#------------------------------------------------------------------------------ #$Date: 2017-06-05 15:54:18 +0100 (Mon, 05 Jun 2017) $ #$Revision: 197526 $ #$URL: svn://www.crystallography.net/cod/cif/3/50/00/3500070.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500070 loop_ _publ_author_name 'Thierry Maris' _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. ; _journal_name_full 'Personal communication to COD' _journal_year 2017 _chemical_formula_moiety 'C5 H4 Br N O' _chemical_formula_sum 'C5 H4 Br N O' _chemical_formula_weight 174.00 _chemical_name_systematic '5-Bromo-2(1H)-pyridone ' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2016-12-20 _audit_creation_method ; Olex2 1.2 (compiled 2016.11.30 svn.r3356 for OlexSys, GUI svn.r5269) ; _cell_angle_alpha 90 _cell_angle_beta 121.1850(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.1602(7) _cell_length_b 9.0351(5) _cell_length_c 11.5554(9) _cell_measurement_reflns_used 8333 _cell_measurement_temperature 100 _cell_measurement_theta_max 60.669 _cell_measurement_theta_min 3.892 _cell_volume 1175.44(13) _computing_cell_refinement ; SAINT (2013) V8.37A; Integration Software for Single Crystal Data. Bruker AXS Inc., Madison, WI 53719-1173. ; _computing_data_collection ; APEX 2 (2013) Bruker AXS Inc., Madison, WI 53719-1173. ; _computing_data_reduction ; SAINT (2013) V8.37A; Integration Software for Single Crystal Data. Bruker AXS Inc., Madison, WI 53719-1173. ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 100 _diffrn_detector 'CMOS Area detector' _diffrn_detector_area_resol_mean 10.24 _diffrn_detector_type 'Bruker Photon 100 CMOS Detector' _diffrn_measured_fraction_theta_full 0.964 _diffrn_measured_fraction_theta_max 0.970 _diffrn_measurement_device 'k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker Venture Metaljet' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_collimation 'Focusing mirrors' _diffrn_radiation_monochromator 'Helios MX Mirror Optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0342 _diffrn_reflns_av_unetI/netI 0.0242 _diffrn_reflns_Laue_measured_fraction_full 0.964 _diffrn_reflns_Laue_measured_fraction_max 0.970 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 8496 _diffrn_reflns_point_group_measured_fraction_full 0.964 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 60.638 _diffrn_reflns_theta_min 5.586 _diffrn_source 'Metal Jet' _diffrn_source_target Ga _diffrn_source_type 'Gallium Liquid Metal Jet Source' _exptl_absorpt_coefficient_mu 5.741 _exptl_absorpt_correction_T_max 0.2626 _exptl_absorpt_correction_T_min 0.1566 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1008 before and 0.0555 after correction. The Ratio of minimum to maximum transmission is 0.5963. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.966 _exptl_crystal_description chunk _exptl_crystal_F_000 672 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.11 _exptl_special_details ; X-ray crystallographic data for I were collected from a single crystal sample, which was mounted on a loop fiber. Data were collected using a Bruker Venture diffractometer equipped with a Photon 100 CMOS Detector, a Helios MX optics and a Kappa goniometer. The crystal-to-detector distance was 4.0 cm, and the data collection was carried out in 1024 x 1024 pixel mode. ; _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _refine_diff_density_max 1.039 _refine_diff_density_min -0.621 _refine_diff_density_rms 0.119 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.165 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 77 _refine_ls_number_reflns 1313 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.165 _refine_ls_R_factor_all 0.0375 _refine_ls_R_factor_gt 0.0373 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0262P)^2^+9.9569P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1057 _refine_ls_wR_factor_ref 0.1058 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1301 _reflns_number_total 1313 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file T0595.cif _cod_data_source_block t0595 _cod_depositor_comments ; The following automatic conversions were performed: '_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according to the built-in table from CIF Core dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29. Automatic conversion script Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas ; _cod_database_code 3500070 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.571 _shelx_estimated_absorpt_t_min 0.522 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C5(H5) ; _shelx_res_file ; t0595.res created by SHELXL-2014/7 TITL t0595_a.res in C2/c REM Old TITL T0595 in C2/c #15 REM SHELXT solution in C2/c REM R1 0.124, Rweak 0.004, Alpha 0.046, Orientation as input REM Formula found by SHELXT: C5 N O Br CELL 1.34139 13.1602 9.0351 11.5554 90 121.185 90 ZERR 8 0.0007 0.0005 0.0009 0 0.001 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Br N O DISP Br -0.934 1.001 7839.9 DISP C 0.014 0.007 57.748 DISP H -0 0 0.648 DISP N 0.025 0.014 110.512 DISP O 0.039 0.025 193.954 UNIT 40 32 8 8 8 EQIV $1 +X,1-Y,0.5+Z EQIV $2 -X,1-Y,-Z EQIV $3 0.5+X,0.5-Y,0.5+Z EQIV $4 0.5-X,0.5-Y,-Z L.S. 25 PLAN 8 SIZE 0.11 0.12 0.13 TEMP -173 HTAB C2 O1_$1 HTAB C3 O1_$2 HTAB C5 O1_$3 HTAB N1 O1_$4 BOND $H LIST 4 MORE -1 CONF HTAB fmap 2 53 acta OMIT -1 5 5 OMIT -12 4 5 OMIT -11 5 10 OMIT 10 4 1 OMIT 10 2 4 OMIT -1 5 3 OMIT -12 2 10 OMIT -11 3 4 OMIT -12 2 6 REM REM REM WGHT 0.026200 9.956900 FVAR 0.50606 BR1 3 0.398633 0.391436 0.565669 11.00000 0.04113 0.04161 = 0.02177 -0.00283 0.01405 0.00078 O1 5 0.116276 0.335443 -0.033352 11.00000 0.02884 0.03518 = 0.02205 0.00052 0.01398 0.00213 N1 4 0.286076 0.299761 0.169718 11.00000 0.02621 0.02854 = 0.02262 0.00015 0.01442 0.00226 C2 1 0.187946 0.425606 0.304106 11.00000 0.03290 0.02766 = 0.02677 0.00032 0.01816 0.00206 AFIX 43 H2 2 0.154271 0.468600 0.351719 11.00000 -1.20000 AFIX 0 C4 1 0.171135 0.348842 0.092802 11.00000 0.02609 0.02628 = 0.02348 0.00049 0.01398 -0.00016 C3 1 0.122066 0.413753 0.166432 11.00000 0.03462 0.02963 = 0.02677 0.00251 0.02009 0.00259 AFIX 43 H3 2 0.042583 0.449041 0.118805 11.00000 -1.20000 AFIX 0 C1 1 0.306295 0.373746 0.375478 11.00000 0.03226 0.02698 = 0.02122 -0.00018 0.01294 -0.00084 C5 1 0.354065 0.311133 0.307569 11.00000 0.02663 0.03089 = 0.02387 0.00124 0.01125 0.00105 AFIX 43 H5 2 0.433516 0.275730 0.355025 11.00000 -1.20000 AFIX 0 H1 2 0.317930 0.266564 0.130100 11.00000 0.02848 HKLF 4 REM t0595_a.res in C2/c REM R1 = 0.0373 for 1301 Fo > 4sig(Fo) and 0.0375 for all 1313 data REM 77 parameters refined using 0 restraints END WGHT 0.0262 9.9552 REM Instructions for potential hydrogen bonds HTAB C2 O1_$1 HTAB C3 O1_$2 HTAB C5 O1_$3 HTAB N1 O1_$4 REM Highest difference peak 1.039, deepest hole -0.621, 1-sigma level 0.119 Q1 1 0.4802 0.3994 0.5666 11.00000 0.05 1.04 Q2 1 0.2990 0.4002 0.5674 11.00000 0.05 0.97 Q3 1 0.5745 0.3983 0.5681 11.00000 0.05 0.82 Q4 1 0.2175 0.3986 0.5745 11.00000 0.05 0.68 Q5 1 0.4379 0.3282 0.5647 11.00000 0.05 0.65 Q6 1 0.1632 0.1122 0.0628 11.00000 0.05 0.56 Q7 1 0.5264 0.3266 0.5556 11.00000 0.05 0.48 Q8 1 0.2559 0.1187 0.0679 11.00000 0.05 0.46 ; _shelx_res_checksum 12070 _shelx_hkl_file ; 2 0 -2 95.09 4.80 -8 0 8 1102.59 53.19 -8 0 8 1067.39 53.39 -8 0 8 1085.79 53.09 8 0 -8 1114.49 53.19 -10 0 10 873.01 43.10 -10 0 10 884.51 42.80 10 0 -10 854.71 42.80 -10 0 10 892.61 42.70 -12 0 12 484.95 23.50 -12 0 12 463.15 23.80 12 0 -12 485.25 23.50 1 1 -1 1355.36 62.79 -1 1 1 1099.99 62.29 -1 -1 1 1048.20 61.99 1 -1 -1 1354.46 63.19 -3 1 3 674.13 31.10 3 1 -3 624.64 30.80 3 -1 -3 606.34 31.10 -5 1 5 886.61 43.30 5 1 -5 919.31 43.30 -5 1 5 861.31 43.30 -5 1 5 936.21 43.40 5 -1 -5 904.91 43.30 -5 -1 5 918.91 43.30 -5 -1 5 810.52 43.30 -7 1 7 1440.26 