22.30 2.10 0 -8 10 24.20 2.60 0 -8 10 27.00 2.30 -1 8 -10 12.10 2.40 -1 8 -10 9.50 1.40 -1 8 -10 8.80 1.30 1 -8 10 11.70 1.50 1 -8 10 10.00 2.10 1 -8 10 10.70 1.50 -2 8 -10 156.68 4.30 -2 8 -10 154.28 4.30 -2 8 -10 155.78 5.50 2 -8 10 155.18 5.90 2 -8 10 156.18 4.50 2 -8 10 147.09 3.80 2 -8 10 154.98 4.30 -3 8 -10 -0.40 1.10 -3 8 -10 2.30 1.90 -3 8 -10 0.20 1.30 3 -8 10 -2.10 1.50 3 -8 10 0.90 0.90 3 -8 10 -0.10 1.20 3 -8 10 0.10 1.10 -4 8 -10 67.99 2.90 -4 8 -10 68.79 4.10 -4 8 -10 66.89 2.90 4 -8 10 64.09 2.90 4 -8 10 63.79 2.70 4 -8 10 67.69 2.90 4 -8 10 62.39 4.30 -5 8 -10 26.80 2.30 -5 8 -10 25.40 2.80 5 -8 10 28.50 2.10 5 -8 10 25.80 2.30 5 -8 10 30.70 2.40 5 -8 10 21.80 2.70 -6 8 -10 2.70 2.10 -6 8 -10 -1.30 1.20 -6 8 -10 0.50 1.40 6 -8 10 -1.80 1.70 6 -8 10 1.10 1.20 6 -8 10 -2.30 1.30 -7 8 -10 10.20 1.80 -7 8 -10 8.70 2.40 7 -8 10 7.40 2.30 7 -8 10 7.00 1.70 7 -8 10 6.90 1.60 -8 8 -10 1.30 2.40 -8 8 -10 2.90 1.60 -8 8 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7 -7 10 15.90 1.90 7 -7 10 16.40 2.40 7 -7 10 14.80 1.90 -8 7 -10 -0.60 1.70 -8 7 -10 -0.50 1.50 -8 7 -10 -0.80 2.10 8 -7 10 0.60 1.70 8 -7 10 1.10 2.00 8 -7 10 0.50 1.40 -9 7 -10 1.00 1.70 -9 7 -10 1.90 2.40 -9 7 -10 1.80 1.70 9 -7 10 3.00 2.00 9 -7 10 3.20 2.20 9 -7 10 2.50 1.70 8 6 -10 17.10 2.50 8 6 -10 17.60 3.60 8 6 -10 19.80 3.10 -8 -6 10 12.50 2.50 -8 -6 10 20.70 2.70 -8 -6 10 17.10 2.50 7 6 -10 1.70 2.50 7 6 -10 1.30 1.90 -7 -6 10 2.40 1.70 -7 -6 10 2.20 2.10 -7 -6 10 3.00 1.90 6 6 -10 12.10 2.10 6 6 -10 13.70 2.00 6 6 -10 14.70 2.40 -6 -6 10 15.00 2.60 -6 -6 10 16.30 2.40 -6 -6 10 18.30 2.10 -6 -6 10 12.40 1.20 5 6 -10 0.10 1.10 5 6 -10 1.70 1.50 -5 -6 10 1.80 1.70 -5 -6 10 0.30 2.00 -5 -6 10 -2.20 1.40 4 6 -10 7.20 1.30 4 6 -10 8.00 1.60 4 6 -10 5.70 1.10 -4 -6 10 6.20 1.70 -4 -6 10 6.70 1.70 -4 -6 10 7.60 2.20 3 6 -10 171.08 5.50 3 6 -10 175.68 6.00 3 6 -10 175.08 5.00 3 6 -10 177.78 5.10 3 6 -10 177.28 4.10 -3 -6 10 182.98 6.20 -3 -6 10 191.58 5.20 -3 -6 10 176.48 5.10 2 6 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30.10 2.40 5 -6 10 23.90 2.50 5 -6 10 29.60 3.40 5 -6 10 23.00 2.00 5 -6 10 28.50 2.40 -6 6 -10 54.59 3.90 -6 6 -10 54.09 3.00 6 -6 10 55.89 3.10 6 -6 10 54.79 4.10 6 -6 10 52.39 2.90 -7 6 -10 12.70 2.90 -7 6 -10 12.80 1.90 -7 6 -10 9.00 2.40 7 -6 10 9.70 1.60 7 -6 10 15.50 2.00 7 -6 10 9.40 2.00 -8 6 -10 2.90 1.60 -8 6 -10 4.00 1.70 8 -6 10 6.50 1.80 8 -6 10 4.50 1.70 8 -6 10 4.70 1.90 -9 6 -10 2.10 1.70 -9 6 -10 1.10 1.80 9 -6 10 1.10 1.50 9 -6 10 0.00 1.70 9 -6 10 5.20 3.50 -10 6 -10 2.20 1.90 10 -6 10 6.60 2.20 8 5 -10 -3.60 2.20 8 5 -10 -0.10 1.90 -8 -5 10 1.40 2.10 -8 -5 10 2.80 2.10 -8 -5 10 -2.60 3.80 7 5 -10 7.90 2.10 7 5 -10 2.10 2.10 7 5 -10 4.00 1.90 -7 -5 10 2.80 2.20 -7 -5 10 3.20 1.90 -7 -5 10 6.00 2.10 -7 -5 10 3.90 0.80 6 5 -10 30.80 2.60 6 5 -10 28.40 2.90 -6 -5 10 25.60 3.60 -6 -5 10 30.20 3.00 -6 -5 10 28.10 2.90 5 5 -10 30.60 2.80 -5 -5 10 29.70 2.80 -5 -5 10 29.10 3.00 -5 -5 10 21.90 2.40 -5 -5 10 23.40 2.80 4 5 -10 211.08 5.80 4 5 -10 205.18 4.90 4 5 -10 213.58 5.80 4 5 -10 213.38 5.80 -4 -5 10 204.48 6.80 -4 -5 10 203.88 5.60 -4 -5 10 220.38 5.80 -4 -5 10 220.68 5.80 3 5 -10 45.10 2.70 3 5 -10 44.70 2.90 3 5 -10 46.60 2.80 3 5 -10 40.60 3.40 3 5 -10 42.50 1.70 -3 -5 10 43.30 2.70 -3 -5 10 46.40 2.80 -3 -5 10 50.19 2.80 -3 -5 10 49.80 3.70 2 5 -10 27.30 2.30 2 5 -10 29.00 2.50 2 5 -10 29.10 1.00 2 5 -10 28.60 3.00 2 5 -10 30.70 2.30 -2 -5 10 31.80 2.40 -2 -5 10 30.20 2.40 -2 -5 10 32.00 3.20 1 5 -10 57.19 2.60 1 5 -10 52.79 2.60 1 5 -10 55.69 5.00 1 5 -10 58.49 3.10 -1 -5 10 53.79 2.70 -1 -5 10 56.69 2.60 -1 -5 10 56.29 3.50 0 5 -10 7.30 1.50 0 5 -10 11.40 1.40 0 5 -10 9.10 1.30 0 5 -10 8.80 1.70 0 -5 10 8.60 1.30 0 -5 10 7.90 1.30 0 -5 10 7.90 1.60 -1 5 -10 243.68 6.00 -1 5 -10 253.87 6.50 -1 5 -10 255.47 6.90 -1 5 -10 250.17 6.00 1 -5 10 252.77 6.00 1 -5 10 252.77 6.00 1 -5 10 262.37 7.00 -2 5 -10 14.10 1.50 -2 5 -10 18.80 1.60 -2 5 -10 17.10 2.00 2 -5 10 16.80 0.90 2 -5 10 14.70 1.50 2 -5 10 19.20 1.70 2 -5 10 13.40 1.90 -3 5 -10 223.38 5.60 -3 5 -10 224.48 6.20 -3 5 -10 219.38 5.50 3 -5 10 223.68 5.60 3 -5 10 225.28 5.00 3 -5 10 228.18 6.50 3 -5 10 223.78 5.60 -4 5 -10 117.19 3.80 -4 5 -10 113.29 3.90 -4 5 -10 114.09 5.20 4 -5 10 120.59 3.80 4 -5 10 118.29 3.80 4 -5 10 118.49 4.60 -5 5 -10 25.10 2.40 -5 5 -10 26.90 2.30 5 -5 10 22.80 2.30 5 -5 10 25.60 2.10 5 -5 10 22.70 2.30 -6 5 -10 0.00 1.40 -6 5 -10 -0.50 1.30 6 -5 10 1.50 1.60 6 -5 10 -0.60 1.40 6 -5 10 -1.80 1.20 -7 5 -10 3.40 1.70 7 -5 10 1.30 1.60 7 -5 10 1.90 1.40 7 -5 10 0.70 1.50 -8 5 -10 65.39 3.60 -8 5 -10 74.59 3.70 8 -5 10 65.69 3.70 8 -5 10 67.59 3.50 8 -5 10 69.39 4.30 -9 5 -10 0.40 1.90 -9 5 -10 -1.20 1.60 9 -5 10 -1.80 1.50 9 -5 10 0.70 1.80 -10 5 -10 4.10 1.90 -10 5 -10 10.60 2.20 10 -5 10 11.40 2.30 10 -5 10 9.40 2.10 9 4 -10 -0.20 3.80 9 4 -10 3.20 2.10 -9 -4 10 1.20 2.40 -9 -4 10 0.70 1.90 -9 -4 10 4.90 2.40 8 4 -10 -2.30 1.70 8 4 -10 -2.30 2.20 -8 -4 10 1.40 0.80 -8 -4 10 -2.30 1.70 -8 -4 10 -0.90 2.00 -8 -4 10 0.50 2.10 -8 -4 10 -0.50 1.50 7 4 -10 49.60 4.30 7 4 -10 50.29 3.60 7 4 -10 48.90 3.50 -7 -4 10 59.49 3.80 -7 -4 10 51.79 3.50 -7 -4 10 51.59 2.70 -7 -4 10 54.29 2.00 -7 -4 10 56.99 4.60 6 4 -10 4.40 1.80 -6 -4 10 6.20 1.70 -6 -4 10 5.20 1.40 -6 -4 10 3.80 2.00 -6 -4 10 4.30 1.80 5 4 -10 14.60 2.00 -5 -4 10 10.10 1.80 -5 -4 10 8.50 2.00 -5 -4 10 11.90 2.00 4 4 -10 3.80 1.40 4 4 -10 6.80 1.40 4 4 -10 1.90 1.40 4 4 -10 4.20 1.50 -4 -4 10 2.70 1.50 -4 -4 10 6.60 1.40 -4 -4 10 4.60 1.50 -4 -4 10 3.10 1.80 3 4 -10 16.90 2.00 3 4 -10 19.90 1.80 3 4 -10 19.90 2.20 3 4 -10 22.60 1.90 -3 -4 10 15.70 2.00 -3 -4 10 20.00 1.80 -3 -4 10 22.10 2.30 -3 -4 10 23.90 2.40 2 4 -10 42.20 1.10 2 4 -10 41.10 2.40 2 4 -10 42.80 2.50 2 4 -10 39.90 2.50 2 4 -10 42.30 2.90 -2 -4 10 40.50 2.50 -2 -4 10 41.00 3.10 -2 -4 10 39.60 2.50 1 4 -10 -0.70 1.20 1 4 -10 -1.60 1.00 1 4 -10 2.10 1.30 1 4 -10 -0.40 1.10 -1 -4 10 1.60 1.10 -1 -4 10 0.70 1.10 -1 -4 10 -1.80 1.20 0 4 -10 83.29 3.60 0 4 -10 82.89 3.00 0 4 -10 77.89 2.90 0 4 -10 86.79 3.30 0 -4 10 83.69 3.70 0 -4 10 80.29 3.00 0 -4 10 83.19 3.00 -1 4 -10 5.70 1.40 -1 4 -10 7.60 1.50 -1 4 -10 10.00 1.30 -1 4 -10 8.30 1.40 1 -4 10 8.50 1.30 1 -4 10 8.70 1.50 1 -4 10 6.00 1.20 -2 4 -10 13.50 1.80 -2 4 -10 10.00 1.30 -2 4 -10 9.20 1.30 2 -4 10 6.60 1.50 2 -4 10 11.90 1.40 2 -4 10 11.20 0.70 2 -4 10 9.70 1.40 -3 4 -10 -1.00 1.40 -3 4 -10 -0.20 1.00 -3 4 -10 1.20 1.20 3 -4 10 0.10 1.00 3 -4 10 -0.60 1.00 3 -4 10 -1.60 1.20 -4 4 -10 8.70 1.40 -4 4 -10 