#------------------------------------------------------------------------------ #$Date: 2017-06-05 16:04:27 +0100 (Mon, 05 Jun 2017) $ #$Revision: 197527 $ #$URL: svn://www.crystallography.net/cod/cif/3/50/00/3500071.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500071 loop_ _publ_author_name 'Thierry Maris' _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _journal_name_full 'Personal communication to COD' _journal_year 2017 _chemical_formula_moiety 'C7 H3 N3' _chemical_formula_sum 'C7 H3 N3' _chemical_formula_weight 129.12 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2ya' _space_group_name_H-M_alt 'I 1 2/a 1' _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_date 2017-01-04 _audit_creation_method ; Olex2 1.2 (compiled 2017.01.04 svn.r3372 for OlexSys, GUI svn.r5289) ; _cell_angle_alpha 90 _cell_angle_beta 95.757(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.4485(6) _cell_length_b 6.1845(5) _cell_length_c 13.4791(13) _cell_measurement_reflns_used 5877 _cell_measurement_temperature 150 _cell_measurement_theta_max 60.608 _cell_measurement_theta_min 5.678 _cell_volume 617.79(9) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ; APEX 2 (2013) Bruker AXS Inc., Madison, WI 53719-1173. ; _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 150 _diffrn_detector 'CMOS Area detector' _diffrn_detector_area_resol_mean 10.24 _diffrn_detector_type 'Bruker Photon 100 CMOS Detector' _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device 'k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker Venture Metaljet' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_collimation 'Focusing mirrors' _diffrn_radiation_monochromator 'Helios MX Mirror Optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0601 _diffrn_reflns_av_unetI/netI 0.0321 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 6705 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 60.682 _diffrn_reflns_theta_min 5.740 _diffrn_source 'Metal Jet' _diffrn_source_target Ga _diffrn_source_type 'Gallium Liquid Metal Jet Source' _exptl_absorpt_coefficient_mu 0.478 _exptl_absorpt_correction_T_max 0.7519 _exptl_absorpt_correction_T_min 0.4918 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1276 before and 0.0844 after correction. The Ratio of minimum to maximum transmission is 0.6541. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.388 _exptl_crystal_description block _exptl_crystal_F_000 264 _exptl_crystal_size_max 0.27 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.1 _exptl_special_details ; X-ray crystallographic data for I were collected from a single crystal sample, which was mounted on a loop fiber. Data were collected using a Bruker Venture diffractometer equipped with a Photon 100 CMOS Detector, a Helios MX optics and a Kappa goniometer. The crystal-to-detector distance was 4.0 cm, and the data collection was carried out in 1024 x 1024 pixel mode. ; _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _refine_diff_density_max 0.183 _refine_diff_density_min -0.272 _refine_diff_density_rms 0.090 _refine_ls_extinction_coef 0.044(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.085 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 54 _refine_ls_number_reflns 704 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.085 _refine_ls_R_factor_all 0.0527 _refine_ls_R_factor_gt 0.0509 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1064P)^2^+0.0565P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1375 _refine_ls_wR_factor_ref 0.1412 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 645 _reflns_number_total 704 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file SEJDE01.cif _cod_data_source_block sejde01 _cod_depositor_comments ; The following automatic conversions were performed: '_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according to the built-in table from CIF Core dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29. Automatic conversion script Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas ; _cod_database_code 3500071 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.954 _shelx_estimated_absorpt_t_min 0.882 _olex2_refinement_description ; ; _shelx_res_file ; TITL sejde01_a.res in I2/a sejde01.res created by SHELXL-2016/6 at 12:19:18 on 04-Jan-2017 REM Old TITL SEJDE01 in I2/a REM SHELXT solution in I2/a REM R1 0.149, Rweak 0.004, Alpha 0.051, Orientation as input REM Formula found by SHELXT: C7 N3 CELL 1.34139 7.4485 6.1845 13.4791 90 95.757 90 ZERR 4 0.0006 0.0005 0.0013 0 0.003 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H N DISP C 0.014 0.007 57.748 DISP H -0 0 0.648 DISP N 0.025 0.014 110.512 UNIT 28 12 12 EQIV $1 1-X,0.5+Y,0.5-Z L.S. 30 PLAN 10 SIZE 0.1 0.14 0.27 TEMP -123 HTAB C1 N2_$1 HTAB BOND $H list 4 fmap 2 ACTA OMIT 5 5 0 REM REM REM WGHT 0.106400 0.056500 EXTI 0.043573 FVAR 1.21848 N1 3 0.250000 0.601647 0.500000 10.50000 0.05287 0.02700 = 0.04695 0.00000 0.00890 0.00000 C1 1 0.311786 0.490790 0.425449 11.00000 0.05138 0.02928 = 0.04370 0.00192 0.00944 -0.00131 C2 1 0.316596 0.264402 0.423547 11.00000 0.04967 0.03076 = 0.04260 -0.00136 0.00688 0.00116 N2 3 0.457560 0.058205 0.283746 11.00000 0.07623 0.04420 = 0.05549 -0.00470 0.01987 0.00835 C3 1 0.250000 0.147471 0.500000 10.50000 0.05279 0.02588 = 0.04528 0.00000 0.00554 0.00000 C4 1 0.393357 0.151018 0.344548 11.00000 0.05938 0.03210 = 0.04626 0.00033 0.01076 0.00222 