69.49 -7 1 7 1431.26 69.39 7 1 -7 1497.65 69.49 -7 -1 7 1414.36 69.39 7 -1 -7 1435.56 69.49 -7 -1 7 1360.46 69.59 -7 -1 7 1430.06 69.39 -9 1 9 32.80 2.10 -9 1 9 31.30 2.30 9 1 -9 35.70 2.10 -9 1 9 35.20 2.00 -9 -1 9 34.70 2.00 -9 -1 9 32.50 2.10 -9 -1 9 31.10 2.30 9 -1 -9 34.20 2.10 -11 1 11 264.07 13.10 11 1 -11 251.07 12.90 -11 1 11 263.27 13.00 -11 1 11 256.67 13.20 11 1 -11 263.77 12.90 -11 1 11 260.47 12.90 -11 -1 11 251.27 12.80 11 -1 -11 268.37 12.90 -11 -1 11 246.08 13.20 -13 1 13 160.28 8.30 -13 1 13 159.08 8.00 13 1 -13 151.98 8.00 13 -1 -13 162.08 8.10 -13 -1 13 165.58 8.00 -13 -1 13 150.78 8.20 0 2 0 76.49 3.80 2 2 -2 192.68 9.40 -2 2 2 201.48 9.80 -2 2 2 186.88 9.50 2 -2 -2 188.48 9.70 -2 -2 2 188.38 9.40 -2 -2 2 184.78 9.40 -4 2 4 23.80 1.70 4 2 -4 19.00 1.30 -4 2 4 20.60 1.40 6 2 -6 186.68 9.20 6 2 -6 183.48 9.20 -6 2 6 191.28 9.80 -6 2 6 192.48 9.20 -6 2 6 189.88 9.30 6 -2 -6 186.28 9.20 -6 -2 6 182.68 9.20 -6 -2 6 173.18 9.30 -6 -2 6 164.08 9.20 -6 -2 6 192.38 9.20 8 2 -8 35.00 2.00 8 2 -8 32.40 2.10 -8 2 8 34.30 1.90 -8 2 8 32.60 2.00 -8 2 8 33.70 2.30 -8 -2 8 27.40 2.30 8 -2 -8 33.00 2.00 -8 -2 8 31.50 2.00 -8 -2 8 33.80 1.90 -8 -2 8 29.20 2.10 -10 2 10 9.60 1.00 -10 2 10 8.00 1.30 10 2 -10 6.20 1.00 -10 2 10 11.70 1.10 -10 -2 10 8.70 1.40 -10 -2 10 9.40 0.90 -12 2 12 52.39 3.00 -12 2 12 44.50 2.80 12 2 -12 52.99 2.90 12 -2 -12 58.19 3.00 -12 -2 12 48.30 2.80 3 3 -3 1455.25 74.49 -3 3 3 1545.75 74.49 -3 3 3 1604.74 74.99 5 3 -5 2062.59 102.29 -5 3 5 2271.97 102.39 -5 3 5 2271.87 102.99 -5 3 5 2206.98 102.29 5 3 -5 2072.79 102.29 -5 -3 5 2024.00 102.29 -5 -3 5 1859.21 102.29 -7 3 7 1786.82 83.49 7 3 -7 1743.33 83.49 -7 3 7 1707.23 83.49 7 3 -7 1769.22 83.49 7 3 -7 1748.82 83.39 -7 3 7 1689.53 84.29 7 -3 -7 1817.12 83.49 -7 -3 7 1551.04 83.49 -7 -3 7 1657.93 83.39 9 3 -9 17.50 1.40 9 3 -9 20.60 1.60 -9 3 9 22.10 1.50 -9 3 9 15.20 1.80 9 -3 -9 21.80 1.40 -9 -3 9 15.40 1.80 -9 -3 9 15.60 1.60 -9 -3 9 22.10 1.40 -11 3 11 362.76 18.50 -11 3 11 379.26 18.40 11 3 -11 373.16 18.30 -11 3 11 362.96 18.60 11 -3 -11 371.76 18.30 -11 -3 11 367.46 18.20 -13 3 13 119.99 6.60 -13 3 13 122.49 6.60 -13 3 13 130.89 6.80 -13 -3 13 135.39 6.40 -2 4 2 541.05 27.20 2 4 -2 573.24 27.10 -2 4 2 593.54 27.80 2 4 -2 548.45 27.10 -2 4 2 585.74 27.10 -2 -4 2 491.25 27.10 -4 4 4 1495.65 74.59 4 4 -4 1509.25 74.49 4 4 -4 1571.44 74.59 -4 4 4 1683.73 75.39 -4 -4 4 1412.56 74.49 -4 -4 4 1544.35 74.59 -6 4 6 2308.17 107.79 6 4 -6 2323.07 106.19 6 4 -6 2219.68 106.09 -6 4 6 2245.78 106.19 6 4 -6 2197.68 106.19 -6 -4 6 2126.39 106.19 -6 -4 6 1900.91 106.29 -8 4 8 833.42 40.10 -8 4 8 749.13 40.90 8 4 -8 807.32 39.90 8 4 -8 775.52 40.00 -8 4 8 801.22 40.30 -8 4 8 895.01 40.40 8 4 -8 841.62 40.00 -8 -4 8 841.82 40.00 8 -4 -8 843.42 40.10 -8 -4 8 806.12 40.00 -10 4 10 403.16 19.70 -10 4 10 391.56 19.40 -10 4 10 387.76 19.50 10 4 -10 383.96 19.30 -10 -4 10 393.36 19.30 10 -4 -10 391.36 19.30 -10 -4 10 367.46 19.30 -10 -4 10 402.56 19.20 -12 4 12 568.34 27.30 -12 4 12 552.94 27.00 -12 4 12 567.84 27.10 12 4 -12 522.85 27.00 12 4 -12 538.45 27.20 12 -4 -12 549.54 27.00 -12 -4 12 551.04 26.90 -1 5 1 14.40 1.00 3 5 -3 291.77 13.70 -3 5 3 290.37 13.70 3 5 -3 282.47 13.60 -3 5 3 285.97 14.50 -3 5 3 265.97 13.60 -3 5 3 259.47 13.70 -3 -5 3 270.57 13.70 -3 -5 3 261.77 13.60 -5 5 5 36.70 3.20 -5 5 5 39.20 2.40 5 5 -5 41.10 2.20 5 5 -5 36.70 2.20 -5 5 5 38.40 2.20 5 5 -5 38.40 2.20 -5 -5 5 34.00 2.20 -5 -5 5 34.70 2.10 7 5 -7 126.39 6.40 7 5 -7 126.49 6.50 -7 5 7 127.29 6.70 -7 5 7 118.79 7.70 -7 5 7 122.99 6.50 -7 5 7 135.59 6.80 7 5 -7 123.09 6.50 -7 -5 7 130.29 6.50 -7 -5 7 122.89 6.40 -9 5 9 47.20 3.00 9 5 -9 46.50 2.70 9 5 -9 39.60 2.70 -9 -5 9 46.60 2.60 -9 -5 9 44.60 2.80 9 -5 -9 47.60 2.70 -11 5 11 11.60 1.20 11 5 -11 12.20 1.40 -11 5 11 14.00 1.60 -11 5 11 13.90 1.50 11 -5 -11 11.90 1.30 -11 -5 11 11.80 1.10 0 6 0 741.53 35.00 0 6 0 674.83 35.00 0 6 0 810.52 36.00 0 -6 0 641.14 34.90 -2 6 2 187.68 9.70 2 6 -2 211.48 11.20 2 6 -2 193.98 9.60 -2 6 2 173.08 9.60 -2 6 2 196.38 10.70 -2 6 2 202.08 9.70 2 -6 -2 185.18 9.60 -2 -6 2 194.58 9.70 4 6 -4 83.69 4.30 -4 6 4 78.69 5.30 -4 6 4 80.69 4.40 -4 6 4 77.59 4.40 4 6 -4 79.89 4.30 -4 6 4 82.79 4.30 -4 -6 4 83.59 4.40 -4 -6 4 82.09 4.20 6 6 -6 512.25 24.40 6 6 -6 515.85 24.40 -6 6 6 464.65 25.70 6 6 -6 494.35 24.40 -6 6 6 514.95 24.60 -6 6 6 479.25 24.60 -6 6 6 497.65 24.40 -6 -6 6 500.05 24.40 -6 -6 6 496.45 24.50 8 6 -8 34.10 2.30 -8 6 8 34.70 2.50 -8 6 8 38.30 2.50 8 6 -8 37.00 2.30 -8 6 8 35.80 2.30 8 6 -8 32.90 2.30 8 -6 -8 37.70 2.30 -8 -6 8 35.50 2.20 -8 -6 8 38.30 2.30 -10 6 10 30.10 2.10 -10 6 10 31.20 2.30 -10 6 10 32.40 2.00 10 6 -10 29.70 2.00 -10 -6 10 29.50 2.10 -10 -6 10 27.30 2.00 10 -6 -10 27.30 1.90 -10 -6 10 27.90 1.80 -1 7 1 3034.80 153.08 -1 7 1 3266.87 151.98 1 7 -1 3227.08 151.88 1 7 -1 3136.39 152.98 -1 7 1 3003.00 151.88 -1 -7 1 3189.78 151.88 1 -7 -1 3072.99 151.78 -3 7 3 287.27 15.40 -3 7 3 299.27 14.10 3 7 -3 269.77 15.20 -3 7 3 264.97 14.10 -3 7 3 277.67 14.00 3 7 -3 294.87 14.10 -3 -7 3 288.97 14.10 -3 -7 3 276.77 14.00 -5 7 5 950.80 45.40 5 7 -5 876.71 45.80 5 7 -5 961.60 45.40 -5 7 5 912.61 45.50 5 7 -5 974.00 45.40 -5 -7 5 900.71 45.30 -5 -7 5 937.51 45.50 -7 7 7 842.72 44.30 7 7 -7 898.41 43.80 7 7 -7 935.21 43.90 7 7 -7 919.11 44.00 -7 7 7 881.21 43.90 -7 -7 7 889.31 44.00 -7 -7 7 915.11 43.70 9 7 -9 13.60 1.40 -9 7 9 17.50 1.50 -9 -7 9 14.10 1.40 -9 -7 9 11.00 1.20 -9 -7 9 12.10 1.30 9 -7 -9 15.70 1.40 -11 7 11 385.96 17.50 -11 7 11 355.86 17.40 -11 -7 11 321.97 17.40 0 8 0 288.47 13.60 0 8 0 269.97 13.80 0 -8 0 266.17 13.60 -2 8 2 237.38 11.60 2 8 -2 242.18 11.60 -2 8 2 224.28 11.50 2 -8 -2 223.98 11.40 -2 -8 2 223.58 11.50 -2 -8 2 229.38 11.60 -4 8 4 23.70 1.70 4 8 -4 23.10 1.70 4 8 -4 23.60 1.70 -4 8 4 18.30 1.70 -4 -8 4 20.40 1.60 6 8 -6 295.37 14.30 -6 8 6 290.47 14.40 -6 8 6 280.87 14.20 6 8 -6 268.07 14.30 -6 -8 6 286.97 14.30 -6 -8 6 294.57 14.20 8 8 -8 250.67 12.00 -8 8 8 232.48 12.00 -8 8 8 242.18 12.10 8 -8 -8 240.08 12.10 -8 -8 8 233.48 12.10 -8 -8 8 248.48 12.10 10 8 -10 7.30 1.20 -10 8 10 8.00 1.00 -10 8 10 6.20 1.00 -10 -8 10 6.90 1.00 -1 9 1 43.70 2.40 1 9 -1 35.60 2.30 -1 -9 1 32.40 2.20 -1 -9 1 33.30 2.30 -3 9 3 1.90 0.90 3 9 -3 1.30 0.80 3 9 -3 1.70 0.80 -3 -9 3 1.60 0.70 -5 9 5 18.20 1.60 5 9 -5 18.50 1.80 5 9 -5 19.90 1.50 -5 -9 5 19.10 1.50 -7 9 7 4.20 0.80 7 9 -7 2.60 0.80 -7 -9 7 3.10 0.80 -7 -9 7 3.50 0.70 0 10 0 522.75 25.70 0 -10 0 523.05 25.60 2 10 -2 49.50 2.90 2 10 -2 46.90 2.80 -2 -10 2 43.00 2.80 -2 -10 2 49.80 2.70 4 10 -4 65.59 3.70 4 10 -4 63.59 3.50 -4 10 4 59.29 3.50 -4 -10 4 68.39 3.50 -4 -10 4 60.49 3.50 6 10 -6 231.68 11.10 -6 10 6 222.08 11.30 -6 -10 6 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648.04 33.10 -12 4 4 679.63 32.80 12 4 -4 644.24 32.80 12 4 -4 704.93 32.90 10 4 -2 304.87 15.10 -10 4 2 298.07 15.10 10 4 -2 322.97 15.10 10 4 -2 323.97 15.10 10 4 -2 285.47 15.40 10 4 -2 311.57 15.10 10 -4 -2 281.37 15.40 8 4 0 193.08 10.40 8 4 0 206.58 10.20 8 4 0 205.38 10.20 8 4 0 205.28 10.30 -8 4 0 193.38 10.20 8 4 0 200.68 10.20 8 -4 0 208.08 10.20 8 -4 0 206.08 10.20 8 -4 0 201.68 10.20 8 -4 0 206.08 10.50 -6 4 -2 2672.33 132.69 6 4 2 2980.20 132.79 6 4 2 2770.42 132.59 6 4 2 2558.14 132.79 6 4 2 2680.63 132.59 6 4 2 2795.52 132.89 6 4 2 2761.22 132.69 6 -4 2 2710.13 132.79 6 -4 2 2704.83 132.69 6 -4 2 2725.33 132.59 6 -4 2 2726.43 132.89 4 4 4 1188.48 57.29 4 4 4 1106.29 56.59 4 4 4 1181.18 56.69 4 4 4 1178.38 56.69 4 4 4 1132.99 56.69 4 4 4 1157.98 56.59 4 -4 4 1222.98 56.69 4 -4 4 1176.08 56.69 4 -4 4 1131.29 56.89 4 -4 4 1142.59 56.69 4 -4 4 1173.18 56.59 2 4 6 953.90 46.20 2 4 6 849.91 46.10 2 4 6 937.91 46.20 2 4 6 976.90 46.50 2 -4 6 953.50 46.40 2 -4 6 1010.20 46.30 2 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6.20 