#------------------------------------------------------------------------------ #$Date: 2022-10-28 09:00:12 +0100 (Fri, 28 Oct 2022) $ #$Revision: 278854 $ #$URL: svn://www.crystallography.net/cod/cif/3/00/04/3000407.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3000407 loop_ _publ_author_name 'Augustina Jozeli\=unait\.e' 'Aiman Rahmanudin' 'Emilie Baudat' 'Saulius Gra\ 2\s(I)' _journal_article_reference e202202698 _cod_data_source_file PTS_T2_trans-v0.2.0.cif _cod_data_source_block shelx _cod_depositor_comments 'Releasing structure 3000407 into public domain as published material.' _cod_database_code 3000407 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.724 _shelx_estimated_absorpt_t_min 0.724 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C01A(H01A,H01B), C01E(H01D,H01E), C01H(H01N,H01P), C01P(H01U,H01X), C01Q(H01H, H01K), C01T(H1,H), C01Z(H4,HC), C023(H02V,H02W), C024(H02X,H02Y), C025(H02D, H02E), C027(H02Z,HD), C02D(H02J,H02K), C02E(H6,HE), C02F(H02L,H02M), C02G(H02N, H02O), C02H(H02P,H02Q) 2.b Aromatic/amide H refined with riding coordinates: C00P(H00P), C00U(H00U), C00X(H00X), C011(H011), C014(H014), C015(H015), C019(H019), C01B(H01C), C01C(H01L), C01D(H01M), C01F(H01F), C01G(H01G), C01I(H01I), C01J(H01J), C01N(H01T), C01O(H01O), C01R(H01Z), C01S(H01), C01U(H2), C01V(H01V), C01W(H01W), C01Y(H01Y), C020(H020), C022(H022), C028(H028), C029(H029), C02A(H02), C02B(H02I), C02C(H5), C02I(H02R) 2.c Idealised Me refined as rotating group: C01L(H01Q,H01R,H01S), C01X(H3,HA,HB), C021(H02A,H02B,H02C), C026(H02F,H02G, H02H), C02J(H7,HF,HG), C02K(H02S,H02T,H02U) ; _shelx_res_file ; TITL shelx_a.res in P2(1)/c shelx.res created by SHELXL-2018/3 at 18:45:40 on 10-Aug-2022 REM Old TITL shelx in P21/a #14 REM SHELXT solution in P2(1)/c REM R1 0.281, Rweak 0.006, Alpha 0.029, Orientation a'=c, b'=-b, c'=a REM Formula found by SHELXT: C76 N7 O5 S4 CELL 1.54187 22.4116 18.4777 17.2409 90 106.899 90 ZERR 8 0.0016 0.0013 0.0012 0.006 0.008 0.006 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O S UNIT 312 320 16 24 16 L.S. 20 PLAN 10 SIZE 0.2 0.2 0.2 TEMP 292.15 CONF BOND $H list 4 fmap 2 acta MORE -1 REM REM REM WGHT 0.122200 FVAR 0.26440 S001 5 0.035730 0.382252 0.335513 11.00000 0.04594 0.03084 = 0.04902 -0.00050 -0.00548 -0.00477 S002 5 0.464684 0.866685 0.670485 11.00000 0.03785 0.04014 = 0.05170 0.00700 -0.00567 -0.01113 S003 5 0.304941 0.823993 0.615121 11.00000 0.02828 0.05237 = 0.05669 0.02054 -0.00553 0.01376 S004 5 0.194096 0.426244 0.383547 11.00000 0.03309 0.06316 = 0.06020 0.01911 -0.00941 0.02448 O005 4 -0.028465 0.631705 0.309276 11.00000 0.02764 0.03205 = 0.05505 0.00060 -0.01150 0.00406 O006 4 0.142261 0.538845 0.510379 11.00000 0.02720 0.05216 = 0.05270 0.00324 -0.02398 -0.00943 O007 4 0.352659 0.713225 0.492841 11.00000 0.02554 0.05989 = 0.04992 0.00361 -0.02197 -0.00596 O008 4 0.534487 0.619797 0.673902 11.00000 0.02909 0.05017 = 0.05865 0.00231 -0.01526 0.00545 O009 4 0.760931 0.396572 1.178465 11.00000 0.03157 0.05449 = 0.05728 0.02741 -0.00570 0.01186 O00A 4 -0.250426 0.864030 -0.183101 11.00000 0.03393 0.05754 = 0.06873 0.03091 -0.01162 0.01321 N00B 3 0.572467 0.568417 0.984807 11.00000 0.02197 0.04070 = 0.04073 0.00241 -0.00653 0.00532 N00C 3 0.533263 0.538741 0.927284 11.00000 0.02840 0.04271 = 0.03794 0.00385 -0.00709 0.00449 N00D 3 -0.064749 0.682827 0.000204 11.00000 0.02830 0.05008 = 0.04314 0.00452 -0.00596 0.00421 N00E 3 -0.025046 0.711278 0.057671 11.00000 0.03040 0.05267 = 0.04181 0.00720 -0.00446 0.00545 C00F 1 0.037431 0.513466 0.382297 11.00000 0.01557 0.02958 = 0.03214 0.00131 -0.01022 -0.00223 C00G 1 0.099119 0.570629 0.219498 11.00000 0.01379 0.04963 = 0.02909 0.00602 -0.00246 0.00588 C00H 1 0.443132 0.664630 0.583109 11.00000 0.02113 0.04717 = 0.03158 0.00198 -0.00418 -0.00328 C00I 1 0.401143 0.676646 0.772843 11.00000 0.01654 0.03705 = 0.02890 0.00432 -0.00365 -0.00037 C00J 1 0.070849 0.466069 0.350650 11.00000 0.02321 0.02807 = 0.03030 0.00282 -0.01442 0.00021 C00K 1 0.354561 0.724590 0.717086 11.00000 0.01943 0.03581 = 0.03141 0.00403 -0.00558 -0.00051 C00L 1 0.489819 0.588564 0.877555 11.00000 0.02201 0.03725 = 0.03534 0.00609 -0.00310 0.00416 C00M 1 0.617258 0.520232 1.034977 11.00000 0.02097 0.03621 = 0.03313 0.00358 -0.00307 0.00451 C00N 1 0.399657 0.602136 0.760103 11.00000 0.02237 0.03537 = 0.03223 0.00394 -0.00182 -0.00427 C00O 1 0.057282 0.587637 0.409832 11.00000 0.01876 0.03278 = 0.03510 -0.00248 -0.00324 -0.00568 C00P 1 0.444675 0.558917 0.812164 11.00000 0.02742 0.03366 = 0.03585 0.00178 -0.00251 0.00040 AFIX 43 H00P 2 0.444563 0.509303 0.803054 11.00000 -1.20000 AFIX 0 C00Q 1 0.428424 0.783936 0.648064 11.00000 0.02060 0.03650 = 0.03295 0.00905 -0.01046 -0.00259 C00R 1 0.462313 0.738071 0.614861 11.00000 0.01799 0.04329 = 0.02877 0.00674 -0.00833 -0.00394 C00S 1 0.130011 0.477202 0.332574 11.00000 0.02070 0.03874 = 0.03082 0.00234 -0.00984 0.00970 C00T 1 0.051482 0.539936 0.155459 11.00000 0.02338 0.04500 = 0.02870 0.00076 -0.00375 0.00674 C00U 1 0.616746 0.445912 1.028242 11.00000 0.02767 0.04199 = 0.03310 -0.00248 -0.00470 -0.00041 AFIX 43 H00U 2 0.584052 0.422730 0.990613 11.00000 -1.20000 AFIX 0 C00V 1 0.110513 0.599154 0.476594 11.00000 0.02498 0.04576 = 0.03736 -0.00760 -0.00276 -0.01518 C00W 1 0.446421 0.707181 0.840010 11.00000 0.02457 0.03614 = 0.02996 0.00020 -0.00455 0.00016 C00X 1 0.490150 0.662397 0.891086 11.00000 0.02358 0.04127 = 0.03291 -0.00043 -0.00916 -0.00131 AFIX 43 H00X 2 0.520143 0.682227 0.935075 11.00000 -1.20000 AFIX 0 C00Y 1 0.713806 0.440746 1.134236 11.00000 0.02691 0.04381 = 0.03464 0.01222 -0.00094 0.01077 C00Z 1 0.368857 0.772028 0.664251 11.00000 0.01896 0.03666 = 0.03204 0.00589 -0.00857 0.00273 C010 1 0.144128 0.522838 0.277650 11.00000 0.01624 0.04819 = 0.03385 0.00349 -0.00634 0.00712 C011 1 0.664124 0.553424 1.094633 11.00000 0.02535 0.03428 = 0.04778 -0.00134 -0.00494 0.00325 AFIX 43 H011 2 0.663034 0.603310 1.101251 11.00000 -1.20000 AFIX 0 C012 1 0.105188 0.645501 0.227315 11.00000 0.02070 0.04793 = 0.03658 0.00696 -0.00082 -0.00138 C013 1 0.021812 0.647000 0.374026 11.00000 0.02411 0.03400 = 0.04394 -0.00529 -0.00125 -0.00522 C014 1 0.665049 0.406134 1.077685 11.00000 0.03441 0.03207 = 0.04233 0.00212 0.00102 0.00240 AFIX 43 H014 2 0.665016 0.355977 1.073191 11.00000 -1.20000 AFIX 0 C015 1 0.010596 0.585707 0.101123 11.00000 0.02147 0.05342 = 0.02906 0.00345 -0.00815 0.00396 AFIX 43 H015 2 -0.021258 0.565917 0.059251 11.00000 -1.20000 AFIX 0 C016 1 -0.108383 0.733071 -0.048931 11.00000 0.02736 0.04262 = 0.03838 0.00877 -0.00406 0.00579 C017 1 0.387985 0.653201 0.519586 11.00000 0.02845 0.05212 = 0.03277 -0.00131 -0.00536 -0.01141 C018 1 0.016378 0.659655 0.108137 11.00000 0.02435 0.04835 = 0.03557 0.01104 -0.00107 0.00742 C019 1 -0.157527 0.701936 -0.107643 11.00000 0.03058 0.03911 = 0.06194 0.00756 -0.00724 0.00216 AFIX 43 H019 2 -0.158270 0.652144 -0.115738 11.00000 -1.20000 AFIX 0 C01A 1 -0.118258 0.660013 0.200107 11.00000 0.02864 0.03937 = 0.05410 0.01133 0.00107 0.00680 AFIX 23 H01A 2 -0.143400 0.629535 0.224080 11.00000 -1.20000 H01B 2 -0.102219 0.630182 0.164391 11.00000 -1.20000 AFIX 0 C01B 1 -0.153215 0.849944 -0.087333 11.00000 0.03949 0.03766 = 0.04854 0.00567 -0.00356 0.00475 AFIX 43 H01C 2 -0.151370 0.900012 -0.081630 11.00000 -1.20000 AFIX 0 C01C 1 0.712580 0.514001 1.144659 11.00000 0.02461 0.04240 = 0.04175 -0.00256 -0.01024 -0.00094 AFIX 43 H01L 2 0.743809 0.536908 1.184713 11.00000 -1.20000 AFIX 0 C01D 1 0.290570 0.730406 0.715662 11.00000 0.01910 0.06270 = 0.04294 0.00853 0.00116 0.00210 AFIX 43 H01M 2 0.272594 0.701878 0.747275 11.00000 -1.20000 AFIX 0 C01E 1 -0.064587 0.690668 0.266127 11.00000 0.03434 0.03446 = 0.05140 0.00545 0.00219 0.00728 AFIX 23 H01D 2 -0.038974 0.721025 0.242759 11.00000 -1.20000 H01E 2 -0.080137 0.719964 0.302742 11.00000 -1.20000 AFIX 0 C01F 1 -0.105197 0.807377 -0.040859 11.00000 0.02834 0.05136 = 0.03840 0.00166 -0.00928 0.00268 AFIX 43 H01F 2 -0.070864 0.828831 -0.004274 11.00000 -1.20000 AFIX 0 C01G 1 -0.017420 0.481133 0.392916 11.00000 0.01885 0.04515 = 0.04363 0.00050 -0.00376 -0.00459 AFIX 43 H01G 2 -0.045851 0.505887 0.413082 11.00000 -1.20000 AFIX 0 C01H 1 0.663892 0.531485 0.832539 11.00000 0.02586 0.04656 = 0.05204 0.00652 -0.00020 0.00612 AFIX 23 H01N 2 0.639006 0.505053 0.860617 11.00000 -1.20000 H01P 2 0.676417 0.497848 0.796984 11.00000 -1.20000 AFIX 0 C01I 1 0.063688 0.689397 0.171555 11.00000 0.02722 0.04369 = 0.04047 0.00770 -0.00473 0.00039 AFIX 43 H01I 2 0.067474 0.739426 0.176542 11.00000 -1.20000 AFIX 0 C01J 1 -0.205419 0.744275 -0.154235 11.00000 0.02788 0.04787 = 0.05731 0.00635 -0.01423 -0.00010 AFIX 43 H01J 2 -0.238398 0.723116 -0.193397 11.00000 -1.20000 AFIX 0 C01K 1 0.481478 0.605118 0.611774 11.00000 0.02760 0.05079 = 0.04221 -0.00357 -0.00218 -0.00289 C01L 1 0.349860 0.567625 0.691848 11.00000 0.03398 0.04601 = 0.03886 -0.00064 -0.00862 -0.00803 AFIX 137 H01Q 2 0.311536 0.565384 0.706047 11.00000 -1.50000 H01R 2 0.362560 0.519571 0.682554 11.00000 -1.50000 H01S 2 0.343778 0.595945 0.643485 11.00000 -1.50000 AFIX 0 C01M 1 -0.204008 0.817844 -0.142339 11.00000 0.02902 0.04762 = 0.04240 0.01638 -0.00659 0.00828 C01N 1 0.518073 0.771394 0.608975 11.00000 0.01886 0.06435 = 0.04065 0.00977 -0.00514 -0.00748 AFIX 43 H01T 2 0.546946 0.747961 0.588430 11.00000 -1.20000 AFIX 0 C01O 1 -0.023786 0.410993 0.370701 11.00000 0.03028 0.04553 = 0.05040 0.00237 -0.00775 -0.01929 AFIX 43 H01O 2 -0.056714 0.381792 0.374165 11.00000 -1.20000 AFIX 0 C01P 1 0.624224 0.591214 0.781673 11.00000 0.02628 0.05055 = 0.05944 0.00929 -0.00283 0.00647 AFIX 23 H01U 2 0.607368 0.621458 0.816234 11.00000 -1.20000 H01X 2 0.650293 0.621320 0.758768 11.00000 -1.20000 AFIX 0 C01Q 1 -0.158686 0.719693 0.151193 11.00000 0.03388 0.04313 = 0.04783 0.01277 -0.00091 0.00732 AFIX 23 H01H 2 -0.169439 0.753553 0.187991 11.00000 -1.20000 H01K 2 -0.135020 0.745800 0.121200 11.00000 -1.20000 AFIX 0 C01R 1 0.372063 0.585104 0.486987 11.00000 0.04373 0.06660 = 0.04250 -0.00552 -0.00700 -0.01680 AFIX 43 H01Z 2 0.335329 0.578034 0.445452 11.00000 -1.20000 AFIX 0 C01S 1 0.259139 0.781083 0.664209 11.00000 0.01817 0.06184 = 0.05729 0.00462 -0.00316 0.01014 AFIX 43 H01 2 0.217202 0.791603 0.656226 11.00000 -1.20000 AFIX 0 C01T 1 0.571476 0.560953 0.714272 11.00000 0.03327 0.04976 = 0.05360 0.00400 -0.00150 0.01006 AFIX 23 H1 2 0.587781 0.534063 0.676574 11.00000 -1.20000 H 2 0.546446 0.528427 0.736136 11.00000 -1.20000 AFIX 0 C01U 1 0.760919 0.504526 0.947439 11.00000 0.03450 0.04459 = 0.05069 0.00630 -0.00544 -0.00374 AFIX 43 H2 2 0.742660 0.478007 0.980367 11.00000 -1.20000 AFIX 0 C01V 1 0.208167 0.515762 0.278740 11.00000 0.01955 0.07965 = 0.05318 0.01111 0.00319 0.01405 AFIX 43 H01V 2 0.226012 0.542555 0.245577 11.00000 -1.20000 AFIX 0 C01W 1 0.127002 0.668337 0.506166 11.00000 0.04025 0.05144 = 0.04482 -0.00853 -0.00412 -0.02111 AFIX 43 H01W 2 0.162105 0.675950 0.550039 11.00000 -1.20000 AFIX 0 C01X 1 0.447669 0.786321 0.859174 11.00000 0.04522 0.03885 = 0.04255 -0.00292 -0.00951 0.00244 AFIX 137 H3 2 0.473644 0.811070 0.832204 11.00000 -1.50000 HA 2 0.464065 0.793162 0.916661 11.00000 -1.50000 HB 2 0.406099 0.805460 0.840942 11.00000 -1.50000 AFIX 0 C01Y 1 0.038351 0.716395 0.403533 11.00000 0.04629 0.03229 = 0.06665 -0.00807 0.00748 -0.00320 AFIX 43 H01Y 2 0.014777 0.756189 0.379426 11.00000 -1.20000 AFIX 0 C01Z 1 0.846892 0.455784 1.141438 11.00000 0.02627 0.05439 = 0.06128 0.00520 -0.00924 0.00421 AFIX 23 H4 2 0.890268 0.469433 1.164216 11.00000 -1.20000 HC 2 0.823717 0.499149 1.119471 11.00000 -1.20000 AFIX 0 C020 1 0.090548 0.725155 0.469447 11.00000 0.05540 0.04195 = 0.05627 -0.01858 0.00693 -0.02184 AFIX 43 H020 2 0.101280 0.771550 0.489599 11.00000 -1.20000 AFIX 0 C021 1 0.044069 0.459944 0.142880 11.00000 0.04864 0.04757 = 0.03818 -0.00400 -0.01067 0.00776 AFIX 137 H02A 2 0.083924 0.436851 0.163477 11.00000 -1.50000 H02B 2 0.027514 0.449864 0.086031 11.00000 -1.50000 H02C 2 0.016014 0.441788 0.171063 11.00000 -1.50000 AFIX 0 C022 1 0.524987 0.840135 0.636029 11.00000 0.02806 0.06294 = 0.05001 0.01354 -0.00825 -0.02169 AFIX 43 H022 2 0.558657 0.869496 0.635875 11.00000 -1.20000 AFIX 0 C023 1 0.822849 0.426925 1.208399 11.00000 0.03012 0.07055 = 0.05005 0.01283 -0.01178 0.01457 AFIX 23 H02V 2 0.851134 0.389920 1.237924 11.00000 -1.20000 H02W 2 0.822216 0.465820 1.245936 11.00000 -1.20000 AFIX 0 C024 1 0.721743 0.560950 0.894314 11.00000 0.03709 0.04376 = 0.06707 0.00878 -0.01036 -0.00014 AFIX 23 H02X 2 0.746980 0.586142 0.865758 11.00000 -1.20000 H02Y 2 0.708978 0.596030 0.928218 11.00000 -1.20000 AFIX 0 C025 1 -0.312649 0.836430 -0.215259 11.00000 0.03520 0.07362 = 0.06020 0.02104 -0.01701 0.01504 AFIX 23 H02D 2 -0.312566 0.799716 -0.255441 11.00000 -1.20000 H02E 2 -0.339577 0.875450 -0.242604 11.00000 -1.20000 AFIX 0 C026 1 0.154895 0.679866 0.296044 11.00000 0.02944 0.05990 = 0.04716 0.00495 -0.00886 -0.01008 AFIX 137 H02F 2 0.154986 0.657370 0.346269 11.00000 -1.50000 H02G 2 0.146383 0.730609 0.298383 11.00000 -1.50000 H02H 2 0.194913 0.673463 0.287166 11.00000 -1.50000 AFIX 0 C027 1 0.841947 0.402449 1.072656 11.00000 0.05283 0.04420 = 0.06766 0.00793 0.01289 0.01587 AFIX 23 H02Z 2 0.868105 0.360900 1.093678 11.00000 -1.20000 HD 2 0.799220 0.385534 1.052970 11.00000 -1.20000 AFIX 0 C028 1 0.239650 0.466640 0.332380 11.00000 0.02015 0.08988 = 0.07553 0.00790 -0.00284 0.02385 AFIX 43 H028 2 0.281577 0.455854 0.340701 11.00000 -1.20000 AFIX 0 C029 1 0.410952 0.528478 0.516566 11.00000 0.06781 0.05447 = 0.05414 -0.01853 0.00255 -0.01543 AFIX 43 H029 2 0.400604 0.482723 0.494233 11.00000 -1.20000 AFIX 0 C02A 1 0.818584 0.489288 0.951569 11.00000 0.03482 0.05726 = 0.06316 0.01491 0.00187 0.00114 AFIX 43 H02 2 0.835818 0.516694 0.918238 11.00000 -1.20000 AFIX 0 C02B 1 -0.257793 0.748128 0.040566 11.00000 0.04568 0.04834 = 0.07151 0.01441 -0.01626 -0.00721 AFIX 43 H02I 2 -0.239248 0.775701 0.008787 11.00000 -1.20000 AFIX 0 C02C 1 0.466107 0.537486 0.579757 11.00000 0.05365 0.05049 = 0.06030 -0.00693 0.00486 0.00288 AFIX 43 H5 2 0.491900 0.498153 0.599674 11.00000 -1.20000 AFIX 0 C02D 1 -0.217701 0.691169 0.092699 11.00000 0.04464 0.04802 = 0.09096 0.01994 -0.01759 -0.00529 AFIX 23 H02J 2 -0.206698 0.655566 0.057841 11.00000 -1.20000 H02K 2 -0.241879 0.666686 0.123218 11.00000 -1.20000 AFIX 0 C02E 1 0.860860 0.433664 1.002671 11.00000 0.04865 0.06386 = 0.06922 0.01354 0.01006 0.01977 AFIX 23 H6 2 0.901844 0.455194 1.024031 11.00000 -1.20000 HE 2 0.864899 0.394044 0.967631 11.00000 -1.20000 AFIX 0 C02F 1 -0.339563 0.804167 -0.152439 11.00000 0.02962 0.06137 = 0.07406 0.01608 -0.01660 0.00299 AFIX 23 H02L 2 -0.317132 0.759969 -0.131995 11.00000 -1.20000 H02M 2 -0.382735 0.791280 -0.178309 11.00000 -1.20000 AFIX 0 C02G 1 -0.336797 0.854103 -0.081001 11.00000 0.06554 0.04821 = 0.07988 0.01827 0.00662 0.01861 AFIX 23 H02N 2 -0.294298 0.871080 -0.058598 11.00000 -1.20000 H02O 2 -0.362885 0.896003 -0.100654 11.00000 -1.20000 AFIX 0 C02H 1 -0.357715 0.818757 -0.014081 11.00000 0.05894 0.07429 = 0.08429 0.03176 0.01237 0.02352 AFIX 23 H02P 2 -0.363553 0.856364 0.022290 11.00000 -1.20000 H02Q 2 -0.398001 0.796364 -0.038179 11.00000 -1.20000 AFIX 0 C02I 1 -0.314904 0.763009 0.034983 11.00000 0.04579 0.06795 = 0.09408 0.03913 0.00055 0.00231 AFIX 43 H02R 2 -0.332468 0.734232 0.066833 11.00000 -1.20000 AFIX 0 C02J 1 0.293086 0.703654 0.435032 11.00000 0.03150 0.07757 = 0.07139 0.01331 -0.02884 -0.01419 AFIX 137 H7 2 0.298218 0.681664 0.386928 11.00000 -1.50000 HF 2 0.273150 0.749854 0.421669 11.00000 -1.50000 HG 2 0.267785 0.673002 0.457581 11.00000 -1.50000 AFIX 0 C02K 1 0.202981 0.548307 0.566071 11.00000 0.03356 0.08455 = 0.07188 0.01520 -0.02983 -0.01708 AFIX 137 H02S 2 0.228490 0.575575 0.540500 11.00000 -1.50000 H02T 2 0.221641 0.501819 0.582034 11.00000 -1.50000 H02U 2 0.199576 0.573880 0.613069 11.00000 -1.50000 AFIX 0 HKLF 4 REM shelx_a.res in P2(1)/c REM wR2 = 0.2334, GooF = S = 0.993, Restrained GooF = 0.993 for all data REM R1 = 0.0859 for 8307 Fo > 4sig(Fo) and 0.1105 for all 12449 data REM 835 parameters refined using 0 restraints END WGHT 0.1222 0.0000 REM Highest difference peak 0.506, deepest hole -0.924, 1-sigma level 0.133 Q1 1 0.2427 0.4242 0.3724 11.00000 0.05 0.51 Q2 1 -0.1322 0.8791 0.0514 11.00000 0.05 0.51 Q3 1 0.4050 0.9163 0.6261 11.00000 0.05 0.50 Q4 1 -0.2715 0.7107 -0.0875 11.00000 0.05 0.49 Q5 1 0.0185 0.4991 0.3895 11.00000 0.05 0.48 Q6 1 0.7642 0.5509 1.0921 11.00000 0.05 0.48 Q7 1 0.4855 0.7557 0.6087 11.00000 0.05 0.46 Q8 1 0.1849 0.4527 0.5238 11.00000 0.05 0.46 Q9 1 -0.1190 0.8380 0.0969 11.00000 0.05 0.46 Q10 1 0.0569 0.5439 0.2793 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11.32 11 4 0 52.38 25.00 11 4 0 50.81 24.21 12 4 0 3.87 2.11 -12 -4 0 -3.94 40.74 12 -4 0 2.55 1.15 12 4 0 2.99 1.68 12 -4 0 3.82 1.40 12 4 0 3.31 1.97 -12 -4 0 3.15 1.18 12 4 0 3.38 1.91 12 4 0 3.66 1.41 13 4 0 3.40 1.53 -13 -4 0 10.58 40.55 13 -4 0 3.09 1.41 13 4 0 3.41 2.08 13 -4 0 3.88 1.50 13 4 0 3.67 2.37 -13 -4 0 4.30 1.54 13 4 0 4.00 1.63 13 4 0 3.69 1.37 14 4 0 922.60 47.53 14 -4 0 807.19 125.27 14 4 0 800.49 124.77 14 -4 0 888.15 137.96 14 4 0 831.54 137.21 14 4 0 880.68 142.40 14 4 0 778.61 142.15 14 4 0 883.41 143.32 15 4 0 2.95 1.47 15 -4 0 2.53 2.32 15 4 0 2.78 2.52 15 -4 0 2.97 2.21 15 4 0 2.26 2.61 15 4 0 2.01 2.74 15 4 0 2.07 1.91 15 4 0 2.31 2.37 15 4 0 2.92 1.33 16 4 0 10.32 5.10 16 -4 0 10.31 5.60 16 4 0 9.81 5.35 16 -4 0 10.79 5.65 16 4 0 9.22 4.95 16 4 0 9.68 5.15 16 4 0 9.51 4.87 16 4 0 9.17 5.01 16 4 0 10.71 5.27 17 4 0 8.21 2.99 17 -4 0 14.31 6.94 17 4 0 8.70 4.33 17 -4 0 10.09 4.00 17 4 0 7.40 3.34 17 -4 0 8.39 3.82 