11.20 1.50 4 -4 10 7.20 1.40 4 -4 10 8.20 1.60 4 -4 10 9.50 1.30 -5 4 -10 55.59 2.80 -5 4 -10 58.39 2.80 5 -4 10 54.89 2.80 5 -4 10 57.29 3.50 5 -4 10 55.79 2.90 -6 4 -10 15.00 1.80 -6 4 -10 10.80 1.60 6 -4 10 12.40 1.70 6 -4 10 12.30 1.70 6 -4 10 14.80 2.60 -7 4 -10 1.90 1.50 7 -4 10 5.80 1.70 7 -4 10 2.00 1.60 7 -4 10 2.80 1.40 -8 4 -10 -1.20 1.40 8 -4 10 2.00 1.80 8 -4 10 -1.60 1.40 -9 4 -10 18.50 2.40 9 -4 10 17.80 2.20 9 -4 10 18.00 2.40 -10 4 -10 1.10 1.70 -10 4 -10 1.60 1.90 10 -4 10 2.70 1.80 10 -4 10 -1.80 2.00 -11 4 -10 4.90 2.10 11 -4 10 3.20 2.30 9 3 -10 -0.20 2.00 9 3 -10 5.00 2.10 9 3 -10 2.00 2.50 -9 -3 10 5.00 2.20 -9 -3 10 8.20 2.50 -9 -3 10 3.30 1.20 8 3 -10 -0.90 3.90 8 3 -10 -0.40 2.00 -8 -3 10 3.60 2.20 -8 -3 10 0.80 0.80 -8 -3 10 -1.30 1.70 -8 -3 10 1.70 2.00 7 3 -10 2.50 2.00 7 3 -10 2.10 1.80 -7 -3 10 2.70 2.00 -7 -3 10 2.10 1.70 -7 -3 10 2.50 1.00 -7 -3 10 2.20 1.90 -7 -3 10 0.40 1.10 6 3 -10 30.80 2.60 6 3 -10 25.60 2.70 -6 -3 10 28.50 2.90 -6 -3 10 28.20 2.90 -6 -3 10 26.40 2.10 -6 -3 10 29.90 3.10 5 3 -10 1.50 1.50 5 3 -10 0.00 1.50 5 3 -10 -1.30 0.80 -5 -3 10 -1.20 1.60 -5 -3 10 0.00 1.60 -5 -3 10 1.40 1.50 -5 -3 10 1.10 1.10 4 3 -10 3.10 1.20 4 3 -10 2.90 1.50 4 3 -10 1.60 1.40 4 3 -10 3.50 1.40 -4 -3 10 1.40 1.40 -4 -3 10 2.40 1.40 -4 -3 10 1.70 1.10 -4 -3 10 0.70 1.50 3 3 -10 -2.30 1.10 3 3 -10 -0.70 1.00 3 3 -10 0.40 1.30 3 3 -10 -0.40 1.20 -3 -3 10 -0.60 1.20 -3 -3 10 -0.50 1.30 -3 -3 10 -0.70 1.20 2 3 -10 157.48 4.20 2 3 -10 153.48 4.40 2 3 -10 158.08 5.00 2 3 -10 157.58 4.40 -2 -3 10 160.68 4.40 -2 -3 10 152.98 5.00 -2 -3 10 155.28 4.40 1 3 -10 3.90 1.30 1 3 -10 3.90 1.10 1 3 -10 3.50 1.10 1 3 -10 2.00 1.10 -1 -3 10 2.60 1.10 -1 -3 10 3.60 1.20 -1 -3 10 2.10 1.20 0 3 -10 30.60 2.10 0 3 -10 25.40 1.90 0 3 -10 27.80 2.40 0 3 -10 26.40 2.00 0 -3 10 28.90 2.50 0 -3 10 25.80 2.00 0 -3 10 25.00 2.00 -1 3 -10 2.60 1.10 -1 3 -10 1.00 1.00 -1 3 -10 2.70 1.20 -1 3 -10 4.50 1.10 1 -3 10 3.40 1.30 1 -3 10 5.40 1.10 1 -3 10 3.90 1.10 -2 3 -10 3.00 1.10 -2 3 -10 4.70 1.10 2 -3 10 4.90 1.10 2 -3 10 2.90 1.10 -3 3 -10 170.68 4.50 -3 3 -10 167.58 4.50 3 -3 10 168.58 5.00 3 -3 10 169.28 4.50 3 -3 10 170.78 4.50 -4 3 -10 6.30 1.30 -4 3 -10 4.50 1.30 4 -3 10 4.50 1.30 4 -3 10 5.70 1.30 4 -3 10 3.30 1.30 -5 3 -10 147.19 4.40 -5 3 -10 157.68 4.50 5 -3 10 144.89 4.40 5 -3 10 151.08 4.40 5 -3 10 150.78 5.00 -6 3 -10 -0.50 1.30 -6 3 -10 -1.10 1.30 6 -3 10 -1.10 1.90 6 -3 10 -1.00 1.40 6 -3 10 -1.30 1.40 -7 3 -10 -0.20 1.40 7 -3 10 -1.20 1.40 7 -3 10 -0.70 1.30 -8 3 -10 7.80 1.80 8 -3 10 7.00 1.70 8 -3 10 7.20 2.70 -9 3 -10 2.80 1.80 9 -3 10 2.00 1.60 9 -3 10 0.50 1.90 -10 3 -10 21.60 2.40 10 -3 10 31.80 3.20 10 -3 10 30.50 3.00 -11 3 -10 1.30 2.00 -11 3 -10 3.10 2.00 11 -3 10 2.10 2.10 11 -3 10 1.60 1.80 9 2 -10 3.90 2.00 9 2 -10 -0.80 2.20 9 2 -10 5.70 2.20 -9 -2 10 6.00 3.00 -9 -2 10 1.90 2.30 -9 -2 10 5.50 0.90 8 2 -10 7.80 2.10 8 2 -10 3.70 2.30 -8 -2 10 4.20 2.00 -8 -2 10 4.70 1.10 -8 -2 10 5.60 2.10 -8 -2 10 5.50 2.30 -8 -2 10 5.40 1.10 7 2 -10 12.90 2.30 7 2 -10 12.00 2.20 -7 -2 10 13.10 2.20 -7 -2 10 12.30 1.40 -7 -2 10 9.00 1.20 -7 -2 10 7.00 2.10 -7 -2 10 11.30 2.30 6 2 -10 1.20 1.90 6 2 -10 2.00 1.80 -6 -2 10 -0.50 0.90 -6 -2 10 -1.30 1.80 -6 -2 10 3.90 1.80 -6 -2 10 -0.30 1.50 5 2 -10 113.29 4.80 5 2 -10 107.19 4.20 5 2 -10 105.69 4.20 -5 -2 10 116.39 4.30 -5 -2 10 110.29 3.20 -5 -2 10 107.69 4.10 -5 -2 10 113.59 5.00 4 2 -10 11.90 2.70 4 2 -10 13.70 1.30 4 2 -10 14.00 1.80 -4 -2 10 13.30 1.70 -4 -2 10 12.70 1.70 -4 -2 10 16.30 2.10 3 2 -10 85.79 2.80 3 2 -10 93.49 3.40 3 2 -10 85.89 3.30 3 2 -10 88.79 3.90 -3 -2 10 86.89 3.30 -3 -2 10 84.59 3.90 -3 -2 10 87.89 3.40 2 2 -10 142.39 4.10 2 2 -10 133.99 3.00 2 2 -10 139.79 4.50 2 2 -10 140.99 3.70 2 2 -10 136.39 4.10 -2 -2 10 139.69 4.60 -2 -2 10 138.19 4.10 -2 -2 10 137.79 4.00 1 2 -10 0.60 1.10 1 2 -10 1.50 1.10 1 2 -10 0.20 1.00 1 2 -10 1.00 1.00 -1 -2 10 0.70 1.10 -1 -2 10 1.70 1.20 -1 -2 10 0.10 1.00 0 2 -10 430.36 9.90 0 2 -10 396.86 8.60 0 2 -10 388.66 8.60 0 2 -10 397.36 9.00 0 -2 10 400.26 9.00 0 -2 10 401.46 8.60 0 -2 10 387.96 8.50 -1 2 -10 35.00 2.10 -1 2 -10 32.60 2.40 -1 2 -10 37.60 2.10 1 -2 10 36.30 2.40 1 -2 10 34.00 2.10 1 -2 10 33.40 2.10 -2 2 -10 136.59 3.80 -2 2 -10 133.99 3.80 -2 2 -10 126.39 4.00 2 -2 10 134.89 3.80 2 -2 10 126.89 3.70 2 -2 10 133.39 4.20 2 -2 10 130.69 2.80 -3 2 -10 -0.10 1.00 -3 2 -10 -1.30 1.00 3 -2 10 1.90 1.00 3 -2 10 -1.50 1.00 3 -2 10 -2.00 1.10 -4 2 -10 92.69 3.30 -4 2 -10 93.29 3.20 4 -2 10 98.29 3.60 4 -2 10 92.09 3.30 4 -2 10 89.69 3.30 -5 2 -10 9.50 1.50 -5 2 -10 10.80 1.50 5 -2 10 10.10 1.50 5 -2 10 11.50 1.60 5 -2 10 11.00 1.50 -6 2 -10 70.49 3.20 -6 2 -10 72.59 4.30 6 -2 10 74.29 3.20 6 -2 10 71.39 3.50 6 -2 10 70.29 3.30 -7 2 -10 18.20 1.90 -7 2 -10 17.30 1.90 7 -2 10 18.80 1.90 7 -2 10 21.20 2.10 -8 2 -10 -0.50 1.50 -8 2 -10 -1.90 1.50 8 -2 10 1.30 1.50 8 -2 10 -1.90 1.70 -9 2 -10 45.80 3.50 -9 2 -10 41.50 3.20 9 -2 10 40.20 3.60 9 -2 10 38.20 3.20 -10 2 -10 1.00 2.00 -10 2 -10 4.00 2.00 10 -2 10 1.60 1.70 10 -2 10 3.10 2.00 -11 2 -10 3.70 2.00 -11 2 -10 1.80 2.00 11 -2 10 -1.10 2.00 11 -2 10 5.80 2.40 9 1 -10 9.00 3.20 9 1 -10 6.20 2.00 9 1 -10 4.10 2.70 -9 -1 10 5.70 2.10 -9 -1 10 7.50 1.00 8 1 -10 12.00 2.50 8 1 -10 15.60 2.60 -8 -1 10 11.90 1.10 -8 -1 10 14.30 2.30 -8 -1 10 15.10 1.50 -8 -1 10 17.50 2.60 7 1 -10 5.60 1.90 7 1 -10 3.90 1.90 -7 -1 10 6.80 1.30 -7 -1 10 8.60 2.00 -7 -1 10 5.00 0.90 -7 -1 10 4.00 1.80 6 1 -10 22.10 2.30 6 1 -10 16.60 2.20 6 1 -10 22.00 2.20 -6 -1 10 22.60 2.10 -6 -1 10 27.10 2.40 -6 -1 10 18.30 2.20 -6 -1 10 19.30 2.30 5 1 -10 30.20 3.30 5 1 -10 31.30 2.70 5 1 -10 33.70 2.90 -5 -1 10 33.40 3.90 -5 -1 10 27.10 3.80 -5 -1 10 27.90 2.60 4 1 -10 89.39 3.60 4 1 -10 93.89 4.10 4 1 -10 93.09 3.60 -4 -1 10 95.29 4.20 -4 -1 10 99.09 3.60 -4 -1 10 95.69 3.70 3 1 -10 12.30 1.80 3 1 -10 10.40 1.50 3 1 -10 13.60 1.30 -3 -1 10 10.70 1.50 -3 -1 10 14.80 1.80 -3 -1 10 12.90 1.60 2 1 -10 38.20 2.70 2 1 -10 38.80 2.40 2 1 -10 40.20 1.80 2 1 -10 40.70 1.50 2 1 -10 40.00 2.40 -2 -1 10 42.80 2.90 -2 -1 10 41.60 2.30 -2 -1 10 39.10 2.40 1 1 -10 462.15 9.70 1 1 -10 459.45 9.70 1 1 -10 466.05 10.10 1 1 -10 463.05 9.30 1 1 -10 448.56 8.80 -1 -1 10 447.06 9.70 -1 -1 10 453.25 10.10 -1 -1 10 470.55 9.70 0 1 -10 40.60 2.40 0 1 -10 38.20 2.20 0 1 -10 38.00 2.20 0 1 -10 40.30 2.00 0 -1 10 39.70 2.20 0 -1 10 41.00 2.50 0 -1 10 37.00 2.20 -1 1 -10 0.50 1.00 -1 1 -10 0.40 1.00 -1 1 -10 1.60 1.10 1 -1 10 1.00 1.00 1 -1 10 2.40 1.10 1 -1 10 4.20 1.10 -2 