#------------------------------------------------------------------------------ #$Date: 2013-07-14 09:54:37 +0100 (Sun, 14 Jul 2013) $ #$Revision: 87152 $ #$URL: svn://www.crystallography.net/cod/cif/4/00/17/4001775.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4001775 loop_ _publ_author_name 'Zeilinger, Michael' 'Benson, Daryn' 'H\"aussermann, Ulrich' 'F\"assler, Thomas F.' _publ_section_title ; Single Crystal Growth and Thermodynamic Stability of Li17Si4 ; _journal_issue 9 _journal_name_full 'Chemistry of Materials' _journal_page_first 1960 _journal_paper_doi 10.1021/cm400612k _journal_volume 25 _journal_year 2013 _chemical_formula_analytical 'Li17 Si4' _chemical_formula_moiety 'Li17 Si4' _chemical_formula_sum 'Li17 Si4' _chemical_formula_weight 230.34 _chemical_melting_point '754 K, peritectical decomposition' _chemical_name_common 'Lithium Silicide' _chemical_name_systematic ; ? ; _space_group_IT_number 216 _symmetry_cell_setting cubic _symmetry_Int_Tables_number 216 _symmetry_space_group_name_Hall 'F -4 2 3' _symmetry_space_group_name_H-M 'F -4 3 m' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 20 _cell_length_a 18.7353(3) _cell_length_b 18.7353(3) _cell_length_c 18.7353(3) _cell_measurement_reflns_used 44207 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 29.70 _cell_measurement_theta_min 3.61 _cell_volume 6576.31(18) _citation_year 2013 _computing_cell_refinement ;X-Area (1.26) - Software for STOE IPDS 2, Stoe & Cie., Darmstadt (Germany), 2004. ; _computing_data_collection ;X-Area (1.26) - Software for STOE IPDS 2, Stoe & Cie., Darmstadt (Germany), 2004. ; _computing_data_reduction ;X-Red (1.26) - Data Reduction Program, Stoe & Cie., Darmstadt (Germany), 2004. ; _computing_molecular_graphics 'Diamond 3 (Crystal Impact 2011)' _computing_publication_material 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 298(2) _diffrn_detector IPDS _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.988 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device_type 'STOE IPDS 2T' _diffrn_measurement_method 'phi- and omega-rotation' _diffrn_radiation_monochromator 'MONTEL optic' _diffrn_radiation_source 'rotating anode FR591' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0538 _diffrn_reflns_av_sigmaI/netI 0.0098 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 46589 _diffrn_reflns_theta_full 29.16 _diffrn_reflns_theta_max 29.16 _diffrn_reflns_theta_min 3.61 _exptl_absorpt_coefficient_mu 0.389 _exptl_absorpt_correction_type none _exptl_absorpt_process_details none _exptl_crystal_colour 'metallic silver' _exptl_crystal_density_diffrn 1.163 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2140 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.3 _refine_diff_density_max 0.261 _refine_diff_density_min -0.234 _refine_diff_density_rms 0.043 _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.5(3) _refine_ls_extinction_coef 'not refined' _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.255 _refine_ls_matrix_type full _refine_ls_number_parameters 67 _refine_ls_number_reflns 935 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.255 _refine_ls_R_factor_all 0.0205 _refine_ls_R_factor_gt 0.0203 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0130P)^2^+0.3128P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0549 _refine_ls_wR_factor_ref 0.0550 _reflns_number_gt 930 _reflns_number_total 935 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file cm400612k_si_003.cif _[local]_cod_data_source_block Li17Si4_298K _cod_database_code 4001775 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, z+1/2' '-y, -x+1/2, z+1/2' 'y, -x+1/2, -z+1/2' '-y, x+1/2, -z+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'z, y+1/2, x+1/2' 'z, -y+1/2, -x+1/2' '-z, y+1/2, -x+1/2' '-z, -y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, z+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, -x, -z+1/2' '-y+1/2, x, -z+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'z+1/2, y, x+1/2' 'z+1/2, -y, -x+1/2' '-z+1/2, y, -x+1/2' '-z+1/2, -y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, z' '-y+1/2, -x+1/2, z' 'y+1/2, -x+1/2, -z' '-y+1/2, x+1/2, -z' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'z+1/2, y+1/2, x' 'z+1/2, -y+1/2, -x' '-z+1/2, y+1/2, -x' '-z+1/2, -y+1/2, x' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags Si1 Si 0.15980(3) 0.15980(3) 0.15980(3) 0.0114(2) Uani 1 6 d S Si2 Si 0.91674(3) 0.91674(3) 0.91674(3) 0.00961(18) Uani 1 6 d S Si3 Si 0.32106(4) 0.0000 0.0000 0.01160(18) Uani 1 4 d S Si4 Si 0.57004(4) 0.2500 0.2500 0.01090(18) Uani 1 4 d S Li1 Li 0.0733(2) 0.0733(2) 0.0733(2) 0.0268(13) Uani 1 6 d S Li2 Li 0.30308(16) 0.30308(16) 0.30308(16) 0.0195(10) Uani 1 6 d S Li3 Li 0.4177(2) 0.4177(2) 0.4177(2) 0.0172(11) Uani 1 6 d S Li4 Li 0.55730(18) 0.55730(18) 0.55730(18) 0.0216(11) Uani 1 6 d S Li5 Li 0.68755(19) 0.68755(19) 0.68755(19) 0.0229(11) Uani 1 6 d S Li6 Li 0.8313(2) 0.8313(2) 0.8313(2) 0.0267(18) Uani 1 6 d S Li7 Li 0.1685(3) 0.0000 0.0000 0.0230(12) Uani 1 4 d S Li8 Li 0.0749(3) 0.2500 0.2500 0.0233(13) Uani 1 4 d S Li9 Li 0.09141(15) 0.09141(15) 0.2614(2) 0.0278(10) Uani 1 2 d S Li10 Li 0.08996(18) 0.08996(18) 0.76137(19) 0.0277(9) Uani 1 2 d S Li11 Li 0.15444(13) 0.15444(13) 0.5199(2) 0.0266(7) Uani 1 2 d S Li12 Li 0.16351(12) 0.16351(12) 0.0016(3) 0.0216(10) Uani 1 2 d S Li13 Li 0.0000 0.0000 0.0000 0.016(2) Uani 1 24 d S loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0114(2) 0.0114(2) 0.0114(2) -0.00014(15) -0.00014(15) -0.00014(15) Si2 0.00961(18) 0.00961(18) 0.00961(18) -0.00121(15) -0.00121(15) -0.00121(15) Si3 0.0109(3) 0.0120(2) 0.0120(2) -0.0022(3) 