#------------------------------------------------------------------------------ #$Date: 2013-07-14 09:54:14 +0100 (Sun, 14 Jul 2013) $ #$Revision: 87151 $ #$URL: svn://www.crystallography.net/cod/cif/4/00/17/4001774.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4001774 loop_ _publ_author_name 'Zeilinger, Michael' 'Benson, Daryn' 'H\"aussermann, Ulrich' 'F\"assler, Thomas F.' _publ_section_title ; Single Crystal Growth and Thermodynamic Stability of Li17Si4 ; _journal_issue 9 _journal_name_full 'Chemistry of Materials' _journal_page_first 1960 _journal_paper_doi 10.1021/cm400612k _journal_volume 25 _journal_year 2013 _chemical_formula_analytical 'Li17 Si4' _chemical_formula_moiety 'Li17 Si4' _chemical_formula_sum 'Li17 Si4' _chemical_formula_weight 230.34 _chemical_melting_point '754 K, peritectical decomposition' _chemical_name_common 'Lithium Silicide' _chemical_name_systematic ; ? ; _space_group_IT_number 216 _symmetry_cell_setting cubic _symmetry_Int_Tables_number 216 _symmetry_space_group_name_Hall 'F -4 2 3' _symmetry_space_group_name_H-M 'F -4 3 m' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 20 _cell_length_a 18.6563(2) _cell_length_b 18.6563(2) _cell_length_c 18.6563(2) _cell_measurement_reflns_used 9997 _cell_measurement_temperature 123(2) _cell_measurement_theta_max 47.3501 _cell_measurement_theta_min 3.0883 _cell_volume 6493.47(12) _citation_year 2013 _computing_cell_refinement 'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. ' _computing_data_collection ;APEX suite of crystallographic software. APEX 2 Version 2008.4, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. ; _computing_data_reduction 'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. ' _computing_molecular_graphics 'Diamond 3 (Crystal Impact 2011)' _computing_publication_material 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 123(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method 'phi- and omega-rotation' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0356 _diffrn_reflns_av_sigmaI/netI 0.0209 _diffrn_reflns_limit_h_max 37 _diffrn_reflns_limit_h_min -38 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -38 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_number 32178 _diffrn_reflns_theta_full 47.62 _diffrn_reflns_theta_max 47.62 _diffrn_reflns_theta_min 1.89 _exptl_absorpt_coefficient_mu 0.394 _exptl_absorpt_correction_T_max 0.7494 _exptl_absorpt_correction_T_min 0.5967 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS, Bruker, 2008b' _exptl_crystal_colour 'metallic silver' _exptl_crystal_density_diffrn 1.178 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2140 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.3 _refine_diff_density_max 0.199 _refine_diff_density_min -0.405 _refine_diff_density_rms 0.048 _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.49(7) _refine_ls_extinction_coef 'not refined' _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_matrix_type full _refine_ls_number_parameters 67 _refine_ls_number_reflns 2971 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.061 _refine_ls_R_factor_all 0.0284 _refine_ls_R_factor_gt 0.0207 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0130P)^2^+0.3128P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0352 _refine_ls_wR_factor_ref 0.0369 _reflns_number_gt 2620 _reflns_number_total 2971 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file cm400612k_si_002.cif _[local]_cod_data_source_block Li17Si4_123K _cod_original_cell_volume 6493.5(1) _cod_database_code 4001774 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, z+1/2' '-y, -x+1/2, z+1/2' 'y, -x+1/2, -z+1/2' '-y, x+1/2, -z+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'z, y+1/2, x+1/2' 'z, -y+1/2, -x+1/2' '-z, y+1/2, -x+1/2' '-z, -y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, z+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, -x, -z+1/2' '-y+1/2, x, -z+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'z+1/2, y, x+1/2' 'z+1/2, -y, -x+1/2' '-z+1/2, y, -x+1/2' '-z+1/2, -y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, z' '-y+1/2, -x+1/2, z' 'y+1/2, -x+1/2, -z' '-y+1/2, x+1/2, -z' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'z+1/2, y+1/2, x' 'z+1/2, -y+1/2, -x' '-z+1/2, y+1/2, -x' '-z+1/2, -y+1/2, x' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags Si1 Si 0.159759(8) 0.159759(8) 0.159759(8) 0.00689(4) Uani 1 6 d S Si2 Si 0.916599(8) 0.916599(8) 0.916599(8) 0.00626(4) Uani 1 6 d S Si3 Si 0.321327(11) 0.0000 0.0000 0.00701(4) Uani 1 4 d S Si4 Si 0.570307(10) 0.2500 0.2500 0.00681(4) Uani 1 4 d S Li1 Li 0.07410(6) 0.07410(6) 0.07410(6) 0.0149(3) Uani 1 6 d S Li2 Li 0.30284(5) 0.30284(5) 0.30284(5) 0.0125(3) Uani 1 6 d S Li3 Li 0.41794(7) 0.41794(7) 0.41794(7) 0.0127(3) Uani 1 6 d S Li4 Li 0.55713(5) 0.55713(5) 0.55713(5) 0.0125(3) Uani 1 6 d S Li5 Li 0.68687(5) 0.68687(5) 0.68687(5) 0.0123(3) Uani 1 6 d S Li6 Li 0.83168(6) 0.83168(6) 0.83168(6) 0.0135(4) Uani 1 6 d S Li7 Li 0.16807(8) 0.0000 0.0000 0.0118(3) Uani 1 4 d S Li8 Li 0.07492(9) 0.2500 0.2500 0.0139(3) Uani 1 4 d S Li9 Li 0.09068(4) 0.09068(4) 0.26186(6) 0.0157(2) Uani 1 2 d S Li10 Li 0.09013(5) 0.09013(5) 0.76176(6) 0.0160(2) Uani 1 2 d S Li11 Li 0.15503(4) 0.15503(4) 0.51978(6) 0.01613(19) Uani 1 2 d S Li12 Li 0.16327(4) 0.16327(4) 0.00286(7) 0.0143(3) Uani 1 2 d S Li13 Li 0.0000 0.0000 0.0000 0.0105(6) Uani 1 24 d S loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.00689(4) 0.00689(4) 0.00689(4) 0.00014(4) 0.00014(4) 0.00014(4) Si2 0.00626(4) 0.00626(4) 0.00626(4) -0.00017(4) -0.00017(4) -0.00017(4) Si3 0.00649(7) 0.00727(5) 0.00727(5) -0.00067(7) 0.000 0.000 Si4 0.00671(8) 0.00685(5) 0.00685(5) 