H1 2 0.355071 0.566141 0.373350 11.00000 0.04853 H3 2 0.250000 -0.013529 0.500000 10.50000 0.04084 HKLF 4 REM sejde01_a.res in I2/a REM R1 = 0.0509 for 645 Fo > 4sig(Fo) and 0.0527 for all 704 data REM 54 parameters refined using 0 restraints END WGHT 0.1063 0.0564 REM Instructions for potential hydrogen bonds HTAB C1 N2_$1 REM Highest difference peak 0.183, deepest hole -0.272, 1-sigma level 0.090 Q1 1 0.3277 -0.0113 0.1986 11.00000 0.05 0.18 Q2 1 0.2127 0.6010 0.2862 11.00000 0.05 0.18 Q3 1 0.1429 0.4908 0.3675 11.00000 0.05 0.18 Q4 1 0.5129 0.3688 0.4889 11.00000 0.05 0.17 Q5 1 0.4604 0.5391 0.5524 11.00000 0.05 0.17 Q6 1 0.7047 0.1347 0.3232 11.00000 0.05 0.17 Q7 1 0.3817 -0.1205 0.6020 11.00000 0.05 0.17 Q8 1 0.4344 -0.1422 0.5313 11.00000 0.05 0.17 Q9 1 0.2500 0.7500 0.2500 10.50000 0.05 0.17 Q10 1 0.2459 0.6509 0.2401 11.00000 0.05 0.17 ; _shelx_res_checksum 25001 _shelx_hkl_file ; 0 0 2 1278.57 96.49 0 0 2 1335.47 96.49 0 0 2 1154.48 96.49 0 0 2 1516.25 96.49 0 0 -2 1535.15 96.49 0 0 4 481.25 34.60 0 0 4 496.35 34.60 0 0 -4 479.65 34.60 0 0 -4 496.25 34.60 0 0 -6 14.20 1.20 0 0 6 16.20 1.10 0 0 6 15.20 1.20 0 0 6 14.50 1.10 0 0 6 13.50 1.20 0 0 -6 14.10 1.20 0 0 -6 14.30 1.20 0 0 -8 53.29 3.80 0 0 -8 54.39 3.80 0 0 -8 43.60 3.80 0 0 -8 48.70 3.80 0 0 8 51.79 3.80 0 0 8 50.69 3.80 0 0 -8 55.29 3.80 0 0 8 55.19 3.70 0 0 8 47.10 3.70 0 0 8 52.89 3.90 0 0 10 100.99 7.80 0 0 -10 109.79 8.10 0 0 10 118.89 8.00 0 0 -10 115.39 7.90 0 0 -10 116.69 7.90 0 0 10 115.09 8.00 0 0 10 109.39 7.90 0 0 -10 104.69 7.90 0 0 10 96.49 7.90 0 0 12 485.75 33.90 0 0 12 506.15 34.00 0 0 -12 453.75 33.80 0 0 -12 458.95 33.90 0 0 -14 720.03 52.69 0 0 14 800.92 52.79 0 0 14 716.93 52.59 0 0 -14 694.53 52.69 0 0 14 777.12 52.79 0 0 16 0.50 0.60 0 0 -16 1.00 0.60 0 0 -16 2.30 0.90 0 0 16 2.00 1.10 0 -1 1 1025.40 64.59 0 -1 -1 907.81 64.59 0 -1 1 857.41 64.59 0 -1 -1 987.30 64.59 0 -1 1 872.71 64.59 0 1 1 823.52 64.59 0 1 1 880.41 64.59 0 1 1 779.82 64.59 0 1 -1 1033.00 64.59 0 1 -1 981.60 64.59 0 1 -1 894.61 64.59 0 -1 3 2860.11 188.58 0 -1 3 2640.34 188.68 0 -1 -3 2924.01 188.68 0 1 3 2794.62 188.58 0 1 3 2535.05 188.68 0 1 -3 2552.64 188.58 0 1 -3 2739.53 188.58 0 1 3 2584.74 188.58 0 1 -3 2368.26 188.68 0 -1 5 2822.42 195.28 0 -1 5 2376.16 195.28 0 -1 -5 3075.59 195.28 0 -1 5 2834.12 195.28 0 -1 -5 2883.71 195.28 0 -1 5 3094.79 195.28 0 1 5 2731.03 195.28 0 1 5 2770.62 195.28 0 1 -5 2867.61 195.28 0 1 -5 2683.33 195.28 0 1 5 2523.85 195.28 0 1 -5 2456.45 195.28 0 -1 7 23.20 1.70 0 -1 7 24.60 1.60 0 -1 7 23.20 1.70 0 -1 7 19.40 1.90 0 -1 7 19.90 1.70 0 -1 -7 22.90 1.80 0 -1 7 20.50 1.80 0 -1 -7 24.60 1.70 0 -1 -7 20.10 1.70 0 -1 -7 23.60 1.70 0 -1 -7 19.30 1.70 0 1 7 21.20 1.60 0 1 7 21.60 1.70 0 1 7 22.30 1.60 0 1 7 23.90 1.70 0 1 -7 20.50 1.70 0 -1 9 135.59 9.70 0 -1 9 128.19 9.70 0 -1 -9 141.59 9.80 0 -1 9 139.29 9.60 0 -1 9 138.09 9.80 0 -1 -9 136.29 9.70 0 -1 9 133.09 9.60 0 -1 -9 146.29 9.70 0 -1 -9 128.89 9.70 0 -1 -9 149.99 9.70 0 -1 9 134.69 9.80 0 1 9 131.09 9.60 0 1 -9 139.89 9.80 0 1 9 128.29 9.70 0 1 9 125.79 9.60 0 1 9 141.19 9.70 0 1 9 127.59 9.70 0 1 -9 135.69 9.70 0 1 -9 121.39 9.70 0 -1 -11 170.58 13.60 0 -1 -11 176.18 13.60 0 -1 11 205.18 13.80 0 -1 11 187.68 13.70 0 -1 -11 202.98 13.60 0 -1 -11 186.08 13.70 0 -1 11 179.48 13.80 0 -1 -11 189.08 13.60 0 1 -11 188.58 13.60 0 1 11 215.68 13.70 0 1 11 194.78 13.70 0 1 -11 184.18 13.70 0 1 -11 183.98 13.60 0 1 11 196.98 13.70 0 -1 13 4.80 1.10 0 -1 13 3.80 0.70 0 -1 -13 3.90 1.00 0 -1 -13 3.50 0.70 0 1 13 6.00 1.30 0 1 -13 5.50 0.90 0 1 -13 3.00 0.90 0 -1 -15 34.40 2.90 0 -1 -15 33.60 3.00 0 -1 15 38.00 3.10 0 -1 15 35.80 2.90 0 -1 -15 32.90 2.90 0 1 -15 34.50 2.90 0 1 -15 37.20 2.90 0 1 15 40.00 2.90 0 1 15 36.60 2.80 0 1 15 41.50 4.10 0 -1 -17 5.20 1.00 0 -1 17 5.70 1.20 0 -1 -17 1.90 0.60 0 1 17 3.60 0.80 0 1 -17 3.20 0.60 0 1 -17 2.70 1.20 0 -2 0 1130.39 80.09 0 2 0 1011.80 80.09 0 2 0 1201.98 79.99 0 2 0 1219.68 79.99 0 2 0 1112.29 80.09 0 2 0 1111.19 80.09 0 -2 2 521.85 36.50 0 -2 2 538.05 36.50 0 -2 2 485.35 36.50 0 -2 2 487.85 36.50 0 2 -2 549.05 36.50 0 2 2 521.05 36.50 0 2 2 524.85 36.50 0 2 -2 483.85 36.50 0 2 -2 520.75 36.50 0 2 -2 518.55 36.50 0 -2 -4 651.83 44.40 0 -2 4 652.43 44.30 0 -2 4 679.73 44.50 0 -2 4 589.94 44.40 0 -2 -4 631.14 44.40 0 -2 4 569.14 44.40 0 -2 -4 670.63 44.40 0 2 -4 595.24 44.30 0 2 -4 628.94 44.30 0 2 -4 589.34 44.30 0 2 4 609.54 44.30 0 2 -4 611.64 44.40 0 2 4 655.93 44.30 0 2 4 624.84 44.30 0 -2 6 56.59 4.60 0 -2 6 62.89 4.50 0 -2 -6 57.69 4.50 0 -2 -6 67.69 4.60 0 -2 -6 57.19 4.50 0 -2 6 57.19 4.60 0 -2 -6 62.69 4.50 0 -2 6 70.69 4.40 0 -2 -6 62.79 4.50 0 -2 6 57.39 4.40 0 -2 -6 71.09 4.50 0 2 6 56.49 4.50 0 2 -6 60.29 4.50 0 2 -6 65.49 4.50 0 2 6 62.79 4.50 0 2 6 57.99 4.40 0 -2 -8 0.60 0.40 0 -2 8 0.60 0.60 0 -2 -8 0.90 0.50 0 -2 8 -0.20 0.40 0 -2 8 -0.30 1.00 0 -2 8 0.40 0.40 0 -2 -8 0.50 0.40 0 -2 -8 0.10 0.60 0 -2 -8 0.30 0.60 0 -2 8 1.10 0.70 0 -2 -8 0.40 0.50 0 -2 8 0.30 0.50 0 2 8 0.50 0.30 0 2 8 -0.30 0.40 0 2 8 0.40 0.40 0 2 8 0.30 0.40 0 2 -8 0.40 0.50 0 2 -8 0.30 0.50 0 -2 -10 51.89 4.00 0 -2 -10 47.70 3.80 0 -2 10 48.70 4.00 0 -2 10 45.50 3.90 0 -2 10 53.69 4.10 0 -2 -10 51.29 3.90 0 -2 -10 48.90 3.90 0 -2 -10 56.19 3.80 0 -2 -10 56.49 3.90 0 2 -10 48.50 4.10 0 2 -10 51.09 3.90 0 2 10 59.29 3.90 0 2 10 52.19 3.90 0 -2 12 47.30 3.50 0 -2 12 37.10 3.50 0 -2 -12 44.10 3.20 0 -2 -12 43.50 3.20 0 -2 -12 