0.000 0.000 Si4 0.0098(3) 0.0114(2) 0.0114(2) 0.0008(2) 0.000 0.000 Li1 0.0268(13) 0.0268(13) 0.0268(13) -0.0015(14) -0.0015(14) -0.0015(14) Li2 0.0195(10) 0.0195(10) 0.0195(10) 0.0023(11) 0.0023(11) 0.0023(11) Li3 0.0172(11) 0.0172(11) 0.0172(11) -0.0010(11) -0.0010(11) -0.0010(11) Li4 0.0216(11) 0.0216(11) 0.0216(11) 0.0051(13) 0.0051(13) 0.0051(13) Li5 0.0229(11) 0.0229(11) 0.0229(11) 0.0006(12) 0.0006(12) 0.0006(12) Li6 0.0267(18) 0.0267(18) 0.0267(18) 0.0001(13) 0.0001(13) 0.0001(13) Li7 0.020(2) 0.0243(15) 0.0243(15) 0.010(2) 0.000 0.000 Li8 0.024(2) 0.0232(18) 0.0232(18) -0.012(2) 0.000 0.000 Li9 0.0242(14) 0.0242(14) 0.035(2) 0.0069(10) 0.0069(10) -0.0048(15) Li10 0.0305(14) 0.0305(14) 0.0221(17) 0.0019(10) 0.0019(10) -0.0048(18) Li11 0.0265(10) 0.0265(10) 0.0266(18) 0.0006(10) 0.0006(10) -0.0057(14) Li12 0.0195(10) 0.0195(10) 0.0258(17) -0.0013(10) -0.0013(10) -0.0058(13) Li13 0.016(2) 0.016(2) 0.016(2) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Li9 Si1 Li9 117.94(5) . 9 Li9 Si1 Li9 117.94(5) . 5 Li9 Si1 Li9 117.94(5) 9 5 Li9 Si1 Li1 81.67(10) . . Li9 Si1 Li1 81.67(10) 9 . Li9 Si1 Li1 81.67(10) 5 . Li9 Si1 Li2 113.60(9) . 28 Li9 Si1 Li2 113.60(9) 9 28 Li9 Si1 Li2 63.72(14) 5 28 Li1 Si1 Li2 145.38(10) . 28 Li9 Si1 Li2 63.72(14) . 74 Li9 Si1 Li2 113.60(9) 9 74 Li9 Si1 Li2 113.60(9) 5 74 Li1 Si1 Li2 145.38(10) . 74 Li2 Si1 Li2 58.94(17) 28 74 Li9 Si1 Li2 113.60(9) . 51 Li9 Si1 Li2 63.72(14) 9 51 Li9 Si1 Li2 113.60(9) 5 51 Li1 Si1 Li2 145.38(10) . 51 Li2 Si1 Li2 58.94(17) 28 51 Li2 Si1 Li2 58.94(17) 74 51 Li9 Si1 Li8 65.83(6) . . Li9 Si1 Li8 65.83(6) 9 . Li9 Si1 Li8 167.25(13) 5 . Li1 Si1 Li8 111.08(10) . . Li2 Si1 Li8 103.54(15) 28 . Li2 Si1 Li8 55.87(8) 74 . Li2 Si1 Li8 55.87(8) 51 . Li9 Si1 Li8 65.83(6) . 5 Li9 Si1 Li8 167.25(13) 9 5 Li9 Si1 Li8 65.83(6) 5 5 Li1 Si1 Li8 111.08(10) . 5 Li2 Si1 Li8 55.87(8) 28 5 Li2 Si1 Li8 55.87(8) 74 5 Li2 Si1 Li8 103.54(15) 51 5 Li8 Si1 Li8 107.82(11) . 5 Li9 Si1 Li8 167.26(13) . 9 Li9 Si1 Li8 65.83(6) 9 9 Li9 Si1 Li8 65.83(6) 5 9 Li1 Si1 Li8 111.08(10) . 9 Li2 Si1 Li8 55.87(8) 28 9 Li2 Si1 Li8 103.54(15) 74 9 Li2 Si1 Li8 55.87(8) 51 9 Li8 Si1 Li8 107.82(11) . 9 Li8 Si1 Li8 107.82(11) 5 9 Li9 Si1 Li12 60.47(5) . 9 Li9 Si1 Li12 138.30(12) 9 9 Li9 Si1 Li12 60.47(5) 5 9 Li1 Si1 Li12 56.63(6) . 9 Li2 Si1 Li12 102.44(9) 28 9 Li2 Si1 Li12 102.44(9) 74 9 Li2 Si1 Li12 157.98(12) 51 9 Li8 Si1 Li12 125.98(4) . 9 Li8 Si1 Li12 54.44(10) 5 9 Li8 Si1 Li12 125.98(4) 9 9 Li9 Si1 Li12 60.47(5) . 5 Li9 Si1 Li12 60.47(5) 9 5 Li9 Si1 Li12 138.30(12) 5 5 Li1 Si1 Li12 56.63(6) . 5 Li2 Si1 Li12 157.98(12) 28 5 Li2 Si1 Li12 102.44(9) 74 5 Li2 Si1 Li12 102.44(9) 51 5 Li8 Si1 Li12 54.44(10) . 5 Li8 Si1 Li12 125.98(4) 5 5 Li8 Si1 Li12 125.98(4) 9 5 Li12 Si1 Li12 92.65(9) 9 5 Li12 Si2 Li12 110.95(9) 10_666 6_666 Li12 Si2 Li12 110.95(9) 10_666 2_666 Li12 Si2 Li12 110.95(9) 6_666 2_666 Li12 Si2 Li13 107.94(9) 10_666 1_666 Li12 Si2 Li13 107.94(9) 6_666 1_666 Li12 Si2 Li13 107.94(9) 2_666 1_666 Li12 Si2 Li7 69.46(6) 10_666 10_666 Li12 Si2 Li7 69.46(6) 6_666 10_666 Li12 Si2 Li7 179.12(15) 2_666 10_666 Li13 Si2 Li7 71.18(10) 1_666 10_666 Li12 Si2 Li7 69.46(6) 10_666 2_666 Li12 Si2 Li7 179.12(15) 6_666 2_666 Li12 Si2 Li7 69.46(6) 2_666 2_666 Li13 Si2 Li7 71.18(10) 1_666 2_666 Li7 Si2 Li7 110.11(10) 10_666 2_666 Li12 Si2 Li7 179.12(15) 10_666 6_666 Li12 Si2 Li7 69.46(6) 6_666 6_666 Li12 Si2 Li7 69.46(6) 2_666 6_666 Li13 Si2 Li7 71.18(10) 1_666 6_666 Li7 Si2 Li7 110.11(10) 10_666 6_666 Li7 Si2 Li7 110.11(10) 2_666 6_666 Li12 Si2 Li6 72.06(9) 10_666 . Li12 Si2 Li6 72.06(9) 6_666 . Li12 Si2 Li6 72.06(9) 2_666 . Li13 Si2 Li6 180.00(7) 1_666 . Li7 Si2 Li6 108.82(10) 10_666 . Li7 Si2 Li6 108.82(10) 2_666 . Li7 Si2 Li6 108.82(10) 6_666 . Li12 Si2 Li10 55.68(5) 10_666 2_665 Li12 Si2 Li10 55.68(5) 6_666 2_665 Li12 Si2 Li10 123.30(14) 2_666 2_665 Li13 Si2 Li10 128.75(10) 1_666 2_665 Li7 Si2 Li10 57.58(12) 10_666 2_665 Li7 Si2 Li10 124.82(6) 2_666 2_665 Li7 Si2 Li10 124.82(6) 6_666 2_665 Li6 Si2 Li10 51.25(10) . 2_665 Li12 Si2 Li10 55.68(5) 10_666 6_566 Li12 Si2 Li10 123.30(14) 6_666 6_566 Li12 Si2 Li10 55.68(5) 2_666 6_566 Li13 Si2 Li10 128.75(10) 1_666 6_566 Li7 Si2 Li10 124.82(6) 10_666 6_566 Li7 Si2 Li10 57.58(12) 2_666 6_566 Li7 Si2 Li10 124.82(6) 6_666 6_566 Li6 Si2 Li10 51.25(10) . 6_566 Li10 Si2 Li10 84.97(14) 2_665 6_566 Li12 Si2 Li10 123.30(14) 10_666 10_656 Li12 Si2 Li10 55.68(5) 6_666 10_656 Li12 Si2 Li10 55.68(5) 2_666 10_656 Li13 Si2 Li10 128.75(10) 1_666 10_656 Li7 Si2 Li10 124.82(6) 10_666 10_656 Li7 Si2 Li10 124.82(6) 2_666 10_656 Li7 Si2 Li10 57.58(12) 6_666 10_656 Li6 Si2 Li10 51.25(10) . 10_656 Li10 Si2 Li10 84.97(14) 2_665 10_656 Li10 Si2 Li10 84.97(14) 6_566 10_656 Li12 Si2 Li1 124.19(6) 10_666 4_666 Li12 Si2 Li1 58.37(17) 6_666 4_666 Li12 Si2 Li1 124.19(6) 2_666 4_666 Li13 Si2 Li1 49.57(13) 1_666 4_666 Li7 Si2 Li1 55.29(6) 10_666 4_666 Li7 Si2 Li1 120.75(19) 2_666 4_666 Li7 Si2 Li1 55.29(6) 6_666 4_666 Li6 Si2 Li1 130.43(13) . 