#------------------------------------------------------------------------------ #$Date: 2016-02-16 20:30:59 +0000 (Tue, 16 Feb 2016) $ #$Revision: 176467 $ #$URL: svn://www.crystallography.net/cod/cif/4/00/07/4000752.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4000752 loop_ _publ_author_name 'Guiot, V.' 'Janod, E.' 'Corraze, B.' 'Cario, L.' _publ_section_title ; Control of the Electronic Properties and Resistive Switching in the New Series of Mott Insulators GaTa4Se8--yTey(0 ≤y≤ 6.5) ; _journal_issue 10 _journal_name_full 'Chemistry of Materials' _journal_page_first 2611 _journal_paper_doi 10.1021/cm200266n _journal_volume 23 _journal_year 2011 _chemical_formula_sum 'Ga Se2 Ta4 Te6' _chemical_formula_weight 1717 _chemical_name_systematic ' ?' _space_group_IT_number 216 _symmetry_cell_setting cubic _symmetry_space_group_name_Hall 'F -4 2 3' _symmetry_space_group_name_H-M 'F -4 3 m' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.9955(13) _cell_length_b 10.9955(13) _cell_length_c 10.9955(13) _cell_measurement_reflns_used 5563 _cell_measurement_temperature 295 _cell_measurement_theta_max 34.81 _cell_measurement_theta_min 6.43 _cell_volume 1329.4(3) _computing_publication_material 'Jana2006 (Petricek, Dusek & Palatinus, 2006)' _computing_structure_refinement 'Jana2006 (Petricek, Dusek & Palatinus, 2006)' _diffrn_ambient_temperature 295 _diffrn_measured_fraction_theta_full 0.98 _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Nonius CCD' _diffrn_measurement_method ;'462 images collected with a CCD camera' 'and 1° rotation and 45s exposure per frame' ; _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71069 _diffrn_reflns_av_R_equivalents 0.0752 _diffrn_reflns_av_sigmaI/netI 0.0147 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 5563 _diffrn_reflns_theta_full 34.81 _diffrn_reflns_theta_max 34.81 _diffrn_reflns_theta_min 6.43 _exptl_absorpt_coefficient_mu 53.132 _exptl_absorpt_correction_T_max 0.5203 _exptl_absorpt_correction_T_min 0.2176 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details 'Jana2006 (Petricek, Dusek & Palatinus, 2000)' _exptl_crystal_colour 'metallic grey' _exptl_crystal_density_diffrn 8.5763(18) _exptl_crystal_description 'small slab from bigger single crystal' _exptl_crystal_F_000 2812 _exptl_crystal_size_max 0.040 _exptl_crystal_size_mid 0.027 _exptl_crystal_size_min 0.020 _refine_diff_density_max 2.40 _refine_diff_density_min -1.77 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_gt 1.16 _refine_ls_goodness_of_fit_ref 1.15 _refine_ls_number_constraints 3 _refine_ls_number_parameters 12 _refine_ls_number_reflns 331 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0479 _refine_ls_R_factor_gt 0.0475 _refine_ls_shift/su_max 0.0043 _refine_ls_shift/su_mean 0.0010 _refine_ls_structure_factor_coef F _refine_ls_weighting_scheme sigma _refine_ls_wR_factor_gt 0.0519 _refine_ls_wR_factor_ref 0.0521 _reflns_number_gt 329 _reflns_number_total 331 _reflns_threshold_expression I>2\s(I) _cod_data_source_file cm200266n_si_003.cif _cod_data_source_block (I) _cod_original_cell_volume 1329.4(5) _cod_original_formula_sum 'Ga1 Se2 Ta4 Te6' _cod_database_code 4000752 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,-y,z 3 -x,y,-z 4 x,-y,-z 5 z,x,y 6 z,-x,-y 7 -z,-x,y 8 -z,x,-y 9 y,z,x 10 -y,z,-x 11 y,-z,-x 12 -y,-z,x 13 y,x,z 14 -y,-x,z 15 y,-x,-z 16 -y,x,-z 17 x,z,y 18 -x,z,-y 19 -x,-z,y 20 x,-z,-y 21 z,y,x 22 z,-y,-x 23 -z,y,-x 24 -z,-y,x 25 x,y+1/2,z+1/2 26 -x,-y+1/2,z+1/2 27 -x,y+1/2,-z+1/2 28 x,-y+1/2,-z+1/2 29 z,x+1/2,y+1/2 30 z,-x+1/2,-y+1/2 31 -z,-x+1/2,y+1/2 32 -z,x+1/2,-y+1/2 33 y,z+1/2,x+1/2 34 -y,z+1/2,-x+1/2 35 y,-z+1/2,-x+1/2 36 -y,-z+1/2,x+1/2 37 y,x+1/2,z+1/2 38 -y,-x+1/2,z+1/2 39 y,-x+1/2,-z+1/2 40 -y,x+1/2,-z+1/2 41 x,z+1/2,y+1/2 42 -x,z+1/2,-y+1/2 43 -x,-z+1/2,y+1/2 44 x,-z+1/2,-y+1/2 45 z,y+1/2,x+1/2 46 z,-y+1/2,-x+1/2 47 -z,y+1/2,-x+1/2 48 -z,-y+1/2,x+1/2 49 x+1/2,y,z+1/2 50 -x+1/2,-y,z+1/2 51 -x+1/2,y,-z+1/2 52 x+1/2,-y,-z+1/2 53 z+1/2,x,y+1/2 54 z+1/2,-x,-y+1/2 55 -z+1/2,-x,y+1/2 56 -z+1/2,x,-y+1/2 57 y+1/2,z,x+1/2 58 -y+1/2,z,-x+1/2 59 y+1/2,-z,-x+1/2 60 -y+1/2,-z,x+1/2 61 y+1/2,x,z+1/2 62 -y+1/2,-x,z+1/2 63 y+1/2,-x,-z+1/2 64 -y+1/2,x,-z+1/2 65 x+1/2,z,y+1/2 66 -x+1/2,z,-y+1/2 67 -x+1/2,-z,y+1/2 68 x+1/2,-z,-y+1/2 69 z+1/2,y,x+1/2 70 z+1/2,-y,-x+1/2 71 -z+1/2,y,-x+1/2 72 -z+1/2,-y,x+1/2 73 x+1/2,y+1/2,z 74 -x+1/2,-y+1/2,z 75 -x+1/2,y+1/2,-z 76 x+1/2,-y+1/2,-z 77 z+1/2,x+1/2,y 78 z+1/2,-x+1/2,-y 79 -z+1/2,-x+1/2,y 80 -z+1/2,x+1/2,-y 81 y+1/2,z+1/2,x 82 -y+1/2,z+1/2,-x 83 y+1/2,-z+1/2,-x 84 -y+1/2,-z+1/2,x 85 y+1/2,x+1/2,z 86 -y+1/2,-x+1/2,z 87 y+1/2,-x+1/2,-z 88 -y+1/2,x+1/2,-z 89 x+1/2,z+1/2,y 90 -x+1/2,z+1/2,-y 91 -x+1/2,-z+1/2,y 92 x+1/2,-z+1/2,-y 93 z+1/2,y+1/2,x 94 z+1/2,-y+1/2,-x 95 -z+1/2,y+1/2,-x 96 -z+1/2,-y+1/2,x loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag Ta1 Ta 0.59876(8) 0.59876(8) 0.59876(8) Uani 0.00921(16) 16 1 d Te1 Te 0.86363(19) 0.86363(19) 0.86363(19) Uani 0.0085(2) 16 1 d Se1 Se 0.3632(3) 0.3632(3) 0.3632(3) Uani 0.0121(5) 16 0.50(5) d Te2 Te 0.3632(3) 0.3632(3) 0.3632(3) Uani 