41.70 3.30 0 -2 -12 42.30 3.40 0 -2 12 37.00 3.20 0 -2 -12 39.80 3.30 0 -2 -12 40.30 3.10 0 2 12 48.20 3.30 0 2 -12 39.10 3.10 0 2 -12 39.70 3.20 0 -2 14 9.50 1.30 0 -2 -14 11.30 1.30 0 -2 14 11.30 1.50 0 -2 -14 11.40 1.40 0 2 14 11.80 1.20 0 2 -14 10.80 1.40 0 2 -14 10.00 1.20 0 2 14 11.40 1.10 0 -2 -16 -1.10 0.70 0 -2 16 -0.60 0.80 0 -2 16 0.90 0.90 0 -2 -16 -0.40 0.50 0 2 16 -0.10 0.60 0 2 16 -0.60 0.50 0 2 -16 0.30 0.50 0 -3 -1 1337.97 89.59 0 -3 1 1264.67 89.69 0 -3 1 1193.38 89.59 0 -3 -1 1149.78 89.59 0 -3 -1 1215.98 89.59 0 -3 1 1238.78 89.59 0 -3 1 1330.07 89.59 0 -3 -1 1249.57 89.59 0 -3 -1 1159.78 89.59 0 -3 -1 1194.08 89.59 0 -3 1 1206.88 89.59 0 3 1 1241.78 89.59 0 3 1 1366.46 89.59 0 3 -1 1215.58 89.59 0 3 1 1419.86 89.59 0 3 -1 1456.15 89.59 0 3 -1 1296.17 89.59 0 3 1 1246.08 89.59 0 -3 -3 47.80 3.40 0 -3 3 44.30 3.40 0 -3 3 43.60 3.40 0 -3 -3 47.00 3.30 0 -3 -3 44.40 3.40 0 -3 3 42.20 3.50 0 -3 3 45.50 3.50 0 -3 3 46.30 3.40 0 -3 3 42.90 3.40 0 -3 3 41.70 3.40 0 -3 -3 44.40 3.40 0 -3 -3 45.50 3.30 0 -3 -3 48.10 3.40 0 3 3 49.10 3.30 0 3 -3 48.50 3.30 0 3 3 50.99 3.30 0 3 3 45.00 3.30 0 -3 -5 117.89 8.70 0 -3 5 117.29 8.70 0 -3 -5 117.39 8.70 0 -3 5 122.59 8.70 0 -3 5 122.19 8.70 0 -3 5 126.69 8.80 0 -3 -5 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5.10 2 -4 0 67.69 4.90 -2 -4 0 68.59 4.90 2 -4 0 71.69 4.90 -2 -4 0 64.69 4.90 2 -4 0 70.69 5.00 2 -4 0 70.69 4.90 -2 -4 0 64.99 5.00 2 -4 0 73.99 5.00 2 4 0 67.29 4.90 2 4 0 65.79 5.00 -2 4 0 65.59 4.90 -2 4 0 74.89 4.90 -2 4 0 71.19 4.80 2 4 0 61.69 4.90 -2 -4 2 66.79 5.40 2 -4 -2 76.09 5.30 2 -4 -2 74.39 5.20 -2 -4 2 66.49 5.30 -2 -4 2 69.19 5.30 2 -4 -2 79.89 5.30 2 -4 -2 75.89 5.30 2 -4 -2 67.59 5.20 2 -4 -2 64.29 5.20 -2 -4 2 68.39 5.30 -2 -4 2 69.19 5.30 2 -4 -2 78.19 5.30 -2 -4 2 61.69 5.30 2 -4 -2 69.49 5.20 -2 4 2 75.59 5.30 -2 4 2 76.99 5.20 2 4 -2 71.29 5.30 -2 4 2 75.29 5.20 -2 4 2 79.39 5.20 2 4 -2 74.59 5.30 2 4 -2 65.69 5.20 -2 -4 4 1762.22 137.79 -2 -4 4 1805.42 137.79 2 -4 -4 1873.51 137.59 -2 -4 4 1900.31 137.69 -2 -4 4 2056.79 137.69 2 -4 -4 1827.12 137.69 -2 -4 4 1976.10 137.79 2 -4 -4 2048.40 137.69 -2 -4 4 1794.42 137.69 2 -4 -4 2100.19 137.69 2 -4 -4 2202.58 137.69 2 -4 -4 1907.01 137.69 2 4 -4 1724.83 137.59 2 4 -4 1909.51 137.69 -2 4 4 1972.30 137.59 -2 4 4 2094.39 137.69 -2 4 4 2049.99 137.59 2 4 -4 2037.80 137.69 2 4 -4 1808.22 137.59 -2 4 4 2030.50 137.59 -2 -4 6 1063.39 77.99 2 -4 -6 1177.48 77.79 -2 -4 6 957.50 77.89 2 -4 -6 1175.18 77.89 -2 -4 6 1114.69 77.79 2 -4 -6 1045.50 77.89 2 -4 -6 1078.79 77.79 -2 -4 6 971.00 77.89 2 -4 -6 1214.18 77.89 2 -4 -6 1248.78 77.89 2 4 -6 1114.09 77.79 -2 4 6 1062.69 77.69 2 4 -6 982.20 77.79 2 4 -6 1207.78 77.89 -2 4 6 1049.20 77.79 -2 4 6 1102.69 77.79 2 -4 -8 4.50 0.90 2 -4 -8 5.50 1.10 2 -4 -8 5.60 1.10 2 -4 -8 6.30 1.00 -2 -4 8 5.60 1.10 2 -4 -8 6.00 0.90 2 -4 -8 6.00 0.80 -2 -4 8 5.60 1.40 2 4 -8 6.90 1.30 2 4 -8 5.60 0.90 -2 4 8 7.80 1.30 -2 -4 10 0.70 1.50 2 -4 -10 1.60 1.10 2 -4 -10 0.20 0.60 2 -4 -10 0.80 0.60 -2 -4 10 0.00 1.20 2 -4 -10 -0.80 0.70 -2 4 10 -0.70 0.80 2 -4 -12 14.40 1.70 2 -4 -12 16.90 1.60 -2 -4 12 12.40 1.80 2 -4 -12 16.40 1.40 2 -4 -12 14.20 1.60 -2 -4 12 16.10 1.90 2 -4 -12 14.70 1.40 2 4 -12 13.90 1.60 2 4 -12 16.40 1.50 -2 4 12 14.20 1.60 2 -4 -14 6.60 1.10 2 -4 -14 6.80 1.20 2 -4 -14 6.40 0.90 -2 -4 14 4.50 1.30 -2 -4 14 5.60 1.30 2 -4 -14 6.30 1.10 -2 4 14 4.60 0.80 2 4 -14 6.20 1.00 2 -5 11 13.50 2.00 -2 -5 -11 10.50 2.10 -2 -5 -11 12.80 1.40 -2 -5 -11 16.50 1.40 2 5 11 12.20 1.30 -2 -5 -9 162.28 12.40 -2 -5 -9 171.88 12.30 2 -5 9 173.98 12.60 -2 -5 -9 165.68 12.30 -2 -5 -9 169.18 12.30 2 -5 9 169.08 12.40 2 5 9 179.08 12.20 -2 -5 -7 122.09 9.20 -2 -5 -7 133.69 9.20 -2 -5 -7 117.69 9.30 2 5 7 130.59 9.20 -2 -5 -5 30.60 2.50 -2 -5 -5 31.00 2.70 2 -5 5 31.70 2.80 -2 -5 -5 30.50 2.60 -2 -5 -5 29.80 2.50 -2 -5 -5 32.70 2.70 2 5 5 31.80 2.50 -2 -5 -3 22.00 2.00 -2 -5 -3 25.60 2.20 2 -5 3 24.70 2.10 2 -5 3 21.20 2.00 -2 -5 -3 23.70 2.10 -2 -5 -3 22.90 2.00 2 -5 3 24.60 2.30 -2 -5 -3 24.60 2.00 2 5 3 24.10 2.10 2 5 3 25.60 2.00 -2 -5 -1 45.60 3.50 -2 -5 -1 43.60 3.60 2 -5 1 48.60 3.70 2 -5 1 46.40 3.60 2 -5 1 48.80 3.60 -2 -5 -1 48.70 3.60 2 -5 1 49.99 3.70 2 -5 1 43.80 3.50 -2 -5 -1 44.70 3.50 -2 -5 -1 45.50 3.70 2 5 1 44.40 3.50 -2 -5 1 10.70 1.40 2 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225.08 15.50 -3 -1 6 190.08 15.40 3 -1 -6 188.88 15.50 -3 1 6 229.88 15.50 3 1 -6 216.18 15.50 3 1 -6 235.88 15.60 3 1 -6 212.08 15.40 3 1 -6 197.18 15.60 3 1 -6 211.58 15.60 3 1 -6 216.08 15.40 -3 1 6 208.58 15.50 -3 1 6 225.78 15.40 -3 -1 8 10.20 1.00 -3 -1 8 9.00 1.10 3 -1 -8 10.60 1.20 -3 -1 8 10.00 1.00 3 -1 -8 9.40 1.20 3 -1 -8 9.50 0.90 3 -1 -8 9.90 1.00 3 -1 -8 10.70 1.10 -3 -1 8 9.50 0.90 3 -1 -8 9.30 1.10 3 -1 -8 10.90 1.20 -3 -1 8 9.70 1.00 -3 1 8 9.50 0.90 -3 1 8 8.40 0.90 3 1 -8 7.00 1.50 3 1 -8 7.90 1.00 3 1 -8 11.00 1.00 3 1 -8 8.10 1.40 -3 -1 10 432.56 32.60 3 -1 -10 452.25 32.70 3 -1 -10 448.86 32.60 3 -1 -10 494.25 32.50 -3 -1 10 466.25 32.70 3 -1 -10 438.76 32.70 3 -1 -10 461.15 32.60 3 -1 -10 422.66 32.60 -3 1 10 506.25 32.60 3 1 -10 423.56 32.60 3 1 -10 483.35 32.70 3 1 -10 466.55 32.60 3 -1 -12 24.20 2.40 -3 -1 12 27.70 2.20 3 -1 -12 26.40 2.30 -3 -1 12 29.40 2.40 3 -1 -12 25.90 2.40 -3 -1 12 22.50 2.70 3 -1 -12 29.20 2.30 3 -1 -12 27.30 2.20 -3 1 12 29.20 2.30 3 1 -12 29.70 2.40 -3 1 12 29.70 2.20 3 1 -12 26.30 2.20 