17 4 0 7.47 3.32 17 4 0 7.79 3.22 17 4 0 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181.67 59.50 -13 -5 0 136.48 71.46 13 -5 0 179.39 54.47 13 5 0 183.11 56.00 13 -5 0 198.40 60.33 13 5 0 198.86 60.78 -13 -5 0 177.23 5.55 13 -5 0 244.29 75.46 13 5 0 179.94 56.46 13 5 0 171.29 6.03 13 5 0 187.55 60.36 14 5 0 23.01 7.33 14 -5 0 22.15 6.95 14 5 0 19.75 6.24 14 -5 0 22.53 7.07 14 5 0 21.97 7.22 -14 -5 0 21.92 6.98 14 -5 0 26.57 3.74 14 5 0 22.50 7.40 14 5 0 19.58 6.66 14 5 0 21.85 6.95 15 5 0 82.22 13.94 15 -5 0 79.50 13.17 15 5 0 72.81 12.33 15 -5 0 75.89 12.74 15 5 0 76.46 13.89 15 -5 0 82.53 14.23 15 5 0 74.31 12.88 15 5 0 63.22 6.98 15 5 0 77.19 13.47 16 5 0 12.44 4.21 16 -5 0 15.19 5.23 16 5 0 14.62 5.36 16 -5 0 12.48 4.22 16 5 0 12.20 3.44 16 -5 0 13.08 4.69 16 5 0 11.86 3.96 16 5 0 10.29 5.53 16 5 0 12.16 1.87 17 5 0 68.92 13.55 17 -5 0 86.36 16.93 17 5 0 75.64 14.92 17 -5 0 70.23 14.18 17 5 0 67.68 13.74 17 -5 0 73.97 15.11 17 5 0 65.66 13.27 17 5 0 61.01 12.74 17 5 0 65.95 12.82 18 5 0 10.77 4.60 18 -5 0 15.38 6.86 18 5 0 14.15 6.84 18 -5 0 13.07 5.58 18 5 0 11.98 5.73 18 -5 0 12.32 5.88 18 5 0 10.40 6.03 18 5 0 11.24 5.08 19 -5 0 82.12 23.99 19 5 0 91.77 26.90 19 -5 0 67.95 20.06 19 5 0 71.64 21.15 19 -5 0 69.69 21.26 19 5 0 66.09 19.46 -19 5 0 15.82 8.63 19 5 0 70.98 20.78 20 -5 0 4.63 3.67 20 5 0 5.20 4.76 20 5 0 4.05 4.16 20 -5 0 4.24 4.22 20 5 0 3.80 3.69 -20 5 0 1.71 6.62 20 5 0 4.17 3.28 21 5 0 16.72 7.38 21 5 0 13.08 5.98 21 -5 0 11.50 5.90 21 5 0 11.21 5.24 -21 5 0 2.47 8.42 21 5 0 13.34 5.50 22 5 0 10.11 7.57 22 5 0 8.91 6.58 22 -5 0 6.80 5.75 22 5 0 7.47 5.37 22 5 0 8.89 5.91 23 5 0 8.82 7.28 23 5 0 7.95 6.63 23 5 0 7.33 5.61 0 -6 0 10.40 30.35 1 -6 0 170.28 58.23 -1 -6 0 185.76 58.34 1 6 0 68.59 32.84 2 -6 0 -113.77 39.13 -2 -6 0 13.05 26.67 2 6 0 13.74 4.21 -3 -6 0 -0.31 22.19 3 6 0 1.98 1.40 -4 -6 0 0.38 19.56 4 6 0 0.42 1.16 -5 -6 0 332.99 91.76 5 6 0 321.67 81.54 5 -6 0 293.71 74.46 -6 -6 0 7.27 20.64 6 6 0 6.63 1.22 -6 -6 0 7.84 2.45 6 -6 0 13.76 4.28 6 6 0 6.62 1.16 7 6 0 167.28 42.52 -7 -6 0 151.38 52.14 7 6 0 148.91 37.85 7 6 0 126.92 32.21 -7 -6 0 166.30 42.21 7 -6 0 202.16 51.38 7 6 0 166.72 42.45 7 6 0 163.87 41.67 8 6 0 5.46 2.52 8 6 0 5.00 2.35 8 6 0 4.98 2.24 8 6 0 4.29 1.97 -8 -6 0 5.65 2.64 8 6 0 6.29 3.34 8 6 0 6.09 2.80 9 6 0 6.55 3.02 9 -6 0 7.60 3.14 9 6 0 6.93 2.98 9 6 0 7.35 3.19 -9 -6 0 6.80 3.05 9 -6 0 20.34 6.73 9 6 0 9.55 2.70 9 6 0 6.62 3.11 10 6 0 1.79 1.64 10 -6 0 1.11 0.84 10 6 0 1.39 1.25 10 -6 0 1.24 1.01 10 6 0 1.68 1.59 -10 -6 0 1.54 1.68 10 -6 0 2.19 2.06 10 6 0 2.65 2.35 10 6 0 2.19 1.92 11 6 0 543.16 171.58 -11 -6 0 454.77 160.98 11 -6 0 480.82 151.60 11 6 0 523.49 165.76 11 -6 0 580.90 183.08 11 6 0 639.88 201.78 -11 -6 0 562.49 177.77 11 -6 0 772.16 247.78 11 6 0 570.85 180.00 11 6 0 578.92 182.39 12 6 0 28.65 10.06 -12 -6 0 29.51 44.01 12 -6 0 30.75 10.08 12 6 0 31.23 10.35 12 -6 0 35.81 11.75 12 6 0 38.25 12.74 -12 -6 0 33.13 10.95 12 -6 0 48.06 15.95 12 6 0 33.29 11.05 12 6 0 31.57 10.63 12 6 0 34.82 11.68 13 6 0 458.78 84.70 13 -6 0 435.30 68.02 13 6 0 425.85 67.92 13 -6 0 487.35 76.62 13 6 0 508.36 85.65 -13 -6 0 432.60 69.04 13 -6 0 612.85 115.45 13 6 0 445.06 72.31 13 6 0 425.49 68.77 13 6 0 459.18 86.13 14 6 0 1.17 1.61 14 -6 0 1.94 1.56 14 6 0 1.14 1.98 14 -6 0 1.62 1.68 14 6 0 1.64 2.35 -14 -6 0 1.07 1.89 14 -6 0 1.30 2.57 14 6 0 1.48 1.68 14 6 0 1.75 2.44 14 6 0 2.06 1.48 15 6 0 6.35 3.41 15 -6 0 6.95 3.95 15 6 0 6.10 2.56 15 -6 0 6.39 3.46 15 6 0 5.72 2.53 15 -6 0 7.36 4.52 15 6 0 5.38 2.38 15 6 0 4.54 1.88 15 6 0 4.93 2.72 15 6 0 5.39 1.73 16 6 0 0.40 1.86 16 -6 0 1.48 2.45 16 6 0 0.37 3.38 16 -6 0 0.90 1.77 16 6 0 1.38 3.37 16 -6 0 0.06 3.19 16 6 0 0.13 2.27 -16 6 0 -1.01 3.93 16 6 0 0.60 2.14 16 6 0 1.51 3.55 16 6 0 0.73 1.84 17 6 0 16.56 6.69 17 -6 0 19.53 7.86 17 6 0 17.48 7.58 17 6 0 16.51 9.53 17 -6 0 17.58 8.03 17 6 0 14.21 6.09 -17 6 0 4.10 6.27 17 6 0 13.98 5.98 18 6 0 1.74 2.06 18 -6 0 2.71 2.62 18 6 0 0.61 4.24 18 6 0 1.28 4.55 18 -6 0 1.89 3.54 18 6 0 1.70 4.36 18 6 0 1.62 2.94 19 6 0 5.96 1.91 19 6 0 9.54 4.75 19 6 0 6.41 4.24 19 -6 0 7.73 3.66 19 6 0 5.82 4.55 19 6 0 6.81 2.84 20 6 0 0.83 3.93 20 6 0 0.80 3.91 20 -6 0 0.54 3.97 20 6 0 0.36 3.18 20 6 0 0.92 2.61 21 6 0 203.95 44.65 21 6 0 164.44 36.15 21 -6 0 138.62 40.06 21 6 0 140.01 30.93 21 6 0 160.28 34.98 22 6 0 25.42 11.22 22 6 0 21.82 11.80 22 6 0 17.72 9.77 22 6 0 21.07 11.20 23 6 0 38.59 14.66 23 6 0 36.32 13.91 23 6 0 29.41 12.14 23 6 0 32.82 12.35 24 6 0 3.63 4.71 24 6 0 2.70 2.86 0 -7 0 1.48 33.27 1 -7 0 0.43 32.20 -1 -7 0 3.95 33.15 2 -7 0 -44.97 28.79 -2 -7 0 86.87 51.82 2 7 0 38.39 12.19 -3 -7 0 15.65 24.34 3 7 0 13.17 3.99 -3 -7 0 16.03 4.94 4 7 0 119.45 30.98 -4 -7 0 138.85 51.33 4 7 0 152.56 39.04 -4 -7 0 173.25 44.06 4 7 0 123.45 31.48 5 7 0 8.54 2.64 -5 -7 0 11.54 25.05 5 7 0 9.80 3.07 -5 -7 0 11.82 3.55 5 -7 0 9.69 2.91 5 7 0 8.86 2.71 -6 -7 0 55.90 37.62 6 7 0 48.38 20.66 -6 -7 0 58.43 24.90 -7 -7 0 302.85 50.43 7 7 0 259.85 21.48 7 7 0 242.05 19.84 -7 -7 0 315.49 26.27 7 7 0 215.24 18.55 7 7 0 332.48 27.66 8 7 0 2204.02 185.79 -8 -7 0 1893.12 179.20 8 7 0 2033.07 164.44 8 7 0 1780.25 144.11 -8 -7 0 2031.28 164.96 8 -7 0 1265.76 421.32 8 -7 0 2654.83 235.00 8 7 0 2378.73 192.55 8 7 0 2083.68 171.20 9 7 0 9.91 2.44 -9 -7 0 8.09 34.61 9 7 0 9.13 2.18 9 7 0 9.30 2.23 -9 -7 0 10.41 2.62 9 -7 0 5.93 2.21 9 -7 0 12.86 4.33 9 7 0 10.61 2.74 9 7 0 11.40 3.26 9 7 0 9.30 2.39 10 7 0 178.80 55.51 -10 -7 0 144.12 66.49 10 -7 0 110.28 38.54 10 7 0 158.31 49.12 10 7 0 176.08 54.61 -10 -7 0 188.37 5.78 10 -7 0 225.91 72.30 10 7 0 196.13 61.90 10 7 0 204.73 64.52 10 7 0 181.38 4.76 11 7 0 316.50 96.05 11 -7 0 260.00 78.83 11 7 0 274.26 83.19 11 7 0 332.56 100.80 -11 -7 0 321.79 97.78 11 -7 0 418.52 129.50 11 7 0 347.76 105.68 11 7 0 315.08 95.61 12 7 0 1.05 1.30 12 -7 0 0.80 0.94 12 7 0 0.26 1.71 12 7 0 0.81 2.20 -12 -7 0 0.14 1.84 12 -7 0 0.19 2.41 12 7 0 0.44 2.44 12 7 0 0.94 1.43 13 7 0 15.41 4.95 13 -7 0 14.24 4.50 13 7 0 14.05 4.70 13 7 0 18.13 6.10 -13 -7 0 15.04 4.98 13 -7 0 21.25 7.20 13 7 0 14.78 5.14 13 7 0 15.77 5.36 14 7 0 118.27 21.25 14 -7 0 118.23 19.32 14 7 0 114.43 18.89 14 7 0 134.27 23.34 -14 -7 0 123.07 20.37 14 -7 0 157.36 27.56 14 7 0 113.92 18.93 14 7 0 122.03 20.63 14 7 0 120.39 22.53 15 7 0 17.82 5.66 15 -7 0 21.24 6.51 15 7 0 19.24 6.06 15 7 0 21.02 6.85 -15 -7 0 19.27 6.19 15 -7 0 26.22 9.96 15 7 0 17.92 5.77 15 7 0 19.45 10.03 15 7 0 19.95 6.30 16 7 0 10.43 3.73 16 -7 0 10.21 3.61 16 7 0 9.83 4.23 16 7 0 10.63 4.84 16 -7 0 10.68 4.76 16 7 0 9.19 3.92 16 7 0 8.47 3.49 16 7 0 9.95 4.65 16 7 0 9.50 3.60 17 7 0 33.52 10.60 17 7 0 34.58 11.24 17 7 0 33.56 11.79 17 -7 0 35.76 12.01 17 7 0 30.12 9.88 17 7 0 29.47 4.23 17 7 0 32.47 10.26 18 7 0 165.36 27.59 18 7 0 191.34 31.66 18 7 0 168.38 28.33 18 -7 0 166.33 35.56 18 7 0 147.56 25.12 18 7 0 153.19 26.94 18 7 0 160.49 26.42 19 7 0 188.48 19.20 19 7 0 254.41 25.43 19 7 0 210.42 22.22 19 -7 0 191.15 35.30 19 7 0 191.49 20.66 19 7 0 189.85 20.99 20 7 0 12.24 6.02 20 7 0 9.34 3.85 20 7 0 9.00 3.34 20 7 0 9.54 3.03 21 7 0 1.14 4.22 21 7 0 1.24 3.55 21 7 0 0.47 3.76 21 7 0 1.45 2.78 22 7 0 132.16 23.37 22 7 0 118.77 21.12 22 7 0 96.64 17.29 22 7 0 113.58 20.03 23 7 0 43.62 6.32 23 7 0 43.21 6.48 23 7 0 33.65 14.13 23 7 0 38.98 16.17 24 7 0 5.10 5.20 24 7 0 3.77 4.77 0 8 0 477.74 11.40 0 -8 0 595.37 62.79 0 8 0 484.29 12.22 1 8 0 6.32 1.14 1 -8 0 2.33 29.24 -1 -8 0 8.43 29.89 1 -8 0 11.98 5.19 1 8 0 7.08 1.70 2 8 0 314.03 79.70 -2 -8 0 400.56 52.65 2 -8 0 490.99 13.07 2 8 0 337.32 85.54 3 8 0 1.73 1.21 -3 -8 0 4.13 29.97 3 8 0 0.80 0.40 -3 -8 0 2.48 2.02 3 -8 0 3.32 1.09 3 8 0 1.43 1.57 4 8 0 1272.48 116.54 -4 -8 0 1381.32 179.45 4 8 0 951.53 77.97 -4 -8 0 1677.77 222.08 4 -8 0 1497.90 130.86 4 8 0 1291.50 110.20 5 8 0 0.67 1.32 -5 -8 0 4.36 36.21 5 8 0 0.72 1.05 -5 -8 0 1.28 1.47 5 8 0 0.01 0.80 5 8 0 0.51 1.24 6 8 0 10.05 3.40 -6 -8 0 5.51 32.51 6 8 0 5.64 2.44 6 8 0 4.20 1.76 -6 -8 0 6.06 2.75 6 -8 0 3.65 1.98 6 8 0 0.00 0.76 -7 -8 0 -2.11 33.34 7 8 0 0.64 0.90 -7 -8 0 0.27 1.25 7 -8 0 0.26 0.80 7 8 0 0.18 1.57 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1057.66 244.23 15 8 0 5.13 1.99 15 8 0 4.44 2.30 15 8 0 5.33 2.64 -15 -8 0 3.96 2.71 15 -8 0 5.06 4.21 15 8 0 5.21 2.33 15 8 0 5.58 3.48 15 8 0 4.79 2.16 16 8 0 275.32 38.68 16 8 0 266.44 34.86 16 8 0 277.16 37.58 16 8 0 252.21 33.10 16 8 0 234.68 32.31 16 8 0 260.28 37.82 17 8 0 0.86 2.17 17 8 0 0.83 3.09 17 8 0 0.25 3.95 17 8 0 0.55 3.05 17 8 0 0.49 2.59 17 8 0 0.68 2.08 18 8 0 121.68 20.38 18 8 0 133.35 22.21 18 8 0 119.55 20.19 18 8 0 106.12 31.10 18 8 0 107.81 31.89 18 8 0 113.50 5.43 19 8 0 1.65 2.15 19 8 0 2.64 3.67 19 8 0 2.16 3.52 19 8 0 1.69 3.12 19 8 0 2.06 2.91 20 8 0 84.21 18.97 20 8 0 69.59 15.72 20 8 0 61.71 14.03 20 8 0 66.06 14.97 21 8 0 2.08 4.02 21 8 0 1.52 3.41 21 8 0 0.74 3.24 21 8 0 1.04 2.94 22 8 0 33.38 12.89 22 8 0 29.67 11.45 22 8 0 25.54 10.77 22 8 0 29.46 11.31 23 8 0 -0.17 3.31 23 8 0 -0.08 2.94 24 8 0 86.60 20.70 24 8 0 72.70 17.68 0 9 0 0.23 0.59 0 -9 0 25.42 148.10 0 -9 0 -0.01 1.26 1 9 0 294.60 25.07 -1 9 0 287.43 24.78 1 -9 0 598.77 164.88 -1 -9 0 395.53 117.63 1 -9 0 552.06 46.20 1 9 0 316.17 27.59 -1 9 0 319.64 27.71 2 9 0 164.83 6.90 -2 9 0 170.26 5.68 -2 -9 0 240.71 76.88 2 -9 0 300.63 26.62 2 9 0 171.44 4.85 -2 9 0 186.27 15.67 3 9 0 28.42 9.02 -3 9 0 28.93 9.19 -3 -9 0 22.26 46.42 -3 -9 0 45.41 20.24 3 -9 0 40.00 17.56 3 9 0 29.31 9.41 -3 9 0 30.86 9.85 4 9 0 915.12 92.48 -4 -9 0 932.46 119.80 -4 -9 0 1146.68 139.93 4 -9 0 1129.85 113.73 4 9 0 931.96 86.54 5 9 0 24.46 7.16 -5 -9 0 26.08 42.28 5 9 0 6.94 1.42 -5 -9 0 24.44 7.15 5 -9 0 23.03 6.65 5 -9 0 18.06 5.31 5 9 0 -0.05 0.65 5 9 0 23.79 6.94 6 9 0 112.60 53.16 -6 -9 0 90.99 63.70 6 9 0 77.37 36.12 -6 -9 0 108.97 50.89 6 -9 0 78.23 39.42 6 9 0 0.00 0.79 6 9 0 107.88 50.37 7 9 0 26.45 7.60 -7 -9 0 16.56 48.83 7 9 0 19.43 5.57 -7 -9 0 24.74 7.11 7 -9 0 16.91 6.09 7 9 0 0.14 0.98 -8 -9 0 37.22 49.47 8 9 0 38.79 11.68 -8 -9 0 44.67 13.54 8 -9 0 25.28 12.48 8 9 0 27.97 8.97 -9 -9 0 86.87 63.55 9 9 0 86.92 31.54 -9 -9 0 101.20 36.65 9 -9 0 40.53 19.76 9 9 0 127.35 46.13 9 9 0 114.70 41.71 9 9 0 111.48 40.43 10 9 0 96.43 34.93 -10 -9 0 70.51 63.23 10 9 0 83.31 30.18 10 9 0 77.03 28.09 -10 -9 0 89.69 32.53 10 9 0 98.99 35.88 10 9 0 114.31 41.55 10 9 0 92.66 33.64 11 9 0 65.13 19.40 11 9 0 57.10 17.87 11 9 0 60.70 2.82 -11 -9 0 66.32 19.69 11 9 0 68.46 20.34 11 9 0 80.09 23.89 11 9 0 66.23 19.65 12 9 0 37.14 11.12 12 9 0 33.89 9.95 12 9 0 36.76 11.00 -12 -9 0 39.65 11.90 12 9 0 39.93 11.93 12 9 0 45.52 13.88 12 9 0 37.60 11.25 13 9 0 40.72 14.20 13 9 0 36.08 12.61 13 9 0 39.95 14.10 -13 -9 0 43.80 3.30 13 9 0 48.79 18.17 13 9 0 42.07 14.72 14 9 0 11.96 4.31 14 9 0 10.24 3.79 14 9 0 11.38 4.51 -14 -9 0 12.34 4.56 14 9 0 11.93 4.56 15 9 0 29.07 3.05 15 9 0 29.30 3.11 15 9 0 32.21 10.46 -15 -9 0 28.46 10.62 15 9 0 29.83 9.58 16 9 0 107.05 26.56 16 9 0 101.93 24.85 16 9 0 101.03 24.80 16 9 0 96.68 23.81 16 9 0 97.57 24.63 17 9 0 1.59 2.32 17 9 0 1.01 2.95 17 9 0 0.57 3.37 17 9 0 -0.03 2.85 17 9 0 0.80 2.80 17 9 0 1.84 2.48 18 9 0 4.32 3.41 18 9 0 4.63 3.92 18 9 0 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4 -10 0 0.97 1.66 -4 10 0 0.63 1.27 5 10 0 181.11 36.05 -5 -10 0 146.37 84.92 -5 -10 0 178.59 40.85 5 -10 0 176.54 46.33 5 10 0 174.00 10.24 6 10 0 3.08 5.03 -6 -10 0 6.15 45.60 -6 -10 0 2.48 2.61 7 10 0 175.63 54.77 -7 -10 0 116.73 69.10 7 10 0 115.87 36.07 -7 -10 0 133.73 41.55 7 -10 0 81.30 27.94 7 10 0 0.06 0.89 7 10 0 165.88 51.67 -8 -10 0 -7.52 58.81 8 10 0 1.10 1.14 -8 -10 0 1.89 1.96 8 -10 0 1.12 0.87 8 10 0 -0.14 2.09 -9 -10 0 81.86 66.83 9 10 0 88.42 26.06 -9 -10 0 101.63 30.01 9 -10 0 37.55 18.65 9 10 0 131.18 4.58 9 10 0 98.23 29.40 10 10 0 1.80 1.56 -10 -10 0 2.20 3.67 10 -10 0 0.71 0.80 10 10 0 2.62 2.83 10 10 0 2.61 3.67 10 10 0 2.43 2.23 11 10 0 31.91 9.52 11 10 0 25.29 7.55 -11 -10 0 28.89 8.72 11 10 0 31.70 9.51 11 10 0 39.07 12.04 11 10 0 32.29 9.69 12 10 0 19.84 6.20 12 10 0 19.34 5.99 -12 -10 0 21.73 2.82 12 10 0 21.71 2.91 12 10 0 21.58 2.74 13 10 0 16.87 7.69 13 10 0 16.30 7.36 13 10 0 15.53 7.14 -13 -10 0 17.41 8.06 13 10 0 17.32 8.04 13 10 0 17.43 7.97 14 10 0 5.29 3.36 14 10 0 5.08 3.00 14 10 0 4.50 5.30 -14 -10 0 5.07 3.77 14 10 0 5.73 3.82 14 10 0 5.14 3.66 15 10 0 210.28 68.76 15 10 0 224.18 72.79 15 10 0 205.56 66.85 -15 -10 0 208.33 67.71 15 10 0 218.97 71.60 16 10 0 2.06 2.51 16 10 0 1.96 2.70 16 10 0 2.24 2.87 -16 -10 0 1.72 3.73 16 10 0 2.18 2.50 17 10 0 40.02 18.09 17 10 0 49.34 13.61 17 10 0 41.65 17.99 17 10 0 42.17 18.29 17 10 0 43.30 18.71 18 10 0 15.98 6.74 18 10 0 20.74 9.18 18 10 0 16.89 6.74 18 10 0 16.09 6.49 18 10 0 16.33 6.58 18 10 0 17.75 7.83 19 10 0 38.57 14.04 19 10 0 48.19 17.60 19 10 0 38.48 14.23 19 10 0 36.14 13.30 19 10 0 36.72 13.47 19 10 0 38.64 14.03 20 10 0 1.66 2.16 20 10 0 3.23 3.67 20 10 0 2.80 3.38 20 10 0 2.40 3.12 20 10 0 2.72 3.10 21 10 0 13.51 7.10 21 10 0 13.23 7.35 21 10 0 12.12 6.36 21 10 0 13.53 7.20 22 10 0 1.74 3.16 22 10 0 0.99 3.06 22 10 0 1.07 2.91 23 10 0 3.52 4.29 23 10 0 5.16 5.07 23 10 0 2.77 3.51 0 11 0 0.17 0.74 0 -11 0 1.58 1.78 0 11 0 0.82 0.92 1 11 0 20.57 6.30 -1 11 0 21.60 6.61 -1 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93.16 19.84 -11 -11 0 108.58 22.57 11 11 0 120.60 25.08 11 11 0 118.98 24.83 12 11 0 45.98 15.91 12 11 0 37.71 13.00 -12 -11 0 43.98 15.41 12 11 0 46.70 16.22 12 11 0 46.73 16.22 13 11 0 24.48 9.04 13 11 0 21.10 7.74 -13 -11 0 24.58 9.25 13 11 0 23.81 8.90 13 11 0 26.30 9.71 14 11 0 212.10 68.94 14 11 0 176.69 5.69 -14 -11 0 201.87 66.30 14 11 0 201.44 65.44 14 11 0 212.24 68.95 15 11 0 3.69 2.87 15 11 0 3.42 2.94 -15 -11 0 3.70 3.55 15 11 0 3.27 3.59 15 11 0 3.40 3.32 16 11 0 4.47 3.81 16 11 0 2.90 2.83 -16 -11 0 3.08 4.76 16 11 0 3.94 3.05 17 11 0 30.01 3.84 17 11 0 25.72 11.04 17 11 0 26.41 11.44 17 11 0 28.51 12.20 18 11 0 30.49 15.62 18 11 0 28.44 14.61 18 11 0 28.11 14.46 18 11 0 29.87 15.26 19 11 0 37.82 15.70 19 11 0 35.76 14.98 19 11 0 31.53 13.19 19 11 0 33.66 14.11 19 11 0 35.63 14.77 20 11 0 15.66 7.70 20 11 0 18.02 7.97 20 11 0 16.46 7.28 20 11 0 15.98 8.08 21 11 0 10.19 8.52 21 11 0 8.94 7.43 21 11 0 9.53 7.89 22 11 0 23.43 7.92 22 11 0 18.07 10.54 22 11 0 20.19 6.90 0 12 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0 75.32 22.36 -2 13 0 95.71 28.31 3 13 0 13.09 4.25 -3 13 0 14.68 4.74 3 -13 0 21.43 7.10 3 13 0 13.02 4.18 -3 13 0 14.65 5.02 4 13 0 24.89 7.63 -4 13 0 25.38 7.61 4 -13 0 30.38 11.82 4 13 0 21.83 6.58 -4 13 0 4.36 2.84 5 13 0 -0.07 2.04 -5 -13 0 0.20 1.96 5 -13 0 0.49 2.43 5 13 0 0.12 2.05 6 13 0 66.49 11.97 -6 -13 0 53.40 16.87 6 -13 0 44.79 20.96 6 13 0 58.38 17.53 7 13 0 117.43 26.19 -7 -13 0 82.08 29.83 7 -13 0 65.36 36.24 7 13 0 101.36 21.78 8 13 0 459.00 101.61 -8 -13 0 323.28 79.46 8 -13 0 205.04 101.97 8 13 0 429.46 94.38 8 13 0 428.34 97.34 9 13 0 0.43 4.46 -9 -13 0 1.78 2.56 9 -13 0 0.08 1.49 9 13 0 0.06 5.34 9 13 0 0.91 5.13 -10 -13 0 336.38 61.77 10 13 0 397.61 73.01 -11 -13 0 1.24 2.78 11 13 0 1.38 3.60 -12 -13 0 36.15 11.75 12 13 0 44.83 4.07 12 13 0 45.19 3.97 13 13 0 225.64 37.16 13 13 0 194.18 31.74 -13 -13 0 179.91 29.51 13 13 0 218.43 35.77 13 13 0 226.98 37.43 14 13 0 4.12 3.48 14 13 0 3.68 2.91 -14 -13 0 4.25 3.38 14 13 0 4.22 3.56 14 13 0 4.36 3.85 15 13 0 64.86 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14 -3 61.16 19.11 12 14 -3 51.85 14.83 -12 -14 3 34.21 12.65 12 -14 -3 10.46 3.57 12 14 -3 37.99 14.22 12 14 -3 48.42 14.40 11 14 -3 1.49 3.41 -11 -14 3 2.69 2.52 11 14 -3 2.46 2.29 11 14 -3 1.20 3.84 10 14 -3 15.97 6.93 -10 -14 3 15.30 7.24 10 -14 -3 6.52 3.70 10 14 -3 12.41 5.32 10 14 -3 14.84 6.66 9 14 -3 413.24 63.23 9 -14 -3 211.70 102.75 9 14 -3 346.39 55.70 9 14 -3 397.59 63.55 8 14 -3 1.89 2.59 -8 14 3 0.88 2.79 8 -14 -3 0.47 2.61 8 14 -3 1.95 1.97 8 14 -3 2.26 2.72 7 14 -3 492.53 95.58 -7 14 3 462.59 96.89 -7 -14 3 588.24 126.72 7 -14 -3 460.27 104.99 7 14 -3 511.90 101.77 7 14 -3 485.67 91.39 -7 14 3 243.30 45.04 6 14 -3 0.65 2.81 -6 14 3 0.39 2.52 -6 -14 3 1.34 2.84 6 -14 -3 0.99 3.11 6 14 -3 0.44 2.10 6 14 -3 0.67 3.15 -6 14 3 0.23 3.03 5 14 -3 206.35 47.14 -5 14 3 241.27 52.70 -5 -14 3 236.98 58.47 5 -14 -3 234.31 56.70 5 14 -3 252.02 55.23 5 14 -3 215.38 47.17 -5 14 3 241.03 59.24 4 14 -3 0.24 2.54 -4 -14 3 0.10 2.70 4 14 -3 -0.02 3.57 3 14 -3 4.03 2.45 -3 14 3 4.29 1.74 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1.67 14.66 5 11 4 2.09 1.47 -5 -11 -4 3.45 2.28 5 11 4 3.05 2.33 6 11 4 68.98 12.00 6 11 4 67.01 11.58 -6 -11 -4 80.28 14.33 6 11 4 84.51 14.49 6 11 4 73.05 12.62 7 11 4 4.95 3.56 7 11 4 2.81 2.47 -7 -11 -4 3.33 3.17 7 11 4 5.27 3.80 8 11 4 289.16 63.33 8 11 4 261.32 57.74 -8 -11 -4 357.37 80.58 8 11 4 321.88 70.36 8 11 4 272.60 60.19 9 11 4 62.33 22.65 9 11 4 55.72 20.35 9 11 4 52.62 18.97 -9 -11 -4 70.46 26.14 9 11 4 61.95 22.43 9 11 4 55.17 19.98 10 11 4 171.35 8.14 10 11 4 165.37 34.91 10 11 4 159.52 33.92 -10 -11 -4 163.56 37.70 10 11 4 167.50 35.55 10 11 4 161.42 34.39 11 11 4 72.41 18.60 11 11 4 67.37 17.15 11 11 4 70.26 17.42 -11 -11 -4 21.73 8.60 11 11 4 71.54 17.80 11 11 4 71.74 17.82 12 11 4 13.33 7.81 12 11 4 12.58 7.27 12 11 4 13.67 8.10 -12 -11 -4 3.95 2.21 12 11 4 14.02 8.32 12 11 4 13.42 8.08 12 11 4 13.95 8.15 13 11 4 3.75 2.30 13 11 4 3.17 2.57 13 11 4 3.72 3.11 13 11 4 4.55 3.06 13 11 4 3.34 3.84 13 11 4 4.64 2.48 14 11 4 184.40 20.20 14 11 4 166.94 16.65 14 11 4 167.55 17.06 14 11 4 173.17 17.71 14 11 4 182.25 18.91 14 11 4 192.54 19.83 15 11 4 53.56 14.03 15 11 4 49.79 12.77 15 11 4 46.73 12.04 15 11 4 41.98 10.83 15 11 4 51.12 13.30 15 11 4 54.95 14.36 15 11 4 52.64 13.44 16 11 4 45.67 