0.0121(5) 16 0.50(5) d Ga1 Ga 0 0 0 Uani 0.0091(8) 4 1 d loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ta1 Ta 0.0092(3) 0.0092(3) 0.0092(3) 0.0000(3) 0.0000(3) 0.0000(3) Te1 Te 0.0085(4) 0.0085(4) 0.0085(4) -0.0005(5) -0.0005(5) -0.0005(5) Se1 Se 0.0121(8) 0.0121(8) 0.0121(8) 0.0023(7) 0.0023(7) 0.0023(7) Te2 Te 0.0121(8) 0.0121(8) 0.0121(8) 0.0023(7) 0.0023(7) 0.0023(7) Ga1 Ga 0.0091(14) 0.0091(14) 0.0091(14) 0 0 0 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ga 0.231 1.608 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ta -0.705 6.523 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Se -0.093 2.226 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Te -0.531 1.675 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle Ta1 Te1 Se1 88.948(55) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Ta1 Te1 74_665 2.971(2) yes Ta1 Te1 51_656 2.971(2) yes Ta1 Te1 28_566 2.971(2) yes Ta1 Se1 2_665 2.656(3) yes Ta1 Se1 3_656 2.656(3) yes Ta1 Se1 4_566 2.656(3) yes Ta1 Te2 2_665 2.656(3) yes Ta1 Te2 3_656 2.656(3) yes Ta1 Te2 4_566 2.656(3) yes Te1 Ga1 1_666 2.597(2) yes Se1 Te2 . 0 yes loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status -2 2 2 156.22 134.68 1.05 o 2 2 2 140.93 149.17 0.87 o -3 3 3 297.68 292.98 1.86 o -1 3 3 192.47 201.49 1.21 o 1 3 3 199.17 193.50 1.13 o 3 3 3 292.72 296.90 2.31 o 0 0 4 618.76 662.96 4.98 o -2 2 4 298.48 296.16 2.05 o 0 2 4 12.51 7.08 0.83 o 2 2 4 296.76 298.23 1.85 o -4 4 4 422.83 424.60 3.95 o -2 4 4 90.98 91.58 0.64 o 0 4 4 575.44 580.46 4.05 o 2 4 4 91.83 90.65 0.78 o 4 4 4 427.25 419.14 3.60 o -1 1 5 244.79 246.58 1.57 o 1 1 5 248.69 240.66 1.58 o -3 3 5 41.01 42.17 0.51 o -1 3 5 37.01 29.39 0.45 o 1 3 5 31.51 35.18 0.35 o 3 3 5 44.18 39.02 0.61 o -5 5 5 277.51 280.99 1.97 o -3 5 5 105.98 99.39 0.77 o -1 5 5 202.57 205.14 1.17 o 1 5 5 206.59 197.85 1.53 o 3 5 5 100.57 104.35 1.00 o 5 5 5 284.86 273.15 1.89 o 0 0 6 74.24 73.03 0.89 o -2 2 6 169.97 166.14 1.24 o 0 2 6 75.94 74.43 0.47 o 2 2 6 169.25 167.56 1.06 o -4 4 6 22.50 40.92 1.07 o -2 4 6 205.18 200.66 1.20 o 0 4 6 82.12 81.41 0.53 o 2 4 6 202.59 202.12 1.23 o 4 4 6 43.68 21.86 0.87 o -6 6 6 186.18 164.24 2.30 o -4 6 6 196.25 187.40 1.31 o -2 6 6 191.25 175.37 1.34 o 0 6 6 260.07 258.51 1.74 o 2 6 6 176.25 187.86 1.64 o 4 6 6 189.81 192.47 1.28 o 6 6 6 166.23 183.12 1.92 o -1 1 7 151.30 146.69 1.01 o 1 1 7 146.24 149.99 1.19 o -3 3 7 239.30 227.47 1.36 o -1 3 7 146.11 147.98 0.91 o 1 3 7 149.56 144.73 0.92 o 3 3 7 231.19 236.86 1.50 o -5 5 7 107.56 109.64 0.87 o -3 5 