3 1 -12 24.00 2.20 3 -1 -14 32.40 2.40 3 -1 -14 23.40 2.50 -3 -1 14 31.50 2.50 3 -1 -14 26.50 2.50 -3 -1 14 27.90 2.30 3 -1 -14 27.60 2.30 -3 1 14 29.40 2.40 3 1 -14 30.70 2.40 3 1 -14 24.10 2.40 -3 1 14 28.30 2.50 3 1 -14 28.90 2.30 3 -1 -16 1.00 0.90 -3 -1 16 0.20 0.90 3 -1 -16 0.60 0.50 3 -1 -16 0.60 0.80 -3 -1 16 -0.40 0.70 -3 1 16 -0.30 0.60 3 1 -16 -0.30 0.90 3 1 -16 0.20 0.50 -3 -2 -15 13.30 1.30 3 -2 15 14.10 1.30 3 -2 15 14.60 1.60 -3 -2 -15 13.60 1.40 3 -2 15 13.70 1.60 -3 2 -15 13.60 1.30 3 2 15 11.60 1.30 3 2 15 14.10 1.40 -3 -2 -13 2.50 0.50 3 -2 13 2.50 0.70 3 -2 13 1.10 0.90 -3 -2 -13 3.20 0.80 3 -2 13 2.70 1.00 3 2 13 2.50 0.60 -3 2 -13 2.90 0.70 3 2 13 4.20 1.20 3 2 13 2.30 0.80 3 -2 11 46.90 4.20 3 -2 11 46.50 4.20 3 -2 11 54.79 3.90 -3 -2 -11 53.19 4.10 3 2 11 46.30 3.70 3 2 11 47.10 3.80 -3 2 -11 43.50 3.70 -3 -2 -9 284.17 21.50 3 -2 9 316.97 21.60 3 -2 9 335.57 21.80 3 -2 9 291.27 21.60 -3 -2 -9 280.57 21.50 3 2 9 302.87 21.50 -3 2 -9 286.47 21.50 3 2 9 315.67 21.60 3 -2 7 182.68 12.70 -3 -2 -7 164.98 12.60 3 -2 7 165.68 12.60 3 -2 7 168.18 12.60 -3 -2 -7 187.08 12.50 3 -2 7 174.58 12.60 -3 2 -7 198.58 12.70 3 2 7 167.18 12.50 3 2 7 186.28 12.60 3 2 7 153.88 12.50 3 -2 5 10.00 1.80 3 -2 5 12.70 1.20 -3 -2 -5 13.90 1.10 3 -2 5 13.40 1.40 3 -2 5 12.20 1.20 -3 -2 -5 12.30 1.20 3 2 5 12.70 1.10 -3 2 -5 15.50 1.30 3 2 5 12.30 1.30 3 2 5 10.10 1.40 3 -2 3 2011.40 146.19 3 -2 3 2237.08 146.19 3 -2 3 2026.00 146.29 -3 -2 -3 1973.50 146.19 3 -2 3 2021.40 146.19 -3 -2 -3 2085.09 146.19 3 -2 3 2029.30 146.29 3 -2 3 1998.20 146.29 -3 -2 -3 2089.39 146.19 -3 -2 -3 2100.19 146.19 -3 -2 -3 2301.87 146.39 3 -2 3 2133.79 146.19 3 2 3 2015.70 146.19 -3 2 -3 2183.08 146.29 3 2 3 1991.50 146.19 3 2 3 1907.91 146.19 3 2 3 2011.90 146.29 -3 -2 -1 6.30 0.90 -3 -2 -1 7.70 0.70 3 -2 1 6.30 0.70 3 -2 1 6.40 0.80 3 -2 1 7.20 0.90 3 -2 1 6.00 1.10 -3 -2 -1 7.20 0.80 -3 -2 -1 7.50 0.80 3 -2 1 8.70 0.80 3 2 1 5.90 0.80 3 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3 -4 49.40 3.70 -3 3 4 52.39 3.50 -3 3 4 43.70 3.50 3 3 -4 45.60 3.80 3 3 -4 46.90 3.50 -3 3 4 51.79 3.50 -3 -3 6 59.49 4.50 3 -3 -6 60.99 4.40 -3 -3 6 49.99 4.40 3 -3 -6 60.69 4.40 -3 -3 6 64.09 4.40 3 -3 -6 59.59 4.30 3 -3 -6 58.29 4.40 3 -3 -6 60.29 4.40 3 -3 -6 65.29 4.40 3 3 -6 53.49 4.30 3 3 -6 63.49 4.50 -3 3 6 61.79 4.30 3 3 -6 56.49 4.30 -3 3 6 62.99 4.40 3 3 -6 54.59 4.50 3 3 -6 52.09 4.30 -3 3 6 58.99 4.30 3 -3 -8 201.78 15.20 3 -3 -8 206.18 15.10 3 -3 -8 220.28 15.10 3 -3 -8 213.38 15.20 -3 -3 8 186.88 15.10 -3 -3 8 214.28 15.10 3 -3 -8 195.78 15.10 -3 -3 8 215.88 15.20 3 -3 -8 239.58 15.10 3 3 -8 215.28 15.20 3 3 -8 206.68 15.00 3 -3 -10 13.70 1.50 3 -3 -10 14.80 1.60 3 -3 -10 16.30 1.40 3 -3 -10 17.30 1.50 3 -3 -10 13.50 1.50 -3 -3 10 14.30 1.80 3 -3 -10 13.00 1.70 -3 -3 10 12.90 1.60 3 3 -10 14.30 1.40 3 3 -10 14.30 1.70 -3 -3 12 34.40 3.10 3 -3 -12 34.50 2.60 3 -3 -12 31.50 2.90 3 -3 -12 34.20 2.70 -3 -3 12 31.10 2.90 3 -3 -12 32.70 2.80 -3 3 12 34.80 2.70 3 3 -12 35.10 2.70 3 3 -12 34.90 3.00 3 3 -12 32.70 2.70 -3 -3 14 18.90 2.30 3 -3 -14 20.30 1.90 3 -3 -14 20.40 1.70 3 -3 -14 19.40 1.80 3 -3 -14 17.70 1.90 -3 -3 14 20.00 2.00 3 3 -14 20.60 1.80 -3 3 14 23.60 1.80 3 3 -14 18.10 1.90 -3 -4 -13 8.90 1.10 3 -4 13 8.90 1.10 3 -4 13 9.30 1.50 -3 -4 -13 6.70 1.00 3 4 13 9.30 0.90 -3 4 -13 8.50 1.00 3 4 13 7.70 1.10 -3 -4 -11 0.50 0.70 3 -4 11 0.50 0.70 -3 -4 -11 0.50 0.50 3 -4 11 0.40 1.20 3 4 11 0.70 0.50 -3 4 -11 0.70 0.50 3 4 11 1.90 0.60 -3 -4 -9 35.30 3.00 3 -4 9 37.80 3.00 3 -4 9 36.10 3.30 -3 -4 -9 37.00 2.90 3 4 9 36.00 2.90 -3 -4 -7 50.29 3.90 -3 -4 -7 52.39 3.90 3 -4 7 51.79 4.30 -3 -4 -7 49.70 3.90 -3 -4 -7 48.00 4.00 3 -4 7 46.90 3.90 3 -4 7 59.89 4.10 3 4 7 50.69 3.90 -3 -4 -5 20.20 2.00 -3 -4 -5 21.00 1.80 -3 -4 -5 21.70 1.80 -3 -4 -5 19.50 1.80 -3 -4 -5 19.30 1.80 3 -4 5 18.00 1.70 3 -4 5 16.10 2.10 3 4 5 20.60 1.70 -3 -4 -3 40.40 3.50 -3 -4 -3 48.90 3.30 3 -4 3 44.40 3.40 -3 -4 -3 45.50 3.40 3 -4 3 45.70 3.40 -3 -4 -3 45.80 3.30 3 -4 3 43.00 3.50 3 -4 3 41.00 3.30 -3 -4 -3 42.60 3.30 3 4 3 45.20 3.30 3 4 3 36.40 3.30 3 4 3 44.30 3.30 -3 4 -3 45.00 3.50 3 4 3 39.20 3.30 -3 -4 -1 52.49 3.70 3 -4 1 51.19 3.80 3 -4 1 47.70 3.90 -3 -4 -1 52.19 3.80 3 -4 1 52.39 3.80 3 -4 1 49.60 3.70 -3 -4 -1 40.40 4.40 -3 -4 -1 52.89 3.80 -3 -4 -1 50.59 3.70 3 4 1 50.59 3.70 -3 4 -1 47.90 3.80 3 4 1 44.60 3.70 -3 4 -1 51.49 3.80 3 4 1 51.09 3.80 -3 -4 1 153.78 11.60 3 -4 -1 172.68 11.60 -3 -4 1 160.28 11.70 -3 -4 1 164.78 11.60 3 -4 -1 157.28 11.60 3 -4 -1 161.68 11.60 3 -4 -1 174.78 11.60 3 -4 -1 157.28 11.50 -3 -4 1 162.48 11.60 3 -4 -1 176.38 11.60 -3 -4 1 154.38 11.70 -3 4 1 177.98 11.60 3 4 -1 164.78 11.60 -3 4 1 175.78 11.60 3 4 -1 150.48 11.60 -3 4 1 143.39 11.60 3 4 -1 136.89 11.50 -3 -4 3 71.49 6.00 -3 -4 3 74.19 6.10 3 -4 -3 82.89 6.00 3 -4 -3 95.39 6.10 -3 -4 3 80.99 6.20 -3 -4 3 89.19 6.00 3 -4 -3 83.19 6.00 3 -4 -3 80.29 6.00 -3 -4 3 77.39 6.20 3 -4 -3 92.89 6.00 3 -4 -3 80.29 6.00 3 4 -3 74.49 6.00 -3 4 3 88.39 5.90 -3 4 3 79.89 5.90 3 4 -3 82.89 6.00 3 4 -3 79.29 5.90 3 -4 -5 18.70 1.70 3 -4 -5 20.00 1.70 3 -4 -5 19.50 1.80 3 -4 -5 20.70 1.80 -3 -4 5 20.40 2.00 3 -4 -5 21.20 1.80 3 -4 -5 22.00 1.70 -3 -4 5 19.60 1.80 3 -4 -5 19.70 1.70 3 4 -5 20.80 1.90 3 4 -5 19.50 1.60 3 4 -5 15.20 1.90 -3 4 5 16.00 1.80 -3 4 5 20.60 1.70 3 -4 -7 179.68 12.30 3 -4 -7 151.18 12.30 -3 -4 7 170.58 12.40 3 -4 -7 165.08 12.30 3 -4 -7 180.68 