0.00035(6) 0.000 0.000 Li1 0.0149(3) 0.0149(3) 0.0149(3) -0.0002(3) -0.0002(3) -0.0002(3) Li2 0.0125(3) 0.0125(3) 0.0125(3) 0.0009(3) 0.0009(3) 0.0009(3) Li3 0.0127(3) 0.0127(3) 0.0127(3) 0.0015(3) 0.0015(3) 0.0015(3) Li4 0.0125(3) 0.0125(3) 0.0125(3) 0.0007(3) 0.0007(3) 0.0007(3) Li5 0.0123(3) 0.0123(3) 0.0123(3) 0.0019(3) 0.0019(3) 0.0019(3) Li6 0.0135(4) 0.0135(4) 0.0135(4) -0.0006(3) -0.0006(3) -0.0006(3) Li7 0.0130(6) 0.0112(4) 0.0112(4) 0.0002(6) 0.000 0.000 Li8 0.0118(6) 0.0150(5) 0.0150(5) -0.0007(6) 0.000 0.000 Li9 0.0159(3) 0.0159(3) 0.0151(5) 0.0032(2) 0.0032(2) -0.0028(4) Li10 0.0167(3) 0.0167(3) 0.0148(5) -0.0002(2) -0.0002(2) -0.0018(4) Li11 0.0157(3) 0.0157(3) 0.0169(5) -0.0012(3) -0.0012(3) -0.0016(4) Li12 0.0139(3) 0.0139(3) 0.0152(5) -0.0005(3) -0.0005(3) -0.0031(3) Li13 0.0105(6) 0.0105(6) 0.0105(6) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Li9 Si1 Li9 117.868(13) 9 5 Li9 Si1 Li9 117.868(14) 9 . Li9 Si1 Li9 117.868(13) 5 . Li9 Si1 Li1 81.53(3) 9 . Li9 Si1 Li1 81.53(3) 5 . Li9 Si1 Li1 81.53(3) . . Li9 Si1 Li2 113.65(3) 9 28 Li9 Si1 Li2 64.03(4) 5 28 Li9 Si1 Li2 113.65(3) . 28 Li1 Si1 Li2 145.56(3) . 28 Li9 Si1 Li2 113.65(3) 9 74 Li9 Si1 Li2 113.65(3) 5 74 Li9 Si1 Li2 64.03(4) . 74 Li1 Si1 Li2 145.56(3) . 74 Li2 Si1 Li2 58.66(5) 28 74 Li9 Si1 Li2 64.03(4) 9 51 Li9 Si1 Li2 113.65(3) 5 51 Li9 Si1 Li2 113.65(3) . 51 Li1 Si1 Li2 145.56(3) . 51 Li2 Si1 Li2 58.66(5) 28 51 Li2 Si1 Li2 58.66(5) 74 51 Li9 Si1 Li8 65.907(17) 9 9 Li9 Si1 Li8 65.907(17) 5 9 Li9 Si1 Li8 167.35(4) . 9 Li1 Si1 Li8 111.12(3) . 9 Li2 Si1 Li8 55.88(2) 28 9 Li2 Si1 Li8 103.32(4) 74 9 Li2 Si1 Li8 55.88(2) 51 9 Li9 Si1 Li8 167.35(4) 9 5 Li9 Si1 Li8 65.907(17) 5 5 Li9 Si1 Li8 65.906(17) . 5 Li1 Si1 Li8 111.12(3) . 5 Li2 Si1 Li8 55.88(2) 28 5 Li2 Si1 Li8 55.88(2) 74 5 Li2 Si1 Li8 103.32(4) 51 5 Li8 Si1 Li8 107.77(3) 9 5 Li9 Si1 Li8 65.907(17) 9 . Li9 Si1 Li8 167.35(4) 5 . Li9 Si1 Li8 65.906(17) . . Li1 Si1 Li8 111.12(3) . . Li2 Si1 Li8 103.32(4) 28 . Li2 Si1 Li8 55.88(2) 74 . Li2 Si1 Li8 55.88(2) 51 . Li8 Si1 Li8 107.77(3) 9 . Li8 Si1 Li8 107.77(3) 5 . Li9 Si1 Li12 60.406(15) 9 . Li9 Si1 Li12 60.406(15) 5 . Li9 Si1 Li12 138.08(3) . . Li1 Si1 Li12 56.549(19) . . Li2 Si1 Li12 102.63(3) 28 . Li2 Si1 Li12 157.90(4) 74 . Li2 Si1 Li12 102.63(3) 51 . Li8 Si1 Li12 54.57(3) 9 . Li8 Si1 Li12 126.001(12) 5 . Li8 Si1 Li12 126.000(12) . . Li9 Si1 Li12 138.08(3) 9 9 Li9 Si1 Li12 60.406(15) 5 9 Li9 Si1 Li12 60.407(15) . 9 Li1 Si1 Li12 56.549(19) . 9 Li2 Si1 Li12 102.63(3) 28 9 Li2 Si1 Li12 102.63(3) 74 9 Li2 Si1 Li12 157.90(4) 51 9 Li8 Si1 Li12 126.001(12) 9 9 Li8 Si1 Li12 54.57(3) 5 9 Li8 Si1 Li12 126.000(12) . 9 Li12 Si1 Li12 92.54(3) . 9 Li12 Si2 Li12 111.49(3) 10_666 6_666 Li12 Si2 Li12 111.49(3) 10_666 2_666 Li12 Si2 Li12 111.49(3) 6_666 2_666 Li12 Si2 Li13 107.37(3) 10_666 1_666 Li12 Si2 Li13 107.37(3) 6_666 1_666 Li12 Si2 Li13 107.37(3) 2_666 1_666 Li12 Si2 Li7 69.297(18) 10_666 10_666 Li12 Si2 Li7 69.297(18) 6_666 10_666 Li12 Si2 Li7 178.31(4) 2_666 10_666 Li13 Si2 Li7 70.94(3) 1_666 10_666 Li12 Si2 Li7 69.297(17) 10_666 2_666 Li12 Si2 Li7 178.31(4) 6_666 2_666 Li12 Si2 Li7 69.297(17) 2_666 2_666 Li13 Si2 Li7 70.94(3) 1_666 2_666 Li7 Si2 Li7 109.88(3) 10_666 2_666 Li12 Si2 Li7 178.31(4) 10_666 6_666 Li12 Si2 Li7 69.297(17) 6_666 6_666 Li12 Si2 Li7 69.297(18) 2_666 6_666 Li13 Si2 Li7 70.94(3) 1_666 6_666 Li7 Si2 Li7 109.88(3) 10_666 6_666 Li7 Si2 Li7 109.88(3) 2_666 6_666 Li12 Si2 Li6 72.63(3) 10_666 . Li12 Si2 Li6 72.63(3) 6_666 . Li12 Si2 Li6 72.63(3) 2_666 . Li13 Si2 Li6 180.000(19) 1_666 . Li7 Si2 Li6 109.06(3) 10_666 . Li7 Si2 Li6 109.06(3) 2_666 . Li7 Si2 Li6 109.06(3) 6_666 . Li12 Si2 Li10 56.014(16) 10_666 2_665 Li12 Si2 Li10 56.014(16) 6_666 2_665 Li12 Si2 Li10 123.85(4) 2_666 2_665 Li13 Si2 Li10 128.78(3) 1_666 2_665 Li7 Si2 Li10 57.84(3) 10_666 2_665 Li7 Si2 Li10 124.958(16) 2_666 2_665 Li7 Si2 Li10 124.958(16) 6_666 2_665 Li6 Si2 Li10 51.22(3) . 2_665 Li12 Si2 Li10 56.014(16) 10_666 6_566 Li12 Si2 Li10 123.85(4) 6_666 6_566 Li12 Si2 Li10 56.014(16) 2_666 6_566 Li13 Si2 Li10 128.78(3) 1_666 6_566 Li7 Si2 Li10 124.958(16) 10_666 6_566 Li7 Si2 Li10 57.84(3) 2_666 6_566 Li7 Si2 Li10 124.958(16) 6_666 6_566 Li6 Si2 Li10 51.22(3) . 6_566 Li10 Si2 Li10 84.93(4) 2_665 6_566 Li12 Si2 Li10 123.85(4) 10_666 10_656 Li12 Si2 Li10 56.014(16) 6_666 10_656 Li12 Si2 Li10 56.014(16) 2_666 10_656 Li13 Si2 Li10 128.78(3) 1_666 10_656 Li7 Si2 Li10 124.958(16) 10_666 10_656 Li7 Si2 Li10 124.958(16) 2_666 10_656 Li7 Si2 Li10 57.84(3) 6_666 10_656 Li6 Si2 Li10 51.22(3) . 10_656 Li10 Si2 Li10 84.93(4) 2_665 10_656 Li10 Si2 Li10 84.93(4) 6_566 10_656 Li12 Si2 Li1 123.876(17) 10_666 4_666 Li12 Si2 Li1 57.41(5) 6_666 4_666 Li12 Si2 Li1 123.876(17) 2_666 4_666 Li13 Si2 Li1 49.96(4) 1_666 4_666 Li7 Si2 Li1 55.115(16) 10_666 4_666 Li7 Si2 Li1 120.90(5) 2_666 4_666 Li7 Si2 Li1 55.115(16) 6_666 4_666 Li6 Si2 Li1 130.04(4) . 4_666 Li10 Si2 Li1 96.00(2) 2_665 4_666 Li10 Si2 Li1 178.74(5) 6_566 4_666 Li10 Si2 Li1 96.00(2) 10_656 4_666 Li9 Si3 Li9 130.24(5) 6 5 Li9 Si3 Li4 110.51(2) 6 27_645 Li9 Si3 Li4 110.51(2) 5 27_645 Li9 Si3 Li4 110.51(2) 6 26_654 Li9 Si3 Li4 110.51(2) 5 26_654 Li4 Si3 Li4 67.23(7) 27_645 26_654 Li9 Si3 Li3 165.10(6) 6 28 Li9 Si3 Li3 64.66(4) 5 28 Li4 Si3 Li3 57.80(4) 27_645 28 Li4 Si3 Li3 57.80(4) 26_654 28 Li9 Si3 Li3 64.66(4) 6 25_544 Li9 Si3 Li3 165.10(6) 5 25_544 Li4 Si3 Li3 57.80(4) 27_645 25_544 Li4 Si3 Li3 57.80(4) 26_654 25_544 Li3 Si3 Li3 100.44(9) 28 25_544 Li9 Si3 Li10 76.718(16) 6 8_655 Li9 Si3 Li10 76.718(16) 5 8_655 Li4 Si3 Li10 89.48(4) 27_645 8_655 Li4 Si3 Li10 156.72(4) 26_654 8_655 Li3 Si3 Li10 110.45(2) 28 8_655 Li3 Si3 Li10 110.45(2) 25_544 8_655 Li9 Si3 Li10 76.718(16) 6 7_655 Li9 Si3 Li10 76.718(16) 5 7_655 Li4 Si3 Li10 156.72(4) 27_645 7_655 Li4 Si3 Li10 89.48(4) 26_654 7_655 Li3 Si3 Li10 110.45(2) 28 7_655 Li3 Si3 Li10 110.45(2) 25_544 7_655 Li10 Si3 Li10 113.80(4) 8_655 7_655 Li9 Si3 Li7 65.12(3) 6 . Li9 Si3 Li7 65.12(3) 5 . Li4 Si3 Li7 146.38(3) 27_645 . Li4 Si3 Li7 146.38(3) 26_654 . Li3 Si3 Li7 129.78(4) 28 . Li3 Si3 Li7 129.78(4) 25_544 . Li10 Si3 Li7 56.90(2) 8_655 . Li10 Si3 Li7 56.90(2) 7_655 . Li9 Si3 Li11 127.721(19) 6 84 Li9 Si3 Li11 60.92(2) 5 84 Li4 Si3 Li11 107.96(3) 27_645 84 Li4 Si3 Li11 56.12(3) 26_654 84 Li3 Si3 Li11 55.90(2) 28 84 Li3 Si3 Li11 111.67(3) 25_544 84 Li10 Si3 Li11 137.46(2) 8_655 84 Li10 Si3 Li11 55.01(2) 7_655 84 Li7 Si3 Li11 98.602(16) . 