1 -10 77.89 2.80 -2 1 -10 77.19 2.80 -2 1 -10 78.29 3.00 2 -1 10 74.39 2.70 2 -1 10 72.49 2.90 2 -1 10 72.99 2.80 -3 1 -10 761.52 15.10 -3 1 -10 753.82 15.10 3 -1 10 757.42 15.30 3 -1 10 754.62 15.10 3 -1 10 757.82 15.10 -4 1 -10 10.90 1.40 -4 1 -10 9.90 1.40 4 -1 10 7.30 1.30 4 -1 10 7.60 1.30 4 -1 10 9.70 1.40 -5 1 -10 33.00 2.40 -5 1 -10 37.80 2.50 5 -1 10 40.20 2.50 5 -1 10 38.10 2.50 5 -1 10 37.90 2.50 -6 1 -10 68.19 3.20 -6 1 -10 76.19 3.30 6 -1 10 72.29 3.30 6 -1 10 71.79 3.20 6 -1 10 70.99 3.20 -7 1 -10 46.20 3.00 -7 1 -10 43.00 2.90 7 -1 10 41.70 3.50 7 -1 10 42.30 2.90 -8 1 -10 73.29 4.10 -8 1 -10 70.89 3.70 8 -1 10 71.49 3.60 8 -1 10 71.29 3.70 -9 1 -10 51.89 3.70 -9 1 -10 48.30 3.40 9 -1 10 46.50 3.30 9 -1 10 50.09 3.80 -10 1 -10 3.40 2.10 -10 1 -10 0.80 2.00 10 -1 10 2.60 2.00 10 -1 10 1.90 2.10 -11 1 -10 9.00 2.30 -11 1 -10 11.60 2.30 11 -1 10 16.30 2.60 11 -1 10 13.10 2.30 9 0 -10 -3.70 2.10 9 0 -10 4.10 2.40 9 0 -10 0.50 1.80 -9 0 10 0.70 1.20 -9 0 10 3.10 2.30 -9 0 10 2.30 2.00 8 0 -10 9.70 2.20 8 0 -10 6.60 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200.78 4.50 -3 -7 11 209.98 5.80 -3 -7 11 202.98 5.70 -3 -7 11 213.78 7.20 2 7 -11 29.70 2.50 2 7 -11 28.50 3.20 -2 -7 11 24.10 2.80 -2 -7 11 28.40 2.60 -2 -7 11 26.60 2.50 1 7 -11 10.40 1.60 1 7 -11 10.80 1.70 1 7 -11 7.70 1.90 -1 -7 11 9.00 1.60 -1 -7 11 6.30 1.90 -1 -7 11 6.20 1.40 0 7 -11 66.49 3.00 0 7 -11 71.49 4.00 0 7 -11 66.09 3.00 0 -7 11 66.89 4.20 0 -7 11 65.09 3.10 0 -7 11 65.09 3.00 -1 7 -11 98.69 4.50 -1 7 -11 96.89 3.40 -1 7 -11 96.59 3.50 1 -7 11 98.09 3.50 1 -7 11 89.79 4.60 1 -7 11 98.09 3.50 -2 7 -11 59.09 3.80 -2 7 -11 57.29 2.80 -2 7 -11 55.99 2.80 2 -7 11 50.79 2.70 2 -7 11 52.69 1.80 2 -7 11 54.59 2.80 2 -7 11 58.09 3.80 -3 7 -11 4.60 1.40 -3 7 -11 6.50 2.10 -3 7 -11 2.10 1.30 3 -7 11 4.60 1.40 3 -7 11 3.60 1.30 3 -7 11 4.40 1.80 3 -7 11 4.40 0.90 -4 7 -11 6.10 1.40 -4 7 -11 6.80 1.50 -4 7 -11 4.70 2.00 4 -7 11 8.10 2.00 4 -7 11 4.40 1.50 4 -7 11 6.10 1.40 4 -7 11 7.20 1.20 -5 7 -11 1.40 1.30 -5 7 -11 -0.80 1.90 5 -7 11 2.80 1.80 5 -7 11 3.30 1.30 5 -7 11 1.70 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11 0.50 1.80 2 6 -11 12.50 1.60 2 6 -11 17.60 1.80 2 6 -11 14.40 3.00 -2 -6 11 16.20 2.40 -2 -6 11 14.20 1.70 -2 -6 11 19.50 1.90 1 6 -11 73.59 3.20 1 6 -11 81.29 3.20 -1 -6 11 79.19 3.30 -1 -6 11 79.39 3.30 -1 -6 11 79.39 4.20 0 6 -11 152.98 4.50 0 6 -11 155.38 4.50 0 6 -11 154.48 5.60 0 -6 11 164.38 5.70 0 -6 11 142.99 6.10 0 -6 11 154.58 4.50 -1 6 -11 5.50 1.50 -1 6 -11 10.10 2.00 -1 6 -11 7.00 1.40 -1 6 -11 9.20 1.50 1 -6 11 6.90 2.50 1 -6 11 8.00 1.80 1 -6 11 6.50 1.40 -2 6 -11 77.79 3.10 -2 6 -11 76.29 3.10 -2 6 -11 79.99 3.90 2 -6 11 77.29 1.90 2 -6 11 82.39 4.20 2 -6 11 74.79 3.10 -3 6 -11 115.09 3.80 -3 6 -11 109.09 3.70 -3 6 -11 121.19 4.60 3 -6 11 115.49 3.80 3 -6 11 121.29 3.80 3 -6 11 112.69 4.80 3 -6 11 111.19 3.00 -4 6 -11 2.40 1.40 -4 6 -11 3.30 1.90 -4 6 -11 2.60 1.30 4 -6 11 4.50 1.00 4 -6 11 3.90 1.60 -5 6 -11 91.89 3.60 -5 6 -11 97.29 3.70 -5 6 -11 102.99 4.50 5 -6 11 92.69 3.20 5 -6 11 101.59 3.80 5 -6 11 96.99 3.70 5 -6 11 100.79 4.80 -6 6 -11 57.69 4.10 -6 6 -11 57.09 3.10 6 -6 11 60.79 3.20 6 -6 11 63.59 4.20 6 -6 11 57.09 3.20 -7 6 -11 3.90 1.60 -7 6 -11 3.50 2.20 -7 6 -11 2.90 1.50 7 -6 11 3.70 1.80 7 -6 11 3.50 1.60 7 -6 11 1.30 1.70 -8 6 -11 49.10 3.30 -8 6 -11 49.00 3.50 8 -6 11 50.89 3.30 8 -6 11 57.89 4.40 8 -6 11 49.90 3.50 -9 6 -11 0.10 1.80 -9 6 -11 1.60 1.70 9 -6 11 1.40 2.80 9 -6 11 2.70 1.90 9 -6 11 1.90 2.70 8 5 -11 -4.90 2.30 8 5 -11 1.80 3.00 -8 -5 11 0.60 2.20 -8 -5 11 0.40 2.10 -8 -5 11 -1.20 1.80 7 5 -11 1.20 1.90 7 5 -11 -0.50 2.10 7 5 -11 4.60 2.00 -7 -5 11 2.80 2.30 -7 -5 11 6.00 1.80 -7 -5 11 4.70 2.20 -7 -5 11 2.10 1.00 6 5 -11 -1.40 1.80 6 5 -11 0.10 3.00 6 5 -11 3.20 2.20 -6 -5 11 2.40 1.70 -6 -5 11 1.00 1.80 -6 -5 11 1.30 2.10 5 5 -11 28.80 2.50 -5 -5 11 37.30 3.20 -5 -5 11 33.00 3.00 -5 -5 11 32.20 3.90 4 5 -11 2.90 1.00 4 5 -11 6.90 1.70 4 5 -11 4.10 1.60 -4 -5 11 3.60 1.60 -4 -5 11 5.00 2.10 -4 -5 11 4.20 1.50 -4 -5 11 3.40 1.50 3 5 -11 10.60 1.70 3 5 -11 12.30 1.90 3 5 -11 14.70 2.00 -3 -5 11 12.80 2.20 -3 -5 11 14.40 1.90 -3 -5 11 11.70 1.80 2 5 -11 37.30 2.60 2 5 -11 46.00 2.80 2 5 -11 42.60 2.90 -2 -5 11 39.40 2.70 -2 -5 11 44.60 2.70 -2 -5 11 43.70 3.60 1 5 -11 15.10 1.90 1 5 -11 19.00 1.80 1 5 -11 20.90 1.80 1 5 -11 15.90 1.90 -1 -5 11 21.90 1.90 -1 -5 11 16.00 2.90 -1 -5 11 21.20 1.90 0 5 -11 68.09 3.60 0 5 -11 66.79 3.40 0 5 -11 69.59 2.90 0 5 -11 69.39 3.40 0 -5 11 74.59 3.90 0 -5 11 70.69 3.00 0 -5 11 72.69 3.00 -1 5 -11 -0.50 1.30 -1 5 -11 0.90 1.50 -1 5 -11 1.10 1.30 1 -5 11 -1.00 1.10 1 -5 11 -1.00 1.30 1 -5 11 -0.40 1.10 -2 5 -11 217.18 7.30 -2 5 -11 217.28 6.10 -2 5 -11 212.48 5.40 2 -5 11 217.78 5.50 2 -5 11 217.18 6.40 2 -5 11 207.58 5.40 -3 5 -11 6.70 1.40 -3 5 -11 7.50 2.40 -3 5 -11 6.30 1.40 3 -5 11 5.90 1.40 3 -5 11 8.30 1.50 3 -5 11 7.70 1.60 3 -5 11 8.80 0.80 -4 5 -11 -0.90 1.20 -4 5 -11 -0.30 1.10 -4 5 -11 -0.20 1.70 4 -5 11 1.80 1.50 4 -5 11 1.20 1.50 4 -5 11 -1.10 1.20 -5 5 -11 0.70 1.30 -5 5 -11 -0.40 1.40 5 -5 11 1.60 1.40 5 -5 11 -0.90 1.20 5 -5 11 1.30 1.50 -6 5 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1.60 3 4 -11 10.50 1.70 3 4 -11 8.60 1.60 3 4 -11 5.70 1.60 -3 -4 11 8.90 1.70 -3 -4 11 6.10 1.80 -3 -4 11 8.80 1.70 2 4 -11 -0.20 1.30 2 4 -11 1.90 1.30 2 4 -11 0.70 1.30 2 4 -11 2.30 1.30 -2 -4 11 3.50 1.50 -2 -4 11 0.20 1.30 -2 -4 11 4.10 1.50 1 4 -11 301.37 8.20 1 4 -11 308.57 7.20 1 4 -11 310.57 7.40 1 4 -11 310.27 7.70 -1 -4 11 307.97 8.00 -1 -4 11 323.67 7.30 -1 -4 11 315.27 7.30 0 4 -11 70.39 3.50 0 4 -11 68.09 3.20 0 4 -11 65.99 2.80 0 4 -11 69.89 2.90 0 -4 11 67.19 2.90 0 -4 11 68.69 2.90 0 -4 11 68.39 3.60 -1 4 -11 0.50 1.10 -1 4 -11 0.60 1.30 -1 4 -11 -0.90 1.10 -1 4 -11 0.20 1.30 1 -4 11 -0.40 1.10 1 -4 11 0.70 1.20 1 -4 11 0.30 1.10 -2 4 -11 1.10 1.20 -2 4 -11 1.60 1.30 -2 4 -11 1.70 1.20 -2 4 -11 0.40 1.40 2 -4 11 1.90 1.20 2 -4 11 0.50 1.30 2 -4 11 0.60 1.10 -3 4 -11 56.09 3.20 -3 4 -11 53.89 2.70 -3 4 -11 56.99 2.70 3 -4 11 59.79 3.30 3 -4 11 51.59 2.70 3 -4 11 54.69 2.70 -4 4 -11 1.50 1.20 -4 4 -11 2.10 1.30 4 -4 11 1.80 1.40 4 -4 11 1.60 1.30 4 -4 11 1.50 1.30 -5 4 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12 205.98 4.30 -4 -4 -12 28.70 2.30 -4 -4 -12 27.20 2.50 4 4 12 28.00 2.60 4 4 12 31.30 1.20 4 4 12 28.60 2.40 -5 -4 -12 13.30 1.80 -5 -4 -12 13.80 1.80 5 4 12 12.10 1.70 5 4 12 14.00 1.80 5 4 12 11.10 1.90 5 4 12 11.60 1.10 -6 -4 -12 1.50 1.50 -6 -4 -12 -0.50 1.60 6 4 12 -0.50 0.70 6 4 12 1.60 2.00 6 4 12 0.10 1.20 6 4 12 -2.20 1.50 -7 -4 -12 4.00 1.70 -7 -4 -12 5.20 1.70 7 4 12 6.30 2.10 7 4 12 5.30 1.10 7 4 12 4.00 0.90 7 4 12 4.20 1.60 -8 -4 -12 27.60 2.60 -8 -4 -12 18.20 2.10 8 4 12 20.20 2.30 8 4 12 20.80 2.70 8 4 12 24.70 2.10 8 4 12 25.10 2.40 -9 -4 -12 5.70 1.90 9 4 12 3.10 2.00 9 4 12 3.30 1.30 9 4 12 6.20 2.00 -10 -4 -12 11.60 2.50 -10 -4 -12 10.70 2.50 10 4 12 11.30 2.30 10 4 12 9.00 1.70 10 4 12 11.80 2.20 7 -5 -12 7.80 2.20 7 -5 -12 4.80 2.20 -7 5 12 4.50 1.90 -7 5 12 5.70 2.20 -7 5 12 5.70 1.90 6 -5 -12 10.40 2.30 6 -5 -12 10.30 2.80 6 -5 -12 8.40 1.90 -6 5 12 10.90 1.90 -6 5 12 7.50 2.20 -6 5 12 7.50 1.80 5 -5 -12 -2.70 1.50 5 -5 -12 1.00 1.70 5 -5 -12 -1.90 1.60 -5 5 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-5 -20 15.70 2.10 1 5 20 12.00 2.00 1 5 20 21.80 3.70 -2 -5 -20 2.90 1.70 -2 -5 -20 0.60 2.00 2 5 20 1.40 1.70 2 5 20 4.10 2.30 2 5 20 1.10 1.90 -3 -5 -20 2.20 2.10 -3 -5 -20 -1.00 1.80 3 5 20 -1.00 1.90 3 5 20 3.60 1.80 3 5 20 3.20 1.80 -4 -5 -20 10.00 2.20 4 5 20 9.00 2.20 4 5 20 5.20 1.90 -1 2 -21 17.30 2.50 -1 2 -21 13.40 2.30 -1 2 -21 6.60 3.60 -1 2 -21 25.40 3.90 1 -2 21 18.80 2.50 1 -2 21 22.10 3.10 1 -2 21 11.50 2.50 -2 2 -21 -2.10 2.20 -2 2 -21 0.80 1.90 -2 2 -21 0.20 1.80 -2 2 -21 -1.30 2.00 2 -2 21 -2.90 1.90 2 -2 21 -0.30 1.80 2 -2 21 1.50 2.20 -3 2 -21 0.50 2.00 -3 2 -21 4.40 2.90 -3 2 -21 1.90 2.10 3 -2 21 1.30 1.90 3 -2 21 -0.80 2.10 3 -2 21 -2.10 1.90 0 1 -21 2.30 2.00 0 1 -21 3.10 2.40 0 1 -21 1.70 1.70 0 -1 21 4.70 2.20 0 -1 21 1.00 2.30 0 -1 21 -0.20 1.90 -1 1 -21 4.80 2.20 -1 1 -21 1.40 1.80 -1 1 -21 0.30 2.10 -1 1 -21 1.60 1.80 1 -1 21 3.50 2.00 1 -1 21 6.40 2.30 1 -1 21 2.90 2.10 -2 1 -21 3.10 2.00 -2 1 -21 -0.30 2.20 -2 1 -21 1.00 1.70 -2 1 -21 -3.30 1.70 2 -1 21 2.70 2.10 2 -1 21 1.30 2.20 -3 1 -21 3.60 1.90 -3 1 -21 4.00 2.40 3 -1 21 1.00 1.80 3 -1 21 4.50 2.40 3 -1 21 3.60 1.90 -4 1 -21 2.60 2.50 -4 1 -21 -0.20 2.20 4 -1 21 -0.50 2.20 4 -1 21 5.20 2.10 4 -1 21 -1.90 1.70 0 0 -21 6.00 2.40 0 0 -21 4.00 2.00 0 0 -21 3.70 1.90 0 0 21 4.70 2.00 0 0 21 4.20 2.40 -1 0 -21 13.30 2.10 -1 0 -21 8.20 2.40 -1 0 -21 10.90 2.10 1 0 21 8.40 2.30 1 0 21 9.80 2.00 1 0 21 8.80 2.50 -2 0 -21 -0.20 1.80 -2 0 -21 3.40 1.70 -2 0 -21 0.20 2.10 2 0 21 -2.80 1.60 2 0 21 0.10 2.10 2 0 21 -0.20 1.80 -3 0 -21 5.70 2.40 -3 0 -21 6.00 3.60 3 0 21 4.10 2.40 3 0 21 2.70 2.30 -4 0 -21 3.40 3.00 -4 0 -21 -2.50 2.20 4 0 21 0.90 2.20 4 0 21 -0.80 0.90 4 0 21 -0.70 1.60 5 0 21 5.40 1.30 0 -1 -21 1.90 1.50 0 -1 -21 1.40 1.90 0 -1 -21 2.80 2.20 0 -1 -21 3.00 1.80 0 1 21 5.40 2.30 0 1 21 2.20 1.90 0 1 21 3.70 2.00 -1 -1 -21 0.50 2.40 -1 -1 -21 1.80 1.70 -1 -1 -21 -0.40 1.70 -1 -1 -21 2.90 1.70 1 1 21 0.10 2.00 1 1 21 4.10 1.90 1 1 21 -0.80 1.60 -2 -1 -21 2.30 2.00 -2 -1 -21 7.30 3.90 -2 -1 -21 0.40 1.50 2 1 21 -1.70 1.50 2 1 21 -0.30 1.80 2 1 21 3.10 2.10 -3 -1 -21 3.20 2.20 -3 -1 -21 4.30 2.70 3 1 21 0.90 2.20 3 1 21 3.30 2.00 -4 -1 -21 9.90 2.50 -4 -1 -21 7.40 2.10 4 1 21 5.10 2.00 4 1 21 3.60 2.30 4 1 21 3.20 1.30 4 1 21 3.60 1.60 -5 -1 -21 -2.40 1.90 -5 -1 -21 -0.70 2.20 5 1 21 -3.10 1.40 5 1 21 2.10 2.30 5 1 21 0.30 1.30 5 1 21 -0.80 2.50 0 -2 -21 8.90 1.60 0 -2 -21 9.30 4.80 0 -2 -21 11.10 2.30 0 -2 -21 8.40 2.00 0 2 21 6.10 1.90 0 2 21 9.10 2.40 -1 -2 -21 -0.40 1.50 -1 -2 -21 -1.10 2.10 -1 -2 -21 0.50 1.90 1 2 21 0.60 2.00 1 2 21 4.30 2.00 1 2 21 -1.60 1.50 -2 -2 -21 0.20 2.20 -2 -2 -21 -2.60 1.80 -2 -2 -21 0.10 1.40 2 2 21 1.60 2.00 2 2 21 -0.80 1.50 2 2 21 -1.00 2.10 -3 -2 -21 6.80 2.10 -3 -2 -21 7.60 2.70 3 2 21 7.30 1.50 3 2 21 5.20 2.30 3 2 21 6.00 1.70 3 2 21 7.50 2.30 -4 -2 -21 1.60 1.80 4 2 21 -1.20 1.70 4 2 21 1.10 1.50 4 2 21 -0.90 1.30 4 2 21 1.30 2.20 -1 -3 -21 5.40 1.90 -1 -3 -21 5.40 1.60 -1 -3 -21 5.40 2.40 -2 -3 -21 -1.30 1.70 -2 -3 -21 2.20 2.30 2 3 21 0.60 1.80 2 3 21 1.10 1.40 -3 -3 -21 13.20 2.20 -3 -3 -21 21.10 2.90 3 3 21 16.30 2.30 3 3 21 12.90 2.30 3 3 21 14.80 1.80 -4 -3 -21 4.90 2.10 -4 -3 -21 0.00 2.30 4 3 21 1.70 1.40 4 3 21 2.00 1.60 4 3 21 1.00 2.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 42193 _shelx_res_file ; TITL umd2790g_a.res in P-1 umd2790g_a.res created by SHELXL-2018/3 at 22:19:24 on 21-Nov-2022 REM Old TITL umd2790g in P-1 REM SHELXT solution in P-1: R1 0.169, Rweak 0.006, Alpha 0.044 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C40 Cl2 N4 O2 rem colorless block CELL 0.71073 10.1895 10.9117 17.6887 86.798 79.34 87.587 ZERR 4 0.0009 0.0007 0.0014 0.003 0.003 0.003 LATT 1 SFAC C H Cl N O UNIT 80 100 4 8 4 EQIV $1 2-X,2-Y,1-Z EQIV $2 1-X,1-Y,-Z EQIV $3 2-X,1-Y,1-Z EQIV $4 1-X,-Y,-Z DFIX 0.87 0.01 N1 H1 N3 H3a DFIX 0.95 0.01 N2 H2a N2 H2b N4 H4b N4 H4a L.S. 10 PLAN 11 SIZE 0.2 0.27 0.3 TEMP 27 CONF HTAB C30 O2 HTAB N1 Cl1_$1 HTAB N3 Cl2_$2 HTAB N2 Cl1_$3 HTAB N4 Cl2_$4 HTAB N2 Cl1 HTAB N4 Cl2 BOND $H LIST 4 htab 2 fmap 2 acta MORE -1 OMIT -7 2 8 OMIT -8 5 2 OMIT 8 -6 1 OMIT 0 1 3 REM REM REM WGHT 0.045300 0.720400 FVAR 0.55941 CL1 3 0.923233 0.673001 0.446334 11.00000 0.07054 0.04640 = 0.05519 0.00211 -0.00807 0.00666 CL2 3 0.346338 0.140331 -0.047452 11.00000 0.07824 0.04649 = 0.05037 -0.00195 -0.01672 0.00892 O1 5 0.962456 0.755884 0.816827 11.00000 0.07138 0.04885 = 0.04611 0.00753 -0.02073 -0.00953 O2 5 0.582203 0.248051 0.287022 11.00000 0.07997 0.05132 = 0.05528 0.00251 -0.03175 -0.00161 N1 4 1.003897 1.055535 0.621395 11.00000 0.07218 0.04302 = 0.05512 0.00850 -0.01362 -0.00215 N2 4 0.880710 0.543118 0.610227 11.00000 0.04965 0.04165 = 0.04882 -0.00591 -0.00376 -0.00193 N3 4 0.552049 0.600811 0.136212 11.00000 0.07067 0.04276 = 0.05611 0.00198 -0.00769 -0.00326 N4 4 0.448951 0.071698 0.105854 11.00000 0.05469 0.04236 = 0.03720 -0.00748 -0.00723 -0.00072 C1 1 0.936349 0.959174 0.603963 11.00000 0.05859 0.05261 = 0.04537 -0.00105 -0.01100 0.00409 AFIX 43 H1A 2 0.902311 0.955148 0.558905 11.00000 -1.20000 AFIX 0 C2 1 1.038284 1.030707 0.691850 11.00000 0.05432 0.04062 = 0.05208 -0.00168 -0.00820 0.00012 C3 1 1.107921 1.102147 0.732828 11.00000 0.07279 0.04358 = 0.07159 -0.00154 -0.01787 -0.01104 AFIX 43 H3 2 1.138537 1.178820 0.713479 11.00000 -1.20000 AFIX 0 C4 1 1.129186 1.054690 0.802524 11.00000 0.08301 0.05439 = 0.07596 -0.01073 -0.03012 -0.01411 AFIX 43 H4 2 1.176174 1.099975 0.831038 11.00000 -1.20000 AFIX 0 C5 1 1.082508 0.939679 0.832724 11.00000 0.07824 0.05882 = 0.05578 -0.00063 -0.02791 -0.00725 AFIX 43 H5 2 1.098189 0.910655 0.880799 11.00000 -1.20000 AFIX 0 C6 1 1.013643 0.869239 0.791884 11.00000 0.05598 0.04299 = 0.04834 -0.00126 -0.01191 -0.00138 C7 1 0.990320 0.913811 0.719347 11.00000 0.04385 0.03798 = 0.04429 -0.00368 -0.00664 0.00111 C8 1 0.925127 0.869172 0.661339 11.00000 0.04237 0.04352 = 0.04213 -0.00530 -0.00598 0.00389 C9 1 0.854180 0.752852 0.659540 11.00000 0.04115 0.05053 = 0.05058 -0.01181 -0.00338 0.00043 AFIX 23 H9A 2 0.801952 0.761737 0.618827 11.00000 -1.20000 H9B 2 0.792351 0.740893 0.707906 11.00000 -1.20000 AFIX 0 C10 1 0.944590 0.638825 0.646800 11.00000 0.04917 0.04791 = 0.05555 -0.00585 -0.01270 -0.00033 AFIX 23 H10A 2 1.028450 0.660588 0.614039 11.00000 -1.20000 H10B 2 0.963891 0.606101 0.695828 11.00000 -1.20000 AFIX 0 C11 1 0.749894 0.495540 0.652334 11.00000 0.05358 0.05504 = 0.08343 -0.00871 0.00654 -0.00896 AFIX 13 H11 2 0.692227 0.565425 0.671627 11.00000 -1.20000 AFIX 0 C12 1 0.685988 0.433547 0.595254 11.00000 0.08520 0.12477 = 0.17059 -0.05237 -0.01443 -0.04359 AFIX 137 H12A 2 0.600112 0.405005 0.620140 11.00000 -1.50000 H12B 2 0.741760 0.365091 0.575636 11.00000 -1.50000 H12C 2 0.675264 0.490939 0.553517 11.00000 -1.50000 AFIX 0 C13 1 0.772291 0.413268 0.719309 11.00000 0.10147 0.11307 = 0.11610 0.04900 0.03560 0.00374 AFIX 137 H13A 2 0.688711 0.380818 0.745018 11.00000 -1.50000 H13B 2 0.809615 0.459136 0.754522 11.00000 -1.50000 H13C 2 0.832962 0.346907 0.701486 11.00000 -1.50000 AFIX 0 C14 1 0.988028 0.709155 0.890421 11.00000 0.09978 0.05934 = 0.05538 0.01050 -0.03267 -0.01211 AFIX 23 H14A 2 0.941757 0.760771 0.930509 11.00000 -1.20000 H14B 2 1.083012 0.710211 0.890900 11.00000 -1.20000 AFIX 0 C15 1 0.940779 0.580556 0.905570 11.00000 0.06614 0.04959 = 0.04531 0.00408 -0.01924 0.00319 C16 1 1.001471 0.487254 0.862107 11.00000 0.10311 0.07444 = 0.05403 -0.00449 -0.00072 0.01221 AFIX 43 H16 2 1.069007 0.504242 0.820162 11.00000 -1.20000 AFIX 0 C17 1 0.962766 0.367899 0.880320 11.00000 0.15767 0.06096 = 0.07980 -0.02216 -0.03548 0.02652 AFIX 43 H17 2 1.003586 0.304756 0.850290 11.00000 -1.20000 AFIX 0 C18 1 0.864055 0.342195 0.942724 11.00000 0.12523 0.05727 = 0.09158 0.01386 -0.05743 -0.02226 AFIX 43 H18 2 0.838464 0.261697 0.955274 11.00000 -1.20000 AFIX 0 C19 1 0.804249 0.434523 0.985837 11.00000 0.06160 0.08207 = 0.08064 0.02156 -0.02115 -0.01218 AFIX 43 H19 2 0.737486 0.417467 1.028176 11.00000 -1.20000 AFIX 0 C20 1 0.841967 0.553453 0.967185 11.00000 0.06044 0.06273 = 0.05765 0.00203 -0.01457 0.01245 AFIX 43 H20 2 0.799728 0.616432 0.996864 11.00000 -1.20000 AFIX 0 C21 1 0.487394 0.508047 0.111447 11.00000 0.06308 0.05414 = 0.04530 -0.00353 -0.01240 0.00543 AFIX 43 H21 2 0.443699 0.515233 0.069597 11.00000 -1.20000 AFIX 0 C22 1 0.604183 0.557941 0.198878 11.00000 0.04723 0.04750 = 0.05034 -0.00708 -0.00068 -0.00333 C23 1 0.675265 0.619557 0.244228 11.00000 0.06230 0.05692 = 0.07184 -0.01598 -0.00566 -0.01650 AFIX 43 H23 2 0.695515 0.701766 0.233628 11.00000 -1.20000 AFIX 0 C24 1 0.713809 0.554695 0.304568 11.00000 0.06369 0.08169 = 0.07009 -0.02324 -0.01573 -0.02031 AFIX 43 H24 2 0.760723 0.593864 0.336106 11.00000 -1.20000 AFIX 0 C25 1 0.685113 0.430675 0.320777 11.00000 0.06007 0.07854 = 0.05538 -0.00643 -0.02133 -0.00758 AFIX 43 H25 2 0.713598 0.389018 0.362452 11.00000 -1.20000 AFIX 0 C26 1 0.615110 0.369542 0.275685 11.00000 0.04922 0.05246 = 0.04679 -0.00613 -0.01001 -0.00264 C27 1 0.571516 0.433561 0.213265 11.00000 0.04166 0.04414 = 0.04044 -0.00803 -0.00434 -0.00105 C28 1 0.495602 0.403451 0.156416 11.00000 0.04748 0.04470 = 0.03885 -0.00729 -0.00600 0.00244 C29 1 0.428408 0.286748 0.148695 11.00000 0.04840 0.05084 = 0.04668 -0.01082 -0.00912 0.00005 AFIX 23 H29A 2 0.367867 0.302283 0.112632 11.00000 -1.20000 H29B 2 0.375132 0.262903 0.198241 11.00000 -1.20000 AFIX 0 C30 1 0.522219 0.180763 0.121753 11.00000 0.04841 0.04829 = 0.04361 -0.01053 -0.00455 -0.00321 AFIX 23 H30A 2 0.582922 0.206845 0.075240 11.00000 -1.20000 H30B 2 0.575094 0.157353 0.160871 11.00000 -1.20000 AFIX 0 C31 1 0.342742 0.021168 0.168869 11.00000 0.05969 0.05272 = 0.04888 -0.00479 0.00005 -0.00844 AFIX 13 H31 2 0.275339 0.086446 0.183618 11.00000 -1.20000 AFIX 0 C32 1 0.401250 -0.020515 0.238221 11.00000 0.10803 0.09506 = 0.04914 0.01367 -0.00868 -0.01901 AFIX 137 H32A 2 0.436550 0.048546 0.258190 11.00000 -1.50000 H32B 2 0.471660 -0.080659 0.223843 11.00000 -1.50000 H32C 2 0.332963 -0.056095 0.276988 11.00000 -1.50000 AFIX 0 C33 1 0.277086 -0.081237 0.136614 11.00000 0.07667 0.06388 = 0.08508 -0.00751 -0.00642 -0.02140 AFIX 137 H33A 2 0.204093 -0.111016 0.174616 11.00000 -1.50000 H33B 2 0.341352 -0.147018 0.123327 11.00000 -1.50000 H33C 2 0.244225 -0.050541 0.091469 11.00000 -1.50000 AFIX 0 C34 1 0.655431 0.170547 0.333969 11.00000 0.07641 0.06591 = 0.05618 -0.00273 -0.02175 0.01945 AFIX 23 H34A 2 0.747301 0.196068 0.324815 11.00000 -1.20000 H34B 2 0.655949 0.086874 0.318031 11.00000 -1.20000 AFIX 0 C35 1 0.600640 0.172153 0.418814 11.00000 0.05402 0.04764 = 0.05552 -0.00049 -0.01868 0.00549 C36 1 0.476141 0.216494 0.448418 11.00000 0.05936 0.12797 = 0.07285 0.00594 -0.02340 0.02444 AFIX 43 H36 2 0.422403 0.251246 0.415227 11.00000 -1.20000 AFIX 0 C37 1 0.427825 0.210987 0.526782 11.00000 0.05989 0.13398 = 0.08199 0.00251 0.00192 0.01773 AFIX 43 H37 2 0.342522 0.242462 0.545606 11.00000 -1.20000 AFIX 0 C38 1 0.502630 0.160769 0.575896 11.00000 0.08927 0.07951 = 0.05915 0.00614 -0.00583 0.00413 AFIX 43 H38 2 0.469508 0.155762 0.628582 11.00000 -1.20000 AFIX 0 C39 1 0.626284 0.117804 0.547668 11.00000 0.10667 0.12784 = 0.05748 0.00582 -0.02483 0.04611 AFIX 43 H39 2 0.679341 0.083373 0.581328 11.00000 -1.20000 AFIX 0 C40 1 0.675941 0.123804 0.469794 11.00000 0.07571 0.11203 = 0.06170 -0.00265 -0.01925 0.04405 AFIX 43 H40 2 0.762384 0.094324 0.451731 11.00000 -1.20000 AFIX 0 H1 2 1.014609 1.124337 0.594220 11.00000 0.06659 H2A 2 0.944331 0.477813 0.600627 11.00000 0.06267 H2B 2 0.867755 0.578873 0.562151 11.00000 0.06366 H3A 2 0.566545 0.670662 0.111259 11.00000 0.08225 H4A 2 0.513411 0.008446 0.091953 11.00000 0.05326 H4B 2 0.408595 0.090111 0.062643 11.00000 0.06075 HKLF 4 REM umd2790g_a.res in P-1 REM wR2 = 0.1133, GooF = S = 1.015, Restrained GooF = 1.015 for all data REM R1 = 0.0406 for 5589 Fo > 4sig(Fo) and 0.0584 for all 7362 data REM 461 parameters refined using 6 restraints END WGHT 0.0453 0.7204 REM Instructions for potential hydrogen bonds HTAB C30 O2 HTAB N1 Cl1_$1 HTAB N2 Cl1_$3 HTAB N2 Cl1 HTAB N3 Cl2_$2 HTAB N4 Cl2_$4 HTAB N4 Cl2 REM Highest difference peak 0.263, deepest hole -0.289, 1-sigma level 0.033 Q1 1 0.9947 0.6862 0.4700 11.00000 0.05 0.26 Q2 1 0.9281 0.8862 