4_666 Li10 Si2 Li1 96.26(8) 2_665 4_666 Li10 Si2 Li1 178.3(2) 6_566 4_666 Li10 Si2 Li1 96.26(8) 10_656 4_666 Li9 Si3 Li9 130.43(19) 6 5 Li9 Si3 Li4 110.42(8) 6 27_645 Li9 Si3 Li4 110.42(8) 5 27_645 Li9 Si3 Li4 110.42(8) 6 26_654 Li9 Si3 Li4 110.42(8) 5 26_654 Li4 Si3 Li4 67.3(2) 27_645 26_654 Li9 Si3 Li3 165.06(18) 6 28 Li9 Si3 Li3 64.51(14) 5 28 Li4 Si3 Li3 57.87(12) 27_645 28 Li4 Si3 Li3 57.87(12) 26_654 28 Li9 Si3 Li3 64.51(14) 6 25_544 Li9 Si3 Li3 165.06(18) 5 25_544 Li4 Si3 Li3 57.87(12) 27_645 25_544 Li4 Si3 Li3 57.87(12) 26_654 25_544 Li3 Si3 Li3 100.6(3) 28 25_544 Li9 Si3 Li10 76.82(6) 6 8_655 Li9 Si3 Li10 76.82(6) 5 8_655 Li4 Si3 Li10 89.27(15) 27_645 8_655 Li4 Si3 Li10 156.61(14) 26_654 8_655 Li3 Si3 Li10 110.34(7) 28 8_655 Li3 Si3 Li10 110.34(7) 25_544 8_655 Li9 Si3 Li10 76.82(6) 6 7_655 Li9 Si3 Li10 76.82(6) 5 7_655 Li4 Si3 Li10 156.61(14) 27_645 7_655 Li4 Si3 Li10 89.27(15) 26_654 7_655 Li3 Si3 Li10 110.34(7) 28 7_655 Li3 Si3 Li10 110.34(7) 25_544 7_655 Li10 Si3 Li10 114.12(16) 8_655 7_655 Li9 Si3 Li7 65.21(9) 6 . Li9 Si3 Li7 65.21(9) 5 . Li4 Si3 Li7 146.33(12) 27_645 . Li4 Si3 Li7 146.33(12) 26_654 . Li3 Si3 Li7 129.72(14) 28 . Li3 Si3 Li7 129.72(14) 25_544 . Li10 Si3 Li7 57.06(8) 8_655 . Li10 Si3 Li7 57.06(8) 7_655 . Li9 Si3 Li11 127.81(7) 6 84 Li9 Si3 Li11 61.13(8) 5 84 Li4 Si3 Li11 107.71(10) 27_645 84 Li4 Si3 Li11 55.74(10) 26_654 84 Li3 Si3 Li11 55.70(7) 28 84 Li3 Si3 Li11 111.40(10) 25_544 84 Li10 Si3 Li11 137.80(8) 8_655 84 Li10 Si3 Li11 55.13(7) 7_655 84 Li7 Si3 Li11 98.94(5) . 84 Li9 Si3 Li11 127.81(7) 6 51 Li9 Si3 Li11 61.13(8) 5 51 Li4 Si3 Li11 55.74(10) 27_645 51 Li4 Si3 Li11 107.71(10) 26_654 51 Li3 Si3 Li11 55.70(7) 28 51 Li3 Si3 Li11 111.40(10) 25_544 51 Li10 Si3 Li11 55.13(7) 8_655 51 Li10 Si3 Li11 137.80(8) 7_655 51 Li7 Si3 Li11 98.94(5) . 51 Li11 Si3 Li11 102.90(15) 84 51 Li9 Si3 Li11 61.13(8) 6 50_554 Li9 Si3 Li11 127.81(7) 5 50_554 Li4 Si3 Li11 107.71(10) 27_645 50_554 Li4 Si3 Li11 55.74(10) 26_654 50_554 Li3 Si3 Li11 111.40(10) 28 50_554 Li3 Si3 Li11 55.70(7) 25_544 50_554 Li10 Si3 Li11 137.80(8) 8_655 50_554 Li10 Si3 Li11 55.13(7) 7_655 50_554 Li7 Si3 Li11 98.94(5) . 50_554 Li11 Si3 Li11 74.25(16) 84 50_554 Li11 Si3 Li11 162.12(11) 51 50_554 Li12 Si4 Li12 119.3(2) 56 79 Li12 Si4 Li11 79.88(5) 56 5 Li12 Si4 Li11 79.88(5) 79 5 Li12 Si4 Li11 79.88(5) 56 30 Li12 Si4 Li11 79.88(5) 79 30 Li11 Si4 Li11 139.29(18) 5 30 Li12 Si4 Li8 59.64(10) 56 74 Li12 Si4 Li8 59.64(10) 79 74 Li11 Si4 Li8 69.65(9) 5 74 Li11 Si4 Li8 69.65(9) 30 74 Li12 Si4 Li5 113.83(9) 56 4_566 Li12 Si4 Li5 113.83(9) 79 4_566 Li11 Si4 Li5 147.28(16) 5 4_566 Li11 Si4 Li5 73.43(15) 30 4_566 Li8 Si4 Li5 143.08(13) 74 4_566 Li12 Si4 Li5 113.83(9) 56 25_544 Li12 Si4 Li5 113.83(9) 79 25_544 Li11 Si4 Li5 73.43(15) 5 25_544 Li11 Si4 Li5 147.28(16) 30 25_544 Li8 Si4 Li5 143.08(13) 74 25_544 Li5 Si4 Li5 73.8(3) 4_566 25_544 Li12 Si4 Li6 169.71(18) 56 75_646 Li12 Si4 Li6 71.00(17) 79 75_646 Li11 Si4 Li6 103.09(7) 5 75_646 Li11 Si4 Li6 103.09(7) 30 75_646 Li8 Si4 Li6 130.64(14) 74 75_646 Li5 Si4 Li6 58.62(12) 4_566 75_646 Li5 Si4 Li6 58.62(12) 25_544 75_646 Li12 Si4 Li6 71.00(17) 56 50_664 Li12 Si4 Li6 169.71(18) 79 50_664 Li11 Si4 Li6 103.09(7) 5 50_664 Li11 Si4 Li6 103.09(7) 30 50_664 Li8 Si4 Li6 130.64(14) 74 50_664 Li5 Si4 Li6 58.62(12) 4_566 50_664 Li5 Si4 Li6 58.62(12) 25_544 50_664 Li6 Si4 Li6 98.7(3) 75_646 50_664 Li12 Si4 Li10 135.17(8) 56 76_556 Li12 Si4 Li10 54.23(8) 79 76_556 Li11 Si4 Li10 130.73(7) 5 76_556 Li11 Si4 Li10 55.47(8) 30 76_556 Li8 Si4 Li10 97.08(7) 74 76_556 Li5 Si4 Li10 60.72(10) 4_566 76_556 Li5 Si4 Li10 106.99(10) 25_544 76_556 Li6 Si4 Li10 49.53(10) 75_646 76_556 Li6 Si4 Li10 119.25(11) 50_664 76_556 Li12 Si4 Li10 54.23(8) 56 59_565 Li12 Si4 Li10 135.17(8) 79 59_565 Li11 Si4 Li10 130.73(7) 5 59_565 Li11 Si4 Li10 55.47(8) 30 59_565 Li8 Si4 Li10 97.08(7) 74 59_565 Li5 Si4 Li10 60.72(10) 4_566 59_565 Li5 Si4 Li10 106.99(10) 25_544 59_565 Li6 Si4 Li10 119.25(11) 75_646 59_565 Li6 Si4 Li10 49.53(10) 50_664 59_565 Li10 Si4 Li10 97.12(13) 76_556 59_565 Li12 Si4 Li10 135.17(8) 56 81_545 Li12 Si4 Li10 54.22(8) 79 81_545 Li11 Si4 Li10 55.47(8) 5 81_545 Li11 Si4 Li10 130.73(7) 30 81_545 Li8 Si4 Li10 97.08(7) 74 81_545 Li5 Si4 Li10 106.99(10) 4_566 81_545 Li5 Si4 Li10 60.72(10) 25_544 81_545 Li6 Si4 Li10 49.53(10) 75_646 81_545 Li6 Si4 Li10 119.25(11) 50_664 81_545 Li10 Si4 Li10 81.12(14) 76_556 81_545 Li10 Si4 Li10 165.84(14) 59_565 81_545 Li13 Li1 Li7 77.86(16) . 9 Li13 Li1 Li7 77.86(16) . 5 Li7 Li1 Li7 115.70(11) 9 5 Li13 Li1 Li7 77.86(16) . . Li7 Li1 Li7 115.70(11) 9 . Li7 Li1 Li7 115.70(11) 5 . Li13 Li1 Li12 115.42(17) . 9 Li7 Li1 Li12 69.44(6) 9 9 Li7 Li1 Li12 166.7(3) 5 9 Li7 Li1 Li12 69.44(6) . 9 Li13 Li1 Li12 115.42(17) . 5 Li7 Li1 Li12 69.44(6) 9 5 Li7 Li1 Li12 69.44(6) 5 5 Li7 Li1 Li12 166.7(3) . 5 Li12 Li1 Li12 102.9(2) 9 5 Li13 Li1 Li12 115.42(17) . . Li7 Li1 Li12 166.7(3) 9 . Li7 Li1 Li12 69.44(6) 5 . Li7 Li1 Li12 69.44(6) . . Li12 Li1 Li12 102.9(2) 9 . Li12 Li1 Li12 102.9(2) 5 . Li13 Li1 Si1 180.0(5) . . Li7 Li1 Si1 102.14(16) 9 . Li7 Li1 Si1 102.14(16) 5 . Li7 Li1 Si1 102.14(16) . . Li12 Li1 Si1 64.58(17) 9 . Li12 Li1 Si1 64.58(17) 5 . Li12 Li1 Si1 64.58(17) . . Li13 Li1 Si2 59.90(13) . 2_664 Li7 Li1 Si2 137.8(3) 9 2_664 Li7 Li1 Si2 58.11(7) 5 2_664 Li7 Li1 Si2 58.11(7) . 2_664 Li12 Li1 Si2 127.30(4) 9 2_664 Li12 Li1 Si2 127.30(4) 5 2_664 Li12 Li1 Si2 55.53(10) . 2_664 Si1 Li1 Si2 120.10(13) . 2_664 Li13 Li1 Si2 59.90(13) . 4_466 Li7 Li1 Si2 58.11(7) 9 4_466 Li7 Li1 Si2 58.11(7) 5 4_466 Li7 Li1 Si2 137.8(3) . 4_466 Li12 Li1 Si2 127.30(4) 9 4_466 Li12 Li1 Si2 55.53(10) 5 4_466 Li12 Li1 Si2 127.30(4) . 4_466 Si1 Li1 Si2 120.10(13) . 4_466 Si2 Li1 Si2 97.05(17) 2_664 4_466 Li13 Li1 Si2 59.90(13) . 3_646 Li7 Li1 Si2 58.11(7) 9 3_646 Li7 Li1 Si2 137.8(3) 5 3_646 Li7 Li1 Si2 58.11(7) . 3_646 Li12 Li1 Si2 55.53(10) 9 3_646 Li12 Li1 Si2 127.30(4) 5 3_646 Li12 Li1 Si2 127.30(4) . 3_646 Si1 Li1 Si2 120.10(13) . 