84 Li9 Si3 Li11 127.721(19) 6 51 Li9 Si3 Li11 60.92(2) 5 51 Li4 Si3 Li11 56.12(3) 27_645 51 Li4 Si3 Li11 107.96(3) 26_654 51 Li3 Si3 Li11 55.90(2) 28 51 Li3 Si3 Li11 111.67(3) 25_544 51 Li10 Si3 Li11 55.01(2) 8_655 51 Li10 Si3 Li11 137.46(2) 7_655 51 Li7 Si3 Li11 98.602(16) . 51 Li11 Si3 Li11 102.89(4) 84 51 Li9 Si3 Li11 60.92(2) 6 50_554 Li9 Si3 Li11 127.721(19) 5 50_554 Li4 Si3 Li11 107.96(3) 27_645 50_554 Li4 Si3 Li11 56.12(3) 26_654 50_554 Li3 Si3 Li11 111.67(3) 28 50_554 Li3 Si3 Li11 55.90(2) 25_544 50_554 Li10 Si3 Li11 137.46(2) 8_655 50_554 Li10 Si3 Li11 55.01(2) 7_655 50_554 Li7 Si3 Li11 98.602(16) . 50_554 Li11 Si3 Li11 74.46(5) 84 50_554 Li11 Si3 Li11 162.80(3) 51 50_554 Li12 Si4 Li12 118.37(6) 56 79 Li12 Si4 Li11 79.608(16) 56 5 Li12 Si4 Li11 79.608(16) 79 5 Li12 Si4 Li11 79.608(16) 56 30 Li12 Si4 Li11 79.608(16) 79 30 Li11 Si4 Li11 138.77(5) 5 30 Li12 Si4 Li8 59.18(3) 56 74 Li12 Si4 Li8 59.18(3) 79 74 Li11 Si4 Li8 69.38(3) 5 74 Li11 Si4 Li8 69.38(3) 30 74 Li12 Si4 Li5 114.00(2) 56 4_566 Li12 Si4 Li5 114.00(2) 79 4_566 Li11 Si4 Li5 148.07(5) 5 4_566 Li11 Si4 Li5 73.16(4) 30 4_566 Li8 Si4 Li5 142.55(4) 74 4_566 Li12 Si4 Li5 114.00(2) 56 25_544 Li12 Si4 Li5 114.00(2) 79 25_544 Li11 Si4 Li5 73.16(4) 5 25_544 Li11 Si4 Li5 148.07(5) 30 25_544 Li8 Si4 Li5 142.55(4) 74 25_544 Li5 Si4 Li5 74.90(7) 4_566 25_544 Li12 Si4 Li6 170.50(5) 56 75_646 Li12 Si4 Li6 71.13(4) 79 75_646 Li11 Si4 Li6 103.17(2) 5 75_646 Li11 Si4 Li6 103.17(2) 30 75_646 Li8 Si4 Li6 130.32(4) 74 75_646 Li5 Si4 Li6 59.09(3) 4_566 75_646 Li5 Si4 Li6 59.09(3) 25_544 75_646 Li12 Si4 Li6 71.13(4) 56 50_664 Li12 Si4 Li6 170.50(5) 79 50_664 Li11 Si4 Li6 103.17(2) 5 50_664 Li11 Si4 Li6 103.17(2) 30 50_664 Li8 Si4 Li6 130.32(4) 74 50_664 Li5 Si4 Li6 59.09(3) 4_566 50_664 Li5 Si4 Li6 59.09(3) 25_544 50_664 Li6 Si4 Li6 99.37(7) 75_646 50_664 Li12 Si4 Li10 135.08(2) 56 76_556 Li12 Si4 Li10 54.38(2) 79 76_556 Li11 Si4 Li10 130.547(19) 5 76_556 Li11 Si4 Li10 55.69(2) 30 76_556 Li8 Si4 Li10 97.048(19) 74 76_556 Li5 Si4 Li10 60.55(3) 4_566 76_556 Li5 Si4 Li10 107.27(3) 25_544 76_556 Li6 Si4 Li10 49.29(3) 75_646 76_556 Li6 Si4 Li10 119.57(3) 50_664 76_556 Li12 Si4 Li10 54.38(2) 56 59_565 Li12 Si4 Li10 135.08(2) 79 59_565 Li11 Si4 Li10 130.547(19) 5 59_565 Li11 Si4 Li10 55.69(2) 30 59_565 Li8 Si4 Li10 97.048(19) 74 59_565 Li5 Si4 Li10 60.55(3) 4_566 59_565 Li5 Si4 Li10 107.27(3) 25_544 59_565 Li6 Si4 Li10 119.57(3) 75_646 59_565 Li6 Si4 Li10 49.29(3) 50_664 59_565 Li10 Si4 Li10 97.42(4) 76_556 59_565 Li12 Si4 Li10 135.08(2) 56 81_545 Li12 Si4 Li10 54.38(2) 79 81_545 Li11 Si4 Li10 55.69(2) 5 81_545 Li11 Si4 Li10 130.547(19) 30 81_545 Li8 Si4 Li10 97.048(19) 74 81_545 Li5 Si4 Li10 107.27(3) 4_566 81_545 Li5 Si4 Li10 60.55(3) 25_544 81_545 Li6 Si4 Li10 49.29(3) 75_646 81_545 Li6 Si4 Li10 119.57(3) 50_664 81_545 Li10 Si4 Li10 80.84(4) 76_556 81_545 Li10 Si4 Li10 165.90(4) 59_565 81_545 Li13 Li1 Li7 77.14(5) . . Li13 Li1 Li7 77.14(5) . 9 Li7 Li1 Li7 115.20(3) . 9 Li13 Li1 Li7 77.14(5) . 5 Li7 Li1 Li7 115.20(3) . 5 Li7 Li1 Li7 115.20(3) 9 5 Li13 Li1 Li12 115.27(5) . . Li7 Li1 Li12 69.767(18) . . Li7 Li1 Li12 167.59(8) 9 . Li7 Li1 Li12 69.767(18) 5 . Li13 Li1 Li12 115.27(5) . 9 Li7 Li1 Li12 69.767(18) . 9 Li7 Li1 Li12 69.766(18) 9 9 Li7 Li1 Li12 167.59(9) 5 9 Li12 Li1 Li12 103.10(6) . 9 Li13 Li1 Li12 115.27(5) . 5 Li7 Li1 Li12 167.59(9) . 5 Li7 Li1 Li12 69.766(18) 9 5 Li7 Li1 Li12 69.766(18) 5 5 Li12 Li1 Li12 103.10(6) . 5 Li12 Li1 Li12 103.10(6) 9 5 Li13 Li1 Si1 180.00(13) . . Li7 Li1 Si1 102.86(5) . . Li7 Li1 Si1 102.86(5) 9 . Li7 Li1 Si1 102.86(5) 5 . Li12 Li1 Si1 64.73(5) . . Li12 Li1 Si1 64.73(5) 9 . Li12 Li1 Si1 64.73(5) 5 . Li13 Li1 Si2 59.51(4) . 2_664 Li7 Li1 Si2 57.79(2) . 2_664 Li7 Li1 Si2 136.65(8) 9 2_664 Li7 Li1 Si2 57.80(2) 5 2_664 Li12 Li1 Si2 55.76(3) . 2_664 Li12 Li1 Si2 127.317(12) 9 2_664 Li12 Li1 Si2 127.317(12) 5 2_664 Si1 Li1 Si2 120.49(3) . 2_664 Li13 Li1 Si2 59.51(4) . 4_466 Li7 Li1 Si2 136.65(8) . 4_466 Li7 Li1 Si2 57.80(2) 9 4_466 Li7 Li1 Si2 57.80(2) 5 4_466 Li12 Li1 Si2 127.317(12) . 4_466 Li12 Li1 Si2 127.317(12) 9 4_466 Li12 Li1 Si2 55.76(3) 5 4_466 Si1 Li1 Si2 120.49(3) . 4_466 Si2 Li1 Si2 96.53(5) 2_664 4_466 Li13 Li1 Si2 59.51(4) . 3_646 Li7 Li1 Si2 57.79(2) . 3_646 Li7 Li1 Si2 57.80(2) 9 3_646 Li7 Li1 Si2 136.65(8) 5 3_646 Li12 Li1 Si2 127.317(12) . 3_646 Li12 Li1 Si2 55.76(3) 9 3_646 Li12 Li1 Si2 127.317(12) 5 3_646 Si1 Li1 Si2 120.49(3) . 3_646 Si2 Li1 Si2 96.53(5) 2_664 3_646 Si2 Li1 Si2 96.53(5) 4_466 3_646 Li13 Li1 Li9 132.38(3) . 5 Li7 Li1 Li9 55.24(3) . 5 Li7 Li1 Li9 120.67(4) 9 5 Li7 Li1 Li9 120.67(4) 5 5 Li12 Li1 Li9 51.56(3) . 5 Li12 Li1 Li9 51.56(3) 9 5 Li12 Li1 Li9 112.35(7) 5 5 Si1 Li1 Li9 47.62(3) . 