16.47 16 11 4 47.73 17.26 16 11 4 43.88 15.94 16 11 4 39.90 14.52 16 11 4 48.43 17.57 17 11 4 0.23 2.86 17 11 4 0.03 2.69 17 11 4 -0.04 2.27 17 11 4 0.22 2.61 18 11 4 32.41 12.38 18 11 4 24.39 10.07 18 11 4 22.76 9.39 18 11 4 27.33 11.18 19 11 4 1.02 3.00 19 11 4 1.58 2.48 19 11 4 1.38 2.47 20 11 4 17.78 10.41 20 11 4 14.58 8.67 22 12 -4 0.07 2.05 22 12 -4 -0.06 1.83 22 12 -4 0.01 2.65 22 12 -4 0.03 1.96 21 12 -4 0.25 2.25 21 12 -4 0.42 2.22 21 12 -4 0.52 2.70 21 12 -4 0.53 2.22 20 12 -4 10.11 6.97 20 12 -4 9.44 6.41 20 12 -4 11.43 5.84 20 12 -4 11.70 5.79 19 12 -4 17.43 9.51 19 12 -4 16.06 8.59 19 12 -4 20.19 10.87 19 12 -4 19.23 10.29 18 12 -4 156.97 40.02 18 12 -4 158.25 34.81 18 12 -4 197.22 43.56 18 12 -4 189.92 42.34 17 12 -4 0.48 2.31 17 12 -4 0.15 3.20 17 12 -4 0.81 2.67 16 -12 -4 4.98 3.04 16 12 -4 30.72 13.31 16 12 -4 36.16 15.80 16 12 -4 37.97 16.81 -15 -12 4 0.75 2.17 15 12 -4 1.39 2.69 14 12 -4 18.42 7.83 -14 -12 4 11.98 7.04 14 -12 -4 2.83 1.54 14 12 -4 13.60 8.06 13 12 -4 38.32 12.47 -13 -12 4 27.51 10.04 13 -12 -4 8.16 4.96 13 12 -4 28.36 10.57 13 12 -4 36.77 12.18 12 12 -4 11.54 5.16 -12 -12 4 9.50 3.53 12 -12 -4 3.20 2.02 12 12 -4 8.46 3.49 12 12 -4 10.78 4.58 11 12 -4 1.26 2.24 -11 -12 4 1.14 2.48 11 -12 -4 0.38 0.93 11 12 -4 0.89 1.65 11 12 -4 1.15 2.51 10 12 -4 128.07 30.07 10 -12 -4 65.29 34.71 10 12 -4 107.37 24.38 10 12 -4 123.65 31.42 9 12 -4 0.52 1.81 9 -12 -4 0.26 0.97 9 12 -4 0.36 1.57 9 12 -4 0.52 2.06 -9 12 4 0.22 1.48 8 12 -4 6.10 3.61 8 -12 -4 4.00 2.42 8 12 -4 5.87 3.50 8 12 -4 5.45 3.42 -8 12 4 3.08 1.79 7 12 -4 -0.01 1.53 -7 -12 4 0.83 2.78 7 -12 -4 0.08 1.10 7 12 -4 -0.03 1.59 7 12 -4 0.13 1.86 -7 12 4 -0.12 1.81 6 12 -4 150.56 24.44 -6 -12 4 187.99 31.35 6 -12 -4 126.38 37.12 6 12 -4 205.79 32.44 6 12 -4 160.93 25.47 -6 12 4 170.65 26.87 5 12 -4 2.89 1.99 -5 -12 4 3.40 1.86 5 -12 -4 2.88 1.35 5 12 -4 3.40 2.49 -5 12 4 2.79 1.57 4 12 -4 57.02 18.04 -4 -12 4 47.56 15.22 4 12 -4 66.28 19.86 -4 12 4 50.07 15.69 3 12 -4 5.63 3.45 -3 -12 4 4.20 1.60 3 12 -4 4.98 3.07 -3 12 4 4.25 1.50 2 12 -4 4.78 2.48 -2 12 4 3.95 1.69 -2 -12 4 3.22 1.56 2 -12 -4 3.29 1.48 2 12 -4 1.20 2.91 -2 12 4 2.98 1.52 1 12 -4 0.23 1.57 -1 12 4 1.92 1.75 -1 -12 4 1.82 1.39 1 -12 -4 1.59 1.65 1 12 -4 -0.18 1.43 -1 12 4 1.65 1.75 0 12 4 20.65 6.55 0 -12 4 13.00 6.42 0 -12 -4 20.53 6.61 0 12 4 19.86 6.35 1 12 4 5.88 4.32 1 -12 4 3.28 1.83 -1 -12 -4 6.58 4.12 1 12 4 5.66 4.08 2 12 4 58.75 18.53 2 12 4 56.75 17.73 2 -12 4 38.42 18.35 -2 -12 -4 60.01 19.28 2 12 4 76.62 22.74 3 12 4 0.41 1.72 3 12 4 0.24 1.44 -3 -12 -4 0.29 2.16 3 12 4 1.25 2.44 4 12 4 61.94 18.16 -4 -12 -4 63.83 6.17 5 12 4 2.64 1.81 -5 -12 -4 3.50 3.15 6 12 4 285.70 63.15 6 12 4 273.17 60.51 -6 -12 -4 298.34 67.02 7 12 4 24.89 8.93 7 12 4 22.68 8.15 -7 -12 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0.21 1.25 -1 13 4 60.96 18.44 0 13 4 164.99 52.21 0 -13 4 117.79 35.52 0 -13 -4 176.52 57.00 0 13 4 174.67 55.27 1 13 4 368.80 116.84 1 -13 4 266.37 109.02 -1 -13 -4 376.55 120.76 1 13 4 400.08 126.25 2 13 4 1.26 2.21 2 -13 4 0.98 1.51 -2 -13 -4 1.16 2.74 2 13 4 1.68 3.41 -3 -13 -4 -0.24 2.61 4 13 4 463.08 103.66 4 13 4 417.97 91.33 -4 -13 -4 406.79 95.02 4 13 4 507.84 113.46 5 13 4 58.13 20.85 -5 -13 -4 55.11 20.58 6 13 4 40.66 14.00 -6 -13 -4 38.90 14.08 7 13 4 55.65 11.49 7 13 4 49.35 9.78 -7 -13 -4 52.67 11.17 7 13 4 51.97 10.49 8 13 4 4.82 2.56 8 13 4 4.43 4.63 -8 -13 -4 5.40 3.71 8 13 4 4.80 3.28 8 13 4 5.14 3.72 9 13 4 29.38 9.95 9 13 4 27.49 9.11 -9 -13 -4 35.58 12.12 9 13 4 34.71 11.66 9 13 4 29.26 9.86 10 13 4 5.89 2.84 10 13 4 5.87 2.66 -10 -13 -4 6.31 4.66 10 13 4 6.03 3.28 10 13 4 7.45 3.40 10 13 4 5.40 2.55 11 13 4 0.25 2.59 11 13 4 0.19 2.46 -11 -13 -4 0.12 3.90 11 13 4 0.22 2.43 12 13 4 -0.12 2.38 12 13 4 0.08 2.64 -12 -13 -4 -0.63 2.96 12 13 4 -0.13 2.52 13 13 4 5.92 3.43 13 13 4 5.10 4.02 -13 -13 -4 0.89 1.71 13 13 4 6.05 3.53 14 13 4 55.56 20.03 14 13 4 53.54 19.30 14 13 4 51.85 18.70 14 13 4 58.04 20.88 15 13 4 1.65 2.22 15 13 4 1.40 2.83 15 13 4 1.43 2.63 15 13 4 1.19 2.42 15 13 4 1.32 2.09 16 13 4 3.77 2.56 16 13 4 3.58 3.07 16 13 4 3.24 2.93 16 13 4 3.64 2.99 17 13 4 6.91 4.33 17 13 4 6.28 3.84 17 13 4 6.76 4.09 18 13 4 -0.14 2.65 18 13 4 -0.07 2.16 18 13 4 0.15 2.28 20 14 -4 1.02 2.05 20 14 -4 0.92 1.77 20 14 -4 0.70 2.50 20 14 -4 0.81 1.99 19 14 -4 111.25 14.58 19 14 -4 100.91 11.79 19 14 -4 123.79 14.56 19 14 -4 118.37 13.97 18 14 -4 10.37 5.43 18 14 -4 10.41 5.15 18 14 -4 12.25 6.23 18 14 -4 12.73 6.23 17 14 -4 0.74 2.03 17 14 -4 0.71 2.69 17 14 -4 1.15 2.84 16 14 -4 4.59 3.04 16 14 -4 5.99 5.22 15 14 -4 124.58 18.65 -15 -14 4 78.74 10.88 15 -14 -4 19.77 10.20 15 14 -4 98.59 14.34 14 14 -4 2.96 3.08 -14 -14 4 1.50 1.94 14 -14 -4 0.45 0.66 14 14 -4 1.96 2.58 14 14 -4 2.15 2.96 13 14 -4 17.63 7.46 -13 -14 4 11.17 6.13 13 -14 -4 3.13 1.81 13 14 -4 11.81 6.55 13 14 -4 15.16 6.62 12 14 -4 0.56 3.09 -12 -14 4 0.11 2.36 12 -14 -4 0.07 1.02 12 14 -4 -0.18 2.06 12 14 -4 0.13 3.24 11 14 -4 174.68 13.57 11 -14 -4 64.00 27.56 11 14 -4 136.11 34.56 11 14 -4 159.73 42.38 10 14 -4 4.35 2.86 -10 14 4 3.23 2.64 10 -14 -4 1.84 1.43 10 14 -4 4.11 2.32 10 14 -4 4.27 3.03 9 14 -4 44.76 14.26 -9 14 4 39.09 12.57 9 -14 -4 26.85 11.65 9 14 -4 46.06 14.68 9 14 -4 43.84 14.81 8 14 -4 1.02 2.09 -8 14 4 0.12 2.75 -8 -14 4 1.52 2.96 8 -14 -4 0.40 1.66 8 14 -4 0.77 2.09 8 14 -4 1.20 2.40 -8 14 4 -0.39 2.55 7 14 -4 48.47 17.05 -7 14 4 55.15 10.87 -7 -14 4 62.36 12.63 7 -14 -4 46.92 16.27 7 14 -4 62.16 12.37 7 14 -4 52.03 11.43 -7 14 4 49.22 5.19 6 14 -4 5.47 2.11 -6 14 4 5.73 2.92 -6 -14 4 7.29 3.88 6 -14 -4 5.17 2.22 6 14 -4 6.40 2.76 -6 14 4 6.26 3.38 5 14 -4 227.87 42.10 -5 14 4 300.49 55.25 -5 -14 4 327.27 62.49 5 -14 -4 286.77 52.65 5 14 -4 354.95 65.18 -5 14 4 357.08 65.43 4 14 -4 1.43 3.00 -4 14 4 1.12 1.86 -4 -14 4 1.13 2.15 4 -14 -4 0.46 2.61 4 14 -4 1.34 3.92 -4 14 4 1.81 2.24 3 14 -4 1.31 2.82 -3 14 4 1.16 1.85 -3 -14 4 0.90 1.83 3 14 -4 0.38 3.84 -3 14 4 1.63 2.20 2 14 -4 -0.11 2.47 -2 14 4 -0.09 1.80 -2 -14 4 -0.01 1.61 2 14 -4 -0.75 2.07 -2 14 4 -0.43 2.23 -1 14 4 40.22 14.35 -1 -14 4 30.57 11.87 1 -14 -4 44.90 16.61 1 14 -4 -0.01 1.07 -1 14 4 44.81 16.48 0 14 4 0.59 2.40 0 -14 4 0.62 1.70 0 -14 -4 0.37 2.00 0 14 4 0.86 2.96 1 14 4 22.69 8.90 1 -14 4 17.28 6.86 -1 -14 -4 22.90 8.67 1 14 4 25.37 10.40 2 14 4 1.61 4.94 2 -14 4 1.19 1.67 -2 -14 -4 2.20 2.73 2 14 4 1.53 5.71 3 14 4 235.71 44.97 -3 -14 -4 193.38 40.96 3 14 4 249.00 48.41 4 14 4 28.92 11.77 -4 -14 -4 21.18 10.52 4 14 4 29.07 12.40 -5 -14 -4 6.26 3.52 5 14 4 7.56 5.49 6 14 4 1.97 1.93 -6 -14 -4 2.27 4.04 7 14 4 7.11 2.39 -7 -14 -4 6.65 3.17 8 14 4 14.56 8.51 8 14 4 13.31 7.77 -8 -14 -4 14.50 8.58 8 14 4 13.99 8.27 9 14 4 251.16 43.75 9 14 4 247.35 42.50 -9 -14 -4 288.29 50.25 9 14 4 240.54 41.01 10 14 4 0.14 2.46 10 14 4 -0.09 2.33 -10 -14 -4 0.48 4.53 10 14 4 0.11 2.93 10 14 4 0.56 2.96 11 14 4 46.41 20.02 11 14 4 46.88 3.55 -11 -14 -4 37.42 16.70 11 14 4 44.48 19.26 11 14 4 44.09 19.11 12 14 4 3.06 3.10 12 14 4 2.78 2.88 -12 -14 -4 0.92 3.37 12 14 4 2.97 3.09 13 14 4 63.65 14.31 13 14 4 61.73 13.76 -13 -14 -4 8.41 9.27 13 14 4 60.58 3.91 14 14 4 1.98 2.19 14 14 4 1.60 2.50 14 14 4 1.62 2.38 15 14 4 25.61 14.03 15 14 4 23.90 13.22 15 14 4 20.79 11.53 15 14 4 22.87 12.65 15 14 4 23.89 13.15 16 14 4 3.89 4.50 16 14 4 3.39 3.96 16 14 4 3.53 4.08 17 14 4 32.82 10.57 17 14 4 25.82 8.43 17 14 4 29.33 9.49 19 15 -4 0.19 2.00 19 15 -4 0.17 1.68 19 15 -4 0.44 2.45 19 15 -4 0.24 2.07 18 15 -4 15.22 7.27 18 15 -4 18.38 8.88 18 15 -4 18.01 8.66 17 15 -4 14.91 7.27 17 15 -4 18.20 7.68 17 15 -4 18.60 7.85 16 15 -4 56.06 10.68 16 15 -4 44.20 12.23 16 15 -4 49.68 13.89 15 15 -4 3.55 2.69 -15 -15 4 2.47 1.75 15 15 -4 2.34 2.03 15 15 -4 2.87 2.36 15 15 -4 3.32 2.80 14 15 -4 33.84 12.50 -14 -15 4 21.10 10.76 14 -15 -4 6.49 5.02 14 15 -4 27.13 13.87 14 15 -4 32.22 12.19 13 15 -4 49.81 13.11 -13 -15 4 33.46 8.68 13 -15 -4 10.89 3.61 13 15 -4 37.50 9.78 13 15 -4 45.53 12.63 12 15 -4 1.80 2.95 -12 -15 4 1.36 2.13 12 -15 -4 0.20 0.94 12 15 -4 0.67 1.93 12 15 -4 0.73 2.88 11 15 -4 97.04 28.70 11 -15 -4 36.18 18.65 11 15 -4 87.08 25.73 11 15 -4 93.90 28.66 10 15 -4 158.72 27.83 10 -15 -4 81.66 35.89 10 15 -4 148.65 26.04 10 15 -4 148.40 27.88 9 15 -4 66.60 16.30 -9 15 4 53.43 12.56 -9 -15 4 73.04 16.83 9 -15 -4 38.99 17.16 9 15 -4 69.69 16.38 9 15 -4 63.29 15.64 8 15 -4 19.53 7.71 -8 15 4 15.67 6.36 -8 -15 4 25.47 9.92 8 -15 -4 14.82 8.41 8 15 -4 23.53 9.14 8 15 -4 20.00 8.23 -8 15 4 15.82 6.54 7 15 -4 11.01 4.73 -7 15 4 11.79 5.24 -7 -15 4 14.71 6.34 7 -15 -4 10.16 4.44 7 15 -4 12.32 5.30 -7 15 4 10.58 5.15 6 15 -4 86.47 22.47 -6 15 4 87.47 21.80 -6 -15 4 97.80 24.46 6 -15 -4 78.14 20.11 6 15 -4 95.25 4.56 -6 15 4 101.36 25.70 5 15 -4 343.59 44.95 -5 15 4 336.58 43.69 -5 -15 4 444.24 59.09 5 -15 -4 365.13 53.88 5 15 -4 482.70 62.62 -5 15 4 480.57 63.84 4 15 -4 22.24 9.79 -4 15 4 20.38 7.69 -4 -15 4 21.90 8.28 4 -15 -4 21.19 8.56 4 15 -4 26.76 10.53 -4 15 4 27.48 10.25 3 15 -4 45.37 14.51 -3 15 4 77.99 19.35 -3 -15 4 88.87 25.17 3 15 -4 60.05 15.75 -3 15 4 99.01 24.88 2 15 -4 32.71 20.47 -2 15 4 105.17 22.36 -2 -15 4 102.01 27.20 2 15 -4 -0.27 1.37 -2 15 4 129.84 27.61 -1 15 4 16.77 7.66 -1 -15 4 16.97 8.16 1 -15 -4 18.39 8.37 -1 15 4 19.04 8.75 0 15 4 16.50 7.07 0 -15 4 15.91 7.13 0 -15 -4 16.36 6.96 0 15 4 18.66 3.62 1 15 4 93.81 5.84 1 -15 4 72.41 21.23 -1 -15 -4 86.48 23.58 1 15 4 101.04 25.52 2 15 4 264.69 35.88 2 -15 4 153.91 44.95 -2 -15 -4 208.71 35.41 2 15 4 266.34 35.96 3 15 4 7.27 4.81 -3 -15 -4 4.42 4.82 3 15 4 7.62 4.74 4 15 4 66.44 17.01 -4 -15 -4 44.94 14.46 4 15 4 65.67 16.89 5 15 4 21.68 8.58 -5 -15 -4 14.25 8.19 5 15 4 20.91 8.41 -6 -15 -4 99.54 26.07 -7 -15 -4 13.55 6.11 8 15 4 45.92 12.95 -8 -15 -4 43.05 12.44 8 15 4 45.47 13.22 9 15 4 173.74 21.71 -9 -15 -4 186.42 22.06 9 15 4 185.74 23.31 9 15 4 171.72 20.86 10 15 4 130.20 19.59 10 15 4 127.20 17.37 -10 -15 -4 140.83 22.01 10 15 4 132.74 18.93 10 15 4 128.64 19.30 11 15 4 6.57 5.40 11 15 4 5.94 4.76 -11 -15 -4 6.92 6.36 11 15 4 7.23 6.01 11 15 4 6.21 5.24 12 15 4 67.98 13.73 12 15 4 74.88 13.05 -12 -15 -4 55.67 10.95 12 15 4 76.18 13.58 12 15 4 74.10 13.63 13 15 4 9.81 6.70 13 15 4 9.74 6.62 -13 -15 -4 2.44 2.46 13 15 4 10.15 2.70 14 15 4 52.97 19.55 14 15 4 49.91 18.42 14 15 4 50.30 18.60 15 15 4 6.31 3.79 15 15 4 5.04 4.47 15 15 4 5.71 4.83 16 15 4 24.05 7.87 16 15 4 26.97 8.80 18 16 -4 20.54 6.86 18 16 -4 19.75 6.60 17 16 -4 1.07 1.69 17 16 -4 1.15 1.98 16 16 -4 2.56 2.40 16 16 -4 2.04 1.62 16 16 -4 2.13 2.02 15 16 -4 6.69 5.07 15 16 -4 4.91 3.71 15 16 -4 5.43 4.17 15 16 -4 6.13 4.73 14 16 -4 6.78 4.68 -14 -16 4 4.09 2.70 14 16 -4 5.30 3.57 14 16 -4 5.97 4.44 13 16 -4 0.22 2.70 -13 -16 4 0.39 1.75 13 -16 -4 0.08 0.68 13 16 -4 0.08 1.92 13 16 -4 0.74 2.90 12 16 -4 263.25 59.04 -12 -16 4 194.98 42.99 12 -16 -4 73.94 28.36 12 16 -4 221.27 48.81 12 16 -4 240.68 56.00 11 16 -4 8.36 3.56 11 -16 -4 2.74 2.25 11 16 -4 7.84 3.97 11 16 -4 7.99 4.39 10 16 -4 15.16 6.02 10 -16 -4 6.70 4.51 10 16 -4 15.59 6.09 10 16 -4 13.54 7.53 9 16 -4 9.59 2.41 -9 16 4 8.90 5.56 -9 -16 4 12.53 7.12 9 -16 -4 6.85 4.35 9 16 -4 12.30 6.73 9 16 -4 10.55 6.00 8 16 -4 44.73 12.66 -8 16 4 39.32 11.13 -8 -16 4 53.48 14.66 8 -16 -4 31.45 12.98 8 16 -4 45.02 12.53 7 16 -4 5.72 2.22 -7 16 4 5.74 2.66 -7 -16 4 6.65 2.35 7 -16 -4 4.82 1.88 7 16 -4 5.95 2.67 -7 16 4 4.24 3.10 6 16 -4 19.65 7.66 -6 16 4 21.89 8.87 -6 -16 4 27.12 2.81 6 -16 -4 21.08 9.16 6 16 -4 25.19 9.76 -6 16 4 23.07 9.75 5 16 -4 1.97 2.23 -5 16 4 1.72 2.82 -5 -16 4 3.01 2.29 5 -16 -4 2.30 2.33 5 16 -4 3.20 2.88 -5 16 4 2.45 3.58 4 16 -4 141.98 38.07 -4 16 4 128.51 32.51 -4 -16 4 140.57 35.47 4 -16 -4 127.33 33.77 4 16 -4 143.31 34.98 -4 16 4 178.57 59.16 3 16 -4 0.15 3.49 -3 -16 4 0.48 2.54 3 16 -4 -1.47 4.36 -2 16 4 63.49 15.40 -2 -16 4 62.93 14.67 2 16 -4 -0.05 1.21 -2 16 4 80.84 20.99 -1 16 4 5.00 5.52 -1 -16 4 4.81 2.32 -1 16 4 6.66 5.01 0 16 4 9.20 3.22 0 -16 4 7.06 2.46 0 -16 -4 8.44 3.45 0 16 4 10.37 6.41 1 16 4 2.61 2.98 1 -16 4 2.04 1.80 -1 -16 -4 2.20 2.50 1 16 4 2.46 3.16 2 16 4 324.88 106.11 2 -16 4 193.93 66.26 -2 -16 -4 232.45 80.58 2 16 4 318.12 103.91 3 16 4 20.52 3.39 -3 -16 -4 12.64 2.54 3 16 4 18.65 8.35 4 16 4 25.77 9.76 -4 -16 -4 15.63 6.79 4 16 4 23.60 9.29 5 16 4 0.75 2.62 -5 -16 -4 0.00 1.79 5 16 4 0.82 2.92 6 16 4 8.89 5.79 -6 -16 -4 5.78 3.83 6 16 4 8.91 5.77 -7 -16 -4 0.90 2.20 -8 -16 -4 55.93 14.60 8 16 4 70.55 6.43 9 16 4 -0.01 2.46 -9 -16 -4 -0.19 2.70 9 16 4 -0.26 2.88 9 16 4 -0.75 2.76 10 16 4 60.83 5.53 -10 -16 -4 63.45 14.67 10 16 4 60.20 6.38 10 16 4 60.72 5.92 11 16 4 1.53 2.83 -11 -16 -4 0.66 2.82 11 16 4 1.11 2.83 11 16 4 0.70 2.86 12 16 4 52.73 10.02 -12 -16 -4 24.61 19.70 12 16 4 53.86 10.07 12 16 4 55.16 10.63 13 16 4 0.01 2.25 13 16 4 -0.41 2.49 13 16 4 0.04 2.37 14 16 4 0.30 1.98 14 16 4 0.45 2.07 15 16 4 0.96 1.86 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9.24 3.87 -6 4 -5 58.12 24.83 -6 -4 -5 39.54 1.99 6 -4 5 76.78 32.80 6 4 5 85.31 36.36 6 4 5 89.27 38.04 6 4 5 83.23 35.44 6 4 5 76.53 32.78 7 4 5 0.41 0.70 -7 4 -5 0.50 2.45 -7 -4 -5 0.67 0.88 7 -4 5 0.40 0.95 7 4 5 0.34 1.11 7 -4 5 1.13 1.28 7 4 5 0.24 2.24 7 4 5 0.04 2.13 7 4 5 0.55 0.88 8 4 5 4.99 1.39 -8 -4 -5 4.56 2.12 8 -4 5 5.22 1.67 8 4 5 5.12 1.56 8 -4 5 9.97 2.57 8 4 5 4.92 2.51 8 -4 5 4.02 1.25 8 4 5 4.73 2.19 -9 -4 -5 1.29 3.03 9 -4 5 2.35 1.30 9 4 5 3.13 1.79 9 -4 5 2.96 1.36 9 4 5 3.06 2.99 9 -4 5 1.40 1.26 9 4 5 2.86 2.28 -10 -4 -5 2.99 5.24 10 -4 5 3.96 1.51 10 4 5 4.40 2.70 10 -4 5 4.66 1.41 10 4 5 3.71 1.39 10 4 5 3.88 3.19 10 -4 5 2.38 1.57 10 4 5 3.27 2.28 11 -4 5 0.32 1.69 11 4 5 0.66 2.56 11 -4 5 0.72 1.16 11 -4 5 0.40 1.20 11 4 5 0.01 1.49 11 4 5 0.88 3.20 11 -4 5 0.45 1.43 12 -4 5 24.09 7.26 12 4 5 30.12 9.08 12 -4 5 21.22 6.44 12 -4 5 22.66 6.95 12 4 5 26.95 8.11 12 4 5 23.55 7.87 12 -4 5 17.35 7.05 13 -4 5 0.47 2.19 13 4 5 0.25 4.26 13 -4 5 0.48 1.51 13 -4 5 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5 -5 2.74 1.35 -8 5 5 2.97 1.36 7 5 -5 652.31 54.39 -7 -5 5 823.21 47.64 7 -5 -5 757.41 48.90 7 5 -5 690.92 77.47 7 -5 -5 714.05 23.89 -7 5 5 812.66 20.52 7 5 -5 1219.45 113.75 7 5 -5 601.63 64.65 6 5 -5 239.25 62.28 -6 -5 5 194.14 53.00 6 -5 -5 254.81 69.09 6 5 -5 197.68 60.89 -6 -5 5 380.12 27.07 6 -5 -5 309.32 78.45 6 -5 -5 222.67 56.58 -6 5 5 200.36 50.85 6 5 -5 222.05 62.10 -6 5 5 179.22 45.44 -5 -5 5 68.06 34.47 5 -5 -5 76.70 39.11 5 5 -5 62.99 37.26 5 -5 -5 117.68 29.92 5 -5 -5 80.04 38.37 -5 5 5 58.44 28.00 -5 5 5 64.95 31.10 -4 -5 5 9.61 5.55 4 5 -5 11.91 19.46 4 -5 -5 23.18 7.47 4 -5 -5 14.92 4.30 -4 5 5 12.68 3.61 3 5 -5 33.77 21.19 3 -5 -5 51.15 24.56 2 5 -5 675.68 76.12 2 -5 -5 1018.29 25.85 -2 -5 5 1161.94 50.33 1 5 -5 33.82 19.46 -1 -5 5 55.49 26.69 0 5 -5 458.50 38.18 -1 5 -5 59.82 31.74 1 5 5 85.10 40.77 1 -5 5 82.95 39.78 1 5 5 81.53 39.07 -2 5 -5 296.54 78.53 2 5 5 373.10 11.27 2 5 5 409.76 12.79 2 -5 5 441.71 12.35 2 5 5 406.20 11.69 2 5 5 392.35 10.96 3 5 5 2101.19 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42.26 13.45 8 -11 -5 19.34 5.90 8 11 -5 41.67 13.72 8 11 -5 30.19 10.39 -8 11 5 26.77 2.08 7 11 -5 10.81 3.70 -7 -11 5 12.75 4.47 7 -11 -5 6.35 3.37 7 11 -5 15.56 5.44 7 11 -5 12.49 4.32 -7 11 5 9.88 5.05 6 11 -5 1.62 1.70 -6 -11 5 1.20 2.37 6 11 -5 2.00 2.21 -6 11 5 0.96 1.45 5 11 -5 494.55 150.15 -5 -11 5 372.34 128.17 5 11 -5 678.92 206.06 -5 11 5 369.97 112.89 4 11 -5 2.27 2.95 -4 11 5 1.54 0.98 -4 -11 5 2.54 1.41 4 -11 -5 1.26 1.30 4 11 -5 2.04 4.35 -4 11 5 2.08 1.44 3 11 -5 16.90 9.45 -3 11 5 32.06 10.49 -3 -11 5 32.94 11.33 3 -11 -5 27.57 9.05 3 11 -5 7.23 2.50 -3 11 5 31.28 10.23 2 11 -5 1.60 1.42 -2 11 5 16.90 5.75 -2 -11 5 15.07 6.02 2 -11 -5 15.85 5.48 2 11 -5 0.83 1.72 -2 11 5 17.74 6.09 1 -11 -5 109.05 39.80 -1 11 5 147.63 53.45 -1 -11 5 119.17 48.96 1 -11 -5 147.13 53.64 -1 -11 5 107.62 39.08 -1 11 5 153.07 55.33 0 11 5 12.36 4.61 0 -11 -5 8.28 3.35 0 11 5 9.82 3.50 0 -11 5 6.69 2.04 0 -11 -5 10.32 3.83 0 -11 5 7.63 2.84 0 11 5 10.84 4.02 1 11 5 10.51 4.07 -1 -11 -5 7.66 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9.70 11 11 5 51.55 12.57 11 11 5 53.92 12.46 11 11 5 52.06 12.05 -11 -11 -5 9.82 6.18 11 11 5 57.11 13.40 11 11 5 50.48 11.83 11 11 5 53.48 12.48 12 11 5 19.15 8.61 12 11 5 16.97 7.35 12 11 5 16.87 7.47 12 11 5 19.70 8.59 12 11 5 16.28 7.37 12 11 5 17.77 7.81 13 11 5 22.95 8.67 13 11 5 22.68 8.67 13 11 5 23.91 9.26 13 11 5 23.28 9.05 13 11 5 23.42 9.42 13 11 5 23.21 8.83 14 11 5 17.87 7.79 14 11 5 17.40 7.76 14 11 5 16.85 6.85 14 11 5 17.94 8.16 14 11 5 18.35 8.73 14 11 5 17.02 6.55 15 11 5 0.95 2.72 15 11 5 1.32 2.84 15 11 5 1.15 2.47 15 11 5 1.23 2.56 15 11 5 1.64 3.89 16 11 5 5.14 3.91 16 11 5 4.82 3.72 16 11 5 4.76 3.48 16 11 5 5.35 3.88 17 11 5 0.06 2.90 17 11 5 0.13 2.65 17 11 5 0.18 2.38 17 11 5 0.27 2.28 18 11 5 4.98 5.22 18 11 5 3.81 4.52 18 11 5 3.46 4.02 18 11 5 3.63 4.06 19 11 5 73.17 17.53 19 11 5 67.03 16.11 19 11 5 69.61 16.67 22 12 -5 1.29 2.13 22 12 -5 1.81 2.39 22 12 -5 2.23 3.28 22 12 -5 2.20 2.68 21 12 -5 1.58 2.23 21 12 -5 1.32 1.94 21 12 -5 1.30 2.79 21 12 -5 1.87 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1.63 -9 -12 5 1.62 2.28 9 -12 -5 0.81 0.97 9 12 -5 1.31 1.81 9 12 -5 0.92 1.89 -9 12 5 1.12 1.93 8 12 -5 84.52 15.05 -8 -12 5 95.50 16.76 8 -12 -5 54.22 15.98 8 12 -5 125.47 23.08 8 12 -5 88.02 17.23 -8 12 5 82.04 13.58 7 12 -5 0.15 1.70 -7 -12 5 1.57 2.22 7 -12 -5 0.13 1.07 7 12 -5 0.14 2.35 7 12 -5 0.39 2.54 -7 12 5 0.33 1.78 6 12 -5 157.19 27.90 -6 -12 5 134.32 24.09 6 12 -5 178.39 56.29 -6 12 5 122.93 20.01 5 12 -5 0.02 2.71 -5 -12 5 -0.29 1.83 5 12 -5 -0.42 3.82 -5 12 5 -0.05 1.74 4 12 -5 0.92 3.14 -4 -12 5 0.41 1.42 4 -12 -5 0.61 1.20 4 12 -5 0.10 4.31 -4 12 5 0.83 1.54 3 12 -5 -0.12 2.79 -3 -12 5 0.39 1.31 3 -12 -5 0.49 1.16 3 12 -5 -0.26 2.05 -3 12 5 0.68 1.29 2 12 -5 2.48 1.52 -2 -12 5 76.94 25.82 2 -12 -5 84.70 25.26 2 12 -5 1.41 1.58 -2 12 5 90.70 26.77 -1 12 5 6.90 4.05 -1 12 5 4.99 1.21 -1 -12 5 3.97 1.94 1 -12 -5 5.72 3.12 -1 12 5 5.60 3.23 0 12 5 306.27 48.62 0 12 5 256.88 40.29 0 -12 5 211.90 54.35 0 -12 -5 279.89 45.91 0 12 5 292.22 46.44 1 12 5 0.96 3.98 1 -12 5 1.48 1.35 -1 -12 -5 0.66 3.41 2 12 5 150.49 24.95 2 12 5 141.82 22.99 -2 -12 -5 160.44 12.61 2 12 5 164.53 51.99 3 12 5 33.36 9.85 -3 -12 -5 37.01 11.87 4 12 5 3.02 1.74 -4 -12 -5 0.35 3.10 5 12 5 1.02 2.41 5 12 5 0.81 2.07 -5 -12 -5 0.74 3.16 5 12 5 0.72 2.43 6 12 5 210.74 47.06 6 12 5 208.31 46.30 -6 -12 -5 245.40 58.18 6 12 5 239.20 53.43 6 12 5 226.68 50.46 7 12 5 3.75 2.44 7 12 5 2.66 2.11 -7 -12 -5 2.58 3.26 7 12 5 3.25 2.58 7 12 5 3.19 2.50 8 12 5 60.24 15.18 8 12 5 55.47 13.90 -8 -12 -5 73.19 19.27 8 12 5 61.66 15.49 8 12 5 56.39 14.25 9 12 5 5.07 3.74 9 12 5 4.45 4.82 -9 -12 -5 2.89 5.57 9 12 5 3.89 4.79 9 12 5 5.23 3.56 10 12 5 21.12 8.36 10 12 5 18.78 7.49 -10 -12 -5 10.24 6.75 10 12 5 19.22 7.79 10 12 5 19.51 7.75 11 12 5 2.01 3.17 11 12 5 0.48 2.97 11 12 5 1.98 3.31 -11 -12 -5 -0.11 1.85 11 12 5 2.58 3.83 11 12 5 1.04 4.23 11 12 5 1.58 3.09 12 12 5 0.87 2.08 12 12 5 0.44 2.28 12 12 5 0.35 2.67 12 12 5 1.03 2.85 12 12 5 0.54 3.41 12 12 5 1.02 2.29 13 12 5 0.20 2.29 13 12 5 -0.31 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5 49.17 17.73 3 13 -5 10.47 5.45 -3 13 5 36.58 10.95 -3 -13 5 25.56 8.13 3 -13 -5 29.62 8.74 3 13 -5 1.34 1.82 -3 13 5 34.49 10.18 -2 13 5 72.65 12.35 -2 -13 5 48.58 17.86 2 13 -5 0.09 1.57 -2 13 5 67.99 11.56 -1 13 5 301.88 94.98 -1 -13 5 262.30 94.10 1 -13 -5 292.83 93.47 -1 13 5 291.10 91.59 0 13 5 176.87 55.75 0 -13 5 139.04 36.40 0 -13 -5 175.20 56.36 0 13 5 185.29 58.65 1 13 5 69.04 24.98 1 13 5 61.60 22.07 1 -13 5 47.91 19.14 -1 -13 -5 65.65 24.18 1 13 5 74.50 27.00 2 13 5 118.23 25.31 2 13 5 110.26 22.85 -2 -13 -5 115.98 26.29 2 13 5 128.30 27.66 3 13 5 653.93 142.60 -3 -13 -5 681.69 162.36 3 13 5 785.33 173.84 4 13 5 282.85 51.79 -4 -13 -5 296.31 62.21 5 13 5 23.18 10.21 -5 -13 -5 25.24 11.60 6 13 5 0.50 2.29 6 13 5 0.69 1.85 -6 -13 -5 0.14 2.66 6 13 5 0.25 2.60 7 13 5 11.35 5.26 7 13 5 10.33 4.62 -7 -13 -5 13.32 6.11 7 13 5 10.81 5.13 8 13 5 87.87 22.23 8 13 5 84.21 20.86 -8 -13 -5 91.82 23.89 8 13 5 95.96 23.70 8 13 5 85.20 21.37 9 13 5 1.13 2.37 9 13 5 0.78 2.16 -9 -13 -5 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15 14 -5 107.20 15.79 -15 -14 5 77.11 10.69 15 -14 -5 22.12 12.53 15 14 -5 84.25 11.75 15 14 -5 80.31 11.47 15 14 -5 99.63 15.49 14 14 -5 2.90 3.47 -14 -14 5 2.08 2.07 14 -14 -5 0.59 0.87 14 14 -5 2.01 2.16 14 14 -5 2.32 3.05 13 14 -5 6.97 4.66 -13 -14 5 6.01 3.86 13 -14 -5 2.13 1.91 13 14 -5 6.00 3.76 13 14 -5 6.62 4.47 12 14 -5 17.80 7.76 12 -14 -5 6.93 2.32 12 14 -5 15.65 6.71 12 14 -5 16.40 7.29 11 14 -5 36.65 12.15 -11 14 5 45.65 4.09 11 -14 -5 14.11 10.66 11 14 -5 33.43 10.92 11 14 -5 33.13 11.19 10 14 -5 1.53 2.32 -10 -14 5 1.68 2.68 10 -14 -5 0.54 1.42 10 14 -5 1.25 2.50 10 14 -5 1.00 2.53 -10 14 5 0.80 3.03 9 14 -5 57.70 14.78 -9 -14 5 70.98 17.71 9 -14 -5 35.03 11.29 9 14 -5 75.59 19.20 9 14 -5 58.11 15.70 -9 14 5 63.25 15.76 8 14 -5 0.29 1.95 -8 -14 5 0.54 2.30 8 -14 -5 0.11 1.24 8 14 -5 -1.24 2.52 8 14 -5 0.05 2.33 -8 14 5 0.16 2.49 7 14 -5 11.46 4.07 -7 14 5 10.54 4.58 -7 -14 5 12.45 4.88 7 -14 -5 6.96 3.76 7 14 -5 12.08 4.41 -7 14 5 10.71 4.82 6 14 -5 1.07 2.54 -6 14 5 0.42 2.29 -6 -14 5 1.21 2.24 6 -14 -5 0.48 1.64 6 14 -5 0.95 3.36 -6 14 5 0.77 2.66 5 14 -5 -0.56 3.53 -5 14 5 0.90 1.99 -5 -14 5 0.06 2.11 5 14 -5 -0.42 4.72 -5 14 5 0.48 2.01 4 14 -5 7.06 4.04 -4 14 5 8.40 3.10 -4 -14 5 7.57 3.08 4 14 -5 3.56 5.40 -4 14 5 9.87 3.81 3 14 -5 3.42 2.45 -3 14 5 23.98 10.80 -3 -14 5 23.41 10.61 3 -14 -5 21.44 9.48 3 14 -5 -0.02 1.55 -3 14 5 25.14 11.23 -2 14 5 5.17 2.26 -2 -14 5 4.83 1.80 2 -14 -5 4.72 2.16 2 14 -5 -0.04 1.23 -2 14 5 5.07 2.78 -1 14 5 149.35 31.68 -1 -14 5 130.02 33.98 1 -14 -5 147.88 33.08 -1 14 5 157.44 33.38 0 14 5 31.32 11.12 0 -14 5 27.57 10.22 0 -14 -5 30.39 10.99 0 14 5 33.56 11.97 1 14 5 256.33 66.25 1 -14 5 178.22 40.75 -1 -14 -5 237.62 48.75 1 14 5 259.71 56.27 2 14 5 1.94 9.76 2 14 5 1.94 12.96 3 14 5 422.94 79.36 -3 -14 -5 349.67 69.08 3 14 5 441.07 83.25 4 14 5 2.09 1.49 -4 -14 -5 1.59 2.29 5 14 5 39.56 12.23 -5 -14 -5 37.46 12.47 6 14 5 1.31 2.49 6 14 5 0.76 1.92 -6 -14 -5 1.50 2.43 7 14 5 132.12 32.55 7 14 5 124.50 30.38 -7 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12 11 -6 47.54 16.52 12 11 -6 44.30 15.94 -12 11 6 51.74 10.30 11 11 -6 92.00 19.92 11 -11 -6 51.02 22.71 11 11 -6 114.24 24.92 11 11 -6 87.54 10.49 -11 11 6 99.43 21.15 10 11 -6 4.06 2.09 -10 -11 6 6.29 3.77 10 -11 -6 2.50 1.44 10 11 -6 6.77 4.24 10 11 -6 4.40 2.18 -10 11 6 5.24 2.06 9 11 -6 74.47 13.66 -9 -11 6 86.25 14.50 9 -11 -6 44.06 13.02 9 11 -6 110.63 20.03 9 11 -6 74.03 13.64 -9 11 6 69.17 11.46 8 11 -6 1.50 1.69 -8 -11 6 0.95 1.86 8 11 -6 0.93 2.98 8 11 -6 1.41 2.06 -8 11 6 1.55 1.39 7 11 -6 78.43 13.87 -7 -11 6 64.35 4.89 7 11 -6 91.73 16.22 -7 11 6 54.11 15.91 6 11 -6 333.90 68.22 -6 -11 6 208.85 38.12 6 -11 -6 121.45 35.61 6 11 -6 359.77 64.10 -6 11 6 193.90 30.35 5 11 -6 19.06 7.37 -5 -11 6 26.83 2.60 5 -11 -6 16.91 5.19 5 11 -6 17.74 7.85 -5 11 6 24.44 7.47 4 11 -6 20.05 7.18 -4 11 6 121.52 35.80 -4 -11 6 101.37 31.46 4 -11 -6 79.75 23.59 -4 -11 6 83.38 24.76 4 11 -6 18.75 6.43 -4 11 6 103.02 30.37 3 11 -6 -0.13 1.38 -3 11 6 0.50 1.14 -3 -11 6 0.95 1.14 3 -11 -6 0.49 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117.34 8 11 6 614.79 113.84 8 11 6 527.27 99.60 -8 -11 -6 236.30 45.46 8 11 6 513.29 94.84 8 11 6 572.03 108.06 9 11 6 91.71 23.38 9 11 6 92.56 22.95 9 11 6 76.68 19.14 -9 -11 -6 15.73 10.48 9 11 6 77.23 19.39 9 11 6 82.47 20.71 10 11 6 5.04 2.51 10 11 6 6.29 2.81 10 11 6 4.40 2.53 10 11 6 4.21 3.10 10 11 6 4.51 2.20 11 11 6 37.20 13.85 11 11 6 44.71 12.47 11 11 6 38.65 3.04 11 11 6 47.44 13.52 11 11 6 38.00 14.11 11 11 6 41.58 11.80 12 11 6 2.01 1.98 12 11 6 2.19 2.75 12 11 6 2.43 3.28 12 11 6 2.22 2.90 12 11 6 1.85 3.78 12 11 6 2.38 2.25 13 11 6 7.45 3.50 13 11 6 8.03 3.13 13 11 6 8.53 3.24 13 11 6 8.06 2.86 13 11 6 8.63 4.49 13 11 6 7.92 3.84 14 11 6 18.19 7.73 14 11 6 17.43 7.58 14 11 6 17.77 7.52 14 11 6 16.45 7.66 14 11 6 20.08 11.05 15 11 6 7.92 5.53 15 11 6 7.48 5.40 15 11 6 7.27 5.03 15 11 6 6.96 4.84 15 11 6 8.82 6.60 16 11 6 7.03 5.29 16 11 6 6.02 4.83 16 11 6 7.49 5.41 16 11 6 6.04 4.56 17 11 6 -0.35 2.85 17 11 6 0.10 2.75 17 11 6 0.27 2.20 17 11 6 0.07 1.99 18 11 6 53.68 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997.75 61.73 3 10 7 605.58 190.37 3 10 7 600.31 189.81 3 10 7 613.12 192.59 4 10 7 12.21 4.91 4 10 7 11.83 4.65 4 10 7 12.22 5.01 -4 -10 -7 19.98 7.56 4 10 7 12.18 5.01 4 10 7 12.17 5.47 4 10 7 13.03 5.29 5 10 7 80.01 13.22 5 10 7 81.97 13.49 5 10 7 81.41 13.62 -5 -10 -7 85.31 14.88 5 10 7 79.61 13.30 5 10 7 88.95 14.88 6 10 7 4.40 1.98 6 10 7 4.16 1.73 6 10 7 3.78 2.40 -6 -10 -7 1.76 2.57 6 10 7 3.81 2.57 6 10 7 3.96 2.05 7 10 7 3.61 2.26 7 10 7 2.88 2.25 7 10 7 2.57 2.28 -7 -10 -7 0.63 1.64 7 10 7 3.27 2.70 7 10 7 2.66 2.22 8 10 7 0.23 2.28 8 10 7 0.31 2.50 8 10 7 1.53 2.50 8 10 7 0.55 3.01 8 10 7 0.57 2.27 9 10 7 113.34 29.02 9 10 7 111.46 27.81 9 10 7 97.33 24.79 9 10 7 98.38 24.84 9 10 7 98.09 27.51 10 10 7 0.68 2.31 10 10 7 1.10 2.81 10 10 7 0.78 2.81 10 10 7 0.67 3.58 10 10 7 0.85 2.21 11 10 7 71.17 22.04 11 10 7 96.79 28.17 11 10 7 88.06 25.86 11 10 7 95.16 28.90 11 10 7 88.31 25.88 11 10 7 88.42 25.84 12 10 7 0.64 3.35 12 10 7 -0.18 3.50 12 10 7 0.42 3.15 12 10 7 -0.58 4.09 13 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9.18 15 -11 -7 9.96 2.64 15 11 -7 22.09 8.25 15 11 -7 25.51 9.74 14 11 -7 0.70 2.13 14 -11 -7 0.20 1.07 14 11 -7 1.12 2.09 14 11 -7 1.19 2.24 -14 11 7 0.94 2.43 13 11 -7 32.86 10.34 13 -11 -7 17.90 8.45 13 11 -7 40.08 12.53 13 11 -7 31.16 9.98 -13 11 7 40.73 12.76 12 11 -7 21.54 9.64 -12 -11 7 25.46 11.41 12 -11 -7 11.60 3.77 12 11 -7 32.60 11.58 12 11 -7 20.28 9.18 -12 11 7 27.32 2.73 11 11 -7 41.20 14.35 -11 -11 7 46.45 16.15 11 -11 -7 21.31 9.75 11 11 -7 60.83 12.55 11 11 -7 37.60 13.50 -11 11 7 45.46 15.66 10 11 -7 34.16 12.12 -10 -11 7 30.32 10.75 10 11 -7 34.91 12.96 10 11 -7 31.49 11.19 -10 11 7 31.48 11.02 9 11 -7 2.35 2.20 -9 -11 7 1.79 1.52 9 11 -7 -0.33 1.93 9 11 -7 2.81 2.37 -9 11 7 1.57 1.43 8 11 -7 121.39 21.31 -8 -11 7 65.46 6.55 8 11 -7 118.49 19.66 -8 11 7 70.10 11.56 7 11 -7 115.83 24.09 -7 -11 7 102.21 20.50 7 -11 -7 65.35 2.22 7 11 -7 181.45 57.55 -7 11 7 109.32 17.86 6 11 -7 5.01 5.06 -6 -11 7 14.35 5.62 6 -11 -7 8.84 4.75 6 11 -7 4.41 5.19 -6 11 7 14.40 5.53 5 11 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6 11 7 252.04 46.79 6 11 7 302.38 56.40 7 11 7 236.70 32.20 7 11 7 237.61 31.39 7 11 7 210.00 29.08 -7 -11 -7 61.38 25.97 7 11 7 190.28 47.34 7 11 7 224.63 30.71 8 11 7 234.61 31.53 8 11 7 234.73 31.16 8 11 7 202.90 28.04 -8 -11 -7 31.59 12.69 8 11 7 188.81 46.87 8 11 7 210.39 29.86 9 11 7 5.70 2.48 9 11 7 5.95 3.29 9 11 7 4.65 2.36 9 11 7 4.64 2.77 9 11 7 5.70 2.31 10 11 7 13.67 6.62 10 11 7 18.03 7.94 10 11 7 15.42 6.76 10 11 7 14.80 6.80 10 11 7 14.71 6.40 11 11 7 2.13 2.01 11 11 7 2.44 3.06 11 11 7 1.57 2.92 11 11 7 2.09 2.86 11 11 7 1.97 3.37 11 11 7 2.16 2.19 12 11 7 -0.09 1.77 12 11 7 -0.47 3.32 12 11 7 0.51 3.62 12 11 7 0.51 2.87 12 11 7 0.48 3.89 12 11 7 0.35 1.99 13 11 7 28.97 14.91 13 11 7 27.54 14.26 13 11 7 28.55 14.66 13 11 7 24.43 12.88 13 11 7 29.60 15.42 14 11 7 14.06 9.34 14 11 7 13.69 9.27 14 11 7 13.23 8.71 14 11 7 11.26 7.64 14 11 7 16.00 9.36 15 11 7 7.00 5.26 15 11 7 6.66 5.26 15 11 7 7.53 5.44 15 11 7 6.28 4.66 15 11 7 8.61 7.21 16 11 7 5.11 3.98 16 11 7 4.55 3.74 16 11 7 4.34 3.29 16 11 7 4.32 3.13 17 11 7 3.11 4.22 17 11 7 2.12 2.92 17 11 7 2.15 2.16 18 11 7 14.21 8.46 22 12 -7 2.18 2.70 22 12 -7 3.98 4.69 22 12 -7 3.02 3.36 21 12 -7 0.46 2.28 21 12 -7 0.74 2.61 21 12 -7 0.71 2.27 20 12 -7 -0.11 2.67 20 12 -7 0.12 2.80 19 -12 -7 0.78 0.76 19 12 -7 4.15 3.49 19 12 -7 5.28 4.51 18 12 -7 369.39 16.54 18 12 -7 343.58 8.65 17 12 -7 21.62 11.67 17 -12 -7 5.10 4.22 17 12 -7 17.99 7.73 16 12 -7 1.94 3.06 16 -12 -7 1.16 0.97 16 12 -7 1.74 2.18 16 12 -7 2.16 2.99 15 12 -7 5.21 3.57 15 -12 -7 1.69 1.11 15 12 -7 4.56 2.92 15 12 -7 5.34 3.62 14 12 -7 32.87 12.19 14 -12 -7 12.07 4.79 14 12 -7 31.38 11.59 14 12 -7 30.05 11.34 13 12 -7 10.38 6.10 13 -12 -7 4.65 1.31 13 12 -7 12.05 6.99 13 12 -7 9.74 5.74 -13 12 7 13.13 7.90 12 12 -7 52.79 13.36 -12 -12 7 60.77 15.44 12 -12 -7 22.45 9.16 12 12 -7 73.14 18.29 12 12 -7 48.03 15.20 -12 12 7 63.85 16.59 11 12 -7 7.83 4.00 -11 -12 7 9.12 4.41 11 -12 -7 3.49 3.61 11 12 -7 12.34 6.16 11 12 -7 8.09 4.15 -11 12 7 7.95 4.07 10 12 -7 0.14 2.45 -10 -12 7 0.25 1.82 10 -12 -7 0.03 0.91 10 12 -7 -0.47 3.06 10 12 -7 0.53 2.64 -10 12 7 0.62 1.87 9 12 -7 1.01 2.35 -9 -12 7 0.67 1.80 9 12 -7 1.54 2.65 -9 12 7 0.66 1.69 8 12 -7 117.81 26.01 -8 -12 7 62.22 23.04 8 12 -7 110.20 23.32 -8 12 7 68.95 24.69 7 12 -7 10.06 6.53 -7 -12 7 5.89 1.61 7 -12 -7 3.55 1.02 7 12 -7 8.74 7.54 -7 12 7 6.56 3.55 6 12 -7 0.73 3.48 -6 12 7 1.83 1.36 -6 -12 7 2.10 1.42 6 -12 -7 0.86 0.97 6 12 -7 -1.09 3.68 -6 12 7 1.21 1.72 5 12 -7 0.12 1.77 -5 12 7 0.83 1.38 -5 -12 7 0.74 1.24 5 -12 -7 1.34 1.09 5 12 -7 0.09 2.05 -5 12 7 1.38 1.83 -4 -12 7 76.28 28.53 4 -12 -7 62.17 22.22 -4 12 7 84.84 30.35 -3 12 7 0.23 1.48 -3 -12 7 0.04 1.18 3 -12 -7 0.21 1.42 -3 12 7 0.11 1.86 -2 12 7 17.64 5.50 -2 -12 7 13.87 4.49 2 -12 -7 15.54 4.98 -2 12 7 17.86 5.92 -1 12 7 23.95 9.12 -1 12 7 17.64 5.61 1 -12 -7 17.56 5.70 -1 12 7 19.77 6.69 0 12 7 34.12 11.97 0 -12 -7 38.62 13.70 0 12 7 37.17 13.24 1 12 7 7.07 4.08 -1 -12 -7 8.13 5.29 2 12 7 244.55 53.44 2 12 7 244.55 53.38 -2 -12 -7 311.49 69.97 3 12 7 7.83 3.31 3 12 7 8.05 3.38 -3 -12 -7 10.61 4.70 3 12 7 8.77 4.01 4 12 7 479.82 88.20 4 12 7 489.15 89.60 -4 -12 -7 620.82 122.46 4 12 7 528.69 97.37 5 12 7 31.44 11.55 5 12 7 32.69 11.84 -5 -12 -7 34.29 12.96 5 12 7 34.93 13.25 6 12 7 18.47 3.08 6 12 7 17.81 7.24 6 12 7 17.10 7.00 -6 -12 -7 14.85 7.14 6 12 7 14.34 6.09 6 12 7 18.10 3.08 7 12 7 11.51 6.83 7 12 7 11.43 6.76 7 12 7 9.82 5.88 -7 -12 -7 4.51 2.86 7 12 7 8.85 2.80 7 12 7 10.38 6.30 8 12 7 27.14 2.94 8 12 7 26.37 10.09 8 12 7 23.35 9.07 -8 -12 -7 4.79 2.06 8 12 7 19.52 7.76 8 12 7 25.20 9.75 9 12 7 6.48 3.13 9 12 7 6.56 2.97 9 12 7 6.83 3.11 9 12 7 4.60 3.14 9 12 7 6.46 2.89 10 12 7 79.03 21.59 10 12 7 87.43 23.62 10 12 7 76.61 21.19 10 12 7 86.69 24.27 10 12 7 70.49 19.19 10 12 7 75.29 20.38 11 12 7 0.67 2.06 11 12 7 0.35 2.80 11 12 7 1.22 2.97 11 12 7 0.65 2.82 11 12 7 -0.27 3.48 11 12 7 0.20 2.14 12 12 7 46.39 16.85 12 12 7 57.19 20.63 12 12 7 51.60 18.83 12 12 7 51.49 19.05 12 12 7 53.06 19.39 12 12 7 50.49 18.29 13 12 7 1.44 3.10 13 12 7 2.07 3.36 13 12 7 1.68 2.42 13 12 7 2.45 2.99 13 12 7 2.03 4.35 14 12 7 27.67 8.18 14 12 7 25.08 13.93 14 12 7 23.54 13.00 14 12 7 23.17 12.92 14 12 7 28.86 9.15 15 12 7 1.96 2.85 15 12 7 1.69 2.05 15 12 7 1.34 2.26 16 12 7 1.92 2.72 16 12 7 2.17 2.04 16 12 7 1.96 2.09 17 12 7 0.12 2.42 21 13 -7 1.06 2.36 21 13 -7 1.58 2.31 20 13 -7 2.37 2.41 20 13 -7 2.27 2.63 19 13 -7 0.24 2.56 19 13 -7 0.36 2.37 18 13 -7 100.96 18.56 18 -13 -7 24.46 14.79 18 13 -7 92.14 16.23 17 13 -7 10.98 7.67 17 -13 -7 2.38 1.22 17 13 -7 8.54 5.63 17 13 -7 11.25 7.69 16 13 -7 116.23 25.84 16 -13 -7 32.25 16.55 16 13 -7 91.85 20.25 16 13 -7 114.84 25.74 15 13 -7 11.25 4.74 15 -13 -7 3.50 2.63 15 13 -7 9.85 2.11 15 13 -7 10.71 2.82 14 13 -7 139.90 14.65 14 -13 -7 50.26 20.88 14 13 -7 140.72 14.32 14 13 -7 130.88 14.89 13 13 -7 0.11 2.35 13 -13 -7 0.09 1.07 13 13 -7 0.00 2.53 13 13 -7 0.31 2.42 -13 13 7 0.01 3.25 12 13 -7 3.78 2.54 -12 -13 7 3.55 2.81 12 -13 -7 1.98 1.17 12 13 -7 3.84 3.00 12 13 -7 2.74 2.21 -12 13 7 4.32 3.13 11 13 -7 42.19 13.69 -11 -13 7 46.02 10.67 11 -13 -7 18.24 7.61 11 13 -7 52.33 12.72 11 13 -7 40.10 13.36 -11 13 7 49.61 11.84 10 13 -7 45.91 14.49 -10 -13 7 41.69 13.03 10 -13 -7 19.41 7.09 10 13 -7 42.84 13.59 -10 13 7 45.24 14.13 9 13 -7 5.86 3.70 -9 -13 7 5.01 2.78 9 13 -7 6.28 4.04 -9 13 7 6.63 3.46 8 13 -7 32.10 10.83 -8 -13 7 20.60 7.56 8 13 -7 34.09 11.23 -8 13 7 23.87 8.73 7 13 -7 39.13 14.56 -7 -13 7 46.94 16.40 7 13 -7 58.95 12.73 -7 13 7 51.14 10.04 6 13 -7 16.03 9.53 -6 -13 7 62.79 14.53 6 -13 -7 42.88 14.66 6 13 -7 12.39 5.29 -6 13 7 73.05 14.07 5 13 -7 0.70 1.39 -5 13 7 77.75 14.95 -5 -13 7 80.87 15.88 5 -13 -7 58.88 11.28 5 13 -7 1.21 1.97 -5 13 7 87.11 16.64 -4 13 7 1.97 1.43 -4 -13 7 1.69 1.43 4 -13 -7 0.92 1.53 4 13 -7 0.08 1.62 -4 13 7 2.28 2.00 -3 13 7 10.31 3.43 -3 -13 7 7.32 2.58 3 -13 -7 8.12 2.94 -3 13 7 9.36 3.36 -2 13 7 50.11 10.01 -2 13 7 40.06 13.81 -2 -13 7 32.89 13.34 2 -13 -7 38.24 13.32 -2 13 7 43.24 15.02 -1 13 7 155.09 33.06 -1 13 7 129.50 27.44 1 -13 -7 128.60 27.64 -1 13 7 135.08 28.60 0 13 7 47.97 16.74 0 13 7 42.32 14.64 0 -13 -7 44.83 15.83 0 13 7 46.08 16.17 1 13 7 115.00 24.35 -1 -13 -7 133.56 30.00 1 13 7 124.93 27.02 2 13 7 42.20 14.58 -2 -13 -7 48.74 17.31 3 13 7 65.05 16.22 3 13 7 63.98 15.80 -3 -13 -7 76.54 20.11 4 13 7 31.96 10.18 4 13 7 31.05 9.82 -4 -13 -7 37.59 12.33 4 13 7 36.12 11.60 5 13 7 43.54 14.19 5 13 7 43.34 14.07 -5 -13 -7 47.09 11.85 5 13 7 47.22 11.47 6 13 7 257.28 83.85 6 13 7 242.28 78.94 -6 -13 -7 232.38 77.67 6 13 7 256.10 83.69 7 13 7 144.45 24.09 7 13 7 138.17 22.84 -7 -13 -7 72.82 21.52 7 13 7 139.44 23.89 8 13 7 14.34 6.35 8 13 7 14.43 6.35 -8 -13 -7 3.20 2.26 8 13 7 11.26 2.91 8 13 7 13.81 6.30 9 13 7 0.41 2.30 9 13 7 -0.31 2.27 9 13 7 -0.09 2.55 9 13 7 -0.14 2.31 10 13 7 2.02 2.10 10 13 7 1.71 2.71 10 13 7 2.06 2.77 10 13 7 1.97 2.68 10 13 7 1.86 2.31 11 13 7 0.43 1.83 11 13 7 0.17 3.18 11 13 7 0.56 2.64 11 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9 205.61 38.13 10 4 9 181.58 33.49 10 4 9 173.45 7.22 10 -4 9 140.32 31.63 10 4 9 158.76 34.53 11 -4 9 12.69 5.94 11 4 9 17.67 11.06 11 4 9 14.55 7.09 11 4 9 11.93 8.48 11 -4 9 9.70 4.98 11 4 9 11.78 6.19 12 -4 9 84.22 23.25 12 4 9 111.10 27.23 12 4 9 97.05 23.71 12 -4 9 60.91 14.86 13 -4 9 4.91 2.29 13 4 9 6.06 4.51 13 4 9 5.51 3.17 13 -4 9 3.87 2.42 14 -4 9 276.45 36.91 14 4 9 360.56 49.08 14 4 9 295.14 39.12 14 -4 9 197.38 30.73 15 -4 9 0.36 2.14 15 4 9 0.32 3.94 15 4 9 0.23 2.69 15 4 9 1.14 3.53 16 -4 9 9.76 6.59 16 4 9 10.11 6.93 16 4 9 10.73 7.67 17 4 9 0.37 2.84 17 4 9 0.60 4.49 18 4 9 3.80 4.22 18 4 9 4.13 4.64 25 5 -9 6.37 3.71 25 5 -9 7.00 3.98 -25 5 9 5.16 4.37 -25 -5 9 6.40 5.21 24 5 -9 1.72 2.19 24 -5 -9 0.87 1.07 24 5 -9 2.17 2.33 -24 5 9 1.55 2.54 -24 -5 9 2.85 7.63 24 5 -9 2.14 1.93 23 5 -9 15.27 10.65 23 -5 -9 17.05 2.94 -23 5 9 27.91 8.61 -23 -5 9 36.28 15.04 23 5 -9 29.04 8.41 22 5 -9 20.17 13.52 22 -5 -9 19.58 10.58 -22 5 9 35.76 15.47 -22 -5 9 41.06 12.74 22 5 -9 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1.42 6 5 -9 2.80 2.96 5 5 -9 1.13 2.64 5 -5 -9 10.82 1.80 -5 -5 9 6.68 1.48 -5 5 9 7.82 1.56 5 5 -9 2.55 3.08 4 -5 -9 5.62 2.13 -4 -5 9 3.42 1.35 -4 5 9 3.97 1.61 4 5 -9 0.55 2.85 -4 5 9 3.15 1.06 -3 -5 9 63.30 29.57 -3 5 9 96.25 44.91 3 -5 -9 194.86 37.58 -3 -5 9 104.15 48.65 -3 5 9 112.24 52.39 -3 5 9 107.56 50.21 -2 5 9 286.03 89.99 2 -5 -9 628.02 197.71 -2 -5 9 351.04 111.49 -2 5 9 392.76 123.71 -2 5 9 397.33 125.01 -1 5 9 483.40 152.08 1 -5 -9 872.79 274.54 -1 -5 9 555.14 177.14 -1 5 9 651.52 205.06 -1 5 9 671.24 211.23 0 5 9 365.49 115.03 0 -5 9 423.09 135.65 0 5 9 457.39 143.98 0 5 9 445.63 140.58 1 5 9 7.80 1.45 1 5 9 9.04 1.86 1 5 9 7.70 1.25 -2 -5 -9 125.58 45.58 2 -5 9 