3_646 Si2 Li1 Si2 97.05(17) 2_664 3_646 Si2 Li1 Si2 97.05(17) 4_466 3_646 Li8 Li2 Li8 119.59(3) 58 30 Li8 Li2 Li8 119.59(3) 58 74 Li8 Li2 Li8 119.59(3) 30 74 Li8 Li2 Li2 109.90(11) 58 28 Li8 Li2 Li2 109.90(11) 30 28 Li8 Li2 Li2 58.41(13) 74 28 Li8 Li2 Li2 58.41(13) 58 74 Li8 Li2 Li2 109.90(11) 30 74 Li8 Li2 Li2 109.90(11) 74 74 Li2 Li2 Li2 60.0 28 74 Li8 Li2 Li2 109.90(11) 58 51 Li8 Li2 Li2 58.41(13) 30 51 Li8 Li2 Li2 109.90(11) 74 51 Li2 Li2 Li2 60.0 28 51 Li2 Li2 Li2 60.0 74 51 Li8 Li2 Si1 168.5(2) 58 74 Li8 Li2 Si1 62.29(3) 30 74 Li8 Li2 Si1 62.29(3) 74 74 Li2 Li2 Si1 60.53(8) 28 74 Li2 Li2 Si1 110.12(10) 74 74 Li2 Li2 Si1 60.53(8) 51 74 Li8 Li2 Si1 62.29(3) 58 28 Li8 Li2 Si1 62.29(3) 30 28 Li8 Li2 Si1 168.5(2) 74 28 Li2 Li2 Si1 110.12(10) 28 28 Li2 Li2 Si1 60.53(8) 74 28 Li2 Li2 Si1 60.53(8) 51 28 Si1 Li2 Si1 113.43(8) 74 28 Li8 Li2 Si1 62.29(3) 58 51 Li8 Li2 Si1 168.5(2) 30 51 Li8 Li2 Si1 62.29(3) 74 51 Li2 Li2 Si1 60.53(8) 28 51 Li2 Li2 Si1 60.53(8) 74 51 Li2 Li2 Si1 110.12(10) 51 51 Si1 Li2 Si1 113.43(8) 74 51 Si1 Li2 Si1 113.43(8) 28 51 Li8 Li2 Li9 64.69(7) 58 58 Li8 Li2 Li9 137.2(2) 30 58 Li8 Li2 Li9 64.69(7) 74 58 Li2 Li2 Li9 106.93(9) 28 58 Li2 Li2 Li9 106.93(9) 74 58 Li2 Li2 Li9 164.38(10) 51 58 Si1 Li2 Li9 122.63(7) 74 58 Si1 Li2 Li9 122.63(7) 28 58 Si1 Li2 Li9 54.26(8) 51 58 Li8 Li2 Li9 137.2(2) 58 74 Li8 Li2 Li9 64.69(7) 30 74 Li8 Li2 Li9 64.69(7) 74 74 Li2 Li2 Li9 106.93(9) 28 74 Li2 Li2 Li9 164.38(10) 74 74 Li2 Li2 Li9 106.93(9) 51 74 Si1 Li2 Li9 54.26(8) 74 74 Si1 Li2 Li9 122.63(7) 28 74 Si1 Li2 Li9 122.63(7) 51 74 Li9 Li2 Li9 84.43(15) 58 74 Li8 Li2 Li9 64.69(7) 58 30 Li8 Li2 Li9 64.69(7) 30 30 Li8 Li2 Li9 137.2(2) 74 30 Li2 Li2 Li9 164.38(10) 28 30 Li2 Li2 Li9 106.93(9) 74 30 Li2 Li2 Li9 106.93(9) 51 30 Si1 Li2 Li9 122.63(7) 74 30 Si1 Li2 Li9 54.26(8) 28 30 Si1 Li2 Li9 122.63(7) 51 30 Li9 Li2 Li9 84.43(15) 58 30 Li9 Li2 Li9 84.43(15) 74 30 Li4 Li3 Li4 68.5(2) 4_566 3_656 Li4 Li3 Li4 68.5(2) 4_566 2_665 Li4 Li3 Li4 68.5(2) 3_656 2_665 Li4 Li3 Li11 116.64(15) 4_566 58 Li4 Li3 Li11 59.17(16) 3_656 58 Li4 Li3 Li11 116.64(15) 2_665 58 Li4 Li3 Li11 59.17(16) 4_566 30 Li4 Li3 Li11 116.64(15) 3_656 30 Li4 Li3 Li11 116.64(15) 2_665 30 Li11 Li3 Li11 117.22(10) 58 30 Li4 Li3 Li11 116.64(15) 4_566 74 Li4 Li3 Li11 116.64(15) 3_656 74 Li4 Li3 Li11 59.17(16) 2_665 74 Li11 Li3 Li11 117.22(10) 58 74 Li11 Li3 Li11 117.22(10) 30 74 Li4 Li3 Si3 59.29(9) 4_566 81 Li4 Li3 Si3 59.29(9) 3_656 81 Li4 Li3 Si3 115.5(2) 2_665 81 Li11 Li3 Si3 64.38(3) 58 81 Li11 Li3 Si3 64.38(3) 30 81 Li11 Li3 Si3 174.7(3) 74 81 Li4 Li3 Si3 59.29(9) 4_566 53 Li4 Li3 Si3 115.5(2) 3_656 53 Li4 Li3 Si3 59.29(9) 2_665 53 Li11 Li3 Si3 174.7(3) 58 53 Li11 Li3 Si3 64.38(3) 30 53 Li11 Li3 Si3 64.38(3) 74 53 Si3 Li3 Si3 113.54(11) 81 53 Li4 Li3 Si3 115.5(2) 4_566 25 Li4 Li3 Si3 59.29(9) 3_656 25 Li4 Li3 Si3 59.29(9) 2_665 25 Li11 Li3 Si3 64.38(3) 58 25 Li11 Li3 Si3 174.7(3) 30 25 Li11 Li3 Si3 64.38(3) 74 25 Si3 Li3 Si3 113.54(11) 81 25 Si3 Li3 Si3 113.54(11) 53 25 Li4 Li3 Li9 103.86(11) 4_566 74 Li4 Li3 Li9 103.86(11) 3_656 74 Li4 Li3 Li9 170.5(2) 2_665 74 Li11 Li3 Li9 60.93(10) 58 74 Li11 Li3 Li9 60.93(10) 30 74 Li11 Li3 Li9 130.3(3) 74 74 Si3 Li3 Li9 55.01(8) 81 74 Si3 Li3 Li9 122.44(10) 53 74 Si3 Li3 Li9 122.44(10) 25 74 Li4 Li3 Li9 103.86(11) 4_566 58 Li4 Li3 Li9 170.5(2) 3_656 58 Li4 Li3 Li9 103.86(11) 2_665 58 Li11 Li3 Li9 130.3(3) 58 58 Li11 Li3 Li9 60.93(10) 30 58 Li11 Li3 Li9 60.93(10) 74 58 Si3 Li3 Li9 122.44(10) 81 58 Si3 Li3 Li9 55.01(8) 53 58 Si3 Li3 Li9 122.44(10) 25 58 Li9 Li3 Li9 83.1(2) 74 58 Li4 Li3 Li9 170.5(2) 4_566 30 Li4 Li3 Li9 103.86(11) 3_656 30 Li4 Li3 Li9 103.86(11) 2_665 30 Li11 Li3 Li9 60.93(10) 58 30 Li11 Li3 Li9 130.3(3) 30 30 Li11 Li3 Li9 60.93(10) 74 30 Si3 Li3 Li9 122.44(10) 81 30 Si3 Li3 Li9 122.44(10) 53 30 Si3 Li3 Li9 55.01(8) 25 30 Li9 Li3 Li9 83.1(2) 74 30 Li9 Li3 Li9 83.1(2) 58 30 Li11 Li4 Li11 83.86(18) 57 29 Li11 Li4 Li11 83.86(18) 57 73 Li11 Li4 Li11 83.86(18) 29 73 Li11 Li4 Li3 126.06(7) 57 4_566 Li11 Li4 Li3 60.57(12) 29 4_566 Li11 Li4 Li3 126.06(7) 73 4_566 Li11 Li4 Li3 126.06(7) 57 2_665 Li11 Li4 Li3 126.06(7) 29 2_665 Li11 Li4 Li3 60.57(12) 73 2_665 Li3 Li4 Li3 107.83(14) 4_566 2_665 Li11 Li4 Li3 60.57(12) 57 3_656 Li11 Li4 Li3 126.06(7) 29 3_656 Li11 Li4 Li3 126.06(7) 73 3_656 Li3 Li4 Li3 107.83(14) 4_566 3_656 Li3 Li4 Li3 107.83(14) 2_665 3_656 Li11 Li4 Si3 66.21(6) 57 26_655 Li11 Li4 Si3 138.9(2) 29 26_655 Li11 Li4 Si3 66.21(6) 73 26_655 Li3 Li4 Si3 160.5(2) 4_566 26_655 Li3 Li4 Si3 62.84(4) 2_665 26_655 Li3 Li4 Si3 62.84(4) 3_656 26_655 Li11 Li4 Si3 138.9(2) 57 54_565 Li11 Li4 Si3 66.21(6) 29 54_565 Li11 Li4 Si3 66.21(6) 73 54_565 Li3 Li4 Si3 62.84(4) 4_566 54_565 Li3 Li4 Si3 62.84(4) 2_665 54_565 Li3 Li4 Si3 160.5(2) 3_656 54_565 Si3 Li4 Si3 119.923(12) 26_655 54_565 Li11 Li4 Si3 66.21(6) 57 82_556 Li11 Li4 Si3 66.21(6) 29 82_556 Li11 Li4 Si3 138.9(2) 73 82_556 Li3 Li4 Si3 62.84(4) 4_566 82_556 Li3 Li4 Si3 160.5(2) 2_665 82_556 Li3 Li4 Si3 62.84(4) 3_656 82_556 Si3 Li4 Si3 119.923(12) 26_655 82_556 Si3 Li4 Si3 119.923(12) 54_565 82_556 Li11 Li4 Li4 107.26(11) 57 2_665 Li11 Li4 Li4 107.26(11) 29 2_665 Li11 Li4 Li4 164.77(12) 73 2_665 Li3 Li4 Li4 55.75(10) 4_566 2_665 Li3 Li4 Li4 104.20(13) 2_665 2_665 Li3 Li4 Li4 55.75(10) 3_656 2_665 Si3 Li4 Li4 108.13(10) 26_655 2_665 Si3 Li4 Li4 108.13(10) 54_565 2_665 Si3 Li4 Li4 56.33(12) 82_556 2_665 Li11 Li4 Li4 107.26(10) 57 4_566 Li11 Li4 Li4 164.77(12) 29 4_566 Li11 Li4 Li4 107.26(10) 73 4_566 Li3 Li4 Li4 104.20(13) 4_566 4_566 Li3 Li4 Li4 55.75(10) 2_665 4_566 Li3 Li4 Li4 55.75(10) 3_656 4_566 Si3 Li4 Li4 56.33(12) 26_655 4_566 Si3 Li4 Li4 108.13(10) 54_565 4_566 Si3 Li4 Li4 108.13(10) 82_556 4_566 Li4 Li4 Li4 60.0 2_665 4_566 Li11 Li4 Li4 164.77(12) 57 3_656 Li11 Li4 Li4 107.26(10) 29 3_656 Li11 Li4 Li4 107.26(10) 73 3_656 Li3 Li4 Li4 55.75(10) 4_566 3_656 Li3 Li4 Li4 55.75(10) 2_665 3_656 Li3 Li4 Li4 104.20(13) 3_656 3_656 Si3 Li4 Li4 108.13(10) 26_655 3_656 Si3 Li4 Li4 56.33(12) 54_565 3_656 Si3 Li4 Li4 108.13(10) 82_556 3_656 Li4 Li4 Li4 60.0 2_665 3_656 Li4 Li4 Li4 