5 Si2 Li1 Li9 91.363(15) 2_664 5 Si2 Li1 Li9 168.11(7) 4_466 5 Si2 Li1 Li9 91.363(15) 3_646 5 Li8 Li2 Li8 119.559(9) 58 30 Li8 Li2 Li8 119.559(9) 58 74 Li8 Li2 Li8 119.559(9) 30 74 Li8 Li2 Li2 110.03(3) 58 28 Li8 Li2 Li2 110.03(3) 30 28 Li8 Li2 Li2 58.56(4) 74 28 Li8 Li2 Li2 58.56(4) 58 74 Li8 Li2 Li2 110.03(3) 30 74 Li8 Li2 Li2 110.03(3) 74 74 Li2 Li2 Li2 60.0 28 74 Li8 Li2 Li2 110.03(3) 58 51 Li8 Li2 Li2 58.56(4) 30 51 Li8 Li2 Li2 110.03(3) 74 51 Li2 Li2 Li2 60.0 28 51 Li2 Li2 Li2 60.0 74 51 Li8 Li2 Si1 168.85(7) 58 74 Li8 Li2 Si1 62.310(7) 30 74 Li8 Li2 Si1 62.310(7) 74 74 Li2 Li2 Si1 60.67(3) 28 74 Li2 Li2 Si1 110.29(3) 74 74 Li2 Li2 Si1 60.67(3) 51 74 Li8 Li2 Si1 62.310(7) 58 28 Li8 Li2 Si1 62.310(7) 30 28 Li8 Li2 Si1 168.85(7) 74 28 Li2 Li2 Si1 110.29(3) 28 28 Li2 Li2 Si1 60.67(3) 74 28 Li2 Li2 Si1 60.67(3) 51 28 Si1 Li2 Si1 113.57(2) 74 28 Li8 Li2 Si1 62.310(7) 58 51 Li8 Li2 Si1 168.85(7) 30 51 Li8 Li2 Si1 62.310(7) 74 51 Li2 Li2 Si1 60.67(3) 28 51 Li2 Li2 Si1 60.67(3) 74 51 Li2 Li2 Si1 110.29(3) 51 51 Si1 Li2 Si1 113.57(2) 74 51 Si1 Li2 Si1 113.57(2) 28 51 Li8 Li2 Li9 64.701(19) 58 58 Li8 Li2 Li9 136.66(6) 30 58 Li8 Li2 Li9 64.701(19) 74 58 Li2 Li2 Li9 107.27(3) 28 58 Li2 Li2 Li9 107.27(3) 74 58 Li2 Li2 Li9 164.78(3) 51 58 Si1 Li2 Li9 122.48(2) 74 58 Si1 Li2 Li9 122.48(2) 28 58 Si1 Li2 Li9 54.49(2) 51 58 Li8 Li2 Li9 136.66(6) 58 74 Li8 Li2 Li9 64.701(19) 30 74 Li8 Li2 Li9 64.701(19) 74 74 Li2 Li2 Li9 107.27(3) 28 74 Li2 Li2 Li9 164.78(3) 74 74 Li2 Li2 Li9 107.27(3) 51 74 Si1 Li2 Li9 54.49(2) 74 74 Si1 Li2 Li9 122.48(2) 28 74 Si1 Li2 Li9 122.48(2) 51 74 Li9 Li2 Li9 83.84(5) 58 74 Li8 Li2 Li9 64.701(19) 58 30 Li8 Li2 Li9 64.701(19) 30 30 Li8 Li2 Li9 136.66(6) 74 30 Li2 Li2 Li9 164.78(3) 28 30 Li2 Li2 Li9 107.27(3) 74 30 Li2 Li2 Li9 107.27(3) 51 30 Si1 Li2 Li9 122.48(2) 74 30 Si1 Li2 Li9 54.49(2) 28 30 Si1 Li2 Li9 122.48(2) 51 30 Li9 Li2 Li9 83.84(5) 58 30 Li9 Li2 Li9 83.84(5) 74 30 Li4 Li3 Li4 68.49(6) 4_566 3_656 Li4 Li3 Li4 68.49(6) 4_566 2_665 Li4 Li3 Li4 68.49(6) 3_656 2_665 Li4 Li3 Li11 116.96(5) 4_566 58 Li4 Li3 Li11 59.59(5) 3_656 58 Li4 Li3 Li11 116.96(5) 2_665 58 Li4 Li3 Li11 59.59(5) 4_566 30 Li4 Li3 Li11 116.96(5) 3_656 30 Li4 Li3 Li11 116.96(5) 2_665 30 Li11 Li3 Li11 116.98(3) 58 30 Li4 Li3 Li11 116.96(5) 4_566 74 Li4 Li3 Li11 116.96(5) 3_656 74 Li4 Li3 Li11 59.59(5) 2_665 74 Li11 Li3 Li11 116.98(3) 58 74 Li11 Li3 Li11 116.98(3) 30 74 Li4 Li3 Si3 59.33(3) 4_566 81 Li4 Li3 Si3 59.33(3) 3_656 81 Li4 Li3 Si3 115.57(7) 2_665 81 Li11 Li3 Si3 64.519(10) 58 81 Li11 Li3 Si3 64.519(10) 30 81 Li11 Li3 Si3 175.16(9) 74 81 Li4 Li3 Si3 59.33(3) 4_566 53 Li4 Li3 Si3 115.57(7) 3_656 53 Li4 Li3 Si3 59.33(3) 2_665 53 Li11 Li3 Si3 175.16(9) 58 53 Li11 Li3 Si3 64.519(10) 30 53 Li11 Li3 Si3 64.519(10) 74 53 Si3 Li3 Si3 113.58(3) 81 53 Li4 Li3 Si3 115.57(7) 4_566 25 Li4 Li3 Si3 59.33(3) 3_656 25 Li4 Li3 Si3 59.33(3) 2_665 25 Li11 Li3 Si3 64.519(10) 58 25 Li11 Li3 Si3 175.16(9) 30 25 Li11 Li3 Si3 64.519(10) 74 25 Si3 Li3 Si3 113.58(3) 81 25 Si3 Li3 Si3 113.58(3) 53 25 Li4 Li3 Li9 103.65(3) 4_566 74 Li4 Li3 Li9 103.65(3) 3_656 74 Li4 Li3 Li9 170.26(7) 2_665 74 Li11 Li3 Li9 60.60(3) 58 74 Li11 Li3 Li9 60.60(3) 30 74 Li11 Li3 Li9 130.15(9) 74 74 Si3 Li3 Li9 54.69(2) 81 74 Si3 Li3 Li9 122.44(3) 53 74 Si3 Li3 Li9 122.44(3) 25 74 Li4 Li3 Li9 103.65(3) 4_566 58 Li4 Li3 Li9 170.26(7) 3_656 58 Li4 Li3 Li9 103.65(3) 2_665 58 Li11 Li3 Li9 130.15(9) 58 58 Li11 Li3 Li9 60.60(3) 30 58 Li11 Li3 Li9 60.60(3) 74 58 Si3 Li3 Li9 122.44(3) 81 58 Si3 Li3 Li9 54.69(2) 53 58 Si3 Li3 Li9 122.44(3) 25 58 Li9 Li3 Li9 83.52(6) 74 58 Li4 Li3 Li9 170.26(7) 4_566 30 Li4 Li3 Li9 103.65(3) 3_656 30 Li4 Li3 Li9 103.65(3) 2_665 30 Li11 Li3 Li9 60.60(3) 58 30 Li11 Li3 Li9 130.15(9) 30 30 Li11 Li3 Li9 60.60(3) 74 30 Si3 Li3 Li9 122.44(3) 81 30 Si3 Li3 Li9 122.44(3) 53 30 Si3 Li3 Li9 54.69(2) 25 30 Li9 Li3 Li9 83.52(6) 74 30 Li9 Li3 Li9 83.52(6) 58 30 Li11 Li4 Li11 83.66(5) 57 29 Li11 Li4 Li11 83.66(5) 57 73 Li11 Li4 Li11 83.66(5) 29 73 Li11 Li4 Li3 126.05(2) 57 4_566 Li11 Li4 Li3 60.69(4) 29 4_566 Li11 Li4 Li3 126.05(2) 73 4_566 Li11 Li4 Li3 126.05(2) 57 2_665 Li11 Li4 Li3 126.05(2) 29 2_665 Li11 Li4 Li3 60.69(4) 73 2_665 Li3 Li4 Li3 107.84(4) 4_566 2_665 Li11 Li4 Li3 60.69(4) 57 3_656 Li11 Li4 Li3 126.05(2) 29 3_656 Li11 Li4 Li3 126.05(2) 73 3_656 Li3 Li4 Li3 107.84(4) 4_566 3_656 Li3 Li4 Li3 107.84(4) 2_665 3_656 Li11 Li4 Si3 66.219(16) 57 26_655 Li11 Li4 Si3 138.71(6) 29 26_655 Li11 Li4 Si3 66.219(16) 73 26_655 Li3 Li4 Si3 160.60(7) 4_566 26_655 Li3 Li4 Si3 62.865(11) 2_665 26_655 Li3 Li4 Si3 62.865(11) 3_656 26_655 Li11 Li4 Si3 138.71(6) 57 54_565 Li11 Li4 Si3 66.219(16) 29 54_565 Li11 Li4 Si3 66.219(16) 73 54_565 Li3 Li4 Si3 62.865(11) 4_566 54_565 Li3 Li4 Si3 62.865(11) 2_665 54_565 Li3 Li4 Si3 160.60(7) 3_656 54_565 Si3 Li4 Si3 119.918(3) 26_655 54_565 Li11 Li4 Si3 66.219(16) 57 82_556 Li11 Li4 Si3 66.219(16) 29 82_556 Li11 Li4 Si3 138.71(6) 73 82_556 Li3 Li4 Si3 62.865(11) 4_566 82_556 Li3 Li4 Si3 160.60(7) 2_665 82_556 Li3 Li4 Si3 62.865(11) 3_656 82_556 Si3 Li4 Si3 119.918(3) 26_655 82_556 Si3 Li4 Si3 119.918(3) 54_565 82_556 Li11 Li4 Li4 107.37(3) 57 2_665 Li11 Li4 Li4 107.37(3) 29 2_665 Li11 Li4 Li4 164.90(3) 73 2_665 Li3 Li4 Li4 55.76(3) 4_566 2_665 Li3 Li4 Li4 104.21(4) 2_665 2_665 Li3 Li4 Li4 55.76(3) 3_656 2_665 Si3 Li4 Li4 108.18(3) 26_655 2_665 Si3 Li4 Li4 108.18(3) 54_565 2_665 Si3 Li4 Li4 56.38(3) 82_556 2_665 Li11 Li4 Li4 107.37(3) 57 4_566 Li11 Li4 Li4 164.90(3) 29 4_566 Li11 Li4 Li4 107.37(3) 73 4_566 Li3 Li4 Li4 104.21(4) 4_566 4_566 Li3 Li4 Li4 55.76(3) 2_665 4_566 Li3 Li4 Li4 55.76(3) 3_656 4_566 Si3 Li4 Li4 56.38(3) 26_655 4_566 Si3 Li4 Li4 108.18(3) 54_565 4_566 Si3 Li4 Li4 108.18(3) 82_556 4_566 Li4 Li4 Li4 60.0 2_665 4_566 Li11 Li4 Li4 164.90(3) 57 3_656 Li11 Li4 Li4 107.37(3) 29 3_656 Li11 Li4 Li4 107.37(3) 73 3_656 Li3 Li4 Li4 55.76(3) 4_566 3_656 Li3 Li4 Li4 55.76(3) 2_665 3_656 Li3 Li4 Li4 104.21(4) 3_656 3_656 Si3 Li4 Li4 108.18(3) 26_655 3_656 Si3 Li4 Li4 56.38(3) 54_565 