#------------------------------------------------------------------------------
#$Date: 2021-05-18 17:36:50 +0100 (Tue, 18 May 2021) $
#$Revision: 265307 $
#$URL: svn://www.crystallography.net/cod/cif/3/00/01/3000114.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3000114
loop_
_publ_author_name
'Bubnova, Rimma'
'Volkov, Sergey'
'Barbara Albert'
'Filatov, Stanislav'
_publ_section_title
;
 Borates--Crystal Structures of Prospective Nonlinear Optical Materials:
 High Anisotropy of the Thermal Expansion Caused by Anharmonic Atomic
 Vibrations
;
_journal_issue                   3
_journal_name_full               Crystals
_journal_page_first              93
_journal_paper_doi               10.3390/cryst7030093
_journal_volume                  7
_journal_year                    2017
_chemical_formula_sum            'B3 Li O5'
_chemical_formula_weight         119.4
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      33
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.478(5)
_cell_length_b                   7.398(4)
_cell_length_c                   5.220(3)
_cell_measurement_temperature    98
_cell_volume                     327.4(3)
_diffrn_ambient_temperature      98
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.99
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'IPDS Stoe'
_diffrn_measurement_method       '??integration method??'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0437
_diffrn_reflns_av_unetI/netI     0.0374
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       6
_diffrn_reflns_limit_l_min       -7
_diffrn_reflns_number            1907
_diffrn_reflns_theta_full        29.29
_diffrn_reflns_theta_max         29.29
_diffrn_reflns_theta_min         3.66
_exptl_absorpt_coefficient_mu    0.226
_exptl_crystal_density_diffrn    2.4216
_exptl_crystal_F_000             232
_refine_diff_density_max         0.20
_refine_diff_density_min         -0.22
_refine_ls_abs_structure_details
'  268 of Friedel pairs used in the refinement'
_refine_ls_extinction_coef       2500(400)
_refine_ls_extinction_method
'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)'
_refine_ls_goodness_of_fit_gt    1.49
_refine_ls_goodness_of_fit_ref   1.39
_refine_ls_number_constraints    1
_refine_ls_number_parameters     83
_refine_ls_number_reflns         760
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0405
_refine_ls_R_factor_gt           0.0285
_refine_ls_shift/su_max          0.0026
_refine_ls_shift/su_mean         0.0007
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0277
_refine_ls_wR_factor_ref         0.0290
_reflns_number_gt                617
_reflns_number_total             760
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            LiB3O5_98K.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according
to the built-in table from CIF Core dictionary named 'cif_core.dic'
version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 4624 2016-04-14 12:54:50Z antanas 

 Released structure into public domain as published material.

 Antanas Vaitkus,
 2021-05-18
;
_cod_original_sg_symbol_Hall     'P -2xabc;-2yab;2zc'
_cod_original_formula_sum        'B3 Li1 O5'
_cod_database_code               3000114
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,z+1/2
3 x+1/2,-y+1/2,z
4 -x+1/2,y+1/2,z+1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Li1 Li 0.4160(4) 0.5677(5) -0.0073(9) Uani 0.0115(11) 4 1 d . . .
B1 B 0.5094(3) 0.8357(3) 0.3530(5) Uani 0.0067(7) 4 1 d . . .
B2 B 0.6949(3) 0.0578(4) 0.5492(6) Uani 0.0065(7) 4 1 d . . .
B3 B 0.6575(2) 0.7510(3) 0.7317(6) Uani 0.0067(7) 4 1 d . . .
O1 O 0.58596(14) 0.9970(2) 0.3466(3) Uani 0.0063(4) 4 1 d . . .
O2 O 0.38335(15) 0.7943(2) 0.1974(3) Uani 0.0065(4) 4 1 d . . .
O3 O 0.55842(15) 0.7014(2) 0.5272(3) Uani 0.0071(4) 4 1 d . . .
O4 O 0.74019(16) 0.90979(19) 0.7321(3) Uani 0.0059(4) 4 1 d . . .