10 6 -2 218.38 10.70 10 6 -2 207.28 10.70 10 6 -2 203.48 11.00 10 6 -2 193.08 10.70 -10 6 2 222.08 10.70 10 -6 -2 227.18 11.00 8 6 0 11.30 1.20 8 6 0 9.80 1.70 8 6 0 12.20 1.30 8 6 0 12.70 1.20 -8 6 0 11.00 1.20 8 -6 0 10.30 1.90 8 -6 0 10.50 1.10 -6 6 -2 248.28 12.40 6 6 2 253.27 12.40 6 6 2 244.08 12.30 6 6 2 250.37 12.30 6 6 2 250.17 12.50 6 -6 2 252.17 12.30 6 -6 2 246.28 12.50 6 -6 2 238.58 12.30 6 -6 2 234.48 12.40 4 6 4 419.16 21.10 4 6 4 426.56 21.10 4 6 4 421.36 21.00 4 -6 4 441.36 21.00 4 -6 4 405.46 21.10 4 -6 4 446.56 21.10 4 -6 4 429.86 21.10 2 6 6 31.40 2.10 2 6 6 31.60 2.30 2 -6 6 35.50 2.30 2 -6 6 36.50 2.20 2 -6 6 35.50 2.10 2 -6 6 34.00 2.20 2 -6 6 31.90 2.40 2 -6 6 32.40 2.20 0 6 8 581.44 27.90 0 -6 8 596.94 27.90 0 -6 8 567.84 27.90 0 -6 8 522.45 27.90 0 -6 8 561.74 27.80 0 -6 8 573.44 27.90 0 -6 8 576.24 28.10 -2 6 10 147.89 7.10 -2 6 10 129.79 7.40 -2 -6 10 148.49 7.10 -2 -6 10 137.89 7.20 -2 -6 10 140.59 7.00 2 -6 -10 124.99 7.10 -4 6 12 29.50 1.90 -4 -6 12 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44.00 9 -1 0 935.51 44.20 7 1 2 1960.60 98.39 -7 1 -2 1873.61 98.49 7 1 2 2015.50 98.59 7 1 2 2060.89 98.69 7 1 2 2122.49 98.49 7 1 2 2069.09 98.49 7 1 2 2030.80 98.59 7 1 2 1955.20 98.79 7 -1 2 2115.29 98.69 7 -1 2 2036.60 98.49 7 -1 2 2058.59 98.89 7 -1 2 2053.19 98.69 7 -1 2 2029.50 98.59 5 1 4 18.60 1.50 5 1 4 18.60 1.50 5 1 4 16.60 1.50 5 1 4 16.70 1.60 5 1 4 16.50 1.40 5 1 4 16.70 1.30 5 -1 4 15.90 1.30 5 -1 4 17.60 1.40 5 -1 4 19.00 1.60 5 -1 4 16.20 1.60 5 -1 4 15.20 1.40 3 1 6 1161.18 56.69 3 1 6 1157.28 56.69 3 1 6 1122.39 56.49 3 1 6 1152.08 56.69 3 1 6 1107.49 56.69 3 1 6 1185.38 56.79 3 1 6 1243.68 56.99 3 -1 6 1208.38 56.89 3 -1 6 1085.69 56.49 3 -1 6 1098.49 56.49 3 -1 6 1216.48 56.79 3 -1 6 1234.68 56.69 3 -1 6 1157.58 56.69 1 1 8 1230.28 66.69 1 1 8 1439.06 66.69 1 1 8 1415.86 66.79 1 1 8 1411.86 66.99 1 1 8 1368.86 66.69 1 -1 8 1375.26 66.89 1 -1 8 1398.76 66.69 1 -1 8 1347.97 66.49 1 -1 8 1399.26 66.99 1 -1 8 1342.27 66.79 1 -1 8 1381.46 66.69 1 -1 8 1326.97 66.69 -1 1 10 100.49 5.60 -1 1 10 95.59 5.40 -1 -1 10 95.19 5.30 -1 -1 10 95.69 5.50 -1 -1 10 97.59 5.30 -1 -1 10 106.09 5.10 -1 -1 10 91.59 5.20 -3 1 12 825.52 40.90 -3 1 12 832.02 40.60 -3 -1 12 808.42 40.60 -3 -1 12 844.22 40.40 -3 -1 12 838.12 40.90 -5 1 14 319.07 15.90 -5 1 14 334.17 16.10 -5 -1 14 326.07 15.70 -5 -1 14 318.97 15.80 -5 -1 14 299.17 16.00 16 2 -7 110.79 5.40 16 2 -7 90.59 5.50 16 2 -7 111.99 5.50 16 -2 -7 96.29 5.70 16 -2 -7 113.69 5.50 14 2 -5 601.14 26.90 -14 2 5 540.15 26.80 14 2 -5 558.04 26.90 14 2 -5 534.85 27.00 14 -2 -5 502.05 27.10 12 2 -3 194.18 9.60 12 2 -3 197.58 9.40 -12 2 3 173.58 9.30 12 2 -3 178.38 9.30 12 -2 -3 180.88 9.40 12 -2 -3 182.88 9.40 -10 2 1 338.07 17.20 10 2 -1 356.46 17.50 10 2 -1 319.67 17.30 10 2 -1 360.36 17.30 10 2 -1 346.27 17.20 10 2 -1 351.96 17.30 10 2 -1 361.06 17.30 10 -2 -1 341.37 17.50 10 -2 -1 359.66 17.30 10 -2 -1 358.86 17.20 10 -2 -1 338.27 17.30 -8 2 -1 2660.43 133.39 8 2 1 2623.04 133.59 8 2 1 2820.52 133.39 8 2 1 2765.62 133.39 8 2 1 2692.03 133.39 8 2 1 2615.34 133.49 8 2 1 2879.61 133.39 8 -2 1 2738.33 133.59 8 -2 1 2856.31 133.49 8 -2 1 2775.22 133.49 8 -2 1 2825.22 133.39 6 2 3 1552.64 76.09 6 2 3 1486.55 76.19 6 2 3 1579.24 76.29 6 2 3 1688.63 76.39 6 2 3 1585.54 76.09 6 2 3 1575.94 76.09 6 2 3 1542.45 76.39 6 -2 3 1641.94 76.49 6 -2 3 1587.04 76.29 6 -2 3 1537.55 76.09 6 -2 3 1475.55 76.39 6 -2 3 1561.04 76.19 4 2 5 2256.87 116.69 4 2 5 2358.36 116.89 4 2 5 2431.06 116.79 4 2 5 2463.45 116.69 4 2 5 2460.25 116.59 4 -2 5 2281.17 116.59 4 -2 5 2480.45 116.79 4 -2 5 2357.56 116.79 4 -2 5 2379.96 116.59 4 -2 5 2485.55 116.99 4 -2 5 2494.85 116.69 2 2 7 2852.31 135.69 2 2 7 2711.63 135.49 2 2 7 2828.42 135.99 2 2 7 2708.93 135.69 2 2 7 2759.22 135.69 2 2 7 2741.73 135.59 2 2 7 2872.21 135.59 2 -2 7 3045.20 135.69 2 -2 7 2782.72 135.59 2 -2 7 2708.73 135.79 2 -2 7 2888.31 135.79 2 -2 7 2680.43 135.69 2 -2 7 2729.33 135.69 2 -2 7 2871.61 135.99 2 -2 7 2762.72 135.49 0 2 9 237.38 11.70 0 2 9 227.88 12.00 0 -2 9 231.98 11.60 0 -2 9 227.18 11.60 0 -2 9 234.28 11.70 0 -2 9 230.28 11.90 0 -2 9 243.48 11.70 0 -2 9 233.08 11.90 0 -2 9 220.18 11.70 -2 2 11 252.77 12.50 -2 2 11 236.28 12.20 -2 -2 11 250.67 12.50 -2 -2 11 239.68 12.20 -2 -2 11 232.78 12.10 -2 -2 11 241.88 12.20 -4 2 13 1130.29 56.79 -4 2 13 1219.08 57.09 -4 -2 13 1204.48 56.59 -4 -2 13 1136.19 56.69 -4 -2 13 1132.99 56.89 15 3 -6 30.60 1.90 -15 3 6 27.30 1.80 15 3 -6 29.50 1.90 15 3 -6 24.30 2.10 15 -3 -6 26.20 2.20 13 3 -4 53.89 3.10 13 3 -4 58.69 3.10 -13 3 4 52.89 3.10 13 3 -4 50.49 3.40 13 -3 -4 53.09 3.50 11 3 -2 22.60 1.70 11 3 -2 20.30 1.80 11 3 -2 21.90 1.60 11 3 -2 24.70 2.00 -11 3 2 24.20 1.70 11 -3 -2 23.20 2.10 11 -3 -2 23.10 1.90 11 -3 -2 17.70 2.00 -9 3 0 220.48 10.90 9 3 0 211.18 10.90 9 3 0 228.68 10.90 9 3 0 214.08 11.00 9 3 0 214.28 10.90 9 3 0 212.68 11.10 9 -3 0 213.88 10.90 9 -3 0 214.88 11.20 9 -3 0 223.48 10.90 7 3 2 366.06 18.30 7 3 2 371.06 18.30 7 3 2 379.16 18.50 7 3 2 374.66 18.30 7 3 2 337.37 18.60 -7 3 -2 358.66 18.40 7 3 2 393.06 18.90 7 -3 2 380.76 18.40 7 -3 2 363.56 18.30 7 -3 2 386.86 18.60 7 -3 2 374.86 18.40 5 3 4 21.70 1.60 5 3 4 17.70 1.60 5 3 4 18.50 1.70 5 3 4 19.70 1.80 5 3 4 17.60 1.50 5 3 4 19.20 1.40 5 -3 4 21.70 1.60 5 -3 4 21.20 1.40 5 -3 4 19.50 1.70 3 3 6 1.50 0.60 3 3 6 1.60 0.70 3 3 6 2.00 0.90 3 3 6 2.30 0.90 3 3 6 1.80 0.90 3 3 6 1.80 0.80 3 -3 6 0.80 0.60 3 -3 6 3.60 0.80 3 -3 6 3.30 0.90 1 3 8 977.20 43.20 1 3 8 825.72 43.10 1 -3 8 980.70 43.30 1 -3 8 970.70 43.10 1 -3 8 917.81 43.40 1 -3 8 732.83 43.30 1 -3 8 782.72 43.20 1 -3 8 837.22 43.30 1 -3 8 929.81 43.30 -1 3 10 211.98 10.70 -1 3 10 203.78 10.90 -1 -3 10 204.38 10.70 -1 -3 10 213.98 10.60 -1 -3 10 216.58 10.90 -1 -3 10 210.28 10.60 -3 3 12 327.67 16.90 -3 3 12 345.07 16.60 -3 -3 12 321.87 16.50 -3 -3 12 329.47 16.70 -3 -3 12 329.47 16.50 -3 -3 12 345.27 16.50 -5 3 14 140.09 7.60 -5 -3 14 152.98 7.30 -5 -3 14 140.49 7.40 16 4 -7 25.30 1.70 -16 4 7 23.70 1.60 16 4 -7 20.30 1.80 16 4 -7 26.00 1.60 -16 -4 7 26.10 1.70 16 -4 -7 22.00 1.90 14 4 -5 62.89 3.50 14 4 -5 61.99 3.80 -14 4 5 63.69 3.50 14 4 -5 72.59 3.70 14 -4 -5 59.69 3.90 12 4 -3 87.19 4.90 12 4 -3 85.49 4.50 -12 4 3 79.49 4.50 12 4 -3 85.69 4.50 12 -4 -3 78.69 4.90 10 4 -1 51.39 3.20 10 4 -1 55.39 3.20 10 -4 -1 62.29 3.30 8 4 1 357.66 18.00 8 4 1 338.17 17.90 8 4 1 352.26 17.80 8 4 1 356.86 17.80 8 4 1 365.86 17.80 -8 4 -1 359.66 17.90 8 -4 1 379.86 17.80 8 -4 1 363.06 17.80 8 -4 1 360.06 18.10 8 -4 1 363.76 17.80 6 4 3 61.19 3.50 6 4 3 60.19 3.50 6 4 3 64.49 3.50 6 4 3 58.59 3.80 6 4 3 60.99 3.70 6 4 3 63.19 3.60 6 -4 3 67.49 3.70 6 -4 3 62.79 3.40 6 -4 3 66.49 3.50 6 -4 3 65.49 3.60 4 4 5 105.89 5.50 4 4 5 108.09 5.60 4 4 5 93.89 5.60 4 4 5 102.09 5.70 4 -4 5 106.59 5.50 4 -4 5 105.79 5.80 4 -4 5 106.39 5.50 4 -4 5 108.69 5.70 4 -4 5 100.29 5.50 4 -4 5 112.49 5.70 2 4 7 68.49 4.20 2 4 7 66.39 4.40 2 4 7 72.99 4.00 2 4 7 72.49 3.90 2 -4 7 71.79 4.10 2 -4 7 70.29 4.20 2 -4 7 72.49 3.90 2 -4 7 72.79 3.90 2 -4 7 76.99 4.00 2 -4 7 73.39 4.20 2 -4 7 76.09 4.10 2 -4 7 71.19 4.00 0 4 9 274.57 14.30 0 4 9 257.77 13.90 0 4 9 286.37 14.00 0 -4 9 260.07 13.80 0 -4 9 286.57 14.00 0 -4 9 298.47 14.00 0 -4 9 274.77 14.20 0 -4 9 312.77 14.10 0 -4 9 265.47 14.00 0 -4 9 282.97 14.20 -2 4 11 28.40 2.30 -2 4 11 24.30 1.80 -2 4 11 25.30 2.00 -2 -4 11 25.50 1.90 -2 -4 11 24.50 1.70 -2 -4 11 23.10 2.30 -2 -4 11 26.70 1.80 -4 4 13 134.49 7.10 -4 -4 13 130.09 6.80 -4 -4 13 136.29 6.80 15 5 -6 74.79 4.00 15 5 -6 79.69 4.10 15 5 -6 76.69 4.30 -15 5 6 70.59 4.00 15 -5 -6 72.69 4.30 -15 -5 6 80.49 4.40 13 5 -4 333.77 15.20 -13 5 4 309.67 15.10 13 5 -4 289.67 15.30 13 5 -4 298.67 15.10 13 -5 -4 289.17 15.30 11 5 -2 115.69 5.50 11 5 -2 90.99 5.40 9 