46.07 15.45 2 5 9 80.07 29.14 2 5 9 80.90 29.38 2 5 9 68.83 25.13 -3 -5 -9 533.62 161.83 3 -5 9 261.56 85.80 3 5 9 369.94 112.30 3 5 9 351.16 106.48 3 5 9 263.35 80.98 4 5 9 2.17 1.16 4 -5 9 1.26 0.89 4 5 9 0.92 1.92 4 5 9 1.05 2.49 4 5 9 1.17 1.04 5 -5 9 489.43 84.04 5 5 9 675.27 105.70 5 5 9 696.16 108.59 5 5 9 485.08 103.57 6 -5 9 0.51 1.29 6 5 9 0.61 1.83 6 5 9 0.38 2.93 6 -5 9 0.24 1.13 7 -5 9 3.86 1.68 7 5 9 3.92 1.92 7 5 9 5.95 3.90 7 5 9 4.88 5.19 7 5 9 3.01 5.13 7 -5 9 2.49 1.32 8 -5 9 41.35 15.21 8 5 9 47.03 17.07 8 5 9 47.95 17.43 8 5 9 48.04 17.94 8 -5 9 29.80 10.81 8 5 9 42.26 15.12 9 -5 9 8.70 3.36 9 5 9 10.70 5.14 9 5 9 9.78 4.60 9 5 9 12.87 3.33 9 5 9 10.54 5.60 9 -5 9 6.10 2.65 9 5 9 10.38 5.10 10 5 9 258.59 34.10 10 5 9 234.24 31.24 10 5 9 312.36 44.96 10 5 9 230.12 30.66 10 -5 9 161.73 44.02 10 5 9 208.31 27.94 11 -5 9 9.34 3.37 11 5 9 12.45 7.94 11 5 9 11.64 7.19 11 5 9 14.76 10.14 11 -5 9 5.81 3.92 12 -5 9 11.54 2.42 12 5 9 15.29 7.29 12 5 9 13.05 6.16 12 5 9 11.79 4.29 12 -5 9 8.24 2.20 13 -5 9 116.53 12.27 13 5 9 159.49 16.77 13 5 9 143.56 14.98 13 5 9 118.57 12.87 14 5 9 0.75 4.06 14 5 9 0.78 3.20 15 5 9 25.90 13.85 15 5 9 22.38 11.85 16 5 9 27.80 8.56 16 5 9 25.84 14.31 17 5 9 17.25 7.59 17 5 9 14.11 7.77 17 5 9 14.82 7.86 18 5 9 3.57 4.65 18 5 9 3.25 3.97 18 5 9 3.90 5.10 19 5 9 1.42 3.04 19 5 9 1.01 2.43 25 6 -9 6.87 5.37 25 6 -9 7.34 5.20 -25 6 9 5.85 5.16 -25 -6 9 5.72 5.45 24 6 -9 1.45 2.17 24 -6 -9 0.43 0.78 24 6 -9 1.69 2.53 -24 6 9 0.71 2.03 -24 -6 9 1.09 5.11 24 6 -9 1.31 2.01 23 6 -9 61.14 35.13 23 -6 -9 54.15 13.59 -23 6 9 96.80 17.53 -23 -6 9 140.89 27.82 23 6 -9 142.71 25.30 23 6 -9 115.90 21.22 22 6 -9 3.30 2.76 22 -6 -9 3.44 1.54 -22 6 9 5.87 4.99 -22 -6 9 8.82 12.02 22 6 -9 7.64 5.47 22 6 -9 6.13 4.25 21 6 -9 6.45 6.76 21 -6 -9 6.12 4.92 -21 6 9 11.68 6.42 -21 -6 9 14.29 14.16 21 6 -9 13.52 6.15 21 6 -9 12.68 5.55 20 -6 -9 4.41 3.04 -20 6 9 7.30 5.14 -20 -6 9 6.70 14.57 20 6 -9 8.17 2.62 20 6 -9 7.97 4.07 19 -6 -9 26.91 11.22 -19 6 9 50.90 14.57 -19 -6 9 48.86 19.80 19 6 -9 41.11 11.36 19 6 -9 48.49 13.36 -19 6 9 31.46 11.77 18 6 -9 8.93 2.99 18 -6 -9 6.73 2.20 -18 6 9 10.40 6.83 -18 -6 9 12.25 16.43 18 6 -9 9.64 2.01 -18 6 9 5.98 1.97 17 6 -9 15.19 8.71 17 -6 -9 13.32 7.79 -17 6 9 18.18 7.61 -17 -6 9 24.49 19.73 17 6 -9 16.77 6.56 -17 6 9 9.77 5.58 16 6 -9 5.50 2.88 16 -6 -9 4.11 4.13 -16 6 9 5.43 3.77 -16 -6 9 7.28 18.75 16 6 -9 6.44 3.39 -16 6 9 3.22 3.24 15 6 -9 13.08 1.77 -15 6 9 13.40 6.33 -15 -6 9 24.20 20.56 15 6 -9 21.04 9.66 15 6 -9 14.81 6.71 -15 6 9 11.57 3.91 14 6 -9 31.71 11.03 -14 6 9 25.38 9.09 -14 -6 9 60.96 28.06 14 6 -9 69.62 25.16 14 6 -9 34.36 11.95 -14 6 9 29.16 10.58 13 6 -9 112.41 18.49 13 -6 -9 103.24 17.28 -13 6 9 83.49 13.79 -13 -6 9 209.58 69.41 13 6 -9 236.40 74.64 13 6 -9 107.41 17.47 -13 6 9 101.47 18.22 12 6 -9 1.76 1.59 12 -6 -9 1.68 1.43 -12 6 9 0.81 1.46 -12 -6 9 1.76 9.47 12 6 -9 0.79 4.80 12 6 -9 1.68 1.51 -12 6 9 1.86 1.50 11 6 -9 112.19 33.11 11 -6 -9 62.30 18.58 -11 6 9 51.17 16.00 -11 -6 9 115.74 37.02 11 6 -9 49.74 16.44 11 6 -9 83.32 24.57 -11 6 9 72.35 21.35 10 6 -9 30.16 10.12 10 -6 -9 12.93 4.05 -10 6 9 11.61 3.68 10 6 -9 4.97 3.83 10 6 -9 23.53 7.44 -10 6 9 15.94 5.00 9 6 -9 3.12 3.78 9 -6 -9 1.21 1.09 -9 6 9 1.62 1.50 9 6 -9 -0.31 3.84 9 6 -9 2.67 3.23 -9 6 9 1.54 1.29 8 6 -9 2.98 4.74 8 -6 -9 2.71 1.08 -8 6 9 3.89 1.69 8 6 -9 0.99 3.50 8 6 -9 5.44 3.71 -8 6 9 2.98 1.43 7 6 -9 118.55 43.47 7 -6 -9 294.30 89.24 -7 -6 9 304.80 92.53 -7 6 9 518.20 157.12 -7 6 9 268.58 82.86 7 6 -9 273.47 83.47 -7 6 9 276.36 83.88 6 6 -9 0.52 2.73 6 -6 -9 1.58 1.37 -6 -6 9 1.50 1.30 -6 6 9 1.15 1.09 6 6 -9 0.24 2.91 -6 6 9 1.70 1.26 5 6 -9 14.82 7.26 5 -6 -9 196.72 62.03 -5 -6 9 134.01 41.72 -5 6 9 142.47 44.62 5 6 -9 36.53 12.18 4 -6 -9 70.04 21.92 -4 -6 9 39.47 11.95 -4 6 9 39.91 13.30 4 6 -9 7.67 4.13 -3 6 9 15.96 1.28 3 -6 -9 30.16 9.29 -3 -6 9 16.64 1.73 -3 6 9 18.71 1.73 -3 6 9 22.50 6.92 2 -6 -9 5.12 0.21 2 -6 -9 109.24 34.04 -2 -6 9 58.36 18.34 -2 6 9 70.77 22.09 -2 6 9 80.27 25.08 1 -6 -9 9.58 0.82 -1 6 9 16.96 1.37 -1 6 9 23.78 7.36 1 -6 -9 29.51 9.08 -1 -6 9 15.06 1.72 -1 6 9 19.76 6.17 -1 6 9 23.67 7.28 0 -6 -9 151.11 54.64 0 6 9 132.00 47.70 0 6 9 154.51 55.86 0 -6 -9 190.35 57.88 0 -6 9 135.45 49.46 0 6 9 148.25 53.63 0 6 9 151.47 54.86 -1 -6 -9 163.81 59.29 1 6 9 114.57 41.43 1 6 9 116.83 42.31 1 6 9 115.87 41.93 1 6 9 107.67 39.86 2 6 9 10.85 4.22 2 6 9 10.67 4.38 2 6 9 10.78 5.00 2 6 9 8.45 3.54 3 6 9 7.96 4.10 3 6 9 7.54 4.09 3 6 9 7.27 4.01 3 6 9 6.16 3.97 3 6 9 8.89 4.50 4 6 9 0.35 1.30 4 6 9 0.34 2.08 4 6 9 -0.21 2.57 4 6 9 0.31 2.36 4 6 9 -0.57 3.64 4 6 9 0.57 1.42 5 6 9 446.24 140.67 5 6 9 445.01 140.68 5 6 9 517.81 162.70 5 6 9 486.37 153.26 5 6 9 453.73 143.22 6 6 9 1.08 1.84 6 6 9 0.89 3.76 6 6 9 1.17 1.53 7 6 9 178.52 7.82 7 6 9 208.77 45.84 8 6 9 9.60 4.14 8 6 9 10.89 6.15 8 -6 9 5.07 1.69 8 6 9 9.19 4.94 9 6 9 58.69 11.94 9 6 9 96.65 20.98 9 6 9 58.93 12.20 9 -6 9 33.70 12.76 9 6 9 54.38 11.73 10 6 9 31.39 10.51 10 6 9 53.36 13.75 10 6 9 25.87 9.53 10 6 9 29.10 7.23 10 -6 9 14.97 6.74 10 6 9 27.61 11.21 11 6 9 682.82 221.57 11 6 9 1112.02 360.47 11 6 9 477.45 156.68 11 6 9 609.52 197.76 12 6 9 4.42 3.88 12 6 9 3.86 3.47 12 6 9 5.93 3.86 12 6 9 3.46 4.26 13 6 9 35.79 15.88 13 6 9 34.28 15.23 13 6 9 28.91 12.99 14 6 9 1.79 3.74 14 6 9 2.00 3.77 14 6 9 1.52 3.94 15 6 9 26.75 11.60 15 6 9 26.60 11.43 15 6 9 23.62 10.35 16 6 9 0.72 3.56 16 6 9 0.26 2.99 17 6 9 2.54 3.23 17 6 9 2.34 2.62 18 6 9 0.35 3.57 25 7 -9 9.75 5.99 25 7 -9 11.01 6.55 24 7 -9 15.35 10.15 -24 7 9 23.38 9.94 -24 -7 9 23.37 10.25 24 7 -9 29.01 12.03 23 -7 -9 0.78 0.87 -23 7 9 1.35 2.44 -23 -7 9 1.48 5.59 23 7 -9 2.13 2.99 23 7 -9 2.02 2.10 22 7 -9 3.15 2.54 22 -7 -9 2.04 1.12 -22 7 9 4.35 3.51 -22 -7 9 7.16 9.21 22 7 -9 6.31 4.93 22 7 -9 5.07 4.35 21 7 -9 5.68 5.85 21 -7 -9 4.82 3.81 -21 7 9 9.59 5.17 -21 -7 9 12.81 11.64 21 7 -9 11.74 5.75 21 7 -9 10.86 5.26 20 -7 -9 18.16 8.64 -20 7 9 34.89 9.46 -20 -7 9 43.76 17.04 20 7 -9 38.92 10.14 20 7 -9 40.35 10.49 19 -7 -9 -0.10 1.29 -19 7 9 -0.39 3.26 -19 -7 9 -0.55 12.46 19 7 -9 -0.07 2.21 19 7 -9 0.11 2.36 18 7 -9 14.33 6.44 18 -7 -9 8.78 2.49 -18 7 9 14.25 6.67 -18 -7 9 16.90 14.70 18 7 -9 14.21 6.12 -18 7 9 10.36 2.34 17 7 -9 6.29 2.33 17 -7 -9 4.03 1.78 -17 7 9 5.54 2.57 -17 -7 9 9.50 13.76 17 7 -9 6.47 2.31 -17 7 9 4.58 1.64 16 7 -9 39.55 12.88 16 -7 -9 31.16 11.86 -16 7 9 38.67 12.12 -16 -7 9 70.19 23.74 16 7 -9 55.51 13.75 16 7 -9 48.12 14.85 -16 7 9 33.64 10.52 15 7 -9 15.35 6.85 -15 7 9 13.14 2.09 -15 -7 9 29.81 18.28 15 7 -9 26.18 11.68 15 7 -9 17.02 7.64 -15 7 9 12.00 3.80 14 7 -9 10.31 3.41 -14 7 9 7.45 2.78 -14 -7 9 21.29 16.16 14 7 -9 22.94 10.64 14 7 -9 10.64 3.48 -14 7 9 9.16 3.07 13 7 -9 70.03 25.15 -13 7 9 49.56 17.78 -13 -7 9 124.46 29.91 13 7 -9 133.95 28.51 13 7 -9 64.69 23.15 -13 7 9 66.50 23.85 12 7 -9 36.12 10.93 12 -7 -9 25.59 7.54 -12 7 9 22.87 6.82 12 7 -9 23.11 8.36 12 7 -9 30.73 9.09 -12 7 9 30.49 8.98 11 7 -9 37.09 11.27 11 -7 -9 18.29 6.90 -11 7 9 18.66 1.69 11 7 -9 10.77 5.61 11 7 -9 29.47 8.78 -11 7 9 23.32 6.93 10 7 -9 6.15 6.18 10 -7 -9 3.17 1.11 -10 7 9 3.93 1.36 10 7 -9 1.16 3.41 10 7 -9 6.12 3.78 -10 7 9 4.19 1.50 9 7 -9 113.23 33.86 9 -7 -9 67.28 19.91 -9 7 9 117.51 34.59 9 7 -9 8.41 5.90 9 7 -9 156.48 25.29 -9 7 9 92.61 27.27 8 7 -9 70.59 21.47 8 -7 -9 83.29 24.51 -8 -7 9 113.50 33.50 -8 7 9 169.53 26.95 8 7 -9 122.91 36.65 -8 7 9 100.71 29.64 7 7 -9 0.02 3.13 7 -7 -9 0.74 1.32 -7 -7 9 0.93 1.35 7 7 -9 0.06 3.54 -7 7 9 1.02 1.31 6 7 -9 0.29 3.07 6 -7 -9 0.57 1.20 -6 -7 9 1.40 1.23 -6 7 9 0.38 1.13 6 7 -9 -0.05 2.97 -6 7 9 1.82 1.30 5 -7 -9 141.51 51.15 -5 -7 9 106.82 38.71 -5 7 9 115.80 41.94 5 7 -9 22.69 8.79 -4 7 9 114.25 41.31 4 -7 -9 170.53 61.64 -4 -7 9 99.10 35.97 -4 7 9 132.79 48.03 4 7 -9 13.33 6.07 3 -7 -9 2.72 0.19 -3 7 9 21.71 7.13 3 -7 -9 38.34 12.57 -3 -7 9 20.18 6.69 -3 7 9 26.39 8.79 -3 7 9 30.99 10.22 2 -7 -9 103.05 37.20 -2 7 9 196.08 59.48 2 -7 -9 345.77 104.88 -2 -7 9 172.67 7.84 -2 7 9 241.27 73.20 -2 7 9 296.96 90.11 1 -7 -9 36.48 11.95 -1 7 9 38.49 12.60 -1 7 9 49.65 16.46 1 -7 -9 60.57 22.38 -1 -7 9 34.60 11.51 -1 7 9 42.79 14.03 -1 7 9 53.87 19.66 0 -7 -9 34.74 11.49 0 7 9 28.53 9.39 0 7 9 30.08 9.94 0 -7 -9 40.92 13.56 0 -7 9 24.70 8.25 0 7 9 29.57 9.80 0 7 9 33.24 10.92 -1 -7 -9 53.53 3.36 1 7 9 42.28 13.83 1 7 9 41.05 13.48 -1 -7 -9 50.29 16.66 1 7 9 39.24 12.89 1 7 9 39.17 13.01 2 7 9 152.21 24.37 2 7 9 143.70 22.94 2 7 9 160.68 25.33 2 7 9 141.25 22.41 2 7 9 139.63 22.41 3 7 9 87.32 25.76 3 7 9 86.87 25.78 3 7 9 87.10 25.91 3 7 9 92.48 27.32 3 7 9 86.78 25.80 3 7 9 81.13 24.00 4 7 9 222.67 70.06 4 7 9 223.88 70.85 4 7 9 225.41 71.12 4 7 9 243.77 76.75 4 7 9 235.86 74.43 4 7 9 213.35 67.80 5 7 9 14.09 5.47 5 7 9 14.56 5.80 5 7 9 16.28 6.57 5 7 9 18.90 4.46 5 7 9 18.25 8.57 5 7 9 13.88 5.54 6 7 9 11.60 5.67 6 7 9 11.04 5.55 6 7 9 12.01 2.27 6 7 9 14.12 5.98 6 7 9 12.60 5.77 6 7 9 10.88 5.54 7 7 9 62.98 24.03 7 7 9 74.43 26.82 7 7 9 82.88 29.97 7 -7 9 37.97 14.75 7 7 9 71.04 25.49 8 7 9 217.94 41.26 8 7 9 229.60 44.73 8 7 9 255.64 47.25 9 7 9 44.60 14.29 9 7 9 49.43 15.98 9 7 9 44.83 14.71 10 7 9 83.95 20.96 10 7 9 143.53 35.13 10 7 9 57.25 13.14 10 7 9 85.18 21.45 11 7 9 1.45 4.63 11 7 9 4.45 3.54 11 7 9 1.43 1.90 11 7 9 2.58 5.11 12 7 9 0.09 4.25 12 7 9 0.78 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52.23 2 8 9 176.78 55.81 3 8 9 0.33 1.84 3 8 9 0.09 1.92 3 8 9 0.37 2.03 3 8 9 1.29 2.95 3 8 9 -0.52 4.69 3 8 9 0.30 1.67 4 8 9 822.74 258.90 4 8 9 830.37 263.60 4 8 9 864.85 272.97 4 8 9 902.01 17.71 4 8 9 861.27 271.19 4 8 9 866.57 272.24 5 8 9 4.64 1.64 5 8 9 3.90 1.83 5 8 9 4.79 2.42 5 8 9 5.29 3.28 5 8 9 4.69 4.17 5 8 9 4.71 1.79 6 8 9 20.50 6.18 6 8 9 18.52 5.73 6 8 9 21.76 2.86 6 8 9 23.20 9.02 6 8 9 21.91 4.49 6 8 9 21.32 6.66 7 8 9 2.18 1.62 7 8 9 2.13 2.41 7 8 9 2.01 2.91 7 8 9 2.30 4.54 7 8 9 2.33 1.92 8 8 9 246.17 33.57 8 8 9 252.37 36.53 8 8 9 292.66 38.93 8 8 9 250.56 32.59 9 8 9 4.39 3.25 9 8 9 4.13 3.07 9 8 9 5.42 4.98 10 8 9 44.92 12.64 10 8 9 43.20 12.16 10 8 9 76.23 22.45 10 8 9 43.05 12.07 10 8 9 48.08 13.87 11 8 9 -0.25 3.24 11 8 9 -0.47 3.29 11 8 9 -0.15 3.27 11 8 9 -0.48 1.93 11 8 9 -0.62 4.26 12 8 9 59.78 15.62 12 8 9 60.18 16.50 12 8 9 92.92 13.30 12 8 9 47.52 12.17 12 8 9 59.91 15.77 13 8 9 1.04 3.53 13 8 9 1.41 3.19 13 8 9 1.32 4.62 14 8 9 3.33 3.18 14 8 9 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9 41.72 13.02 7 9 9 42.07 13.25 7 9 9 45.75 14.51 7 9 9 46.98 15.18 7 9 9 43.17 13.43 8 9 9 7.59 2.41 8 9 9 7.46 3.18 8 9 9 7.43 3.19 8 9 9 8.52 4.72 8 9 9 7.57 2.60 9 9 9 41.00 13.40 9 9 9 39.48 13.09 9 9 9 44.37 5.31 10 9 9 0.13 3.10 10 9 9 -0.47 3.23 10 9 9 -0.04 2.38 10 9 9 -0.29 4.25 11 9 9 77.72 21.25 11 9 9 75.83 21.08 11 9 9 104.27 5.97 11 9 9 67.77 18.57 11 9 9 80.11 21.97 12 9 9 22.60 9.97 12 9 9 23.19 10.33 12 9 9 29.92 3.47 12 9 9 19.75 8.54 12 9 9 23.28 10.52 13 9 9 24.24 12.70 13 9 9 25.70 13.42 13 9 9 29.28 15.00 13 9 9 19.34 7.95 13 9 9 25.77 13.71 14 9 9 8.58 6.44 14 9 9 9.00 6.61 14 9 9 9.04 7.28 15 9 9 8.36 6.56 15 9 9 9.21 7.04 15 9 9 9.55 6.01 16 9 9 1.78 2.70 16 9 9 1.82 3.74 17 9 9 50.45 12.33 23 10 -9 7.33 5.61 23 10 -9 11.20 6.68 22 -10 -9 3.64 3.59 22 10 -9 22.71 9.71 22 10 -9 20.61 9.82 21 -10 -9 1.32 0.86 21 10 -9 5.92 4.11 21 10 -9 5.60 4.10 20 10 -9 4.89 4.33 20 -10 -9 1.16 0.96 20 10 -9 5.00 4.03 19 10 -9 193.49 44.55 19 -10 -9 60.79 22.66 19 10 -9 201.65 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22.67 -7 10 9 414.74 90.75 7 -10 -9 318.50 69.25 7 10 -9 108.11 23.30 -7 10 9 603.12 131.57 6 10 -9 -0.05 2.26 -6 10 9 3.17 1.10 -6 -10 9 4.16 2.55 6 -10 -9 2.55 1.89 6 10 -9 -0.28 3.31 -6 10 9 4.81 3.60 -5 10 9 79.73 13.06 5 -10 -9 72.07 11.72 5 10 -9 0.88 2.73 -5 10 9 113.13 18.53 -4 10 9 9.09 1.29 -4 10 9 12.11 4.89 4 -10 -9 8.60 4.71 -4 10 9 13.80 5.86 -4 10 9 12.36 5.00 -3 10 9 0.20 1.48 -3 10 9 0.67 2.02 3 -10 -9 0.43 1.63 -3 10 9 5.17 4.12 -2 10 9 7.48 4.32 -2 10 9 7.60 4.58 2 -10 -9 8.49 4.96 -2 10 9 9.06 3.70 -1 10 9 483.42 151.95 -1 10 9 464.95 146.16 1 -10 -9 583.50 183.37 -1 10 9 481.24 151.23 -1 10 9 495.65 155.80 0 10 9 0.04 2.12 0 10 9 0.02 2.35 0 -10 -9 0.29 4.27 0 10 9 -0.88 4.30 0 10 9 0.57 2.84 1 10 9 799.48 174.14 1 10 9 739.41 160.90 1 10 9 684.57 149.04 -1 -10 -9 1038.57 226.20 1 10 9 634.63 138.01 1 10 9 758.86 165.42 2 10 9 14.13 4.75 2 10 9 13.91 4.60 2 10 9 14.54 5.19 -2 -10 -9 16.60 6.75 2 10 9 11.74 6.03 2 10 9 12.70 5.06 2 10 9 14.66 5.02 3 10 9 61.63 11.93 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8.29 5.85 13 10 9 8.02 5.77 13 10 9 7.85 5.20 13 10 9 6.39 4.36 13 10 9 8.97 6.78 14 10 9 5.61 4.35 14 10 9 5.59 4.53 14 10 9 5.84 5.14 15 10 9 0.74 2.64 15 10 9 0.87 2.89 15 10 9 0.86 3.94 16 10 9 2.24 3.40 16 10 9 2.48 3.50 22 11 -9 2.71 3.35 22 11 -9 2.79 3.41 21 -11 -9 16.45 8.21 21 11 -9 73.55 8.94 21 11 -9 78.27 9.52 20 11 -9 11.98 6.36 20 -11 -9 2.46 1.03 20 11 -9 11.56 5.96 19 11 -9 11.82 8.35 19 -11 -9 2.78 1.35 19 11 -9 11.23 7.42 18 11 -9 6.64 5.51 18 -11 -9 1.63 1.16 18 11 -9 6.17 4.97 18 11 -9 7.39 4.46 17 11 -9 0.40 2.15 17 -11 -9 0.33 0.92 17 11 -9 0.61 2.33 17 11 -9 0.56 2.75 16 11 -9 21.25 7.94 16 -11 -9 7.98 5.06 16 11 -9 28.07 12.29 16 11 -9 21.79 8.16 -16 11 9 26.39 11.71 15 11 -9 5.23 3.28 15 -11 -9 1.96 1.03 15 11 -9 7.17 4.86 15 11 -9 4.99 3.17 -15 11 9 5.92 4.06 14 11 -9 3.28 1.95 14 -11 -9 1.42 1.11 14 11 -9 4.68 3.53 14 11 -9 3.24 2.05 -14 11 9 3.44 2.39 13 11 -9 54.96 12.61 13 11 -9 52.46 13.09 13 11 -9 48.92 11.27 -13 11 9 53.54 12.28 12 11 -9 104.48 25.60 12 11 -9 14.58 8.77 12 11 -9 93.38 22.84 -12 11 9 82.80 20.24 11 11 -9 25.05 9.74 11 11 -9 23.36 9.19 -11 11 9 16.10 6.51 10 11 -9 3.12 5.67 -10 11 9 1.38 1.05 10 -11 -9 0.64 0.84 10 11 -9 4.49 6.22 -10 11 9 1.84 1.77 9 11 -9 1.62 4.63 -9 11 9 3.10 0.93 9 -11 -9 1.88 0.79 9 11 -9 3.20 6.47 -9 11 9 4.74 1.76 8 11 -9 0.16 2.26 -8 11 9 0.21 0.95 -8 -11 9 0.47 1.28 8 -11 -9 0.27 0.76 8 11 -9 0.12 2.84 -8 11 9 0.76 1.84 7 11 -9 0.33 2.24 -7 11 9 6.29 1.14 -7 -11 9 6.76 1.63 7 -11 -9 4.59 0.98 7 11 -9 0.63 2.84 -7 11 9 10.29 3.67 -6 11 9 2.32 1.00 -6 -11 9 3.03 1.68 6 -11 -9 1.82 1.06 6 11 -9 -0.13 2.65 -6 11 9 3.27 2.13 -5 11 9 105.77 21.86 -5 11 9 139.00 28.67 -5 -11 9 126.60 27.34 5 -11 -9 81.01 28.91 5 11 -9 -0.30 2.42 -5 11 9 135.34 27.95 -4 11 9 174.06 5.01 -4 11 9 198.81 43.47 4 -11 -9 143.63 29.53 -4 11 9 205.23 44.90 -3 11 9 16.05 5.05 -3 11 9 17.12 5.60 3 -11 -9 15.06 4.99 -3 11 9 19.10 6.70 -3 11 9 19.55 6.56 -2 11 9 47.33 17.04 -2 11 9 48.26 17.49 2 -11 -9 49.38 17.87 -2 11 9 51.86 18.94 -1 11 9 279.24 60.98 -1 11 9 261.17 57.24 1 -11 -9 323.93 70.90 -1 11 9 283.03 61.94 0 11 9 222.23 48.80 0 11 9 192.03 42.15 0 11 9 185.27 40.67 0 -11 -9 258.14 56.61 0 11 9 190.35 41.75 0 11 9 210.35 46.17 1 11 9 141.63 29.99 1 11 9 135.66 28.66 1 11 9 133.06 28.26 -1 -11 -9 184.23 34.33 1 11 9 125.11 26.68 1 11 9 146.25 30.99 2 11 9 34.36 12.07 2 11 9 35.58 12.37 2 11 9 35.41 12.53 -2 -11 -9 43.24 15.71 2 11 9 33.34 11.91 2 11 9 39.30 13.83 3 11 9 88.07 21.65 3 11 9 91.74 22.44 3 11 9 93.77 4.54 -3 -11 -9 76.50 19.71 3 11 9 99.83 24.93 4 11 9 62.59 15.53 4 11 9 67.75 16.67 4 11 9 67.40 16.68 -4 -11 -9 24.68 9.16 4 11 9 55.04 13.77 4 11 9 71.72 17.82 5 11 9 15.20 8.64 5 11 9 16.08 6.33 5 11 9 16.54 6.75 5 11 9 12.92 7.52 5 11 9 16.81 6.80 6 11 9 83.95 20.52 6 11 9 91.76 22.36 6 11 9 83.07 20.59 6 11 9 75.09 17.16 6 11 9 88.20 21.63 7 11 9 93.02 26.96 7 11 9 98.34 28.53 7 11 9 86.45 25.27 7 11 9 76.72 23.30 7 11 9 88.76 25.87 8 11 9 0.16 2.03 8 11 9 -0.34 3.37 8 11 9 -0.09 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7.02 -4 12 9 45.39 15.60 4 -12 -9 32.29 11.12 -4 12 9 47.09 16.22 -3 12 9 72.86 14.17 3 -12 -9 60.10 11.70 -3 12 9 78.62 15.36 -2 12 9 507.79 92.92 2 -12 -9 512.98 93.70 -2 12 9 535.86 98.50 -1 12 9 35.87 12.42 -1 12 9 35.43 12.37 1 -12 -9 43.05 15.16 0 12 9 71.52 17.84 0 12 9 62.15 15.29 0 12 9 65.04 16.22 0 -12 -9 82.73 20.65 1 12 9 20.62 8.38 1 12 9 18.28 3.34 1 12 9 20.27 8.72 -1 -12 -9 27.65 10.90 1 12 9 22.55 9.81 2 12 9 1236.54 20.65 2 12 9 1201.37 39.95 2 12 9 1295.80 22.63 2 12 9 1448.64 32.14 3 12 9 0.48 3.08 3 12 9 0.45 2.18 3 12 9 0.79 3.23 -3 -12 -9 -0.41 4.81 3 12 9 0.93 3.71 4 12 9 2.05 2.35 4 12 9 1.92 1.81 4 12 9 2.97 2.70 -4 -12 -9 0.41 2.44 4 12 9 2.02 2.97 5 12 9 4.82 2.19 5 12 9 5.30 2.08 5 12 9 5.27 2.45 -5 -12 -9 0.69 1.47 5 12 9 5.35 2.58 6 12 9 45.86 12.73 6 12 9 50.21 13.87 6 12 9 46.87 13.09 6 12 9 34.08 12.76 6 12 9 46.18 12.86 7 12 9 1.63 2.50 7 12 9 2.00 2.80 7 12 9 1.62 2.60 7 12 9 1.48 2.54 7 12 9 1.66 2.44 8 12 9 11.11 2.33 8 12 9 13.00 5.73 8 12 9 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13 -9 44.97 11.47 14 -13 -9 16.27 6.28 14 13 -9 41.25 10.53 -14 13 9 54.06 14.02 13 13 -9 20.28 7.85 13 -13 -9 7.04 4.40 13 13 -9 17.80 6.86 -13 13 9 22.57 8.61 12 13 -9 202.42 20.73 12 13 -9 180.93 18.82 -12 13 9 155.33 15.69 11 13 -9 9.91 4.89 11 13 -9 7.88 4.56 -11 13 9 5.82 2.36 10 13 -9 3.88 4.80 -10 13 9 3.05 1.58 10 13 -9 2.90 4.93 -10 13 9 2.75 1.89 9 13 -9 -0.41 3.70 -9 13 9 0.32 1.54 9 -13 -9 0.16 0.80 9 13 -9 -0.86 5.28 -9 13 9 0.08 1.86 8 13 -9 0.17 1.69 -8 13 9 0.28 1.69 8 -13 -9 0.41 0.86 8 13 -9 -0.32 2.25 -8 13 9 0.62 2.39 -7 13 9 10.16 5.93 -7 -13 9 10.41 5.99 7 -13 -9 5.68 1.12 7 13 -9 -0.06 2.20 -7 13 9 11.37 6.70 -6 13 9 37.42 12.16 -6 -13 9 41.44 13.50 6 -13 -9 19.62 7.73 6 13 -9 -0.25 1.91 -6 13 9 41.83 13.82 -5 13 9 216.38 28.24 5 -13 -9 125.02 33.22 -5 13 9 228.34 29.75 -4 13 9 50.28 15.57 4 -13 -9 35.45 11.13 -4 13 9 53.89 13.74 -3 13 9 6.09 4.05 -3 13 9 4.76 2.25 3 -13 -9 5.19 3.10 -3 13 9 5.51 3.55 -2 13 9 20.69 7.67 2 -13 -9 19.90 7.55 -2 13 9 21.46 8.15 -1 13 9 