60.0 4_566 3_656 Li6 Li5 Li6 103.70(17) 28_566 51_656 Li6 Li5 Li6 103.70(17) 28_566 74_665 Li6 Li5 Li6 103.70(17) 51_656 74_665 Li6 Li5 Si4 153.6(3) 28_566 25 Li6 Li5 Si4 62.23(4) 51_656 25 Li6 Li5 Si4 62.23(4) 74_665 25 Li6 Li5 Si4 62.23(4) 28_566 53 Li6 Li5 Si4 153.6(3) 51_656 53 Li6 Li5 Si4 62.23(4) 74_665 53 Si4 Li5 Si4 119.917(12) 25 53 Li6 Li5 Si4 62.23(4) 28_566 81 Li6 Li5 Si4 62.23(4) 51_656 81 Li6 Li5 Si4 153.6(3) 74_665 81 Si4 Li5 Si4 119.917(12) 25 81 Si4 Li5 Si4 119.917(12) 53 81 Li6 Li5 Li10 126.41(3) 28_566 57 Li6 Li5 Li10 51.36(13) 51_656 57 Li6 Li5 Li10 126.41(3) 74_665 57 Si4 Li5 Li10 64.28(4) 25 57 Si4 Li5 Li10 155.1(2) 53 57 Si4 Li5 Li10 64.28(4) 81 57 Li6 Li5 Li10 51.36(13) 28_566 29 Li6 Li5 Li10 126.41(3) 51_656 29 Li6 Li5 Li10 126.41(3) 74_665 29 Si4 Li5 Li10 155.1(2) 25 29 Si4 Li5 Li10 64.28(4) 53 29 Si4 Li5 Li10 64.28(4) 81 29 Li10 Li5 Li10 101.50(16) 57 29 Li6 Li5 Li10 126.41(3) 28_566 73 Li6 Li5 Li10 126.41(3) 51_656 73 Li6 Li5 Li10 51.36(13) 74_665 73 Si4 Li5 Li10 64.28(4) 25 73 Si4 Li5 Li10 64.28(4) 53 73 Si4 Li5 Li10 155.1(2) 81 73 Li10 Li5 Li10 101.50(16) 57 73 Li10 Li5 Li10 101.50(16) 29 73 Li6 Li5 Li11 92.20(10) 28_566 57 Li6 Li5 Li11 153.9(2) 51_656 57 Li6 Li5 Li11 92.20(10) 74_665 57 Si4 Li5 Li11 109.75(13) 25 57 Si4 Li5 Li11 52.53(9) 53 57 Si4 Li5 Li11 109.75(13) 81 57 Li10 Li5 Li11 102.5(2) 57 57 Li10 Li5 Li11 50.99(9) 29 57 Li10 Li5 Li11 50.99(9) 73 57 Li6 Li5 Li11 153.9(2) 28_566 29 Li6 Li5 Li11 92.20(10) 51_656 29 Li6 Li5 Li11 92.20(10) 74_665 29 Si4 Li5 Li11 52.53(9) 25 29 Si4 Li5 Li11 109.75(13) 53 29 Si4 Li5 Li11 109.75(13) 81 29 Li10 Li5 Li11 50.99(9) 57 29 Li10 Li5 Li11 102.5(2) 29 29 Li10 Li5 Li11 50.99(9) 73 29 Li11 Li5 Li11 66.25(16) 57 29 Li6 Li5 Li11 92.20(10) 28_566 73 Li6 Li5 Li11 92.20(10) 51_656 73 Li6 Li5 Li11 153.9(2) 74_665 73 Si4 Li5 Li11 109.75(13) 25 73 Si4 Li5 Li11 109.75(13) 53 73 Si4 Li5 Li11 52.53(9) 81 73 Li10 Li5 Li11 50.99(9) 57 73 Li10 Li5 Li11 50.99(9) 29 73 Li10 Li5 Li11 102.5(2) 73 73 Li11 Li5 Li11 66.25(16) 57 73 Li11 Li5 Li11 66.25(16) 29 73 Li10 Li6 Li10 106.1(2) 10_656 6_566 Li10 Li6 Li10 106.1(2) 10_656 2_665 Li10 Li6 Li10 106.1(2) 6_566 2_665 Li10 Li6 Li5 126.69(13) 10_656 28_566 Li10 Li6 Li5 68.38(17) 6_566 28_566 Li10 Li6 Li5 126.69(13) 2_665 28_566 Li10 Li6 Li5 68.38(17) 10_656 51_656 Li10 Li6 Li5 126.69(13) 6_566 51_656 Li10 Li6 Li5 126.69(13) 2_665 51_656 Li5 Li6 Li5 74.3(2) 28_566 51_656 Li10 Li6 Li5 126.69(13) 10_656 74_665 Li10 Li6 Li5 126.69(13) 6_566 74_665 Li10 Li6 Li5 68.38(17) 2_665 74_665 Li5 Li6 Li5 74.3(2) 28_566 74_665 Li5 Li6 Li5 74.3(2) 51_656 74_665 Li10 Li6 Si2 67.38(19) 10_656 . Li10 Li6 Si2 67.38(19) 6_566 . Li10 Li6 Si2 67.38(19) 2_665 . Li5 Li6 Si2 135.76(15) 28_566 . Li5 Li6 Si2 135.76(15) 51_656 . Li5 Li6 Si2 135.76(15) 74_665 . Li10 Li6 Si4 69.27(4) 10_656 34_656 Li10 Li6 Si4 69.27(4) 6_566 34_656 Li10 Li6 Si4 171.5(3) 2_665 34_656 Li5 Li6 Si4 59.15(8) 28_566 34_656 Li5 Li6 Si4 59.15(8) 51_656 34_656 Li5 Li6 Si4 120.1(3) 74_665 34_656 Si2 Li6 Si4 104.09(14) . 34_656 Li10 Li6 Si4 171.5(3) 10_656 78_566 Li10 Li6 Si4 69.27(4) 6_566 78_566 Li10 Li6 Si4 69.27(4) 2_665 78_566 Li5 Li6 Si4 59.15(8) 28_566 78_566 Li5 Li6 Si4 120.1(3) 51_656 78_566 Li5 Li6 Si4 59.15(8) 74_665 78_566 Si2 Li6 Si4 104.09(14) . 78_566 Si4 Li6 Si4 114.27(11) 34_656 78_566 Li10 Li6 Si4 69.27(4) 10_656 50_665 Li10 Li6 Si4 171.5(3) 6_566 50_665 Li10 Li6 Si4 69.27(4) 2_665 50_665 Li5 Li6 Si4 120.1(3) 28_566 50_665 Li5 Li6 Si4 59.15(8) 51_656 50_665 Li5 Li6 Si4 59.15(8) 74_665 50_665 Si2 Li6 Si4 104.09(14) . 50_665 Si4 Li6 Si4 114.27(11) 34_656 50_665 Si4 Li6 Si4 114.27(11) 78_566 50_665 Li10 Li6 Li12 119.6(3) 10_656 10_666 Li10 Li6 Li12 53.10(10) 6_566 10_666 Li10 Li6 Li12 53.10(10) 2_665 10_666 Li5 Li6 Li12 99.37(9) 28_566 10_666 Li5 Li6 Li12 172.0(2) 51_656 10_666 Li5 Li6 Li12 99.37(9) 74_665 10_666 Si2 Li6 Li12 52.26(11) . 10_666 Si4 Li6 Li12 122.17(9) 34_656 10_666 Si4 Li6 Li12 51.83(7) 78_566 10_666 Si4 Li6 Li12 122.17(9) 50_665 10_666 Li10 Li6 Li12 53.10(10) 10_656 2_666 Li10 Li6 Li12 53.10(10) 6_566 2_666 Li10 Li6 Li12 119.6(3) 2_665 2_666 Li5 Li6 Li12 99.37(9) 28_566 2_666 Li5 Li6 Li12 99.37(9) 51_656 2_666 Li5 Li6 Li12 172.0(2) 74_665 2_666 Si2 Li6 Li12 52.26(11) . 2_666 Si4 Li6 Li12 51.83(7) 34_656 2_666 Si4 Li6 Li12 122.17(9) 78_566 2_666 Si4 Li6 Li12 122.17(9) 50_665 2_666 Li12 Li6 Li12 86.44(16) 10_666 2_666 Li1 Li7 Li1 94.8(3) 4 . Li1 Li7 Li10 109.07(10) 4 8_655 Li1 Li7 Li10 109.07(10) . 8_655 Li1 Li7 Li10 109.07(10) 4 7_655 Li1 Li7 Li10 109.07(10) . 7_655 Li10 Li7 Li10 122.3(3) 8_655 7_655 Li1 Li7 Si2 66.61(11) 4 3_646 Li1 Li7 Si2 66.61(11) . 3_646 Li10 Li7 Si2 172.9(2) 8_655 3_646 Li10 Li7 Si2 64.77(8) 7_655 3_646 Li1 Li7 Si2 66.61(11) 4 2_664 Li1 Li7 Si2 66.61(11) . 2_664 Li10 Li7 Si2 64.77(8) 8_655 2_664 Li10 Li7 Si2 172.9(2) 7_655 2_664 Si2 Li7 Si2 108.2(2) 3_646 2_664 Li1 Li7 Si3 132.60(16) 4 . Li1 Li7 Si3 132.60(16) . . Li10 Li7 Si3 61.15(14) 8_655 . Li10 Li7 Si3 61.15(14) 7_655 . Si2 Li7 Si3 125.91(10) 3_646 . Si2 Li7 Si3 125.91(10) 2_664 . Li1 Li7 Li9 173.1(2) 4 5 Li1 Li7 Li9 78.28(17) . 5 Li10 Li7 Li9 73.65(11) 8_655 5 Li10 Li7 Li9 73.65(11) 7_655 5 Si2 Li7 Li9 110.01(4) 3_646 5 Si2 Li7 Li9 110.01(4) 2_664 5 Si3 Li7 Li9 54.32(12) . 5 Li1 Li7 Li9 78.28(17) 4 6 Li1 Li7 Li9 173.1(2) . 6 Li10 Li7 Li9 73.65(11) 8_655 6 Li10 Li7 Li9 73.65(11) 7_655 6 Si2 Li7 Li9 110.01(4) 3_646 6 Si2 Li7 Li9 110.01(4) 2_664 6 Si3 Li7 Li9 54.32(12) . 6 Li9 Li7 Li9 108.6(2) 5 6 Li1 Li7 Li12 56.90(13) 4 11 Li1 Li7 Li12 120.30(15) . 11 Li10 Li7 Li12 53.27(8) 8_655 11 Li10 Li7 Li12 128.88(13) 7_655 11 Si2 Li7 Li12 123.28(14) 3_646 11 Si2 Li7 Li12 54.21(8) 2_664 11 Si3 Li7 Li12 91.76(11) . 