0.7055 11.00000 0.05 0.17 Q3 1 0.8642 0.3754 0.7223 11.00000 0.05 0.16 Q4 1 0.5143 0.4120 0.1945 11.00000 0.05 0.16 Q5 1 0.5002 0.1408 0.4293 11.00000 0.05 0.15 Q6 1 1.0568 0.6606 0.8577 11.00000 0.05 0.15 Q7 1 0.9810 0.9771 0.7186 11.00000 0.05 0.15 Q8 1 0.4202 0.1616 -0.0311 11.00000 0.05 0.15 Q9 1 0.6536 0.3628 0.7193 11.00000 0.05 0.14 Q10 1 0.5999 0.3964 0.2328 11.00000 0.05 0.14 Q11 1 1.0938 0.6765 0.8612 11.00000 0.05 0.14 ; _shelx_res_checksum 97886 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl1 0.92323(5) 0.67300(4) 0.44633(3) 0.05824(14) Uani d 1 . . Cl Cl2 0.34634(5) 0.14033(4) -0.04745(3) 0.05806(14) Uani d 1 . . O O1 0.96246(14) 0.75588(11) 0.81683(7) 0.0543(3) Uani d 1 . . O O2 0.58220(15) 0.24805(12) 0.28702(8) 0.0599(4) Uani d 1 . . N N1 1.00390(18) 1.05554(15) 0.62139(10) 0.0569(4) Uani d 1 . . N N2 0.88071(16) 0.54312(14) 0.61023(9) 0.0472(4) Uani d 1 . . N N3 0.55205(18) 0.60081(15) 0.13621(10) 0.0571(4) Uani d 1 . . N N4 0.44895(16) 0.07170(13) 0.10585(8) 0.0447(3) Uani d 1 . . C C1 0.9363(2) 0.95917(17) 0.60396(11) 0.0522(4) Uani d 1 . . H H1A 0.902311 0.955148 0.558905 0.063 Uiso calc 1 . . C C2 1.03828(19) 1.03071(16) 0.69185(11) 0.0493(4) Uani d 1 . . C C3 1.1079(2) 1.10215(18) 0.73283(13) 0.0618(5) Uani d 1 . . H H3 1.138537 1.178820 0.713479 0.074 Uiso calc 1 . . C C4 1.1292(2) 1.05469(19) 0.80252(13) 0.0685(6) Uani d 1 . . H H4 1.176174 1.099975 0.831038 0.082 Uiso calc 1 . . C C5 1.0825(2) 0.93968(19) 0.83272(12) 0.0622(5) Uani d 1 . . H H5 1.098189 0.910655 0.880799 0.075 Uiso calc 1 . . C C6 1.01364(19) 0.86924(16) 0.79188(10) 0.0488(4) Uani d 1 . . C C7 0.99032(17) 0.91381(15) 0.71935(10) 0.0422(4) Uani d 1 . . C C8 0.92513(17) 0.86917(15) 0.66134(10) 0.0429(4) Uani d 1 . . C C9 0.85418(17) 0.75285(16) 0.65954(11) 0.0478(4) Uani d 1 . . H H9A 0.801952 0.761737 0.618827 0.057 Uiso calc 1 . . H H9B 0.792351 0.740893 0.707906 0.057 Uiso calc 1 . . C C10 0.94459(19) 0.63883(16) 0.64680(11) 0.0504(4) Uani d 1 . . H H10A 1.028450 0.660588 0.614039 0.060 Uiso calc 1 . . H H10B 0.963891 0.606101 0.695828 0.060 Uiso calc 1 . . C C11 0.7499(2) 0.4955(2) 0.65233(14) 0.0660(6) Uani d 1 . . H H11 0.692227 0.565425 0.671627 0.079 Uiso calc 1 . . C C12 0.6860(3) 0.4335(3) 0.5953(2) 0.1251(13) Uani d 1 . . H H12A 0.600112 0.405005 0.620140 0.188 Uiso calc 1 . . H H12B 0.741760 0.365091 0.575636 0.188 Uiso calc 1 . . H H12C 0.675264 0.490939 0.553517 0.188 Uiso calc 1 . . C C13 0.7723(3) 0.4133(3) 0.71931(19) 0.1196(12) Uani d 1 . . H H13A 0.688711 0.380818 0.745018 0.179 Uiso calc 1 . . H H13B 0.809615 0.459136 0.754522 0.179 Uiso calc 1 . . H H13C 0.832962 0.346907 0.701486 0.179 Uiso calc 1 . . C C14 0.9880(3) 0.70915(19) 0.89042(12) 0.0694(6) Uani d 1 . . H H14A 0.941757 0.760771 0.930509 0.083 Uiso calc 1 . . H H14B 1.083012 0.710211 0.890900 0.083 Uiso calc 1 . . C C15 0.9408(2) 0.58056(17) 0.90557(11) 0.0529(5) Uani d 1 . . C C16 1.0015(3) 0.4873(2) 0.86211(13) 0.0793(7) Uani d 1 . . H H16 1.069007 0.504242 0.820162 0.095 Uiso calc 1 . . C C17 0.9628(4) 0.3679(2) 0.88032(17) 0.0979(10) Uani d 1 . . H H17 1.003586 0.304756 0.850290 0.117 Uiso calc 1 . . C C18 0.8641(3) 0.3422(2) 0.94272(17) 0.0867(8) Uani d 1 . . H H18 0.838464 0.261697 0.955274 0.104 Uiso calc 1 . . C C19 0.8042(2) 0.4345(2) 0.98584(15) 0.0744(7) Uani d 1 . . H H19 0.737486 0.417467 1.028176 0.089 Uiso calc 1 . . C C20 0.8420(2) 0.55345(19) 0.96718(12) 0.0604(5) Uani d 1 . . H H20 0.799728 0.616432 0.996864 0.072 Uiso calc 1 . . C C21 0.4874(2) 0.50805(17) 0.11145(11) 0.0540(5) Uani d 1 . . H H21 0.443699 0.515233 0.069597 0.065 Uiso calc 1 . . C C22 0.60418(18) 0.55794(16) 0.19888(11) 0.0492(4) Uani d 1 . . C C23 0.6753(2) 0.6196(2) 0.24423(13) 0.0636(5) Uani d 1 . . H H23 0.695515 0.701766 0.233628 0.076 Uiso calc 1 . . C C24 0.7138(2) 0.5547(2) 0.30457(14) 0.0701(6) Uani d 1 . . H H24 0.760723 0.593864 0.336106 0.084 Uiso calc 1 . . C C25 0.6851(2) 0.4307(2) 0.32078(12) 0.0630(5) Uani d 1 . . H H25 0.713598 0.389018 0.362452 0.076 Uiso calc 1 . . C C26 0.61511(19) 0.36954(17) 0.27569(10) 0.0492(4) Uani d 1 . . C C27 0.57152(17) 0.43356(15) 0.21327(9) 0.0423(4) Uani d 1 . . C C28 0.49560(18) 0.40345(15) 0.15642(9) 0.0438(4) Uani d 1 . . C C29 0.42841(18) 0.28675(16) 0.14869(10) 0.0483(4) Uani d 1 . . H H29A 0.367867 0.302283 0.112632 0.058 Uiso calc 1 . . H H29B 0.375132 0.262903 0.198241 0.058 Uiso calc 1 . . C C30 0.52222(18) 0.18076(16) 0.12175(10) 0.0469(4) Uani d 1 . . H H30A 0.582922 0.206845 0.075240 0.056 Uiso calc 1 . . H H30B 0.575094 0.157353 0.160871 0.056 Uiso calc 1 . . C C31 0.3427(2) 0.02117(18) 0.16887(11) 0.0548(5) Uani d 1 . . H H31 0.275339 0.086446 0.183618 0.066 Uiso calc 1 . . C C32 0.4012(3) -0.0205(2) 0.23822(13) 0.0850(8) Uani d 1 . . H H32A 0.436550 0.048546 0.258190 0.128 Uiso calc 1 . . H H32B 0.471660 -0.080659 0.223843 0.128 Uiso calc 1 . . H H32C 0.332963 -0.056095 0.276988 0.128 Uiso calc 1 . . C C33 0.2771(2) -0.0812(2) 0.13661(15) 0.0756(7) Uani d 1 . . H H33A 0.204093 -0.111016 0.174616 0.113 Uiso calc 1 . . H H33B 0.341352 -0.147018 0.123327 0.113 Uiso calc 1 . . H H33C 0.244225 -0.050541 0.091469 0.113 Uiso calc 1 . . C C34 0.6554(2) 0.1705(2) 0.33397(12) 0.0656(6) Uani d 1 . . H H34A 0.747301 0.196068 0.324815 0.079 Uiso calc 1 . . H H34B 0.655949 0.086874 0.318031 0.079 Uiso calc 1 . . C C35 0.60064(19) 0.17215(17) 0.41881(11) 0.0516(4) Uani d 1 . . C C36 0.4761(2) 0.2165(3) 0.44842(15) 0.0865(8) Uani d 1 . . H H36 0.422403 0.251246 0.415227 0.104 Uiso calc 1 . . C C37 0.4278(3) 0.2110(3) 0.52678(16) 0.0948(9) Uani d 1 . . H H37 0.342522 0.242462 0.545606 0.114 Uiso calc 1 . . C C38 0.5026(3) 0.1608(2) 0.57590(14) 0.0775(7) Uani d 1 . . H H38 0.469508 0.155762 0.628582 0.093 Uiso calc 1 . . C C39 0.6263(3) 0.1178(3) 0.54767(14) 0.0979(9) Uani d 1 . . H H39 0.679341 0.083373 0.581328 0.117 Uiso calc 1 . . C C40 0.6759(3) 0.1238(3) 0.46979(13) 0.0837(8) Uani d 1 . . H H40 0.762384 0.094324 0.451731 0.100 Uiso calc 1 . . H H1 1.015(2) 1.1243(12) 0.5942(11) 0.067(6) Uiso d 1 . . H H2A 0.9443(16) 0.4778(14) 0.6006(11) 0.063(6) Uiso d 1 . . H H2B 0.868(2) 0.5789(17) 0.5622(7) 0.064(6) Uiso d 1 . . H H3A 0.567(2) 0.6707(13) 0.1113(12) 0.082(8) Uiso d 1 . . H H4A 0.5134(15) 0.0084(13) 0.0920(10) 0.053(5) Uiso d 1 . . H H4B 0.4086(19) 0.0901(18) 0.0626(8) 0.061(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.0705(3) 0.0464(3) 0.0552(3) 0.0067(2) -0.0081(2) 0.0021(2) Cl2 0.0782(4) 0.0465(3) 0.0504(3) 0.0089(2) -0.0167(2) -0.00195(19) O1 0.0714(9) 