5 0 615.54 30.30 9 5 0 641.24 30.30 -9 5 0 646.34 30.40 9 5 0 609.64 30.60 9 5 0 634.84 30.30 9 -5 0 589.54 30.30 9 -5 0 575.04 30.30 9 -5 0 627.34 30.30 9 -5 0 626.44 31.30 7 5 2 1415.06 73.89 7 5 2 1477.15 73.69 7 5 2 1447.86 73.69 7 5 2 1568.44 73.89 -7 5 -2 1580.04 73.79 7 5 2 1499.15 73.79 7 -5 2 1626.14 73.69 7 -5 2 1518.75 73.79 7 -5 2 1507.55 73.69 7 -5 2 1521.55 73.99 5 5 4 9.40 1.00 5 5 4 7.60 1.30 5 5 4 7.20 1.10 5 5 4 10.10 1.60 5 5 4 8.60 1.80 5 -5 4 7.00 1.00 5 -5 4 8.60 1.30 5 -5 4 9.40 1.10 3 5 6 2130.09 102.59 3 5 6 2149.39 102.59 3 5 6 1895.31 102.69 3 -5 6 2115.79 102.59 3 -5 6 2166.18 102.69 3 -5 6 2087.89 102.79 3 -5 6 2065.59 102.89 3 -5 6 2099.39 102.79 3 -5 6 2072.09 102.69 3 -5 6 2222.28 102.69 3 -5 6 2233.68 102.59 1 5 8 687.73 35.10 1 5 8 760.12 35.00 1 -5 8 750.42 35.20 1 -5 8 703.33 35.10 1 -5 8 771.72 35.00 1 -5 8 629.14 35.10 1 -5 8 722.03 35.00 1 -5 8 636.34 35.20 1 -5 8 760.12 35.00 -1 5 10 2.40 1.10 -1 5 10 3.00 1.20 -1 5 10 2.10 0.80 -1 -5 10 3.80 0.80 -1 -5 10 1.90 0.70 -3 5 12 557.74 27.70 -3 5 12 551.34 27.50 -3 -5 12 605.64 27.50 -3 -5 12 531.05 27.50 -14 6 5 258.17 13.00 14 6 -5 254.07 12.90 14 6 -5 266.07 12.90 14 6 -5 233.18 13.00 -14 6 5 292.67 13.20 14 -6 -5 232.08 13.00 -14 -6 5 276.47 12.90 12 6 -3 12.30 1.30 -12 6 3 12.90 1.20 12 6 -3 17.20 1.40 12 6 -3 13.90 1.70 12 -6 -3 11.90 1.70 10 6 -1 76.39 4.00 10 6 -1 70.69 4.00 10 6 -1 71.29 4.00 8 6 1 913.01 41.70 8 6 1 859.41 41.30 -8 6 -1 829.12 41.40 8 -6 1 833.82 41.50 8 -6 1 847.22 41.60 8 -6 1 809.92 41.20 8 -6 1 823.82 41.30 6 6 3 111.39 5.90 6 6 3 115.99 6.10 -6 6 -3 115.79 6.00 6 6 3 108.49 5.90 6 6 3 110.59 6.00 6 -6 3 106.79 6.00 6 -6 3 111.59 6.10 6 -6 3 114.09 5.90 6 -6 3 117.59 5.90 4 6 5 338.97 16.00 4 6 5 296.07 15.90 4 -6 5 312.37 16.00 4 -6 5 322.27 16.00 4 -6 5 323.97 16.00 4 -6 5 322.27 16.00 4 -6 5 331.97 16.00 2 6 7 288.97 14.60 2 -6 7 305.57 14.60 2 -6 7 295.17 14.50 2 -6 7 292.47 14.60 2 -6 7 284.47 14.80 2 -6 7 288.47 14.60 2 -6 7 292.07 14.60 0 6 9 434.66 21.60 0 -6 9 424.16 21.50 0 -6 9 427.56 21.60 0 -6 9 451.15 21.50 0 -6 9 482.75 21.60 0 -6 9 422.86 21.70 0 -6 9 420.96 21.80 -2 6 11 36.10 2.20 -2 -6 11 38.40 2.20 -2 -6 11 35.10 2.40 13 7 -4 18.50 1.70 13 7 -4 17.40 2.00 13 7 -4 21.40 1.60 -13 -7 4 22.40 1.90 13 -7 -4 18.50 1.80 11 7 -2 9.40 1.20 -11 7 2 9.40 1.10 11 7 -2 8.80 1.60 11 7 -2 10.70 1.20 -11 -7 2 10.10 1.20 11 -7 -2 9.80 1.50 9 7 0 1.80 1.10 -9 7 0 0.90 0.60 9 7 0 1.20 0.90 9 7 0 0.90 0.70 9 7 0 1.50 0.80 -9 -7 0 0.40 0.80 9 -7 0 0.40 0.90 9 -7 0 1.60 0.60 7 7 2 4.40 1.30 7 7 2 5.80 0.90 -7 7 -2 4.20 0.90 7 7 2 7.10 1.20 7 7 2 5.10 1.10 -7 -7 -2 3.60 1.40 7 -7 2 4.10 1.10 7 -7 2 4.80 0.80 7 -7 2 4.30 1.10 -5 7 -4 28.30 2.00 5 7 4 27.00 2.10 5 7 4 28.60 1.90 5 -7 4 28.10 1.90 5 -7 4 28.90 1.80 5 -7 4 24.60 2.10 3 7 6 30.30 2.00 -3 7 -6 31.60 2.10 3 -7 6 32.00 1.90 3 -7 6 26.40 2.50 3 -7 6 28.30 2.30 3 -7 6 29.70 2.00 3 -7 6 29.70 2.30 3 -7 6 30.30 2.10 1 7 8 195.28 9.10 1 -7 8 205.38 9.10 1 -7 8 163.18 9.00 1 -7 8 150.88 9.00 -1 7 10 8.60 1.10 -1 -7 10 11.50 1.10 -1 -7 10 10.50 1.30 -1 -7 10 8.90 1.20 12 8 -3 65.19 3.60 -12 8 3 64.09 3.40 12 8 -3 61.59 3.40 12 8 -3 57.99 3.60 -12 -8 3 69.89 3.50 12 -8 -3 56.49 3.60 10 8 -1 14.90 1.60 10 8 -1 13.60 1.30 10 8 -1 14.10 1.40 -10 -8 1 16.50 1.40 -8 8 -1 157.98 8.40 8 8 1 155.18 8.50 8 8 1 173.08 8.50 8 8 1 164.58 8.30 8 8 1 166.68 8.30 8 -8 1 165.18 8.50 8 -8 1 171.18 8.30 -8 -8 -1 163.18 8.40 -6 8 -3 169.78 8.20 6 8 3 155.68 8.10 6 8 3 157.28 8.80 6 8 3 152.78 8.10 6 -8 3 166.08 8.10 4 8 5 43.20 2.50 4 8 5 40.80 2.80 -4 8 -5 44.20 2.70 4 -8 5 46.30 2.50 4 -8 5 42.10 2.70 4 -8 5 45.30 2.60 -2 8 -7 304.47 15.30 2 8 7 312.07 15.20 2 -8 7 317.97 15.20 2 -8 7 289.27 15.20 2 -8 7 313.57 15.20 0 8 9 120.09 6.50 0 -8 9 137.19 6.70 0 -8 9 124.19 6.40 9 9 0 179.78 9.00 9 9 0 174.18 9.00 9 9 0 181.78 9.10 -9 9 0 185.08 9.00 -7 9 -2 254.07 12.50 7 9 2 257.07 12.60 7 9 2 236.58 12.50 7 9 2 246.58 12.50 7 -9 2 265.57 12.50 5 9 4 7.00 1.30 -5 9 -4 8.00 1.10 5 9 4 7.40 1.00 5 -9 4 9.90 1.10 5 -9 4 9.00 0.90 -3 9 -6 281.47 14.60 3 9 6 292.77 14.70 3 -9 6 310.87 14.60 3 -9 6 297.87 14.60 16 0 -6 460.55 21.60 16 0 -6 404.46 22.10 16 0 -6 451.55 21.60 14 0 -4 35.20 2.80 14 0 -4 37.90 2.40 14 0 -4 40.10 2.40 14 0 -4 36.10 2.50 12 0 -2 255.37 13.70 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1295.27 65.69 3 -1 7 1408.06 65.79 3 -1 7 1398.06 65.49 3 -1 7 1412.26 65.69 1 1 9 108.89 5.90 1 1 9 112.09 5.70 1 1 9 105.99 5.90 1 1 9 109.39 6.00 1 1 9 108.39 5.60 1 1 9 106.49 5.70 1 -1 9 114.39 6.00 1 -1 9 104.89 5.60 1 -1 9 104.09 5.80 1 -1 9 109.29 5.90 1 -1 9 108.19 6.10 1 -1 9 109.39 5.70 1 -1 9 90.59 5.70 -1 1 11 976.90 47.40 -1 1 11 939.51 47.70 -1 -1 11 1001.70 47.20 -1 -1 11 990.90 47.40 -1 -1 11 890.31 47.30 -1 -1 11 1022.10 47.70 -3 1 13 367.36 17.90 -3 1 13 362.26 18.60 -3 -1 13 357.96 18.10 -3 -1 13 356.26 17.90 16 2 -6 18.30 1.70 16 2 -6 23.50 1.60 16 2 -6 20.80 1.50 16 -2 -6 16.80 1.90 16 -2 -6 20.90 1.60 -14 2 4 2.30 0.80 14 2 -4 2.40 0.80 14 2 -4 2.80 1.00 14 2 -4 2.40 0.80 14 -2 -4 2.00 0.90 14 -2 -4 2.20 1.10 12 2 -2 54.69 3.10 12 -2 -2 53.79 3.20 10 2 0 137.59 7.70 10 2 0 152.38 7.70 10 -2 0 178.98 7.80 10 -2 0 156.18 7.80 10 -2 0 128.79 7.60 8 2 2 8.70 1.30 8 2 2 6.50 1.30 8 2 2 7.80 1.30 -8 2 -2 7.20 1.20 8 2 2 8.40 1.10 8 2 2 8.00 1.00 8 2 2 5.90 1.00 8 2 2 7.20 1.60 8 -2 2 8.40 1.20 8 -2 2 6.50 1.10 8 -2 2 7.00 1.10 6 2 4 1.80 0.60 6 2 4 2.80 0.90 6 2 4 2.80 0.80 6 2 4 3.40 0.80 6 2 4 2.70 0.80 6 2 4 2.70 0.90 6 -2 4 2.60 0.90 6 -2 4 2.60 0.80 6 -2 4 3.60 0.90 6 -2 4 3.00 0.80 4 2 6 11.20 1.40 4 2 6 11.60 1.30 4 2 6 15.70 1.30 4 2 6 10.50 1.20 4 2 6 11.70 1.50 4 2 6 12.40 1.40 4 2 6 15.40 1.50 4 -2 6 12.90 1.30 4 -2 6 15.70 1.40 4 -2 6 14.40 1.20 4 -2 6 10.90 1.20 4 -2 6 11.00 1.50 4 -2 6 10.80 1.20 2 2 8 168.18 8.30 2 2 8 159.28 8.30 2 2 8 161.48 8.50 2 2 8 140.49 8.30 2 2 8 164.88 8.60 2 2 8 161.68 8.30 2 2 8 167.88 8.20 2 -2 8 165.28 8.50 2 -2 8 162.58 8.40 2 -2 8 165.18 8.60 2 -2 8 162.68 8.60 2 -2 8 157.98 8.40 2 -2 8 170.38 8.40 2 -2 8 165.08 8.20 0 2 10 29.20 2.30 0 2 10 29.50 2.10 0 -2 10 31.40 2.10 0 -2 10 27.00 2.10 0 -2 10 31.00 2.00 0 -2 10 27.60 2.20 0 -2 10 26.60 2.10 0 -2 10 30.90 2.10 0 -2 10 30.40 2.30 -2 2 12 78.69 4.30 -2 2 12 67.89 3.90 -2 -2 12 63.69 4.10 -2 -2 12 74.19 3.80 -2 -2 12 69.39 3.90 -4 2 14 29.40 2.20 -4 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1413.76 67.39 3 3 7 663.43 35.50 3 3 7 698.43 35.80 3 3 7 690.63 35.40 3 3 7 742.83 35.50 3 3 7 760.42 35.40 3 -3 7 714.93 35.60 3 -3 7 740.83 35.70 3 -3 7 765.92 35.80 3 -3 7 754.82 35.50 3 -3 7 725.73 35.60 3 -3 7 720.23 35.40 3 -3 7 702.63 35.60 3 -3 7 741.73 35.40 1 -3 9 28.30 2.10 -1 3 11 1024.10 50.99 -1 3 11 1047.60 50.69 -1 -3 11 1046.10 50.89 -1 -3 11 951.70 50.69 -1 -3 11 1077.79 50.69 -1 -3 11 1090.39 50.59 -3 3 13 303.67 15.70 -3 3 13 309.37 15.50 -3 -3 13 308.17 15.40 -3 -3 13 297.77 15.60 -3 -3 13 337.27 15.40 14 4 -4 4.10 0.80 14 4 -4 4.10 0.90 14 4 -4 3.00 1.00 -14 4 4 4.30 0.80 14 -4 -4 2.10 1.10 12 4 -2 141.49 7.10 -12 4 2 139.79 7.10 12 4 -2 134.79 7.40 12 4 -2 135.09 7.10 12 -4 -2 137.29 7.40 10 4 0 1053.89 52.59 10 4 0 1024.90 52.79 10 4 0 1060.29 52.69 10 4 0 1165.28 52.69 -10 4 0 1087.09 52.59 10 4 0 1112.79 52.59 10 -4 0 1056.29 52.59 10 -4 0 1045.70 52.59 10 -4 0 1105.19 52.89 8 4 2 178.18 8.70 -8 4 -2 160.98 8.60 8 4 2 167.38 8.50 8 4 2 170.48 8.70 8 4 2 166.88 8.50 8 4 2 164.28 8.50 8 -4 2 160.68 8.80 8 -4 2 167.18 8.50 8 -4 2 163.58 8.50 8 -4 2 171.08 8.60 6 4 4 882.31 44.70 6 4 4 862.31 44.50 6 4 4 912.71 44.60 6 4 4 896.61 44.70 6 4 4 964.70 44.70 6 -4 4 878.61 44.80 6 -4 4 932.51 44.70 6 -4 4 990.90 44.60 6 -4 4 887.81 45.10 6 -4 4 925.61 44.60 4 4 6 859.71 40.80 4 4 6 769.22 41.00 4 4 6 803.82 40.90 4 4 6 852.41 40.80 4 -4 6 815.92 