12.20 3 -4 -7 170.48 12.20 3 -4 -7 169.38 12.30 -3 -4 7 174.88 12.30 3 4 -7 168.68 12.20 3 4 -7 169.88 12.30 -3 -4 9 59.49 4.90 3 -4 -9 63.99 4.90 3 -4 -9 73.29 4.90 3 -4 -9 58.19 5.00 3 -4 -9 68.29 4.90 3 -4 -9 70.09 5.00 -3 -4 9 66.59 5.10 -3 -4 9 55.49 5.00 -3 4 9 66.29 4.90 3 4 -9 66.89 4.80 3 4 -9 64.59 5.00 -3 -4 11 21.90 2.30 3 -4 -11 27.80 2.00 3 -4 -11 24.20 2.20 -3 -4 11 23.90 2.50 3 -4 -11 27.40 2.10 3 -4 -11 23.50 2.10 3 -4 -11 23.50 2.30 -3 4 11 20.90 2.10 3 4 -11 25.90 2.10 -3 -4 13 2.00 1.00 3 -4 -13 1.80 0.70 -3 -4 13 1.70 1.10 3 -4 -13 0.60 0.60 3 -4 -13 1.40 0.60 3 -4 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26.70 1.80 -3 -5 12 22.80 2.30 -3 -5 12 18.30 2.30 3 -5 -12 22.70 1.90 3 -5 -12 19.50 2.10 3 5 -12 23.90 2.00 3 5 -12 22.20 1.90 -3 5 12 20.00 1.80 -3 -6 -9 5.50 1.00 -3 -6 -9 7.20 1.00 3 6 9 8.40 1.20 3 6 9 6.10 0.80 3 -6 7 3.20 0.90 -3 -6 -7 4.40 0.90 -3 -6 -7 3.00 0.60 3 6 7 4.40 0.80 3 6 7 4.10 1.00 -3 -6 -5 62.99 4.70 -3 -6 -5 61.79 4.70 -3 -6 -5 52.89 4.80 3 6 5 69.89 4.70 3 -6 3 93.89 6.70 -3 -6 -3 85.69 6.60 -3 -6 -3 84.69 6.50 -3 -6 -3 85.09 6.70 3 6 3 88.29 6.50 3 -6 1 195.98 12.90 -3 -6 -1 172.38 12.90 -3 -6 -1 165.28 12.90 -3 -6 -1 168.68 12.80 -3 -6 -1 180.28 12.90 3 6 1 178.58 12.80 3 -6 -1 0.10 0.90 3 -6 -1 1.60 0.60 3 -6 -1 0.00 0.80 -3 -6 1 1.40 0.90 -3 -6 1 -0.80 1.10 -3 -6 1 0.70 0.90 3 -6 -1 1.60 0.70 -3 -6 1 1.00 0.90 -3 -6 1 1.30 0.90 3 -6 -1 2.70 0.70 3 6 -1 1.60 0.80 3 6 -1 1.70 0.60 -3 -6 3 7.80 1.40 3 -6 -3 10.30 1.20 -3 -6 3 6.30 2.10 3 -6 -3 8.00 1.10 3 -6 -3 9.00 1.90 3 -6 -3 11.00 1.40 -3 -6 3 6.00 1.60 3 -6 -3 7.80 1.60 3 -6 -3 7.70 1.00 3 6 -3 7.80 1.00 3 6 -3 8.90 1.40 3 -6 -5 11.90 1.40 3 -6 -5 9.50 1.40 3 -6 -5 9.70 1.10 -3 -6 5 8.60 1.40 -3 -6 5 9.90 1.90 3 -6 -5 10.60 1.10 3 6 -5 8.40 1.80 3 6 -5 9.40 1.10 3 -6 -7 7.90 1.30 3 -6 -7 5.60 0.90 3 -6 -7 8.10 1.30 3 -6 -7 6.60 1.20 3 -6 -7 7.60 1.10 -3 -6 7 5.50 1.40 3 6 -7 9.10 1.00 3 -6 -9 176.98 12.30 3 -6 -9 190.48 12.20 3 -6 -9 159.78 12.60 3 -6 -9 149.49 12.30 3 -6 -9 165.28 12.50 -3 -6 9 167.78 12.50 3 6 -9 177.68 12.20 -3 -7 -6 0.70 0.60 3 7 6 1.40 0.60 3 7 4 4.80 1.00 -3 -7 -2 12.00 1.80 3 7 2 15.50 1.50 3 7 2 15.30 1.30 3 -7 0 0.40 0.80 3 -7 0 -0.40 0.60 -3 -7 0 0.30 1.00 3 7 0 1.60 0.90 3 7 0 0.60 0.50 -3 -7 2 74.39 6.20 3 -7 -2 98.79 6.10 3 7 -2 73.89 6.00 3 -7 -4 46.60 3.50 3 -7 -4 47.90 3.70 3 7 -4 41.80 3.40 3 -7 -6 28.20 2.70 3 -7 -6 33.60 2.60 3 -7 -6 32.70 2.50 3 -7 -6 28.70 2.40 3 7 -6 26.10 2.30 -4 0 -14 19.40 1.70 4 0 14 20.30 1.70 4 0 14 20.60 1.90 4 0 12 1.20 0.90 -4 0 -12 1.20 0.60 4 0 12 0.40 0.90 4 0 12 1.60 1.10 -4 0 -12 2.00 0.70 4 0 12 1.40 0.60 -4 0 -10 7.80 1.00 4 0 10 7.30 1.20 -4 0 -10 7.30 0.90 4 0 10 7.40 1.00 4 0 10 7.00 1.40 4 0 10 6.50 1.20 -4 0 -8 1.60 0.60 4 0 8 1.50 0.90 4 0 8 2.40 0.60 4 0 8 1.50 0.70 4 0 8 1.40 0.60 -4 0 -8 -0.10 1.00 4 0 6 12.00 1.20 4 0 6 11.80 1.20 -4 0 -6 10.90 1.20 4 0 6 13.50 1.30 -4 0 -6 12.20 1.30 4 0 6 11.50 1.10 4 0 6 11.10 1.40 -4 0 -4 5507.15 389.86 -4 0 -4 5919.81 389.86 4 0 4 5256.47 389.96 4 0 4 5381.16 389.86 4 0 4 5285.67 389.86 4 0 4 5311.77 389.96 -4 0 -4 6100.99 389.96 4 0 4 5322.17 389.86 4 0 2 1143.19 86.49 -4 0 -2 1162.98 86.39 4 0 2 1327.37 86.39 4 0 2 1190.18 86.39 -4 0 -2 1196.48 86.39 -4 0 -2 1242.88 86.39 4 0 2 1277.67 86.39 -4 0 0 183.88 13.00 4 0 0 181.48 13.10 4 0 0 158.48 13.00 4 0 0 156.68 13.10 4 0 0 205.08 13.00 -4 0 0 186.98 13.00 -4 0 0 200.08 13.00 -4 0 0 181.98 13.00 4 0 0 187.98 13.00 4 0 -2 1.90 0.60 -4 0 2 2.60 0.50 4 0 -2 2.60 0.60 4 0 -2 3.10 0.40 4 0 -2 2.10 0.60 4 0 -2 2.70 0.70 -4 0 2 2.60 0.50 -4 0 2 2.90 0.40 4 0 -2 3.10 0.50 4 0 -2 3.00 0.50 4 0 -4 118.69 8.70 4 0 -4 126.49 8.80 4 0 -4 122.99 8.70 4 0 -4 121.49 8.80 4 0 -4 130.69 8.70 4 0 -4 103.79 8.80 -4 0 4 127.39 8.70 -4 0 4 121.89 8.70 4 0 -6 63.99 4.80 4 0 -6 59.99 4.90 -4 0 6 64.79 4.80 4 0 -6 74.09 4.90 4 0 -6 68.49 4.80 4 0 -6 73.79 4.90 -4 0 6 59.19 4.80 -4 0 6 64.59 4.80 -4 0 8 394.26 28.30 -4 0 8 352.56 28.30 4 0 -8 370.26 28.40 4 0 -8 392.46 28.50 4 0 -8 412.86 28.30 4 0 -8 419.26 28.40 4 0 -8 375.16 28.40 -4 0 8 406.16 28.40 4 0 -8 406.66 28.40 4 0 -8 456.05 28.40 4 0 -10 2008.10 143.79 4 0 -10 2135.19 143.89 4 0 -10 1791.22 143.79 -4 0 10 2374.16 143.89 4 0 -10 2020.10 143.99 4 0 -10 2041.60 143.89 4 0 -10 2014.90 143.79 4 0 -10 1860.81 143.79 4 0 -12 5.60 1.10 4 0 -12 5.10 1.20 4 0 -12 7.50 1.30 4 0 -12 5.90 1.10 -4 0 12 7.60 1.10 4 0 -12 6.20 1.10 -4 0 14 29.00 2.30 4 0 -14 22.90 2.20 -4 0 14 26.30 2.20 4 0 -14 27.00 2.20 4 0 -14 21.00 2.10 4 0 -16 2.10 0.60 -4 0 16 2.90 1.10 4 0 -16 4.40 1.20 -4 0 16 2.20 1.00 4 -1 13 1.70 0.60 4 -1 13 -0.20 1.00 4 -1 13 0.50 0.80 -4 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-1 -7 211.58 15.50 4 -1 -7 226.18 15.40 4 -1 -7 207.98 15.40 4 -1 -7 208.28 15.40 4 -1 -7 221.88 15.50 4 1 -7 233.88 15.50 -4 1 7 230.08 15.40 -4 1 7 232.68 15.40 4 1 -7 217.48 15.30 4 1 -7 193.38 15.50 4 1 -7 218.48 15.40 -4 1 7 213.48 15.30 -4 1 7 188.78 15.30 4 -1 -9 18.60 1.70 4 -1 -9 19.40 1.50 -4 -1 9 15.30 1.60 -4 -1 9 15.60 1.50 4 -1 -9 15.00 1.60 -4 1 9 15.90 1.50 4 1 -9 16.90 1.80 4 1 -9 15.90 1.50 4 1 -9 16.30 1.50 -4 -1 11 72.99 5.30 4 -1 -11 65.89 5.20 4 -1 -11 71.09 5.20 4 -1 -11 71.49 5.30 4 -1 -11 64.09 5.20 4 -1 -11 68.19 5.10 -4 -1 11 72.29 5.20 4 -1 -11 69.99 5.40 4 1 -11 71.09 5.30 4 1 -11 61.99 5.10 -4 1 11 79.69 5.20 4 1 -11 69.69 5.10 4 1 -11 59.59 5.10 4 -1 -13 71.09 