3_656 Si3 Li4 Li4 108.18(3) 82_556 3_656 Li4 Li4 Li4 60.0 2_665 3_656 Li4 Li4 Li4 60.0 4_566 3_656 Si4 Li5 Si4 119.855(5) 81 25 Si4 Li5 Si4 119.855(5) 81 53 Si4 Li5 Si4 119.855(5) 25 53 Si4 Li5 Li6 62.033(12) 81 28_566 Si4 Li5 Li6 152.81(7) 25 28_566 Si4 Li5 Li6 62.033(12) 53 28_566 Si4 Li5 Li6 62.033(12) 81 51_656 Si4 Li5 Li6 62.033(12) 25 51_656 Si4 Li5 Li6 152.81(7) 53 51_656 Li6 Li5 Li6 103.42(5) 28_566 51_656 Si4 Li5 Li6 152.81(7) 81 74_665 Si4 Li5 Li6 62.033(11) 25 74_665 Si4 Li5 Li6 62.033(12) 53 74_665 Li6 Li5 Li6 103.42(5) 28_566 74_665 Li6 Li5 Li6 103.42(5) 51_656 74_665 Si4 Li5 Li10 64.395(12) 81 57 Si4 Li5 Li10 64.395(12) 25 57 Si4 Li5 Li10 156.15(7) 53 57 Li6 Li5 Li10 126.347(9) 28_566 57 Li6 Li5 Li10 51.04(4) 51_656 57 Li6 Li5 Li10 126.347(9) 74_665 57 Si4 Li5 Li10 64.395(12) 81 29 Si4 Li5 Li10 156.15(7) 25 29 Si4 Li5 Li10 64.395(12) 53 29 Li6 Li5 Li10 51.04(4) 28_566 29 Li6 Li5 Li10 126.347(9) 51_656 29 Li6 Li5 Li10 126.347(9) 74_665 29 Li10 Li5 Li10 102.18(4) 57 29 Si4 Li5 Li10 156.15(7) 81 73 Si4 Li5 Li10 64.395(12) 25 73 Si4 Li5 Li10 64.395(12) 53 73 Li6 Li5 Li10 126.347(9) 28_566 73 Li6 Li5 Li10 126.347(9) 51_656 73 Li6 Li5 Li10 51.04(4) 74_665 73 Li10 Li5 Li10 102.18(4) 57 73 Li10 Li5 Li10 102.18(4) 29 73 Si4 Li5 Li11 110.38(4) 81 57 Si4 Li5 Li11 110.38(4) 25 57 Si4 Li5 Li11 52.53(2) 53 57 Li6 Li5 Li11 92.07(3) 28_566 57 Li6 Li5 Li11 154.66(6) 51_656 57 Li6 Li5 Li11 92.07(3) 74_665 57 Li10 Li5 Li11 103.62(6) 57 57 Li10 Li5 Li11 51.34(2) 29 57 Li10 Li5 Li11 51.34(2) 73 57 Si4 Li5 Li11 110.38(4) 81 29 Si4 Li5 Li11 52.53(2) 25 29 Si4 Li5 Li11 110.38(4) 53 29 Li6 Li5 Li11 154.66(6) 28_566 29 Li6 Li5 Li11 92.07(3) 51_656 29 Li6 Li5 Li11 92.07(3) 74_665 29 Li10 Li5 Li11 51.34(2) 57 29 Li10 Li5 Li11 103.62(6) 29 29 Li10 Li5 Li11 51.34(2) 73 29 Li11 Li5 Li11 67.10(5) 57 29 Si4 Li5 Li11 52.53(2) 81 73 Si4 Li5 Li11 110.38(4) 25 73 Si4 Li5 Li11 110.38(4) 53 73 Li6 Li5 Li11 92.07(3) 28_566 73 Li6 Li5 Li11 92.07(3) 51_656 73 Li6 Li5 Li11 154.66(6) 74_665 73 Li10 Li5 Li11 51.34(2) 57 73 Li10 Li5 Li11 51.34(2) 29 73 Li10 Li5 Li11 103.62(6) 73 73 Li11 Li5 Li11 67.10(5) 57 73 Li11 Li5 Li11 67.10(5) 29 73 Li10 Li6 Li10 106.35(5) 10_656 6_566 Li10 Li6 Li10 106.35(5) 10_656 2_665 Li10 Li6 Li10 106.35(5) 6_566 2_665 Li10 Li6 Si2 67.57(5) 10_656 . Li10 Li6 Si2 67.57(5) 6_566 . Li10 Li6 Si2 67.57(5) 2_665 . Li10 Li6 Li5 126.59(3) 10_656 28_566 Li10 Li6 Li5 67.96(5) 6_566 28_566 Li10 Li6 Li5 126.59(3) 2_665 28_566 Si2 Li6 Li5 135.53(4) . 28_566 Li10 Li6 Li5 126.59(3) 10_656 74_665 Li10 Li6 Li5 126.59(3) 6_566 74_665 Li10 Li6 Li5 67.96(5) 2_665 74_665 Si2 Li6 Li5 135.53(4) . 74_665 Li5 Li6 Li5 74.70(6) 28_566 74_665 Li10 Li6 Li5 67.96(5) 10_656 51_656 Li10 Li6 Li5 126.59(3) 6_566 51_656 Li10 Li6 Li5 126.59(3) 2_665 51_656 Si2 Li6 Li5 135.53(4) . 51_656 Li5 Li6 Li5 74.70(6) 28_566 51_656 Li5 Li6 Li5 74.70(6) 74_665 51_656 Li10 Li6 Si4 69.355(11) 10_656 34_656 Li10 Li6 Si4 69.355(11) 6_566 34_656 Li10 Li6 Si4 171.99(8) 2_665 34_656 Si2 Li6 Si4 104.42(4) . 34_656 Li5 Li6 Si4 58.87(2) 28_566 34_656 Li5 Li6 Si4 120.05(7) 74_665 34_656 Li5 Li6 Si4 58.87(2) 51_656 34_656 Li10 Li6 Si4 171.99(8) 10_656 78_566 Li10 Li6 Si4 69.355(11) 6_566 78_566 Li10 Li6 Si4 69.355(11) 2_665 78_566 Si2 Li6 Si4 104.42(4) . 78_566 Li5 Li6 Si4 58.87(2) 28_566 78_566 Li5 Li6 Si4 58.87(2) 74_665 78_566 Li5 Li6 Si4 120.05(7) 51_656 78_566 Si4 Li6 Si4 114.02(3) 34_656 78_566 Li10 Li6 Si4 69.355(11) 10_656 50_665 Li10 Li6 Si4 171.99(8) 6_566 50_665 Li10 Li6 Si4 69.355(11) 2_665 50_665 Si2 Li6 Si4 104.42(4) . 50_665 Li5 Li6 Si4 120.05(7) 28_566 50_665 Li5 Li6 Si4 58.87(2) 74_665 50_665 Li5 Li6 Si4 58.87(2) 51_656 50_665 Si4 Li6 Si4 114.02(3) 34_656 50_665 Si4 Li6 Si4 114.02(3) 78_566 50_665 Li10 Li6 Li12 119.91(7) 10_656 10_666 Li10 Li6 Li12 53.20(3) 6_566 10_666 Li10 Li6 Li12 53.20(3) 2_665 10_666 Si2 Li6 Li12 52.35(3) . 10_666 Li5 Li6 Li12 99.13(3) 28_566 10_666 Li5 Li6 Li12 99.13(3) 74_665 10_666 Li5 Li6 Li12 172.12(6) 51_656 10_666 Si4 Li6 Li12 122.38(2) 34_656 10_666 Si4 Li6 Li12 52.07(2) 78_566 10_666 Si4 Li6 Li12 122.38(2) 50_665 10_666 Li10 Li6 Li12 53.20(3) 10_656 2_666 Li10 Li6 Li12 53.20(3) 6_566 2_666 Li10 Li6 Li12 119.91(7) 2_665 2_666 Si2 Li6 Li12 52.35(3) . 2_666 Li5 Li6 Li12 99.13(3) 28_566 2_666 Li5 Li6 Li12 172.12(6) 74_665 2_666 Li5 Li6 Li12 99.13(3) 51_656 2_666 Si4 Li6 Li12 52.07(2) 34_656 2_666 Si4 Li6 Li12 122.38(2) 78_566 2_666 Si4 Li6 Li12 122.38(2) 50_665 2_666 Li12 Li6 Li12 86.57(4) 10_666 2_666 Li1 Li7 Li1 96.24(9) . 4 Li1 Li7 Si2 67.09(3) . 3_646 Li1 Li7 Si2 67.09(3) 4 3_646 Li1 Li7 Si2 67.09(3) . 2_664 Li1 Li7 Si2 67.09(3) 4 2_664 Si2 Li7 Si2 108.65(5) 3_646 2_664 Li1 Li7 Li10 108.78(3) . 8_655 Li1 Li7 Li10 108.78(3) 4 8_655 Si2 Li7 Li10 173.16(6) 3_646 8_655 Si2 Li7 Li10 64.51(2) 2_664 8_655 Li1 Li7 Li10 108.78(3) . 7_655 Li1 Li7 Li10 108.78(3) 4 7_655 Si2 Li7 Li10 64.51(2) 3_646 7_655 Si2 Li7 Li10 173.16(6) 2_664 7_655 Li10 Li7 Li10 122.33(8) 8_655 7_655 Li1 Li7 Si3 131.88(5) . . Li1 Li7 Si3 131.88(5) 4 . Si2 Li7 Si3 125.67(3) 3_646 . Si2 Li7 Si3 125.67(3) 2_664 . Li10 Li7 Si3 61.16(4) 8_655 . Li10 Li7 Si3 61.16(4) 7_655 . Li1 Li7 Li9 78.06(5) . 5 Li1 Li7 Li9 174.30(6) 4 5 Si2 Li7 Li9 110.138(10) 3_646 5 Si2 Li7 Li9 110.138(10) 2_664 5 Li10 Li7 Li9 73.46(3) 8_655 5 Li10 Li7 Li9 73.46(3) 7_655 5 Si3 Li7 Li9 53.82(3) . 5 Li1 Li7 Li9 174.30(6) . 6 Li1 Li7 Li9 78.06(5) 4 6 Si2 Li7 Li9 110.138(10) 3_646 6 Si2 Li7 Li9 110.138(10) 2_664 6 Li10 Li7 Li9 73.46(3) 8_655 6 Li10 Li7 Li9 73.46(3) 7_655 6 Si3 Li7 Li9 53.82(3) . 6 Li9 Li7 Li9 107.64(6) 5 6 Li1 Li7 Li12 56.29(3) . . Li1 Li7 Li12 121.05(4) 4 . Si2 Li7 Li12 123.16(4) 3_646 . Si2 Li7 Li12 54.47(2) 2_664 . Li10 Li7 Li12 53.55(2) 8_655 . Li10 Li7 Li12 128.49(4) 7_655 . Si3 Li7 Li12 91.68(3) . . Li9 Li7 Li12 55.73(2) 5 . Li9 Li7 Li12 126.71(4) 6 . Li1 Li7 Li12 121.05(4) . 