0.0488(7) 0.0461(7) -0.0095(6) -0.0207(6) 0.0075(5) O2 0.0800(10) 0.0513(8) 0.0553(8) -0.0016(7) -0.0317(7) 0.0025(6) N1 0.0722(11) 0.0430(9) 0.0551(10) -0.0021(8) -0.0136(8) 0.0085(7) N2 0.0496(9) 0.0416(8) 0.0488(9) -0.0019(7) -0.0038(7) -0.0059(7) N3 0.0707(11) 0.0428(9) 0.0561(10) -0.0033(8) -0.0077(8) 0.0020(7) N4 0.0547(9) 0.0424(8) 0.0372(8) -0.0007(7) -0.0072(7) -0.0075(6) C1 0.0586(12) 0.0526(11) 0.0454(10) 0.0041(9) -0.0110(9) -0.0011(8) C2 0.0543(11) 0.0406(9) 0.0521(10) 0.0001(8) -0.0082(8) -0.0017(8) C3 0.0728(14) 0.0436(11) 0.0716(13) -0.0110(9) -0.0179(11) -0.0015(9) C4 0.0830(16) 0.0544(12) 0.0760(15) -0.0141(11) -0.0301(12) -0.0107(10) C5 0.0782(15) 0.0588(12) 0.0558(12) -0.0073(10) -0.0279(11) -0.0006(9) C6 0.0560(11) 0.0430(10) 0.0483(10) -0.0014(8) -0.0119(8) -0.0013(8) C7 0.0439(9) 0.0380(9) 0.0443(9) 0.0011(7) -0.0066(7) -0.0037(7) C8 0.0424(9) 0.0435(9) 0.0421(9) 0.0039(7) -0.0060(7) -0.0053(7) C9 0.0411(10) 0.0505(10) 0.0506(10) 0.0004(8) -0.0034(8) -0.0118(8) C10 0.0492(11) 0.0479(10) 0.0556(11) -0.0003(8) -0.0127(8) -0.0059(8) C11 0.0536(12) 0.0550(12) 0.0834(15) -0.0090(9) 0.0065(11) -0.0087(10) C12 0.085(2) 0.125(3) 0.171(3) -0.0436(19) -0.014(2) -0.052(2) C13 0.101(2) 0.113(2) 0.116(2) 0.0037(18) 0.0356(19) 0.049(2) C14 0.0998(18) 0.0593(13) 0.0554(12) -0.0121(12) -0.0327(12) 0.0105(10) C15 0.0661(13) 0.0496(11) 0.0453(10) 0.0032(9) -0.0192(9) 0.0041(8) C16 0.103(2) 0.0744(16) 0.0540(13) 0.0122(13) -0.0007(12) -0.0045(11) C17 0.158(3) 0.0610(16) 0.0798(18) 0.0265(17) -0.0355(19) -0.0222(13) C18 0.125(2) 0.0573(15) 0.0916(19) -0.0223(15) -0.0574(18) 0.0139(13) C19 0.0616(14) 0.0821(17) 0.0806(16) -0.0122(12) -0.0211(12) 0.0216(13) C20 0.0604(13) 0.0627(13) 0.0576(12) 0.0125(10) -0.0146(10) 0.0020(9) C21 0.0631(12) 0.0541(11) 0.0453(10) 0.0054(9) -0.0124(9) -0.0035(8) C22 0.0472(10) 0.0475(10) 0.0503(10) -0.0033(8) -0.0007(8) -0.0071(8) C23 0.0623(13) 0.0569(12) 0.0718(14) -0.0165(10) -0.0057(11) -0.0160(10) C24 0.0637(14) 0.0817(16) 0.0701(14) -0.0203(12) -0.0157(11) -0.0232(12) C25 0.0601(13) 0.0785(15) 0.0554(12) -0.0076(11) -0.0213(10) -0.0064(10) C26 0.0492(11) 0.0525(11) 0.0468(10) -0.0026(8) -0.0100(8) -0.0061(8) C27 0.0417(9) 0.0441(9) 0.0404(9) -0.0010(7) -0.0043(7) -0.0080(7) C28 0.0475(10) 0.0447(9) 0.0389(9) 0.0024(7) -0.0060(7) -0.0073(7) C29 0.0484(10) 0.0508(10) 0.0467(10) 0.0001(8) -0.0091(8) -0.0108(8) C30 0.0484(10) 0.0483(10) 0.0436(9) -0.0032(8) -0.0046(8) -0.0105(7) C31 0.0597(12) 0.0527(11) 0.0489(10) -0.0084(9) 0.0001(9) -0.0048(8) C32 0.108(2) 0.0951(18) 0.0491(12) -0.0190(15) -0.0087(13) 0.0137(12) C33 0.0767(16) 0.0639(14) 0.0851(16) -0.0214(12) -0.0064(13) -0.0075(12) C34 0.0764(15) 0.0659(13) 0.0562(12) 0.0195(11) -0.0217(11) -0.0027(10) C35 0.0540(11) 0.0476(10) 0.0555(11) 0.0055(8) -0.0187(9) -0.0005(8) C36 0.0594(14) 0.128(2) 0.0729(16) 0.0244(14) -0.0234(12) 0.0059(15) C37 0.0599(15) 0.134(3) 0.0820(18) 0.0177(15) 0.0019(13) 0.0025(17) C38 0.0893(18) 0.0795(16) 0.0592(13) 0.0041(13) -0.0058(13) 0.0061(11) C39 0.107(2) 0.128(2) 0.0575(14) 0.0461(19) -0.0248(14) 0.0058(14) C40 0.0757(16) 0.112(2) 0.0617(14) 0.0441(14) -0.0193(12) -0.0026(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 O1 C14 . . 115.71(14) ? C26 O2 C34 . . 117.54(16) ? C1 N1 C2 . . 108.70(15) ? C1 N1 H1 . . 124.7(15) ? C2 N1 H1 . . 126.2(15) ? C10 N2 C11 . . 117.90(15) ? C10 N2 H2A . . 106.6(13) ? C10 N2 H2B . . 105.5(13) ? C11 N2 H2A . . 110.2(13) ? C11 N2 H2B . . 108.4(13) ? H2A N2 H2B . . 107.8(18) ? C21 N3 C22 . . 108.79(15) ? C21 N3 H3A . . 123.8(17) ? C22 N3 H3A . . 126.8(17) ? C30 N4 C31 . . 118.11(13) ? C30 N4 H4A . . 107.1(12) ? C30 N4 H4B . . 109.6(12) ? C31 N4 H4A . . 108.1(12) ? C31 N4 H4B . . 107.0(13) ? H4A N4 H4B . . 106.4(17) ? N1 C1 H1A . . 124.5 ? N1 C1 C8 . . 111.04(17) ? C8 C1 H1A . . 124.5 ? N1 C2 C3 . . 129.08(18) ? N1 C2 C7 . . 107.80(16) ? C3 C2 C7 . . 123.13(18) ? C2 C3 H3 . . 121.5 ? C4 C3 C2 . . 116.96(18) ? C4 C3 H3 . . 121.5 ? C3 C4 H4 . . 118.9 ? C3 C4 C5 . . 122.12(19) ? C5 C4 H4 . . 118.9 ? C4 C5 H5 . . 119.7 ? C6 C5 C4 . . 120.69(19) ? C6 C5 H5 . . 119.7 ? O1 C6 C7 . . 115.58(15) ? C5 C6 O1 . . 125.13(17) ? C5 C6 C7 . . 119.28(17) ? C2 C7 C8 . . 106.75(15) ? C6 C7 C2 . . 117.81(16) ? C6 C7 C8 . . 135.44(16) ? C1 C8 C7 . . 105.72(16) ? C1 C8 C9 . . 123.63(17) ? C7 C8 C9 . . 130.62(16) ? C8 C9 H9A . . 108.6 ? C8 C9 H9B . . 108.6 ? C8 C9 C10 . . 114.85(15) ? H9A C9 H9B . . 107.5 ? C10 C9 H9A . . 108.6 ? C10 C9 H9B . . 108.6 ? N2 C10 C9 . . 111.09(15) ? N2 C10 H10A . . 109.4 ? N2 C10 H10B . . 109.4 ? C9 C10 H10A . . 109.4 ? C9 C10 H10B . . 109.4 ? H10A C10 H10B . . 108.0 ? N2 C11 H11 . . 108.6 ? N2 C11 C12 . . 107.6(2) ? C12 C11 H11 . . 108.6 ? C13 C11 N2 . . 109.8(2) ? C13 C11 H11 . . 108.6 ? C13 C11 C12 . . 113.6(3) ? C11 C12 H12A . . 109.5 ? C11 C12 H12B . . 109.5 ? C11 C12 H12C . . 109.5 ? H12A C12 H12B . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C11 C13 H13A . . 109.5 ? C11 C13 H13B . . 109.5 ? C11 C13 H13C . . 109.5 ? H13A C13 H13B . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? O1 C14 H14A . . 109.7 ? O1 C14 H14B . . 109.8 ? O1 C14 C15 . . 109.60(16) ? H14A C14 H14B . . 108.2 ? C15 C14 H14A . . 109.7 ? C15 C14 H14B . . 109.8 ? C16 C15 C14 . . 121.0(2) ? C16 C15 C20 . . 119.0(2) ? C20 C15 C14 . . 119.89(19) ? C15 C16 H16 . . 119.9 ? C15 C16 C17 . . 120.2(2) ? C17 C16 H16 . . 119.9 ? C16 C17 H17 . . 119.9 ? C18 C17 C16 . . 120.1(2) ? C18 C17 H17 . . 119.9 ? C17 C18 H18 . . 120.2 ? C19 C18 C17 . . 119.7(2) ? C19 C18 H18 . . 120.2 ? C18 C19 H19 . . 119.9 ? C18 C19 C20 . . 120.1(2) ? C20 C19 H19 . . 119.9 ? C15 C20 C19 . . 120.9(2) ? C15 C20 H20 . . 119.5 ? C19 C20 H20 . . 119.5 ? N3 C21 H21 . . 124.6 ? C28 C21 N3 . . 110.75(17) ? C28 C21 H21 . . 124.6 ? N3 C22 C23 . . 129.43(18) ? N3 C22 C27 . . 107.60(16) ? C23 C22 C27 . . 122.96(19) ? C22 C23 H23 . . 121.4 ? C24 C23 C22 . . 117.2(2) ? C24 C23 H23 . . 121.4 ? C23 C24 H24 . . 119.0 ? C23 C24 C25 . . 122.00(19) ? C25 C24 H24 . . 119.0 ? C24 C25 H25 . . 119.6 ? C26 C25 C24 . . 120.8(2) ? C26 C25 H25 . . 119.6 ? O2 C26 C25 . . 124.99(18) ? O2 C26 C27 . . 115.83(15) ? C25 C26 C27 . . 119.19(18) ? C22 C27 C28 . . 107.04(15) ? C26 C27 C22 . . 117.85(16) ? C26 C27 C28 . . 135.10(16) ? C21 C28 C27 . . 105.81(16) ? C21 C28 C29 . . 124.87(17) ? C27 C28 C29 . . 129.18(16) ? C28 C29 H29A . . 108.6 ? C28 C29 H29B . . 108.6 ? C28 C29 C30 . . 114.73(15) ? H29A C29 H29B . . 107.6 ? C30 C29 H29A . . 108.6 ? C30 C29 H29B . . 108.6 ? N4 C30 C29 . . 112.12(15) ? N4 C30 H30A . . 