5.90 4 -1 -13 74.69 5.80 4 -1 -13 70.79 5.70 -4 -1 13 86.39 5.90 4 -1 -13 86.59 5.90 -4 -1 13 83.89 5.80 4 -1 -13 77.19 5.90 -4 1 13 89.09 5.90 4 1 -13 69.59 5.80 4 1 -13 76.09 5.80 -4 1 13 84.59 5.80 4 1 -13 67.19 5.80 4 -1 -15 108.09 7.10 4 -1 -15 83.49 7.00 -4 -1 15 97.19 7.00 4 -1 -15 85.09 7.00 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0.50 4 2 -2 3.60 0.80 -4 2 2 3.90 0.50 4 2 -2 3.10 0.70 4 2 -2 3.10 0.50 4 -2 -4 22.70 1.80 4 -2 -4 19.80 1.80 -4 -2 4 26.00 1.80 -4 -2 4 18.50 1.70 4 -2 -4 23.20 1.80 -4 -2 4 21.80 1.90 4 -2 -4 21.70 1.80 4 -2 -4 25.50 1.90 4 -2 -4 20.60 2.00 -4 2 4 21.90 1.70 -4 2 4 22.30 1.70 4 2 -4 23.80 1.70 4 2 -4 24.30 1.90 -4 2 4 25.20 1.80 4 2 -4 21.90 1.90 4 2 -4 18.50 1.70 -4 -2 6 119.79 8.10 4 -2 -6 108.29 8.10 -4 -2 6 117.39 8.00 4 -2 -6 112.39 8.10 4 -2 -6 111.39 8.00 -4 -2 6 103.09 8.00 4 -2 -6 107.09 8.00 4 -2 -6 103.29 8.00 4 2 -6 105.99 8.00 4 2 -6 113.89 8.00 -4 2 6 111.19 7.90 -4 2 6 107.69 7.90 -4 2 6 122.79 8.00 4 2 -6 111.09 8.00 4 2 -6 107.99 8.10 4 -2 -8 100.19 7.80 4 -2 -8 110.39 7.80 4 -2 -8 104.79 7.80 4 -2 -8 107.19 7.70 4 -2 -8 99.89 7.70 -4 -2 8 106.59 7.80 4 -2 -8 114.49 7.80 4 2 -8 102.99 7.80 4 2 -8 104.39 7.70 -4 2 8 118.69 7.70 -4 2 8 101.79 7.70 4 2 -8 101.89 7.60 4 -2 -10 40.70 3.00 4 -2 -10 37.30 3.00 -4 -2 10 32.30 2.90 4 -2 -10 33.30 3.00 4 -2 -10 33.50 2.80 4 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1 74.69 5.40 4 -3 -1 74.19 5.40 4 -3 -1 74.29 5.30 4 -3 -1 75.69 5.40 4 -3 -1 79.69 5.40 -4 3 1 83.89 5.40 4 3 -1 74.59 5.40 4 3 -1 63.39 5.30 -4 3 1 63.89 5.40 4 3 -1 80.59 5.40 -4 -3 3 119.19 8.80 4 -3 -3 140.39 8.90 -4 -3 3 126.89 8.80 -4 -3 3 111.99 8.90 -4 -3 3 136.79 8.80 4 -3 -3 120.99 8.90 4 -3 -3 124.09 8.90 4 -3 -3 125.09 8.90 -4 -3 3 119.99 9.00 4 -3 -3 128.29 8.80 4 -3 -3 127.99 8.80 -4 -3 3 116.69 8.90 4 3 -3 105.09 8.80 4 3 -3 126.39 8.90 4 3 -3 122.69 8.80 -4 3 3 127.79 8.70 -4 3 3 102.59 8.90 4 3 -3 124.69 8.90 -4 -3 5 241.28 15.50 -4 -3 5 216.88 15.60 4 -3 -5 217.68 15.50 4 -3 -5 226.48 15.50 4 -3 -5 224.78 15.50 -4 -3 5 182.08 15.50 4 -3 -5 209.08 15.50 4 -3 -5 219.18 15.50 4 3 -5 204.38 15.40 -4 3 5 229.18 15.50 -4 3 5 214.18 15.40 4 3 -5 208.78 15.50 4 3 -5 220.28 15.60 -4 -3 7 1.90 0.70 -4 -3 7 2.50 0.80 4 -3 -7 2.30 0.90 -4 -3 7 1.00 0.70 4 -3 -7 1.80 0.60 4 -3 -7 0.60 0.70 4 -3 -7 1.60 0.60 4 -3 -7 1.60 0.70 4 3 -7 2.00 0.90 4 3 -7 0.70 0.70 4 3 -7 1.40 0.60 -4 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12.30 1.30 5 -4 1 41.70 3.20 -5 -4 -1 39.10 3.20 -5 -4 -1 41.10 3.20 -5 -4 -1 35.00 3.40 5 -4 1 46.40 3.20 5 4 1 38.60 3.30 5 4 1 42.60 3.20 -5 -4 1 21.00 1.80 5 -4 -1 21.10 1.90 5 -4 -1 19.50 1.80 5 -4 -1 22.80 1.90 -5 -4 1 19.00 1.80 5 -4 -1 21.40 2.00 -5 -4 1 19.50 2.10 5 4 -1 19.90 2.00 5 4 -1 23.00 1.90 5 4 -1 21.70 1.70 5 -4 -3 16.70 1.60 5 -4 -3 17.20 1.60 5 -4 -3 19.50 1.70 5 -4 -3 18.60 1.70 -5 -4 3 19.50 1.70 5 -4 -3 15.60 1.80 5 -4 -3 16.50 1.80 -5 -4 3 17.00 1.90 5 4 -3 19.60 1.50 5 4 -3 15.40 1.90 5 4 -3 20.00 1.80 5 -4 -5 103.99 7.50 5 -4 -5 102.19 7.40 5 -4 -5 96.69 7.40 -5 -4 5 98.09 7.60 5 -4 -5 101.49 7.40 5 -4 -5 108.69 7.50 -5 -4 5 109.09 7.40 5 4 -5 104.19 7.50 5 4 -5 99.69 7.30 5 4 -5 86.99 7.50 5 4 -5 97.69 7.30 -5 -4 7 44.60 3.20 5 -4 -7 39.90 3.30 5 -4 -7 37.20 3.10 -5 -4 7 33.00 3.30 5 -4 -7 43.80 3.20 5 -4 -7 37.80 3.20 5 -4 -7 40.60 3.20 -5 -4 7 41.90 3.50 5 4 -7 44.00 3.30 5 4 -7 43.00 3.50 5 4 -7 37.70 3.10 5 -4 -9 14.90 1.80 5 -4 -9 15.70 1.70 -5 -4 9 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527.95 37.60 -5 -5 2 490.65 37.80 5 -5 -2 517.55 37.60 5 -5 -2 529.25 37.60 5 -5 -2 523.25 37.60 5 5 -2 521.85 37.70 5 5 -2 504.25 37.50 -5 -5 4 1.40 1.00 5 -5 -4 0.90 0.80 -5 -5 4 1.60 0.80 5 -5 -4 0.00 0.90 5 -5 -4 1.30 0.80 5 -5 -4 2.80 0.80 5 -5 -4 0.40 1.00 5 -5 -4 2.90 0.80 5 5 -4 0.30 0.90 5 5 -4 2.90 0.70 5 -5 -6 -1.10 0.70 5 -5 -6 -0.80 0.80 5 -5 -6 0.60 1.10 5 -5 -6 -0.50 0.70 5 -5 -6 -1.40 0.80 -5 -5 6 1.00 1.00 5 5 -6 -0.40 1.00 5 5 -6 0.10 0.60 5 -5 -8 1.50 0.80 5 -5 -8 0.10 0.70 -5 -5 8 -0.20 1.00 5 -5 -8 0.10 0.80 -5 -5 8 0.50 0.90 5 -5 -8 0.30 1.20 5 -5 -8 0.10 0.80 5 5 -8 1.10 1.10 5 5 -8 0.40 0.70 5 -5 -10 20.50 2.10 5 -5 -10 22.70 1.80 5 -5 -10 22.20 2.20 5 -5 -10 19.40 1.90 5 5 -10 25.50 2.30 5 5 -10 22.40 1.90 5 -6 5 43.80 3.40 5 6 5 40.00 3.10 5 6 5 46.80 3.50 5 6 5 36.60 3.70 -5 6 -5 41.60 3.20 5 -6 3 62.09 5.50 -5 -6 -3 69.99 5.40 5 6 3 72.69 5.20 5 6 3 80.19 5.30 -5 -6 1 0.60 0.80 5 -6 -1 -0.60 1.10 5 6 -1 1.50 0.60 5 6 -1 2.30 0.90 -5 -6 3 7.30 1.20 5 -6 -3 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9.00 1.30 7 3 6 6.50 1.30 -7 -3 -4 32.60 2.80 -7 -3 -4 34.10 2.80 7 -3 4 41.60 2.90 7 3 4 37.40 3.00 7 3 4 37.40 2.80 7 3 4 33.80 2.90 -7 -3 -2 4.50 1.00 -7 -3 -2 4.40 0.80 -7 -3 -2 5.80 1.20 7 -3 2 4.90 1.10 7 -3 2 5.40 1.10 7 3 2 6.90 1.20 7 3 2 4.70 0.90 7 3 2 5.20 1.10 7 -3 0 0.70 0.70 -7 -3 0 0.60 0.60 7 -3 0 0.50 0.70 -7 -3 0 0.00 0.80 7 3 0 1.40 0.90 -7 3 0 0.40 0.80 7 3 0 0.00 0.80 7 -3 -2 14.40 1.40 -7 -3 2 12.20 1.40 7 -3 -2 14.60 1.40 -7 -3 2 11.90 1.50 7 -3 -2 15.00 1.50 7 3 -2 12.90 1.60 7 3 -2 13.50 1.60 7 3 -2 13.20 1.30 -7 -3 4 33.40 2.70 7 -3 -4 35.30 2.70 7 -3 -4 37.60 2.90 7 -3 -4 36.50 2.80 -7 -3 4 31.70 2.90 7 3 -4 32.80 2.90 7 3 -4 30.00 2.90 -7 3 4 34.10 2.90 7 3 -4 31.50 2.60 -7 -3 6 18.20 1.70 -7 -3 6 14.50 1.60 7 -3 -6 14.30 1.50 7 -3 -6 13.20 1.50 7 -3 -6 16.70 1.70 -7 -3 6 14.70 1.70 7 3 -6 10.30 1.70 7 