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Information card for entry 4060112
Preview
| Coordinates | 4060112.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | benzothiagermete |
|---|---|
| Formula | C45 H80 Ge S Si6 |
| Calculated formula | C45 H80 Ge S Si6 |
| Title of publication | Reactions of a Germacyclopropabenzene with Elemental Chalcogens: Syntheses and Structures of a Series of Stable 2H-Benzo[c][1,2]chalcogenagermetes |
| Authors of publication | Sasamori, Takahiro; Sasaki, Takayo; Takeda, Nobuhiro; Tokitoh, Norihiro |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 4 |
| Pages of publication | 612 - 618 |
| a | 10.125 ± 0.003 Å |
| b | 11.941 ± 0.003 Å |
| c | 22.971 ± 0.007 Å |
| α | 76.768 ± 0.011° |
| β | 83.65 ± 0.012° |
| γ | 72.101 ± 0.009° |
| Cell volume | 2570.3 ± 1.3 Å3 |
| Cell temperature | 93 ± 2 K |
| Ambient diffraction temperature | 93 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.065 |
| Residual factor for significantly intense reflections | 0.0522 |
| Weighted residual factors for significantly intense reflections | 0.0959 |
| Weighted residual factors for all reflections included in the refinement | 0.1004 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.115 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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