11 Li9 Li7 Li12 126.70(14) 5 11 Li9 Li7 Li12 55.82(8) 6 11 Li1 Li7 Li12 120.30(15) 4 9 Li1 Li7 Li12 56.90(13) . 9 Li10 Li7 Li12 128.88(13) 8_655 9 Li10 Li7 Li12 53.27(8) 7_655 9 Si2 Li7 Li12 54.21(8) 3_646 9 Si2 Li7 Li12 123.28(14) 2_664 9 Si3 Li7 Li12 91.76(11) . 9 Li9 Li7 Li12 55.82(8) 5 9 Li9 Li7 Li12 126.70(14) 6 9 Li12 Li7 Li12 176.5(2) 11 9 Li1 Li7 Li12 56.90(13) 4 4 Li1 Li7 Li12 120.30(15) . 4 Li10 Li7 Li12 128.88(13) 8_655 4 Li10 Li7 Li12 53.27(8) 7_655 4 Si2 Li7 Li12 54.21(8) 3_646 4 Si2 Li7 Li12 123.28(14) 2_664 4 Si3 Li7 Li12 91.76(11) . 4 Li9 Li7 Li12 126.70(14) 5 4 Li9 Li7 Li12 55.82(8) 6 4 Li12 Li7 Li12 88.82(19) 11 4 Li12 Li7 Li12 91.07(19) 9 4 Li12 Li8 Li12 118.2(3) 5 30 Li12 Li8 Li2 115.95(11) 5 51 Li12 Li8 Li2 115.95(11) 30 51 Li12 Li8 Li2 115.95(11) 5 74 Li12 Li8 Li2 115.95(11) 30 74 Li2 Li8 Li2 63.2(3) 51 74 Li12 Li8 Si4 59.09(14) 5 74 Li12 Li8 Si4 59.09(14) 30 74 Li2 Li8 Si4 148.40(13) 51 74 Li2 Li8 Si4 148.40(13) 74 74 Li12 Li8 Si1 64.57(9) 5 . Li12 Li8 Si1 177.3(2) 30 . Li2 Li8 Si1 61.83(11) 51 . Li2 Li8 Si1 61.83(11) 74 . Si4 Li8 Si1 123.66(10) 74 . Li12 Li8 Si1 177.3(2) 5 28 Li12 Li8 Si1 64.57(9) 30 28 Li2 Li8 Si1 61.83(11) 51 28 Li2 Li8 Si1 61.83(11) 74 28 Si4 Li8 Si1 123.66(10) 74 28 Si1 Li8 Si1 112.7(2) . 28 Li12 Li8 Li9 127.73(11) 5 28 Li12 Li8 Li9 59.64(9) 30 28 Li2 Li8 Li9 61.18(13) 51 28 Li2 Li8 Li9 107.80(18) 74 28 Si4 Li8 Li9 95.94(13) 74 28 Si1 Li8 Li9 118.99(16) . 28 Si1 Li8 Li9 53.17(7) 28 28 Li12 Li8 Li9 127.73(11) 5 35 Li12 Li8 Li9 59.64(9) 30 35 Li2 Li8 Li9 107.80(18) 51 35 Li2 Li8 Li9 61.18(13) 74 35 Si4 Li8 Li9 95.94(13) 74 35 Si1 Li8 Li9 118.99(16) . 35 Si1 Li8 Li9 53.17(7) 28 35 Li9 Li8 Li9 97.49(15) 28 35 Li12 Li8 Li9 59.64(9) 5 9 Li12 Li8 Li9 127.73(11) 30 9 Li2 Li8 Li9 61.18(13) 51 9 Li2 Li8 Li9 107.80(18) 74 9 Si4 Li8 Li9 95.94(13) 74 9 Si1 Li8 Li9 53.17(7) . 9 Si1 Li8 Li9 118.99(16) 28 9 Li9 Li8 Li9 81.27(16) 28 9 Li9 Li8 Li9 168.1(3) 35 9 Li12 Li8 Li9 59.63(9) 5 . Li12 Li8 Li9 127.73(11) 30 . Li2 Li8 Li9 107.80(18) 51 . Li2 Li8 Li9 61.18(13) 74 . Si4 Li8 Li9 95.94(13) 74 . Si1 Li8 Li9 53.17(7) . . Si1 Li8 Li9 118.99(16) 28 . Li9 Li8 Li9 168.1(3) 28 . Li9 Li8 Li9 81.27(16) 35 . Li9 Li8 Li9 97.49(15) 9 . Li12 Li8 Li11 72.85(11) 5 56 Li12 Li8 Li11 72.85(11) 30 56 Li2 Li8 Li11 156.6(2) 51 56 Li2 Li8 Li11 93.44(13) 74 56 Si4 Li8 Li11 54.96(11) 74 56 Si1 Li8 Li11 108.55(3) . 56 Si1 Li8 Li11 108.55(3) 28 56 Li9 Li8 Li11 132.46(16) 28 56 Li9 Li8 Li11 56.21(7) 35 56 Li9 Li8 Li11 132.46(16) 9 56 Li9 Li8 Li11 56.21(7) . 56 Si1 Li9 Si3 158.39(19) . 9 Si1 Li9 Li12 65.68(12) . 9 Si3 Li9 Li12 101.32(13) 9 9 Si1 Li9 Li12 65.68(12) . 5 Si3 Li9 Li12 101.32(13) 9 5 Li12 Li9 Li12 98.5(2) 9 5 Si1 Li9 Li11 123.50(11) . 35 Si3 Li9 Li11 64.34(10) 9 35 Li12 Li9 Li11 74.20(9) 9 35 Li12 Li9 Li11 161.32(19) 5 35 Si1 Li9 Li11 123.50(11) . 56 Si3 Li9 Li11 64.34(10) 9 56 Li12 Li9 Li11 161.32(19) 9 56 Li12 Li9 Li11 74.20(9) 5 56 Li11 Li9 Li11 107.21(18) 35 56 Si1 Li9 Li2 62.03(12) . 74 Si3 Li9 Li2 139.59(17) 9 74 Li12 Li9 Li2 104.73(12) 9 74 Li12 Li9 Li2 104.73(12) 5 74 Li11 Li9 Li2 93.82(14) 35 74 Li11 Li9 Li2 93.82(14) 56 74 Si1 Li9 Li3 141.1(2) . 74 Si3 Li9 Li3 60.48(12) 9 74 Li12 Li9 Li3 129.68(10) 9 74 Li12 Li9 Li3 129.68(10) 5 74 Li11 Li9 Li3 55.50(9) 35 74 Li11 Li9 Li3 55.50(9) 56 74 Li2 Li9 Li3 79.11(17) 74 74 Si1 Li9 Li7 97.92(16) . 9 Si3 Li9 Li7 60.47(12) 9 9 Li12 Li9 Li7 63.58(12) 9 9 Li12 Li9 Li7 63.58(12) 5 9 Li11 Li9 Li7 98.02(13) 35 9 Li11 Li9 Li7 98.02(13) 56 9 Li2 Li9 Li7 159.94(18) 74 9 Li3 Li9 Li7 120.95(18) 74 9 Si1 Li9 Li8 61.00(9) . . Si3 Li9 Li8 126.88(11) 9 . Li12 Li9 Li8 126.36(17) 9 . Li12 Li9 Li8 54.49(9) 5 . Li11 Li9 Li8 143.4(2) 35 . Li11 Li9 Li8 63.61(11) 56 . Li2 Li9 Li8 54.13(13) 74 . Li3 Li9 Li8 97.04(13) 74 . Li7 Li9 Li8 117.96(15) 9 . Si1 Li9 Li8 61.00(9) . 5 Si3 Li9 Li8 126.88(11) 9 5 Li12 Li9 Li8 54.49(9) 9 5 Li12 Li9 Li8 126.36(17) 5 5 Li11 Li9 Li8 63.61(11) 35 5 Li11 Li9 Li8 143.4(2) 56 5 Li2 Li9 Li8 54.13(13) 74 5 Li3 Li9 Li8 97.04(13) 74 5 Li7 Li9 Li8 117.96(15) 9 5 Li8 Li9 Li8 101.6(3) . 5 Si1 Li9 Li10 113.43(11) . 4_556 Si3 Li9 Li10 53.85(9) 9 4_556 Li12 Li9 Li10 48.21(10) 9 4_556 Li12 Li9 Li10 112.83(15) 5 4_556 Li11 Li9 Li10 49.49(8) 35 4_556 Li11 Li9 Li10 118.09(16) 56 4_556 Li2 Li9 Li10 135.61(9) 74 4_556 Li3 Li9 Li10 93.76(12) 74 4_556 Li7 Li9 Li10 49.68(9) 9 4_556 Li8 Li9 Li10 167.08(17) . 4_556 Li8 Li9 Li10 84.05(12) 5 4_556 Li6 Li10 Li12 77.93(14) 2_665 11_556 Li6 Li10 Li12 77.93(14) 2_665 8_556 Li12 Li10 Li12 113.7(2) 11_556 8_556 Li6 Li10 Li11 114.86(19) 2_665 33_545 Li12 Li10 Li11 81.00(11) 11_556 33_545 Li12 Li10 Li11 163.00(17) 8_556 33_545 Li6 Li10 Li11 114.86(19) 2_665 53_455 Li12 Li10 Li11 163.00(17) 11_556 53_455 Li12 Li10 Li11 81.00(11) 8_556 53_455 Li11 Li10 Li11 83.3(2) 33_545 53_455 Li6 Li10 Li7 119.0(2) 2_665 10_556 Li12 Li10 Li7 70.12(13) 11_556 10_556 Li12 Li10 Li7 70.12(13) 8_556 10_556 Li11 Li10 Li7 109.65(17) 33_545 10_556 Li11 Li10 Li7 109.65(17) 53_455 10_556 Li6 Li10 Si3 179.2(3) 2_665 10_556 Li12 Li10 Si3 102.49(14) 11_556 10_556 Li12 Li10 Si3 102.49(14) 8_556 10_556 Li11 Li10 Si3 64.58(9) 33_545 10_556 Li11 Li10 Si3 64.58(9) 53_455 10_556 Li7 Li10 Si3 61.80(15) 10_556 10_556 Li6 Li10 Si2 61.37(17) 2_665 2_665 Li12 Li10 Si2 57.08(11) 11_556 2_665 Li12 Li10 Si2 57.08(11) 8_556 2_665 Li11 Li10 Si2 138.05(11) 33_545 2_665 Li11 Li10 Si2 138.05(11) 53_455 2_665 Li7 Li10 Si2 57.66(12) 10_556 2_665 Si3 Li10 Si2 119.45(16) 10_556 2_665 Li6 Li10 Li5 60.3(2) 2_665 73_445 Li12 Li10 Li5 109.56(16) 11_556 73_445 Li12 Li10 Li5 109.56(16) 8_556 73_445 Li11 Li10 Li5 70.86(13) 33_545 73_445 Li11 Li10 Li5 70.86(13) 53_455 73_445 Li7 Li10 Li5 179.3(2) 