3 -6 14.10 1.40 7 -3 -8 12.10 1.30 -7 -3 8 12.60 1.50 7 -3 -8 9.80 1.40 7 -3 -8 11.50 1.30 -7 -3 8 10.30 1.40 7 -3 -8 13.20 1.50 7 3 -8 12.40 1.20 7 3 -8 11.50 1.60 -7 3 8 12.20 1.40 7 3 -8 7.80 1.30 7 3 -8 9.60 1.20 -7 -3 10 27.30 2.30 -7 -3 10 19.10 2.80 7 -3 -10 26.00 2.10 7 -3 -10 21.40 2.60 7 -3 -10 28.20 2.30 7 -3 -10 23.50 2.00 7 3 -10 23.10 2.20 7 3 -10 22.40 2.00 -7 -4 -7 0.80 0.60 7 -4 7 0.00 0.70 -7 -4 -7 1.10 0.70 7 4 7 0.70 0.70 -7 4 -7 -0.40 0.50 7 4 7 1.70 0.90 -7 -4 -5 1.60 1.10 7 -4 5 0.20 0.80 7 4 5 3.00 0.80 7 4 5 2.20 0.90 7 -4 3 9.30 1.30 -7 -4 -3 10.40 1.30 7 4 3 10.10 1.30 7 4 3 8.10 1.30 7 -4 1 2.50 0.90 -7 -4 -1 3.40 0.70 -7 -4 -1 3.10 1.10 -7 4 -1 1.90 0.90 7 4 1 2.80 1.00 7 4 1 4.20 1.00 7 -4 -1 8.60 1.30 7 -4 -1 9.90 1.40 -7 -4 1 9.50 1.20 -7 -4 1 8.30 1.50 7 4 -1 9.30 1.40 7 4 -1 8.20 1.50 7 -4 -3 30.20 2.70 7 -4 -3 38.50 2.80 7 -4 -3 38.20 2.80 -7 -4 3 30.10 2.90 -7 -4 3 31.40 2.70 7 4 -3 30.40 2.80 7 4 -3 33.20 2.60 7 4 -3 31.90 2.80 -7 -4 5 10.20 1.40 7 -4 -5 11.90 1.50 -7 -4 5 8.80 1.50 7 -4 -5 13.30 1.40 7 -4 -5 9.20 1.30 7 4 -5 10.70 1.10 7 4 -5 11.70 1.50 7 -4 -7 5.10 0.90 7 -4 -7 5.40 1.10 -7 -4 7 4.70 1.00 7 -4 -7 3.30 1.10 7 -4 -7 4.60 0.90 -7 -4 7 6.40 1.70 7 4 -7 3.30 1.20 7 4 -7 4.40 1.10 -7 -4 9 -0.20 0.80 7 -4 -9 -0.10 0.60 7 -4 -9 0.50 0.70 7 -4 -9 0.10 0.90 7 -4 -9 0.60 0.90 7 4 -9 0.60 0.60 7 4 -9 -0.30 0.80 -7 -5 -2 -0.20 1.00 7 -5 2 0.50 0.80 7 5 2 -0.70 0.80 7 5 2 -1.10 0.90 -7 -5 0 132.19 9.90 7 5 0 128.59 10.00 7 5 0 151.28 10.00 -7 -5 2 8.10 1.20 7 -5 -2 7.40 1.60 -7 -5 2 5.20 1.20 7 -5 -2 8.90 1.40 7 5 -2 6.50 1.30 7 5 -2 7.70 0.90 7 -5 -4 -1.40 0.90 -7 -5 4 1.20 0.90 -7 -5 4 0.70 0.80 7 -5 -4 0.40 1.00 7 5 -4 -0.30 0.90 7 5 -4 -0.80 0.70 -7 -5 6 1.40 0.90 7 -5 -6 1.60 1.00 -7 -5 6 0.80 1.00 7 -5 -6 2.20 0.90 7 -5 -6 1.90 0.90 7 5 -6 0.30 1.00 8 0 8 141.39 9.10 -8 0 -8 117.99 9.00 8 0 8 126.89 9.00 -8 0 -8 112.39 9.00 -8 0 -6 96.09 7.10 8 0 6 88.29 7.20 8 0 6 98.59 7.10 8 0 6 108.69 7.30 8 0 4 11.30 1.20 8 0 4 9.20 1.40 8 0 4 13.10 1.50 -8 0 -4 11.70 1.20 8 0 2 1.10 0.60 8 0 2 0.70 1.00 -8 0 -2 1.30 0.60 8 0 2 0.10 1.00 8 0 2 1.00 0.60 -8 0 0 16.50 1.50 8 0 0 12.50 1.70 8 0 0 15.40 1.50 8 0 0 13.80 1.40 8 0 0 17.00 1.70 8 0 -2 0.40 0.60 8 0 -2 0.90 0.90 -8 0 2 1.40 0.80 8 0 -2 1.00 0.70 8 0 -2 1.20 1.00 -8 0 2 1.20 0.80 8 0 -4 36.00 3.00 8 0 -4 34.50 3.00 8 0 -4 38.50 2.80 8 0 -4 35.10 2.90 8 0 -4 29.50 3.10 -8 0 4 40.80 3.10 8 0 -6 398.96 30.70 8 0 -6 451.05 30.80 8 0 -6 422.66 30.80 8 0 -6 399.96 30.80 8 0 -6 447.76 30.70 -8 0 6 468.35 30.90 -8 0 8 28.20 2.50 8 0 -8 25.40 2.50 8 0 -8 26.40 2.60 8 0 -8 27.50 2.20 8 0 -8 27.80 2.40 8 0 -8 23.80 2.30 -8 0 8 32.50 2.40 8 0 -10 8.20 1.20 -8 0 10 11.90 1.20 8 0 -10 10.50 1.30 -8 -1 -7 2.10 0.90 8 -1 7 1.70 1.00 8 -1 7 2.60 0.90 -8 -1 -7 1.60 0.60 8 1 7 2.40 0.60 8 1 7 2.40 0.80 8 1 7 2.20 1.50 -8 1 -7 2.80 0.60 -8 -1 -5 34.00 3.00 8 -1 5 39.60 2.90 8 -1 5 41.60 3.00 -8 -1 -5 35.60 2.90 -8 1 -5 40.80 2.90 8 1 5 39.90 3.10 8 1 5 37.90 2.90 8 1 5 34.70 3.00 8 1 5 31.20 2.80 8 -1 3 2.50 0.70 8 -1 3 1.80 0.90 -8 -1 -3 3.00 0.80 -8 -1 -3 2.70 0.60 8 -1 3 3.40 1.10 8 1 3 3.90 0.80 8 1 3 2.50 0.60 -8 1 -3 3.10 0.70 8 1 3 3.60 0.90 8 -1 1 13.80 1.50 -8 -1 -1 13.10 1.60 8 -1 1 13.90 1.40 8 -1 1 12.90 1.40 -8 -1 -1 13.30 1.40 8 -1 1 11.10 1.70 8 1 1 14.80 1.70 8 1 1 13.70 1.40 -8 1 -1 17.10 1.40 8 1 1 14.10 1.30 8 -1 -1 32.30 2.50 8 -1 -1 29.20 2.60 8 -1 -1 30.50 2.70 -8 -1 1 27.60 2.60 8 -1 -1 33.10 2.50 -8 -1 1 29.50 2.50 -8 1 1 33.40 2.50 8 1 -1 30.40 2.50 8 1 -1 29.80 2.40 8 1 -1 29.40 2.60 8 -1 -3 8.60 1.10 8 -1 -3 8.20 1.30 8 -1 -3 8.70 1.10 -8 -1 3 9.00 1.30 -8 -1 3 7.80 1.30 8 1 -3 7.70 1.00 8 1 -3 5.20 1.30 -8 1 3 8.80 1.30 8 1 -3 7.20 1.30 8 1 -3 7.50 1.20 -8 -1 5 6.00 1.20 8 -1 -5 4.50 0.90 8 -1 -5 5.90 1.00 8 -1 -5 7.90 1.30 8 1 -5 4.20 1.10 8 1 -5 6.00 1.20 8 1 -5 4.70 1.00 8 1 -5 6.50 0.90 8 1 -5 6.30 1.10 -8 1 5 6.10 1.30 8 -1 -7 12.60 1.30 8 -1 -7 10.80 1.40 -8 -1 7 12.20 1.50 8 -1 -7 14.10 1.70 8 -1 -7 12.30 1.40 -8 1 7 12.00 1.70 8 1 -7 12.90 1.60 8 1 -7 13.20 1.30 8 1 -7 11.90 1.30 -8 -1 9 47.60 3.80 8 -1 -9 42.40 3.60 8 -1 -9 46.50 3.50 8 -1 -9 50.89 3.80 8 -1 -9 44.70 3.60 8 1 -9 41.70 3.50 8 1 -9 44.10 3.50 -8 1 9 55.09 3.60 8 1 -9 45.00 3.70 8 -1 -11 23.10 1.90 -8 -1 11 25.90 2.10 8 -1 -11 22.70 2.20 8 -1 -11 22.50 2.00 8 1 -11 22.00 2.10 8 1 -11 23.60 2.00 -8 1 11 27.60 2.10 8 -2 6 0.40 0.60 8 -2 6 0.60 1.20 -8 -2 -6 -0.70 0.50 -8 -2 -6 -1.40 1.30 8 2 6 1.10 0.60 -8 2 -6 1.70 0.60 8 2 6 1.00 0.80 -8 -2 -4 1.80 0.80 -8 -2 -4 2.90 0.70 8 -2 4 3.00 0.80 8 -2 4 3.30 0.70 8 2 4 4.00 0.60 -8 -2 -2 0.10 0.60 8 -2 2 -0.20 0.70 8 -2 2 0.40 0.60 -8 -2 -2 0.10 0.70 8 2 2 0.30 0.70 -8 2 -2 0.60 0.70 8 2 2 0.10 0.50 8 2 2 1.50 0.80 8 -2 0 4.50 0.80 8 -2 0 4.20 0.90 8 -2 0 2.20 0.90 -8 -2 0 2.50 0.70 8 2 0 2.50 0.80 -8 2 0 2.70 0.90 8 2 0 3.00 0.70 8 2 0 2.50 0.90 -8 -2 2 6.90 1.10 8 -2 -2 8.60 1.20 -8 -2 2 5.50 1.10 8 -2 -2 6.50 1.00 8 -2 -2 6.30 1.00 8 2 -2 5.80 1.10 8 2 -2 5.80 1.10 8 2 -2 6.10 1.20 8 2 -2 5.40 0.80 8 -2 -4 15.40 1.60 -8 -2 4 13.70 1.60 8 -2 -4 16.20 1.50 -8 -2 4 12.00 1.60 8 -2 -4 15.60 1.50 8 2 -4 14.40 1.30 -8 2 4 15.20 1.70 8 2 -4 12.20 1.60 8 2 -4 12.40 1.70 8 -2 -6 2.20 0.80 8 -2 -6 2.60 0.80 -8 -2 6 1.30 0.80 8 -2 -6 1.60 1.00 -8 -2 6 2.70 0.80 8 2 -6 -0.40 0.90 8 2 -6 1.10 0.70 8 2 -6 1.20 0.60 -8 -2 8 -0.50 0.80 8 -2 -8 1.00 0.90 8 -2 -8 -0.20 1.00 -8 -2 8 -0.20 0.70 8 -2 -8 