O5 O 0.65948(16) 0.6263(2) 0.9270(3) Uani 0.0062(4) 4 1 d . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_type_symbol
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Li1 Li 0.0134(17) 0.0082(18) 0.013(2) 0.0000(15) -0.0049(16) 0.0021(18)
B1 B 0.0087(10) 0.0057(13) 0.0056(12) 0.0022(9) 0.0041(10) -0.0010(11)
B2 B 0.0075(11) 0.0045(12) 0.0075(14) 0.0003(9) 0.0005(10) 0.0003(11)
B3 B 0.0050(9) 0.0062(11) 0.0088(14) 0.0027(7) 0.0022(10) -0.0026(13)
O1 O 0.0080(6) 0.0050(7) 0.0057(8) -0.0001(5) -0.0017(7) 0.0002(7)
O2 O 0.0071(6) 0.0038(7) 0.0084(9) 0.0000(6) -0.0011(7) 0.0005(8)
O3 O 0.0081(7) 0.0062(7) 0.0068(8) -0.0010(6) -0.0009(6) 0.0001(8)
O4 O 0.0068(6) 0.0046(7) 0.0064(8) -0.0004(5) 0.0000(7) 0.0012(8)
O5 O 0.0061(6) 0.0062(8) 0.0064(8) -0.0004(5) -0.0012(6) -0.0004(7)
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B 0.0013 0.0007 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Li -0.0003 0.0001 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
O1 O2 . . 2.410(3)
O1 O2 . 2_675 2.409(3)
O1 O3 . . 2.393(3)
O1 O4 . . 2.485(3)
O1 O5 . 4_654 2.398(3)
O2 O3 . . 2.375(3)
O2 O4 . 2_674 2.433(3)
O2 O5 . 3_464 2.437(3)
O3 O4 . . 2.428(3)
O3 O5 . . 2.324(3)
O4 O5 . . 2.429(3)
O4 O5 . 4_654 2.414(3)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 1.69 1.31 5.39 <
4 0 0 427.09 451.50 5.48 o
6 0 0 164.03 148.58 4.93 o
8 0 0 0.09 -1.01 5.13 <
10 0 0 17.23 30.27 6.06 o
1 1 0 407.59 350.92 7.64 o
2 1 0 368.57 347.72 5.38 o
3 1 0 1.26 2.24 3.32 <
4 1 0 5.24 8.15 3.19 <
5 1 0 0.36 4.66 3.04 <
6 1 0 352.65 357.12 3.67 o
7 1 0 131.03 130.41 3.54 o
8 1 0 348.70 357.19 3.79 o
9 1 0 240.78 250.22 4.58 o
10 1 0 63.83 63.30 5.11 o
11 1 0 28.23 28.76 5.69 o
0 2 0 143.98 143.59 9.93 o
1 2 0 286.69 279.51 6.54 o
2 2 0 412.55 386.95 6.16 o
3 2 0 898.34 909.47 5.34 o
4 2 0 135.58 141.15 3.94 o
5 2 0 716.92 716.58 4.68 o
6 2 0 305.50 313.68 4.23 o
7 2 0 240.67 239.71 3.85 o
8 2 0 43.60 41.49 4.05 o
9 2 0 28.13 27.81 4.42 o
10 2 0 100.69 104.11 5.31 o
11 2 0 0.33 -6.94 5.91 <
1 3 0 406.74 437.05 6.29 o
2 3 0 4.09 14.14 4.81 <
3 3 0 107.82 115.42 3.89 o
4 3 0 106.73 99.64 3.89 o
5 3 0 34.76 35.84 3.88 o
6 3 0 160.90 156.56 4.17 o
7 3 0 271.41 275.72 4.48 o
8 3 0 7.74 9.14 4.44 <
9 3 0 326.86 335.37 5.15 o
10 3 0 131.59 137.27 5.57 o
11 3 0 1.45 5.26 6.77 <
0 4 0 41.21 39.48 6.69 o
1 4 0 634.47 660.07 9.50 o
2 4 0 443.16 448.13 5.64 o
3 4 0 441.07 416.34 5.63 o