7 63.23 60.93 0.56 o -1 5 7 58.33 60.96 0.54 o 1 5 7 61.42 58.48 0.53 o 3 5 7 61.28 62.85 0.58 o 5 5 7 110.36 107.02 0.73 o -7 7 7 163.76 152.76 1.75 o -5 7 7 31.17 32.79 1.10 o -3 7 7 186.84 178.27 1.25 o -1 7 7 112.41 119.18 1.06 o 1 7 7 119.28 110.66 1.13 o 3 7 7 180.75 184.28 1.57 o 5 7 7 32.28 32.96 1.32 o 7 7 7 155.09 163.01 1.10 o 0 0 8 361.14 352.52 3.08 o -2 2 8 384.08 383.64 2.35 o 0 2 8 11.92 10.47 0.93 o 2 2 8 385.92 382.66 2.79 o -4 4 8 277.77 282.69 1.56 o -2 4 8 94.87 103.74 0.73 o 0 4 8 258.51 253.99 1.75 o 2 4 8 105.00 94.78 0.77 o 4 4 8 287.44 273.06 1.83 o -6 6 8 179.14 175.85 1.15 o -4 6 8 37.09 48.44 0.81 o -2 6 8 241.44 235.17 1.42 o 0 6 8 64.13 64.22 0.64 o 2 6 8 237.16 235.85 1.62 o 4 6 8 48.50 36.61 0.60 o 6 6 8 178.28 177.31 1.32 o -8 8 8 211.40 222.13 2.22 o -6 8 8 63.61 79.99 1.02 o -4 8 8 182.54 194.26 1.42 o -2 8 8 110.67 108.79 0.98 o 0 8 8 194.90 191.37 1.40 o 2 8 8 111.35 106.98 1.16 o 4 8 8 195.20 181.18 1.61 o 6 8 8 81.23 66.06 1.05 o 8 8 8 224.83 208.21 3.58 o -1 1 9 103.16 106.35 0.99 o 1 1 9 108.00 101.55 1.28 o -3 3 9 128.96 123.19 0.93 o -1 3 9 96.49 90.49 0.81 o 1 3 9 92.63 94.28 0.74 o 3 3 9 122.66 127.33 0.97 o -5 5 9 136.19 142.42 1.07 o -3 5 9 37.82 31.39 0.67 o -1 5 9 159.60 163.23 1.14 o 1 5 9 165.05 156.39 1.32 o 3 5 9 31.31 37.00 0.67 o 5 5 9 143.30 133.83 1.05 o -7 7 9 96.45 92.45 1.00 o -5 7 9 35.87 38.49 1.00 o -3 7 9 109.34 106.99 0.76 o -1 7 9 89.77 93.06 0.72 o 1 7 9 93.78 89.16 0.73 o 3 7 9 106.88 107.08 0.79 o 5 7 9 38.51 35.15 0.90 o 7 7 9 91.22 95.92 0.96 o -9 9 9 49.44 57.41 3.29 o -7 9 9 77.32 79.30 0.85 o -5 9 9 110.98 118.50 1.01 o -3 9 9 97.80 95.98 1.24 o -1 9 9 93.52 99.10 1.00 o 1 9 9 101.33 92.61 0.80 o 3 9 9 97.92 96.96 1.77 o 5 9 9 118.17 109.93 1.77 o 7 9 9 81.00 78.32 1.30 o 9 9 9 53.75 48.09 1.25 o 0 0 10 77.21 76.13 1.45 o -2 2 10 208.20 199.93 1.32 o 0 2 10 119.72 117.62 0.79 o 2 2 10 204.99 204.02 1.37 o -4 4 10 31.22 10.45 0.76 o -2 4 10 72.66 65.69 0.81 o 0 4 10 18.47 13.87 1.23 o 2 4 10 65.44 71.21 0.90 o 4 4 10 15.13 30.29 1.96 o -6 6 10 174.36 156.96 1.19 o -4 6 10 202.71 194.96 1.17 o -2 6 10 162.94 152.75 1.16 o 0 6 10 212.13 208.61 1.34 o 2 6 10 154.89 159.91 1.07 o 4 6 10 197.14 199.62 1.20 o 6 6 10 157.11 172.96 1.15 o -8 8 10 67.60 65.98 1.55 o -6 8 10 83.47 79.36 1.13 o -4 8 10 85.28 82.69 0.91 o -2 8 10 82.31 76.29 0.81 o 0 8 10 49.23 48.62 0.78 o 2 8 10 77.06 80.56 0.81 o 4 8 10 82.73 85.63 0.87 o 6 8 10 79.24 83.71 0.91 o 8 8 10 66.18 69.43 0.94 o -10 10 10 103.77 93.81 1.43 o -8 10 10 102.08 101.15 1.45 