46.24 10.69 1 -13 -9 50.75 11.95 0 13 9 154.03 37.47 0 13 9 148.49 36.09 0 -13 -9 168.45 8.56 1 13 9 282.47 91.76 1 13 9 276.80 89.84 -1 -13 -9 326.61 106.09 1 13 9 315.50 102.51 2 13 9 63.91 14.64 2 13 9 66.73 15.24 -2 -13 -9 73.77 17.16 2 13 9 75.76 17.46 3 13 9 81.82 24.08 3 13 9 84.11 24.53 -3 -13 -9 73.63 21.90 3 13 9 95.86 28.14 4 13 9 9.28 3.13 4 13 9 9.60 2.82 -4 -13 -9 3.87 3.12 4 13 9 10.39 3.30 5 13 9 0.38 2.87 5 13 9 0.89 2.56 -5 -13 -9 0.01 1.75 5 13 9 0.34 3.57 6 13 9 20.45 7.83 6 13 9 19.52 7.56 6 13 9 20.08 7.85 7 13 9 4.90 3.71 7 13 9 5.20 2.91 7 13 9 4.62 3.72 8 13 9 56.98 20.61 8 13 9 59.40 21.35 8 13 9 55.20 19.85 9 13 9 11.30 7.38 9 13 9 13.44 8.89 9 13 9 13.58 9.09 9 13 9 9.72 6.78 9 13 9 11.85 7.78 10 13 9 3.16 3.32 10 13 9 2.66 2.45 10 13 9 3.25 3.04 10 13 9 2.83 2.04 11 13 9 -0.64 3.15 11 13 9 -0.11 1.43 11 13 9 -0.26 2.16 11 13 9 -0.15 3.31 12 13 9 43.87 16.46 12 13 9 28.10 11.19 12 13 9 37.58 14.05 13 13 9 14.10 7.10 13 13 9 11.95 9.47 14 13 9 10.49 6.51 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7 10 4.50 3.00 8 -7 10 2.41 1.65 9 7 10 3.06 3.32 9 7 10 3.89 2.13 9 7 10 3.19 6.12 9 7 10 2.11 5.54 10 7 10 53.43 15.19 10 7 10 44.41 12.36 10 7 10 53.69 15.48 11 7 10 38.08 16.67 11 7 10 37.12 16.69 12 7 10 141.50 20.65 12 7 10 127.43 17.90 13 7 10 24.87 12.98 13 7 10 25.10 13.16 13 7 10 22.48 12.07 14 7 10 0.01 3.16 14 7 10 0.45 2.85 14 7 10 0.21 3.62 15 7 10 4.59 3.96 15 7 10 4.17 3.71 15 7 10 3.81 4.32 16 7 10 -0.04 2.94 16 7 10 0.37 2.57 16 7 10 0.26 3.34 17 7 10 25.39 8.51 17 7 10 21.23 7.30 17 7 10 25.91 8.85 24 8 -10 7.45 5.42 24 8 -10 8.41 6.02 24 8 -10 7.28 5.21 23 8 -10 1.03 2.69 23 -8 -10 0.65 0.68 23 8 -10 2.32 2.14 22 -8 -10 0.07 0.80 -22 8 10 0.29 4.09 22 8 -10 0.20 2.33 22 8 -10 0.59 2.12 21 -8 -10 0.42 0.90 -21 8 10 1.28 3.98 21 8 -10 1.03 2.35 21 8 -10 1.00 2.27 20 8 -10 32.77 12.82 20 -8 -10 15.80 8.05 -20 8 10 70.15 16.33 20 8 -10 41.73 15.13 19 8 -10 3.89 3.32 19 -8 -10 1.86 1.36 -19 8 10 6.94 4.64 -19 -8 10 4.99 5.45 19 8 -10 4.55 3.56 -19 8 10 3.50 2.70 18 8 -10 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2 8 10 44.44 16.12 2 8 10 41.41 14.81 2 8 10 42.85 14.97 3 8 10 0.55 1.74 3 8 10 1.06 2.25 3 8 10 0.90 2.82 3 8 10 1.14 3.67 3 8 10 1.12 5.05 3 8 10 0.34 1.78 4 8 10 128.01 27.09 4 8 10 134.31 28.75 4 8 10 142.50 30.45 4 8 10 152.73 32.39 4 8 10 148.32 31.62 4 8 10 134.11 28.70 5 8 10 0.71 1.61 5 8 10 0.49 2.05 5 8 10 0.41 2.40 5 8 10 0.78 3.73 5 8 10 1.07 4.48 5 8 10 0.73 1.74 6 8 10 125.19 30.98 6 8 10 124.09 30.98 6 8 10 134.50 33.76 6 8 10 153.33 38.03 6 8 10 148.80 37.06 6 8 10 134.29 33.67 7 8 10 6.94 4.09 7 8 10 7.56 4.81 7 8 10 5.59 7.82 7 8 10 7.25 3.60 8 8 10 3.36 2.49 8 8 10 2.76 2.72 8 8 10 2.24 5.46 9 8 10 0.10 3.20 9 8 10 0.41 2.50 9 8 10 1.11 4.98 10 8 10 19.21 7.71 10 8 10 16.96 6.59 10 8 10 20.90 8.80 11 8 10 2.36 3.48 11 8 10 1.72 1.91 11 8 10 1.12 4.59 12 8 10 5.13 5.11 12 8 10 5.03 5.90 13 8 10 1.32 3.36 13 8 10 1.82 4.27 14 8 10 36.94 10.64 14 8 10 35.87 10.58 15 8 10 1.23 2.86 15 8 10 1.31 2.98 15 8 10 0.57 3.87 16 8 10 14.23 8.46 16 8 10 13.89 8.25 16 8 10 15.41 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0.26 4.04 6 10 10 0.08 4.37 6 10 10 1.34 2.31 7 10 10 407.44 71.21 7 10 10 458.67 75.11 7 10 10 422.97 71.32 7 10 10 448.46 73.03 7 10 10 411.82 67.72 8 10 10 -0.15 3.20 8 10 10 -0.13 3.23 8 10 10 -0.01 4.24 8 10 10 0.14 1.85 9 10 10 288.19 39.08 9 10 10 252.32 35.19 9 10 10 258.12 34.38 9 10 10 276.41 37.44 9 10 10 264.06 35.16 10 10 10 4.12 3.80 10 10 10 2.58 2.85 10 10 10 3.24 2.80 10 10 10 3.70 4.31 11 10 10 0.85 3.24 11 10 10 0.87 3.31 11 10 10 1.34 2.09 11 10 10 0.35 4.35 12 10 10 0.27 3.12 12 10 10 -0.50 3.35 12 10 10 -0.37 1.82 12 10 10 -0.48 4.37 13 10 10 3.80 3.68 13 10 10 4.14 4.09 13 10 10 4.33 4.83 14 10 10 -0.58 3.57 14 10 10 -1.60 4.61 14 10 10 -0.24 4.20 15 10 10 22.49 7.56 15 10 10 21.51 7.27 15 10 10 26.32 9.08 22 11 -10 22.17 7.56 22 11 -10 24.19 8.01 21 11 -10 11.82 9.49 21 -11 -10 2.67 1.42 21 11 -10 12.50 9.88 20 11 -10 2.12 2.32 20 -11 -10 0.55 0.68 20 11 -10 2.01 1.87 19 11 -10 10.07 6.89 19 -11 -10 2.42 1.08 19 11 -10 10.15 2.34 19 11 -10 11.40 5.76 18 11 -10 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5 11 148.49 36.53 8 -5 11 79.55 14.56 8 5 11 136.69 33.64 9 5 11 141.62 24.99 9 5 11 121.40 20.73 9 5 11 141.58 23.97 9 -5 11 75.81 25.59 9 5 11 126.44 21.56 10 5 11 4.35 4.47 10 5 11 3.49 3.16 10 5 11 3.50 4.66 10 -5 11 2.39 2.21 10 5 11 3.42 3.73 11 5 11 17.17 3.96 11 5 11 13.95 5.90 11 5 11 14.29 6.54 11 -5 11 6.75 3.44 12 5 11 -0.21 3.53 12 5 11 0.16 2.76 12 5 11 0.85 3.95 13 5 11 0.48 3.20 13 5 11 -0.08 2.50 13 5 11 -0.21 3.32 14 5 11 16.31 8.21 14 5 11 14.35 6.89 15 5 11 5.15 4.25 15 5 11 4.09 3.50 16 5 11 3.96 2.68 16 5 11 4.07 4.40 24 6 -11 6.36 4.72 24 -6 -11 2.03 1.73 24 6 -11 5.77 5.19 -24 6 11 10.23 7.10 -24 -6 11 2.96 2.92 24 6 -11 6.18 5.41 23 6 -11 9.83 5.33 23 -6 -11 3.55 2.38 -23 6 11 16.30 7.82 -23 -6 11 5.30 3.37 23 6 -11 8.80 6.45 22 -6 -11 18.41 10.81 -22 6 11 54.55 10.68 -22 -6 11 28.48 8.37 22 6 -11 42.49 18.57 21 -6 -11 0.55 1.21 -21 6 11 1.10 3.63 -21 -6 11 0.88 2.68 21 6 -11 1.30 2.29 -21 6 11 0.69 1.50 20 6 -11 5.04 4.49 20 -6 -11 3.16 2.04 -20 6 11 6.68 5.65 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6 12 4.37 1.91 -2 6 12 5.01 2.40 -2 6 12 4.06 1.61 -1 6 12 60.00 21.51 -1 6 12 58.86 21.22 -1 6 12 57.96 21.40 0 6 12 2.92 2.10 0 6 12 2.85 2.71 0 6 12 2.15 1.58 1 6 12 236.24 43.36 1 6 12 228.70 42.12 1 6 12 170.19 18.16 2 6 12 14.58 6.55 2 6 12 17.88 8.21 2 6 12 18.03 8.27 2 6 12 17.76 8.52 2 6 12 13.30 2.26 3 6 12 158.46 33.80 3 6 12 167.82 35.42 3 6 12 159.91 33.88 3 6 12 122.60 34.92 4 6 12 5.36 3.50 4 6 12 6.02 3.79 4 6 12 6.69 4.55 4 6 12 6.63 4.90 5 6 12 3.96 2.93 5 6 12 4.19 2.82 5 6 12 4.13 5.60 5 -6 12 2.85 1.80 6 6 12 22.32 8.92 6 6 12 22.33 9.03 6 6 12 23.79 10.45 6 -6 12 10.62 6.50 7 6 12 6.47 2.76 7 6 12 6.58 2.68 7 6 12 8.96 5.15 7 -6 12 3.12 1.64 7 6 12 9.80 5.03 8 6 12 8.05 5.62 8 6 12 6.55 5.08 8 6 12 7.51 6.87 8 -6 12 3.75 2.65 8 6 12 8.45 7.08 9 6 12 23.04 10.24 9 6 12 20.69 9.04 9 6 12 21.45 9.96 9 -6 12 9.93 2.55 9 6 12 22.10 10.09 10 6 12 1.05 4.00 10 6 12 -0.12 3.04 10 6 12 0.49 4.63 11 6 12 1.58 3.67 11 6 12 1.42 2.81 11 6 12 0.68 3.80 12 6 12 -0.09 3.47 12 6 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19 12.86 10.39 -14 3 19 8.48 7.12 -14 -3 19 8.94 7.39 -13 3 19 14.11 6.80 -13 3 19 12.76 10.17 -13 3 19 8.02 3.24 -13 -3 19 6.87 4.03 -11 3 19 18.32 7.52 -11 3 19 14.57 7.24 -11 3 19 18.89 8.81 -11 3 19 10.73 5.94 -10 3 19 -0.07 1.73 -10 3 19 0.00 2.49 -9 3 19 0.16 1.56 -9 3 19 -0.01 1.29 -9 3 19 -0.22 2.24 -9 -3 19 -0.24 2.43 -9 3 19 -0.13 1.23 -8 3 19 2.21 1.54 -8 3 19 1.96 1.43 -8 3 19 1.87 2.36 -7 3 19 24.69 9.87 -7 3 19 19.92 8.19 -7 3 19 20.50 9.64 -7 -3 19 28.01 12.87 -6 3 19 1.14 2.00 -6 3 19 1.05 2.44 -5 3 19 11.15 5.46 -5 3 19 12.02 5.92 -5 3 19 8.78 7.61 -5 -3 19 11.54 6.91 -4 3 19 16.53 6.69 -4 3 19 19.98 8.11 -4 3 19 14.58 8.68 -3 3 19 0.04 1.29 -3 3 19 -0.09 2.34 -3 3 19 -0.75 3.17 -2 3 19 33.64 13.81 -2 3 19 39.15 16.55 -2 3 19 32.36 15.70 -2 -3 19 22.04 14.16 -1 3 19 -0.06 1.44 -1 3 19 -0.49 2.69 -1 3 19 -0.17 3.04 -1 -3 19 0.04 1.38 0 3 19 24.08 10.03 0 3 19 26.53 11.63 0 -3 19 13.62 8.11 0 3 19 21.57 10.08 0 -3 19 11.75 9.77 1 3 19 -0.01 1.51 1 3 19 -0.18 2.96 1 -3 19 -0.32 1.74 1 -3 19 0.07 1.27 2 3 19 0.78 1.77 2 3 19 1.04 2.77 2 -3 19 -0.41 2.24 2 3 19 0.71 2.69 2 -3 19 0.01 1.60 -16 4 19 3.07 3.25 -16 4 19 2.86 3.13 -15 4 19 1.40 1.94 -15 4 19 1.14 1.56 -14 4 19 9.47 7.62 -14 4 19 6.06 3.64 -14 -4 19 6.32 3.55 -13 4 19 -0.19 1.91 -12 4 19 0.03 1.66 -12 4 19 -0.15 1.43 -11 4 19 3.49 3.70 -11 4 19 2.26 1.83 -10 4 19 1.34 1.60 -10 4 19 1.70 3.04 -10 4 19 0.91 1.49 -9 4 19 -0.13 1.37 -9 4 19 -0.25 2.54 -9 4 19 -0.06 1.34 -8 4 19 3.82 2.58 -8 4 19 4.19 3.68 -8 -4 19 4.41 3.73 -8 4 19 3.39 2.44 -7 4 19 -0.36 1.31 -7 4 19 -0.26 2.56 -7 -4 19 -0.20 3.24 -6 4 19 30.68 11.83 -6 4 19 27.37 10.90 -6 4 19 27.42 12.88 -6 -4 19 33.99 15.67 -5 4 19 1.93 1.56 -5 4 19 1.78 1.35 -5 4 19 1.73 2.90 -5 4 19 1.44 2.70 -4 4 19 26.95 10.78 -4 4 19 28.56 2.71 -4 4 19 31.24 12.04 -4 4 19 23.21 12.43 -3 4 19 24.62 10.19 -3 4 19 26.98 11.18 -3 4 19 29.19 12.58 -3 4 19 23.82 11.62 -3 -4 19 17.92 9.81 -2 4 19 37.97 15.53 -2 4 19 45.74 5.55 -2 4 19 46.04 7.00 -2 4 19 37.77 17.52 -2 -4 19 24.04 12.66 -1 4 19 0.25 1.25 -1 4 19 0.26 1.29 -1 4 19 0.34 2.81 -1 4 19 0.22 3.04 -1 -4 19 0.12 1.21 0 4 19 4.21 4.12 0 4 19 4.61 4.89 0 -4 19 3.79 4.20 0 4 19 4.05 4.99 0 -4 19 2.00 2.01 1 4 19 1.00 1.42 1 -4 19 0.81 2.24 2 4 19 50.84 12.57 2 4 19 54.43 14.79 2 -4 19 56.16 17.02 -15 5 19 0.86 1.59 -15 5 19 0.53 1.58 -15 5 19 0.41 1.44 -14 5 19 0.48 1.72 -14 5 19 0.57 1.83 -14 5 19 0.34 1.36 -13 5 19 1.87 1.81 -13 5 19 1.67 1.91 -13 5 19 1.05 1.41 -12 5 19 8.09 2.05 -12 5 19 7.61 4.22 -12 5 19 4.50 3.90 -11 5 19 9.04 7.29 -11 5 19 8.00 2.20 -11 5 19 5.45 4.63 -10 5 19 2.66 2.08 -10 5 19 1.79 1.72 -9 5 19 1.69 1.70 -9 5 19 2.05 3.45 -9 5 19 1.30 1.52 -8 5 19 8.69 6.26 -8 5 19 11.21 6.38 -8 5 19 6.86 5.14 -7 5 19 1.99 1.51 -7 5 19 1.41 1.82 -7 5 19 2.09 3.12 -7 -5 19 2.67 2.82 -6 5 19 7.77 5.58 -6 5 19 6.34 4.83 -6 5 19 8.35 6.68 -5 5 19 4.95 4.06 -5 5 19 4.02 3.86 -5 5 19 5.59 5.34 -4 5 19 25.55 10.52 -4 5 19 27.65 11.94 -4 5 19 27.64 12.27 -4 -5 19 21.88 10.53 -3 5 19 26.81 11.03 -3 5 19 27.59 11.85 -3 5 19 30.53 13.48 -3 -5 19 18.14 9.42 -2 5 19 9.68 7.59 -2 5 19 10.06 8.20 -2 5 19 9.78 8.10 -2 -5 19 5.32 4.48 -1 5 19 0.76 1.14 -1 5 19 0.42 2.70 -1 -5 19 0.84 1.98 -1 5 19 0.88 2.98 -1 -5 19 0.43 1.29 0 5 19 11.64 6.74 0 5 19 11.75 7.37 0 -5 19 13.26 8.41 0 5 19 12.06 7.46 0 -5 19 7.61 5.34 1 5 19 8.35 5.65 1 5 19 9.81 6.73 1 -5 19 10.05 6.50 1 5 19 9.63 6.37 -14 6 19 5.16 4.52 -14 6 19 4.69 4.20 -14 6 19 3.67 3.88 -13 6 19 0.00 1.82 -13 6 19 -0.11 1.78 -12 6 19 2.51 3.00 -12 6 19 2.28 2.49 -12 6 19 1.36 1.50 -11 6 19 0.05 1.95 -11 6 19 -0.30 1.89 -11 6 19 0.08 1.41 -10 6 19 0.20 2.08 -10 6 19 -0.27 1.93 -10 6 19 -0.28 1.54 -9 6 19 6.95 5.25 -9 6 19 6.12 4.96 -9 6 19 4.76 4.05 -8 6 19 20.48 9.71 -8 6 19 17.39 8.25 -8 6 19 25.02 11.02 -8 6 19 13.13 2.64 -7 6 19 1.19 1.95 -7 6 19 1.07 1.63 -7 6 19 2.16 3.72 -6 6 19 10.85 8.61 -6 6 19 9.08 7.21 -6 6 19 11.37 9.45 -5 6 19 1.78 1.99 -5 6 19 1.41 1.62 -5 6 19 2.17 3.96 -5 -6 19 0.91 1.79 -4 6 19 25.68 10.67 -4 6 19 21.59 8.97 -4 6 19 26.91 11.50 -4 -6 19 15.12 7.74 -3 6 19 22.00 9.13 -3 6 19 19.61 9.13 -3 6 19 17.25 8.61 -3 6 19 21.95 9.52 -3 -6 19 13.18 3.47 -2 6 19 3.36 3.34 -2 6 19 4.45 5.08 -2 -6 19 1.99 2.04 -1 6 19 16.05 9.10 -1 6 19 15.21 8.99 -1 -6 19 20.81 8.20 -1 6 19 20.76 7.24 -1 -6 19 11.69 7.13 0 6 19 1.29 2.60 -13 7 19 -0.29 1.66 -13 7 19 -0.32 1.81 -13 7 19 -0.16 1.38 -12 7 19 0.61 1.75 -12 7 19 0.62 1.78 -12 7 19 0.21 1.54 -11 7 19 11.27 6.67 -11 7 19 11.55 6.86 -11 7 19 6.98 4.95 -10 7 19 1.86 2.31 -9 7 19 27.48 8.94 -9 7 19 24.82 8.10 -9 7 19 16.57 9.68 -8 7 19 0.99 2.18 -8 7 19 0.77 2.03 -8 7 19 0.56 1.56 -7 7 19 26.44 11.05 -7 7 19 24.42 10.18 -6 7 19 12.00 9.66 -6 7 19 11.06 8.75 -6 7 19 14.50 7.85 -6 -7 19 8.81 7.34 -5 7 19 56.11 13.52 -5 7 19 46.44 11.23 -5 7 19 56.65 14.14 -5 -7 19 35.63 10.86 -4 7 19 7.61 5.40 -4 7 19 6.24 2.25 -4 7 19 7.56 5.93 -4 -7 19 4.14 4.26 -3 7 19 11.88 3.45 -3 7 19 10.48 6.08 -3 7 19 11.00 6.84 -3 -7 19 6.90 4.92 -2 7 19 0.64 1.86 -2 7 19 0.57 1.36 -2 7 19 0.45 2.55 -2 -7 19 0.63 1.46 -1 7 19 22.00 7.25 -1 7 19 17.05 9.63 -1 7 19 18.14 10.65 -11 8 19 1.86 2.58 -10 8 19 2.76 3.10 -10 8 19 3.21 3.67 -10 8 19 1.94 2.13 -9 8 19 1.96 2.60 -9 8 19 2.55 3.18 -9 8 19 1.77 2.07 -8 8 19 21.47 7.36 -8 8 19 23.97 8.03 -8 8 19 16.16 9.46 -7 8 19 5.42 4.85 -7 8 19 5.46 5.00 -6 8 19 -0.08 2.04 -6 8 19 -0.09 1.94 -6 -8 19 0.37 2.00 -5 8 19 2.80 3.33 -5 8 19 2.71 3.08 -5 8 19 3.46 4.53 -5 -8 19 2.16 2.43 -4 8 19 32.74 10.45 -4 8 19 27.74 8.91 -4 8 19 31.24 10.39 -4 -8 19 19.76 7.12 -3 8 19 4.48 4.61 -3 8 19 3.96 4.09 -3 -8 19 2.55 2.81 -13 0 20 15.23 9.14 -12 0 20 2.30 2.58 -12 0 20 1.36 1.85 -11 0 20 -0.39 1.92 -11 0 20 -0.29 1.62 -10 0 20 44.53 5.69 -10 0 20 20.92 6.21 -9 0 20 6.86 4.02 -9 0 20 3.45 3.68 -8 0 20 5.17 4.35 -8 0 20 2.48 2.25 -7 0 20 0.80 1.67 -7 0 20 0.57 1.96 -6 0 20 16.78 7.94 -6 0 20 10.37 9.57 -5 0 20 2.12 1.83 -5 0 20 1.41 2.19 -4 0 20 3.87 3.98 -4 0 20 2.29 3.43 -3 0 20 1.24 2.31 -2 0 20 42.64 19.20 -1 0 20 55.42 20.46 -1 0 20 57.66 17.56 -14 1 20 5.76 5.21 -13 1 20 10.87 6.59 -13 -1 20 6.06 5.38 -12 -1 20 21.04 6.98 -12 1 20 23.75 7.89 -12 1 20 14.36 8.52 -12 -1 20 12.10 7.34 -11 -1 20 7.56 5.31 -11 1 20 7.87 5.59 -11 1 20 4.49 4.63 -11 -1 20 3.62 3.80 -10 1 20 0.10 1.64 -10 -1 20 0.41 1.48 -9 -1 20 2.49 1.97 -9 1 20 2.44 1.94 -9 1 20 1.19 1.75 -9 -1 20 1.18 2.00 -8 -1 20 6.32 3.59 -8 1 20 7.24 3.97 -8 1 20 3.79 4.03 -8 -1 20 3.98 3.83 -7 -1 20 1.59 1.61 -7 1 20 1.42 1.55 -7 1 20 0.61 1.95 -7 -1 20 0.83 2.25 -6 1 20 1.33 1.46 -6 1 20 0.87 1.99 -6 -1 20 0.74 2.18 -5 1 20 -0.23 1.46 -5 1 20 -0.82 2.41 -5 -1 20 -0.14 2.11 -4 1 20 13.10 7.56 -4 1 20 9.87 6.92 -4 1 20 9.11 6.59 -4 -1 20 9.30 6.69 -3 1 20 23.42 7.74 -3 1 20 18.16 11.97 -3 1 20 17.97 12.23 -2 1 20 8.56 5.93 -2 -1 20 6.42 5.12 -2 1 20 8.84 6.73 -1 1 20 31.22 12.00 -1 -1 20 20.32 9.87 -1 -1 20 22.79 10.10 -13 2 20 9.48 5.73 -13 -2 20 5.48 4.90 -12 2 20 1.22 2.03 -12 -2 20 0.69 1.52 -11 2 20 -0.12 1.88 -11 2 20 0.17 1.93 -10 2 20 -0.55 1.83 -10 2 20 -0.30 1.96 -9 2 20 13.77 6.63 -9 2 20 7.67 4.72 -9 -2 20 8.98 7.76 -8 2 20 1.25 1.77 -8 2 20 0.95 2.03 -7 2 20 5.10 4.18 -7 2 20 3.12 3.80 -7 -2 20 4.60 4.56 -6 2 20 4.24 3.55 -6 2 20 2.92 3.63 -6 -2 20 3.20 4.97 -5 2 20 0.32 1.43 -5 2 20 0.05 2.10 -5 2 20 0.36 2.30 -4 2 20 0.13 1.41 -4 2 20 0.15 2.51 -4 2 20 -0.12 2.75 -3 2 20 37.43 9.17 -3 2 20 36.68 12.16 -3 2 20 34.37 15.25 -2 2 20 0.27 1.36 -2 2 20 -0.15 2.67 -2 2 20 0.39 2.99 -2 -2 20 0.45 1.71 -1 2 20 -0.76 2.65 -1 2 20 0.67 2.84 -1 -2 20 0.25 1.51 -13 3 20 0.46 2.02 -13 -3 20 -0.02 1.55 -12 3 20 1.19 2.02 -11 3 20 9.76 5.86 -11 3 20 8.41 5.80 -11 -3 20 5.65 5.06 -10 3 20 -0.47 1.77 -10 3 20 -0.11 2.13 -10 -3 20 -0.26 1.91 -9 3 20 -0.02 1.71 -8 3 20 13.22 7.60 -8 3 20 9.28 5.96 -8 -3 20 11.79 4.59 -7 3 20 0.43 1.50 -7 3 20 0.08 2.07 -7 -3 20 0.14 2.46 -6 3 20 12.99 7.43 -6 3 20 10.02 6.26 -6 3 20 9.38 6.10 -6 -3 20 11.29 7.67 -5 3 20 8.18 5.50 -5 3 20 7.86 5.67 -5 3 20 6.25 3.43 -4 3 20 6.62 4.55 -4 3 20 6.13 5.52 -4 3 20 5.03 5.27 -3 3 20 0.24 1.21 -3 3 20 -0.17 2.53 -3 3 20 -0.47 2.85 -3 -3 20 0.34 1.60 -2 3 20 0.06 1.22 -2 3 20 -0.02 2.73 -2 -3 20 0.11 1.41 -2 3 20 0.91 3.03 -2 -3 20 0.02 1.44 -12 4 20 16.32 9.43 -12 4 20 12.84 7.47 -12 -4 20 9.21 5.71 -11 4 20 -0.17 1.99 -11 -4 20 -0.30 1.85 -10 4 20 0.06 1.91 -9 4 20 6.65 4.74 -9 4 20 5.84 5.05 -9 4 20 4.96 4.77 -9 -4 20 4.85 4.72 -8 4 20 -0.27 1.67 -8 4 20 -0.47 2.50 -8 -4 20 -0.50 2.36 -7 4 20 -0.09 1.58 -7 4 20 0.05 1.39 -7 4 20 0.02 2.23 -7 -4 20 -0.27 2.33 -6 4 20 2.93 3.01 -6 4 20 1.90 2.32 -6 4 20 2.52 3.50 -5 4 20 1.53 1.35 -5 4 20 1.11 2.56 -4 4 20 6.42 4.40 -4 4 20 5.79 5.31 -4 4 20 5.73 5.51 -4 -4 20 4.75 4.49 -3 4 20 2.51 2.57 -3 4 20 2.44 3.32 -3 4 20 2.83 3.74 -3 -4 20 1.57 1.55 -11 5 20 0.97 1.82 -11 -5 20 0.88 2.34 -10 5 20 1.26 1.73 -10 -5 20 1.81 2.88 -9 5 20 -0.19 1.62 -9 -5 20 0.37 2.42 -8 5 20 -0.80 2.63 -8 -5 20 0.21 2.40 -7 5 20 2.17 2.20 -7 5 20 2.71 3.61 -5 5 20 6.43 4.95 -5 -5 20 5.60 5.15 -4 5 20 2.91 3.05 -4 5 20 2.69 3.59 -4 -5 20 2.26 2.52 -8 6 20 6.76 4.89 -8 6 20 6.11 5.