4 4 0 379.28 385.01 4.65 o
5 4 0 220.96 220.66 4.24 o
6 4 0 160.10 159.33 4.30 o
7 4 0 278.10 283.39 4.63 o
8 4 0 67.38 74.09 4.47 o
9 4 0 29.65 27.40 5.13 o
10 4 0 33.00 37.60 5.78 o
1 5 0 328.87 332.10 6.14 o
2 5 0 132.25 113.87 5.75 o
3 5 0 222.90 209.00 5.54 o
4 5 0 8.57 17.89 4.03 o
5 5 0 249.71 230.32 4.82 o
6 5 0 14.10 16.34 4.33 o
7 5 0 137.29 140.61 4.73 o
8 5 0 0.38 10.54 4.96 <
9 5 0 48.40 54.43 5.52 o
10 5 0 0.36 -2.72 6.12 <
0 6 0 6.79 6.47 8.15 <
1 6 0 58.96 55.92 5.48 o
2 6 0 690.71 644.61 8.69 o
3 6 0 51.64 54.77 5.91 o
4 6 0 20.31 18.09 4.42 o
5 6 0 141.23 140.03 4.53 o
6 6 0 0.63 0.50 4.66 <
7 6 0 22.86 24.43 4.96 o
8 6 0 1.47 -0.17 5.39 <
9 6 0 1.17 3.71 5.97 <
1 7 0 83.42 89.33 5.87 o
2 7 0 149.85 165.60 6.37 o
3 7 0 475.95 451.09 8.78 o
4 7 0 282.72 262.40 5.60 o
5 7 0 87.51 87.08 5.37 o
6 7 0 23.83 29.66 5.39 o
7 7 0 104.38 108.40 5.89 o
8 7 0 9.05 9.03 5.99 <
0 8 0 3.78 7.67 9.42 <
1 8 0 9.36 13.45 6.68 <
2 8 0 18.70 20.33 6.81 <
3 8 0 309.46 297.98 6.97 o
4 8 0 104.90 116.31 7.34 o
5 8 0 7.13 12.57 5.37 <
6 8 0 51.71 58.12 6.08 o
7 8 0 8.53 5.93 6.83 <
1 9 0 0.09 5.35 7.05 <
2 9 0 147.74 150.81 7.86 o
3 9 0 0.81 3.56 7.39 <
4 9 0 59.26 68.78 6.56 o
5 9 0 307.70 331.94 7.20 o
0 10 0 100.18 107.94 12.62 o
1 10 0 64.70 74.30 8.91 o
2 0 1 2360.69 2301.71 15.62 o
2 0 -1 2361.23 2383.86 11.06 o
4 0 1 2156.16 2185.32 11.65 o
4 0 -1 2157.79 2193.80 8.18 o
6 0 1 290.06 300.52 4.75 o
6 0 -1 289.99 294.52 5.11 o
8 0 1 259.67 266.24 7.77 o
8 0 -1 259.89 256.68 5.43 o
10 0 1 46.04 48.35 8.97 o
10 0 -1 45.80 48.93 6.32 o
0 1 -1 38.44 33.98 8.30 o
1 1 1 1169.01 1161.48 10.65 o
1 1 -1 1168.94 1162.32 8.82 o
2 1 1 1605.50 1574.14 7.68 o
2 1 -1 1605.94 1533.86 7.47 o
3 1 1 1167.76 1200.44 5.94 o
3 1 -1 1169.04 1198.41 5.09 o
4 1 1 495.16 499.58 4.50 o
4 1 -1 496.23 502.56 3.87 o
5 1 1 184.48 177.81 3.98 o
5 1 -1 184.31 174.85 3.42 o
6 1 1 86.52 85.01 3.99 o
6 1 -1 86.66 92.15 3.26 o
7 1 1 71.13 75.19 4.08 o
7 1 -1 70.77 70.64 3.37 o
8 1 1 79.35 79.62 4.36 o
8 1 -1 78.93 85.66 3.75 o
9 1 1 72.04 76.00 4.75 o
9 1 -1 71.93 78.84 4.06 o
10 1 1 257.91 262.90 6.05 o
10 1 -1 257.76 255.32 4.30 o
11 1 1 2.00 6.85 6.53 <
11 1 -1 2.06 -2.76 5.80 <
1 2 1 658.51 647.11 7.44 o
1 2 -1 657.93 646.34 8.54 o
2 2 1 1774.61 1807.23 7.92 o
2 2 -1 1773.53 1715.58 9.07 o
3 2 1 146.64 158.46 4.22 o
3 2 -1 146.63 159.98 4.20 o
4 2 1 252.57 265.57 4.16 o
4 2 -1 252.81 267.50 3.43 o
5 2 1 21.02 29.65 4.08 o