o -6 10 10 115.57 100.01 1.80 o -4 10 10 179.07 174.08 1.45 o -2 10 10 112.65 103.41 1.23 o 0 10 10 250.25 246.22 1.79 o 2 10 10 103.38 112.58 1.21 o 4 10 10 176.19 177.18 1.56 o 6 10 10 98.93 115.82 1.64 o 8 10 10 101.98 104.31 1.84 o 10 10 10 91.18 107.77 3.85 o -1 1 11 118.65 116.94 1.13 o 1 1 11 120.43 117.48 1.01 o -3 3 11 94.67 88.29 0.90 o -1 3 11 92.12 95.88 0.72 o 1 3 11 96.80 91.13 0.91 o 3 3 11 90.27 93.85 0.91 o -5 5 11 136.24 136.63 1.06 o -3 5 11 41.26 39.70 0.80 o -1 5 11 156.78 156.01 1.10 o 1 5 11 158.82 155.52 1.11 o 3 5 11 38.20 39.89 0.84 o 5 5 11 138.97 135.87 1.20 o -7 7 11 75.47 65.31 1.41 o -5 7 11 23.19 23.46 1.34 o -3 7 11 82.27 72.22 0.67 o -1 7 11 58.94 62.03 1.09 o 1 7 11 61.82 58.78 0.69 o 3 7 11 72.91 81.76 0.70 o 5 7 11 22.57 25.70 1.51 o 7 7 11 65.41 72.89 1.38 o -9 9 11 50.90 56.06 2.28 o -7 9 11 58.36 57.69 1.19 o -5 9 11 103.80 106.10 1.12 o -3 9 11 68.97 66.03 0.74 o -1 9 11 77.53 77.43 0.84 o 1 9 11 77.34 77.17 0.93 o 3 9 11 64.81 68.04 0.94 o 5 9 11 106.79 105.58 1.19 o 7 9 11 55.87 58.56 0.99 o 9 9 11 53.74 54.87 2.00 o -7 11 11 70.29 67.69 1.72 o -5 11 11 89.15 92.07 1.56 o -3 11 11 39.16 32.08 1.91 o -1 11 11 54.46 56.04 1.49 o 1 11 11 54.37 54.78 1.34 o 3 11 11 28.72 38.12 2.81 o 5 11 11 89.19 93.46 1.53 o 7 11 11 67.04 72.21 1.42 o 0 0 12 50.86 45.73 5.87 o -2 2 12 312.07 306.35 2.36 o 0 2 12 59.66 59.39 0.64 o 2 2 12 312.63 305.73 2.35 o -4 4 12 84.02 96.75 1.43 o -2 4 12 52.21 56.03 0.68 o 0 4 12 85.06 83.95 0.93 o 2 4 12 54.73 52.09 0.75 o 4 4 12 95.41 83.49 1.45 o -6 6 12 143.02 150.17 1.26 o -4 6 12 95.71 103.58 1.02 o -2 6 12 204.47 203.84 1.46 o 0 6 12 89.79 88.90 0.77 o 2 6 12 206.85 201.52 1.33 o 4 6 12 104.15 95.89 0.73 o 6 6 12 150.22 143.33 1.90 o -8 8 12 142.77 154.08 1.76 o -6 8 12 25.70 40.11 1.69 o -4 8 12 125.84 135.76 1.26 o -2 8 12 57.98 69.00 0.85 o 0 8 12 60.85 63.87 1.04 o 2 8 12 68.77 59.60 1.09 o 4 8 12 134.78 124.97 1.13 o 6 8 12 41.22 27.69 1.09 o 8 8 12 150.36 144.86 2.05 o -8 10 12 75.83 78.23 1.16 o -6 10 12 56.53 67.24 0.94 o -4 10 12 87.20 90.88 1.31 o -2 10 12 71.39 77.55 1.05 o 0 10 12 127.81 126.42 1.40 o 2 10 12 76.91 72.59 1.15 o 4 10 12 91.25 89.76 1.19 o 6 10 12 63.29 59.63 0.93 o 8 10 12 74.24 77.61 2.20 o -4 12 12 93.59 101.34 1.94 o -2 12 12 28.29 19.07 2.65 o 0 12 12 82.43 84.79 1.39 o 2 12 12 16.47 24.49 6.22 < 4 12 12 96.04 95.57 1.88 o -1 1 13 57.09 60.80 0.86 o 1 1 13 60.28 55.07 1.21 o -3 3 13 139.58 140.68 0.93 o -1 3 13 78.27 80.75 0.94 o 1 3 13 80.48 79.49 1.16 o 3 3 13 142.83 138.56 1.24 o -5 5 13 