11 Li1 Li7 Li12 56.29(3) 4 11 Si2 Li7 Li12 123.16(4) 3_646 11 Si2 Li7 Li12 54.47(2) 2_664 11 Li10 Li7 Li12 53.55(2) 8_655 11 Li10 Li7 Li12 128.49(4) 7_655 11 Si3 Li7 Li12 91.68(3) . 11 Li9 Li7 Li12 126.70(4) 5 11 Li9 Li7 Li12 55.73(2) 6 11 Li12 Li7 Li12 91.95(5) . 11 Li1 Li7 Li12 56.29(3) . 9 Li1 Li7 Li12 121.05(4) 4 9 Si2 Li7 Li12 54.47(2) 3_646 9 Si2 Li7 Li12 123.16(4) 2_664 9 Li10 Li7 Li12 128.49(4) 8_655 9 Li10 Li7 Li12 53.55(2) 7_655 9 Si3 Li7 Li12 91.68(3) . 9 Li9 Li7 Li12 55.73(2) 5 9 Li9 Li7 Li12 126.70(4) 6 9 Li12 Li7 Li12 87.95(5) . 9 Li12 Li7 Li12 176.64(6) 11 9 Li12 Li8 Li12 119.12(9) 5 30 Li12 Li8 Li2 115.61(3) 5 51 Li12 Li8 Li2 115.61(3) 30 51 Li12 Li8 Li2 115.61(3) 5 74 Li12 Li8 Li2 115.61(3) 30 74 Li2 Li8 Li2 62.87(8) 51 74 Li12 Li8 Si4 59.56(4) 5 74 Li12 Li8 Si4 59.56(4) 30 74 Li2 Li8 Si4 148.56(4) 51 74 Li2 Li8 Si4 148.56(4) 74 74 Li12 Li8 Si1 176.82(7) 5 28 Li12 Li8 Si1 64.05(3) 30 28 Li2 Li8 Si1 61.81(3) 51 28 Li2 Li8 Si1 61.81(3) 74 28 Si4 Li8 Si1 123.62(3) 74 28 Li12 Li8 Si1 64.05(3) 5 . Li12 Li8 Si1 176.83(7) 30 . Li2 Li8 Si1 61.81(3) 51 . Li2 Li8 Si1 61.81(3) 74 . Si4 Li8 Si1 123.61(3) 74 . Si1 Li8 Si1 112.77(6) 28 . Li12 Li8 Li9 59.32(3) 5 . Li12 Li8 Li9 127.57(3) 30 . Li2 Li8 Li9 108.03(5) 51 . Li2 Li8 Li9 61.51(4) 74 . Si4 Li8 Li9 95.63(4) 74 . Si1 Li8 Li9 119.11(4) 28 . Si1 Li8 Li9 53.471(18) . . Li12 Li8 Li9 127.57(3) 5 28 Li12 Li8 Li9 59.32(3) 30 28 Li2 Li8 Li9 61.51(4) 51 28 Li2 Li8 Li9 108.03(5) 74 28 Si4 Li8 Li9 95.63(4) 74 28 Si1 Li8 Li9 53.472(18) 28 28 Si1 Li8 Li9 119.12(4) . 28 Li9 Li8 Li9 168.74(7) . 28 Li12 Li8 Li9 127.57(3) 5 35 Li12 Li8 Li9 59.32(3) 30 35 Li2 Li8 Li9 108.03(5) 51 35 Li2 Li8 Li9 61.51(4) 74 35 Si4 Li8 Li9 95.63(4) 74 35 Si1 Li8 Li9 53.472(18) 28 35 Si1 Li8 Li9 119.12(4) . 35 Li9 Li8 Li9 81.01(4) . 35 Li9 Li8 Li9 97.87(4) 28 35 Li12 Li8 Li9 59.32(3) 5 9 Li12 Li8 Li9 127.57(3) 30 9 Li2 Li8 Li9 61.51(4) 51 9 Li2 Li8 Li9 108.03(5) 74 9 Si4 Li8 Li9 95.63(4) 74 9 Si1 Li8 Li9 119.12(4) 28 9 Si1 Li8 Li9 53.471(18) . 9 Li9 Li8 Li9 97.88(4) . 9 Li9 Li8 Li9 81.01(4) 28 9 Li9 Li8 Li9 168.74(7) 35 9 Li12 Li8 Li11 73.03(3) 5 56 Li12 Li8 Li11 73.03(3) 30 56 Li2 Li8 Li11 156.62(6) 51 56 Li2 Li8 Li11 93.75(4) 74 56 Si4 Li8 Li11 54.81(3) 74 56 Si1 Li8 Li11 108.605(8) 28 56 Si1 Li8 Li11 108.604(8) . 56 Li9 Li8 Li11 55.968(19) . 56 Li9 Li8 Li11 132.28(4) 28 56 Li9 Li8 Li11 55.968(19) 35 56 Li9 Li8 Li11 132.28(4) 9 56 Si1 Li9 Si3 158.61(5) . 9 Si1 Li9 Li12 64.95(3) . 9 Si3 Li9 Li12 102.15(4) 9 9 Si1 Li9 Li12 64.95(3) . 5 Si3 Li9 Li12 102.15(4) 9 5 Li12 Li9 Li12 97.67(6) 9 5 Si1 Li9 Li11 122.79(3) . 35 Si3 Li9 Li11 64.96(3) 9 35 Li12 Li9 Li11 74.40(3) 9 35 Li12 Li9 Li11 162.11(6) 5 35 Si1 Li9 Li11 122.79(3) . 56 Si3 Li9 Li11 64.96(3) 9 56 Li12 Li9 Li11 162.11(6) 9 56 Li12 Li9 Li11 74.40(3) 5 56 Li11 Li9 Li11 108.33(5) 35 56 Si1 Li9 Li2 61.48(3) . 74 Si3 Li9 Li2 139.90(5) 9 74 Li12 Li9 Li2 103.93(4) 9 74 Li12 Li9 Li2 103.93(4) 5 74 Li11 Li9 Li2 93.63(4) 35 74 Li11 Li9 Li2 93.63(4) 56 74 Si1 Li9 Li3 140.73(6) . 74 Si3 Li9 Li3 60.66(4) 9 74 Li12 Li9 Li3 130.30(3) 9 74 Li12 Li9 Li3 130.30(3) 5 74 Li11 Li9 Li3 55.94(2) 35 74 Li11 Li9 Li3 55.94(2) 56 74 Li2 Li9 Li3 79.25(5) 74 74 Si1 Li9 Li7 97.55(4) . 9 Si3 Li9 Li7 61.06(3) 9 9 Li12 Li9 Li7 63.64(3) 9 9 Li12 Li9 Li7 63.64(3) 5 9 Li11 Li9 Li7 98.58(4) 35 9 Li11 Li9 Li7 98.58(4) 56 9 Li2 Li9 Li7 159.04(5) 74 9 Li3 Li9 Li7 121.72(5) 74 9 Si1 Li9 Li8 60.62(3) . 5 Si3 Li9 Li8 127.21(3) 9 5 Li12 Li9 Li8 54.29(3) 9 5 Li12 Li9 Li8 125.27(5) 5 5 Li11 Li9 Li8 63.28(3) 35 5 Li11 Li9 Li8 143.19(6) 56 5 Li2 Li9 Li8 53.79(4) 74 5 Li3 Li9 Li8 97.06(4) 74 5 Li7 Li9 Li8 117.83(4) 9 5 Si1 Li9 Li8 60.62(3) . . Si3 Li9 Li8 127.21(3) 9 . Li12 Li9 Li8 125.27(5) 9 . Li12 Li9 Li8 54.29(3) 5 . Li11 Li9 Li8 143.19(6) 35 . Li11 Li9 Li8 63.28(3) 56 . Li2 Li9 Li8 53.79(4) 74 . Li3 Li9 Li8 97.06(4) 74 . Li7 Li9 Li8 117.83(4) 9 . Li8 Li9 Li8 100.91(7) 5 . Si1 Li9 Li10 113.12(3) . 4_556 Si3 Li9 Li10 54.30(3) 9 4_556 Li12 Li9 Li10 48.60(3) 9 4_556 Li12 Li9 Li10 113.03(4) 5 4_556 Li11 Li9 Li10 49.73(2) 35 4_556 Li11 Li9 Li10 119.14(5) 56 4_556 Li2 Li9 Li10 135.45(2) 74 4_556 Li3 Li9 Li10 94.27(3) 74 4_556 Li7 Li9 Li10 49.90(3) 9 4_556 Li8 Li9 Li10 84.04(3) 5 4_556 Li8 Li9 Li10 166.95(5) . 4_556 Li6 Li10 Li12 78.38(4) 2_665 11_556 Li6 Li10 Li12 78.38(4) 2_665 8_556 Li12 Li10 Li12 114.01(6) 11_556 8_556 Li6 Li10 Li11 114.87(5) 2_665 33_545 Li12 Li10 Li11 80.58(3) 11_556 33_545 Li12 Li10 Li11 162.81(5) 8_556 33_545 Li6 Li10 Li11 114.87(5) 2_665 53_455 Li12 Li10 Li11 162.81(5) 11_556 53_455 Li12 Li10 Li11 80.58(3) 8_556 53_455 Li11 Li10 Li11 83.69(6) 33_545 53_455 Li6 Li10 Li7 118.86(6) 2_665 10_556 Li12 Li10 Li7 69.76(4) 11_556 10_556 Li12 Li10 Li7 69.76(4) 8_556 10_556 Li11 Li10 Li7 109.61(5) 33_545 10_556 Li11 Li10 Li7 109.61(5) 53_455 10_556 Li6 Li10 Si3 179.20(7) 2_665 10_556 Li12 Li10 Si3 102.03(4) 11_556 10_556 Li12 Li10 Si3 102.03(4) 8_556 10_556 Li11 Li10 Si3 64.59(3) 33_545 10_556 Li11 Li10 Si3 64.59(3) 53_455 10_556 Li7 Li10 Si3 61.93(4) 10_556 10_556 Li6 Li10 Si2 61.21(5) 2_665 2_665 Li12 Li10 Si2 57.29(3) 11_556 2_665 Li12 Li10 Si2 57.29(3) 8_556 2_665 Li11 Li10 Si2 137.85(3) 33_545 2_665 Li11 Li10 Si2 137.85(3) 53_455 2_665 Li7 Li10 Si2 57.65(3) 10_556 2_665 Si3 Li10 Si2 119.58(4) 10_556 2_665 Li6 Li10 Li5 61.00(6) 2_665 73_445 Li12 Li10 Li5 110.17(4) 11_556 73_445 Li12 Li10 Li5 110.17(4) 8_556 73_445 Li11 Li10 Li5 70.49(4) 33_545 73_445 Li11 Li10 Li5 70.49(4) 53_455 73_445 Li7 Li10 Li5 179.86(8) 10_556 73_445 Si3 Li10 Li5 118.20(4) 10_556 73_445 Si2 Li10 Li5 122.21(5) 2_665 73_445 Li6 Li10 