0.90 0.70 8 -2 -8 0.00 0.70 8 2 -8 1.30 0.90 8 2 -8 -0.40 0.60 -8 2 8 0.60 0.70 8 2 -8 0.80 0.60 8 -2 -10 5.60 1.10 -8 -2 10 6.10 1.00 8 -2 -10 4.80 1.00 -8 -2 10 7.50 1.40 8 -2 -10 4.60 0.90 8 2 -10 3.10 1.00 8 2 -10 6.50 1.20 -8 2 10 5.00 1.00 8 2 -10 5.20 0.90 8 -3 5 1.70 0.80 8 -3 5 2.50 0.80 -8 -3 -5 2.80 0.60 -8 3 -5 2.20 0.70 8 3 5 3.20 0.80 8 3 5 4.60 0.90 8 3 5 2.90 0.50 -8 -3 -3 1.20 0.60 8 -3 3 1.10 0.80 -8 -3 -3 -0.30 0.90 8 -3 3 1.30 0.70 -8 3 -3 0.80 0.70 8 3 3 1.90 0.80 8 3 3 2.00 0.50 8 3 3 -0.40 0.80 -8 -3 -1 6.00 1.20 8 -3 1 7.80 1.10 8 -3 1 9.30 1.20 -8 -3 -1 5.80 1.00 -8 3 -1 6.70 1.20 8 3 1 6.60 1.20 8 3 1 7.00 0.90 8 3 1 8.80 1.40 8 -3 -1 10.50 1.40 -8 -3 1 9.90 1.40 -8 -3 1 9.70 1.20 8 3 -1 10.50 1.10 8 3 -1 10.60 1.40 8 3 -1 11.40 1.40 8 -3 -3 7.10 1.10 -8 -3 3 6.90 1.20 8 -3 -3 5.00 1.10 8 -3 -3 5.10 1.00 -8 -3 3 4.10 0.90 8 3 -3 4.80 1.10 8 3 -3 5.70 1.20 -8 3 3 7.90 1.40 8 3 -3 6.30 0.80 8 -3 -5 37.10 2.80 -8 -3 5 30.60 2.80 -8 -3 5 31.90 3.40 -8 -3 5 36.30 2.90 8 3 -5 36.80 2.70 8 3 -5 35.90 2.90 8 3 -5 31.50 2.70 -8 -3 7 7.60 1.30 -8 -3 7 5.60 1.20 8 -3 -7 8.80 1.30 8 3 -7 6.60 1.30 -8 3 7 8.90 1.20 8 3 -7 7.20 0.90 8 3 -7 5.50 0.90 -8 -4 -2 50.79 4.10 8 -4 2 56.79 4.10 8 4 2 58.99 4.00 8 4 2 50.79 4.20 8 4 2 54.89 4.10 -8 -4 0 124.79 9.90 8 4 0 147.09 9.80 8 4 0 133.59 9.80 8 4 0 135.39 9.80 -8 -4 2 14.90 1.60 -8 -4 2 11.80 1.60 8 -4 -2 17.20 1.70 8 4 -2 11.30 1.60 8 4 -2 16.80 1.40 8 -4 -4 0.00 1.00 8 -4 -4 0.50 0.80 -8 -4 4 0.00 0.80 8 -4 -4 0.00 0.90 -8 -4 4 2.40 0.90 8 4 -4 0.40 0.90 8 4 -4 1.00 0.60 8 4 -4 1.90 1.10 8 -4 -6 1.70 0.70 8 -4 -6 1.20 0.90 -8 -4 6 2.00 0.80 8 -4 -6 1.80 0.80 8 4 -6 2.40 0.70 8 4 -6 1.80 0.90 8 4 -6 0.70 0.70 -9 0 -3 1.00 0.70 9 0 3 0.40 0.50 -9 0 -3 0.60 1.10 9 0 3 -1.00 0.90 -9 0 -1 0.50 0.70 9 0 1 -0.30 0.80 9 0 1 -1.60 0.90 9 0 1 0.60 0.60 -9 0 -1 0.70 0.70 9 0 -1 0.40 0.90 9 0 -1 -0.60 0.60 9 0 -1 -0.40 0.70 -9 0 1 1.20 0.80 9 0 -3 0.50 0.60 9 0 -3 0.60 0.70 -9 0 3 -0.40 0.70 9 0 -3 -2.30 2.00 9 0 -5 1.70 1.30 9 0 -5 2.10 1.50 9 0 -5 0.30 0.60 -9 0 7 1.90 1.00 -9 0 7 -0.30 0.70 9 0 -7 -0.20 0.60 9 0 -7 -1.70 1.00 9 -1 4 0.70 0.60 9 -1 4 1.30 1.00 -9 -1 -4 1.10 0.50 -9 -1 -4 1.30 0.70 -9 1 -4 0.30 0.60 9 1 4 0.90 0.50 9 1 4 0.70 0.80 9 -1 2 1.80 0.60 9 -1 2 2.30 1.00 -9 -1 -2 1.30 0.70 -9 -1 -2 3.70 1.10 9 1 2 2.50 0.60 9 1 2 3.30 0.80 9 1 2 2.80 1.10 -9 1 -2 2.20 0.70 9 -1 0 8.10 1.00 9 -1 0 9.50 1.10 -9 -1 0 7.10 1.10 9 -1 0 6.10 1.30 -9 -1 0 8.50 1.20 9 1 0 9.10 1.00 9 1 0 9.00 1.20 -9 1 0 5.90 1.30 9 1 0 6.60 0.90 -9 1 0 8.80 1.20 9 -1 -2 3.10 1.00 9 -1 -2 4.50 0.90 -9 -1 2 4.60 1.10 -9 -1 2 2.90 1.10 9 -1 -2 4.00 0.80 -9 1 2 4.80 1.10 9 1 -2 4.50 0.90 9 1 -2 3.80 0.90 9 1 -2 4.20 0.70 -9 -1 4 32.80 2.70 9 -1 -4 30.80 2.80 9 -1 -4 31.60 2.60 9 -1 -4 32.50 2.60 -9 1 4 32.20 2.70 9 1 -4 32.20 2.50 9 -1 -6 15.60 2.10 -9 -1 6 16.80 1.70 9 -1 -6 18.60 1.60 -9 -1 6 18.70 1.70 9 -1 -6 15.70 1.90 -9 1 6 14.10 1.90 9 1 -6 18.70 1.90 -9 -2 -3 17.50 1.50 9 -2 3 19.90 1.70 9 -2 3 18.90 1.60 -9 2 -3 17.20 1.60 9 2 3 19.20 1.60 9 2 3 15.90 1.50 9 2 3 18.80 1.70 9 -2 1 26.90 2.20 -9 -2 -1 24.30 2.10 9 2 1 26.10 2.00 9 2 1 25.30 2.10 9 2 1 27.20 2.30 -9 -2 1 3.70 0.80 9 -2 -1 5.70 0.90 -9 -2 1 4.20 1.00 9 -2 -1 5.10 1.10 -9 2 1 4.00 1.00 9 2 -1 5.50 0.80 9 2 -1 4.60 0.90 9 -2 -3 2.50 0.80 -9 -2 3 2.90 0.80 9 -2 -3 1.60 0.70 9 -2 -3 2.70 1.40 -9 -2 3 1.40 0.70 9 2 -3 0.30 1.10 9 2 -3 2.50 0.80 9 2 -3 1.10 0.50 -9 2 3 0.40 0.90 9 -2 -5 37.70 2.70 -9 -2 5 33.00 2.70 -9 -2 5 33.80 2.90 9 -2 -5 33.60 2.70 9 -2 -5 37.00 2.90 9 2 -5 32.20 2.60 9 2 -5 32.00 2.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 62020 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.250000 0.60165(18) 0.500000 0.0420(4) Uani 1 2 d S T P . . C1 C 0.31179(14) 0.49079(17) 0.42545(8) 0.0411(4) Uani 1 1 d . . . . . C2 C 0.31660(13) 0.26440(18) 0.42355(7) 0.0409(4) Uani 1 1 d . . . . . N2 N 0.45756(15) 0.05821(18) 0.28375(8) 0.0577(4) Uani 1 1 d . . . . . C3 C 0.250000 0.1475(2) 0.500000 0.0413(5) Uani 1 2 d S T P . . C4 C 0.39336(16) 0.15102(18) 0.34455(8) 0.0455(4) Uani 1 1 d . . . . . H1 H 0.3551(17) 0.566(3) 0.3734(10) 0.049(4) Uiso 1 1 d . . . . . H3 H 0.250000 -0.014(3) 0.500000 0.041(4) Uiso 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0529(7) 0.0270(7) 0.0469(7) 0.000 0.0089(5) 0.000 C1 0.0514(6) 0.0293(6) 0.0437(6) 0.0019(4) 0.0094(4) -0.0013(4) C2 0.0497(6) 0.0308(7) 0.0426(6) -0.0014(3) 0.0069(4) 0.0012(4) N2 0.0762(8) 0.0442(7) 0.0555(7) -0.0047(4) 0.0199(5) 0.0083(5) C3 0.0528(8) 0.0259(7) 0.0453(8) 0.000 0.0055(6) 0.000 C4 0.0594(7) 0.0321(6) 0.0463(7) 0.0003(4) 0.0108(5) 0.0022(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0140 0.0070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0250 0.0140 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 N1 C1 118.24(12) 2_556 . N1 C1 C2 122.55(10) . . N1 C1 H1 118.9(9) . . C2 C1 H1 118.5(9) . . C1 C2 C4 120.86(9) . . C3 C2 C1 119.64(10) . . C3 C2 C4 119.49(11) . . C2 C3 C2 117.33(14) 2_556 . C2 C3 H3 121.34(7) 2_556 . C2 C3 H3 121.34(7) . . N2 C4 C2 178.11(12) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 N1 C1 1.3358(12) 2_556 N1 C1 1.3358(12) . C1 C2 1.4009(16) . C1 H1 0.927(15) . C2 C3 1.3905(13) . C2 C4 1.4404(15) . N2 C4 1.1439(16) . C3 H3 1.00(2) . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C1 H1 N2 0.927(15) 2.651(13) 3.4711(15) 147.8(12) 4 _cod_database_fobs_code 3500071