10_556 73_445 Si3 Li10 Li5 118.92(16) 10_556 73_445 Si2 Li10 Li5 121.63(19) 2_665 73_445 Li6 Li10 Si4 61.21(11) 2_665 49_455 Li12 Li10 Si4 138.85(18) 11_556 49_455 Li12 Li10 Si4 55.58(9) 8_556 49_455 Li11 Li10 Si4 119.17(16) 33_545 49_455 Li11 Li10 Si4 56.04(8) 53_455 49_455 Li7 Li10 Si4 124.80(7) 10_556 49_455 Si3 Li10 Si4 118.43(8) 10_556 49_455 Si2 Li10 Si4 96.17(9) 2_665 49_455 Li5 Li10 Si4 55.00(8) 73_445 49_455 Li6 Li10 Si4 61.21(11) 2_665 29_545 Li12 Li10 Si4 55.58(9) 11_556 29_545 Li12 Li10 Si4 138.85(18) 8_556 29_545 Li11 Li10 Si4 56.04(8) 33_545 29_545 Li11 Li10 Si4 119.17(16) 53_455 29_545 Li7 Li10 Si4 124.80(7) 10_556 29_545 Si3 Li10 Si4 118.43(8) 10_556 29_545 Si2 Li10 Si4 96.17(9) 2_665 29_545 Li5 Li10 Si4 55.00(8) 73_445 29_545 Si4 Li10 Si4 103.83(14) 49_455 29_545 Li6 Li10 Li9 130.96(8) 2_665 3_556 Li12 Li10 Li9 126.6(2) 11_556 3_556 Li12 Li10 Li9 53.92(9) 8_556 3_556 Li11 Li10 Li9 110.97(15) 33_545 3_556 Li11 Li10 Li9 54.41(9) 53_455 3_556 Li7 Li10 Li9 56.66(12) 10_556 3_556 Si3 Li10 Li9 49.33(9) 10_556 3_556 Si2 Li10 Li9 94.69(11) 2_665 3_556 Li5 Li10 Li9 123.71(10) 73_445 3_556 Si4 Li10 Li9 82.02(5) 49_455 3_556 Si4 Li10 Li9 167.01(13) 29_545 3_556 Li4 Li11 Li10 94.23(13) 73_445 33_545 Li4 Li11 Li10 94.23(13) 73_445 53_455 Li10 Li11 Li10 115.7(2) 33_545 53_455 Li4 Li11 Si4 144.42(19) 73_445 9 Li10 Li11 Si4 68.48(10) 33_545 9 Li10 Li11 Si4 68.48(10) 53_455 9 Li4 Li11 Li3 60.3(2) 73_445 74 Li10 Li11 Li3 119.63(11) 33_545 74 Li10 Li11 Li3 119.63(11) 53_455 74 Si4 Li11 Li3 155.3(2) 9 74 Li4 Li11 Li9 106.58(13) 73_445 35 Li10 Li11 Li9 76.10(11) 33_545 35 Li10 Li11 Li9 155.6(2) 53_455 35 Si4 Li11 Li9 99.27(12) 9 35 Li3 Li11 Li9 63.57(13) 74 35 Li4 Li11 Li9 106.58(13) 73_445 56 Li10 Li11 Li9 155.6(2) 33_545 56 Li10 Li11 Li9 76.10(11) 53_455 56 Si4 Li11 Li9 99.27(12) 9 56 Li3 Li11 Li9 63.57(13) 74 56 Li9 Li11 Li9 85.6(2) 35 56 Li4 Li11 Si3 58.04(7) 73_445 30 Li10 Li11 Si3 60.30(10) 33_545 30 Li10 Li11 Si3 149.71(17) 53_455 30 Si4 Li11 Si3 126.19(5) 9 30 Li3 Li11 Si3 59.92(7) 74 30 Li9 Li11 Si3 54.52(8) 35 30 Li9 Li11 Si3 120.72(14) 56 30 Li4 Li11 Si3 58.04(7) 73_445 50 Li10 Li11 Si3 149.71(17) 33_545 50 Li10 Li11 Si3 60.30(9) 53_455 50 Si4 Li11 Si3 126.19(5) 9 50 Li3 Li11 Si3 59.92(7) 74 50 Li9 Li11 Si3 120.72(14) 35 50 Li9 Li11 Si3 54.52(8) 56 50 Si3 Li11 Si3 106.77(10) 30 50 Li4 Li11 Li8 160.19(19) 73_445 58 Li10 Li11 Li8 96.27(11) 33_545 58 Li10 Li11 Li8 96.27(11) 53_455 58 Si4 Li11 Li8 55.39(12) 9 58 Li3 Li11 Li8 99.9(2) 74 58 Li9 Li11 Li8 60.17(12) 35 58 Li9 Li11 Li8 60.17(12) 56 58 Si3 Li11 Li8 113.88(10) 30 58 Si3 Li11 Li8 113.88(10) 50 58 Li4 Li11 Li5 90.38(16) 73_445 73_445 Li10 Li11 Li5 58.15(12) 33_545 73_445 Li10 Li11 Li5 58.15(12) 53_455 73_445 Si4 Li11 Li5 54.04(9) 9 73_445 Li3 Li11 Li5 150.6(2) 74 73_445 Li9 Li11 Li5 132.36(10) 35 73_445 Li9 Li11 Li5 132.36(10) 56 73_445 Si3 Li11 Li5 106.17(10) 30 73_445 Si3 Li11 Li5 106.17(10) 50 73_445 Li8 Li11 Li5 109.43(16) 58 73_445 Li4 Li11 Li12 137.84(7) 73_445 28 Li10 Li11 Li12 48.61(9) 33_545 28 Li10 Li11 Li12 117.85(13) 53_455 28 Si4 Li11 Li12 49.49(8) 9 28 Li3 Li11 Li12 115.94(14) 74 28 Li9 Li11 Li12 52.40(9) 35 28 Li9 Li11 Li12 107.21(17) 56 28 Si3 Li11 Li12 83.08(4) 30 28 Si3 Li11 Li12 161.68(16) 50 28 Li8 Li11 Li12 47.92(9) 58 28 Li5 Li11 Li12 85.11(12) 73_445 28 Li10 Li12 Li10 97.9(2) 11_565 8_655 Li10 Li12 Si2 67.24(13) 11_565 2_664 Li10 Li12 Si2 67.24(13) 8_655 2_664 Li10 Li12 Si4 70.19(14) 11_565 58 Li10 Li12 Si4 70.19(14) 8_655 58 Si2 Li12 Si4 112.85(18) 2_664 58 Li10 Li12 Li8 109.30(16) 11_565 9 Li10 Li12 Li8 109.30(16) 8_655 9 Si2 Li12 Li8 174.1(2) 2_664 9 Si4 Li12 Li8 61.27(14) 58 9 Li10 Li12 Li1 109.2(2) 11_565 . Li10 Li12 Li1 109.2(2) 8_655 . Si2 Li12 Li1 66.10(17) 2_664 . Si4 Li12 Li1 179.0(3) 58 . Li8 Li12 Li1 119.8(3) 9 . Li10 Li12 Li9 77.86(10) 11_565 9 Li10 Li12 Li9 171.5(2) 8_655 9 Si2 Li12 Li9 116.90(10) 2_664 9 Si4 Li12 Li9 101.32(10) 58 9 Li8 Li12 Li9 65.87(11) 9 9 Li1 Li12 Li9 79.29(15) . 9 Li10 Li12 Li9 171.5(2) 11_565 5 Li10 Li12 Li9 77.86(10) 8_655 5 Si2 Li12 Li9 116.90(10) 2_664 5 Si4 Li12 Li9 101.32(10) 58 5 Li8 Li12 Li9 65.87(11) 9 5 Li1 Li12 Li9 79.29(15) . 5 Li9 Li12 Li9 105.3(2) 9 5 Li10 Li12 Si1 131.05(12) 11_565 . Li10 Li12 Si1 131.05(12) 8_655 . Si2 Li12 Si1 124.89(13) 2_664 . Si4 Li12 Si1 122.26(14) 58 . Li8 Li12 Si1 60.98(13) 9 . Li1 Li12 Si1 58.79(16) . . Li9 Li12 Si1 53.85(11) 9 . Li9 Li12 Si1 53.85(11) 5 . Li10 Li12 Li7 56.61(13) 11_565 5 Li10 Li12 Li7 123.25(18) 8_655 5 Si2 Li12 Li7 56.33(9) 2_664 5 Si4 Li12 Li7 125.88(13) 58 5 Li8 Li12 Li7 126.35(13) 9 5 Li1 Li12 Li7 53.67(13) . 5 Li9 Li12 Li7 60.60(12) 9 5 Li9 Li12 Li7 131.89(18) 5 5 Si1 Li12 Li7 89.26(10) . 5 Li10 Li12 Li7 123.25(18) 11_565 . Li10 Li12 Li7 56.61(13) 8_655 . Si2 Li12 Li7 56.33(9) 2_664 . Si4 Li12 Li7 125.88(13) 58 . Li8 Li12 Li7 126.35(13) 9 . Li1 Li12 Li7 53.67(13) . . Li9 Li12 Li7 131.89(18) 9 . Li9 Li12 Li7 60.60(12) 5 . Si1 Li12 Li7 89.26(10) . . Li7 Li12 Li7 93.5(2) 5 . Li10 Li12 Li6 48.97(12) 11_565 2_664 Li10 Li12 Li6 48.97(12) 8_655 2_664 Si2 Li12 Li6 55.69(14) 2_664 2_664 Si4 Li12 Li6 57.16(13) 58 2_664 Li8 Li12 Li6 118.44(19) 9 2_664 Li1 Li12 Li6 121.8(2) . 2_664 Li9 Li12 Li6 126.05(11) 9 2_664 Li9 Li12 Li6 126.05(11) 5 2_664 Si1 Li12 Li6 179.42(16) . 2_664 Li7 Li12 Li6 91.13(13) 5 2_664 Li7 Li12 Li6 91.13(13) . 2_664 Li1 Li13 Li1 109.5 4 3 Li1 Li13 Li1 109.5 4 2 Li1 Li13 Li1 109.5 3 2 Li1 Li13 Li1 109.5 4 . Li1 Li13 Li1 109.471(1) 3 . Li1 Li13 Li1 109.5 2 . Li1 Li13 Si2 70.5 4 1_444 Li1 Li13 Si2 70.5 3 1_444 Li1 Li13 Si2 70.5 2 1_444 Li1 Li13 Si2 180.0(2) . 1_444 Li1 Li13 Si2 70.5 4 2_664 Li1 Li13 Si2 70.5 3 2_664 Li1 Li13 Si2 180.0(2) 2 2_664 Li1 Li13 Si2 70.5 . 