Si4 61.36(3) 2_665 49_455 Li12 Li10 Si4 139.48(5) 11_556 49_455 Li12 Li10 Si4 55.99(3) 8_556 49_455 Li11 Li10 Si4 119.15(5) 33_545 49_455 Li11 Li10 Si4 55.77(2) 53_455 49_455 Li7 Li10 Si4 124.90(2) 10_556 49_455 Si3 Li10 Si4 118.28(2) 10_556 49_455 Si2 Li10 Si4 96.33(3) 2_665 49_455 Li5 Li10 Si4 55.06(2) 73_445 49_455 Li6 Li10 Si4 61.36(3) 2_665 29_545 Li12 Li10 Si4 55.99(3) 11_556 29_545 Li12 Li10 Si4 139.48(5) 8_556 29_545 Li11 Li10 Si4 55.77(2) 33_545 29_545 Li11 Li10 Si4 119.15(5) 53_455 29_545 Li7 Li10 Si4 124.90(2) 10_556 29_545 Si3 Li10 Si4 118.28(2) 10_556 29_545 Si2 Li10 Si4 96.33(3) 2_665 29_545 Li5 Li10 Si4 55.06(2) 73_445 29_545 Si4 Li10 Si4 103.75(4) 49_455 29_545 Li6 Li10 Li9 131.30(2) 2_665 3_556 Li12 Li10 Li9 126.10(6) 11_556 3_556 Li12 Li10 Li9 53.81(3) 8_556 3_556 Li11 Li10 Li9 110.73(4) 33_545 3_556 Li11 Li10 Li9 54.24(3) 53_455 3_556 Li7 Li10 Li9 56.64(3) 10_556 3_556 Si3 Li10 Li9 48.98(3) 10_556 3_556 Si2 Li10 Li9 94.96(3) 2_665 3_556 Li5 Li10 Li9 123.43(3) 73_445 3_556 Si4 Li10 Li9 82.294(14) 49_455 3_556 Si4 Li10 Li9 166.50(4) 29_545 3_556 Li10 Li11 Li10 115.68(6) 33_545 53_455 Li10 Li11 Li4 94.09(4) 33_545 73_445 Li10 Li11 Li4 94.09(4) 53_455 73_445 Li10 Li11 Si4 68.54(3) 33_545 9 Li10 Li11 Si4 68.54(3) 53_455 9 Li4 Li11 Si4 144.29(5) 73_445 9 Li10 Li11 Li3 119.44(3) 33_545 74 Li10 Li11 Li3 119.44(3) 53_455 74 Li4 Li11 Li3 59.72(6) 73_445 74 Si4 Li11 Li3 156.00(7) 9 74 Li10 Li11 Li9 76.03(3) 33_545 35 Li10 Li11 Li9 156.41(6) 53_455 35 Li4 Li11 Li9 105.82(4) 73_445 35 Si4 Li11 Li9 100.00(3) 9 35 Li3 Li11 Li9 63.45(4) 74 35 Li10 Li11 Li9 156.41(6) 33_545 56 Li10 Li11 Li9 76.03(3) 53_455 56 Li4 Li11 Li9 105.82(4) 73_445 56 Si4 Li11 Li9 100.00(3) 9 56 Li3 Li11 Li9 63.45(4) 74 56 Li9 Li11 Li9 86.29(6) 35 56 Li10 Li11 Si3 149.24(5) 33_545 50 Li10 Li11 Si3 60.40(3) 53_455 50 Li4 Li11 Si3 57.66(2) 73_445 50 Si4 Li11 Si3 126.457(15) 9 50 Li3 Li11 Si3 59.58(2) 74 50 Li9 Li11 Si3 120.47(4) 35 50 Li9 Li11 Si3 54.12(2) 56 50 Li10 Li11 Si3 60.40(3) 33_545 30 Li10 Li11 Si3 149.24(5) 53_455 30 Li4 Li11 Si3 57.66(2) 73_445 30 Si4 Li11 Si3 126.457(15) 9 30 Li3 Li11 Si3 59.58(2) 74 30 Li9 Li11 Si3 54.12(2) 35 30 Li9 Li11 Si3 120.47(4) 56 30 Si3 Li11 Si3 106.12(3) 50 30 Li10 Li11 Li8 96.56(3) 33_545 58 Li10 Li11 Li8 96.56(3) 53_455 58 Li4 Li11 Li8 159.91(5) 73_445 58 Si4 Li11 Li8 55.81(4) 9 58 Li3 Li11 Li8 100.19(7) 74 58 Li9 Li11 Li8 60.75(3) 35 58 Li9 Li11 Li8 60.75(3) 56 58 Si3 Li11 Li8 114.09(3) 50 58 Si3 Li11 Li8 114.09(3) 30 58 Li10 Li11 Li5 58.17(3) 33_545 73_445 Li10 Li11 Li5 58.17(3) 53_455 73_445 Li4 Li11 Li5 89.98(5) 73_445 73_445 Si4 Li11 Li5 54.30(3) 9 73_445 Li3 Li11 Li5 149.70(7) 74 73_445 Li9 Li11 Li5 132.60(3) 35 73_445 Li9 Li11 Li5 132.60(3) 56 73_445 Si3 Li11 Li5 105.89(3) 50 73_445 Si3 Li11 Li5 105.89(3) 30 73_445 Li8 Li11 Li5 110.11(5) 58 73_445 Li10 Li11 Li12 48.92(3) 33_545 28 Li10 Li11 Li12 118.42(4) 53_455 28 Li4 Li11 Li12 137.70(2) 73_445 28 Si4 Li11 Li12 50.03(2) 9 28 Li3 Li11 Li12 115.77(4) 74 28 Li9 Li11 Li12 52.35(2) 35 28 Li9 Li11 Li12 107.72(5) 56 28 Si3 Li11 Li12 161.83(4) 50 28 Si3 Li11 Li12 83.130(13) 30 28 Li8 Li11 Li12 47.93(3) 58 28 Li5 Li11 Li12 85.91(3) 73_445 28 Li10 Li12 Li10 96.80(7) 11_565 8_655 Li10 Li12 Si2 66.70(4) 11_565 2_664 Li10 Li12 Si2 66.70(4) 8_655 2_664 Li10 Li12 Li8 109.17(4) 11_565 9 Li10 Li12 Li8 109.17(4) 8_655 9 Si2 Li12 Li8 173.07(7) 2_664 9 Li10 Li12 Si4 69.64(4) 11_565 58 Li10 Li12 Si4 69.64(4) 8_655 58 Si2 Li12 Si4 111.82(5) 2_664 58 Li8 Li12 Si4 61.26(4) 9 58 Li10 Li12 Li1 109.55(5) 11_565 . Li10 Li12 Li1 109.55(5) 8_655 . Si2 Li12 Li1 66.83(5) 2_664 . Li8 Li12 Li1 120.09(7) 9 . Si4 Li12 Li1 178.65(7) 58 . Li10 Li12 Li9 77.59(3) 11_565 9 Li10 Li12 Li9 170.60(6) 8_655 9 Si2 Li12 Li9 116.79(3) 2_664 9 Li8 Li12 Li9 66.39(3) 9 9 Si4 Li12 Li9 101.18(3) 58 9 Li1 Li12 Li9 79.60(4) . 9 Li10 Li12 Li9 170.60(6) 11_565 5 Li10 Li12 Li9 77.59(3) 8_655 5 Si2 Li12 Li9 116.79(3) 2_664 5 Li8 Li12 Li9 66.39(3) 9 5 Si4 Li12 Li9 101.18(3) 58 5 Li1 Li12 Li9 79.60(4) . 5 Li9 Li12 Li9 106.90(7) 9 5 Li10 Li12 Si1 131.59(4) 11_565 . Li10 Li12 Si1 131.59(4) 8_655 . Si2 Li12 Si1 125.55(4) 2_664 . Li8 Li12 Si1 61.37(4) 9 . Si4 Li12 Si1 122.63(4) 58 . Li1 Li12 Si1 58.72(5) . . Li9 Li12 Si1 54.64(3) 9 . Li9 Li12 Si1 54.64(3) 5 . Li10 Li12 Li7 122.59(5) 11_565 . Li10 Li12 Li7 56.68(3) 8_655 . Si2 Li12 Li7 56.23(2) 2_664 . Li8 Li12 Li7 126.89(4) 9 . Si4 Li12 Li7 125.46(4) 58 . Li1 Li12 Li7 53.94(3) . . Li9 Li12 Li7 132.71(5) 9 . Li9 Li12 Li7 60.62(3) 5 . Si1 Li12 Li7 89.76(3) . . Li10 Li12 Li7 56.68(3) 11_565 5 Li10 Li12 Li7 122.59(5) 8_655 5 Si2 Li12 Li7 56.24(2) 2_664 5 Li8 Li12 Li7 126.89(4) 9 5 Si4 Li12 Li7 125.46(4) 58 5 Li1 Li12 Li7 53.94(3) . 5 Li9 Li12 Li7 60.62(3) 9 5 Li9 Li12 Li7 132.71(5) 5 5 Si1 Li12 Li7 89.76(3) . 5 Li7 Li12 Li7 93.35(6) . 5 Li10 Li12 Li6 48.42(4) 11_565 2_664 Li10 Li12 Li6 48.42(4) 8_655 2_664 Si2 Li12 Li6 55.02(4) 2_664 2_664 Li8 Li12 Li6 118.05(5) 9 2_664 Si4 Li12 Li6 56.79(3) 58 2_664 Li1 Li12 Li6 121.86(6) . 2_664 Li9 Li12 Li6 125.26(3) 9 2_664 Li9 Li12 Li6 125.26(3) 5 2_664 Si1 Li12 Li6 179.42(5) . 2_664 Li7 Li12 Li6 90.64(4) . 2_664 Li7 Li12 Li6 90.64(4) 5 2_664 Li1 Li13 Li1 109.5 . 4 Li1 Li13 Li1 109.5 . 3 Li1 Li13 Li1 109.5 4 3 Li1 Li13 Li1 109.5 . 2 Li1 Li13 Li1 109.5 4 2 Li1 Li13 Li1 109.5 3 2 Li1 Li13 Si2 180.00(7) . 1_444 Li1 Li13 Si2 70.5 4 1_444 Li1 Li13 Si2 70.5 3 1_444 Li1 Li13 Si2 70.5 2 1_444 Li1 Li13 Si2 70.5 . 3_646 Li1 Li13 Si2 70.5 4 3_646 Li1 Li13 Si2 180.00(7) 3 3_646 Li1 Li13 Si2 70.5 2 3_646 Si2 Li13 Si2 109.5 1_444 3_646 Li1 Li13 Si2 70.5 . 4_466 Li1 Li13 Si2 180.00(7) 4 4_466 Li1 Li13 Si2 70.5 3 4_466 Li1 Li13 Si2 70.5 2 4_466 Si2 Li13 Si2 109.5 1_444 4_466 Si2 Li13 Si2 109.5 3_646 4_466 Li1 Li13 Si2 70.5 . 