5 2 -1 21.06 27.06 3.32 o
6 2 1 203.76 208.20 4.24 o
6 2 -1 204.10 214.30 3.33 o
7 2 1 266.90 269.51 4.37 o
7 2 -1 266.98 250.30 3.79 o
8 2 1 87.80 87.35 4.45 o
8 2 -1 87.34 92.50 3.84 o
9 2 1 1.01 6.51 4.46 <
9 2 -1 1.00 -5.30 4.14 <
10 2 1 36.56 37.84 4.68 o
10 2 -1 36.56 37.75 5.28 o
11 2 1 35.20 38.23 7.37 o
11 2 -1 35.22 40.15 5.30 o
0 3 1 1653.65 1738.78 19.56 o
0 3 -1 1650.86 1695.15 11.25 o
1 3 1 156.51 171.04 6.19 o
1 3 -1 156.41 175.46 5.93 o
2 3 1 259.73 277.18 4.95 o
2 3 -1 259.60 264.56 5.69 o
3 3 1 451.93 466.80 4.88 o
3 3 -1 452.24 452.71 5.86 o
4 3 1 68.89 76.34 4.17 o
4 3 -1 68.87 84.57 5.24 o
5 3 1 356.41 341.07 4.56 o
5 3 -1 356.29 344.17 4.32 o
6 3 1 220.92 220.72 4.04 o
6 3 -1 220.57 219.40 4.22 o
7 3 1 250.34 249.34 4.43 o
7 3 -1 250.47 252.78 4.43 o
8 3 1 336.20 331.74 4.83 o
8 3 -1 336.69 334.76 4.81 o
9 3 1 125.09 126.87 5.05 o
9 3 -1 125.07 125.43 5.05 o
10 3 1 7.74 10.15 5.17 <
10 3 -1 7.72 10.04 5.13 <
11 3 1 6.25 13.69 8.75 <
1 4 1 546.35 527.02 10.63 o
1 4 -1 546.05 555.77 8.01 o
2 4 1 677.92 678.44 5.62 o
2 4 -1 677.05 626.58 6.34 o
3 4 1 36.10 35.83 4.29 o
3 4 -1 35.90 32.48 4.83 o
4 4 1 22.43 21.93 4.33 o
4 4 -1 22.50 25.85 4.77 o
5 4 1 331.82 339.97 4.68 o
5 4 -1 332.33 325.54 4.62 o
6 4 1 23.94 19.84 4.38 o
6 4 -1 23.94 23.11 4.16 o
7 4 1 81.16 87.04 4.70 o
7 4 -1 81.38 81.15 4.47 o
8 4 1 97.54 91.32 4.51 o
8 4 -1 97.36 100.23 4.79 o
9 4 1 120.26 113.30 5.33 o
9 4 -1 120.24 111.51 5.27 o
10 4 1 62.01 59.46 5.89 o
10 4 -1 61.89 48.09 5.87 o
0 5 1 57.43 66.63 8.89 o
0 5 -1 57.15 64.80 6.90 o
1 5 1 93.19 97.70 6.39 o
1 5 -1 93.16 90.77 5.03 o
2 5 1 18.65 16.15 5.24 o
2 5 -1 18.73 21.69 5.58 o
3 5 1 85.14 84.11 4.71 o
3 5 -1 85.35 79.06 5.40 o
4 5 1 93.92 94.46 4.58 o
4 5 -1 93.78 94.11 5.53 o
5 5 1 437.24 431.22 4.95 o
5 5 -1 436.98 421.68 4.64 o
6 5 1 24.14 25.63 4.61 o
6 5 -1 23.91 26.65 4.40 o
7 5 1 160.23 161.38 4.86 o
7 5 -1 160.13 151.55 4.77 o
8 5 1 28.46 35.08 5.37 o
8 5 -1 28.55 25.92 5.05 o
9 5 1 15.71 19.03 5.56 o
9 5 -1 15.70 10.35 5.54 <
1 6 1 321.55 320.94 7.19 o
1 6 -1 321.50 316.15 5.50 o
2 6 1 185.31 185.62 6.25 o
2 6 -1 185.93 187.68 5.25 o
3 6 1 100.30 100.63 4.77 o
3 6 -1 100.26 97.58 5.70 o
4 6 1 76.00 74.44 4.81 o
4 6 -1 75.72 70.64 6.11 o
5 6 1 77.06 78.25 4.79 o
5 6 -1 76.63 70.48 4.77 o
6 6 1 8.05 10.56 5.17 <
6 6 -1 8.07 10.32 4.70 <
7 6 1 7.72 8.08 5.00 <
7 6 -1 7.73 11.23 5.00 <
8 6 1 2.63 -2.89 5.80 <