41.00 4 -4 6 813.32 40.80 4 -4 6 853.91 40.90 4 -4 6 859.31 40.70 4 -4 6 885.51 40.90 4 -4 6 839.42 41.10 2 4 8 270.77 14.60 2 4 8 294.47 14.50 2 4 8 284.27 14.40 2 -4 8 278.47 14.50 2 -4 8 290.87 14.60 2 -4 8 294.07 14.60 2 -4 8 301.97 14.40 2 -4 8 281.87 14.70 2 -4 8 279.67 14.70 2 -4 8 288.87 14.30 2 -4 8 303.67 14.40 0 4 10 326.57 15.00 0 4 10 292.27 14.90 0 4 10 279.37 15.20 0 -4 10 297.37 15.20 0 -4 10 297.67 15.00 0 -4 10 309.67 15.00 0 -4 10 286.67 15.00 0 -4 10 310.77 14.90 0 -4 10 301.67 15.20 -2 4 12 860.11 41.30 -2 4 12 841.72 41.10 -2 -4 12 804.62 41.10 -2 -4 12 927.71 41.10 -2 -4 12 773.72 41.20 15 5 -5 2.20 0.70 -15 5 5 2.20 0.60 15 5 -5 3.00 0.90 15 5 -5 2.40 0.90 15 -5 -5 1.40 0.90 13 5 -3 23.20 1.70 13 5 -3 19.80 1.90 -13 5 3 19.70 1.50 13 5 -3 19.10 1.50 13 -5 -3 19.40 1.90 11 5 -1 44.40 2.70 11 5 -1 46.80 3.00 -11 5 1 47.00 2.60 11 5 -1 37.50 2.60 11 5 -1 42.80 2.60 11 -5 -1 46.10 3.00 9 5 1 22.90 1.80 9 5 1 21.10 2.30 9 5 1 21.10 1.60 9 5 1 18.90 1.90 -9 5 -1 23.80 1.70 9 -5 1 20.20 2.30 9 -5 1 22.30 1.90 9 -5 1 19.30 1.80 7 5 3 9.70 1.40 -7 5 -3 9.40 1.30 7 5 3 10.30 1.10 7 5 3 9.00 1.30 7 5 3 8.90 1.60 7 5 3 12.60 1.70 7 -5 3 10.90 1.10 7 -5 3 11.00 1.20 7 -5 3 12.30 1.60 7 -5 3 10.20 1.40 5 5 5 1.80 1.00 5 5 5 0.50 1.20 5 5 5 0.90 0.70 5 -5 5 0.70 0.50 5 -5 5 1.30 0.80 5 -5 5 0.90 0.70 3 5 7 359.16 16.90 3 5 7 305.07 17.00 3 -5 7 349.87 17.20 3 -5 7 345.47 17.00 3 -5 7 329.77 17.10 3 -5 7 331.07 17.00 3 -5 7 361.46 17.00 3 -5 7 357.66 16.90 3 -5 7 330.87 17.00 3 -5 7 340.97 16.90 1 5 9 15.80 1.80 1 5 9 18.50 1.50 1 -5 9 19.70 1.60 1 -5 9 16.80 1.50 1 -5 9 18.50 1.90 1 -5 9 16.50 1.40 1 -5 9 17.90 1.50 1 -5 9 18.70 1.70 1 -5 9 18.80 2.50 -1 5 11 138.79 8.40 -1 5 11 177.68 8.20 -1 -5 11 170.28 8.30 -14 6 4 24.90 2.30 14 6 -4 28.40 1.80 14 6 -4 22.00 1.90 14 6 -4 24.00 1.60 -14 6 4 25.10 1.60 14 -6 -4 22.10 1.90 -14 -6 4 29.00 1.80 12 6 -2 28.10 2.30 -12 6 2 33.10 2.10 12 -6 -2 36.60 2.40 10 6 0 373.56 16.80 -10 6 0 375.26 16.60 10 6 0 274.17 16.50 10 6 0 283.47 16.50 10 -6 0 365.06 16.80 8 6 2 8.90 1.50 -8 6 -2 9.40 1.20 8 6 2 7.50 1.30 8 6 2 8.20 1.10 8 6 2 10.00 1.30 8 -6 2 10.00 1.10 8 -6 2 9.00 1.50 8 -6 2 8.10 1.40 8 -6 2 11.40 1.50 6 6 4 27.60 1.80 -6 6 -4 24.20 1.90 6 6 4 24.10 2.10 6 6 4 21.50 2.30 6 -6 4 30.60 1.90 6 -6 4 29.40 2.10 6 -6 4 27.70 2.10 6 -6 4 26.90 1.70 4 6 6 148.39 7.70 4 -6 6 150.38 8.00 4 -6 6 146.09 7.80 4 -6 6 151.28 7.70 4 -6 6 154.28 7.80 4 -6 6 147.29 7.80 4 -6 6 155.68 7.90 4 -6 6 153.88 7.80 2 6 8 294.87 14.00 2 -6 8 292.47 14.00 2 -6 8 283.37 14.00 2 -6 8 291.87 14.10 2 -6 8 257.97 14.00 2 -6 8 260.07 14.20 2 -6 8 282.77 13.90 0 6 10 137.29 6.80 0 -6 10 120.59 6.90 0 -6 10 144.49 6.90 13 7 -3 9.20 1.00 -13 7 3 9.20 1.00 13 7 -3 8.00 1.30 13 7 -3 10.40 1.40 13 -7 -3 12.30 1.40 -13 -7 3 10.50 1.10 11 7 -1 304.97 15.00 11 7 -1 296.87 15.00 11 7 -1 306.17 15.20 11 7 -1 270.47 15.10 11 -7 -1 339.97 15.20 -11 -7 1 303.47 15.10 9 7 1 503.05 26.20 9 7 1 547.35 26.80 9 7 1 552.74 26.10 9 7 1 530.05 26.00 -9 7 -1 515.15 26.10 -9 -7 -1 560.64 26.10 9 -7 1 507.85 26.10 7 7 3 52.09 2.90 7 7 3 42.30 3.30 7 7 3 51.19 3.10 -7 7 -3 51.29 3.00 7 7 3 48.60 3.00 7 -7 3 51.19 3.00 7 -7 3 53.39 3.10 7 -7 3 53.39 2.90 -5 7 -5 843.02 39.60 5 7 5 855.41 39.50 5 -7 5 843.42 39.50 5 -7 5 818.52 39.50 5 -7 5 741.23 39.60 5 -7 5 747.43 39.50 5 -7 5 825.62 39.50 5 -7 5 791.02 39.50 3 7 7 209.88 10.30 -3 7 -7 203.78 10.40 3 -7 7 199.98 10.30 3 -7 7 209.78 10.30 3 -7 7 203.98 10.40 1 7 9 2.70 0.70 1 -7 9 3.40 0.70 1 -7 9 4.60 1.00 1 -7 9 2.20 0.90 10 8 0 123.89 6.80 10 8 0 124.99 6.90 -10 8 0 136.39 6.70 10 8 0 129.59 6.80 10 8 0 137.39 6.80 10 -8 0 127.49 6.80 -10 -8 0 138.49 6.70 8 8 2 7.60 1.00 8 8 2 7.30 1.20 -8 8 -2 9.50 1.00 8 8 2 9.10 1.50 8 -8 2 7.80 0.90 8 -8 2 6.50 1.60 -6 8 -4 9.90 1.10 6 8 4 9.10 1.50 6 8 4 8.00 1.00 6 -8 4 7.70 1.60 6 -8 4 10.70 1.20 6 -8 4 9.70 1.00 -4 8 -6 181.48 8.90 4 8 6 181.78 8.80 4 -8 6 174.38 8.80 4 -8 6 156.48 8.90 4 -8 6 183.88 8.80 2 8 8 175.78 8.70 -2 8 -8 170.18 8.80 2 -8 8 172.68 8.70 2 -8 8 176.48 8.80 -7 9 -3 8.90 1.00 7 9 3 9.00 1.00 7 -9 3 9.90 0.90 7 -9 3 9.40 1.10 -5 9 -5 1.20 0.70 5 9 5 1.30 0.60 5 -9 5 0.10 0.50 5 -9 5 0.90 0.50 16 0 -5 0.40 0.80 16 0 -5 0.10 0.70 14 0 -3 0.10 0.70 14 0 -3 -0.10 1.00 14 0 -3 -0.10 0.80 14 0 -3 -0.10 0.90 8 0 3 1.20 0.90 8 0 3 -0.20 0.60 8 0 3 0.90 0.60 8 0 3 1.00 0.70 8 0 3 0.60 0.80 6 0 5 2.00 0.70 6 0 5 1.40 0.90 6 0 5 0.60 0.80 6 0 5 0.00 0.70 4 0 7 0.20 0.70 4 0 7 0.40 0.80 4 0 7 -0.10 0.70 4 0 7 0.40 0.80 4 0 7 1.70 0.70 4 0 7 -0.10 0.70 2 0 9 1.60 0.80 2 0 9 1.40 0.90 2 0 9 -0.40 1.20 2 0 9 0.30 0.70 2 0 9 0.30 0.80 2 0 9 0.10 0.80 0 0 11 2.30 0.80 0 0 11 3.20 1.00 -2 0 13 0.90 0.90 -2 0 13 0.20 0.60 15 1 -4 0.90 0.90 15 1 -4 1.60 0.80 15 1 -4 1.10 0.70 15 -1 -4 -0.30 0.90 15 -1 -4 1.20 1.00 15 -1 -4 1.90 0.70 13 1 -2 345.57 19.70 13 1 -2 435.86 19.70 13 1 -2 412.96 19.80 13 1 -2 396.46 19.70 13 1 -2 405.46 19.60 13 -1 -2 392.66 19.60 13 -1 -2 355.86 19.60 13 -1 -2 416.36 19.60 13 -1 -2 424.06 19.70 13 -1 -2 387.46 19.80 11 1 0 263.37 13.90 11 1 0 278.97 13.90 11 1 0 254.67 13.70 11 1 0 304.67 14.20 11 1 0 280.17 13.80 11 -1 0 277.57 14.00 11 -1 0 283.57 13.70 11 -1 0 256.97 13.80 11 -1 0 284.57 13.90 9 1 2 82.29 4.40 9 1 2 78.69 4.30 9 1 2 73.39 4.50 -9 1 -2 79.09 4.50 9 1 2 84.59 4.60 9 1 2 87.69 4.60 9 -1 2 82.79 4.50 9 -1 2 85.39 4.50 9 -1 2 76.29 4.30 9 -1 2 85.29 4.70 7 1 4 282.37 14.20 7 1 4 304.47 14.60 7 1 4 294.07 14.20 7 1 4 288.07 14.40 7 1 4 278.97 14.30 7 1 4 287.37 14.40 7 -1 4 291.77 14.40 7 -1 4 277.27 14.50 7 -1 4 268.77 14.90 7 -1 4 296.77 14.40 5 1 6 1269.47 62.89 5 1 6 1292.07 63.09 5 1 6 1249.18 62.89 5 1 6 1244.48 63.29 5 1 6 1337.57 62.99 5 1 6 1266.67 62.99 5 1 6 1286.97 62.69 5 -1 6 1282.47 63.19 5 -1 6 1327.77 62.99 5 -1 6 1410.26 63.09 5 -1 6 1245.98 62.99 3 1 8 1.70 0.80 3 1 8 0.50 0.90 3 1 8 3.80 0.90 3 1 8 0.70 0.80 3 -1 8 0.10 0.80 3 -1 8 1.10 0.80 3 -1 8 0.40 0.70 3 -1 8 1.60 0.90 3 -1 8 1.80 0.70 3 -1 8 2.10 0.80 1 1 10 1434.66 63.89 1 1 10 1317.87 63.49 1 1 10 1101.49 63.49 1 -1 10 1320.57 63.79 1 -1 10 1265.97 63.69 1 -1 10 1336.87 63.49 1 -1 10 1231.48 63.59 1 -1 10 1307.17 63.49 1 -1 10 1417.26 63.59 -1 1 12 475.35 23.10 -1 1 12 440.36 22.80 -1 -1 12 455.95 23.00 -1 -1 12 478.95 22.80 16 2 -5 1.90 0.90 16 2 -5 0.90 0.90 16 2 -5 1.10 0.70 16 -2 -5 1.10 0.90 16 -2 -5 1.30 1.10 14 2 -3 148.39 7.10 14 2 -3 139.09 7.20 14 2 -3 135.99 7.10 14 -2 -3 129.29 7.40 -12 2 1 1032.50 54.99 12 2 -1 1128.69 55.09 12 2 -1 1119.39 55.29 12 2 -1 1177.98 55.19 12 2 -1 1022.20 55.19 12 -2 -1 1137.69 55.39 12 -2 -1 1187.88 55.19 12 -2 -1 1248.78 55.29 10 2 1 40.50 2.60 10 2 1 39.60 2.40 10 2 1 43.20 2.70 10 2 1 38.00 2.30 -10 2 -1 37.00 2.40 10 2 1 35.60 2.50 10 2 1 33.20 2.40 10 -2 1 38.90 2.30 10 -2 1 35.40 2.40 10 -2 1 38.40 2.50 8 2 3 1557.74 79.29 -8 2 -3 1538.85 79.39 8 2 3 1665.03 79.59 8 2 3 1675.43 79.49 8 2 3 1650.53 79.29 8 2 3 1646.54 79.39 8 -2 3 1648.24 79.49 8 -2 3 1655.83 79.89 8 -2 3 1688.33 79.59 8 -2 3 1608.14 79.59 6 2 5 780.82 38.60 6 2 5 752.82 38.50 6 2 5 782.42 38.30 6 2 5 831.42 39.00 6 2 5 761.02 38.40 6 2 5 787.12 38.50 6 2 5 757.52 38.40 6 -2 5 724.13 38.50 6 -2 5 810.52 38.50 6 -2 5 828.42 38.60 6 -2 5 829.92 38.80 4 2 7 154.78 7.80 4 2 7 154.38 8.00 4 2 7 156.68 7.80 4 2 7 153.98 7.70 4 2 7 142.39 8.00 4 2 7 154.28 7.90 4 2 7 152.08 7.80 4 -2 7 153.08 7.80 4 -2 7 143.49 7.90 4 -2 7 153.48 8.10 4 -2 7 143.89 7.90 4 -2 7 154.38 8.10 2 2 9 575.84 27.90 2 2 9 580.14 27.60 2 2 9 504.55 27.60 2 2 9 543.75 27.60 2 -2 9 621.54 28.00 2 -2 9 582.74 27.60 2 -2 9 524.25 27.70 2 -2 9 558.44 27.90 2 -2 9 560.94 27.80 2 -2 9 566.04 27.70 0 2 11 1417.86 67.19 0 2 11 1398.66 67.49 0 -2 11 1425.46 67.49 0 -2 11 1470.15 67.19 0 -2 11 1236.08 67.39 0 -2 11 1333.17 67.19 -2 2 13 59.69 