109.2 ? N4 C30 H30B . . 109.2 ? C29 C30 H30A . . 109.2 ? C29 C30 H30B . . 109.2 ? H30A C30 H30B . . 107.9 ? N4 C31 H31 . . 108.5 ? N4 C31 C33 . . 107.79(16) ? C32 C31 N4 . . 110.56(18) ? C32 C31 H31 . . 108.5 ? C32 C31 C33 . . 112.83(19) ? C33 C31 H31 . . 108.5 ? C31 C32 H32A . . 109.5 ? C31 C32 H32B . . 109.5 ? C31 C32 H32C . . 109.5 ? H32A C32 H32B . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? C31 C33 H33A . . 109.5 ? C31 C33 H33B . . 109.5 ? C31 C33 H33C . . 109.5 ? H33A C33 H33B . . 109.5 ? H33A C33 H33C . . 109.5 ? H33B C33 H33C . . 109.5 ? O2 C34 H34A . . 108.7 ? O2 C34 H34B . . 108.7 ? O2 C34 C35 . . 114.29(17) ? H34A C34 H34B . . 107.6 ? C35 C34 H34A . . 108.7 ? C35 C34 H34B . . 108.7 ? C36 C35 C34 . . 123.43(19) ? C36 C35 C40 . . 117.1(2) ? C40 C35 C34 . . 119.48(19) ? C35 C36 H36 . . 119.3 ? C35 C36 C37 . . 121.4(2) ? C37 C36 H36 . . 119.3 ? C36 C37 H37 . . 119.7 ? C38 C37 C36 . . 120.6(2) ? C38 C37 H37 . . 119.7 ? C37 C38 H38 . . 120.6 ? C37 C38 C39 . . 118.7(2) ? C39 C38 H38 . . 120.6 ? C38 C39 H39 . . 119.4 ? C38 C39 C40 . . 121.1(2) ? C40 C39 H39 . . 119.4 ? C35 C40 C39 . . 121.0(2) ? C35 C40 H40 . . 119.5 ? C39 C40 H40 . . 119.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C6 . 1.380(2) ? O1 C14 . 1.436(2) ? O2 C26 . 1.376(2) ? O2 C34 . 1.435(2) ? N1 C1 . 1.360(3) ? N1 C2 . 1.366(2) ? N1 H1 . 0.868(9) ? N2 C10 . 1.490(2) ? N2 C11 . 1.500(2) ? N2 H2A . 0.944(9) ? N2 H2B . 0.945(9) ? N3 C21 . 1.365(3) ? N3 C22 . 1.367(2) ? N3 H3A . 0.863(10) ? N4 C30 . 1.498(2) ? N4 C31 . 1.501(2) ? N4 H4A . 0.943(9) ? N4 H4B . 0.941(9) ? C1 H1A . 0.9300 ? C1 C8 . 1.365(2) ? C2 C3 . 1.392(3) ? C2 C7 . 1.413(2) ? C3 H3 . 0.9300 ? C3 C4 . 1.361(3) ? C4 H4 . 0.9300 ? C4 C5 . 1.403(3) ? C5 H5 . 0.9300 ? C5 C6 . 1.378(3) ? C6 C7 . 1.405(2) ? C7 C8 . 1.438(2) ? C8 C9 . 1.492(2) ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C9 C10 . 1.518(2) ? C10 H10A . 0.9700 ? C10 H10B . 0.9700 ? C11 H11 . 0.9800 ? C11 C12 . 1.503(4) ? C11 C13 . 1.492(4) ? C12 H12A . 0.9600 ? C12 H12B . 0.9600 ? C12 H12C . 0.9600 ? C13 H13A . 0.9600 ? C13 H13B . 0.9600 ? C13 H13C . 0.9600 ? C14 H14A . 0.9700 ? C14 H14B . 0.9700 ? C14 C15 . 1.497(3) ? C15 C16 . 1.367(3) ? C15 C20 . 1.368(3) ? C16 H16 . 0.9300 ? C16 C17 . 1.380(4) ? C17 H17 . 0.9300 ? C17 C18 . 1.374(4) ? C18 H18 . 0.9300 ? C18 C19 . 1.353(4) ? C19 H19 . 0.9300 ? C19 C20 . 1.374(3) ? C20 H20 . 0.9300 ? C21 H21 . 0.9300 ? C21 C28 . 1.363(2) ? C22 C23 . 1.392(3) ? C22 C27 . 1.409(2) ? C23 H23 . 0.9300 ? C23 C24 . 1.357(3) ? C24 H24 . 0.9300 ? C24 C25 . 1.399(3) ? C25 H25 . 0.9300 ? C25 C26 . 1.378(3) ? C26 C27 . 1.405(2) ? C27 C28 . 1.437(2) ? C28 C29 . 1.495(2) ? C29 H29A . 0.9700 ? C29 H29B . 0.9700 ? C29 C30 . 1.509(2) ? C30 H30A . 0.9700 ? C30 H30B . 0.9700 ? C31 H31 . 0.9800 ? C31 C32 . 1.501(3) ? C31 C33 . 1.516(3) ? C32 H32A . 0.9600 ? C32 H32B . 0.9600 ? C32 H32C . 0.9600 ? C33 H33A . 0.9600 ? C33 H33B . 0.9600 ? C33 H33C . 0.9600 ? C34 H34A . 0.9700 ? C34 H34B . 0.9700 ? C34 C35 . 1.502(3) ? C35 C36 . 1.360(3) ? C35 C40 . 1.360(3) ? C36 H36 . 0.9300 ? C36 C37 . 1.381(4) ? C37 H37 . 0.9300 ? C37 C38 . 1.339(3) ? C38 H38 . 0.9300 ? C38 C39 . 1.342(4) ? C39 H39 . 0.9300 ? C39 C40 . 1.376(3) ? C40 H40 . 0.9300 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 Cl1 2_776 0.868(9) 2.362(11) 3.1969(17) 161.5(19) yes N2 H2A Cl1 2_766 0.944(9) 2.184(10) 3.1114(16) 167.2(18) yes N2 H2B Cl1 . 0.945(9) 2.226(12) 3.1191(16) 157.2(18) yes N3 H3A Cl2 2_665 0.863(10) 2.416(11) 3.2657(17) 168(2) yes N4 H4A Cl2 2_655 0.943(9) 2.197(10) 3.1360(16) 173.4(16) yes N4 H4B Cl2 . 0.941(9) 2.192(10) 3.1247(16) 171.0(18) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C6 C7 C2 . . . . 178.71(16) ? O1 C6 C7 C8 . . . . -0.9(3) ? O1 C14 C15 C16 . . . . 66.8(3) ? O1 C14 C15 C20 . . . . -118.0(2) ? O2 C26 C27 C22 . . . . -179.31(15) ? O2 C26 C27 C28 . . . . 1.4(3) ? O2 C34 C35 C36 . . . . 15.9(3) ? O2 C34 C35 C40 . . . . -166.3(2) ? N1 C1 C8 C7 . . . . 0.4(2) ? N1 C1 C8 C9 . . . . 178.92(16) ? N1 C2 C3 C4 . . . . -179.8(2) ? N1 C2 C7 C6 . . . . -179.56(16) ? N1 C2 C7 C8 . . . . 0.1(2) ? N3 C21 C28 C27 . . . . -0.2(2) ? N3 C21 C28 C29 . . . . 175.82(16) ? N3 C22 C23 C24 . . . . 178.9(2) ? N3 C22 C27 C26 . . . . -179.99(16) ? N3 C22 C27 C28 . . . . -0.54(19) ? C1 N1 C2 C3 . . . . 179.9(2) ? C1 N1 C2 C7 . . . . 0.1(2) ? C1 C8 C9 C10 . . . . 108.3(2) ? C2 N1 C1 C8 . . . . -0.3(2) ? C2 C3 C4 C5 . . . . -0.6(3) ? C2 C7 C8 C1 . . . . -0.32(19) ? C2 C7 C8 C9 . . . . -178.69(17) ? C3 C2 C7 C6 . . . . 0.6(3) ? C3 C2 C7 C8 . . . . -179.69(18) ? C3 C4 C5 C6 . . . . 0.7(4) ? C4 C5 C6 O1 . . . . -179.2(2) ? C4 C5 C6 C7 . . . . 0.0(3) ? C5 C6 C7 C2 . . . . -0.6(3) ? C5 C6 C7 C8 . . . . 179.9(2) ? C6 O1 C14 C15 . . . . -173.52(17) ? C6 C7 C8 C1 . . . . 179.3(2) ? C6 C7 C8 C9 . . . . 0.9(3) ? C7 C2 C3 C4 . . . . 0.0(3) ? C7 C8 C9 C10 . . . . -73.5(2) ? C8 C9 C10 N2 . . . . -153.55(15) ? C10 N2 C11 C12 . . . . 162.3(2) ? C10 N2 C11 C13 . . . . -73.6(3) ? C11 N2 C10 C9 . . . . -59.7(2) ? C14 O1 C6 C5 . . . . -1.8(3) ? C14 O1 C6 C7 . . . . 179.02(18) ? C14 C15 C16 C17 . . . . 175.4(2) ? C14 C15 C20 C19 . . . . -174.8(2) ? C15 C16 C17 C18 . . . . -0.7(4) ? C16 C15 C20 C19 . . . . 0.4(3) ? C16 C17 C18 C19 . . . . 0.5(4) ? C17 C18 C19 C20 . . . . 0.1(4) ? C18 C19 C20 C15 . . . . -0.6(3) ? C20 C15 C16 C17 . . . . 0.2(4) ? C21 N3 C22 C23 . . . . -178.5(2) ? C21 N3 C22 C27 . . . . 0.4(2) ? C21 C28 C29 C30 . . . . 112.7(2) ? C22 N3 C21 C28 . . . . -0.2(2) ? C22 C23 C24 C25 . . . . 0.6(3) ? C22 C27 C28 C21 . . . . 0.45(19) ? C22 C27 C28 C29 . . . . -175.33(17) ? C23 C22 C27 C26 . . . . -1.0(3) ? C23 C22 C27 C28 . . . . 178.44(17) ? C23 C24 C25 C26 . . . . -0.4(3) ? C24 C25 C26 O2 . . . . -179.99(19) ? C24 C25 C26 C27 . . . . -0.5(3) ? C25 C26 C27 C22 . . . . 1.2(3) ? C25 C26 C27 C28 . . . . -178.05(19) ? C26 O2 C34 C35 . . . . 85.8(2) ? C26 C27 C28 C21 . . . . 179.8(2) ? C26 C27 C28 C29 . . . . 4.0(3) ? C27 C22 C23 C24 . . . . 0.1(3) ? C27 C28 C29 C30 . . . . -72.3(2) ? C28 C29 C30 N4 . . . . -172.94(14) ? C30 N4 C31 C32 . . . . -60.6(2) ? C30 N4 C31 C33 . . . . 175.65(17) ? C31 N4 C30 C29 . . . . -54.9(2) ? C34 O2 C26 C25 . . . . -18.4(3) ? C34 O2 C26 C27 . . . . 162.13(16) ? C34 C35 C36 C37 . . . . 177.0(3) ? C34 C35 C40 C39 . . . . -176.5(3) ? C35 C36 C37 C38 . . . . -0.4(5) ? C36 C35 C40 C39 . . . . 1.5(4) ? C36 C37 C38 C39 . . . . 1.1(5) ? C37 C38 C39 C40 . . . . -0.5(5) ? C38 C39 C40 C35 . . . . -0.8(5) ? C40 C35 C36 C37 . . . . -0.9(4) ? _cod_database_fobs_code 2244237