8 6 -1 2.70 0.39 5.78 <
9 6 1 117.32 133.81 6.56 o
9 6 -1 117.35 79.41 6.50 o
0 7 1 551.17 561.76 11.27 o
0 7 -1 552.03 492.97 8.51 o
1 7 1 378.11 366.14 7.60 o
1 7 -1 378.49 374.74 6.24 o
2 7 1 90.77 92.64 6.88 o
2 7 -1 91.07 80.21 5.87 o
3 7 1 283.93 284.35 5.84 o
3 7 -1 283.56 274.24 8.28 o
4 7 1 0.63 8.17 5.15 <
4 7 -1 0.62 2.35 6.10 <
5 7 1 39.21 36.70 5.41 o
5 7 -1 39.21 36.46 5.13 o
6 7 1 23.34 14.75 5.73 <
6 7 -1 23.53 17.05 5.45 o
7 7 1 82.32 83.25 5.98 o
7 7 -1 82.08 91.81 5.67 o
8 7 1 50.58 53.78 6.53 o
8 7 -1 50.24 54.79 6.17 o
1 8 1 67.20 74.81 7.74 o
1 8 -1 67.50 79.62 6.88 o
2 8 1 165.52 178.12 8.01 o
2 8 -1 166.16 168.21 6.65 o
3 8 1 37.75 39.26 6.06 o
3 8 -1 37.72 39.31 6.10 o
4 8 1 114.29 111.10 6.17 o
4 8 -1 114.22 119.47 6.45 o
5 8 1 90.87 87.31 6.21 o
5 8 -1 90.63 86.38 6.13 o
6 8 1 27.40 15.65 6.49 <
6 8 -1 27.28 34.43 6.17 o
7 8 -1 3.18 9.63 10.86 <
0 9 1 40.59 59.38 12.20 o
0 9 -1 40.95 51.23 9.40 o
1 9 1 4.29 2.50 8.60 <
1 9 -1 4.32 9.03 7.13 <
2 9 1 4.70 5.26 7.16 <
2 9 -1 4.69 5.37 6.77 <
3 9 1 53.63 55.03 7.48 o
3 9 -1 53.41 50.98 7.55 o
4 9 1 205.77 218.05 7.21 o
4 9 -1 205.85 220.21 7.54 o
5 9 1 12.95 7.09 7.59 <
5 9 -1 12.99 14.74 10.89 <
1 10 1 1.21 4.74 10.58 <
1 10 -1 1.26 8.47 7.74 <
0 0 -2 344.22 346.52 8.58 o
2 0 2 707.91 710.01 9.06 o
2 0 -2 709.08 692.36 9.63 o
4 0 2 20.83 16.88 6.71 <
4 0 -2 20.74 19.13 4.51 o
6 0 2 104.92 100.22 7.23 o
6 0 -2 105.46 99.21 4.92 o
8 0 2 679.76 683.44 8.76 o
8 0 -2 678.22 661.94 6.20 o
10 0 2 5.58 1.03 9.27 <
10 0 -2 5.40 4.18 6.57 <
1 1 2 797.91 848.42 7.68 o
1 1 -2 797.92 806.34 7.70 o
2 1 2 730.76 790.17 6.96 o
2 1 -2 731.56 772.17 5.73 o
3 1 2 404.52 408.96 5.55 o
3 1 -2 405.14 415.59 4.62 o
4 1 2 375.06 395.62 5.13 o
4 1 -2 375.30 389.40 3.89 o
5 1 2 260.73 270.01 5.22 o
5 1 -2 261.31 260.33 3.51 o
6 1 2 66.26 65.12 5.07 o
6 1 -2 66.20 65.85 3.47 o
7 1 2 52.09 49.01 5.16 o
7 1 -2 52.19 57.61 3.60 o
8 1 2 7.11 13.77 5.43 <
8 1 -2 7.20 7.91 3.79 <
9 1 2 17.70 21.90 5.41 o
9 1 -2 17.70 19.47 4.20 o
10 1 2 13.58 23.71 5.99 o
10 1 -2 13.48 18.88 4.27 o
11 1 2 30.10 27.77 7.48 o
11 1 -2 30.11 30.55 6.14 o
0 2 -2 703.10 773.40 8.87 o
1 2 2 819.40 880.29 9.31 o
1 2 -2 818.97 883.37 8.10 o
2 2 2 240.21 253.53 6.01 o
2 2 -2 240.45 248.57 5.03 o
3 2 2 344.40 352.85 5.71 o
3 2 -2 344.12 350.94 4.72 o
4 2 2 704.51 708.38 6.36 o
4 2 -2 704.43 714.00 4.72 o
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