2_664 Li1 Li13 Si2 70.5 4 2_664 Li1 Li13 Si2 70.5 3 2_664 Li1 Li13 Si2 180.00(7) 2 2_664 Si2 Li13 Si2 109.5 1_444 2_664 Si2 Li13 Si2 109.5 3_646 2_664 Si2 Li13 Si2 109.5 4_466 2_664 Li1 Li13 Li7 54.7 . . Li1 Li13 Li7 54.736(1) 4 . Li1 Li13 Li7 125.3 3 . Li1 Li13 Li7 125.3 2 . Si2 Li13 Li7 125.3 1_444 . Si2 Li13 Li7 54.7 3_646 . Si2 Li13 Li7 125.3 4_466 . Si2 Li13 Li7 54.7 2_664 . Li1 Li13 Li7 125.3 . 10 Li1 Li13 Li7 54.7 4 10 Li1 Li13 Li7 54.7 3 10 Li1 Li13 Li7 125.3 2 10 Si2 Li13 Li7 54.7 1_444 10 Si2 Li13 Li7 125.3 3_646 10 Si2 Li13 Li7 125.3 4_466 10 Si2 Li13 Li7 54.7 2_664 10 Li7 Li13 Li7 90.0 . 10 Li1 Li13 Li7 125.3 . 2 Li1 Li13 Li7 125.3 4 2 Li1 Li13 Li7 54.7 3 2 Li1 Li13 Li7 54.7 2 2 Si2 Li13 Li7 54.7 1_444 2 Si2 Li13 Li7 125.3 3_646 2 Si2 Li13 Li7 54.7 4_466 2 Si2 Li13 Li7 125.3 2_664 2 Li7 Li13 Li7 180.0 . 2 Li7 Li13 Li7 90.0 10 2 Li1 Li13 Li7 54.7 . 5 Li1 Li13 Li7 125.3 4 5 Li1 Li13 Li7 54.7 3 5 Li1 Li13 Li7 125.3 2 5 Si2 Li13 Li7 125.3 1_444 5 Si2 Li13 Li7 125.3 3_646 5 Si2 Li13 Li7 54.7 4_466 5 Si2 Li13 Li7 54.7 2_664 5 Li7 Li13 Li7 90.0 . 5 Li7 Li13 Li7 90.0 10 5 Li7 Li13 Li7 90.0 2 5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 Li9 2.6364(10) 9 Si1 Li9 2.6364(10) 5 Si1 Li9 2.6364(10) . Si1 Li1 2.768(2) . Si1 Li2 2.8459(5) 28 Si1 Li2 2.8459(5) 74 Si1 Li2 2.8459(4) 51 Si1 Li8 2.8589(9) 9 Si1 Li8 2.8589(9) 5 Si1 Li8 2.8590(9) . Si1 Li12 2.9287(14) . Si1 Li12 2.9287(14) 9 Si2 Li12 2.6515(11) 10_666 Si2 Li12 2.6515(11) 6_666 Si2 Li12 2.6515(11) 2_666 Si2 Li13 2.6950(3) 1_666 Si2 Li7 2.7087(8) 10_666 Si2 Li7 2.7087(8) 2_666 Si2 Li7 2.7087(8) 6_666 Si2 Li6 2.7441(18) . Si2 Li10 2.8942(10) 2_665 Si2 Li10 2.8942(11) 6_566 Si2 Li10 2.8942(11) 10_656 Si2 Li1 2.9487(10) 4_666 Si3 Li9 2.6371(11) 6 Si3 Li9 2.6371(11) 5 Si3 Li4 2.72281(18) 27_645 Si3 Li4 2.72281(18) 26_654 Si3 Li3 2.8171(5) 28 Si3 Li3 2.8171(5) 25_544 Si3 Li10 2.8385(12) 8_655 Si3 Li10 2.8385(12) 7_655 Si3 Li7 2.8593(14) . Si3 Li11 2.9489(6) 84 Si3 Li11 2.9489(6) 51 Si3 Li11 2.9489(6) 50_554 Si4 Li12 2.6644(11) 56 Si4 Li12 2.6644(11) 79 Si4 Li11 2.6771(9) 5 Si4 Li11 2.6771(9) 30 Si4 Li8 2.7096(16) 74 Si4 Li5 2.73923(17) 4_566 Si4 Li5 2.73922(17) 25_544 Si4 Li6 2.8263(5) 75_646 Si4 Li6 2.8263(5) 50_664 Si4 Li10 3.0135(8) 76_556 Si4 Li10 3.0135(8) 59_565 Si4 Li10 3.0135(8) 81_545 Li1 Li13 2.395(2) . Li1 Li7 2.6259(11) . Li1 Li7 2.6260(11) 9 Li1 Li7 2.6260(11) 5 Li1 Li12 2.7022(15) . Li1 Li12 2.7022(15) 9 Li1 Li12 2.7022(14) 5 Li1 Si2 2.9486(10) 2_664 Li1 Si2 2.9486(10) 4_466 Li1 Si2 2.9486(10) 3_646 Li1 Li9 3.5300(19) 5 Li2 Li8 2.6728(14) 58 Li2 Li8 2.6728(14) 30 Li2 Li8 2.6728(14) 74 Li2 Li2 2.788(3) 28 Li2 Li2 2.788(3) 74 Li2 Li2 2.788(3) 51 Li2 Si1 2.8458(5) 74 Li2 Si1 2.8458(5) 28 Li2 Si1 2.8458(5) 51 Li2 Li9 2.9117(16) 58 Li2 Li9 2.9117(16) 74 Li2 Li9 2.9117(16) 30 Li3 Li4 2.6787(18) 4_566 Li3 Li4 2.6787(18) 3_656 Li3 Li4 2.6787(18) 2_665 Li3 Li11 2.7049(9) 58 Li3 Li11 2.7049(10) 30 Li3 Li11 2.7049(10) 74 Li3 Si3 2.8171(5) 81 Li3 Si3 2.8171(5) 53 Li3 Si3 2.8171(5) 25 Li3 Li9 2.9208(16) 74 Li3 Li9 2.9208(16) 58 Li3 Li9 2.9208(16) 30 Li4 Li11 2.6753(15) 57 Li4 Li11 2.6753(15) 29 Li4 Li11 2.6753(15) 73 Li4 Li3 2.6788(18) 4_566 Li4 Li3 2.6788(18) 2_665 Li4 Li3 2.6788(18) 3_656 Li4 Si3 2.72279(18) 26_655 Li4 Si3 2.72279(18) 54_565 Li4 Si3 2.72279(18) 82_556 Li4 Li4 3.015(3) 2_665 Li4 Li4 3.015(3) 4_566 Li4 Li4 3.015(3) 3_656 Li5 Si4 2.73924(17) 81 Li5 Si4 2.73924(17) 25 Li5 Si4 2.73924(17) 53 Li5 Li6 2.7456(15) 28_566 Li5 Li6 2.7456(15) 51_656 Li5 Li6 2.7456(15) 74_665 Li5 Li10 2.9098(15) 57 Li5 Li10 2.9098(15) 29 Li5 Li10 2.9098(15) 73 Li5 Li11 3.2284(16) 57 Li5 Li11 3.2284(17) 29 Li5 Li11 3.2284(16) 73 Li6 Li10 2.4409(15) 10_656 Li6 Li10 2.4409(15) 6_566 Li6 Li10 2.4409(15) 2_665 Li6 Li5 2.7456(15) 28_566 Li6 Li5 2.7456(15) 74_665 Li6 Li5 2.7456(15) 51_656 Li6 Si4 2.8263(5) 34_656 Li6 Si4 2.8263(5) 78_566 Li6 Si4 2.8263(5) 50_665 Li6 Li12 3.1963(16) 10_666 Li6 Li12 3.1963(16) 2_666 Li7 Li1 2.6259(11) 4 Li7 Si2 2.7086(8) 3_646 Li7 Si2 2.7086(8) 2_664 Li7 Li10 2.7145(13) 8_655 Li7 Li10 2.7145(13) 7_655 Li7 Li9 2.9641(16) 5 Li7 Li9 2.9641(16) 6 Li7 Li12 3.0478(6) . Li7 Li12 3.0478(6) 11 Li7 Li12 3.0478(6) 9 Li8 Li12 2.6540(12) 5 Li8 Li12 2.6540(12) 30 Li8 Li2 2.6729(14) 51 Li8 Li2 2.6729(14) 74 Li8 Si4 2.7095(16) 74 Li8 Si1 2.8589(9) 28 Li8 Li9 2.9950(7) . Li8 Li9 2.9951(7) 28 Li8 Li9 2.9951(7) 35 Li8 Li9 2.9951(7) 9 Li8 Li11 3.0659(14) 56 Li9 Si3 2.6372(11) 9 Li9 Li12 2.8111(10) 9 Li9 Li12 2.8111(10) 5 Li9 Li11 2.8446(9) 35 Li9 Li11 2.8446(9) 56 Li9 Li2 2.9116(16) 74 Li9 Li3 2.9207(16) 74 Li9 Li7 2.9641(16) 9 Li9 Li8 2.9950(7) 5 Li9 Li10 3.4018(10) 4_556 Li10 Li6 2.4409(15) 2_665 Li10 Li12 2.6129(10) 11_556 Li10 Li12 2.6129(10) 8_556 Li10 Li11 2.6746(9) 33_545 Li10 Li11 2.6746(9) 53_455 Li10 Li7 2.7145(13) 10_556 Li10 Si3 2.8385(12) 10_556 Li10 Si2 2.8942(10) 2_665 Li10 Li5 2.9098(15) 73_445 Li10 Si4 3.0135(8) 49_455 Li10 Si4 3.0135(8) 29_545 Li10 Li9 3.4018(10) 3_556 Li11 Li10 2.6745(9) 33_545 Li11 Li10 2.6745(9) 53_455 Li11 Li4 2.6753(15) 73_445 Li11 Si4 2.6770(9) 9 Li11 Li3 2.7050(9) 74 Li11 Li9 2.8447(9) 35 Li11 Li9 2.8447(9) 56 Li11 Si3 2.9490(6) 50 Li11 Si3 2.9490(6) 30 Li11 Li8 3.0660(14) 58 Li11 Li5 3.2283(16) 73_445 Li11 Li12 3.4194(10) 28 Li12 Li10 2.6129(10) 11_565 Li12 Li10 2.6129(10) 8_655 Li12 Si2 2.6515(11) 2_664 Li12 Li8 2.6541(12) 9 Li12 Si4 2.6644(11) 58 Li12 Li9 2.8110(10) 9 Li12 Li9 2.8110(10) 5 Li12 Li7 3.0478(6) 5 Li12 Li6 3.1963(16) 2_664 Li13 Li1 2.395(2) 4 Li13 Li1 2.395(2) 3 Li13 Li1 2.395(2) 2 Li13 Si2 2.6949(3) 1_444 Li13 Si2 2.6949(3) 3_646 Li13 Si2 2.6949(3) 4_466 Li13 Si2 2.6949(3) 2_664 Li13 Li7 3.1355(14) 10 Li13 Li7 3.1355(14) 2 Li13 Li7 3.1355(14) 5