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 99968 _olex2_submission_original_sample_id PTS_T2_trans _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S001 S 0.03573(3) 0.38225(4) 0.33551(4) 0.0460(2) Uani 1 1 d . . . . . S002 S 0.46468(3) 0.86668(4) 0.67048(4) 0.0472(2) Uani 1 1 d . . . . . S003 S 0.30494(3) 0.82399(4) 0.61512(5) 0.0496(2) Uani 1 1 d . . . . . S004 S 0.19410(3) 0.42624(5) 0.38355(5) 0.0570(3) Uani 1 1 d . . . . . O005 O -0.02847(8) 0.63170(10) 0.30928(12) 0.0432(5) Uani 1 1 d . . . . . O006 O 0.14226(8) 0.53884(11) 0.51038(12) 0.0516(5) Uani 1 1 d . . . . . O007 O 0.35266(8) 0.71323(12) 0.49284(12) 0.0521(5) Uani 1 1 d . . . . . O008 O 0.53449(8) 0.61980(11) 0.67390(13) 0.0519(5) Uani 1 1 d . . . . . O009 O 0.76093(8) 0.39657(11) 1.17846(12) 0.0517(5) Uani 1 1 d . . . . . O00A O -0.25043(8) 0.86403(12) -0.18310(14) 0.0590(6) Uani 1 1 d . . . . . N00B N 0.57247(9) 0.56842(12) 0.98481(13) 0.0378(5) Uani 1 1 d . . . . . N00C N 0.53326(9) 0.53874(12) 0.92728(13) 0.0399(5) Uani 1 1 d . . . . . N00D N -0.06475(10) 0.68283(13) 0.00020(14) 0.0440(6) Uani 1 1 d . . . . . N00E N -0.02505(10) 0.71128(14) 0.05767(14) 0.0448(6) Uani 1 1 d . . . . . C00F C 0.03743(10) 0.51347(13) 0.38230(14) 0.0294(5) Uani 1 1 d . . . . . C00G C 0.09912(10) 0.57063(14) 0.21950(14) 0.0327(6) Uani 1 1 d . . . . . C00H C 0.44313(11) 0.66463(15) 0.58311(15) 0.0358(6) Uani 1 1 d . . . . . C00I C 0.40114(10) 0.67665(13) 0.77284(14) 0.0297(5) Uani 1 1 d . . . . . C00J C 0.07085(10) 0.46607(13) 0.35065(14) 0.0319(5) Uani 1 1 d . . . . . C00K C 0.35456(10) 0.72459(13) 0.71709(14) 0.0316(5) Uani 1 1 d . . . . . C00L C 0.48982(10) 0.58856(14) 0.87755(15) 0.0340(6) Uani 1 1 d . . . . . C00M C 0.61726(10) 0.52023(14) 1.03498(15) 0.0324(5) Uani 1 1 d . . . . . C00N C 0.39966(10) 0.60214(14) 0.76010(15) 0.0321(5) Uani 1 1 d . . . . . C00O C 0.05728(10) 0.58764(13) 0.40983(15) 0.0312(5) Uani 1 1 d . . . . . C00P C 0.44467(11) 0.55892(14) 0.81216(15) 0.0348(6) Uani 1 1 d . . . . . H00P H 0.444563 0.509303 0.803054 0.042 Uiso 1 1 calc R U . . . C00Q C 0.42842(10) 0.78394(14) 0.64806(15) 0.0339(6) Uani 1 1 d . . . . . C00R C 0.46231(10) 0.73807(14) 0.61486(14) 0.0332(6) Uani 1 1 d . . . . . C00S C 0.13001(10) 0.47720(14) 0.33257(15) 0.0338(6) Uani 1 1 d . . . . . C00T C 0.05148(11) 0.53994(15) 0.15546(15) 0.0348(6) Uani 1 1 d . . . . . C00U C 0.61675(11) 0.44591(15) 1.02824(15) 0.0371(6) Uani 1 1 d . . . . . H00U H 0.584052 0.422730 0.990613 0.045 Uiso 1 1 calc R U . . . C00V C 0.11051(11) 0.59915(15) 0.47659(16) 0.0385(6) Uani 1 1 d . . . . . C00W C 0.44642(11) 0.70718(14) 0.84001(15) 0.0329(5) Uani 1 1 d . . . . . C00X C 0.49015(11) 0.66240(14) 0.89109(15) 0.0363(6) Uani 1 1 d . . . . . H00X H 0.520143 0.682227 0.935075 0.044 Uiso 1 1 calc R U . . . C00Y C 0.71381(11) 0.44075(15) 1.13424(15) 0.0372(6) Uani 1 1 d . . . . . C00Z C 0.36886(10) 0.77203(14) 0.66425(15) 0.0326(6) Uani 1 1 d . . . . . C010 C 0.14413(10) 0.52284(15) 0.27765(15) 0.0356(6) Uani 1 1 d . . . . . C011 C 0.66412(11) 0.55342(15) 1.09463(16) 0.0391(6) Uani 1 1 d . . . . . H011 H 0.663034 0.603310 1.101251 0.047 Uiso 1 1 calc R U . . . C012 C 0.10519(10) 0.64550(15) 0.22732(16) 0.0370(6) Uani 1 1 d . . . . . C013 C 0.02181(11) 0.64700(14) 0.37403(16) 0.0364(6) Uani 1 1 d . . . . . C014 C 0.66505(11) 0.40613(15) 1.07768(16) 0.0384(6) Uani 1 1 d . . . . . H014 H 0.665016 0.355977 1.073191 0.046 Uiso 1 1 calc R U . . . C015 C 0.01060(11) 0.58571(15) 0.10112(15) 0.0379(6) Uani 1 1 d . . . . . H015 H -0.021258 0.565917 0.059251 0.046 Uiso 1 1 calc R U . . . C016 C -0.10838(11) 0.73307(15) -0.04893(16) 0.0390(6) Uani 1 1 d . . . . . C017 C 0.38799(11) 0.65320(16) 0.51959(16) 0.0408(6) Uani 1 1 d . . . . . C018 C 0.01638(11) 0.65966(15) 0.10814(16) 0.0382(6) Uani 1 1 d . . . . . C019 C -0.15753(12) 0.70194(16) -0.10764(19) 0.0483(7) Uani 1 1 d . . . . . H019 H -0.158270 0.652144 -0.115738 0.058 Uiso 1 1 calc R U . . . C01A C -0.11826(12) 0.66001(15) 0.20011(18) 0.0430(7) Uani 1 1 d . . . . . H01A H -0.143400 0.629535 0.224080 0.052 Uiso 1 1 calc R U . . . H01B H -0.102219 0.630182 0.164391 0.052 Uiso 1 1 calc R U . . . C01B C -0.15321(12) 0.84994(16) -0.08733(17) 0.0454(7) Uani 1 1 d . . . . . H01C H -0.151370 0.900012 -0.081630 0.054 Uiso 1 1 calc R U . . . C01C C 0.71258(11) 0.51400(15) 1.14466(17) 0.0405(6) Uani 1 1 d . . . . . H01L H 0.743809 0.536908 1.184713 0.049 Uiso 1 1 calc R U . . . C01D C 0.29057(11) 0.73041(17) 0.71566(17) 0.0432(7) Uani 1 1 d . . . . . H01M H 0.272594 0.701878 0.747275 0.052 Uiso 1 1 calc R U . . . C01E C -0.06459(12) 0.69067(15) 0.26613(18) 0.0422(6) Uani 1 1 d . . . . . H01D H -0.038974 0.721025 0.242759 0.051 Uiso 1 1 calc R U . . . H01E H -0.080137 0.719964 0.302742 0.051 Uiso 1 1 calc R U . . . C01F C -0.10520(12) 0.80738(16) -0.04086(17) 0.0434(7) Uani 1 1 d . . . . . H01F H -0.070864 0.828831 -0.004274 0.052 Uiso 1 1 calc R U . . . C01G C -0.01742(11) 0.48113(15) 0.39292(16) 0.0386(6) Uani 1 1 d . . . . . H01G H -0.045851 0.505887 0.413082 0.046 Uiso 1 1 calc R U . . . C01H C 0.66389(11) 0.53149(16) 0.83254(18) 0.0439(7) Uani 1 1 d . . . . . H01N H 0.639006 0.505053 0.860617 0.053 Uiso 1 1 calc R U . . . H01P H 0.676417 0.497848 0.796984 0.053 Uiso 1 1 calc R U . . . C01I C 0.06369(11) 0.68940(16) 0.17156(16) 0.0402(6) Uani 1 1 d . . . . . H01I H 0.067474 0.739426 0.176542 0.048 Uiso 1 1 calc R U . . . C01J C -0.20542(12) 0.74427(16) -0.15424(19) 0.0500(7) Uani 1 1 d . . . . . H01J H -0.238398 0.723116 -0.193397 0.060 Uiso 1 1 calc R U . . . C01K C 0.48148(12) 0.60512(16) 0.61177(17) 0.0428(7) Uani 1 1 d . . . . . C01L C 0.34986(12) 0.56762(16) 0.69185(17) 0.0437(7) Uani 1 1 d . . . . . H01Q H 0.311536 0.565384 0.706047 0.066 Uiso 1 1 calc R U . . . H01R H 0.362560 0.519571 0.682554 0.066 Uiso 1 1 calc R U . . . H01S H 0.343778 0.595945 0.643485 0.066 Uiso 1 1 calc R U . . . C01M C -0.20401(12) 0.81784(16) -0.14234(17) 0.0433(7) Uani 1 1 d . . . . . C01N C 0.51807(11) 0.77139(17) 0.60897(16) 0.0442(7) Uani 1 1 d . . . . . H01T H 0.546946 0.747961 0.588430 0.053 Uiso 1 1 calc R U . . . C01O C -0.02379(12) 0.41099(16) 0.37070(17) 0.0462(7) Uani 1 1 d . . . . . H01O H -0.056714 0.381792 0.374165 0.055 Uiso 1 1 calc R U . . . C01P C 0.62422(12) 0.59121(17) 0.78167(19) 0.0487(7) Uani 1 1 d . . . . . H01U H 0.607368 0.621458 0.816234 0.058 Uiso 1 1 calc R U . . . H01X H 0.650293 0.621320 0.758768 0.058 Uiso 1 1 calc R U . . . C01Q C -0.15869(12) 0.71969(16) 0.15119(17) 0.0443(7) Uani 1 1 d . . . . . H01H H -0.169439 0.753553 0.187991 0.053 Uiso 1 1 calc R U . . . H01K H -0.135020 0.745800 0.121200 0.053 Uiso 1 1 calc R U . . . C01R C 0.37206(14) 0.58510(19) 0.48699(19) 0.0551(8) Uani 1 1 d . . . . . H01Z H 0.335329 0.578034 0.445452 0.066 Uiso 1 1 calc R U . . . C01S C 0.25914(12) 0.78108(17) 0.66421(19) 0.0488(7) Uani 1 1 d . . . . . H01 H 0.217202 0.791603 0.656226 0.059 Uiso 1 1 calc R U . . . C01T C 0.57148(13) 0.56095(17) 0.71427(19) 0.0485(7) Uani 1 1 d . . . . . H1 H 0.587781 0.534063 0.676574 0.058 Uiso 1 1 calc R U . . . H H 0.546446 0.528427 0.736136 0.058 Uiso 1 1 calc R U . . . C01U C 0.76092(12) 0.50453(16) 0.94744(18) 0.0470(7) Uani 1 1 d . . . . . H2 H 0.742660 0.478007 0.980367 0.056 Uiso 1 1 calc R U . . . C01V C 0.20817(11) 0.51576(19) 0.27874(18) 0.0524(8) Uani 1 1 d . . . . . H01V H 0.226012 0.542555 0.245577 0.063 Uiso 1 1 calc R U . . . C01W C 0.12700(13) 0.66834(17) 0.50617(18) 0.0490(7) Uani 1 1 d . . . . . H01W H 0.162105 0.675950 0.550039 0.059 Uiso 1 1 calc R U . . . C01X C 0.44767(13) 0.78632(16) 0.85917(18) 0.0469(7) Uani 1 1 d . . . . . H3 H 0.473644 0.811070 0.832204 0.070 Uiso 1 1 calc R U . . . HA H 0.464065 0.793162 0.916661 0.070 Uiso 1 1 calc R U . . . HB H 0.406099 0.805460 0.840942 0.070 Uiso 1 1 calc R U . . . C01Y C 0.03835(14) 0.71639(16) 0.4035(2) 0.0503(7) Uani 1 1 d . . . . . H01Y H 0.014777 0.756189 0.379426 0.060 Uiso 1 1 calc R U . . . C01Z C 0.84689(13) 0.45578(18) 1.14144(19) 0.0520(8) Uani 1 1 d . . . . . H4 H 0.890268 0.469433 1.164216 0.062 Uiso 1 1 calc R U . . . HC H 0.823717 0.499149 1.119471 0.062 Uiso 1 1 calc R U . . . C020 C 0.09055(15) 0.72516(17) 0.4694(2) 0.0532(8) Uani 1 1 d . . . . . H020 H 0.101280 0.771550 0.489599 0.064 Uiso 1 1 calc R U . . . C021 C 0.04407(14) 0.45994(17) 0.14288(17) 0.0497(7) Uani 1 1 d . . . . . H02A H 0.083924 0.436851 0.163477 0.075 Uiso 1 1 calc R U . . . H02B H 0.027514 0.449864 0.086031 0.075 Uiso 1 1 calc R U . . . H02C H 0.016014 0.441788 0.171063 0.075 Uiso 1 1 calc R U . . . C022 C 0.52499(12) 0.84013(18) 0.63603(18) 0.0511(8) Uani 1 1 d . . . . . H022 H 0.558657 0.869496 0.635875 0.061 Uiso 1 1 calc R U . . . C023 C 0.82285(13) 0.42693(19) 1.20840(19) 0.0552(8) Uani 1 1 d . . . . . H02V H 0.851134 0.389920 1.237924 0.066 Uiso 1 1 calc R U . . . H02W H 0.822216 0.465820 1.245936 0.066 Uiso 1 1 calc R U . . . C024 C 0.72174(13) 0.56095(17) 0.8943(2) 0.0547(8) Uani 1 1 d . . . . . H02X H 0.746980 0.586142 0.865758 0.066 Uiso 1 1 calc R U . . . H02Y H 0.708978 0.596030 0.928218 0.066 Uiso 1 1 calc R U . . . C025 C -0.31265(13) 0.8364(2) -0.2153(2) 0.0629(9) Uani 1 1 d . . . . . H02D H -0.312566 0.799716 -0.255441 0.075 Uiso 1 1 calc R U . . . H02E H -0.339577 0.875450 -0.242604 0.075 Uiso 1 1 calc R U . . . C026 C 0.15490(12) 0.67987(18) 0.29604(18) 0.0497(7) Uani 1 1 d . . . . . H02F H 0.154986 0.657370 0.346269 0.075 Uiso 1 1 calc R U . . . H02G H 0.146383 0.730609 0.298383 0.075 Uiso 1 1 calc R U . . . H02H H 0.194913 0.673463 0.287166 0.075 Uiso 1 1 calc R U . . . C027 C 0.84195(15) 0.40245(17) 1.0727(2) 0.0559(8) Uani 1 1 d . . . . . H02Z H 0.868105 0.360900 1.093678 0.067 Uiso 1 1 calc R U . . . HD H 0.799220 0.385534 1.052970 0.067 Uiso 1 1 calc R U . . . C028 C 0.23965(13) 0.4666(2) 0.3324(2) 0.0654(10) Uani 1 1 d . . . . . H028 H 0.281577 0.455854 0.340701 0.078 Uiso 1 1 calc R U . . . C029 C 0.41095(17) 0.52848(19) 0.5166(2) 0.0620(9) Uani 1 1 d . . . . . H029 H 0.400604 0.482723 0.494233 0.074 Uiso 1 1 calc R U . . . C02A C 0.81858(13) 0.48929(18) 0.9516(2) 0.0544(8) Uani 1 1 d . . . . . H02 H 0.835818 0.516694 0.918238 0.065 Uiso 1 1 calc R U . . . C02B C -0.25779(15) 0.74813(18) 0.0406(2) 0.0622(9) Uani 1 1 d . . . . . H02I H -0.239248 0.775701 0.008787 0.075 Uiso 1 1 calc R U . . . C02C C 0.46611(15) 0.53749(19) 0.5798(2) 0.0573(8) Uani 1 1 d . . . . . H5 H 0.491900 0.498153 0.599674 0.069 Uiso 1 1 calc R U . . . C02D C -0.21770(14) 0.69117(19) 0.0927(2) 0.0691(10) Uani 1 1 d . . . . . H02J H -0.206698 0.655566 0.057841 0.083 Uiso 1 1 calc R U . . . H02K H -0.241879 0.666686 0.123218 0.083 Uiso 1 1 calc R U . . . C02E C 0.86086(15) 0.4337(2) 1.0027(2) 0.0621(9) Uani 1 1 d . . . . . H6 H 0.901844 0.455194 1.024031 0.074 Uiso 1 1 calc R U . . . HE H 0.864899 0.394044 0.967631 0.074 Uiso 1 1 calc R U . . . C02F C -0.33956(14) 0.80417(19) -0.1524(2) 0.0617(9) Uani 1 1 d . . . . . H02L H -0.317132 0.759969 -0.131995 0.074 Uiso 1 1 calc R U . . . H02M H -0.382735 0.791280 -0.178309 0.074 Uiso 1 1 calc R U . . . C02G C -0.33680(17) 0.85410(19) -0.0810(2) 0.0676(10) Uani 1 1 d . . . . . H02N H -0.294298 0.871080 -0.058598 0.081 Uiso 1 1 calc R U . . . H02O H -0.362885 0.896003 -0.100654 0.081 Uiso 1 1 calc R U . . . C02H C -0.35772(16) 0.8188(2) -0.0141(2) 0.0743(11) Uani 1 1 d . . . . . H02P H -0.363553 0.856364 0.022290 0.089 Uiso 1 1 calc R U . . . H02Q H -0.398001 0.796364 -0.038179 0.089 Uiso 1 1 calc R U . . . C02I C -0.31490(16) 0.7630(2) 0.0350(2) 0.0735(11) Uani 1 1 d . . . . . H02R H -0.332468 0.734232 0.066833 0.088 Uiso 1 1 calc R U . . . C02J C 0.29309(14) 0.7037(2) 0.4350(2) 0.0694(10) Uani 1 1 d . . . . . H7 H 0.298218 0.681664 0.386928 0.104 Uiso 1 1 calc R U . . . HF H 0.273150 0.749854 0.421669 0.104 Uiso 1 1 calc R U . . . HG H 0.267785 0.673002 0.457581 0.104 Uiso 1 1 calc R U . . . C02K C 0.20298(14) 0.5483(2) 0.5661(2) 0.0729(11) Uani 1 1 d . . . . . H02S H 0.228490 0.575575 0.540500 0.109 Uiso 1 1 calc R U . . . H02T H 0.221641 0.501819 0.582034 0.109 Uiso 1 1 calc R U . . . H02U H 0.199576 0.573880 0.613069 0.109 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S001 0.0459(4) 0.0308(4) 0.0490(4) -0.0005(3) -0.0055(3) -0.0048(3) S002 0.0379(4) 0.0401(4) 0.0517(5) 0.0070(3) -0.0057(3) -0.0111(3) S003 0.0283(4) 0.0524(5) 0.0567(5) 0.0205(4) -0.0055(3) 0.0138(3) S004 0.0331(4) 0.0632(5) 0.0602(5) 0.0191(4) -0.0094(3) 0.0245(3) O005 0.0276(9) 0.0321(10) 0.0550(12) 0.0006(8) -0.0115(8) 0.0041(7) O006 0.0272(9) 0.0522(12) 0.0527(12) 0.0032(10) -0.0240(8) -0.0094(9) O007 0.0255(10) 0.0599(13) 0.0499(12) 0.0036(10) -0.0220(8) -0.0060(9) O008 0.0291(10) 0.0502(12) 0.0586(13) 0.0023(10) -0.0153(9) 0.0055(9) O009 0.0316(10) 0.0545(13) 0.0573(12) 0.0274(10) -0.0057(9) 0.0119(9) O00A 0.0339(11) 0.0575(13) 0.0687(14) 0.0309(11) -0.0116(10) 0.0132(9) N00B 0.0220(10) 0.0407(13) 0.0407(12) 0.0024(10) -0.0065(9) 0.0053(9) N00C 0.0284(11) 0.0427(13) 0.0379(12) 0.0039(10) -0.0071(10) 0.0045(10) N00D 0.0283(11) 0.0501(14) 0.0431(13) 0.0045(11) -0.0060(10) 0.0042(10) N00E 0.0304(12) 0.0527(15) 0.0418(13) 0.0072(11) -0.0045(10) 0.0055(10) C00F 0.0156(11) 0.0296(12) 0.0321(12) 0.0013(10) -0.0102(9) -0.0022(9) C00G 0.0138(11) 0.0496(15) 0.0291(12) 0.0060(11) -0.0025(9) 0.0059(10) C00H 0.0211(12) 0.0472(15) 0.0316(13) 0.0020(12) -0.0042(10) -0.0033(11) C00I 0.0165(11) 0.0370(14) 0.0289(12) 0.0043(10) -0.0036(9) -0.0004(10) C00J 0.0232(12) 0.0281(13) 0.0303(13) 0.0028(10) -0.0144(10) 0.0002(10) C00K 0.0194(11) 0.0358(13) 0.0314(13) 0.0040(11) -0.0056(10) -0.0005(10) C00L 0.0220(12) 0.0372(14) 0.0353(14) 0.0061(11) -0.0031(10) 0.0042(10) C00M 0.0210(12) 0.0362(14) 0.0331(13) 0.0036(11) -0.0031(10) 0.0045(10) C00N 0.0224(12) 0.0354(13) 0.0322(13) 0.0039(11) -0.0018(10) -0.0043(10) C00O 0.0188(11) 0.0328(13) 0.0351(13) -0.0025(11) -0.0032(10) -0.0057(10) C00P 0.0274(13) 0.0337(13) 0.0359(14) 0.0018(11) -0.0025(11) 0.0004(10) C00Q 0.0206(12) 0.0365(14) 0.0329(13) 0.0090(11) -0.0105(10) -0.0026(10) C00R 0.0180(11) 0.0433(15) 0.0288(12) 0.0067(11) -0.0083(9) -0.0039(10) C00S 0.0207(12) 0.0387(14) 0.0308(13) 0.0023(11) -0.0098(10) 0.0097(10) C00T 0.0234(12) 0.0450(15) 0.0287(13) 0.0008(11) -0.0037(10) 0.0067(11) C00U 0.0277(13) 0.0420(15) 0.0331(13) -0.0025(12) -0.0047(10) -0.0004(11) C00V 0.0250(13) 0.0458(16) 0.0374(14) -0.0076(12) -0.0028(11) -0.0152(11) C00W 0.0246(12) 0.0361(14) 0.0300(13) 0.0002(11) -0.0045(10) 0.0002(10) C00X 0.0236(12) 0.0413(14) 0.0329(13) -0.0004(12) -0.0092(10) -0.0013(11) C00Y 0.0269(13) 0.0438(15) 0.0346(14) 0.0122(12) -0.0009(11) 0.0108(11) C00Z 0.0190(11) 0.0367(14) 0.0320(13) 0.0059(11) -0.0086(10) 0.0027(10) C010 0.0162(11) 0.0482(15) 0.0338(13) 0.0035(12) -0.0063(10) 0.0071(10) C011 0.0253(13) 0.0343(14) 0.0478(16) -0.0013(12) -0.0049(11) 0.0032(11) C012 0.0207(12) 0.0479(16) 0.0366(14) 0.0070(12) -0.0008(10) -0.0014(11) C013 0.0241(12) 0.0340(14) 0.0439(15) -0.0053(12) -0.0013(11) -0.0052(10) C014 0.0344(14) 0.0321(13) 0.0423(15) 0.0021(12) 0.0010(11) 0.0024(11) C015 0.0215(12) 0.0534(17) 0.0291(13) 0.0035(12) -0.0081(10) 0.0040(11) C016 0.0274(13) 0.0426(15) 0.0384(14) 0.0088(12) -0.0041(11) 0.0058(11) C017 0.0284(13) 0.0521(17) 0.0328(14) -0.0013(13) -0.0054(11) -0.0114(12) C018 0.0243(12) 0.0483(16) 0.0356(14) 0.0110(12) -0.0011(11) 0.0074(11) C019 0.0306(14) 0.0391(15) 0.0619(19) 0.0076(14) -0.0072(13) 0.0022(12) C01A 0.0286(13) 0.0394(15) 0.0541(17) 0.0113(13) 0.0011(12) 0.0068(11) C01B 0.0395(15) 0.0377(15) 0.0485(16) 0.0057(13) -0.0036(13) 0.0047(12) C01C 0.0246(13) 0.0424(15) 0.0417(15) -0.0026(12) -0.0102(11) -0.0009(11) C01D 0.0191(12) 0.0627(18) 0.0429(15) 0.0085(14) 0.0012(11) 0.0021(12) C01E 0.0343(14) 0.0345(14) 0.0514(17) 0.0055(13) 0.0022(12) 0.0073(11) C01F 0.0283(13) 0.0514(17) 0.0384(15) 0.0017(13) -0.0093(11) 0.0027(12) C01G 0.0189(12) 0.0452(15) 0.0436(15) 0.0005(12) -0.0038(10) -0.0046(11) C01H 0.0259(13) 0.0466(16) 0.0520(17) 0.0065(13) -0.0002(12) 0.0061(12) C01I 0.0272(13) 0.0437(16) 0.0405(15) 0.0077(12) -0.0047(11) 0.0004(11) C01J 0.0279(14) 0.0479(17) 0.0573(18) 0.0063(14) -0.0142(13) -0.0001(12) C01K 0.0276(13) 0.0508(17) 0.0422(15) -0.0036(13) -0.0022(11) -0.0029(12) C01L 0.0340(14) 0.0460(16) 0.0389(15) -0.0006(13) -0.0086(12) -0.0080(12) C01M 0.0290(14) 0.0476(17) 0.0424(15) 0.0164(13) -0.0066(12) 0.0083(12) C01N 0.0189(12) 0.064(2) 0.0406(15) 0.0098(14) -0.0051(11) -0.0075(12) C01O 0.0303(14) 0.0455(16) 0.0504(17) 0.0024(13) -0.0077(12) -0.0193(12) C01P 0.0263(14) 0.0505(17) 0.0594(18) 0.0093(15) -0.0028(13) 0.0065(12) C01Q 0.0339(14) 0.0431(16) 0.0478(16) 0.0128(13) -0.0009(12) 0.0073(12) C01R 0.0437(17) 0.067(2) 0.0425(17) -0.0055(15) -0.0070(13) -0.0168(16) C01S 0.0182(13) 0.0618(19) 0.0573(18) 0.0046(15) -0.0032(12) 0.0101(12) C01T 0.0333(14) 0.0498(17) 0.0536(17) 0.0040(14) -0.0015(13) 0.0101(13) C01U 0.0345(15) 0.0446(16) 0.0507(17) 0.0063(13) -0.0054(12) -0.0037(12) C01V 0.0195(13) 0.080(2) 0.0532(17) 0.0111(16) 0.0032(12) 0.0140(14) C01W 0.0402(15) 0.0514(18) 0.0448(16) -0.0085(14) -0.0041(13) -0.0211(14) C01X 0.0452(16) 0.0388(16) 0.0425(16) -0.0029(13) -0.0095(13) 0.0024(13) C01Y 0.0463(17) 0.0323(15) 0.067(2) -0.0081(14) 0.0075(15) -0.0032(13) C01Z 0.0263(14) 0.0544(19) 0.0613(19) 0.0052(15) -0.0092(13) 0.0042(13) C020 0.0554(18) 0.0419(17) 0.0563(18) -0.0186(15) 0.0069(15) -0.0218(15) C021 0.0486(17) 0.0476(17) 0.0382(15) -0.0040(13) -0.0107(13) 0.0078(14) C022 0.0281(14) 0.063(2) 0.0500(17) 0.0135(15) -0.0083(12) -0.0217(13) C023 0.0301(14) 0.071(2) 0.0501(18) 0.0128(16) -0.0118(13) 0.0146(14) C024 0.0371(16) 0.0438(17) 0.067(2) 0.0088(15) -0.0104(14) -0.0001(13) C025 0.0352(16) 0.074(2) 0.060(2) 0.0210(18) -0.0170(14) 0.0150(15) C026 0.0294(14) 0.0599(19) 0.0472(17) 0.0049(14) -0.0089(12) -0.0101(13) C027 0.0528(18) 0.0442(17) 0.068(2) 0.0079(16) 0.0129(16) 0.0159(14) C028 0.0201(14) 0.090(3) 0.076(2) 0.008(2) -0.0028(14) 0.0239(15) C029 0.068(2) 0.054(2) 0.0541(19) -0.0185(17) 0.0026(17) -0.0154(17) C02A 0.0348(16) 0.0573(19) 0.063(2) 0.0149(16) 0.0019(14) 0.0011(14) C02B 0.0457(19) 0.0483(19) 0.072(2) 0.0144(16) -0.0163(16) -0.0072(15) C02C 0.0537(19) 0.0505(19) 0.060(2) -0.0069(16) 0.0049(16) 0.0029(15) C02D 0.0446(18) 0.0480(19) 0.091(3) 0.0199(18) -0.0176(17) -0.0053(15) C02E 0.0487(18) 0.064(2) 0.069(2) 0.0135(17) 0.0101(16) 0.0198(16) C02F 0.0296(15) 0.061(2) 0.074(2) 0.0161(18) -0.0166(15) 0.0030(14) C02G 0.066(2) 0.048(2) 0.080(2) 0.0183(18) 0.0066(19) 0.0186(17) C02H 0.059(2) 0.074(3) 0.084(3) 0.032(2) 0.0124(19) 0.0235(18) C02I 0.046(2) 0.068(2) 0.094(3) 0.039(2) 0.0006(18) 0.0023(17) C02J 0.0315(16) 0.078(2) 0.071(2) 0.0133(19) -0.0288(15) -0.0142(16) C02K 0.0336(16) 0.085(3) 0.072(2) 0.015(2) -0.0298(15) -0.0171(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C01O S001 C00J 92.08(13) . . C022 S002 C00Q 92.10(14) . . C01S S003 C00Z 91.79(13) . . C028 S004 C00S 91.86(14) . . C013 O005 C01E 118.4(2) . . C00V O006 C02K 117.7(2) . . C017 O007 C02J 118.0(2) . . C01K O008 C01T 118.6(2) . . C00Y O009 C023 118.0(2) . . C01M O00A C025 118.9(2) . . N00C N00B C00M 114.6(2) . . N00B N00C C00L 113.2(2) . . N00E N00D C016 113.9(2) . . N00D N00E C018 113.0(2) . . C00J C00F C00O 125.1(2) . . C00J C00F C01G 112.1(2) . . C01G C00F C00O 122.6(2) . . C00T C00G C010 119.9(2) . . C012 C00G C00T 120.3(2) . . C012 C00G C010 119.7(2) . . C017 C00H C00R 121.3(2) . . C01K C00H C00R 120.6(2) . . C01K C00H C017 117.9(3) . . C00N C00I C00K 120.4(2) . . C00N C00I C00W 120.1(2) . . C00W C00I C00K 119.5(2) . . C00F C00J S001 110.97(18) . . C00F C00J C00S 129.2(2) . . C00S C00J S001 119.80(19) . . C00Z C00K C00I 123.7(2) . . C00Z C00K C01D 111.6(2) . . C01D C00K C00I 124.5(2) . . C00P C00L N00C 116.2(2) . . C00X C00L N00C 124.3(2) . . C00X C00L C00P 119.5(2) . . C00U C00M N00B 125.6(2) . . C00U C00M C011 119.4(2) . . C011 C00M N00B 115.0(2) . . C00I C00N C01L 121.3(2) . . C00P C00N C00I 119.1(2) . . C00P C00N C01L 119.6(2) . . C00V C00O C00F 120.4(2) . . C013 