46.44 54.76 1.92 o -3 5 13 35.10 31.11 1.13 o -1 5 13 29.15 30.34 1.18 o 1 5 13 31.08 25.56 1.57 o 3 5 13 30.27 33.89 1.53 o 5 5 13 54.92 47.92 1.18 o -7 7 13 106.79 109.62 1.45 o -5 7 13 20.93 23.08 2.00 o -3 7 13 124.55 122.71 1.09 o -1 7 13 70.26 71.05 1.16 o 1 7 13 70.78 73.09 0.87 o 3 7 13 122.52 123.65 0.96 o 5 7 13 24.04 20.91 2.32 o 7 7 13 106.60 107.92 1.48 o -7 9 13 74.57 76.27 1.11 o -5 9 13 17.89 25.78 2.95 o -3 9 13 92.28 91.86 1.23 o -1 9 13 74.42 76.12 1.15 o 1 9 13 75.77 74.61 0.97 o 3 9 13 92.65 91.87 0.91 o 5 9 13 28.19 20.48 1.63 o 7 9 13 76.86 74.40 1.46 o -3 11 13 52.89 58.00 1.98 o -1 11 13 36.57 42.60 1.63 o 1 11 13 41.49 42.46 1.26 o 3 11 13 53.79 56.22 2.04 o 0 0 14 43.38 46.34 3.05 o -2 2 14 182.94 179.93 1.97 o 0 2 14 45.17 45.59 0.88 o 2 2 14 180.27 181.46 2.22 o -4 4 14 86.64 73.83 1.58 o -2 4 14 71.82 66.47 0.91 o 0 4 14 33.56 34.94 1.17 o 2 4 14 66.23 72.84 1.19 o 4 4 14 74.14 85.93 1.23 o -6 6 14 95.64 88.17 1.39 o -4 6 14 108.06 103.51 0.97 o -2 6 14 126.74 123.84 1.19 o 0 6 14 156.50 155.40 1.31 o 2 6 14 123.72 127.84 1.03 o 4 6 14 103.13 108.40 0.92 o 6 6 14 86.56 97.85 1.83 o -6 8 14 65.84 61.83 1.20 o -4 8 14 89.92 80.77 0.96 o -2 8 14 46.09 40.97 1.85 o 0 8 14 84.92 86.60 1.04 o 2 8 14 37.72 44.87 1.49 o 4 8 14 79.33 91.67 0.78 o 6 8 14 59.13 70.22 1.53 o -4 10 14 138.96 140.32 1.50 o -2 10 14 50.32 43.72 1.20 o 0 10 14 146.48 148.74 1.58 o 2 10 14 37.26 48.70 1.36 o 4 10 14 140.60 141.47 1.96 o -1 1 15 118.31 116.96 1.56 o 1 1 15 117.10 117.89 1.55 o -3 3 15 44.10 46.02 0.75 o -1 3 15 38.60 37.00 1.29 o 1 3 15 35.57 37.25 1.91 o 3 3 15 47.87 43.67 1.20 o -5 5 15 134.60 134.95 1.49 o -3 5 15 57.17 57.05 1.47 o -1 5 15 103.07 101.80 1.38 o 1 5 15 103.36 103.21 1.04 o 3 5 15 56.09 55.84 1.27 o 5 5 15 134.30 136.48 1.83 o -5 7 15 39.75 40.68 1.31 o -3 7 15 11.59 20.31 5.67 < -1 7 15 17.77 13.51 3.11 o 1 7 15 17.71 20.00 3.11 o 3 7 15 19.44 13.24 3.67 o 5 7 15 39.33 42.54 1.74 o -1 9 15 77.15 79.34 1.17 o 1 9 15 76.52 81.10 1.44 o 0 0 16 49.18 47.43 0.98 o -2 2 16 182.74 180.62 2.10 o 0 2 16 32.66 33.21 2.03 o 2 2 16 181.75 179.29 1.46 o -4 4 16 25.91 38.45 2.65 o -2 4 16 40.72 48.23 1.19 o 0 4 16 44.26 44.64 1.36 o 2 4 16 46.26 40.88 1.51 o 4 4 16 36.18 26.78 1.88 o -4 6 16 67.37 77.64 1.19 o -2 6 16 130.86 139.91 1.35 o 0 6 16 112.55 115.27 1.49 o 2 6 16 135.95 134.58 1.61 o 4 6 16 75.27 71.72 1.79 o -1 1 17 44.82 42.89 1.92 o 1 1 17 42.29 47.20 1.89 o -3 3 17 81.67 88.62 1.86 o -1 3 17 46.28 47.29 1.85 o 1 3 17 45.60 50.53 2.02 o 3 3 17 84.85 87.52 2.13 o