2_664 Si2 Li13 Si2 109.5 1_444 2_664 Li1 Li13 Si2 180.0(2) 4 4_466 Li1 Li13 Si2 70.5 3 4_466 Li1 Li13 Si2 70.5 2 4_466 Li1 Li13 Si2 70.5 . 4_466 Si2 Li13 Si2 109.5 1_444 4_466 Si2 Li13 Si2 109.5 2_664 4_466 Li1 Li13 Si2 70.5 4 3_646 Li1 Li13 Si2 180.0(2) 3 3_646 Li1 Li13 Si2 70.5 2 3_646 Li1 Li13 Si2 70.529(1) . 3_646 Si2 Li13 Si2 109.5 1_444 3_646 Si2 Li13 Si2 109.5 2_664 3_646 Si2 Li13 Si2 109.5 4_466 3_646 Li1 Li13 Li7 54.7 4 10 Li1 Li13 Li7 54.7 3 10 Li1 Li13 Li7 125.3 2 10 Li1 Li13 Li7 125.3 . 10 Si2 Li13 Li7 54.7 1_444 10 Si2 Li13 Li7 54.7 2_664 10 Si2 Li13 Li7 125.3 4_466 10 Si2 Li13 Li7 125.3 3_646 10 Li1 Li13 Li7 125.3 4 9 Li1 Li13 Li7 125.3 3 9 Li1 Li13 Li7 54.7 2 9 Li1 Li13 Li7 54.7 . 9 Si2 Li13 Li7 125.3 1_444 9 Si2 Li13 Li7 125.3 2_664 9 Si2 Li13 Li7 54.7 4_466 9 Si2 Li13 Li7 54.7 3_646 9 Li7 Li13 Li7 180.0 10 9 Li1 Li13 Li7 125.3 4 2 Li1 Li13 Li7 54.7 3 2 Li1 Li13 Li7 54.7 2 2 Li1 Li13 Li7 125.3 . 2 Si2 Li13 Li7 54.7 1_444 2 Si2 Li13 Li7 125.3 2_664 2 Si2 Li13 Li7 54.7 4_466 2 Si2 Li13 Li7 125.3 3_646 2 Li7 Li13 Li7 90.0 10 2 Li7 Li13 Li7 90.0 9 2 Li1 Li13 Li7 125.3 4 5 Li1 Li13 Li7 54.7 3 5 Li1 Li13 Li7 125.3 2 5 Li1 Li13 Li7 54.7 . 5 Si2 Li13 Li7 125.3 1_444 5 Si2 Li13 Li7 54.7 2_664 5 Si2 Li13 Li7 54.7 4_466 5 Si2 Li13 Li7 125.3 3_646 5 Li7 Li13 Li7 90.0 10 5 Li7 Li13 Li7 90.0 9 5 Li7 Li13 Li7 90.0 2 5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 Li9 2.628(4) . Si1 Li9 2.628(4) 9 Si1 Li9 2.628(4) 5 Si1 Li1 2.808(8) . Si1 Li2 2.8590(16) 28 Si1 Li2 2.8590(16) 74 Si1 Li2 2.8590(16) 51 Si1 Li8 2.871(3) . Si1 Li8 2.871(3) 5 Si1 Li8 2.871(3) 9 Si1 Li12 2.965(5) 9 Si1 Li12 2.965(5) 5 Si2 Li12 2.655(4) 10_666 Si2 Li12 2.655(4) 6_666 Si2 Li12 2.655(4) 2_666 Si2 Li13 2.7018(9) 1_666 Si2 Li7 2.724(3) 10_666 Si2 Li7 2.724(3) 2_666 Si2 Li7 2.724(3) 6_666 Si2 Li6 2.773(7) . Si2 Li10 2.916(4) 2_665 Si2 Li10 2.916(4) 6_566 Si2 Li10 2.916(4) 10_656 Si2 Li1 2.944(4) 4_666 Si3 Li9 2.668(4) 6 Si3 Li9 2.668(4) 5 Si3 Li4 2.7383(7) 27_645 Si3 Li4 2.7383(7) 26_654 Si3 Li3 2.8340(17) 28 Si3 Li3 2.8340(17) 25_544 Si3 Li10 2.840(4) 8_655 Si3 Li10 2.840(4) 7_655 Si3 Li7 2.858(5) . Si3 Li11 2.953(2) 84 Si3 Li11 2.953(2) 51 Si3 Li11 2.953(2) 50_554 Si4 Li12 2.656(4) 56 Si4 Li12 2.656(4) 79 Si4 Li11 2.701(3) 5 Si4 Li11 2.701(3) 30 Si4 Li8 2.715(6) 74 Si4 Li5 2.7541(7) 4_566 Si4 Li5 2.7541(7) 25_544 Si4 Li6 2.8384(18) 75_646 Si4 Li6 2.8384(18) 50_664 Si4 Li10 3.029(3) 76_556 Si4 Li10 3.029(3) 59_565 Si4 Li10 3.029(3) 81_545 Li1 Li13 2.377(8) . Li1 Li7 2.637(4) 9 Li1 Li7 2.637(4) 5 Li1 Li7 2.637(4) . Li1 Li12 2.742(5) 9 Li1 Li12 2.742(5) 5 Li1 Li12 2.742(5) . Li1 Si2 2.944(4) 2_664 Li1 Si2 2.944(4) 4_466 Li1 Si2 2.944(4) 3_646 Li2 Li8 2.685(5) 58 Li2 Li8 2.685(5) 30 Li2 Li8 2.685(5) 74 Li2 Li2 2.813(8) 28 Li2 Li2 2.813(8) 74 Li2 Li2 2.813(8) 51 Li2 Si1 2.8590(16) 74 Li2 Si1 2.8590(16) 28 Li2 Si1 2.8590(16) 51 Li2 Li9 2.903(5) 58 Li2 Li9 2.903(5) 74 Li2 Li9 2.903(5) 30 Li3 Li4 2.697(6) 4_566 Li3 Li4 2.697(6) 3_656 Li3 Li4 2.697(6) 2_665 Li3 Li11 2.706(3) 58 Li3 Li11 2.706(3) 30 Li3 Li11 2.706(3) 74 Li3 Si3 2.8339(17) 81 Li3 Si3 2.8339(17) 53 Li3 Si3 2.8339(17) 25 Li3 Li9 2.940(5) 74 Li3 Li9 2.940(5) 58 Li3 Li9 2.940(5) 30 Li4 Li11 2.667(5) 57 Li4 Li11 2.667(5) 29 Li4 Li11 2.667(5) 73 Li4 Li3 2.697(6) 4_566 Li4 Li3 2.697(6) 2_665 Li4 Li3 2.697(6) 3_656 Li4 Si3 2.7382(7) 26_655 Li4 Si3 2.7382(7) 54_565 Li4 Si3 2.7382(7) 82_556 Li4 Li4 3.036(9) 2_665 Li4 Li4 3.036(9) 4_566 Li4 Li4 3.036(9) 3_656 Li5 Li6 2.739(6) 28_566 Li5 Li6 2.739(6) 51_656 Li5 Li6 2.739(6) 74_665 Li5 Si4 2.7541(7) 25 Li5 Si4 2.7541(7) 53 Li5 Si4 2.7541(7) 81 Li5 Li10 2.932(6) 57 Li5 Li10 2.932(6) 29 Li5 Li10 2.932(6) 73 Li5 Li11 3.261(6) 57 Li5 Li11 3.261(6) 29 Li5 Li11 3.261(6) 73 Li6 Li10 2.464(5) 10_656 Li6 Li10 2.464(5) 6_566 Li6 Li10 2.464(5) 2_665 Li6 Li5 2.739(6) 28_566 Li6 Li5 2.739(6) 51_656 Li6 Li5 2.739(6) 74_665 Li6 Si4 2.8383(18) 34_656 Li6 Si4 2.8383(18) 78_566 Li6 Si4 2.8383(18) 50_665 Li6 Li12 3.194(6) 10_666 Li6 Li12 3.194(6) 2_666 Li7 Li1 2.637(4) 4 Li7 Li10 2.721(5) 8_655 Li7 Li10 2.721(5) 7_655 Li7 Si2 2.724(3) 3_646 Li7 Si2 2.724(3) 2_664 Li7 Li9 2.982(6) 5 Li7 Li9 2.982(6) 6 Li7 Li12 3.065(2) 11 Li7 Li12 3.065(2) 9 Li7 Li12 3.065(2) 4 Li8 Li12 2.671(4) 5 Li8 Li12 2.671(4) 30 Li8 Li2 2.685(5) 51 Li8 Li2 2.685(5) 74 Li8 Si4 2.715(6) 74 Li8 Si1 2.871(3) 28 Li8 Li9 2.995(3) 28 Li8 Li9 2.995(3) 35 Li8 Li9 2.995(3) 9 Li8 Li9 2.995(3) . Li8 Li11 3.092(5) 56 Li9 Si3 2.668(4) 9 Li9 Li12 2.831(4) 9 Li9 Li12 2.831(4) 5 Li9 Li11 2.869(3) 35 Li9 Li11 2.869(3) 56 Li9 Li2 2.903(5) 74 Li9 Li3 2.940(5) 74 Li9 Li7 2.982(6) 9 Li9 Li8 2.995(3) 5 Li9 Li10 3.425(4) 4_556 Li10 Li6 2.464(5) 2_665 Li10 Li12 2.612(4) 11_556 Li10 Li12 2.612(4) 8_556 Li10 Li11 2.683(3) 33_545 Li10 Li11 2.682(3) 53_455 Li10 Li7 2.721(5) 10_556 Li10 Si3 2.840(4) 10_556 Li10 Si2 2.916(4) 2_665 Li10 Li5 2.932(6) 73_445 Li10 Si4 3.029(3) 49_455 Li10 Si4 3.029(3) 29_545 Li10 Li9 3.425(4) 3_556 Li11 Li4 2.667(5) 73_445 Li11 Li10 2.682(3) 33_545 Li11 Li10 2.682(3) 53_455 Li11 Si4 2.701(3) 9 Li11 Li3 2.706(3) 74 Li11 Li9 2.869(3) 35 Li11 Li9 2.869(3) 56 Li11 Si3 2.953(2) 30 Li11 Si3 2.953(2) 50 Li11 Li8 3.092(5) 58 Li11 Li5 3.261(6) 73_445 Li11 Li12 3.439(3) 28 Li12 Li10 2.612(4) 11_565 Li12 Li10 2.612(4) 8_655 Li12 Si2 2.655(4) 2_664 Li12 Si4 2.656(4) 58 Li12 Li8 2.671(4) 9 Li12 Li9 2.831(4) 9 Li12 Li9 2.831(4) 5 Li12 Li7 3.065(2) 5 Li12 Li6 3.194(6) 2_664 Li13 Li1 2.377(8) 4 Li13 Li1 2.377(8) 3 Li13 Li1 2.377(8) 2 Li13 Si2 2.7018(9) 1_444 Li13 Si2 2.7018(9) 2_664 Li13 Si2 2.7018(9) 4_466 Li13 Si2 2.7018(9) 3_646 Li13 Li7 3.158(5) 10 Li13 Li7 3.158(5) 9 Li13 Li7 3.158(5) 2 Li13 Li7 3.158(5) 5