C00O C00F 120.7(2) . . C013 C00O C00V 118.8(2) . . C00L C00P C00N 121.2(2) . . C00L C00P H00P 119.4 . . C00N C00P H00P 119.4 . . C00R C00Q S002 111.13(18) . . C00R C00Q C00Z 129.5(2) . . C00Z C00Q S002 119.3(2) . . C00Q C00R C00H 125.8(2) . . C00Q C00R C01N 111.5(2) . . C01N C00R C00H 122.5(2) . . C00J C00S S004 119.08(18) . . C010 C00S S004 111.19(18) . . C010 C00S C00J 129.7(2) . . C00G C00T C021 122.5(2) . . C015 C00T C00G 118.9(2) . . C015 C00T C021 118.7(2) . . C00M C00U H00U 120.2 . . C00M C00U C014 119.6(2) . . C014 C00U H00U 120.2 . . O006 C00V C00O 116.0(2) . . O006 C00V C01W 123.2(2) . . C01W C00V C00O 120.7(3) . . C00I C00W C01X 122.2(2) . . C00X C00W C00I 119.2(2) . . C00X C00W C01X 118.6(2) . . C00L C00X C00W 120.9(2) . . C00L C00X H00X 119.5 . . C00W C00X H00X 119.5 . . O009 C00Y C014 115.8(2) . . C01C C00Y O009 123.8(2) . . C01C C00Y C014 120.4(2) . . C00K C00Z S003 111.18(17) . . C00K C00Z C00Q 129.0(2) . . C00Q C00Z S003 119.81(18) . . C00S C010 C00G 125.6(2) . . C00S C010 C01V 111.4(2) . . C01V C010 C00G 122.8(2) . . C00M C011 H011 119.3 . . C00M C011 C01C 121.3(2) . . C01C C011 H011 119.3 . . C00G C012 C026 121.5(2) . . C01I C012 C00G 119.1(2) . . C01I C012 C026 119.4(3) . . O005 C013 C00O 115.4(2) . . O005 C013 C01Y 124.0(2) . . C00O C013 C01Y 120.6(2) . . C00U C014 C00Y 120.3(2) . . C00U C014 H014 119.9 . . C00Y C014 H014 119.9 . . C00T C015 H015 119.4 . . C018 C015 C00T 121.2(2) . . C018 C015 H015 119.4 . . C019 C016 N00D 115.1(2) . . C01F C016 N00D 125.3(2) . . C01F C016 C019 119.6(2) . . O007 C017 C00H 115.7(2) . . O007 C017 C01R 123.2(2) . . C01R C017 C00H 121.1(3) . . C015 C018 N00E 125.4(2) . . C015 C018 C01I 119.4(2) . . C01I C018 N00E 115.1(2) . . C016 C019 H019 119.7 . . C01J C019 C016 120.5(3) . . C01J C019 H019 119.7 . . H01A C01A H01B 108.0 . . C01E C01A H01A 109.4 . . C01E C01A H01B 109.4 . . C01E C01A C01Q 111.3(2) . . C01Q C01A H01A 109.4 . . C01Q C01A H01B 109.4 . . C01F C01B H01C 120.0 . . C01F C01B C01M 119.9(3) . . C01M C01B H01C 120.0 . . C00Y C01C C011 118.8(2) . . C00Y C01C H01L 120.6 . . C011 C01C H01L 120.6 . . C00K C01D H01M 123.4 . . C01S C01D C00K 113.3(2) . . C01S C01D H01M 123.4 . . O005 C01E C01A 108.3(2) . . O005 C01E H01D 110.0 . . O005 C01E H01E 110.0 . . C01A C01E H01D 110.0 . . C01A C01E H01E 110.0 . . H01D C01E H01E 108.4 . . C016 C01F C01B 119.9(2) . . C016 C01F H01F 120.1 . . C01B C01F H01F 120.1 . . C00F C01G H01G 123.5 . . C01O C01G C00F 113.0(2) . . C01O C01G H01G 123.5 . . H01N C01H H01P 107.9 . . C01P C01H H01N 109.1 . . C01P C01H H01P 109.1 . . C024 C01H H01N 109.1 . . C024 C01H H01P 109.1 . . C024 C01H C01P 112.3(2) . . C012 C01I C018 121.1(3) . . C012 C01I H01I 119.5 . . C018 C01I H01I 119.5 . . C019 C01J H01J 120.2 . . C01M C01J C019 119.6(3) . . C01M C01J H01J 120.2 . . O008 C01K C00H 115.1(2) . . C02C C01K O008 123.6(3) . . C02C C01K C00H 121.3(3) . . C00N C01L H01Q 109.5 . . C00N C01L H01R 109.5 . . C00N C01L H01S 109.5 . . H01Q C01L H01R 109.5 . . H01Q C01L H01S 109.5 . . H01R C01L H01S 109.5 . . O00A C01M C01B 115.8(3) . . O00A C01M C01J 123.9(3) . . C01J C01M C01B 120.3(2) . . C00R C01N H01T 123.3 . . C022 C01N C00R 113.5(3) . . C022 C01N H01T 123.3 . . S001 C01O H01O 124.1 . . C01G C01O S001 111.85(19) . . C01G C01O H01O 124.1 . . C01H C01P H01U 109.3 . . C01H C01P H01X 109.3 . . H01U C01P H01X 107.9 . . C01T C01P C01H 111.8(2) . . C01T C01P H01U 109.3 . . C01T C01P H01X 109.3 . . C01A C01Q H01H 109.1 . . C01A C01Q H01K 109.1 . . H01H C01Q H01K 107.8 . . C02D C01Q C01A 112.6(2) . . C02D C01Q H01H 109.1 . . C02D C01Q H01K 109.1 . . C017 C01R H01Z 120.5 . . C029 C01R C017 119.0(3) . . C029 C01R H01Z 120.5 . . S003 C01S H01 123.9 . . C01D C01S S003 112.16(19) . . C01D C01S H01 123.9 . . O008 C01T C01P 108.0(2) . . O008 C01T H1 110.1 . . O008 C01T H 110.1 . . C01P C01T H1 110.1 . . C01P C01T H 110.1 . . H1 C01T H 108.4 . . C024 C01U H2 117.2 . . C02A C01U H2 117.2 . . C02A C01U C024 125.5(3) . . C010 C01V H01V 123.4 . . C028 C01V C010 113.2(3) . . C028 C01V H01V 123.4 . . C00V C01W H01W 120.7 . . C020 C01W C00V 118.6(3) . . C020 C01W H01W 120.7 . . C00W C01X H3 109.5 . . C00W C01X HA 109.5 . . C00W C01X HB 109.5 . . H3 C01X HA 109.5 . . H3 C01X HB 109.5 . . HA C01X HB 109.5 . . C013 C01Y H01Y 120.6 . . C020 C01Y C013 118.7(3) . . C020 C01Y H01Y 120.6 . . H4 C01Z HC 107.6 . . C023 C01Z H4 108.7 . . C023 C01Z HC 108.7 . . C023 C01Z C027 114.0(3) . . C027 C01Z H4 108.7 . . C027 C01Z HC 108.7 . . C01W C020 C01Y 122.6(3) . . C01W C020 H020 118.7 . . C01Y C020 H020 118.7 . . C00T C021 H02A 109.5 . . C00T C021 H02B 109.5 . . C00T C021 H02C 109.5 . . H02A C021 H02B 109.5 . . H02A C021 H02C 109.5 . . H02B C021 H02C 109.5 . . S002 C022 H022 124.1 . . C01N C022 S002 111.74(19) . . C01N C022 H022 124.1 . . O009 C023 C01Z 112.6(2) . . O009 C023 H02V 109.1 . . O009 C023 H02W 109.1 . . C01Z C023 H02V 109.1 . . C01Z C023 H02W 109.1 . . H02V C023 H02W 107.8 . . C01H C024 H02X 108.7 . . C01H C024 H02Y 108.7 . . C01U C024 C01H 114.2(2) . . C01U C024 H02X 108.7 . . C01U C024 H02Y 108.7 . . H02X C024 H02Y 107.6 . . O00A C025 H02D 108.7 . . O00A C025 H02E 108.7 . . O00A C025 C02F 114.2(3) . . H02D C025 H02E 107.6 . . C02F C025 H02D 108.7 . . C02F C025 H02E 108.7 . . C012 C026 H02F 109.5 . . C012 C026 H02G 109.5 . . C012 C026 H02H 109.5 . . H02F C026 H02G 109.5 . . H02F C026 H02H 109.5 . . H02G C026 H02H 109.5 . . C01Z C027 H02Z 108.8 . . C01Z C027 HD 108.8 . . H02Z C027 HD 107.7 . . C02E C027 C01Z 113.8(3) . . C02E C027 H02Z 108.8 . . C02E C027 HD 108.8 . . S004 C028 H028 123.9 . . C01V C028 S004 112.3(2) . . C01V C028 H028 123.9 . . C01R C029 H029 119.2 . . C01R C029 C02C 121.6(3) . . C02C C029 H029 119.2 . . C01U C02A H02 115.6 . . C01U C02A C02E 128.9(3) . . C02E C02A H02 115.6 . . C02D C02B H02I 116.4 . . C02I C02B H02I 116.4 . . C02I C02B C02D 127.2(3) . . C01K C02C C029 119.0(3) . . C01K C02C H5 120.5 . . C029 C02C H5 120.5 . . C01Q C02D H02J 108.7 . . C01Q C02D H02K 108.7 . . C02B C02D C01Q 114.3(3) . . C02B C02D H02J 108.7 . . C02B C02D H02K 108.7 . . H02J C02D H02K 107.6 . . C027 C02E H6 108.0 . . C027 C02E HE 108.0 . . C02A C02E C027 117.2(3) . . C02A C02E H6 108.0 . . C02A C02E HE 108.0 . . H6 C02E HE 107.2 . . C025 C02F H02L 108.7 . . C025 C02F H02M 108.7 . . C025 C02F C02G 114.2(3) . . H02L C02F H02M 107.6 . . C02G C02F H02L 108.7 . . C02G C02F H02M 108.7 . . C02F C02G H02N 108.8 . . C02F C02G H02O 108.8 . . H02N C02G H02O 107.7 . . C02H C02G C02F 113.9(3) . . C02H C02G H02N 108.8 . . C02H C02G H02O 108.8 . . C02G C02H H02P 108.3 . . C02G C02H H02Q 108.3 . . H02P C02H H02Q 107.4 . . C02I C02H C02G 116.1(3) . . C02I C02H H02P 108.3 . . C02I C02H H02Q 108.3 . . C02B C02I C02H 130.7(3) . . C02B C02I H02R 114.6 . . C02H C02I H02R 114.6 . . O007 C02J H7 109.5 . . O007 C02J HF 109.5 . . O007 C02J HG 109.5 . . H7 C02J HF 109.5 . . H7 C02J HG 109.5 . . HF C02J HG 109.5 . . O006 C02K H02S 109.5 . . O006 C02K H02T 109.5 . . O006 C02K H02U 109.5 . . H02S C02K H02T 109.5 . . H02S C02K H02U 109.5 . . H02T C02K H02U 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 S001 C00J 1.722(2) . S001 C01O 1.703(3) . S002 C00Q 1.722(3) . S002 C022 1.699(3) . S003 C00Z 1.728(2) . S003 C01S 1.704(3) . S004 C00S 1.729(2) . S004 C028 1.703(4) . O005 C013 1.365(3) . O005 C01E 1.430(3) . O006 C00V 1.359(3) . O006 C02K 1.430(3) . O007 C017 1.363(3) . O007 C02J 1.426(3) . O008 C01K 1.376(3) . O008 C01T 1.421(3) . O009 C00Y 1.377(3) . O009 C023 1.446(3) . O00A C01M 1.371(3) . O00A C025 1.436(4) . N00B N00C 1.245(3) . N00B C00M 1.430(3) . N00C C00L 1.430(3) . N00D N00E 1.240(3) . N00D C016 1.433(3) . N00E C018 1.435(3) . C00F C00J 1.365(3) . C00F C00O 1.476(3) . C00F C01G 1.426(3) . C00G C00T 1.413(3) . C00G C010 1.488(3) . C00G C012 1.393(4) . C00H C00R 1.480(4) . C00H C017 1.409(3) . C00H C01K 1.395(4) . C00I C00K 1.488(3) . C00I C00N 1.393(3) . C00I C00W 1.416(3) . C00J C00S 1.462(3) . C00K C00Z 1.368(3) . C00K C01D 1.431(3) . C00L C00P 1.390(3) . C00L C00X 1.384(4) . C00M C00U 1.378(4) . C00M C011 1.382(3) . C00N C00P 1.391(3) . C00N C01L 1.508(3) . C00O C00V 1.412(3) . C00O C013 1.390(3) . C00P H00P 0.9300 . C00Q C00R 1.370(4) . C00Q C00Z 1.458(3) . C00R C01N 1.423(3) . C00S C010 1.372(4) . C00T C015 1.390(3) . C00T C021 1.496(4) . C00U H00U 0.9300 . C00U C014 1.379(3) . C00V C01W 1.386(4) . C00W C00X 1.385(3) . C00W C01X 1.498(4) . C00X H00X 0.9300 . C00Y C014 1.391(4) . C00Y C01C 1.367(4) . C010 C01V 1.436(3) . C011 H011 0.9300 . C011 C01C 1.382(3) . C012 C01I 1.388(3) . C012 C026 1.510(4) . C013 C01Y 1.390(4) . C014 H014 0.9300 . C015 H015 0.9300 . C015 C018 1.375(4) . C016 C019 1.386(4) . C016 C01F 1.380(4) . C017 C01R 1.382(4) . C018 C01I 1.396(4) . C019 H019 0.9300 . C019 C01J 1.381(4) . C01A H01A 0.9700 . C01A H01B 0.9700 . C01A C01E 1.506(4) . C01A C01Q 1.518(4) . C01B H01C 0.9300 . C01B C01F 1.385(4) . C01B C01M 1.385(4) . C01C H01L 0.9300 . C01D H01M 0.9300 . C01D C01S 1.340(4) . C01E H01D 0.9700 . C01E H01E 0.9700 . C01F H01F 0.9300 . C01G H01G 0.9300 . C01G C01O 1.347(4) . C01H H01N 0.9700 . C01H H01P 0.9700 . C01H C01P 1.525(4) . C01H C024 1.520(4) . C01I H01I 0.9300 . C01J H01J 0.9300 . C01J C01M 1.374(4) . C01K C02C 1.369(4) . C01L H01Q 0.9600 . C01L H01R 0.9600 . C01L H01S 0.9600 . C01N H01T 0.9300 . C01N C022 1.346(4) . C01O H01O 0.9300 . C01P H01U 0.9700 . C01P H01X 0.9700 . C01P C01T 1.504(4) . C01Q H01H 0.9700 . C01Q H01K 0.9700 . C01Q C02D 1.506(4) . C01R H01Z 0.9300 . C01R C029 1.362(5) . C01S H01 0.9300 . C01T H1 0.9700 . C01T H 0.9700 . C01U H2 0.9300 . C01U C024 1.493(4) . C01U C02A 1.304(4) . C01V H01V 0.9300 . C01V C028 1.341(4) . C01W H01W 0.9300 . C01W C020 1.367(4) . C01X H3 0.9600 . C01X HA 0.9600 . C01X HB 0.9600 . C01Y H01Y 0.9300 . C01Y C020 1.383(4) . C01Z H4 0.9700 . C01Z HC 0.9700 . C01Z C023 1.506(4) . C01Z C027 1.521(5) . C020 H020 0.9300 . C021 H02A 0.9600 . C021 H02B 0.9600 . C021 H02C 0.9600 . C022 H022 0.9300 . C023 H02V 0.9700 . C023 H02W 0.9700 . C024 H02X 0.9700 . C024 H02Y 0.9700 . C025 H02D 0.9700 . C025 H02E 0.9700 . C025 C02F 1.507(5) . C026 H02F 0.9600 . C026 H02G 0.9600 . C026 H02H 0.9600 . C027 H02Z 0.9700 . C027 HD 0.9700 . C027 C02E 1.505(5) . C028 H028 0.9300 . C029 H029 0.9300 . C029 C02C 1.400(5) . C02A H02 0.9300 . C02A C02E 1.498(4) . C02B H02I 0.9300 . C02B C02D 1.501(4) . C02B C02I 1.285(5) . C02C H5 0.9300 . C02D H02J 0.9700 . C02D H02K 0.9700 . C02E H6 0.9700 . C02E HE 0.9700 . C02F H02L 0.9700 . C02F H02M 0.9700 . C02F C02G 1.526(5) . C02G H02N 0.9700 . C02G H02O 0.9700 . C02G C02H 1.514(5) . C02H H02P 0.9700 . C02H H02Q 0.9700 . C02H C02I 1.492(5) . C02I H02R 0.9300 . C02J H7 0.9600 . C02J HF 0.9600 . C02J HG 0.9600 . C02K H02S 0.9600 . C02K H02T 0.9600 . C02K H02U 0.9600 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 S001 C00J C00S S004 -60.0(2) . . . . S001 C00J C00S C010 118.4(3) . . . . S002 C00Q C00R C00H -175.46(19) . . . . S002 C00Q C00R C01N 0.6(3) . . . . S002 C00Q C00Z S003 61.8(3) . . . . S002 C00Q C00Z C00K -116.1(3) . . . . S004 C00S C010 C00G 175.5(2) . . . . S004 C00S C010 C01V -0.6(3) . . . . O005 C013 C01Y C020 -179.7(3) . . . . O006 C00V C01W C020 -177.6(3) . . . . O007 C017 C01R C029 178.7(3) . . . . O008 C01K C02C C029 180.0(3) . . . . O009 C00Y C014 C00U -177.6(2) . . . . O009 C00Y C01C C011 177.5(2) . . . . O00A C025 C02F C02G 53.0(4) . . . . N00B N00C C00L C00P -180.0(2) . . . . N00B N00C C00L C00X -0.4(3) . . . . N00B C00M C00U C014 176.1(2) . . . . N00B C00M C011 C01C -176.3(2) . . . . N00C N00B C00M C00U -5.6(3) . . . . N00C N00B C00M C011 174.6(2) . . . . N00C C00L C00P C00N 179.4(2) . . . . N00C C00L C00X C00W 180.0(2) . . . . N00D N00E C018 C015 -6.6(4) . . . . N00D N00E C018 C01I 177.2(2) . . . . N00D C016 C019 C01J 174.5(3) . . . . N00D C016 C01F C01B -174.3(3) . . . . N00E N00D C016 C019 -172.7(2) . . . . N00E N00D C016 C01F 6.2(4) . . . . N00E C018 C01I C012 176.9(2) . . . . C00F C00J C00S S004 117.3(3) . . . . C00F C00J C00S C010 -64.3(4) . . . . C00F C00O C00V O006 2.3(3) . . . . C00F C00O C00V C01W -175.6(2) . . . . C00F C00O C013 O005 -4.8(3) . . . . C00F C00O C013 C01Y 175.7(2) . . . . C00F C01G C01O S001 -0.6(3) . . . . C00G C00T C015 C018 0.9(4) . . . . C00G C010 C01V C028 -176.1(3) . . . . C00G C012 C01I C018 -0.1(4) . . . . C00H C00R C01N C022 175.4(2) . . . . C00H C017 C01R C029 -0.7(4) . . . . C00H C01K C02C C029 0.5(4) . . . . C00I C00K C00Z S003 -175.08(19) . . . . C00I C00K C00Z C00Q 3.0(4) . . . . C00I C00K C01D C01S 175.4(3) . . . . C00I C00N C00P C00L 1.7(3) . . . . C00I C00W C00X C00L -0.4(4) . . . . C00J S001 C01O C01G 0.1(2) . . . . C00J C00F C00O C00V -64.8(3) . . . . C00J C00F C00O C013 119.4(3) . . . . C00J C00F C01G C01O 0.9(3) . . . . C00J C00S C010 C00G -3.0(4) . . . . C00J C00S C010 C01V -179.1(3) . . . . C00K C00I C00N C00P 178.6(2) . . . . C00K C00I C00N C01L -2.2(3) . . . . C00K C00I C00W C00X -179.2(2) . . . . C00K C00I C00W C01X 2.5(3) . . . . C00K C01D C01S S003 0.1(3) . . . . C00M N00B N00C C00L -179.02(19) . . . . C00M C00U C014 C00Y 0.3(4) . . . . C00M C011 C01C C00Y 0.2(4) . . . . C00N C00I C00K C00Z -110.1(3) . . . . C00N C00I C00K C01D 74.2(3) . . . . C00N C00I C00W C00X 2.0(3) . . . . C00N C00I C00W C01X -176.3(2) . . . . C00O C00F C00J S001 173.87(18) . . . . C00O C00F C00J C00S -3.6(4) . . . . C00O C00F C01G C01O -174.0(2) . . . . C00O C00V C01W C020 0.2(4) . . . . C00O C013 C01Y C020 -0.4(4) . . . . C00P C00L C00X C00W -0.5(4) . . . . C00Q S002 C022 C01N -0.2(2) . . . . C00Q C00R C01N C022 -0.8(3) . . . . C00R C00H C017 O007 -3.1(3) . . . . C00R C00H C017 C01R 176.3(2) . . . . C00R C00H C01K O008 4.3(3) . . . . C00R C00H C01K C02C -176.2(3) . . . . C00R C00Q C00Z S003 -117.0(3) . . . . C00R C00Q C00Z C00K 65.0(4) . . . . C00R C01N C022 S002 0.6(3) . . . . C00S S004 C028 C01V -0.6(3) . . . . C00S C010 C01V C028 0.1(4) . . . . C00T C00G C010 C00S -67.3(3) . . . . C00T C00G C010 C01V 108.3(3) . . . . C00T C00G C012 C01I 0.2(3) . . . . C00T C00G C012 C026 178.8(2) . . . . C00T C015 C018 N00E -176.9(2) . . . . C00T C015 C018 C01I -0.8(4) . . . . C00U C00M C011 C01C 3.9(4) . . . . C00V C00O C013 O005 179.3(2) . . . . C00V C00O C013 C01Y -0.2(4) . . . . C00V C01W C020 C01Y -0.7(4) . . . . C00W C00I C00K C00Z 71.0(3) . . . . C00W C00I C00K C01D -104.6(3) . . . . C00W C00I C00N C00P -2.6(3) . . . . C00W C00I C00N C01L 176.6(2) . . . . C00X C00L C00P C00N -0.2(4) . . . . C00Y O009 C023 C01Z -58.4(3) . . . . C00Z S003 C01S C01D 0.5(3) . . . . C00Z C00K C01D C01S -0.8(4) . . . . C00Z C00Q C00R C00H 3.5(4) . . . . C00Z C00Q C00R C01N 179.5(2) . . . . C010 C00G C00T C015 -179.0(2) . . . . C010 C00G C00T C021 -0.2(3) . . . . C010 C00G C012 C01I 178.6(2) . . . . C010 C00G C012 C026 -2.8(3) . . . . C010 C01V C028 S004 0.4(4) . . . . C011 C00M C00U C014 -4.1(4) . . . . C012 C00G C00T C015 -0.6(3) . . . . C012 C00G C00T C021 178.2(2) . . . . C012 C00G C010 C00S 114.3(3) . . . . C012 C00G C010 C01V -70.1(3) . . . . C013 O005 C01E C01A -177.9(2) . . . . C013 C00O C00V O006 178.2(2) . . . . C013 C00O C00V C01W 0.3(4) . . . . C013 C01Y C020 C01W 0.8(5) . . . . C014 C00Y C01C C011 -4.0(4) . . . . C015 C018 C01I C012 0.4(4) . . . . C016 N00D N00E C018 177.3(2) . . . . C016 C019 C01J C01M 0.3(4) . . . . C017 C00H C00R C00Q 59.2(4) . . . . C017 C00H C00R C01N -116.4(3) . . . . C017 C00H C01K O008 -179.9(2) . . . . C017 C00H C01K C02C -0.4(4) . . . . C017 C01R C029 C02C 0.8(5) . . . . C019 C016 C01F C01B 4.6(4) . . . . C019 C01J C01M O00A -177.3(3) . . . . C019 C01J C01M C01B 3.7(4) . . . . C01A C01Q C02D C02B -177.5(3) . . . . C01C C00Y C014 C00U 3.8(4) . . . . C01D C00K C00Z S003 1.1(3) . . . . C01D C00K C00Z C00Q 179.2(3) . . . . C01E O005 C013 C00O -175.9(2) . . . . C01E O005 C013 C01Y 3.6(4) . . . . C01E C01A C01Q C02D -171.7(3) . . . . C01F C016 C019 C01J -4.5(4) . . . . C01F C01B C01M O00A 177.3(3) . . . . C01F C01B C01M C01J -3.6(4) . . . . C01G C00F C00J S001 -0.9(3) . . . . C01G C00F C00J C00S -178.4(2) . . . . C01G C00F C00O C00V 109.4(3) . . . . C01G C00F C00O C013 -66.4(3) . . . . C01H C01P C01T O008 175.8(2) . . . . C01K O008 C01T C01P -177.1(2) . . . . C01K C00H C00R C00Q -125.1(3) . . . . C01K C00H C00R C01N 59.3(3) . . . . C01K C00H C017 O007 -179.0(2) . . . . C01K C00H C017 C01R 0.5(4) . . . . C01L C00N C00P C00L -177.5(2) . . . . C01M O00A C025 C02F 59.1(4) . . . . C01M C01B C01F C016 -0.6(4) . . . . C01O S001 C00J C00F 0.47(19) . . . . C01O S001 C00J C00S 178.3(2) . . . . C01P C01H C024 C01U 178.0(3) . . . . C01Q C01A C01E O005 -179.7(2) . . . . C01R C029 C02C C01K -0.8(5) . . . . C01S S003 C00Z C00K -0.9(2) . . . . C01S S003 C00Z C00Q -179.2(2) . . . . C01T O008 C01K C00H 171.2(2) . . . . C01T O008 C01K C02C -8.3(4) . . . . C01U C02A C02E C027 -16.1(6) . . . . C01X C00W C00X C00L 178.0(2) . . . . C01Z C027 C02E C02A -69.9(4) . . . . C021 C00T C015 C018 -177.9(2) . . . . C022 S002 C00Q C00R -0.2(2) . . . . C022 S002 C00Q C00Z -179.3(2) . . . . C023 O009 C00Y C014 151.9(3) . . . . C023 O009 C00Y C01C -29.5(4) . . . . C023 C01Z C027 C02E 175.0(2) . . . . C024 C01H C01P C01T 173.1(3) . . . . C024 C01U C02A C02E -179.7(3) . . . . C025 O00A C01M C01B -155.7(3) . . . . C025 O00A C01M C01J 25.2(4) . . . . C025 C02F C02G C02H -174.0(3) . . . . C026 C012 C01I C018 -178.8(2) . . . . C027 C01Z C023 O009 -51.0(3) . . . . C028 S004 C00S C00J 179.4(2) . . . . C028 S004 C00S C010 0.7(2) . . . . C02A C01U C024 C01H 118.4(3) . . . . C02D C02B C02I C02H 179.2(4) . . . . C02F C02G C02H C02I 70.8(5) . . . . C02G C02H C02I C02B 14.2(7) . . . . C02I C02B C02D C01Q -122.3(4) . . . . C02J O007 C017 C00H -173.2(3) . . . . C02J O007 C017 C01R 7.5(4) . . . . C02K O006 C00V C00O 167.0(3) . . . . C02K O006 C00V C01W -15.1(4) . . . .