3.30 -2 2 13 57.79 3.50 -2 -2 13 58.39 3.50 -2 -2 13 57.59 3.30 15 3 -4 12.20 1.30 -15 3 4 9.70 1.30 15 3 -4 8.90 1.30 15 3 -4 11.90 1.10 15 -3 -4 8.70 1.50 -13 3 2 92.19 4.90 13 3 -2 96.29 5.00 13 3 -2 87.89 5.10 13 3 -2 98.09 5.00 13 -3 -2 91.89 5.30 11 3 0 43.10 2.70 11 3 0 43.40 2.70 11 3 0 49.99 3.00 11 3 0 47.50 2.90 11 -3 0 52.19 3.10 11 -3 0 45.50 2.90 11 -3 0 42.50 2.90 9 3 2 12.70 1.20 9 3 2 10.80 1.30 -9 3 -2 12.70 1.30 9 3 2 9.90 1.40 9 -3 2 11.90 1.40 9 -3 2 14.30 1.60 9 -3 2 10.60 1.30 7 3 4 38.30 2.60 -7 3 -4 36.20 2.50 7 3 4 41.50 2.50 7 3 4 34.70 2.80 7 3 4 33.80 2.50 7 3 4 46.30 2.40 7 -3 4 39.30 2.70 7 -3 4 39.80 2.50 7 -3 4 37.80 2.90 7 -3 4 40.20 2.50 7 -3 4 42.00 2.50 5 3 6 796.42 40.20 5 3 6 767.22 40.40 5 3 6 798.82 40.30 5 3 6 837.02 40.20 5 3 6 839.52 40.10 5 -3 6 869.41 40.60 5 -3 6 828.92 40.40 5 -3 6 822.12 40.30 5 -3 6 862.71 40.40 5 -3 6 808.02 40.10 5 -3 6 818.12 40.10 3 3 8 2.60 1.00 3 3 8 2.80 0.90 3 3 8 1.90 0.80 3 3 8 2.50 1.00 3 3 8 3.10 1.70 3 -3 8 1.40 0.70 3 -3 8 2.20 0.90 3 -3 8 4.10 1.00 3 -3 8 1.60 0.80 3 -3 8 1.50 0.90 3 -3 8 1.50 0.70 1 3 10 625.24 27.00 1 3 10 544.15 27.20 1 -3 10 605.54 26.90 1 -3 10 514.65 27.20 1 -3 10 501.75 27.00 1 -3 10 557.74 27.20 1 -3 10 533.95 27.10 1 -3 10 515.55 27.20 1 -3 10 543.35 27.00 -1 3 12 241.28 11.20 -1 3 12 178.68 10.70 -1 -3 12 190.88 10.60 -1 -3 12 239.18 10.60 -1 -3 12 229.18 10.50 -1 -3 12 175.78 10.50 14 4 -3 11.70 1.30 14 4 -3 10.30 1.10 14 4 -3 11.50 1.40 -14 4 3 9.60 1.10 14 -4 -3 8.10 1.50 12 4 -1 87.29 4.70 10 4 1 90.19 5.10 8 4 3 47.30 2.90 8 4 3 52.09 3.10 -8 4 -3 46.00 3.40 8 4 3 48.70 2.90 8 4 3 48.30 3.00 8 -4 3 51.79 2.90 8 -4 3 43.90 3.10 8 -4 3 48.70 3.00 6 4 5 231.48 12.20 6 4 5 249.48 12.10 6 4 5 243.88 12.20 6 4 5 221.28 12.30 6 -4 5 235.48 12.10 6 -4 5 242.68 12.30 6 -4 5 244.08 12.20 6 -4 5 244.28 12.10 6 -4 5 245.08 12.40 6 -4 5 251.67 12.50 4 4 7 259.37 14.40 4 4 7 246.68 14.20 4 4 7 300.37 14.10 4 4 7 289.97 14.20 4 -4 7 294.17 14.40 4 -4 7 300.77 14.30 4 -4 7 274.37 14.30 4 -4 7 288.07 14.10 4 -4 7 295.77 14.30 4 -4 7 295.47 14.60 4 -4 7 287.07 14.10 4 -4 7 281.07 14.50 2 4 9 156.48 8.60 2 4 9 171.28 8.40 2 4 9 157.98 8.40 2 -4 9 171.48 8.50 2 -4 9 177.88 8.60 2 -4 9 162.28 8.70 2 -4 9 167.98 8.70 2 -4 9 155.48 8.50 2 -4 9 169.58 8.40 2 -4 9 163.58 8.50 0 4 11 223.18 12.20 0 4 11 224.78 12.10 0 -4 11 261.47 11.90 0 -4 11 218.28 11.90 0 -4 11 253.37 11.90 0 -4 11 246.18 12.10 15 5 -4 4.80 0.90 13 5 -2 325.97 16.50 -13 5 2 338.27 16.60 13 5 -2 316.67 16.70 13 5 -2 370.16 16.60 13 -5 -2 323.47 16.70 11 5 0 454.15 22.30 -11 5 0 435.56 22.30 11 5 0 456.35 22.30 11 5 0 468.75 22.50 11 5 0 463.95 22.30 11 -5 0 438.86 22.50 -9 5 -2 288.67 14.00 9 5 2 270.07 13.90 9 5 2 269.67 14.10 9 5 2 285.87 13.90 9 5 2 276.77 13.90 9 -5 2 275.77 14.10 9 -5 2 270.47 13.90 9 -5 2 296.27 14.00 7 5 4 651.83 31.40 -7 5 -4 606.84 31.30 7 5 4 626.74 31.20 7 5 4 608.84 31.40 7 -5 4 649.93 31.40 7 -5 4 624.54 31.30 7 -5 4 671.73 31.30 7 -5 4 642.14 31.30 7 -5 4 661.33 31.50 5 5 6 302.47 14.80 5 5 6 302.87 14.70 5 -5 6 281.77 14.80 5 -5 6 299.57 14.90 5 -5 6 295.27 14.80 5 -5 6 297.67 14.80 5 -5 6 303.27 14.70 5 -5 6 290.27 14.70 5 -5 6 286.17 15.00 3 5 8 6.40 1.10 3 -5 8 7.10 1.20 3 -5 8 7.80 1.60 3 -5 8 8.20 1.30 3 -5 8 8.60 1.10 3 -5 8 7.40 1.60 3 -5 8 7.70 1.10 3 -5 8 6.80 1.10 1 5 10 788.12 36.80 1 5 10 687.43 37.00 1 -5 10 737.43 36.80 1 -5 10 748.93 36.90 1 -5 10 808.52 36.80 -1 -5 12 203.18 10.60 -1 -5 12 217.38 10.40 14 6 -3 16.30 1.50 12 6 -1 195.68 9.80 -12 6 1 188.38 9.80 12 6 -1 190.38 10.00 12 6 -1 215.78 9.90 12 -6 -1 189.78 10.00 10 6 1 22.30 2.10 10 6 1 23.70 1.70 10 6 1 21.20 1.80 10 6 1 28.20 2.10 10 -6 1 27.60 2.00 8 6 3 118.09 6.00 -8 6 -3 118.99 6.10 8 6 3 121.69 6.00 8 6 3 107.89 6.20 8 6 3 110.99 6.10 8 -6 3 122.09 6.00 8 -6 3 112.89 6.10 8 -6 3 111.19 6.20 8 -6 3 115.69 6.10 -6 6 -5 516.15 25.60 6 6 5 518.75 25.50 6 -6 5 492.85 25.60 6 -6 5 512.65 25.60 6 -6 5 531.35 25.60 6 -6 5 505.35 25.50 6 -6 5 553.54 25.50 4 6 7 111.19 5.50 4 -6 7 107.29 5.50 4 -6 7 113.29 5.50 4 -6 7 104.99 5.60 4 -6 7 95.49 5.70 4 -6 7 99.29 5.80 4 -6 7 104.89 5.60 2 6 9 233.78 10.90 2 -6 9 215.78 11.00 2 -6 9 218.58 10.90 2 -6 9 204.68 10.90 2 -6 9 223.28 10.90 0 6 11 467.25 23.80 0 -6 11 505.75 23.80 11 7 0 12.10 2.20 11 7 0 9.80 1.60 -11 7 0 12.40 1.10 11 7 0 11.60 1.20 11 7 0 10.50 1.50 -11 -7 0 10.50 1.40 11 -7 0 10.90 1.40 9 7 2 1.40 0.70 9 7 2 2.00 1.00 9 7 2 2.00 1.30 9 7 2 1.90 1.20 -9 7 -2 0.30 0.60 9 -7 2 1.10 0.90 -7 7 -4 8.00 1.10 7 7 4 7.90 1.00 7 -7 4 8.20 0.90 7 -7 4 6.20 1.00 7 -7 4 8.00 1.30 7 -7 4 6.60 1.20 5 7 6 1.00 0.70 -5 7 -6 0.70 0.60 5 -7 6 1.00 0.80 5 -7 6 0.80 1.00 5 -7 6 0.70 0.60 5 -7 6 1.20 0.70 3 7 8 8.20 1.00 -3 7 -8 9.10 1.20 3 -7 8 7.70 1.30 3 -7 8 8.30 1.00 3 -7 8 8.20 1.30 -10 8 -1 1.90 0.60 10 8 1 1.60 0.90 10 8 1 2.70 2.00 10 8 1 1.50 0.70 10 -8 1 3.20 1.50 -8 8 -3 22.40 2.00 8 8 3 19.80 1.60 8 -8 3 21.20 1.60 6 8 5 130.29 6.70 6 -8 5 131.29 6.70 6 -8 5 130.99 6.70 -4 8 -7 94.39 4.90 4 8 7 93.99 4.90 4 -8 7 93.89 4.90 4 -8 7 94.99 4.80 16 0 -4 106.59 6.40 16 0 -4 124.19 5.90 14 0 -2 556.34 28.70 14 0 -2 627.74 28.60 14 0 -2 621.54 28.70 14 0 -2 527.75 28.60 12 0 0 12.10 1.60 12 0 0 11.20 1.20 12 0 0 11.40 1.40 12 0 0 9.90 1.40 10 0 2 915.11 44.00 10 0 2 841.32 44.10 10 0 2 919.11 44.40 10 0 2 933.21 44.20 8 0 4 577.64 29.40 8 0 4 597.14 29.90 8 0 4 597.64 29.60 8 0 4 638.44 29.60 8 0 4 591.54 29.50 6 0 6 91.29 4.80 6 0 6 87.89 4.80 6 0 6 88.79 5.00 6 0 6 81.59 5.00 6 0 6 86.19 4.90 6 0 6 89.39 4.80 4 0 8 843.92 39.90 4 0 8 801.52 40.00 4 0 8 863.91 40.20 4 0 8 806.52 40.00 4 0 8 779.82 39.90 4 0 8 792.92 39.90 2 0 10 1049.49 55.69 2 0 10 1234.28 55.99 2 0 10 1127.99 55.69 2 0 10 1155.38 55.69 0 0 12 47.40 3.10 0 0 12 47.40 2.80 15 1 -3 101.59 5.10 15 1 -3 97.79 5.10 15 1 -3 92.29 5.20 15 -1 -3 96.09 5.20 13 1 -1 41.10 2.80 13 1 -1 38.80 2.60 13 1 -1 39.50 3.10 13 1 -1 41.00 2.40 13 -1 -1 30.90 3.10 13 -1 -1 40.70 2.40 13 -1 -1 38.80 2.70 13 -1 -1 41.40 2.60 11 1 1 76.09 4.10 11 1 1 71.09 4.10 11 -1 1 71.39 4.00 11 -1 1 66.59 4.00 9 1 3 303.37 15.10 9 1 3 291.57 14.90 9 1 3 323.87 15.10 -9 1 -3 293.67 15.00 9 1 3 289.57 15.10 9 -1 3 289.67 15.20 9 -1 3 300.27 15.10 9 -1 3 319.07 15.20 7 1 5 867.11 42.00 7 1 5 869.51 42.00 7 1 5 914.51 41.90 7 1 5 842.92 42.30 7 1 5 826.92 42.10 -7 1 -5 813.82 41.90 7 1 5 821.02 42.00 7 1 5 875.21 42.20 7 -1 5 851.81 42.10 7 -1 5 848.82 42.10 7 -1 5 897.61 42.40 7 -1 5 879.21 42.10 5 1 7 44.50 3.00 5 1 7 48.20 3.10 5 1 7 37.70 3.20 5 1 7 45.30 2.80 5 1 7 46.20 2.90 5 1 7 43.10 2.80 5 -1 7 48.20 3.00 5 -1 7 49.50 3.40 5 -1 7 46.90 3.10 5 -1 7 47.00 3.10 5 -1 7 49.00 2.80 5 -1 7 44.00 2.90 3 1 9 783.12 39.20 3 1 9 829.52 39.30 3 1 9 816.52 39.30 3 1 9 812.62 39.60 3 1 9 783.02 39.30 3 1 9 787.02 39.40 3 -1 9 791.42 39.30 3 -1 9 750.42 39.30 3 -1 9 841.42 39.30 3 -1 9 782.92 39.50 3 -1 9 800.82 39.40 3 -1 9 852.01 39.60 1 1 11 313.07 15.20 1 1 11 315.17 15.00 1 -1 11 323.87 15.20 1 -1 11 290.07 15.00 1 -1 11 272.77 14.90 1 -1 11 286.17 14.90 -1 1 13 80.89 4.60 -1 1 13 80.99 4.30 -1 -1 13 81.29 4.60 -1 -1 13 79.99 4.30 16 2 -4 1.00 0.60 16 2 -4 1.80 0.90 16 -2 -4 0.20 0.90 14 2 -2 1.70 1.00 14 2 -2 1.00 0.70 14 2 -2 0.30 0.80 14 -2 -2 0.00 0.90 14 -2 -2 1.30 1.10 12 2 0 28.20 2.10 12 2 0 38.10 2.40 12 -2 0 30.80 2.20 8 2 4 222.58 12.00 8 2 4 232.78 11.80 8 2 4 244.48 11.70 8 2 4 238.98 11.60 -8 2 -4 224.38 11.70 8 2 4 213.78 11.60 8 2 4 243.28 12.00 8 -2 4 239.08 12.10 8 -2 4 241.18 11.80 8 -2 4 219.58 11.90 8 -2 4 239.68 12.10 6 2 6 24.30 1.90 6 2 6 27.80 2.20 6 2 6 24.60 1.90 6 2 6 23.20 2.10 6 -2 6 22.30 2.10 6 -2 6 26.60 1.90 6 -2 6 25.80 1.90 6 -2 6 27.50 2.10 4 2 8 81.39 4.50 4 2 8 80.99 4.50 4 2 8 81.89 4.70 4 2 8 75.09 4.60 4 -2 8 88.09 4.50 4 -2 8 82.89 4.80 4 -2 8 81.09 4.60 4 -2 8 81.79 4.70 4 -2 8 78.39 4.50 4 -2 8 85.69 4.60 2 2 10 67.49 4.00 2 2 10 74.49 4.30 2 -2 10 77.09 4.10 2 -2 10 72.79 4.00 2 -2 10 70.69 4.00 2 -2 10 71.09 4.20 2 -2 10 69.19 4.30 2 -2 10 69.39 4.10 0 2 12 2.10 1.00 0 2 12 0.70 0.70 0 -2 12 1.40 1.00 0 -2 12 0.40 0.70 15 3 -3 262.67 12.50 15 3 -3 259.17 12.50 15 3 -3 253.77 12.60 15 -3 -3 229.78 12.60 -13 3 1 92.09 5.10 13 3 -1 101.09 5.20 13 3 -1 98.39 5.20 13 3 -1 99.29 5.40 13 -3 -1 107.39 5.30 13 -3 -1 92.59 5.40 11 3 1 164.88 9.10 11 3 1 184.58 9.30 11 3 1 190.88 9.30 11 -3 1 194.18 9.20 11 -3 1 164.28 9.10 9 3 3 321.47 16.40 9 3 3 350.46 16.50 9 3 3 304.27 16.20 -9 3 -3 331.57 16.30 9 3 3 333.07 16.20 9 -3 3 316.67 16.30 9 -3 3 334.07 16.40 9 -3 3 327.97 16.50 7 3 5 561.24 30.80 7 3 5 626.14 30.70 7 3 5 602.74 30.60 7 3 5 647.04 30.50 -7 3 -5 613.34 30.60 7 -3 5 660.13 30.80 7 -3 5 650.13 30.60 7 -3 5 604.24 30.70 7 -3 5 645.34 31.00 5 3 7 42.70 2.90 5 3 7 46.10 2.70 5 3 7 46.10 2.80 5 3 7 46.80 2.60 5 3 7 42.10 2.90 5 -3 7 41.40 2.80 5 -3 7 43.60 2.80 5 -3 7 46.20 3.10 5 -3 7 45.30 2.80 5 -3 7 44.60 2.90 5 -3 7 43.30 3.00 3 3 9 1021.60 50.29 3 3 9 995.30 50.59 3 -3 9 1083.39 50.59 3 -3 9 987.60 50.59 3 -3 9 1014.20 50.39 3 -3 9 1124.49 50.69 3 -3 9 980.30 50.39 3 -3 9 1053.59 50.49 1 3 11 333.97 17.00 1 -3 11 330.57 16.80 1 -3 11 348.97 16.80 1 -3 11 339.57 16.90 14 4 -2 252.67 11.70 14 4 -2 223.68 11.70 14 4 -2 237.98 11.60 -14 4 2 224.58 11.70 14 -4 -2 226.18 12.10 12 4 0 8.80 1.30 -12 4 0 7.50 1.00 12 4 0 8.50 1.30 12 4 0 6.90 1.10 12 -4 0 6.10 1.30 12 -4 0 5.20 1.00 10 4 2 435.76 20.50 10 4 2 421.46 20.60 10 4 2 366.26 20.50 10 4 2 395.66 20.40 -10 4 -2 429.86 20.50 10 -4 2 435.56 20.70 10 -4 2 402.66 20.50 10 -4 2 428.76 20.50 8 4 4 640.24 30.20 -8 4 -4 608.34 30.20 8 4 4 606.44 30.40 8 4 4 626.24 30.30 8 -4 4 616.34 30.30 8 -4 4 586.54 30.10 8 -4 4 639.24 30.30 8 -4 4 604.44 30.40 6 4 6 24.40 1.70 6 4 6 18.70 2.20 6 4 6 25.50 2.00 6 4 6 22.60 2.10 6 -4 6 22.80 1.80 6 -4 6 22.50 1.80 6 -4 6 24.00 1.90 6 -4 6 23.20 1.80 4 4 8 407.36 22.60 4 4 8 474.35 22.40 4 -4 8 475.35 22.80 4 -4 8 463.75 22.60 4 -4 8 477.75 22.60 4 -4 8 428.86 22.60 4 -4 8 448.16 22.40 4 -4 8 443.56 22.70 4 -4 8 485.95 22.60 2 4 10 614.14 32.30 2 -4 10 666.53 32.40 2 -4 10 677.43 32.10 2 -4 10 681.53 32.20 2 -4 10 645.54 32.20 0 4 12 10.50 1.80 0 -4 12 12.70 1.30 13 5 -1 9.30 1.10 -13 5 1 9.60 1.00 13 5 -1 8.70 1.30 13 5 -1 9.00 1.60 11 5 1 4.10 1.00 11 5 1 5.60 1.00 11 5 1 4.10 1.00 11 -5 1 7.70 1.30 9 5 3 8.60 1.40 9 5 3 9.80 1.60 9 5 3 12.30 1.20 -9 5 -3 12.90 1.20 9 -5 3 11.90 1.50 9 -5 3 10.00 1.40 9 -5 3 12.70 1.50 9 -5 3 12.30 1.50 7 5 5 47.80 2.90 7 5 5 42.90 3.00 -7 5 -5 47.20 2.80 7 5 5 45.40 2.60 7 -5 5 45.40 2.80 7 -5 5 45.80 2.80 7 -5 5 40.80 2.70 7 -5 5 47.90 2.80 5 5 7 9.50 1.10 5 -5 7 10.70 1.30 5 -5 7 7.30 1.50 5 -5 7 11.10 1.70 5 -5 7 9.30 1.10 5 -5 7 7.90 1.20 5 -5 7 9.80 1.30 5 -5 7 10.50 1.30 3 5 9 98.49 5.00 3 -5 9 97.19 5.00 3 -5 9 94.39 5.10 3 -5 9 96.39 5.10 1 -5 11 42.40 2.40 1 -5 11 41.80 2.50 -12 6 0 1.80 0.80 12 6 0 2.80 1.00 12 6 0 2.10 0.90 12 -6 0 2.70 0.80 -12 -6 0 3.80 1.00 8 6 4 277.67 15.20 8 6 4 328.17 15.10 -8 6 -4 323.77 15.20 8 -6 4 291.77 15.20 8 -6 4 313.77 15.20 8 -6 4 298.77 15.10 8 -6 4 307.57 15.20 -6 6 -6 67.19 3.70 6 6 6 66.79 3.60 6 -6 6 68.59 3.60 6 -6 6 64.89 3.70 6 -6 6 65.59 3.70 6 -6 6 61.79 3.60 -4 6 -8 167.38 8.50 4 6 8 168.28 8.40 4 -6 8 168.88 8.60 4 -6 8 162.68 8.40 4 -6 8 165.08 8.50 4 -6 8 163.98 8.40 2 6 10 184.98 9.60 2 -6 10 202.98 9.60 11 7 1 148.59 8.00 11 7 1 167.88 7.90 11 7 1 152.08 7.80 9 7 3 218.08 10.70 -9 7 -3 211.18 10.70 9 -7 3 213.78 10.80 9 -7 3 216.08 10.70 7 7 5 113.49 5.60 -7 7 -5 118.29 5.70 7 -7 5 102.59 5.70 7 -7 5 102.89 5.60 5 7 7 36.10 2.10 -5 7 -7 31.10 2.20 5 -7 7 38.00 2.10 5 -7 7 34.20 2.10 16 0 -3 0.40 1.00 14 0 -1 -0.50 1.30 14 0 -1 0.60 1.10 14 0 -1 0.70 0.70 14 0 -1 0.30 0.80 12 0 1 76.19 4.50 10 0 3 9.20 1.30 10 0 3 7.40 1.30 8 0 5 0.10 0.70 8 0 5 0.00 0.90 8 0 5 0.00 0.80 8 0 5 0.10 0.80 6 0 7 0.60 0.90 6 0 7 1.30 1.10 6 0 7 1.40 0.80 6 0 7 0.40 0.80 6 0 7 0.80 1.00 6 0 7 0.90 0.90 4 0 9 0.90 0.90 4 0 9 1.60 1.30 4 0 9 1.90 1.10 4 0 9 2.90 0.80 4 0 9 1.40 0.90 4 0 9 1.30 0.90 2 0 11 1.10 1.00 2 0 11 0.20 0.70 2 0 11 0.20 0.80 15 1 -2 39.60 2.30 15 1 -2 39.30 2.40 15 -1 -2 34.10 2.50 15 -1 -2 38.80 2.50 13 1 0 6.30 1.00 13 1 0 4.20 1.00 13 1 0 5.30 1.00 13 -1 0 4.50 0.90 13 -1 0 3.80 1.10 11 1 2 537.05 27.10 11 1 2 506.15 26.90 11 1 2 574.84 27.10 11 1 2 530.85 27.10 11 -1 2 549.85 27.10 11 -1 2 564.74 27.10 11 -1 2 588.74 27.20 9 1 4 356.46 16.90 9 1 4 294.37 16.60 9 1 4 334.97 16.70 9 1 4 334.47 16.80 9 -1 4 339.97 16.80 9 -1 4 356.06 16.90 9 -1 4 341.57 16.80 7 1 6 110.89 6.20 7 1 6 117.29 6.20 7 1 6 120.79 6.10 7 1 6 107.89 6.40 7 1 6 121.99 6.10 7 1 6 113.39 6.40 -7 1 -6 111.39 6.10 7 -1 6 122.39 6.50 7 -1 6 114.99 6.20 7 -1 6 106.49 6.20 7 -1 6 106.89 6.30 7 -1 6 129.69 6.10 7 -1 6 113.69 6.10 5 1 8 833.92 41.50 5 1 8 881.11 41.30 5 1 8 792.12 41.20 5 1 8 801.42 41.30 5 1 8 874.51 41.70 5 1 8 814.02 41.40 5 -1 8 945.71 41.30 5 -1 8 780.62 41.30 5 -1 8 791.62 41.40 5 -1 8 825.42 41.30 5 -1 8 892.11 41.60 5 -1 8 889.11 41.40 3 1 10 185.38 9.60 3 1 10 191.28 9.90 3 1 10 172.98 9.60 3 -1 10 194.18 9.70 3 -1 10 199.78 9.70 3 -1 10 189.28 9.90 3 -1 10 193.78 9.60 1 1 12 152.58 7.90 1 1 12 143.79 7.70 1 -1 12 158.78 7.70 1 -1 12 151.58 7.90 14 2 -1 3.00 0.90 14 -2 -1 5.20 1.10 14 -2 -1 3.60 1.00 12 2 1 373.46 18.30 12 2 1 392.56 18.50 12 2 1 355.26 18.40 12 -2 1 340.67 18.30 12 -2 1 360.56 18.50 12 -2 1 402.76 18.40 10 2 3 476.85 24.40 -10 2 -3 473.15 24.50 10 2 3 503.45 24.70 10 2 3 501.45 24.60 10 -2 3 523.45 24.60 10 -2 3 539.45 24.70 10 -2 3 473.95 24.70 8 2 5 2.00 1.10 8 2 5 1.00 0.90 8 2 5 1.20 0.90 -8 2 -5 1.10 0.90 8 2 5 3.30 0.90 8 2 5 1.30 0.80 8 -2 5 1.20 0.80 8 -2 5 0.70 0.80 8 -2 5 0.70 0.80 6 2 7 648.14 32.10 6 2 7 667.93 32.20 6 2 7 641.34 32.40 6 2 7 655.33 32.30 6 -2 7 682.53 32.60 6 -2 7 611.34 32.20 6 -2 7 713.23 32.40 6 -2 7 622.84 32.20 6 -2 7 617.94 32.40 6 -2 7 698.83 32.20 4 2 9 667.13 35.60 4 2 9 734.13 35.60 4 2 9 727.83 35.60 4 2 9 692.43 35.80 4 -2 9 698.43 35.80 4 -2 9 789.12 35.70 4 -2 9 759.32 35.80 4 -2 9 671.73 35.70 4 -2 9 753.62 35.70 4 -2 9 781.02 35.90 2 2 11 2.10 0.90 2 2 11 1.40 0.80 2 -2 11 0.60 1.00 2 -2 11 1.00 0.80 2 -2 11 1.40 1.30 15 3 -2 20.30 1.60 15 3 -2 22.20 1.40 15 -3 -2 18.70 1.70 -13 3 0 -0.60 0.90 13 3 0 1.40 0.80 13 3 0 0.40 0.90 13 -3 0 1.70 1.10 13 -3 0 0.60 0.80 11 3 2 117.49 6.40 11 3 2 126.69 6.50 11 3 2 121.89 6.60 -11 3 -2 121.79 6.40 11 -3 2 121.29 6.60 11 -3 2 122.49 6.50 11 -3 2 136.19 6.60 9 3 4 91.79 5.10 -9 3 -4 87.09 4.90 9 3 4 88.99 5.30 9 -3 4 101.29 5.10 9 -3 4 91.29 5.10 7 3 6 2.50 1.10 7 3 6 3.00 1.20 7 3 6 2.30 0.80 7 3 6 1.10 1.00 -7 3 -6 3.10 0.80 7 -3 6 1.80 1.10 7 -3 6 1.50 0.90 7 -3 6 2.10 0.80 7 -3 6 2.30 1.00 5 3 8 293.87 15.90 5 3 8 311.37 15.90 5 3 8 319.47 15.70 5 3 8 287.67 15.80 5 3 8 329.47 15.80 5 -3 8 338.87 16.10 5 -3 8 334.27 15.80 5 -3 8 301.87 16.00 5 -3 8 338.17 15.90 5 -3 8 298.77 15.80 5 -3 8 325.47 15.80 3 3 10 62.99 3.50 3 3 10 57.49 3.60 3 -3 10 58.49 3.40 3 -3 10 60.89 3.50 3 -3 10 58.29 3.50 3 -3 10 67.69 3.80 14 4 -1 43.80 2.40 -14 4 1 40.90 2.40 14 4 -1 40.80 2.80 14 -4 -1 41.70 2.60 12 4 1 36.90 2.30 12 4 1 39.30 2.50 -10 4 -3 283.97 14.20 10 4 3 263.47 14.30 10 4 3 308.77 14.20 10 4 3 292.47 14.30 10 4 3 255.97 14.10 10 -4 3 279.57 14.30 10 -4 3 318.87 14.30 10 -4 3 276.57 14.20 8 4 5 2.60 1.10 8 4 5 1.20 1.00 -8 4 -5 2.10 0.70 8 4 5 0.80 0.70 8 -4 5 1.70 0.80 8 -4 5 1.30 0.80 8 -4 5 1.20 0.80 6 4 7 97.89 4.90 6 4 7 96.59 5.10 -6 4 -7 97.89 5.00 6 4 7 79.09 5.10 6 -4 7 98.29 5.00 6 -4 7 85.79 5.30 6 -4 7 96.49 5.10 6 -4 7 105.59 5.10 6 -4 7 85.09 5.10 4 4 9 121.49 7.10 4 -4 9 138.19 6.90 4 -4 9 134.89 7.20 4 -4 9 146.09 7.00 4 -4 9 130.19 6.90 2 -4 11 7.00 1.00 -13 5 0 60.29 3.40 13 5 0 58.89 3.40 13 5 0 61.19 3.60 13 -5 0 73.59 3.60 11 5 2 269.37 13.40 11 5 2 263.67 13.50 11 5 2 234.18 13.50 11 -5 2 288.77 13.50 11 -5 2 290.07 13.50 9 5 4 194.38 10.50 9 5 4 214.28 10.40 -9 5 -4 215.48 10.40 9 -5 4 202.98 10.50 9 -5 4 224.58 10.50 9 -5 4 190.48 10.40 -7 5 -6 90.99 4.80 7 5 6 94.19 4.80 7 -5 6 88.99 4.90 7 -5 6 87.19 4.90 7 -5 6 93.09 4.90 5 5 8 543.95 28.80 -5 5 -8 612.54 28.60 5 -5 8 562.34 28.60 5 -5 8 614.44 28.60 3 -5 10 140.59 7.10 10 6 3 169.68 7.70 -10 6 -3 146.79 7.50 10 6 3 139.49 7.50 10 -6 3 142.59 7.50 10 -6 3 137.89 7.70 -8 6 -5 4.60 0.80 8 6 5 4.00 0.80 8 -6 5 3.70 0.90 8 -6 5 3.80 0.80 -6 6 -7 116.59 5.80 6 6 7 113.69 5.60 6 -6 7 102.79 5.60 6 -6 7 106.79 5.70 14 0 0 287.17 13.30 14 0 0 246.48 13.30 12 0 2 316.47 16.60 12 0 2 332.07 16.60 12 0 2 352.96 16.60 10 0 4 41.00 2.40 10 0 4 33.10 2.40 10 0 4 34.50 2.40 8 0 6 565.24 26.60 8 0 6 605.74 26.70 8 0 6 487.25 26.80 8 0 6 489.55 26.70 8 0 6 536.05 27.00 8 0 6 566.34 26.70 6 0 8 603.84 28.20 6 0 8 545.15 28.40 6 0 8 551.24 28.10 6 0 8 591.94 28.30 4 0 10 21.60 2.30 4 0 10 21.30 2.00 4 0 10 23.90 1.90 15 1 -1 23.80 1.70 15 1 -1 25.90 1.60 15 -1 -1 21.60 2.00 15 -1 -1 26.40 1.80 13 1 1 175.38 8.50 13 1 1 154.88 8.60 13 1 1 176.58 8.60 13 -1 1 187.58 8.60 13 -1 1 149.29 8.60 11 1 3 27.10 2.00 11 1 3 26.90 1.90 11 1 3 21.90 1.80 11 1 3 25.70 2.00 11 -1 3 26.40 2.00 11 -1 3 24.60 2.00 11 -1 3 25.90 1.90 9 1 5 15.80 1.60 9 1 5 12.90 1.50 9 1 5 12.80 1.50 9 -1 5 14.80 1.40 9 -1 5 12.80 1.90 9 -1 5 10.50 2.20 9 -1 5 15.40 1.50 9 -1 5 14.30 1.50 7 1 7 435.36 23.00 7 1 7 479.75 22.70 7 1 7 469.35 22.80 7 1 7 500.75 22.80 7 -1 7 454.95 23.10 7 -1 7 481.35 22.80 7 -1 7 489.55 22.90 7 -1 7 435.16 23.10 7 -1 7 419.76 22.90 7 -1 7 444.06 22.70 5 1 9 46.20 2.90 5 1 9 43.60 2.90 5 1 9 43.70 2.70 5 1 9 45.60 2.90 5 -1 9 46.50 3.10 5 -1 9 46.40 2.80 5 -1 9 46.70 2.70 5 -1 9 44.00 2.80 3 1 11 35.90 2.40 3 1 11 38.20 2.60 3 -1 11 44.00 2.70 3 -1 11 39.10 2.30 14 2 0 32.40 2.30 14 2 0 36.40 2.10 14 -2 0 34.10 2.30 14 -2 0 38.00 2.30 12 2 2 16.60 1.50 12 2 2 17.90 1.60 12 -2 2 16.70 1.70 12 -2 2 19.50 1.60 10 2 4 82.09 4.60 -8 2 -6 7.30 1.10 8 2 6 7.20 1.40 8 2 6 4.70 1.00 8 2 6 6.90 1.10 8 2 6 6.00 1.40 8 -2 6 6.90 1.20 8 -2 6 6.80 1.20 8 -2 6 5.40 1.20 8 -2 6 6.30 1.20 8 -2 6 5.40 1.40 6 2 8 25.70 2.60 6 2 8 29.00 2.20 -6 2 -8 26.90 2.10 6 2 8 26.00 2.30 6 2 8 26.60 2.20 6 -2 8 28.60 2.00 6 -2 8 31.80 2.10 6 -2 8 30.80 2.00 4 2 10 3.30 1.00 4 2 10 3.70 0.90 4 -2 10 3.90 0.70 4 -2 10 2.40 1.00 4 -2 10 3.50 1.10 13 3 1 225.08 11.80 13 3 1 256.57 12.00 13 -3 1 218.58 11.90 13 -3 1 253.07 11.90 11 3 3 114.09 5.90 11 3 3 110.99 5.90 11 -3 3 117.59 5.90 11 -3 3 113.39 5.90 11 -3 3 103.69 5.90 9 3 5 109.19 6.10 9 3 5 115.99 6.10 -9 3 -5 108.79 6.00 9 3 5 123.99 6.00 9 -3 5 116.19 6.10 9 -3 5 116.29 6.10 9 -3 5 123.19 6.20 7 3 7 530.85 29.50 7 3 7 571.24 29.40 7 3 7 575.74 29.40 -7 3 -7 576.64 29.30 7 3 7 624.54 29.40 7 -3 7 614.54 29.40 7 -3 7 669.73 29.50 7 -3 7 629.64 29.40 -5 3 -9 74.89 5.10 5 3 9 70.59 4.70 5 -3 9 90.99 4.50 5 -3 9 88.69 4.50 5 -3 9 83.89 4.80 5 -3 9 88.49 4.50 12 4 2 106.89 5.90 -12 4 -2 103.49 5.50 12 4 2 98.19 5.50 12 -4 2 116.29 5.70 12 -4 2 114.89 5.70 -10 4 -4 22.70 1.80 10 4 4 22.30 1.80 10 4 4 21.20 1.80 10 -4 4 21.10 1.70 10 -4 4 21.70 1.90 10 -4 4 18.80 1.80 8 4 6 237.88 11.40 8 4 6 222.98 11.50 -8 4 -6 228.58 11.40 8 -4 6 212.38 11.50 8 -4 6 220.88 11.40 8 -4 6 247.68 11.50 -6 4 -8 300.77 15.60 6 -4 8 302.57 15.60 6 -4 8 319.07 15.60 6 -4 8 335.17 15.70 11 5 3 49.30 3.10 11 -5 3 54.89 3.10 11 -5 3 57.29 3.10 9 5 5 9.10 1.10 9 5 5 8.10 1.60 -9 5 -5 9.80 1.10 9 -5 5 10.10 1.10 9 -5 5 9.70 1.20 7 5 7 134.29 7.20 -7 5 -7 143.89 7.20 7 -5 7 154.88 7.30 7 -5 7 135.49 7.20 14 0 1 0.60 0.70 8 0 7 -1.10 0.80 8 0 7 0.60 0.70 8 0 7 1.10 0.90 6 0 9 0.10 0.80 6 0 9 0.50 1.00 6 0 9 0.00 0.70 13 1 2 9.80 1.20 13 -1 2 9.30 1.40 13 -1 2 12.80 1.20 11 1 4 54.29 3.50 11 1 4 69.29 3.60 11 -1 4 62.69 3.60 11 -1 4 69.89 3.50 11 -1 4 56.69 3.50 9 1 6 442.56 22.20 9 1 6 431.46 22.10 9 1 6 455.45 22.20 9 -1 6 438.96 22.20 9 -1 6 448.46 22.20 9 -1 6 486.35 22.30 7 1 8 19.60 1.90 7 1 8 19.00 1.60 7 1 8 18.70 1.90 7 -1 8 20.80 2.00 7 -1 8 22.60 1.60 7 -1 8 19.80 1.80 7 -1 8 22.80 1.70 12 -2 3 52.09 2.90 12 -2 3 46.90 2.90 10 2 5 274.97 13.40 10 2 5 259.87 13.40 10 -2 5 290.77 13.50 10 -2 5 267.97 13.40 10 -2 5 251.37 13.40 8 2 7 248.18 13.00 8 -2 7 254.67 12.90 8 -2 7 258.57 13.00 8 -2 7 278.87 13.10 6 2 9 37.50 2.70 6 2 9 33.80 2.60 6 -2 9 42.40 2.40 6 -2 9 38.50 2.30 11 3 4 25.40 1.90 11 -3 4 26.90 1.90 -9 3 -6 276.37 12.90 9 3 6 230.78 12.70 9 -3 6 234.38 12.70 9 -3 6 277.97 12.80 -7 3 -8 8.30 1.30 7 -3 8 9.70 1.10 7 -3 8 6.80 1.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 63874 _shelx_shelxl_version_number 2014/7 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.39863(4) 0.39144(5) 0.56567(4) 0.0359(2) Uani 1 1 d . . . . . O1 O 0.1163(2) 0.3354(3) -0.0334(3) 0.0283(6) Uani 1 1 d . . . . . N1 N 0.2861(3) 0.2998(4) 0.1697(3) 0.0250(6) Uani 1 1 d . . . . . C2 C 0.1879(4) 0.4256(4) 0.3041(4) 0.0278(8) Uani 1 1 d . . . . . H2 H 0.1543 0.4686 0.3517 0.033 Uiso 1 1 calc R . . . . C4 C 0.1711(3) 0.3488(4) 0.0928(4) 0.0247(7) Uani 1 1 d . . . . . C3 C 0.1221(4) 0.4138(4) 0.1664(4) 0.0284(8) Uani 1 1 d . . . . . H3 H 0.0426 0.4490 0.1188 0.034 Uiso 1 1 calc R . . . . C1 C 0.3063(4) 0.3737(4) 0.3755(4) 0.0272(8) Uani 1 1 d . . . . . C5 C 0.3541(3) 0.3111(4) 0.3076(4) 0.0280(8) Uani 1 1 d . . . . . H5 H 0.4335 0.2757 0.3550 0.034 Uiso 1 1 calc R . . . . H1 H 0.318(4) 0.267(5) 0.130(5) 0.028(12) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0411(3) 0.0416(3) 0.0218(3) -0.00283(16) 0.0141(2) 0.00078(18) O1 0.0288(13) 0.0352(15) 0.0221(12) 0.0005(11) 0.0140(11) 0.0021(11) N1 0.0262(15) 0.0285(16) 0.0226(14) 0.0002(12) 0.0144(13) 0.0023(12) C2 0.0329(19) 0.0277(18) 0.0268(18) 0.0003(15) 0.0182(16) 0.0021(15) C4 0.0261(17) 0.0263(18) 0.0235(16) 0.0005(14) 0.0140(14) -0.0002(14) C3 0.035(2) 0.0296(19) 0.0268(18) 0.0025(15) 0.0201(16) 0.0026(15) C1 0.0323(19) 0.0270(18) 0.0212(17) -0.0002(14) 0.0129(15) -0.0008(15) C5 0.0266(18) 0.0309(19) 0.0239(17) 0.0012(15) 0.0112(15) 0.0010(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0140 0.0070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.9340 1.0010 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0250 0.0140 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0390 0.0250 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C4 N1 H1 118(3) . . C5 N1 C4 124.5(3) . . C5 N1 H1 117(3) . . C3 C2 H2 120.1 . . C3 C2 C1 119.8(4) . . C1 C2 H2 120.1 . . O1 C4 N1 120.0(3) . . O1 C4 C3 124.4(4) . . N1 C4 C3 115.6(3) . . C2 C3 C4 120.9(4) . . C2 C3 H3 119.5 . . C4 C3 H3 119.5 . . C2 C1 Br1 120.1(3) . . C5 C1 Br1 119.8(3) . . C5 C1 C2 120.1(4) . . N1 C5 H5 120.5 . . C1 C5 N1 119.0(4) . . C1 C5 H5 120.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Br1 C1 1.889(4) . O1 C4 1.253(5) . N1 C4 1.372(5) . N1 C5 1.368(5) . N1 H1 0.82(5) . C2 H2 0.9500 . C2 C3 1.366(6) . C2 C1 1.413(6) . C4 C3 1.433(5) . C3 H3 0.9500 . C1 C5 1.357(5) . C5 H5 0.9500 . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C2 H2 O1 0.95 2.42 3.303(5) 155.4 6_566 C3 H3 O1 0.95 2.65 3.513(5) 152.1 5_565 C5 H5 O1 0.95 2.29 3.236(5) 173.6 8_556 N1 H1 O1 0.82(5) 1.96(5) 2.779(4) 173(5) 7 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 Br1 C1 C5 N1 -179.7(3) . . . . O1 C4 C3 C2 -179.4(4) . . . . N1 C4 C3 C2 0.5(6) . . . . C2 C1 C5 N1 0.2(6) . . . . C4 N1 C5 C1 0.6(6) . . . . C3 C2 C1 Br1 179.4(3) . . . . C3 C2 C1 C5 -0.6(6) . . . . C1 C2 C3 C4 0.2(6) . . . . C5 N1 C4 O1 179.0(4) . . . . C5 N1 C4 C3 -0.9(5) . . . . _cod_database_fobs_code 3500070